Document oDvpBgY7pgbxZjmw4g0mm7vrr
MEMBER
AGIL
Sani-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES 178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201)843-2525 FAX (201) 843-4934 E-MAIL sanipure.labs@verlzon.net
Certificate of Laboratory Analysis
PLAINTIFF'S EXHIBIT
CAM-346
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
1/19/05 1/24/05 05,019,c,302 1 of 3
Product Identification Grind Date Ship Name
Luzenac Guangxi #2
1/18/2005
M.V. TAI CHANG
Arrival Date:
ANALYTE
SPECIFICATION
RESULTS
Identification Loss on Ignition (1000 C) Acid-Soluble Substances Reaction and Soluble Substances
Water Soluble Iron Arsenic
Heavy Metals Lead
Microbial Limits Total Bacteria Count
To Pass Test < 6.5% < 2.0% <0.1%
To Pass Test < 3 ppm < 0.004% <0.001%
< 500 per g
Passes Test 6.11% 0.77% 0.034%
Passes Test 0.16 ppm < 40 ppm 1.17 ppm
< 10 per g
Productlon/Asbestos Identification A. IRTest B. C. pH
Loss on Ignition (1075 C) Water Soluble Substances
Iron Aluminum Calcium
Lead Magnesium Microbial Limits Total Bacteria Count Microbial Limits / Fungi Count
To Pass Test
To Pass Test To Pass Test To Pass Test
7.0 to 9.0 < 7.0% < 0.2% < 0.25% < 2.0% < 0.9%
< 10 ppm 17.0%- 19.5%
< 1000 per g < 100 per g
Passes Test
Passes Test Passes Test Passes Test
8.549 6.19% 0.018% 0.064% 0.18% 0.42% 1.17 ppm 17.70%
< 1 0 per g < 10 per g
12/14/04
INTERPRETATION
MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP
MEETS USP
MEETS PhEur
MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur
MEETS PhEur MEETS PhEur
ITA-Ratcliff-000136
MEMBER
Sani-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES
178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201)843-2525 FAX (201) 843-4934 - E-MAIL sanipure.labs@verizon.net
i
Certificate of Laboratory Analysis
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
1/19/05 1/24/05 05,019,c,302 2 of 3
Product Identification Grind Date Ship Name
Luzenac Guangxi #2
1/18/2005
M.V. TAI CHANG
Arrival Date:
ANALYTE
SPECIFICATION
RESULTS
Identification 1 2
Loss on Ignition (450-550 C) Acid or Alkali
Acid Soluble Substances Water Soluble Substances
Iron Sioluble in Water Arsenic
To Pass Test To Pass Test
< 5.0% Neutral < 2.0% < 4.0 mg To Pass Test < 4 ppm
Passes Test Passes Test
4.92% Neutral 0.77% 1.20 mg Passes Test 0.16 ppm
Identification A. B.
Loss on Ignition (800 C) Loss on Drying (105 C) Acid Soluble Substances
Soluble Salts Free Alkali Arsenic Lead
To Pass Test To Pass Test
< 6.0% < 0.5% <; 2.5% < 0.2% < 1.0% < 3 ppm < 5 ppm
Passes Test Passes Test
5.81% 0.16% 0.77% 0.050% < 1.0% 0.16 ppm 1.17 ppm
12/14/04
INTERPRETATION
MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII
MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC
Respectfully submitted,
Ronald A. Schnitzel^"/ Director
ITA-Ratcliff-000137
MEMBER
IL
(
Sani-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES 178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201)843-2525 FAX (201) 843-4934 E-MAIL sanipure.labs@verizon.net
Certificate of Laboratory Analysis
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
1/19/05 1/24/05 05,019,c,302 3 of 3
Product Identification Grind Date Ship Name
ANALYTE
Luzenac Guangxi #2
1/18/2005
M.V. TAI CHANG
Arrival Date:
SPECIFICATION
RESULTS
12/14/04 INTERPRETATION
Identification
A. To Pass Test
B. To Pass Test
C. To Pass Test
pH 7.0 to 9.0
Water Soluble Substances
Not more than 0.2%
Aluminum
Not more than 2.0%
Calcium
Not more than 0.9%
Iron Not more than 0.25%
Magnesium
17.0% to 19.5%
Lead
Not More than 10 ppm
Loss on Ignition (1075 C)
Not More than 7.0 %
Calcium, Soluble in 1 M Sulfuric Acid
Not more than 0.6%
Calcium, Insoluble in 1 M Sulfuric Acid Not more than 500 ppm
Iron, Soluble in 1 M Sulfuric Acid
Not more than 250 ppm
Magnesium, Soluble in 1 M Sulfuric Acid Not more than 0.4%
Carbonate
To Pass Test
Chloride
Not mmore than 140 ppm
Loss on Drying
Not more than 1.0%
Microbial Limits / Total Bacteria Count Not More than 100 per g
Passes Test Passes Test Passes Test
8.549 0.02% 0.18% 0.42% 0.064% 17.70% 1.17 ppm 6.19% 0.40% 237 ppm 68 ppm 0.17% Passes Test Less than 140 ppm 0.16% <10 per g
MEETS BP
MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP
Respectfully submitted,
Ronald A. Schnitzer' Director
ITA-Ratcliff-000138
MEMBER
AGIL
Sami-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES 178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201) 843-2525 FAX (201) 843-4934 E-MAIL sanipure.labs@verlzon.net
Certificate of Laboratory Analysis
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
3/15/05 3/21/05 05,074, k, 201 1 of 3
Product Identification Grind Date Ship Name
Luzenac Guangxi # / '
3/9/05
M .l
-- MA/. Great-Century- Arrival Date:
2/22/05
ANALYTE
SPECIFICATION
RESULTS
INTERPRETATION
Identification Loss on Ignition (1000 C) Acid-Soluble Substances Reaction and Soluble Substances
Water Soluble Iron Arsenic
Heavy Metals Lead
Microbial Limits Total Bacteria Count
To Pass Test -< 6. 5% < 2.0% < 0.1%
To Pass Test < 3 ppm < 0.004% <0.001%
< 500 per g
Passes Test 6.14% 1.42% 0.057%
Passes Test 0.15 ppm < 40 ppm 2.68 ppm
< 10 per g
MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP MEETS USP
MEETS USP
Production/Asbestos Identification A. IRTest B. C. pH
Loss on Ignition (1075 C) Water Soluble Substances
Iron Aluminum Calcium
Lead Magnesium Microbial Limits Total Bacteria Count Microbial Limits / Fungi Count
To Pass Test
To Pass Test To Pass Test To Pass Test
7.0 to 9.0 < 7.0% < 0.2% < 0.25% < 2.0% < 0.9%
<10 ppm 17.0%- 19.5%
< 1000 per g < 100 per g
Passes Test
Passes Test Passes Test Passes Test
8.771 6.20% 0.024% 0.053% 0.14% 0.41% 2.68 ppm 17.20%
< 10 per g < 10 per g
MEETS PhEur
MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur MEETS PhEur
MEETS PhEur MEETS PhEur
Respectfully submitted,
I m &MA ii/k-c
Ronald A. Schnitzer , Director
ITA-Ratcliff-000139
MEMBER
AC1L
Sani-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES 178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201) 843-2525 FAX (201)843-4934 E-MAIL sanipure.labs@verizon.net
Certificate of Laboratory Analysis
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
3/15/05 3/21/05 05,074,k,201 2 of 3
Product Identification Grind Date Ship Name
Luzenac Guangxi / % J O * 3/9/05 Rj& (Zo^Ef Q T M.V. Great-Century Arrival Date:
ANALYTE
SPECIFICATION
RESULTS
Identification 1 2
Loss on Ignition (450-550 C) Acid or Alkali
Acid Soluble Substances Water Soluble Substances
Iron Sioluble in Water Arsenic
To Pass Test To Pass Test
< 5.0% Neutral < 2.0% < 4.0 mg To Pass Test < 4 ppm
Passes Test Passes Test
4.92% Neutral 1.42% 1.32 mg Passes Test 0.15 ppm
Identification A. B.
Loss on Ignition (800 C) Loss on Drying (105 C) Acid Soluble Substances
Soluble Salts Free Alkali Arsenic Lead
To Pass Test To Pass Test
< 6.0% < 0.5% < 2.5% < 0.2% <1.0% < 3 ppm < 5 ppm
Passes Test Passes Test
5.88% 0.11% 1.42% 0.071% < 1.0% 0.15 ppm 2.68 ppm
2/22/05
INTERPRETATION
MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII MEETS JP XIII
MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC MEETS FCC
Respectfully submitted,
l Donald . Schnitzer^j Director
t.
ITA-Ratcliff-000140
MEMBER
AGIL
Sani-Pure Food Laboratories
CHEMISTS TO THE FOOD INDUSTRIES 178-182 Saddle River Road Saddle Brook, New Jersey 07663-4619 VOICE (201) 843-2525 FAX (201)843-4934 E-MAIL sanipure.labs@verizon.net
Certificate of Laboratory Analysis
Luzenac America John Poston 17509 Van Road Houston, TX 77049
Date Received: Date Reported: Lab Number: Page:
3/15/05 3/21/05 0 5 ,0 7 4 ,k ,201 3 of 3
Product Identification Grind Date Ship Name
ANALYTE
Luzenac Guangxi # /
3/9/05 E M.V. G feafG errtury
Arrival Date:
SPECIFICATION
RESULTS
2/22/05 INTERPRETATION
Identification
A. To Pass Test
B. To Pass Test
C. To Pass Test
PH 7.0 to 9.0
Water Soluble Substances
Not more than 0.2%
Aluminum
Not more than 2.0%
Calcium
Not more than 0.9%
Iron Not more than 0.25%
Magnesium
17.0% to 19.5%
Lead
Not More than 10 ppm
Loss on Ignition (1075 C)
Not More than 7.0 %
Calcium, Soluble in 1 M Sulfuric Acid
Not more than 0.6%
Calcium, Insoluble in 1 M Sulfuric Acid Not more than 500 ppm
Iron, Soluble in 1 M Sulfuric Acid
Not more than 250 ppm
Magnesium, Soluble in 1 M Sulfuric Acid Not more than 0.4%
Carbonate
To Pass Test
Chloride
Not mmore than 140 ppm
Loss on Drying
Not more than 1.0%
Microbial Limits / Total Bacteria Count Not More than 100 per g
Passes Test Passes Test Passes Test
8.771 0.02% 0.14% 0.41% 0.053% 17.20% 2.68 ppm 6.20% 0.40% 309 ppm 54 ppm 0.16% Passes Test Less than 140 ppm 0.11% <10 per g
MEETS BP
MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP MEETS BP
Respectfully submitted,
L m
-Ronald A. Schnitzer
Director
ITA-Ratcliff-000141
