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- 2. S Rev.lO'SJ to: subject: INTEROFFICE COMMUNICATION Westlake, Louisiana June 25, 1969 D. G. Duncan Oxy Reactor Thermocouple Attached are sketches showing the location of each thermo couple in the three oxychlorination reactors, R-301, R-302 and R-303. These locations are to be used the next time each reactor is recharged and all other future recharges unless specifically modified, in writing. I agree with your suggestion that each thermowell be long enough to cover the entire range. This will allow us to run a complete manual profile on each thermowell tube if cross checking is ever required again. RHG-PBB cc: LNV DKP RLH JDM RDG PMW* RWC Attachment "* R. H. Geriach 000008227 "Tl>&^SfJ-L' ~ 7'~ -- * J t ; ~i ; i ! -vl 1U ;. ; . Ui 2 1 ! ! ^ TTa ; ^ \K -h* ! - -i : .j. . ia :s : --f -- i"' H. II ; Jl I A 4 i <0 !A L i---- -tv-1---- i i'o; '1 T~` .-VS rvr \U\ rr i i - ~-t- --t' . 1i ! -t-- i1 11 M i r ru j ; 1_ :V !i k- __N5 1__ i i \S : i ! ----- 1-------'Ii V"!` I >> !ii '? ii iI ->--4 x_ _VL. Bjrrmepi i i >> ,' 1 .. ! 5 ' ' ' ! u__L ^1/ i 1| r.^H- 1 t j] 1j O&r Z- -/s/-4_j: i3_L TtfZ.Rno cou_Pl:5____ //j \UGLL5 / 2 :-*>3 //*UL2> i au, 7~<Lf' --! . .02^3 . 4k4~ _.m&i Made sy_. * nv = Date_________ TITLE CONTINENTAL. OIL COMPANY CALCULATION ITET , - Joo No____ o3 y /-/{2J^ojjj'E2'l.L: i!! [i ii i. 000008239 V cCR. NV. *! to: subject: ` JV. V INTEROFFICE COMMUNICATION ! Westlake, L uislana July 24, 1969 M Mr. D. G. Duncan .. - 'v- &3 /-I tf) -A' , . Vj ,,'\f --I ,.'<r, ** 4 V^- ' ,,; *, f' i R-301 Thermocouples A\.-` "i":) Please relocate the top thermocouple in well number three on the first oxy reactor, R-301, from 91" below the top of the top tubesheet to a position 135" from the top of the top tubesheet. This new location is approximately 2" above the top of the bottom tubesheet. This is a temporary change and unless written instructions to the contrary are received, the thermocouple layout described in my letter of June 25, 1969 should be followed on the next reactor loading. RHG-MC ccs LNV DKP RLH JD/ RDG PMW RWC KCC R. H. Gerlach v^r? f * , .AC* \ . ' Afr ' Vi*; r~; V ... V` ' 1 ' 1 * i a, , > t ' ` v ,V'L- '* *' s , VJ *'-' ** f, * A,' ', i>i, 11"> JvV-1 . Vi '<* 1 1 ' V < / #" J 1 - ' "'/ t ' ,, 1 '< !^r,, J .* :: r> *f ' .t . - <h?v ; - ` J . ", :':'A*-AT'`: . 1 .Afc.. , VC . ^****>*,4^4^^ ^" - 4:* i ` 1 'l /it-1 V ' 'r :/ , *" ` ,,r 1 , , ,,V,, > " <V V , - <*V.H % V.-^AVr-A ' . ,"yr' ' - 'l ' '' r ' 4 ' ` / v*'"* , v v v' ' . r, f rt " - y\`r k 000008Z'2 ~f----- -- pa .* -,v& ?: ,r `W-'i, - *' i , " - ` **"'* ' ;.v 4?jii'**-v" v -.v - -* ' s' .t, .j-' , , ,1` j ., i1 "* *' ^ ' ',* -r to: SUBJECT: INTEROFFICE COMMUNICATION Westlake, Louisiana June 25, 1969 D. G. Duncan Oxy Reactor Thermocouple Attached are sketches showing the location of each thermo couple in the three oxychlorination reactors, R-301, R-302 and R-303. These locations are to be used the next time each reactor is recharged and all other future recharges unless specifically modified, in writing, I agree with your suggestion that each thermowell be long enough to cover the entire range. This will allow us to run a complete manual profile on each thermowell tube if cross checking is ever required again. RHG-PBB cc: LNV DKP RLH JDM^ RDG PMW RWC Attachment R. H. Gerlach CCR oooaa3 'ajellS 0000082'1* / A`I (T /'V' ry- '.V- v 't V, ' M^ : iTl iii 3 rr x s. _L to i K y ^1 hi Y iV Y ""L Y rrr i^ i^ ,,s i! 'Y is (S \s 'Y .!; '-o m I! s lit k Ss ! S. \ K\x ;y ! ^| Y ; o$*' *\ i * i lr. % , Bottom .b.h_____ 'BoTT&rf Xb@E- .'. St/7~ \ : o ~&Z "" a ft / V * (/> Yv/ 2d Po/tiT vJBLL PLY a/ CONT:;\[-^iT,'', _,, OIL ' ca lcul;."' ^r-* ., Jen So. ,,7?~_b>_OZ TM-2M> WbLLS CCR 000008235 it- 4 ' //? Page cir__________ __________________________________________ ..... ---------------------- ---- ,_______ __ _______ State f Da re . _____________ i'aOie , ................. cr title...... <3/ Tf/gRMO ^j LLS r- iclo__ 31 a r e .. ,, CCR 000008240  N o.; ;>y C. O i i' " Da C Page ___ __ o CONTINENTAL. 'L C ,,*MT'ANY CALCULA', : :; l . !ET TITLE_____ TsLz^LQkL.-. JOi3 NO--------- rrn ^ CCR 000008241 Fm d ________ ..._ State. ______ ________ r-v ,[- A si-. V/ .. n &p* ^0 /44 chij* __________________ _ R-3!>y t* A ,<ri f 4/ t b - /i / 2 - //#; & / ' b'i m '- 3' /3/ - /3 ^ /6^- 3<f ~~ /..- V stf- f1/- 3$ ' .-- . ___ - ^1:1/-:' I/L .... ........................ - f <2y>^ /*:. /**&) (Oly^ (%>* ^) $' 3ft $'301 * .1 A tf- /*./' tb 5 /J'f it fftx. /o'n" a. i t kt on. JbH - 3^ -. /3./ - - (S'ffjMh* lbs- 3*1 * /3_/' IllhSt* ^r 4s]" --- ?j- *>- fT"_.... * -` ... ._ . -I- X \ 3/ CCft 0000082^4 THIS SHIPPING ORDER Cameras No.. GREYHOUND BUS LINES -(Name of Carrier) Shipper's No._ 221 From At CONTINENTAL V.C.Jj. Plant Westlake,. Louisiana 10-23-70 19 lh prar-erlir rfeierfbad fwraw, in apparent quad m1(, except *5 n<ild <tenlnli and condition .af cojireiifi of packages aniceowe), narked, censFgnsd. and dexllaed as radleafed below, wfcldi said carrier flfie wwdcorrlar bcUf understood fereagheuf tot* cwdract as mn> leg aer person or cerpcwaUon Jn possession of ihe properly under (he eonlracf) agrees fo carry to Ms usual place ef deMvery at said desttoellan. if on Its Teele, otherwise to deliver to another carrier on the rout* to said desllaellea. Jt h reehwEFr agreed, as to each carrier at all or any of sard properly over all or any portion or said ro-j!e to destiaatHa, and as le mc? party at any lima Inlereslod In all or any at said properly. Ihal every sank* 1e be perform** honaader jfialf be sabtoct to all tbo larau amt coed ItIons ( ttw Uwftono rnmaitlr SlsalgM Bill of lading set forth fit to Official, Jo-i'tiern. Wes'"rn and 1111 n-o Is freight tlasslflnllwn Jn effect on toe daTo hereof. If IHs Is a rail or a rail water shipment, (2) It to* applicable motor carrier classification or tariff If thb Is a motor carrtar shipment. Shipper hereby cerliflet Ihal he Is familiar ifh ail Iho and osndillans of the said bill of lading including those eu the back thereof, set forth In the classlffcallen or tariff which governs the Mmsportattort at this shipment, and fhe said terms and mdltleni are hereby agreed to by *he sh pjcr and ac copied f-- k'----- " J ------------ Consigned to Destination CONTI MENTAL OIL COMPANY, PONCA CITY ATT: DR. FRED RADD, RESEARCH 6 DEVELOPMENT BUILDING (Mai! or street address of consignee--For purposes of ratification only.) County. Delivery __Address jr (+To be filled In only when shipper desires and governing tariffs provide for delivery thereat.) Route LAKE CHARLES TO TULSA -- GREYHOUND M-T-fcO - ULSA TO PONCA CITY Delivering Carrier No Packages ________________________________________ Klrd of Package,, Descrlptfon of Articles, Special Marks, and Exceptions _Car or Vehicle Initials- Weight (Sub. to Correction) 1 5-Gal DRUM 100* HARSHAW CATALYST LOT # 70 40# 1 5-Gal DRUM TECO-SIL 48# Class er Rate Cheek Column _No,, Subject to Section 7 of Conditions of applicable bill of lading, If tfrla ship ment Is to be delivered to the consignee without recourse on the consignor, the consignor shall sign the follow fog statement: The carrier shall not make delivery f this shipment without payment of freight and al! other lawful charges {Signature of Consignor.) Jf charges are to be prepaid, write or stamp here, "T be Prepaid " To BePrcpaid (Per C.L. Shaddock) __________ Received &_ to apply In the prepayment of the charges on the property described hereon Agent or Cashier Collect On Delivery, and remit *o C. O. D. Charge {Shipper to be paid by Consignee n (The signature here acknowledges only the amount prepaid.) Charges advanced: Q ____-"_'_S_h_i_p_p_e_r_'s__i_m__p_r_i_n_t__in___li_e_u__o_f__s_t_a_m__p_,__ro__t__a__p_a_r_t__o_f_bbiilllpof ladin_g__a_p__p_ro__v_e_d__b_y_,_t_h_e__i_n_t_e_r_s_ta__te_ Commerce Commission." If fir- i.'mnpi n^ive'. heiwecn Ue poiK by a cm lei by water. rha law requires Ihof (he bill of lading shall slate wfipflior H h "darrlor's or shipper's weight." NOTE -Wl.rr; th e tale - Her^ideii on value, shippers are lequired lo jlale specifically in wrillng Ihe agreed or declared value of the property. 1 1 The agreed sr dec lared v 'ue ar ihe ptopeMy h hereby specifically slated by Ike ih.pper to be nol oxceedmg / ' f Continental VCM Plant P.O. Box 605 Shipper, Per Jesse H. Coplin' The Fibre Boxes used for this shipment conform fo the specifications set forth in the box marker'* certificate thereon, and all other requirements of Consolidated Freight Classification. Greyhound Bus Lines Agent, Per Westlake, Louisiana 70669 Permanent postoffice address of shipper,. ___ ** / SKAP-A-FART mSim / W4r/OAM4/ 47-413 MAMMU.C.A. l CCR 000008245 15??^ Agent must detach and retain this Shipping Order and must sign the Original Bill of Lading I ' (FT* //' / ^ /^Y S'6 ?0 gA-ytst/Sirisi-ct<s^1 'dco^TiJZS -3o5 A' - 60 l /i- 30! 'tidJ^ ^ /ycu.. 1.77Jt -- 3333/^o >u^ . _.. 2 a<Jcu [ so'/i ?W~&jj 3r^ X-C<*'vJ^'-^ U'iUg/l^')- ot'Jiiisjt jJUU THU 5. 3/ yt'Cc^S >,, -t $ /3? u3 ^ sfttc3i - /c? yj s1 / / 5^< 1i r i *T6 ?t , /t//o/7# / Sjk&t ^(sLd.'bi ~?4 J-,/ict-tco <. CJ3t A' 10^ /1 <3- cjC^^ ci.^,'^_^ CCR 000008246 /?70 F'3 o ( /& fac?l/ /tp </(!pCt7u ii//rm /3 /oo?z AO 07/ /< 00/3 /*0//g /<>//? A< 0/0 s /r 0//3 /0O?f A o//z. / oo?A /< 0/67 A*- o/o& A o/a? /. o//o A o/o? /<o/3A \ Ao/<?/ AO//3 A< o/oo / 0/06 f/A/AAA fUsUA AooZ9 /,o/^s /.o/az. A<0072. A< 0/08 Ao/07 /,0//s A`6>07Z /r 00/3 /O/AA- A 0/06 /. 0//2- / o//-A A oo?6 /> 0/0/ A'OoZT Ao/// /'OZ/A A< 0//? /.oo?s> A o/o6 / oo ?A A oo?6 A o//6 Ao//3> A 0078 A.oo?/ /oo/? /.OO/S' A0097 /oo// Ao/oA A 0/03 /0/07 /` 6/07 /< 0920 / o/a 8 / oo 9? AO/// A o/0? A<o//7 AO/// /O//0 AOo9o Ao/oo A`O/28 A oo/? A' o/o? A 0/08 /< o/ZC / 0/33 Ao//? /oo?/ AO//a A'OO?A A-O/AO A<o/A? A'O/oz. /GO 92- A o/o/ AS/AAa ~Z<'-;,/^cro, CCR 00ooa^? '/9>--Z3 OZ /0^<3 ~7>/00/*79'S 7/oV /97<2 7'Ttm/tf 9dtot TrAfctr 0. ??% 0.9997 /, 06/9 0, 9907 0. 99S% /.oooo 0.9993 0.9992- 0. 9998 0. 99J9 0, 9972. 700/7 0. 9999 0.9993 /0008 /. oooz 0.9903 0.9990 0.9903 /<O03l / fOO/O 0.99/9 0.9903 7 00/7 0. 9972. 0. 9997 6.9999 0.9938 0. 9930 /.oo/z 0. 997f 0.992/ 700/0 / 60/9 /.OOZO /, oo// 7 OO/S /.06Z.O 7oco& y.oooy /00/3 /OO/T- 0.9997 0.999/ 6 .9999 0. 999//oooo 0.9997 6. 9999 0.9999 7003/ /9- 9997 0.??/9- /.00Z2 /.ooo/ /,0 0/0 / 6/Z/ 6.9997 /.OO// /`OCQ.0/ /eo/z 7*0090 700/6 /&" 0.9997 0.9990 0.9990 70000 /, 003/ 70003 0. 999/ 700/^ 7rOOOO 7 oooe /, 000 0 7 oo/7 S0OOO0 /cOO/<7 0. 7.000/ 7003/ 7.00/9 700/7 700/7 700/9 OCR 0000082*8 a&>4x - ~aA3 as /O0V-/97& 5* A*p / 0/3Z A0A?? /0/33 A o//7 / a<?73 /1 o//^ /OOSZ /<D0/g /< 0/0 2. 7 0//> /< ooS 3 /<0/33 Ao//6 A O0/3 A 0//A7 O/OO A'Oo?/ /'. 60 2/ A6//7 A-o/sA /c /0/37 A-oo/A A o/3 9 /\ 0/3/ A<oov2A`0//3 A0077 A`0/o9 A* 0/00 A- 0/&8 A00B/ A/o/AA A'6/ZZ- y7f A` o//<? A*o//^ /< OofA At 60?3 A 6/2 A A3//A A0//0 1 7 00& 7 /. 0/3/ A60ES / 0/3.6 A<o/37 A 0/3 A A oof/ A oof/ A 0/0/ A. 6/3 A Ai 0/3/ /. 0/63 A`6/A3 A 6//A A 0/07 A'0/2-8 A` 0/3 J A`0A3 A'00/3, /.6A66 A* 6/3/ / Oo/Z/. 0/3 8 A< 00 76 A` 0/33 7 0/3/ AO/30 A oo.f/ A`007A 7 oofA A`O/33 A'6//A A 60 72. A o//y A<o///f A`6A<3/ A 0/3 8 A-<0/0/ A 6//8 A oo9/ A`0//g A<0A3/ CCR 000008249 ~J),aAiftCtrS -- ,/p 'J'.' , // -/s>/> A O/OZA^co$? /. o/z Z- /.007? A f? /.o/a9 /. 0/2.) / <0/(3 A 0077 A 003 3 A oo?f A<o//7 /< 0/0 ( /. 0/(5/ /. OX? /. 0/0 / A. 0/0? /.o/6S /.00?9 /. 0/0( /. <?//,? J7T 2>. (t hC^rs) /o^y^$ /.o//^r /. & /os /*o//o /c O/OZ. A o/o4- /. <5X52. /. 0//4 A. 0/04- /, o/o / /.oo$ A O/AZ. /*o/o7 />o/// /.o//o /.0/30 A o/a$ /.oo9z. /< O/o3., /. oog ? /. <j>o<?6 /. o//x_ X (J/o "X / 05/XS' / 0//A /. O/OZ / 003& A <V0 A0/(2- /. O Q$ip /<o//7 AO/// A o //s /. /.0/cB A o/oz. A0//8 /< o/oz /.o/o9 /. o /oi /< o/oc, / * OO&fi' /OOfpUp /. <70?/ A >/> /' 0/22. A< Oo ?A A o//$ /,0//3 /. OO?/ / oo/ A AOo$? /. o/($ _/. 0,/I_ /< oo$4- A o>/<2/__ /. OOSS CCR 000008252 ^w) zS) Z?) Z3) Z&) zi) zT) Z9) 30) 30 iS) *) ss) 3$ 37) 3& 3f) n) b/ rfof /.0//3 /'6/02. /< oc%4/'0/v /.0//7 /. 0/02 A eo?& A 0^00 /< 0/02 /G//7 A 0072. Aoofg /< /<c//o /$$/7 aoo73 Aooff / ,o/oS A 0//3 OCR 000008253 / ~J)r'aieX? /7)<g<Z J~.7>. (,'Ajd*>s) /&/? /$ "/&4) /S<q4pv4i 0 /.00^/.-&/>& 0.9977 0. 9906 l) o. 97U 0. 9f/7 3) 0.99/7 0. 9/7/ ) /.GCQp o. ?m 0. 999/ d /*00/2- 0-9773 /. oa/7 6) /. oo/o /. oo/3 0. 999/ /.CO37- O'?/?/- 0.9990 V f) /.OCO-7 0-9U7- 0. 99// 0.99/0 9.003/ 0. 97/6 /o) /<oco 0.999? /. oo//, /') c. 97/7 /.OOof /t) /. 00/3 /.C02.Z. /.ooo% /.OOl/ /*) /. QOOf /c 002 7 /) /, oo// /. co// fb /c 0003 /. 0002. /&) a. 9?77 /.oo/6 /< 00l(, /'Oo2o 0. 9979 /. OO// t7) 9. 99/3 0.9/77 0. 9/7/ A 0. 97/4 0. 77/o t) /ood/- /, OOoZ /-CO/S /. 003 3- /<Z<5) 00/7 2>) 0.99/9 /. Oof2-- Cc c /) 2) 3) y) g) 6>} 7) *) ') /<?) //) /4> /S /?) \ tz) /4) /i) /&) r (Z&C'tiL* &iS &&&o&u, j / 2), /pi &d&Q/j , A 0/30 /,&//? /. OS/2- /ji~^ /O/// . /,OA3/ /, 0 //4 AO//3 AO// 7 /. 0/0f /. 0/$^ /. 0/33 -^ZC/t dir*/. 3zi/. /O/fio /. 0/3 7 /* 0/3 A.O/O'7 /o/o CCR 00008256 3) ~7l^r^id2j ffiO &&& J S&tstfL &&--^Ss&i^tzS^ /) /. 007-3 J) /.OA/3*) / 0073 *) /. 0//0 <#) /0/J?3 <0 /.0//47) 7007/ s) /. 00/2?) / 0/0?3 /a) y,o/// //) /. o//7 /) P&isZ? (%%&**' /3~) / 0//3 /y) /. 00y? /y) 70/0/ /) A 0/03 /?) /. 0/0Q> /&) /. 0/0/ /?) /. 0/30 20) /. 006 / j/) /OOTO CCR 000008257 Q -y) s.w. < A). AJ W. , 'X? ~^x>3 7&&Z /. A. j a*a/&S /O/O& /. oorr A* 00 /. 0/3 /.o/o7 /.0078 /.SO6,2. /o/j>7 V7'a^rs a&j /ty* #.D X // CCR 00000825Q WE! HARSHAW CATALYST Cu-0932 T 3/16" Specificnt:ion Shoot: Harshav; Lot: No. Date - received in Richmond \9.('A/97 Stauffer Code No. tOltri - K.'~ } . For Shipment to _ Sample Cupric Chloride (v:t. %) Potassium Chloride. (v;t. 77) Iron, as re (ppm) Sulfate as S0^_ (v;t. %) Silica as SiO^ (v?t. 77) L.O.I. @ 300 (v;f. 77) 17, A !. 7 9 oc O. 11 O /> * rJ. Specification 18.0 + 1.0 1.80 + 0.25 <800 <0.25 <0.25 <5.0 Bulk Density (ib/ft ) Hardness (wt. 77) Fines through 6 mesh Tyler Screen (v:t. 77) <7-9, 07, i > 40 d; 4 >90 <1.0 Tablet Siee (in.) Avc. Length (in.) Ave. Width (in.) % Outside Range O. /S 7 OJ&.C 0.172 - 0.203 0.172 - 0.203 0.172 - 0.203 < 20% B.E.T. Surface Area (in^/gm) ___ \ 5 rc /5Jj- Total Pore Vol'.'.-e (cc./gm) ___ r ~ ^7 Pore Volume 80-600 (% of TFV) Pores ________ 77________ i Average Pore Diameter (A) (Ball)___ 7 7. {. Average Pore Diameter (A)(BET) <sc /// 195 + 25 >0.40 > 50 > 80 REMARKS ; out /o Cl - / s'V '1- % u- :c '-v-tor-'K. /fMic-'i - SlilTTL. CC/*: o0OOQzs9 ~