Document oDjpNB623xqoMjMwqo5yJ9aRR
STLS F, V F R N I RENT
STL Chicago 2417 Bond Street. University Park, IL 60466
Tel: 703 534 5200 Fax: 703 534 5211
www.5tl-inc.com
Us e v e :R N T R E N T
DORATORI
1...... A N A L T C A L R E P O R T
JOB NU MB ER : 232473
ES
Prepared For :
Weston S o l u t i o n s , Inc.
1,400 . . : We sc orl W a y 5-2........ Building' 19380-1439West Chester / 'PA'
..
Project :. C o n f i d e n t i a l D e cat.nr -:::T e n n e s s e e :R i v e r :.'
At tout ion : Ja: Kesarj..
;/s:2/io:o :
This Report Contains
Leaders in Environm ental Testing
Date S'i'TI C h i c a g o
2417 Bond S t re e L 60466U n i v e r s i t y Park, IL
PHONE: ( 7 0 8 ) 534-5200 F A X . ,,: (708) 534-5211
Pages
Severn Trent I ahorstones, Inc.
WET CHEMISTRY DATA PACKAGE CONFIDENTIAL DECATUR-TENNESSEE RTVER
JOB# 232473
Data Sum m ary.................................................................... 1 Chain of Custody..............................................................16 Case N arrative..................................................................20 Raw D a ta ........................................................................... 22
STL Chicago is part of Severn Trent Laboratories, Inc.
-a :m p :1 :e in f o r m a t :i o n :
Date: 12/22/2004
.
Job Number. 232473 Sue torner... Westen Solutions, Inc. Attn...... Jai Kesari
Project Number...... .
Customer Project ID... Project Description...
20004904 CONFIDENTIAL DECATUR Confidential Decatur - Tehhesscc River
Laboratory sample ID
232473-1 232473-2 232473-3 232473-4 232473-5 232473-6 232473-7 232473-8 232473-9
"Customer Sample ID
DL3-SW-LDC001 DL2-SW-LC001 DBC-SW-LC001 DOU-SU-LQC001 DDO-SW-LOC001 DLl-SW-LOC001 DMC-SW-LOC1 DM-SW-LOC5 DAA-SW-LOC002
Sample / Matrix
Pate Sampled
Water
12/01/2004
Water
12/01/2004
Water
12/02/2004
Water
12/02/2004
Water
12/02/2004
Water
12/02/2004
Water
12/02/2004
Water
12/02/2004
Water
12/02/2004
T me Sampled
13:00 14:45 08:40 09:40 10:40 11:30 13:00 16:15 16:50
' Pate ..Received:' 12/04/2004 12/04/2004 12/04/2004 12/04/2004 12/04/2004 12/04/2004 12/04/2004 12/04/2004 12/04/2004
...T ime Received
10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00 10:00
Page 1
1
STL Chicago is part of Severn Trent Laboratories, [no.
Job Nimber: 232473
:CUSTOMER: Wes tor, Solutions, Inc.
Custonser Sarrpl e [D Date SanpLed..... T ime Sarrpl ed..... Sample Matrix....
OL3-SU-LOC001 12/01/2004 13:00 Water
TEST: METHOD.
:PARAME TER/TEST: DESCRt PTtOH
160.1
Solids, Total Dissolved (TD5) Solids, TotaL Dissolved CTDS>
160.2
Solids, Total Suspended (TSS) Solids, TotaL Suspended (TSSI
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL. DECATUR
Laboratory Sarrple ID: 232473-1 Date Received.......: 12/04/2004 Time Received....... : 10:00
Date:12/22/2004 ATTN: Jai Kesari .
0
SAMPLE RESULT 120 3.0
FLAGS !
. MDL
S .4
4.0
RL
DILUTION
UNITS
BATCH DT ; .DATE/TtME t ech
10
mg/L 136637
12/D8/D4 1439 jmk
5.0
rrg/L 136402
12/07/04 0934 rrm
* ]n Description = Dry Wgt.
Page 2
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 232473
CUSTOMER : Wester,.SoltiMis/ tnc.
Customer Sample ID Date SampLed..... Time Sampled..... Sample Matrix....
DL2-SU-L0C001 12/01/2004
14:45 Water
TEST METHOD 60.1
160.2
:PARAMETER/TEST.0 ESCR1PT]0M
Solids, Total Dissolved ETDS) Solids, Total Dissolved CTDS)
Solids, Total Suspended [TSS) Solids, Total Suspended fTSS)
n
LABORATORY
TEST
RESULTS
/PROJECT: :COW FEDERT1ALDECATUR:
Laboratory Sample ID 232473-2 Date Received...... 12/04/2004 Time Received...... 10:00
D a te :12/22/2004 ATTN: Jai Kesari
T SAMPLE RESULT |0 FLAGS:
92 20
HPL 3.4 4.0
RL 10 5.0
DILUTION UNITS BATCH DT DATE/TIME TECH
mg/L ;136637 mg/L j136402
12/08/04 1442 ! jmk j
12/07/04 0936; rrni ij i
En Description = Dry Wgt.
Page 3
STL Chicago is part of Severn Trent Laboratories, [nc.
Job Number: 232473
CUSTOMER ::Weston !Solutions , Inc.
Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix....
DBC-SU-LOC001
12/02/2004 08:40 Water
TE S T/M E TH O D ;
;PARAMI! TE R/T ST DESCRI PT ION
160.1
Solids, Total Dissolved CTDS) Solids, Total Dissolved HD S)
160.2
Solids, Total Suspended <TSSJ Solids, Total Suspended ITSS)
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECATUR '
Laboratory Sample ID: 232473-3 Date Received....... : 12/04/2004 Time Received.,.... : 10:00
Date:12/22/2004 il;;;/;;; ATTN: Jai Kesari
SAMPLE RESULT IR EUGS: 100 10
M&L 3.4 4.0
RL DILUTION UNITS ! BATCH DT DATE/TIME TECH
10
mg/L
136637
12/08/04 1446
5.0 :-1
mg/L
136402
12/07/04 0938
In Description = Dry Wgt.
Page 4
STL Chicago is part of Severn Trent Laboratories, inc.
Job Nunber: 232473
CUSTOMER: Ueston Solutions, Inc.:
Customer Sample [D: DOU-SU-LOG001 Date Sarrpled...... :12/02/2004 Time Sampled...... :09:40 Sample Matrix..... :Uater
TEST METHCO 160. T
160.2
PARAHETER/TEST DESCRIPTION
Solids, Total Dissolved (TDS) Soli ds, Total Dissolved (TDS)
Sol ids, Total Suspended fTSS) Solids, Total Suspended (T55)
IO
LABORATORY
TEST
RESULTS
PROJECT:. CONFIDENTIAL DECATUR
Laboratory Sanple [D: 232473-4 date Received...... : 12/04/2004 Time Received..... .: 10:00
Date:12/22/2004 ATTN: Jai (Cesari
. SAMPLE RESULT Q FLAGS ' 120 5.5
MOL 8.4 4.0
Ri 10 5.0
DILUTION .; UNITS ; BATCH DT DATE/TIME TECH
1
mg/L 136637
12/03/04 1449 jmk
1
mg/L 136402
12/07/04 0940 rnm
* In Description = Dry Wgt.
Page 5
STL Chicago is part of Severn Trent Laboratories, Inc.
In Description = Dry Ugt.
Page 6
STL Chicago is part of Severn Trent Laboratories, Snc.
Job Nuirber 232473
CUSTOMER: Weston Solutions, Inc.
Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix....
DL1-SW-LDC001 12/02/2004 11:30 Water
TEST METHOD 160.1
160.2
PARAHETER/TEST DE'SCR]PT 1ON
Solids, Total Dissolved (TDS) Solids, Total Dissolved {TDSJ
Solids, Total Suspended <TSS> Solids, Total Suspended <TSS>
LABORATORY
TEST
RESULT S
PROJECT: CONFIDENTIAL DECATUR .
Laboratory Sample ID 232473-6 Date Received..,___ 12/04/2004 Time Received...... 10:00
Date:12/22/2004 ATTN : Jai (Cesari
SAMPLE RESULT 120 18
FLAGS
MDL 8.4 4.0
RL: iD tLUT[OW :UN ITS :BATCH DT DATE/TtME TECH
10
mg/L
136637
12/08/04 1455 ijmk
5.0 !1
mg/L 136402
12/07/04 0944
* In Description = Dry Wgt.
Page 7
STL Chicago is part oi Severn Trent Laboratories, Inc.
Job Number: 232473
CUSTOMER: Weston Solutions , Inc.:;
Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix....
DKC-SU-L0CQQ1 12/02/2004 13:00 Water
TEST METHOD 160.1
160.2
:PARAMETER/TEST DESCRIPT1ON
Solids, Total Dissolved <TDSJ Solids, Total Dissolved ITDS)
Solids, Total Suspended (T5S) Solids, Total Suspended ITSSJ
<}
LABORATORY
TEST
RESULTS
Date:12/22/2004
PROJECT: CONFIDENTIAL DECATUR
.V ::::::::.:::: ATTN: Jai Kesari
Laboratory Sample ID 232473-7 Date Received...... 12/04/2004 Time Received...... 10:00
SAMPLE RESULT |0 TLAGS: 110 7.0
MDL 3.4 4.0
RL 10 5.0
DILUTION UNITS ! BATCH ;DT DATE/TIME: TECH
mg/L !13*637
12/03/04 1459 jrnik
mg/L 136402
12/07/04 0946
* In Description = Dry Wgt.
Page 8
STL Chicago is part o"f Severn Trent Laboratories, Inc.
Job Number: 232473
CUSTOMER? Uston SoLuti/rie
Customer Sample ID Date Sampled..... Time Sampled..... Sample Matrix....
DAA-SW-L0CQQ5 12/02/2004 16:15 Water
TEST. MET a 160.1
160.2
:PARAHETER/TEST DESCRIPTION
Solids, Total Dissolved (TDS) Solids, Total Dissolved (TDS)
Solids, Total Suspended (TSS) Solids, Total Suspended (TSS)
in
LABORATORY
TEST
RESULTS
PRn.lFCT: rnMFTDFWTfAl DFDATIJR
Laboratory Sample ID: 232473-8 Date Received__ ____ : 12/04/2004 Time Received....... : 10:00
Date:12/22/2004 ATTN : Jai (Cesari
SAMPLE-RESULT? T W 6 S 78 5.5
HDL 8.4 4.0
Rl DILUTION UNITS BATCH DT DATE/TIME TECH
10 mg/L '136637
12/08/04 1502 jmk
5.0
mg/L 136402
12/07/04 0948:rrm
* In Description - Dry Ugt.
Page 9
STL Chicago is part of Seyern Trent Laboratories. Ine.
O 'H
* In Description = Dry Ugt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 232473
LABORATORY
CHRONICLE
hate: 1Z/2Z/ZDD4
CUSTOMER: Weston Solutions, Inc.
Lab ID: 232473-1 METHOD
160.1 160.2
Client ID: DL3-SW-LOCQ01 DESCRIPTION
Solids, Total Dissolved (TDS) Solids, TDta l Suspended (TSS)
Lab ID: 232473r2 METHOD
160.1 160.2
Client ID: DL2-SU-LOC001 DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 232473-3 METHOD
160.1 160.2
Client ID: DEC-SU-LOC001 DESCRIPTION Solids, Total Dissolved (TDS)
So Lids, Total Suspended (TSS)
Lab ID: 232473-4 METHOD
160.1 160.2
Client ID: D0U-SW-L0C001
DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 232473-5 METHOD
160.1 160.2
Client ID: DDO-SW-LOC0Q1 DESCRIPTION
Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 232473-6 METHOD
160.1 160.2
Client ID: DL1-SW-LOC0CI1
DESCRIPTION Solids, Total Dissolved (TDS) Solids, Total Suspended (TSS)
Lab ID: 232473-7 METHOD
160.1 160.2
Client ID: DMC-SW'LOCOOl DESCRIPTION
Solids, Total Dissolved (TDS) So lids. TotaL Suspended (TSS)
Lab ID: 2324 73-S METHOD
160,1
160.2
Client ID: DAA-SW-LOC005
DESCRIPTION Sol ids. TotaL Dissolved (TDS) Solids, TotaL Suspended (TSS)
Lab ID: 232473-9 METHOD
160.1 160.2
client ID: DAA-SW-L0CD02 DESCRIPTION
Solids, TotaL Dissolved (TDS) Solids, TotaL Suspended (TSS)
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
Date Rccvd: 12/04/2004 Sample Date: 12/01/2004
RUN# BATCH# PREP BT #<S)
DATE/T1ME ANALYZED
1 136637 136637
12/03/2004 1439
1 136402 136402
12/07/2004 0934
Date Recvd: 12/04/2004 Sample Date: 12/01/2004
RUN# BATCH# PREP ET #(S)
DATE/TIME ANALYZED
1 136637 136637
12/0B/2004 1442
1 136402 136402
12/07/2004 0936
Date Recvd: 12/04/2D04 SampLe Date: 12/02/2004
RUN# BATCH# PREP BT #(5>
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1446
1 136402 136402
12/07/2004 0933
Date Recvd: 12/04/2004 Sample Date: 12/02/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1449
1 136402 136402
12/07/2004 0940
Date Recvd: 12/04/2004 SampLe Date: 12/02/2004
RUN# BATCH# PREP BT #(S>
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1452
1 136402 136402
12/07/2004 0942
Date Recvd: 12/04/2004 Sample Date: 12/02/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1455
1 136402 136402
12/07/2004 0944
Date Recvd: 12/04/2004 Sample Date: 12/02/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1459
1 136402 136402
12/07/2004 0946
Date Recvd: 12/04/2004 Sample Date: 12/02/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 136637 136637
12/03/2004 1502
1 136402 136402
12/07/2004 0948
Date Recvd: 12/04/2004 Sample Date: 12/02/2004
RUN# BATCH# PREP BT #($)
DATE/TIME ANALYZED
1 136637 136637
12/08/2004 1505
1 136402 136402
12/07/2004 0950
DILUTION DILUTION DILUTION DILUTION DILUTION DILUTION DILUTION DILUTION DILUTION
Page 11
11
Job Number.: 232473 ' CUSTOMER'; feston ScUutiOh?. , ino.
QUALITY CONTROL RESULTS PROJECT ; CONFIDENTIAL DECATUR
Report Date.: 12/22/2004
ATTN: Jai Kesari
...............
Test: M e t h o d : . 160.1 . . Method Description. Solids. Total Dissolved (TDS) .
Parameter-'........ . solids. Total Dissolved (TDS)
.. . Batch............ .: 136637 Equipment Code...
Analyst...; link .......
Test cede.: Tos
QC Lab ID
Reagent
Uni ts
MB 136637'001 LCS 136637-002 I4LSTTS1
MD 232473-9 MS 232473-9 I4LSTTS1
mg/L mg/L mg/L mg/L
QC Result
QC Result
8.40000 U 262.00000
84.00000 346.00000
True Value Orig. Value QC Calc. F * Limi ts
Date Time
250.00000 250.00000
8.40000 U 105
82.00000
2.4
82.00000 106
% 80-120
R 20.0 % 75-125
12/08/2004 1400 12//24 1403
12/08/2004 1508 12/08/2004 1512
Test Method....... : 160.2 . 1 1 .1 Method Description.: Solids, total Suspended <TSS>... . Parameter...... ...: Solids. Total Suspended (TSS)
; Batch.
.....:'.136402
Equipment Code.
.
........
Analyst'.,h'.::\rnui1 ..... Test Code.: TSS
QC Leb ID
Reagent
Units
MB 136402-001
mg/L
LCS 136402-002 ID4L5TSS1 mg/L
MD 232473-3
mg/L
MS 232473-3 I04KSTSS2C mg/L
QC Result
QC Result
2.68000 U 201.00000
10.00000 103.00000
True Value
200.00000 100.00000
Orig. Value QC Calc. F * Limits
4.00000 U 100
10.50000 0.50000
10.50000
92
% 80-120
A 5.00000 % 75-125
Date Time
12/07/2004 0930 12/07/2004 0932 12/07/2004 0958 12/07/2004 1000
Page 12
* %*% RC R=:RPD, A=ABS Dlff. D=% Dlff.
O Justin*
Q: U A L I T Y A S S U R A N C E M E T- H 0 D R E F E R E N C E S A N D N O T E.vS'.. " Report Date: 12/22/2004
REPORT COMMENTS 1) ALL pages of this report are integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sample results arc reported on a "dry weight" basis except when analyzed for
Landfill disposal or incineration parameters. ALL other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting Limits are adjusted for sample size Used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 5) According to 40CFR Part 136.3, pH, Chlorine ResiduaL and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters arc not indicated as field (c.g. pH Field) they Were hot analyzed immediately, but as soon as possible on Laboratory receipt.
Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated Limit. < Not detected at or above the reporting Limit. J Result is Less than the RL, but greater than or equal to the method detection Limit. B Result is Less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is Less than the RL, but greater than or equal to the methoddetection limit. Inorganic Flags (Flag Column)
ICV,CCV,ICB,CCB,ISA,ISB,CRI,CRA,MRL: lnstrunent related QC exceed the upper or lower control Limits. * LCS, LCD, MD: Batch QC exceeds the upper or Lower control limits. + MSA correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. E SD: Serial dilution exceeds the control limits. H MB, EB1, EBZ, EB3: Batch QC is greater than reporting Limit or had a negative instrument reading tower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or lower control Limits. U AS(GFAA) Post-digestion spike was outside 35-115% control limits. Organic Qualifiers (Q ' Column) U Analyte was not detected at or above the stated Limit. ND Compound not detected. J Result is an estimated value below the reporting limit or a tentatively identified compound (TIC). Q Result was qualitatively confirmed, but not quantified. C Pesticide identification was confirmed by GC/MS. Y The chromatographic response resembles a typical fuel pattern. Z The chromatographic response docs not resemble a typicel fuel pattern. E Result exceeded calibration range, secondary dilution required. F AFCEE:ResuLt is an estimated value below the reporting Limit or atentativelyidentified compound (TIC) Organic Flags (Flags Column) B MB: Batch QC is greater than reporting limit. * LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or Lowercontrol limits. EB1, EB2, EB3, MLE: Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Manually integrated compound. P The Lower of the two values is reported when the % difference between the results of two GC columns is
Page 13
13
QUA L ITY
S S UR A N C E M E T H OD S
R E F E RN C E S AN D NOT
Report Date: 12/22/2004
greater than 25%.
Abbreviations
AS Rost Digestion Spike (GFAA Sanples - See Note 1 below)
batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set
CAP Capillary Column CCB Continuing Calibration Blank
ccv Continuing calibration Verification
CF Confirmation analysis of original
Cl Confirmation analysis of A1 or Dl
C2 Confirmation analysis of A2 or D2
C3 Confirmation analysis of A3 or D3
CRA Low Level Standard Check - GFAA; Mercury
CRI Low Level Standard Check - iCP
CV Calilbration Verification Standard
Di L Fac Dilution Factor - Secondary dilution analysis
DI Dilution 1
D2 Dilution 2
D3 Di Lution 3
DLFac Detection Limit Factor
DSfi Distilled Standard - High Level
DSL Distilled Standard - Low Level
DSM Distilled Standard * Medium Level
EB1 Extraction Blank 1
EB2 Extraction Blank 2
EB3 DI Blank
ELC Method Extracted LCS
ELD Method Extracted LCD
ICAL
initial calibration
tCB Initial Calibration Blank
ICV initial Calibration Verification
IDL Instrument Detection Limit
ISA interference Check Sample A - 1CAP
1SB Interference Check Sample B - ICAP
Job No. The first six digits of the sangle ID which refers to a specific client, project and sample group
Lab ID An 8 number unique laboratory identification
LCD Laboratory control Standard Duplicate
LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest
MB Method Blank or (PB) Preparation Blank
MD Method Duplicate
MDL Method Detection Limit
MLE Medium Level Extraction Blank
MRL Method Reporting Limit Standard
MSA Method of Standard Additions
MS Matrix Spike
MSD Matrix spike Duplicate
m Not Detected
PREPF Preparation factor used by the Laboratory's Information Management System (LIMS)
RDS Post Digestion Spike (1CAP)
RA Re-analysis of original
A1 Re-analysis of D1
A2 Re-analysis of D2
A3 Re-ana lysis of D3
RD Re-extraction of dilution
RE Re-extract ion of original
RC Re-extract ion Confirmation
RL Reporting Limit
RPD Relative Percent Difference of duplicate (unrounded) analyses
RRF Relative Response Factor
RT Retention Time
Rage 14
m._ X
Q U A L I T Y ASSI) R A N G M T H D S ' '' R E F R E N C E S A N 0 N O T E S
' Report Date: 12/22/2004
RTW Retention Time Window Sample ID A 9 digit hunter unique for each sample, the first
six digits are referred as the job number
SCB Seeded Control Blank
SO Serial Dilution (Calculated when sample concentration exceeds 50 times the MDL)
UCB Unseeded Control Blank
SSV Second Source verification Standard
SLCS
Solid Laboratory Control standard(LCS)
PHC pH Calibration Check LCSP pH Laboratory Control Sample
LCDP
pH Laboratory Control Sample Duplicate
MDPH
pH Sample Duplicate
MDFP
Flashpoint Sample Duplicate
LCFP
Flashpoint LC5
Gl Gelex Check Standard Range 0-1
G2 Gelex Check Standard Range 1-10
G3 Gelex Check Standard Range 10-100
Gi Gelex Check Standard Range 100-1000
Note 1; The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current
abbreviation used. EX. LCS =LCS Post Spike (GFAA); MSS-MS Post Spike (GFAA)
Note 2: The MD calculates an absolute difference (A) when the sample concentration is loss than 5 times the
reporting limit. The control limit is represented as + / - the RL.
Page 15
15
CHAIN OF CUSTODY
IS
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE 1 of 1
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesarr email: i.kesa ritwestonso Iution s.co m
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
Grab Sample Composite
TSS TDS
SAMPLE ANALYSIS
ExyLIMS #
t
b32i l
7
e
1
Client Sam pie Identification DL3 SW LOG 001 0 041201 DL2 SW LGC001 0 041201 DBC SW LOC001 0 041202 DOU SW LOC001 0 041202 DDO SW LOC001 0 041202 DL1 SW LOC001 0 041202 DMC SW LOCQ1 0 041202 DAA SW LOCQ05 0 041202 DAA SW LOC002 0 041202
Collection
Dale 1-Dec-04 1-Dec-04 2-Dec-04 2-Dec-04 2-Dec-Q4 2-Dec-04 2-Dec-04 2-Dec-04 2-Dec-04
Collection
Time
13:00 14:35 8:40 9 40 10:40 11:30 13:00 16:15 16:50
X X X X X X X X X
eoe
o
zo
1 1 1 1 1 1 1 1 1
Sample
Matrix
Water Water Water Water Water Water Water Water Water
Comments
XX XX XX XX XX XX XX XX XX
CHAIN OF CUSTODY cooler id no.
Relinquished By:
Date Time
Received By:
/Z -3
r \iJf - l r
Cooler Temp. (^C)
Date
Time
loot?
PROJECT REQUIREMENTS
(Results Deadline: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data
1__ Other:
|
Sample Lot#:
< 2 )-< 4 n \
STL Chicago internal Sample Custody Transfer Record
Client: (}J
QO H
Sample No.
; /% - f---- f"
Analysis
/
Relinquished by: sA a y *a --
Received by:
Date
______7_7_i_s_____ _
I_ _________
(/
Time
Comments
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CASE NARRATIVE
STL Chicago Wet Chemistry Case Narrative
Client: Job #:
Weston Solutions, Inc, 232473
Date Rec'd: 12/04/04
1. This narrative covers the analysis o f the samples in the above Job # for TSS and TDS by the methods cited on the Laboratory Test Results pages.
2. The analysis was done within the EPA holding times. Refer to the Laboratory Chronicle Page for dates o f sampling, receipt, and analysis.
3. The method blanks were less than the reporting limits.
4. The LCS recoveries were within acceptance limits.
5. The matrix QC done on these samples was within control limits. See the Quality Control Results page for details of all matrix QC and non-matrix QC.
Diane L. Harper Wet Chemistry Section Manager
Date V21
RAW DATA
*** (UK LOG
<VZ )
Page 1
23
*** QC Sinmery
***
<V2 )
Solids, Total Suspended (TSS)
Method Code..: 160.2 Batch Code.**; 156402 Status...... ; RPT
Batch Date... Batch Time...
User Name___
12/07/04 1446
rnm
OC Code....... : $TD Cale Code..... : TSS
Location Code.. : 57222
Grp Smp Sample ID
Pos Test Result
Known
Originai
1 1 ___HB__
7 TSS 1.67
1 2 ___LCS_I04LSTSS1_1
7 TSS 201.00
200
1.67
1 15 23 24 73 _ 3 _ M D _ 5
7 TSS 10.00
10.50
1 16 232473_3_H5104KSTSS2C_5
7 TSS 103.00
100
10.50
Report Date; 12/7/04 15:09 Equipment Code.: Iitport Code___ :
Alternate QC Re$ F QC Res F
100 0.50000
92
Page 1
4
*** RAW TEST DATA
***
(V2 )
Solids, Total Suspended CTSS)
Method Code.. : 160,2 Batch Code : 136402 Status___ : RPT
Batch Date...: 12/07/04 Batch Time...: 144B User Name.,,.: rnm
SAMPLE:
Grp Pos Sample ID
11
MB
12
LCS I04LSTSS1 1
1 3 232473 1
1 4 232473 2
1 5 232473 3
1 6 232473 4
1 7 232473 5
1 8 232473 6
1 9 232473 7
1 10 232473 S
1 11 232473 9
1 12 232484 1
1 13 232484 2
1 14 232484 3
1 15 232473 3 MD 5
1 16 232473 3 MS I04KSTS52C 5
QC Code...
- STD
Calc Code. .... : TSS
Location Code..: 57222
Di lut ion
ID Text
IWGT 9
0.1091 0.1159
0.1141 0.1145
0.1114 0.1127 0.1086 0.1147
0.1146 0.1144
0.1062 0.1144
0.1083 0.1099
0.1161 0.1162
Report Date: 12/7/04 17:18
Equipment Code.: Inport Code ___ :
UT1
9
0.1095 0.1560 0.1159 0.1186 0.1136 0.1139 0.1100 0.1185 0.1162 0.1155 0.1066 0.1183 0.1132 0.1142 0.1183 0.1262
UT2
9
0.1096 0,1561 0.1157 0.1184 0.1135 0.1138 0.1098 0.1184 0.1160 0.1155 0.1064 0.1181 0.1130 0.1140 0,1181 0.1265
WT3 9
Page 1
RAW TEST DATA
**#
(V2 )
Solids, Total Suspended (TSS)
Method code.. 160.2
Batch Code ... 136402
Status....
KPT
Batch Date...: 12/07/04 Batch Timo...: 1443
User Name___ : m m
SAMPLE:
Grp Pos Sample ID
11
MB
12
LCS I04LSSS1 1
1 3 232473 1
1 4 232473 2
1 5 232473 3
1 6 232473 4
1 7 232473 5
1 3 232473 6
1 9 232473 7
1 10 232473 $
1 11 232473 9
1 12 232434 1
1 13 232484 2
1 14 232484 3
1 15 232473 3 MD 5
1 16 232473 3 HS I04KSTSS2C 5
OC Code... Calc Code.
Location Code..
STD
TSS 57222
Di tut ion
ML mL
TSS mg/L
300 1.67
200 201.00 200 8.00
200 19.50 200 10,50 200 5.50 200 6,00 200 18.50 200 7,00
200 5.50 200 1.00 200 18.50 200 23.50
200 20.50 200 10.00 100 103.00
Report Date: 12/7/04 17:1$
Equipment Code.: Import Code ... :
FWGT
9
0,1096 0.1561 0.1157 0.1184 0.1135 0,113$ 0.109$ 0.1184 0.1160 0.1155 0.1064 0,1181 0.1130 0.1140 0,1181 0.1265
dlfac
N/A
0.67 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 2.00
Page 2
Sir
- ti_ C h i c a g o
*1 .1 Suspended / Total VoUlin S o lid * (ITSS / IVSSl
T0 * *
L *b N tB * te h #
Mtthod U*d: T S S -S 160.2; SM 25400
A' V S S -E 160.4; SM 2540E g' prinking Water
Calculation*: TSS mg/t = (A - B) / C x 1,000,000 mg/L [gross(g) - tare(g)] / vot(ml) x 1,000,000
Calculation*: VSS mg/L = ( A - D ) / 0x1,000,000
P a g .* Book*
C 57
^>7T7
A * P * m OW> 4 O y R ew du* V A (a) > - P * r i 0 * * T f VMt (fl)
C -Sampto Volume (mi) D Part D iih fR h Mo* afar ignition (a)
,
m.-,Ovan
Initial Temp
Final Tamp, m Lz c
Balance #:: / j
Desiccator#:
sam ple #
Crue. Sample ID Vol. (ml)
M-MB L
Tare B (0)
1st A (a)
Muffle Furnace #: \ Furnace Temp.: \ ^r
2nd 3rd A or D I TSS I v s s A (Onto) I Result Result (s) I (mod) I (mflIL)
% Rec RP0
m.
- 'an/atoo
\0Jn i, l& jP S .
Y, V / T / \ f a \ & / & ? _ > 7 / 3 9 i / i h v s
200 ! 0J/&D 'Qjofg
~> Vl2r\2pF\e $ j> 4/tf W % 7
i
9 j w x y y
-3
w v & t
WtJ<c<r
W o d \ & J < & ^ A o \m?ym\?jj ?>jbDo\\a,/j //vYYr \\&o,ji/. }
'0?
J b 99 )6 .M
VJsij. \\ m ) \0.pJL J /T
- .. i----------
if
f
1
!
!
}
r" -- 4 ^ ~-- --
_______________ I___ J _____L ________ 1_________ 1________ ___________ , I
111
1!
i
-- ____________________ ______________________________________________I______________ !______________ L . _______ __________
Ovan Ttan*
bfjr/Di& Ux. 10
^ ^ 7 7 1 mo".\:....
Ovan Tima: O u t ^
f - - '^ V
ample *
Mjvw
sSppiking Levels (m g/D
\ ~m
il\%
i HiS
!
Stock Soin, I ID# (LCS) ;
Stock Soin. Il ID# (MS) :
Spiking Calculation:
ai
jl
,1-,Vv 0i<'' 7
{Cone, of Stock S oin. (mg/L) x Val, of Stack Soin, addad (mto))
Vol. or aampi u**d (mis)
i '- 'i
Analyst Signature:
Reviewer Signature: HI+22-12-001/E-OOXM
typ/cyf
27
SoLids, Total Dissolved (TDS) Method Code..: 160.1 Batch Code...: 136637
ros
*** RUN LOG
**#
status.... Batch Date.
Batch Time.
12/09/04 1125
User Name___ oc Code..... Calc Code..,,,,
TEST COPE
STD TDS
T D S
(V2 )
12/9/4 11:34
Location Code..: 57222 Equipment Code.: Import code___ :
SAMPLE: Grp Pos SampLe ID
11
___MB__
12
LCS I04LSTTS1 1
13
232370 6
14
2 3 23 78 1____
15
23237B_2____
16
2 3 23 78 3____
17
232378 4
18
23237S_5____
19
232378Ji____ .
1 10 2 3 23 78 7____
1 11 232378 8____
1 12 2 3 2 3 7 8 ____
1 13 232473J ___ ^
1 14 232473^2____
1 15 232473_3____
1 16 2 3 24 73 4____
1 17 23 24735____
1 18 232473 6___ ,
1 19 232473_7u___
1 20 23Z473_B____
1 21 232473 9____
1 22 23 24 73 J> _M D_ 21
1 23 232473_9_MS^I04LSTTS1_21
1 24 23 244DJ____
D i lution
TEST POS 7 Date / Time 12/8/04 1400 0 12/8/04 1403 0 12/8/04 1407 0 12/8/04 1410 0 12/8/04 1413 0 12/8/04 1416 0 12/8/04 1420 0 12/8/04 1423 0 12/8/04 1426 0 12/8/04 1429 12/8/04 1433 0 12/8/04 1436 0 12/8/04 1439 0 12/8/04 1442 0 12/8/04 1446 0 12/8/04 1449 12/8/04 1452 0 12/8/04 1455 0 12/8/04 1459 0 12/8/04 1502 0 12/8/04 1505 0 12/8/04 1508 0 12/8/04 1512 0 12/8/04 1515 0
3%
QC Surinary
***
(V2 )
Solids, Total Dissolved (TDS)
Method Code.. 160.1 Batch Code... 136637
Status...... RPT
Batch Date,.. Batch Time... User Name---
12/09/04 1125 jmk
QC Code....... Calc Code..... Location code,.
STD TDS 57222
Grp Smp Sample ID
Pos Test Result
Knoun
original
1 1 ___MB__
7 TDS 0
1 2 ___LCS_l04LSTTSl_1
7 TDS 262 250 0
1 22 232473 _9_HD__21
7 TDS 84
82
1 23 232473_9_M5_I04LSTTS1_21
7 TDS 346 250 82
Report Date: 12/9/04 11:34 Equipment Code.: Import Code--- :
Alternate QC Res F QC Res F
105 2.4 106
Page 1
*** HAW TEST DATA
***
(V2 )
Solids, Total Dissolved (TDS)
Method Code.. Status......
160. 1 136637
RPT
Batch Date...: 12/09/04 ftfltch Time__ : 1125
User Name--- : jmk
SAMPLE:
Grp Pos Sample ID
11 12 13
14
15
16
17 18
19 1 10
1 11 1 12
1 13
1 14 1 15 1 16 1 17
1 ia
1 19
1 20 1 21
1 22
1 23 1 24
MB LCS I04LSTTS1 1
232370 6 232378 1
23237S 2 23237S 3 232378 4 232378 5 232378 6 232378 7 232378 8 232378 9 232473 1 232473 2 232473 3 232473 4 232473 5 232473 6 232473 7 232473 8 232473 9 232473 9 MD 21 232473 9 HS I4LSTTS1 21 232440 1
Report Date: 12/9/04 11:34
C Code.,, Calc Coda
STD TDS
Location Code..: 57222
Equipment Code.:
Imoort Code
-
D luti on
ID Text
JWGT
9
55.8042 50.0247 56.3240 50.7072 54.0118 51.7189 51.5221 55.5546 54.6916 55.7664 52.8615 54.1991 49.0821 48.3306 50.3143 51.5809 51.7609 53.8458 53.2286 52.5581 51.8601 53.6914 45.7761 51.7018
UT1
9
55.8043 50.0380 56.3409 50.7191 54.0609 51.7373 51.5431 55.5824 54,7109 55.7957 52.8617 54.2429 49.0881 48.3355 50.3196 51.5868 51.7667 53.8521 53,2341 52,5623 51.8643 53,6957 45.7931 51.7609
WT2
9
55.8042 50.0378 56.3409 50.7190 54.0607 51.7371 51.5430 55.5822 54.7110 55.7954 52.8616 54.2427 49.0880 48.3352 50.3194 51.5869 51.7664 53.8519 53,2340 52.5620 51.8642 53.6956 45.7934 51.7610
WT3 9
Page 1
30
RAW TEST DATA
Solids, Total Dissolved (TDS)
Method Code 160.1
Batch Code. T.: 136637
Status___ _
RPT
Batch Date... 12/09/04 Batch Time... 1125 User Name___ .: jmk
SAMPLE;
Grp Pos Sarrple ID
11 12 13 14
1$ 1&
17
1a
19 1 10
1 ii
1 12 1 13
1 14 1 15
1 16 1 17
1 18 1 19 1 20 1 21 1 22 1 23 1 24
MB LCS I04LSTTS1 1 232370 6
232378 1 232378 2
232378 3 232378 4
232378 5 232378 6
232378 7 232378 8
232378 9
232473 1 232473 2
232473 3
232473 4 232473 5 232473 6 232473 7
232473 8 232473 9
232473 9 MD 21 232473 9 MS I04LSTTS1 21 232440 1
QC Code....... : STD Calc Code..... : TDS Location Code*. : 57222
Dilution
ML ml
TDS mg/L
50 0 50 262 25 676 50 236 50 978 50 364 50 418 30 920 50 388 50 580 50 2
50 872 50 118
50 92 50 102 50 120 50 110 50 122 50 108 50 78 50 82
50 84 50 346 50 1184
<V2 )
Report Date: 12/9/04 11:34
Equipment Code.: Import Code...,;
FWGT 9
55.8042 50.0378 56.3409 50.7190 54.0607 51.7371 51.5430 55*5622 54.7110 55.7954 52.8616 54.2427 49.0880 48.3352 50*3194 51,5869 51.7664 53*8519 53.2340 52.5620 51.8642 53.6956 45.7934 51.7610
Page 2
31
Start Time e n d ^ e:
likteiT
STL Chicago ITS / ITDS / IS1S0 / IVDS / 1TVS
Page # Book#
LabN et Batch#
Method Usodi
CVrnS - E 160.1; SM 2540C
Calculations: TDS / T5 / IS180 mg/L = (A - S) / C x 1,000.000
A- ^ 1 0 o (R O E ) - E 1 6 0 .1 (F ie ld F ilte re d )
m g /L = [gross(g) - tare(g )] / vol(m l) x i ,0 0 0 ,0 0 0
0- !?J c 100.3; SM2S40B
C- IvnDcS//nT/VSS--EE 160,1 and 160.4; SM 2540E Calculation*: VOS / TVS
c ' Drinking Water
mg/L * (A- D)/C x 1,000.000
A *Peln Gian * Dry Rttrtue Wt *g) B =Prtn Dnh TV* Wl lg) C =Sam(H* VdU(n* (ml)
Q=Patn Drah+R***dO* tftw ignition |g
Oven #: S l^f
Tem p . IN: f t ^
Temp. OUT:
C C
S tBalance #:
ZD e s ic c a to r #:
M uffle F urn ace #: F urnace Tem p.:
Sam ple #
Teat Code
MBl -LCSj
Crud. sampl* Tare
ID Voi.
S
(ml) ---
1st A
,aL ,,,
2nd A
X -
3rd A or D
(Circle) is)
f t jS i&M&iSbfi3to f '.o&X j
TDS/ TS
IS1S0 VD3/TVS % Ree.
Result (mg/L)
Result
v h h
RPD
4
3L J 32993-7
mi\/sr-ti\us&v im&aJi/fcwwis&& vss rsvifIrCiL&iSmsHt&nI
j t/d \<t>
m m\92 \ 0
Ir a m i i m r i ^ T
W m i& .w 3 \s o A i< ) m y i? i
w w tt s
V lsC i
_ ___________J m u m m m u
jr,m \s; k z ^ r ^ ^ 9 f ^ f j y 9 i ^ 3 H
R A S H * . > 4 ______ ! / J s u
l
LCS
-- 'fO--
Analyst Slgnatun
Review er Signature:
Stock 5o(n. I ID# (LCS/MS):
> 77?/
\ Spiking C afculfltofl; Cono, of Stfc Soln. * Voi, of Stk Soln. tddU (mLl
Voi. of Sampio uHd (mLt)
O a t*
----
Date:
32
