Document oDBq2D2NNZexXyLE5KrKYRjG7
^^imz ' <rg>ATE )
team (LOT NUMBER)
*#t*ECT- WT. 2608* LBS.
ISV"'^ '' -
- ' ' '
' ''.
*J: PREPARATION NOTES: '_____
_____'______________ _______________
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i
COMT-YP JOB NAME =
vcU v ; - TYPED BY: KLW STANDARD HRS*___
EWK 12/7/81 36RT 695DM0/}
TIME
Xr-NON-BLEEDING
'EQUIP MENT
-NAME; 'BON" RED DARK
1 USE i N-CODE I ACCT
i LBS i
| LBS -
-PREP
| ir \ IF^NEtESSARY, CLEAN,. DRESS SPARKLER 6 PRE-
i L^rtfAT WITH 15* DICALITE FILTER AID
I_______ 1 777-A
J ar\ OBTAIN FOR S & 3-CHL0R0-4-AMIN0 TOLUENE-5 I
I 740--C
i L^dLFONIC ACID
I
I 3^f: OBTAIN FOR S 42 3-BYDR0XY^2~NAPHTH0IC ACID!
!I ] 82-C
|______ |
I |
iU 23 <732G> WATER INTO V-317 WEIGH & POUR IN SODIUM HYD^^CIDE^^^ ^
"TURN ON AGITATOR G STEAM &~DUMP IN FROM S 2 - CHL0R0-4-AM I N0-T0LUENE-5-SULafflj^A'I D io% /yj Z.y-7^1
Ii 42?J
7-D
I 740--C i 1_ 9
11Z&7\
1 215
//e3
3&P--
WSSL -
ON POSTAL SCALE 2-AMINO-TOLUENE-5-
FONIC ACID & ADD LOT At&eZL-
IN ACTIVATED CARBON
'
IN DICALITE, FILTER -AID
TO 214-516,.JPEG. F
WATCH FOAM
RECORD: BY_x_r_t + )/' IF NECESSARY ADJUST
+ BY SODIUM HYDROXIDE * ASSUME 5Z
j STIR 30 MIN. AT 212-214 DEG. F, THEN SHUT
i OFF STEAM . WATCH FOAM
^
NPT'E RECORD: SPARKLER PRESSURE J5l __PSI
IF NOT ZERO, NOTIFY SUPERVISOR
i CIRCULATE 15 MIN OR LONGER THRU SPARKLER
I UNTIL SOLUTION IS CLEAR I MAINTAIN AT 190-^95 DEG. F FOR S ,15.--' | RECORD- ' HT/S^.D^fU-F 6 RECORDBR/J^.D:
RECORD : START802L.TGTAL MI NJfisLCLARITY
\2UZ
ii 50 10
-584-C 113-B 777-A
7-D
1982
l
56
1
41 < 99G) WATER INTO V-10
WHEN S-13 COMPLETE, PUMP V 317 THRU
SPARKLER. MAINTAIN V-317 AT <^\ 95 DEG.F
RECORD: STARTjfjiftTOTAL MIN,,_
SAMPLE FROM HOSE. SHOW -TO
-OR OK
. ... .
iquip jIEn t
: I USE i N-CODE i ACCT
PGE 02 OF 04 CG 36 CODE RT-695-D . (0)" .1 ^LBS ; i
i LBS
I WHEN S 13 COMPLETE, CLOSE V-317 OUTLET'.'^,- 1'
tOP PUMP
,L
it; I RUN IN 7* <216G) WATER 6 HEAT TO 19Q-r^'r I .
i D F
^I
.I
i I I
I
1 I 1
CIRCULATE THRU SPARKLER UNTIL SOLUTION IS I
CLEAR
1
MAINTAIN AT 190-195 DEG*' F FOR S 19 &
1
RECORD; HT^_^___ _DEG* F & RECORDER - . * t
RECORD ; : STARTJSiTQTAL MIN^_CLARITY_4C_ I
WHEN S 18 IS COMPLETE, PUMP V-317 THRU
PARKIER INTO V-100
RUN IN 5* (9QG) WATER & HEAT TO 190-195
1
EG F
I
CIRCULATE 15 MIN THRU SPARKLER, PUMP V-317 I
U SPARKLER INTO V-100-
I
HEN MT, BLOW OUT SPARKLER INTO V-100
I
f HEAT TO 165-170 DEG* F'(TAKE 1 QT*. SAMPLE) I
I (WITH AGITATION ON) '
I
1 TEST FOR CLARITY OF SOLUTION* SHOW 1 QT* |
1 SAMPLE TO SHIFT SUPERVISOR FOR APPROVAL
l
f (EXAMPLE OF 'ACCEPTABLE CLARIFICATION OF . I
' l N-7>^C ISifAVAILABLE IN OFFICE TO COMPARE I
H> ' 1
IF 23 IS OK,- CONTINUE WITH S- 25* IF S 231
NOT ACCEPTABLE, RECLARIFY THRU SPARKLER {
IF S- 23 IS OK , REHEAT V-i 00 TO 165-170
|
DEG* T FOR S 26
I
100 .TO 16* < 1590G) .
[I
1
V-100 TO 165-170 DEG* F
i I'
!
UN IN V-324 HYDROCHLORIC4CID THRU DIRECT
\u?x\AND RINSE TN
___
28-D I 443
IR 15 MIN AT 165-170 DEG* F
I1
I ~y.
ADJ TO 50* (4970G) AT 34-38 DEG*. F '
I
I
! ** -
RECORD : TEMP__3_^r_DEG* F AND IFNECESSARY 150X330 I
57-A I
ADJ TO 34-38 DEG* F 6
Ii
RECORD : . TEMP,_________ ;DEG* F
!_____ I
57-A |__
45*' <4320G) WATER INTO V-i07
{ TURN ON AGITATOR AND- STEAM AND -DUMP IN
GANESE SULPHATE
' ^ >r .
IN BARIUM- SULPHATE
.7
TO 150-UO
F AND STIR .
ORD.': PH
0-5*5) y.;y..
H ABOVE 5.5, ADJ TO PH 5-5 OR LOWER
LFURIC ACID . 7 'ASSUME "78%
ECORD-: PH JTf / % V 1 V-
SSQ^JJOTE: IF PH BELOW 5*0, DO NOT ADJ-UPWARD
3*<r HOLD FOR S 58
-
- .* .
*' -i :
-V* f -
-
I' > 1 JS400 i; 250
1, I' t
I I
1
1
' J v, 336-B 1 -1400g|?;
65-A I .\ f -Sll I ^'47--A'^
27-D
- r;; >,
DUP050101957
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1
i iniNAitu a i i j i i\ww < j. s.*nv. *
wi t un.L
I USE AGE *33 OF 04 CG 36 CODE RT-695-D (0) ! LBS
N-CDDE i AD-CT 1 LBS
IN 47" (1 61 0G > WATER INTO. V-322 UEIGI+^ND POUR IN SODIUM HYDROXIDE
\9JJ\
DUMP,IN FROM S 3 3-HYDR0XY-2-NAPHTH0IC ACID t
I
_ LOT
\zs^\
) 1
7--D I 470
82-C ! 934
1-HYDROXY-2-NAPHTHOIC ACID ON POSTAL
NCE AND ADD LOT %S.J_UTG 70-9 DEG* F
IN BLANCOL N IN ONE TO TWO MINUTES DUMP IN -TETRASODIUM PYROPHOSPHATE 6 STIR 5 NlAU-dfe LONGER TO. DISSOLVE
I"""io"i
I I 27 *i
I
I
WEIGH SODIUM NITRITE 6 POURrlNTO V-JM-
FOR S 50
M__ H3l X\
ieSai. I
I
ADJ V-322 TO 65* <22400 AT 77-80 DEG- F 6 RECORD; TEMP.Jt#__DEG- F
SLURRY TRISULPHOIC SOAP D WITH 30 GALS WATER IN DRUM- POUR IN AND STIR 5 MIN.
16
1
180-C .1 567-B I
479-D I
725-A
39-A
20
27
8
365
160
UN IN N-725-A - FROM S 47 AFAP. INTO V-100 |
30 MIN AT 36-38 DEG- F MAINTAINING
i
+KI
RECORD: TIME STA
R_ iei_Ki__'fr:_
TEMP___
____ /DEG.
NOTE :
<1 > IF CR-, KI- ADD 20F "AS S* INCREMENTS|
HYDROCHLORIC ACID ,
ASSUME 323i
RECORD: CR_______ (+0 , KI_______ <+.)
I
(2) IF CR+, KI- ADD 20$ *AS,IS* INCREMENTS]
SODIUM NITRITE
ASSUME 33%|
RECORD: CR_____ < + ) , KI_______ < + ) TEMP____ |J.Q _ p
| j
COUPLE V-322 THRU UNDERSURFACE DISTRIBUTOR
INTO V-1003 IN 97110 MI N < USE 9/1 6 * ORIEJCE ) Slbkllkt/gm TOTAL MIN__,
RECl
53 COMPLETE STIRJ5 MIN
DTAZO,,ar_<-- )) ;
<+ >
PHj /_ <7-0-8-01 TEMP:,J?ijDEG. F <60- 65 F)
NOTE:
(i ) IF-PH IS 5-0-7-0, WEIGH AND DUMP IN
30$ "AS IS* N-7-B DILUTED TO 30 GAL
AFAP SODIUM HYDROXIDE
ASSUME 50%
<2 ) (FOR PH ADJUSTMENTS USE ONLY -DILUTED
N-28-D AND N-7-D)
ADJ TO PH 9-0-9.5 (SEE ATTACHED PH ADJ AID)
HYDROCHLORIC ACID
ASSUME 32%
2^
(1) IF PH IS- 6.5-7.0, WEIGH ^0$ AS IS
. N-7-D FOUR INTO 50 GAL WATER M/2
FULL) IN PT 6 RUN INTO CV 100 IN 15
MIN 6 RINSE IN PT, STIR 5 MIN &
RECORD : PH
____ ( 9.0-9 - 5 >
57-A ___ 28--A | 725-A 1 ___
7-D I_____-
1 1
28-D 132?
I ir
DUP050101958
:r i
EQUIP MENT
t
PAGE 04 OF 04. CG 36 CODE Rt-695-D <Q)
USE LBS
1:00
11
CONT
! 2) IF PH IS 7*0-7.5, WEIGH "354= AS IS N-7-D 1
r POUR INTO 50 GAL WATER <1/2 FULL) IN PT 6 |
I RUN INTO CV 100 IN 15 MIN. ft RINSE IN PT. j
I I STIR 5 MIN & RECORD: PH__________<9.0-9.5) 1
1 i 3) IF PH IS 7.5-8,0, WEIGH .304= AS IS N-7-D i
1 l POUR' INTO 50 GAL WATER <1/2 FULL) IN Pt & I
I .1 RUN INTO CV 100 IN 15 MIN, RINSE IN PT.
i
I | STIR 5 MIN S* RECORD: PH_,,__________ <9.0-9.5) 1
I ( 4) IF PH IS 8:0-8.5, WEIGH 1 OS AS. IS N-7-D. I
1 [ POUR INTO 50 GAL WATER <1/2 FULL) IN PT St |
I I RUN INTO CV 100- IN. 15 MIN, & RINSE IN PT, !
I ! STIR 5 MIN St RECORD: PH___ ______ <9,0-9.5) I
i \ 5) IF PH IS 8.5-3.9, WEIGH 54= AS IS N-7-D I
I *t POUR INTO *50 GAL WATER <1/2 FULL) IN PT S. |
1 i RUN iNTtfC^ 100 IN 15 MIN. S RINSE IN PT, i
i STIR 5 MIN St RECORD : PH;________ <9.0-9.5)
I.
6.) IF PH iS ABOVE *9.5, DO NOT ADJUST
i
PH_______ SODIUM HYDROXIDE ASSUME 50%1____
NOTE: ADD N-28-D IN 54= *AS IS* INCREMENTS |
TO APPROACH PH 9.0-9.5 THEN USE
LESS N-23-D HYDROXHLORIC ACID
< CONCENTRATED N-23-D St N-7-D AND TOO LOW
COUPLING TEMPERATURE CAUSES MASSTONE TO
TOO LIGHT)
SHUT OFF AGITATOR
DURING S 53 HEAT V-i07 TO 210-212 DEG, F
& SHUT OFF STEAM
NOTE: IF NECESSARY REHEAT V-i07 TO 210-
EG. F PRIOR TO START OF STRIKE
PUMP V-100 INTO V--107 IN 70-75 MIN.
i LET V-107 TEMP DROP TO 200-205 DEG, F
k%URING STRIKE THEN MAINTAIN AT 200-205 DEG.
F FOR BALANCE OF STRIKE WITH AGITATOR SHUT
OFF IN V-i 00.
CORD: STARlMn3frOTAL MlM.
HlHEN STRIKE COMPLETE, HEAT TO 210-212.DEG.
STIR 15 M;IN AT 210-212 DEG.PF
FLOOD TO '130-190* <182400. ' ' '
RECORD: PH_^L/^_<6.5-7.2) AND STOP
r AGITATOR
.
.2m
OPERATOR 02
N-CODE 1 ACCT . i LBS
7-D I______
DUP050101959
DUP050101960
DUP050101961