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Exhibit 5171.0 - Kaylo Pipe Covering Stimulation Study This exhibit is demonstrative evidence please see either Debbie Stewart or Karen Lemon for copies of the transcript and videotape. RICHARD F. SCRUGGS ALWYN H. LUCREY * SAMUEL M. MILLETTE, JR. m. juliet lawson W. STEVE BOZEMAN HAYDEN S. DENT RICHARD F. SCRUGGS, P.A. ATTORNEYS AT LAW 734 DELMAS AVENUE POST OFFICE DRAWER 1425 PASCAGOULA, MISSISSIPPI 39568-1425 June 4, 1991 601-762-6068 601-762-1207 (FAX) Ronald L. Motley, Esquire Ness, Motley, Loadholt, Richardson & Poole 151 Meetings Street, Suite 600 Post Office Box 1137 Charleston, South Caroline 29402 FEDERAL EXPRESS Re: Abrams - Asbestos Personal Injury Cases Dear Ron: Per Dick's request, please find enclosed copies of the Kaylo Air Monitoring results, photographs, etc. on the experiment that was performed in Pascagoula. Should you have any questions or need further assistance please do not hesitate to contact me. Sincerely yours. JBF:sel Enclosure Also Licensed in District of Columbia NOTES ON SAMPLING DURING THE EXPERIMENT PLAINTIFF'S EXHIBIT 5111,0 dhas. ofh'ct On Thursday, May 16, 1991, Materials Analytical Services, Inc. (MAS) agreed to perform an experiment for the law firm of Richard F. Scruggs in Pascagoula, Mississippi. The experiment was designed to see if asbestos fibers were released during the cutting/sawing of the material marked "Kaylo" (on the outer cardboard wrapping) and if released what the concentration would be. The experiment took place in a vacated/sealed office belonging to the Scruggs law firm on Saturday, May 18, 1991 in Pascagoula, Mississippi. Alan Segrave of MAS performed air/dust sampling before, during and after the cutting of the asbestos containing product labelled "Kaylo". Protective clothing and respiratory protection were utilized for the experiment. The experiment involved establishing ambient levels of asbestos in the air by taking air samples outside the contained area. These samples were taken at 10 liters/minute flow rate and were labelled 1, 2 and 3. Results of these three air samples analyzed by transmission electron microscopy (TEM) were negligible. Air samples (4,5,6) were run inside the contained area, (while the material marked "Kaylo" was sealed in plastic) at 10 liters/minute flow rate. Again the samples were analyzed by TEM and the asbestos concentrations were negligible. Samples 1-6 represent levels of possible contaminants inside and outside the containment area before the "Kaylo" material was cut. Samples 7, 8, and 9 (at 10 liters per minute flow rate) and IP, 2P at (2 liters per minute flow rate) were taken as the "Kaylo" was removed from the bag and placed on the sawhorse. IP and 2P represent personnel air samples taken on Alan Segrave and John, who is the person designated to cut the "Kaylo". A series of cuts into the "Kaylo" were made using a hand saw, -and clouds of material were liberated into the air. Other actions simulating what a worker might do during the cutting were performed such as brushing one's arm off, tapping the saw with the hand to clean it, etc. 9d 800 Ifrsfrl 82-80-tGGl Page 2 After the last cut was made all physical activity in the area ceased while the sampling continued for approximately ten minutes. Samples 10, 11, 12 (at 10 liters/minute flow rate) and personnel samples 3P, 4P (at 2 liters/minute flow rate) were taken as the material was swept into piles and placed in plastic bags. During the cutting and sweeping portions of the experiment significant asbestos concentrations were measured by TEM analyses. In addition to the air samples taken, dust samples (1, 2, 3) were taken to measure dust that may have fallen into precleaned containers of a known area. Dust sample 1 was voided due to the fact that during the sweeping of material a significant amount of material was swept into the dust container. Dust sample 2 is representative of the material that was settling out of the air and after TEM analysis was performed, significant levels of asbestos were found to have settled into the tin. Dust sample 3 represents a sealed tin taken to the project (inside the containment, etc.) and back to the lab. No asbestos structures were found in dust sample 3. Od GOO Sfrtfrl G2-G0-IGGI AIR MaJTTORING SERVICES * COPY May 24, 1991 Mr. Richard Scruggs Richard F. Scruggs Law Firm, PA P.O. Drawer 1425 Pascagoula, MS 39568 Dear Mr. Scruggs: Enclosed are the analyses of the air samples received at our facility on May 19, 1991. The samples were sent under your job/purchase order number: Kaylo Experiment, and were labelled: 1 OWA 2 OWA 3 OWA 4 IWA 5 IWA 6 IWA 7 IWA 8 IWA 9 IWA 10 IWA 11 IWA 12 IWA Please call our office at your convenience should you have any questions concerning the analyses of your samples. Sincerely, WEL:lac Enc. Ref: M6366 3597 Parkway Lane Suite 250 Norcross, Georgia 30092 (404) 448-3200 FAX (404) 368-8256 CLIENT NAME: Richard Scruggs Law Firm CLIENT JOB NAME: Kaylo Experiment MAS JOB: M6366 MAS SAMPLE NUMBER SUMMARY OF AIR SAMPLE LOCATIONS 1 2 3 4 5 7 8 9 10 11 12 1, 5/18/91, Background, outside containment 2, 5/18/91, Background, outside containment 3, 5/18/91, Background, outside containment 4, 5/18/91, Inside containment, before cutting 5, 5/18/91, Inside containment, before cutting 6, 5/18/91, Inside containment, before cutting 7, 5/18/91, Inside containment, during cutting 8, 5/18/91, Inside containment, during cutting 9, 5/18/91, Inside containment, during cutting 10, 5/18/91, Inside containment, during sweeping/cleanup 11, 5/18/91, Inside containment, during sweeping/cleanup 12, 5/18/91, Inside containment, during sweeping/cleanup Summary of Results of Analyses by Transmission Electron Microscopy, (TEM) Client Job Name: Kaylo Experiment MAS Job Number: M6366 MAS Sample Number: Number of Asbestos Structures Counted Asbestos Concentration, Structures per Cubic Centimeter 12 21 30 49 51 62 7 103 8 101 9 52 10 101 11 103 12 73 0.135 0.058 <0.079 0.352 0.042 0.073 931.7 281.0 91.4 1084.8 79.3 252.7 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 1 OWA M6366-1 05/19/91 05/24/91 AI1^ 0 >' RVfyWj?,r, <J KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 520 1 47MM Plastic 1.34E+09 /xm2 10 2 7612 nra2 76120 /xm2 20000X 1:2.0 Analytical Sensitivity: 0.068 Asbestos Structures/cc 13.137 Asbestos Structures/mm2 Area Examined < 5 /xm > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 1 0 0 1 0 0 0 0 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 0 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.135 0.000 Total Structures/mm sq = 26 Structures/cc <5 > 5 /Ltrn 0.068 0.000 0.000 0.068 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. * 0.000 display = Below Analytical Sensitivity ''SO* MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of l Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Pro^/ref: RICHARD SCRUGGS 1 OWA M6366-1 05/19/91 05/24/91 AIR RW_^.g Li< SM T11TLtZ-y, KAYIX3 EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 520 1 47MM Plastic 1.34E+09 /XItl2 10 2 7612 ^m2 76120 [m2 20000X 1:2.0 Length Microns Width Microns Photo ID 1 1-2 chr 2 2-3 chr f m 0.50 3.50 0.05 1.80 Types W r" amo - cro non - Chrysotile Amosite Crocidolite Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 2 OWA M6366-2 05/19/91 05/24/91 AIR WS fn-Lut*', \ XiCTM* KAY-LO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 550 1 47MM Plastic 1.34E+09 Mm2 10 2 8331 /im2 83310 /Ltm2 20000X 1:2.0 Analytical Sensitivity: 0.058 Asbestos Structures/cc 12.003 Asbestos Structures/mm2 Area Examined < 5 fxm > 5 fj,m No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 0 0 0 0 0 1 0 0 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 0 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.058 0.058 Total Structures/mm sq = 12 Structures/cc < 5 fj.ro. > 5 fxra. 0.000 0.000 0.000 0.000 0.000 0.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 1 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 2 OWA M6366-2 05/19/91 05/24/91 AIR WS //JlU'fAh-7 KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 550 1 47MM Plastic 1.34E+09 jum2 10 2 8331 /zm2 83310 ]Um2 20000X 1:2.0 Length Microns Width Microns Photo ID 1 1-2 chr b 12.00 0.30 Types ,<r ^ r - Chrysotile ant - Anthophyllite amo - Amosite tre - Tremolite cro - Crocidolite act - Actinolite non - Non-Asbestos Structures f - Fiber b - Bundle c - Cluster m - Matrices  MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 3 OWA M6366-3 05/19/91 05/24/91 AH KAYLO experiment Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 430 1 47MM Plastic 1.34E+09 /xm2 10 2 7920 fMTtl2 79200 jum2 15709X 1:2.0 Analytical Sensitivity: 0.079 Asbestos Structures/cc 12.626 Asbestos, Structures/mra2 Area Examined < 5 /urn > 5 jum No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 0 0 0 0 0 0 0 0 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 0 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.000 0.000 Total Structures/mm sq = 0 Structures/cc < 5 /im > 5 jum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. v. * 0.000 display = Below Analytical Sensitivity J/f' MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro^/ref: RICHARD SCRUGGS 4 OWA M6366-4 05/19/91 05/24/91 AIR MM KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area : Tot Area Examined : Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 /im2 10 2 7878 /zm2 78780 fxrn2 20000X 1:2.0 Analytical Sensitivity: 0.039 Asbestos Structures/cc 12.694 Asbestos Structures/mm2 Area Examined No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: < 5 /xm 6 0 0 1 > 5 /xm 0 1 0 0 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 1 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.352 0.078 Total Structures/mm sq = 114 Structures/cc < 5 jum > 5 nm 0.235 0.000 0.000 0.039 0.000 0.039 0.000 0.000 0.000 0.000 0.000 0.000 0.039 0.000 0.000 0.000 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing /f one asbestos fiber or structure in the total area examined. * 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 1 Client: RICHARD SCRUGGS Sample ID: 4 OWA MAS Log Number: M6366-4 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR Microscoplst: MM rnsJipUJ. rtidT.oyh.-L' u^) Reviewed by: J\ . Client Proj/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sg. Area: Tot Area Examined: Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 jlim2 10 2 7878 jum2 78780 /xm2 20000X 1:2.0 Length Microns Width Microns Photo ID 1 1- 2 chr f 1.20 0.05 2 1- 3 chr f 3.60 0.15 3 1- 4 chr f 1.30 0.09 4 chr f 0.70 0.10 5 chr f 1.20 0.02 6 2- 4 amo f 5.80 0.60 7 chr f 1.40 0.10 8 chr m 2.30 0.50 9 chr b 12.00 2.20 Types U . .r - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro]/ref: RICHARD SCRUGGS 5 IWA M6366-5 05/19/91 05/24/91 AH KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 jum2 10 2 7396 nm2 73960 /im2 15709X 1:2.0 Analytical Sensitivity: 0.042 Asbestos Structures/cc 13.521 Asbestos Structures/mm2 Area Examined < 5 /Lim > 5 jtim No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 0 0 0 0 0 0 0 1 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 0 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.042 0.042 Total Structures/mm sq = 14 Structures/cc < 5 /mi > 5 /un 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 1 Client: Sample ID: MAS Log Number: Sample Received Sample Due Date Type Analysis: Microscoplst: Reviewed by: Client Pro]/ref RICHARD SCRUGGS 5 IWA M6366-5 05/19/91 05/24/91 aAIR AH MKAY EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 {m2 10 2 7396 jum2 73960 /im2 15709X 1:2.0 Length Microns Width Microns Photo ID 1 1-3 chr m 9.00 7.50 Types ir amo cro non - Chrysotile Amosite Crocidolite Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Prou/ref: RICHARD SCRUGGS 6 IWA M6366-6 05/19/91 05/24/91 AIR , / iJs,.JK ^ ICr^', .... (J.ij' KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 /im2 10 2 8419 /im2 84190 /xm2 20000X 1:2.0 Analytical Sensitivity: 0.037 Asbestos Structures/cc 11.878 Asbestos Structures/mm2 Area Examined < 5 fim > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 0 0 1 1 0 0 0 0 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 0 0 0 0 0 0 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 0.073 0.000 Total Structures/mm sq = 24 Structures/cc < 5 /xm > 5 fxm 0.000 0.000 0.037 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 1 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 6 IWA M6366-6 05/19/91 05/24/91 AIR * ;/ JK X. //./AixZ KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 870 1 47MM Plastic 1.34E+09 /Lim2 10 2 8419 /m2 84190 /im2 20000X 1:2.0 Length Microns Width Microns Photo ID 1 1-4 2 2-5 chr chr c m 2.10 1.60 1.20 1.40 Types f r - Chrysotile ant - Anthophyllite amo - Amosite tre - Tremolite cro - Crocidolite act - Actinolite non - Non-Asbestos Structures f - Fiber b - Bundle c - Cluster m - Matrices MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro}/ref: RICHARD SCRUGGS 7 IWA M6366-7 05/19/91 05/24/91 AIR j. i (/'' fir KAA1yLOIEXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 330 1 47MM Plastic 1.34E+09 /xm2 6 2 7482 /xm2 44892 /xm2 15709X 1:100.0 Analytical Sensitivity: 9.045 Asbestos Structures/cc 22.276 Asbestos Structures/mm2 Area Examined < 5 fim. > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 53 4 1 20 2 3 0 3 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 11 0 0 1 4 1 0 0 Total Asbestos Structures/cc (All): 931.664 Total Asbestos Structures/cc (>5 ): 117.589 Total Structures/mm sq = 2294 Structures/cc < 5 /xm > 5 /xm 479.400 36.181 9.045 180.906 18.091 27.136 0.000 27.136 99.498 0.000 0.000 9.045 36.181 9.045 0.000 0.000 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of Client: RICHARD SCRUGGS Sample ID: 7 IWA MAS Log Number: M6366-7 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR / Microscoolst: AH fO(.hj^y\ Reviewed bv: A. Client Pro]/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 330 1 47MM Plastic 1.34E+09 fj,m2 6 2 7482 fim2 44892 /J,m2 15709X 1:100.0 Length Microns Width Microns Photo ID 1 2 3 4 5 6 7 8 9 r 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 1-1 1- 2 chr chr chr chr amo amo chr. chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo amo chr chr chr chr chr f f f f f f f b c ra b f m f m f f f f m m f m f f f f f m f m f 2.50 1.00 0.70 2.50 1.80 2.20 3.00 2.50 4.00 4.00 4.00 2.00 1.80 3.50 1.50 1.00 1.20 1.20 2.50 2.50 1.80 0.80 2.00 1.60 3.50 1.60 3.50 1.20 2.00 1.80 2.50 1.00 0.04 0.04 0.03 0.03 0.30 0.20 0.03 0.20 1.20 3.50 0.15 0.05 1.50 0.05 1.00 0.05 0.05 0.03 0.04 2.00 0.50 0.04 0.50 0.05 0.05 0.20 0.30 0.04 1.20 0.05 2.00 0.03 M5150 Types *r - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc. Page: 2 of Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 7 IWA M6366--7 05/19/91 05/24/91 AIR AH . (,,MtM11a,/yyvM>-- --AIL KA&LO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 330 1 47MM Plastic 1.34E+09 /xm2 6 2 7482 /Ltm2 44892 /m2 15709X 1:100.0 Length Microns Width Photo Microns ID 33 chr f 0.70 0.03 34 amo f 4.00 0.50 35 amo f 1.80 0.20 36 chr b 1.50 0.40 37 chr f 1.80 0.03 38 chr m 6.50 3.00 39 1- 3 chr f 2.00 0.05 40 chr f 0.80 0.04 41 chr f 2.00 0.05 42 chr m 2.00 1.50 43 chr f 2.00 0.05 44 chr f 4.00 0.05 45 chr f 0.70 0.03 46 chr b 2.50 0.15 47 amo b 18.00 0.80 48 amo f 2.80 0.50 49 chr f 2.20 0.05 50 chr f 3.00 0.03 51 chr f 2.00 0.04 52 chr f 1.20 0.03 53 chr f 1.80 0.04 54 amo f 5.00 0.50 55 chr m 2.00 1.80 56 amo f 4.00 0.20 57 2- 1 chr m 2.00 1.20 58 amo f 6.50 0.30 59 chr f 1.80 0.04 60 chr b 15.00 0.20 61 chr f 2.20 0.03 62 chr b 6.50 0.30 63 chr m 2.50 2.00 64 chr m 2.00 0.50 65 chr f 1.50 0.03 66 chr f 1.40 0.03 67 chr b 5.50 0.15 68 chr f 0.80 0.05 69 amo f 1.80 0.20 70 chr f 8.50 0.03 Materials Analytical Services, Inc. Page: 3 of Client: RICHARDSCRUGGS Sample ID: 7 IWA MAS Log Number: M6366-7 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR // MicroscoDist: AH ^. Reviewed by: \ Client Proj/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Gri^ Sq. Area: Tot Area Examined: Screen Mac: Dilution Factor: 330 1 47MM Plastic 1.34E+09 nm2 6 2 7482 /im2 44892 /Lim2 15709X 1:100.0 Length Microns Width Photo Microns ID 72 chr f 2.50 0.05 73 2- 2 chr m 6.00 5.00 74 chr f 2.50 0.05 75 chr f 1.80 0.04 76 chr f 2.50 0.05 77 chr f 5.00 0.04 78 chr f 1.20 0.04 79 amo f 8.00 0.30 80 chr m 2.50 0.80 81 chr f 2.00 0.04 82 chr m 1.50 1.00 83 chr f 3.00 0.03 84 chr m 1.30 1.00 85 chr f 1.80 0.03 86 chr f 1.50 0.05 87 chr f 1.00 0.05 88 chr m 3.50 2.50 89 chr m 9.50 3.50 90 amo f 3.50 0.30 91 2- 3 chr m 3.50 2.00 92 amo f 22.00 0.30 93 chr f 1.80 0.05 94 chr f 1.50 0.04 95 chr f 1.20 0.03 96 chr f 2.20 0.05 97 chr f 1.20 0.04 98 chr f 2.00 0.05 99 amo m 2.50 1.50 100 amo f 3.00 0.50 101 chr f 4.50 0.05 102 chr f 4.00 0.05 103 chr m 2.00 1.50 r MATERIALS ANALYTICAL SERVICES/ INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 8 IWA M6366-8 05/19/91 05/24/91 AIR pf mliJULZaJ.`J ______ . KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 320 1 47MM Plastic 1.34E+09 Mm2 4 2 7525 Mm2 30100 Mm2 20000X 1:20.0 Analytical Sensitivity: 2.782 Asbestos Structures/cc 33.223 Asbestos Structures/mm2 Area Examined < 5 Mm > 5 Mm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 44 1 1 28 2 1 0 12 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 3 3 0 1 1 3 0 1 Total Asbestos Structures/cc (All): 281.022 Total Asbestos Structures/cc (>5 ): 55.648 Total Structures/mm sq = 3355 Structures/cc < 5 M > 5 Mm 122.425 2.782 2.782 77.907 5.565 2.782 0.000 33.389 8.347 8.347 0.000 2.782 2.782 8.347 0.000 2.782 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing ^ one asbestos fiber or structure in the total area examined. v 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of Client: RICHARD SCRUGGS Sample ID: 8 IWA MAS Log Number: M6366-8 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR , /; // Microscooist: RW .LLJ''/'sssZA Reviewed by: ^ Client Pro3/ref: KAYtO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 320 1 47MM Plastic 1.34E+09 jUItl2 4 2 7525 /xm2 30100 fm2 20000X 1:20.0 Length Microns Width Microns Photo ID 1 1- 1 chr m 4.00 1.70 2 chr m 6.00 3.00 3 chr f 3.00 0.05 4 chr f 0.60 0.05 5 chr m 7.00 5.50 6 chr f 1.70 0.05 7 chr f 1.60 0.05 8 chr f 1.50 0.05 9 chr f 4.50 0.05 10 chr m 4.50 2.00 11 chr f 1.00 0.05 12 amo b 9.00 0.30 13 amo b 2.20 0.30 14 chr m 9.00 4.50 15 amo m 2.20 1.00 16 chr m 5.00 1.60 17 chr m 2.70 2.40 18 chr f 0.70 0.05 19 chr m 9.50 8.50 20 chr m 2.50 2.50 21 1- 2 chr m 4.50 1.70 22 chr f 1.60 0.05 23 chr m 1.60 0.50 24 chr f 0.50 0.05 25 chr c 1.60 1.00 26 chr f 1.10 0.05 27 chr m 3.50 1.80 28 chr m 1.00 0.70 29 amo b 11.50 0.35 30 chr f 0.70 0.05 31 chr f 0.80 0.02 32 chr f 0.70 0.05 Types xr - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc Page; 2 Of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 8 IWA M6366-8 05/19/91 05/24/91 AIR . // ^ \L ____ KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area : Tot Area Examined : Screen Mag: Dilution Factor: 320 1 47MM Plastic 1.34E+09 /im2 4 2 7525 lim2 30100 /zm2 20000X 1:20.0 Length Microns Width Microns 33 chr f 1.60 0.05 34 chr m 10.00 4.00 35 chr m 3.00 1.00 36 chr f 0.50 0.05 37 chr m 3.00 2.50 38 amo b 15.00 0.50 39 amo b 2.50 0.40 40 chr m 2.00 1.50 41 chr f 0.50 0.05 42 2- 1 chr m 4.20 2.00 43 chr m 3.50 3.00 44 chr f 0.70 0.05 45 chr m 2.00 1.00 46 chr m 3.50 2.20 47 chr f 1.40 0.05 48 chr m 3.00 2.20 49 chr m 3.50 2.00 50 chr f 1.70 0.08 51 chr f 3.00 0.05 52 chr m 5.50 5.00 53 chr f 1.50 0.05 54 amo f 11.50 0.20 55 chr m 4.20 4.00 56 chr f 2.40 0.05 57 chr f 2.30 0.05 58 chr f 7.50 0.05 59 chr f 1.60 0.05 60 chr m 6.00 5.50 61 chr m 2.50 1.20 62 amo f 3.00 0.15 63 chr f 0.70 0.02 64 chr f 5.50 0.05 65 chr f 1.20 0.05 66 chr b 0.70 0.15 67 amo m 13.50 12.50 68 amo f 3.50 0.20 69 chr m 3.00 2.30 70 amo f 2.30 0.20 71 chr f 1.00 0.05 Materials Analytical Services, Inc. Page: 3 Of 3 Client: RICHARD SCRUGGS Sample ID: 8 IWA MAS Log Number: M6366-8 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR r /, - Microscoplst: RW Reviewed by: Key, Client Pro]/ref: KAtfLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 320 1 47MM Plastic 1.34E+09 \lm2 4 2 7525 im.2 30100 HT0.2 20000X 1:20.0 Length Microns Width Photo Microns ID 72 chr f 2.50 0.05 73 2- 2 chr m 2.00 1.50 74 chr m 10.50 4.00 75 chr m 4.20 2.50 76 chr f 1.50 0.05 77 chr f 3.00 0.05 78 chr f 0.70 0.05 79 chr m 7.00 4.50 80 chr b 6.00 0.20 81 chr f 1.60 0.05 82 chr f 1.70 0.05 83 chr f 0.80 0.05 84 chr m 2.00 1.50 85 chr m 10.00 3.00 86 chr f 1.70 0.05 87 chr f 2.50 0.05 88 chr m 2.20 1.50 89 chr f 1.00 0.05 90 chr f 0.60 0.05 91 chr m 5.50 4.00 92 chr m 2.20 1.00 93 chr f 1.20 0.05 94 chr f 1.80 0.05 95 chr ra 1.00 0.50 96 chr f 0.70 0.05 97 chr m 4.00 2.00 98 chr f 1.80 0.05 99 chr m 1.70 1.60 100 amo b 2.50 0.70 101 chr f 0.50 0.05 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro^/ref: RICHARD SCRUGGS 9 IWA M6366-9 05/19/91 05/24/91 AIR KA-YLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 310 1 47MM Plastic 1.34E+09 /zm2 10 2 8117 /um2 81170 jum2 20000X 1:33.0 Analytical Sensitivity: 1.757 Asbestos Structures/cc 12.320 Asbestos Structures/mm2 Area Examined < 5 /zm >5 /zm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 23 0 0 19 0 0 0 3 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 3 0 0 0 2 0 0 2 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 91.383 12.302 Total Structures/mm sq = 641 Structures/cc < 5 /zm > 5 /zm 40.419 0.000 0.000 33.390 0.000 0.000 0.000 5.272 5.272 0.000 0.000 0.000 3.515 0.000 0.000 3.515 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 2 Client: RICHARD SCRUGGS Sample ID: 9 IWA MAS Log Number: M6366-9 Sample Received: 05/19/91 Sample Due Date: 05/24/91 , Type Analysis: AIR yV Microscooist: SF Reviewed bv: >1 Client Pro3/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 310 1 47MM Plastic 1.34E+09 fJiTti2 10 2 8117 m2 81170 m2 20000X 1:33.0 Length Microns Width Microns Photo ID 1 1-1 chr m 1.80 1.50 2 chr m 1.40 0.40 3 chr m 2.90 2.60 4 1-2 chr f 2.70 0.05 5 chr f 1.90 0.07 6 chr f 3.90 0.05 7 chr f 2.40 0.07 8 chr f 1.60 0.05 9 chr m 1.20 1.10 10 1- 3 chr m 1.00 0.30 11 amo f 4.70 0.20 12 chr f 0.50 0.03 13 chr f 1.00 0.07 14 1- 4 chr m 2.80 1.70 15 chr f 0.90 0.07 16 chr m 1.40 0.30 17 chr m 2.20 1.10 18 chr f 2.80 0.07 19 chr f 1.00 0.03 20 amo f 1.00 0.18 21 1- 5 chr m 3.00 2.00 22 chr f 3.30 0.05 23 chr f 1.70 0.05 24 chr m 2.50 1.80 25 amo f 18.40 0.40 26 chr m 3.40 2.90 27 chr f 2.20 0.07 28 2- 1 amo f 2.70 0.10 29 chr f 1.00 0.05 30 chr f 0.80 0.05 31 amo m 6.20 3.70 32 chr m 2.00 1.60 Types .r - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophy11ite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc. Page: 2 of 2 Client: RICHARD SCRUGGS Sample ID: 9 iwa MAS Log Number: M6366-9 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR Microscoplst: SF Reviewed by: Client Proj/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 310 1 47MM Plastic 1.34E+09 /xm2 10 2 8117 /xm2 81170 fxm2 20000X 1:33.0 Length Microns Width Microns 33 chr m 6.60 4.60 34 chr m 5.40 1.70 35 2- 2 chr m 2.10 0.90 36 chr m 2.00 1.50 37 chr f 1.20 0.03 38 chr m 2.00 1.00 39 chr f 0.90 0.07 40 chr f 3.30 0.05 41 chr m 1.60 0.60 42 2- 3 chr f 3.30 0.10 43 chr m 0.90 0.70 44 chr f 4.70 0.05 45 2- 4 chr f 0.60 0.05 46 chr m 3.60 2.70 47 chr f 1.90 0.10 48 chr f 0.60 0.07 49 chr m 5.30 3.60 50 2- 5 chr m 1.60 0.60 51 amo m 5.50 4.60 52 amo f 12.10 0.60 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: RICHARD SCRUGGS Sample ID: 10 IWA MAS Log Number: M6366-10 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR / Microscopist: Reviewed by: Client Prcg/ref: KAYLb EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 180 1 47MM Plastic 1.34E+09 Mm2 9 2 7701 Mm2 69309 Mm2 20000X 1:100.0 Analytical Sensitivity: 10.741 Asbestos Structures/cc 14.428 Asbestos Structures/mm2 Area Examined No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: < 5 Mm 37 2 0 45 > 5 Mm 1 0 0 5 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 3 0 0 1 5 1 0 1 Total Asbestos Structures/cc (All): 1084.836 Total Asbestos Structures/cc (>5 ): 139.632 Total Structures/mm sq = 1457 Structures/cc <5 Mm > 5 Mm 397.415 21.482 0.000 483.343 10.741 0.000 0.000 53.705 32.223 0.000 0.000 10.741 53.705 10.741 0.000 10.741 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. * 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: l of 3 Client: RICHARD SCRUGGS Sample ID: 10 IWA MAS Log Number: M6366-10 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR </ Microscoolst: J.K \ Reviewed bv: 1 lift Client Pro}/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 180 1 47MM Plastic 1.34E+09 jim2 9 2 7701 69309 [m2 20000X 1:100.0 Length Microns Width Microns Photo ID 1 1-1 chr f 0.50 0.05 2 chr m 3.60 2.60 3 chr f 0.70 0.05 4 chr f 0.70 0.05 5 chr m 3.00 1.10 6 chr f 0.60 0.05 7 chr m 1.20 0.40 8 chr m 2.20 1.60 9 chr m 1.20 0.60 10 chr f 3.80 0.05 11 chr m 2.60 2.00 12 amo f 10.40 0.35 M31747 13 chr f 1.00 0.05 14 chr f 4.40 0.08 15 1- 2 chr m 3.60 1.20 16 chr m 3.00 1.80 17 chr m 3.20 1.80 18 chr m 6.50 4.00 19 chr m 4.80 2.20 20 1- 3 chr f 1.50 0.05 21 chr m 3.00 2.80 22 chr m 1.80 1.00 23 chr m 1.80 1.70 24 chr m 1.50 1.20 25 chr m 1.60 1.00 26 chr f 1.70 0.08 27 amo f 1.00 0.20 28 chr m 1.80 1.60 29 chr m 1.80 1.00 30 1- 4 chr f 6.20 0.05 31 amo f 13.80 0.60 32 chr m 4.80 3.80 Types .xr - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc. Page: 2 Of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro^/ref: RICHARD SCRUGGS 10 IWA M6366-10 05/19/91 05/24/91 AIR V, I / JK A Hz KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 180 1 47MM Plastic 1.34E+09 jum2 9 2 7701 fJLm2 69309 /zm2 20000X 1:100.0 Length Microns Width Photo Microns ID 33 amo f 5.20 0.55 34 chr m 4.40 1.80 35 chr f 0.60 0.05 36 chr f 4.40 0.08 37 chr m 1.10 0.40 38 chr b 3.60 0.10 39 1- 5 chr m 2.80 2.20 40 chr m 3.00 1.60 41 chr m 2.70 1.60 42 chr m 2.40 1.80 43 chr m 1.90 0.80 44 chr m 2.00 1.60 45 chr f 2.00 0.08 46 chr f 1.00 0.05 47 chr f 1.70 0.05 48 chr m 1.40 1.20 49 chr f 0.80 0.05 50 chr f 2.20 0.08 51 chr f 0.60 0.10 52 chr m 5.00 3.80 53 chr f 1.20 0.10 54 chr m 5.20 4.80 55 amo f 15.00 0.25 56 2- 1 chr f 2.80 0.05 57 chr f 2.40 0.08 58 chr m 2.80 1.80 59 chr f 1.60 0.05 60 chr f 1.00 0.05 61 chr m 1.70 1.60 62 chr m 0.90 0.50 63 chr m 1.20 0.60 64 2- 2 chr m 2.10 1.00 65 chr m 2.10 0.60 66 chr m 3.00 2.80 67 chr f 1.00 0.05 68 chr f 1.20 0.05 69 amo f 1.70 0.30 70 chr m 2.70 1.80 71 chr f 0.80 0.10 Materials Analytical Services, Inc. Page: 3 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Mxcroscopist: Reviewed bv: Client Proj/ref: RICHARD SCRUGGS 10 IWA M6366- 10 05/19/91 05/24/91 AIR JR i*\ i / `3A --KAYLO'f EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 180 1 47MM Plastic 1.34E+09 nw2 9 2 7701 2 69309 /Ltm2 20000X 1:100.0 Length Microns Width Photo Microns ID 72 amo m 18.00 8.00 73 chr f 1.00 0.03 74 chr f 1.60 0.05 75 chr f 1.70 0.05 76 2- 3 chr m 2.20 2.00 77 chr m 2.80 1.60 78 chr m 1.20 0.40 79 chr f 1.60 0.08 80 chr f 2.40 0.05 81 chr m 2.00 1.70 82 chr b 1.70 0.15 83 chr f 1.00 0.05 84 chr f 0.50 0.05 85 amo f 5.60 0.40 86 2- 4 chr f 0.50 0.03 87 chr f 0.80 0.05 88 chr f 0.70 0.05 89 chr ro 2.60 0.50 90 chr m 5.00 3.80 91 chr m 2.80 0.60 92 chr m 3.00 2.50 93 chr f 2.80 0.05 94 chr m 2.20 1.20 95 amo b 5.10 0.40 96 chr m 5.00 4.00 97 chr f 1.80 0.08 98 amo m 2.80 1.80 99 amo f 4.40 0.20 100 chr m 1.20 0.20 101 chr m 3.20 3.00 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number; Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 11 IWA M6366-11 05/19/91 05/24/91 rw^ac/Lyi/'lA 0>) KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 160 1 47MM Plastic 1.34E+09 /zm2 10 2 7182 /zm2 71820 /zm2 20000X 1:6.6 Analytical Sensitivity: 0.770 Asbestos Structures/cc 13.924 Asbestos Structures/mm2 Area Examined < 5 /zm > 5 /zm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: NO. of Chrysotile Clusters: NO. of Chrysotile Matrices: 38 9 0 36 0 2 0 5 NO. Free Amphibole Fibers: NO. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 4 2 0 2 1 3 0 1 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 79.272 9.236 Total Structures/mm sq = 1434 Structures/cc <5 /zm > 5 /zm 29.246 6.927 0.000 27.707 0.000 1.539 0.000 3.848 3.079 1.539 0.000 1.539 0.770 2.309 0.000 0.770 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 Of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Pro}/ref: RICHARD SCRUGGS Sample Volume 11 IWA Filter Type: M6366-11 Filter Area: 05/19/91 Grid Openings 05/24/91 Grids Examined: AIRp a /) j j 4 (\,c\ Avg Grid Sq. Area: RW V/'r-/-..:- Tot Area Examined: Screen Mag: KAYLO EXPERIMENT Dilution Factor: 160 1 47MM Plastic 1.34E+09 Mm2 10 2 7182 /im2 71820 Mm2 20000X 1:6.6 Strc. Grid Op Type Structure Length Microns Width Microns Photo ID 1 2 3 4 5 6 7 8 W9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 1-1 1- 2 1- 3 chr amo amo chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr chr chr chr chr chr chr f m b m m f f f m f b b m f f m m f m f f b f f f f f f m m m m 0.60 4.20 6.00 1.70 3.50 1.20 1.60 1.50 1.50 0.60 2.50 2.60 2.20 0.50 0.50 4.00 1.00 2.50 4.50 2.40 0.70 3.00 1.50 2.00 1.80 0.50 0.60 0.70 3.00 2.50 2.20 1.80 0.05 1.80 0.25 0.60 2.50 0.02 0.08 0.05 1.00 0.02 0.20 0.20 0.60 0.05 0.05 2.20 0.50 0.15 3.50 0.05 0.05 0.15 0.05 0.05 0.05 0.05 0.05 0.05 1.80 0.70 2.00 1.80 Types nr - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc. Page: 2 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: RICHARD SCRUGGS 11 IWA M6366-11 05/19/91 05/24/91 RWRfcui UiJL 04 Reviewed by: -------- O,/A*--- Client Pro]/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: 160 Filter Type: 47MM Plastic Filter Area: 1.34E+09 \m2 Grid Openings: 10 Grids Examined: 2 Avg Grid Sq. Area: 7182 im.2 Tot Area Examined: 71820 /im2 Screen Mag: 20000X Dilution Factor: 1:6.6 Length Microns Width Photo Microns ID 33 1- 4 chr m 1.60 0.60 34 chr b 3.20 0.15 35 chr m 4.50 4.00 36 chr f 0.50 0.02 37 amo m 7.00 3.50 38 chr b 2.20 0.15 39 chr f 2.30 0.05 40 chr f 1.50 0.05 41 chr m 1.50 0.70 42 1- 5 chr m 1.50 0.80 43 chr m 6.20 1.50 44 chr m 1.60 1.00 45 chr f 1.50 0.05 46 chr f 2.80 0.05 47 chr m 3.00 1.60 48 chr b 4.20 0.20 49 chr f 0.50 0.05 50 2- 1 amo b 2.40 0.25 51 chr m 5.00 3.00 52 chr f 0.80 0.05 53 chr f 1.50 0.05 54 chr f 0.60 0.05 55 chr m 1.80 1.70 56 chr f 0.60 0.05 57 chr b 1.00 0.15 58 chr f 2.00 0.05 59 amo b 10.00 0.40 60 chr f 1.00 0.02 61 chr b 10.50 0.15 62 amo b 12.50 0.40 63 2- 2 chr m 3.00 1.60 64 chr m 7.00 4.00 65 amo f 1.60 0.10 66 chr m 3.50 2.20 67 chr m 2.30 2.20 68 chr f 0.80 0.05 69 chr m 1.60 0.70 70 71 2- 3 chr chr m m 4.00 2.00 2.50 1.00 Materials Analytical Services, Inc. Page: 3 of Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: MicroscoDist: Reviewed bv: Client Pro3/ref: RICHARD SCRUGGS 11 IWA M6366-11 05/19/91 05/24/91 AIR ,-, /' j) j , RW 'K \ciV.v / OM/rf--- KAYLO" EXPERIMENT a Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mac: Dilution Factor: 160 1 47MM Plastic 1.34E+09 /im2 10 2 7182 /im2 71820 (xm2 20000X 1:6.6 Length Microns Width Photo Microns ID 72 chr f 1.50 0.05 73 chr m 3.00 1.00 74 amo f 2.20 0.15 75 chr m 2.40 1.80 76 chr m 2.30 1.70 77 chr f 1.60 0.05 78 amo f 7.00 0.15 79 chr m 9.00 7.00 to 1 80 amo f 1.80 0.15 81 chr b 3.00 0.15 82 chr f 1.50 0.08 83 chr m 2.50 2.50 84 chr m 10.00 7.00 85 chr m 2.00 2.00 86 chr f 0.60 0.05 87 chr m 2.50 2.20 88 chr m 2.80 2.20 89 chr m 3.50 2.20 90 chr f 0.80 0.05 91 amo b 3.00 0.25 92 2- 5 chr f 0.60 0.05 93 chr m 2.00 1.80 94 chr f 4.00 0.05 95 chr m 2.50 2.20 96 chr m 2.50 1.00 97 chr m 2.00 1.60 98 chr b 2.00 0.20 99 chr b 1.00 0.20 100 chr f 0.60 0.05 101 amo m 2.50 1.50 102 chr f 0.80 0.05 103 chr f 1.20 0.05 aT' % 1 i MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 12 IWA M6366-12 05/19/91 05/24/91 MS li'vQ ^ KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 160 1 47MM Plastic 1.34E+09 /xm2 10 2 8057 /xm2 80570 /xm2 20000X 1:33.3 Analytical Sensitivity: 3.461 Asbestos Structures/cc 12.412 Asbestos Structures/mm2 Area Examined < 5 /xm > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 27 0 0 30 0 0 0 9 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 1 0 0 1 2 1 0 2 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 252.684 48.460 Total Structures/mm sq = 906 Structures/cc < 5 /xm > 5 /xm 93.459 0.000 0.000 103.843 0.000 0.000 0.000 31.153 3.461 0.000 0.000 3.461 6.923 3.461 0.000 6.923 Comments : * The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. * 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of Client: RICHARD SCRUGGS Sample ID: 12 IWA MAS Log Number: M6366-12 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR, . ,00 Microscoolst: MS ) U\ Reviewed bv: A Client Proj/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 160 1 47MM Plastic 1.34E+09 /J,m2 10 2 8057 nm2 80570 fj,m2 20000X 1:33.3 Length Microns Width Microns Photo ID 1 1-1 chr m 3.10 1.20 2 chr m 8.00 5.00 3 chr m 1.60 1.00 4 1-2 chr m 6.10 2.80 5 chr m 2.30 1.80 6 chr m 2.90 1.70 7 chr f 3.80 0.09 8 1-3 amo b 12.30 1.00 9 chr f 2.90 0.05 10 chr f 1.70 0.05 11 chr f 3.50 0.09 12 chr m 2.10 0.80 13 chr f 0.90 0.02 14 1- 4 chr m 4.40 2.20 15 chr m 6.40 2.30 16 chr m 2.70 1.00 17 chr m 1.00 0.80 18 chr m 3.20 1.50 19 chr f 0.60 0.05 20 chr m 1.80 1.00 21 1- 5 chr m 6.50 5.40 22 chr m 2.00 1.60 23 chr f 1.80 0.05 24 chr m 3.00 0.80 25 2- 1 chr m 0.80 0.20 26 chr m 4.20 0.40 27 chr f 0.60 0.05 28 chr m 11.00 9.00 29 chr f 0.50 0.05 30 chr m 1.50 0.35 31 chr f 2.30 0.09 32 chr m 5.70 1.50 Types ;ir - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophy11ite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices * Materials Analytical Services, Inc. Page: 2 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 12 IWA M6366-12 05/19/91 05/24/91 MSjl/il/Ml- KALO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 160 1 47MM Plastic 1.34E+09 jxm2 10 2 8057 im2 80570 /Xm2 20000X 1:33.3 Length Microns Width Photo Microns ID 33 chr f 2.00 0.05 34 chr f 0.70 0.05 35 chr m 1.60 1.60 36 amo m 12.50 11.00 37 chr m 12.50 11.00 38 2- 2 chr m 1.30 0.50 39 chr m 7.80 5.80 40 chr f 2.60 0.09 41 chr m 4.00 3.00 42 chr m 2.90 2.10 43 chr f 1.80 0.05 44 2- 3 chr m 2.00 1.40 45 chr f 0.90 0.02 46 chr f 1.50 0.02 47 chr f 0.50 0.05 48 chr m 2.60 0.80 49 chr f 0.60 0.05 50 chr m 1.50 0.40 51 chr f 1.50 0.09 52 chr m 3.00 2.20 53 amo m 3.00 2.20 54 amo f 8.40 1.10 55 chr f 0.70 0.05 56 chr f 1.00 0.05 57 chr f 1.50 0.05 58 chr m 5.00 1.80 59 2- 4 chr f 0.90 0.09 60 chr m 3.60 2.20 61 chr m 4.20 2.00 62 2- 5 amo f 2.20 0.25 63 amo m 7.40 3.40 64 chr f 1.00 0.05 65 chr m 3.60 2.50 66 chr f 0.70 0.05 67 chr f 0.70 0.05 jr 68 chr m 1.50 0.20 69 chr m 2.00 1.80 70 chr f 0.70 0.05 71 chr m 1.50 0.50 9 Materials Analytical Services, Inc. Page: 3 of 3 Client: RICHARD SCRUGGS Sample ID: 12 IWA MAS Log Number: M6366-12 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR./ . , </ Microscoplst: MS )t-- Reviewed by: ' i) Client Pro]/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 160 1 47MM Plastic 1.34E+09 /xm2 10 2 8057 /Xm2 80570 /xm2 20000X 1:33.3 Length Microns Width Photo Microns ID 72 chr m 2.60 0.90 73 amo f 10.00 0.25 SERVICES * May 24, 1991 Mr. Richard Scruggs Richard F. Scruggs Law Firm, PA P.O. Drawer 1425 Pascagoula, MS 39568 Dear Mr. Scruggs: Enclosed are the analyses of the air samples received at our facility on May 19, 1991. Thesampleswere sent under your job/purchaseorder number: KayloExperiment, andwere labelled: IP IWA 2P IWA 3P IWA 4P IWA Please call our office at your convenience should you have any questions concerning the analyses of your samples. Sincerely, ngo, Ph.D. WEL:lac Enc. Ref: M6368 3597 Parkway Lane Suite 250 Norcross, Georgia 30092 (404) 448-3200 FAX (404) 368-8256 CLIENT NAME: Richard Scruggs Law Firm CLIENT JOB NAME: Kaylo Experiment MAS JOB: M6368 MAS SAMPLE NUMBER SUMMARY OF AIR SAMPLE LOCATIONS 1 IP, 5/18/91, Inside during cutting 2 2P, 5/18/91, Inside during cutting 3 3P, 5/18/91, Inside during sweeping 4 4P, 5/18/91, Inside during sweeping Summary of Results of Analyses by Transmission Electron Microscopy, (TEM) Client Job Name: Kaylo Experiment MAS Job Number: M6368 MAS Sample Number Number of Asbestos Structures Counted Asbestos Concentration, Structures per Cubic Centimeter Hi*. - / i 2 3 4 96 104 110 98 591.4 255.5 304.2 698.3 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro}/ref: RICHARD SCRUGGS IP IWA M6368-1 05/19/91 05/24/91 AIR rw f < ,, \j! a umJj ) \\u]&LK.i KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 74 1 47MM Plastic 1.34E+09 /xm2 2 2 7349 /xm2 14698 jum2 20000X 1:5.0 Analytical Sensitivity: 6.160 Asbestos Structures/cc 68.036 Asbestos Structures/mm2 Area Examined < 5 /xm > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 44 3 0 33 0 1 0 5 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 3 1 0 0 0 6 0 0 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 591.366 73.921 Total Structures/mm sq = 6532 Structures/cc < 5 /xm > 5 /xm 271.043 18.480 0.000 203.282 0.000 6.160 0.000 30.800 18.480 6.160 0.000 0.000 0.000 36.960 0.000 0.000 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC Page: 1 Of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS IP IWA M6368-1 05/19/91 05/24/91 KAYO) EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 74 1 47MM Plastic 1.34E+09 jxm2 2 2 7349 /im2 14698 20000X 1:5.0 Length Microns Width Microns Photo ID 1 1-1 chr m 7.00 4.50 2 chr m 3.00 2.50 3 amo b 12.50 0.40 4 amo b 11.00 0.40 5 amo b 3.00 0.60 6 chr f 2.30 0.05 7 chr m 4.00 2.50 8 chr m 4.00 2.00 9 chr m 2.50 2.50 10 chr f 1.80 0.05 11 chr f 2.20 0.05 12 chr m 1.50 0.50 13 chr m 1.70 1.00 14 chr f 1.00 0.05 15 chr f 0.80 0.05 16 chr m 23.00 3.50 17 chr f 4.50 0.05 18 chr f 2.00 0.05 19 chr m 2.20 1.80 20 chr f 0.70 0.08 21 chr f 1.70 0.08 22 chr f 1.00 0.10 23 chr f 1.20 0.05 24 chr m 10.50 5.00 25 chr m 1.60 0.80 26 chr m 18.50 4.00 27 amo b 41.00 0.80 28 chr m 1.70 0.60 29 chr b 4.50 0.15 30 amo b 11.00 0.40 31 chr f 0.50 0.05 32 chr f 1.60 0.05 Types nr - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc Page: 2 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Proj/ref: RICHARD SCRUGGS IP IWA M6368-1 05/19/91 05/24/91 ' ^vKAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 74 1 47MM Plastic 1.34E+09 /zm2 2 2 7349 jxm2 14698 /zm2 20000X 1:5.0 Length Microns Width Microns 33 chr m 2.00 1.60 34 chr m 3.00 0.60 35 amo f 2.40 0.20 36 amo f 4.50 0.20 37 amo f 3.50 0.20 38 chr f 1.00 0.05 39 chr f 2.50 0.02 40 chr f 2.00 0.05 41 chr f 2.00 0.80 42 2- 1 chr b 2.00 0.20 43 chr m 1.70 0.80 44 chr f 0.70 0.02 45 chr m 2.40 1.50 46 chr b 1.80 0.15 47 chr m 4.00 3.00 48 chr m 3.50 2.20 49 chr m 2.50 1.00 50 chr f 0.70 0.05 51 chr m 4.20 4.00 52 chr f 1.50 0.02 53 chr f 0.60 0.05 54 chr f 2.40 0.05 55 amo b 8.00 0.40 56 chr m 4.00 1.60 57 chr f 0.50 0.02 58 chr f 2.20 0.05 59 chr m 9.50 7.00 60 chr f 0.50 0.05 61 chr m 4.00 1.20 62 chr b 19.00 1.60 63 chr f 2.00 0.05 64 chr f 1.70 0.05 65 chr f 1.50 0.05 66 chr m 3.00 1.50 67 chr f 1.20 0.05 68 chr f 4.00 0.05 69 chr m 3.50 1.20 70 chr m 1.80 0.70 71 chr f 1.00 0.05 Materials Analytical Services, Inc Page: 3 of 3 Client: Sample ID: MAS Log Number: Sample Received Sample Due Date Type Analysis: Microscoprst: Reviewed by: Client Proj/ref RICHARD SCRUGGS IP IWA M6368-1 05/19/91 05/24/91 AXR BW III 1A1 E KAY EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 74 1 47MM Plastic 1.34E+09 jum2 2 2 7349 nm2 14698 /Ltm2 20000X 1:5.0 Length Microns Width Photo Microns ID 72 chr m 2.50 2.20 73 chr f 0.80 0.05 74 chr f 0.50 0.05 75 chr m 2.20 1.50 76 chr m 2.40 1.60 77 chr f 0.50 0.05 78 chr m 1.00 0.70 79 chr m 1.80 1.20 80 chr m 2.50 2.00 81 chr m 1.00 0.60 82 chr m 1.50 1.00 83 chr f 3.00 0.02 84 chr m 3.00 0.60 85 amo b 12.00 0.40 86 chr f 2.00 0.05 87 chr f 1.20 0.05 88 chr f 0.50 0.05 89 chr f 0.60 0.05 90 chr m 2.00 1.80 91 chr f 1.00 0.10 92 chr f 0.70 0.05 93 chr m 2.20 0.70 94 chr f 1.00 0.08 95 chr f 1.80 0.08 96 chr f 2.00 0.05 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro3/ref: RICHARD SCRUGGS 2P IWA M6368-2 05/19/91 05/24/91 AH -- KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 64 1 47MM Plastic 1.34E+09 /Xm2 7 2 8156 /xm2 57092 /xm2 15709X 1:6.7 Analytical Sensitivity: 2.457 Asbestos Structures/cc 17.516 Asbestos Structures/mm2 Area Examined <5 lira. > 5 /xm No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 40 3 0 37 2 0 0 7 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 4 0 0 2 3 1 0 5 Total Asbestos Structures/cc (All): 255.539 Total Asbestos Structures/cc (>5 ): 44.228 Total Structures/mm sq = 1822 Structures/cc < 5 /xm > 5 /xm 98.284 7.371 0.000 90.913 4.914 0.000 0.000 17.200 9.828 0.000 0.000 4.914 7.371 2.457 0.000 12.286 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC Page: 1 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Pro}/ref: RICHARD SCRUGGS 2P IWA M6368-2 05/19/91 05/24/91 AH rui-' iX U17 KAYLO experiment Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 64 1 47MM Plastic 1.34E+09 jUm2 7 2 8156 nm2 57092 /Ltm2 15709X 1:6.7 Length Microns Width Microns Photo ID 1 1-1 chr m 3.40 2.50 2 amo f 2.20 0.20 3 chr f 1.80 0.05 4 amo m 3.00 2.00 5 chr f 2.50 0.05 6 chr m 9.00 8.50 7 chr m 2.50 1.50 8 chr m 2.00 1.50 9 chr m 1.80 1.50 10 chr b 3.20 0.30 11 chr f 2.00 0.04 12 chr f 1.50 0.05 13 chr f 2.50 0.05 14 chr f 1.50 0.05 15 chr m 9.00 8.00 16 chr m 2.80 2.00 17 1- 2 chr f 4.00 0.05 18 chr f 1.50 0.04 19 chr f 1.00 0.03 20 chr f 1.00 0.03 21 chr m 2.50 1.50 22 chr m 3.00 2.00 23 chr m 2.50 1.00 24 amo m 24.00 7.00 25 chr m 2.50 2.00 26 chr f 1.50 0.04 27 1- 3 chr f 2.00 0.05 28 chr m 2.80 2.00 29 chr f 1.00 0.03 30 chr m 7.50 6.00 31 chr m 5.00 3.50 32 chr m 2.00 1.80 Types *r - Chrysotile amo - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc Page: 2 of 3 Client: Sample ID: MAS Log Number: Sample Received Sample Due Date Type Analysis: Microscopist: Reviewed by: Client Proj/ref RICHARD SCRUGGS 2P IWA M6368-2 05/19/91 05/24/91 /f // KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 64 1 47MM Plastic 1.34E+09 jum2 7 2 8156 fj,m2 57092 /um2 15709X 1:6.7 Length Microns Width Microns 33 amo f 6.50 0.30 34 chr m 3.00 1.80 35 chr f 1.30 0.04 36 chr m 2.00 1.20 37 1- 4 chr f 1.00 0.04 38 chr m 3.50 1.80 39 chr f 1.40 0.03 40 chr f 1.20 0.04 41 chr f 6.00 0.05 42 chr f 1.20 0.04 43 chr f 2.00 0.05 44 chr m 2.50 1.50 45 chr m 1.80 1.00 46 chr m 1.20 0.80 47 chr f 2.40 0.05 48 chr b 2.50 0.80 49 amo f 7.00 0.40 50 chr m 3.00 2.00 51 chr f 2.20 0.05 52 amo m 5.80 2.00 53 chr f 5.00 0.05 54 1- 5 amo b 24.00 1.80 55 chr f 1.50 0.04 56 chr f 1.80 0.04 57 chr m 14.00 11.00 58 chr m 1.80 1.20 59 chr m 1.20 0.80 60 chr m 1.80 1.20 61 chr m 3.50 3.00 62 chr m 2.50 2.00 63 chr m 2.50 0.05 64 amo f 4.00 0.20 65 chr m 3.80 1.20 66 chr f 1.50 0.04 67 2- 1 chr f 2.20 0.05 68 chr m 2.00 0.80 69 amo m 8.00 4.00 70 chr f 3.00 0.05 71 chr f 0.80 0.03 Materials Analytical Services, Inc Page 3 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 2P IWA M6368-2 05/19/91 05/24/91 ah',. iir f YLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 64 1 47MM Plastic 1.34E+09 /zm2 7 2 8156 /J,m2 57092 /im2 15709X 1:6.7 Length Microns Width Photo Microns ID 72 chr m 2.00 0.80 73 chr m 2.20 1.00 74 chr f 1.50 0.05 75 chr m 11.00 9.50 76 chr f 1.50 0.05 77 chr f 2.50 0.05 78 chr m 2.00 1.50 79 chr f 3.00 0.05 80 chr m 2.00 1.20 81 chr m 9.00 6.50 82 amo m 2.50 1.50 83 chr m 2.00 1.50 84 chr f 1.20 0.03 85 2- 2 chr f 1.50 0.04 86 chr f 2.50 0.05 87 chr f 3.50 0.05 88 chr m 2.50 2.00 89 amo m 11.50 2.50 90 chr m 1.80 1.20 91 amo f 1.80 0.20 92 chr f 2.20 0.05 93 amo f 2.60 0.20 94 chr m 3.00 2.00 95 chr f 3.50 0.04 96 amo f 5.00 0.10 97 amo m 12.00 3.50 98 chr m 2.80 2.50 99 chr f 1.20 0.03 100 chr f 3.50 0.05 101 chr b 2.50 0.20 102 chr f 1.80 0.04 103 chr ra 2.50 1.50 104 chr m 3.00 2.00 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 3P IWA M6368-3 05/19/91 05/24/91 AIR SF_ KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /im2 5 2 7994 /xm2 39970 /im2 20000X 1:3.3 Analytical Sensitivity: 2.766 Asbestos Structures/cc 25.019 Asbestos Structures/mm2 Area Examined < 5 /im > 5 /m No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 28 4 0 56 1 0 0 9 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 2 0 0 4 0 0 0 6 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 304.241 44.253 Total Structures/mm sq = 2752 Structures/cc < 5 /im > 5 fm 77.443 11.063 0.000 154.886 2.766 0.000 0.000 24.892 5.532 0.000 0.000 11.063 0.000 0.000 0.000 16.595 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: l of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 3P IWA M6368-3 05/19/91 05/24/91 SF fftdfakij; (An Jt h KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 fm2 5 2 7994 tm2 39970 /Xm2 20000X 1:3.3 Length Microns Width Microns Photo ID 1 1- 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 1- 2 20 21 22 23 24 25 26 27 28 29 30 31 32 chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr chr chr chr amo chr amo amo chr chr m f m m m m b f f m m f m m m m m ra m m f m m m m m m m m m b m 1.40 1.90 3.90 3.20 2.00 3.10 2.00 0.50 1.30 6.30 3.80 1.10 1.60 2.00 6.60 4.20 2.30 2.40 2.80 5.90 3.90 5.40 2.80 6.10 1.10 1.70 6.10 4.20 5.00 4.40 1.40 0.70 0.30 0.10 3.80 2.80 1.60 1.70 0.20 0.03 0.07 6.00 3.00 0.07 1.60 1.50 5.00 2.10 1.10 1.50 2.80 2.40 0.05 5.20 2.00 1.90 0.70 0.30 2.90 1.10 2.40 3.60 0.20 0.30 Types Xamo cro - non - Chrysotile Amosite Crocidolite Non-Asbestos ant - Anthophyllite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc. Page: 2 of 3 Client: RICHARD SCRUGGS Sample ID: 3P IWA MAS Log Number: M6368-3 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR Microscopist: SF Reviewed by: Client Proj/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /im2 5 2 7994 jum2 39970 (j,m2 20000X 1:3.3 Length Microns Width Microns 33 34 35 36 37 38 39 40 41 42 43 44 2- 1 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 CM 1 CM chr amo chr chr chr chr chr amo chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr amo amo chr f 0.50 0.03 m 9.80 5.60 m 2.80 2.40 f 0.60 0.05 f 0.90 0.05 m 2.80 0.90 m 2.00 1.60 m 8.40 2.10 m 1.80 1.60 m 6.40 3.80 m 4.80 2.90 m 3.80 1.80 f 1.00 0.10 f 0.50 0.07 m 3.90 0.50 m 3.20 0.40 f 2.40 0.05 f 2.00 0.10 m 1.90 0.40 m 3.30 2.00 m 2.00 1.00 f 0.70 0.05 m , 6.40 3.70 m 1.00 0.60 f 3.20 0.07 m 1.70 1.60 m 2.80 0.50 m 3.70 3.00 f 1.70 0.05 f 0.60 0.07 m 2.80 1.90 m 5.20 0.70 f 0.50 0.03 m 3.80 2.80 m 0.80 0.30 m 1.70 0.70 f 4.40 0.40 f 3.90 0.30 m 2.10 1.10 Materials Analytical Services, Inc Page: 3 of 3 Client: Sample ID: MAS Log Number: Sample Received Sample Due Date Type Analysis: Microscoplst: Reviewed by: Client Pro3/ref RICHARD SCRUGGS 3P IWA M6368-3 05/19/91 05/24/91 AIR SF YLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /xm2 5 2 7994 txm2 39970 /xm2 20000X 1:3.3 Length Microns Width Microns 72 chr m 1.20 0.60 73 chr f 2.30 0.07 74 chr b 1.30 0.25 75 chr f 0.60 0.05 76 amo m 4.20 3.70 77 chr m 5.30 4.00 78 chr f 0.50 0.05 79 chr m 2.20 1.50 80 chr m 2.00 1.90 81 chr m 4.20 0.60 82 chr m 1.80 1.80 83 chr f 2.10 0.05 84 chr m 3.00 1.00 85 chr m 4.20 2.30 86 chr m 3.40 1.80 87 chr m 2.60 1.50 88 chr f 1.80 0.05 89 2- 3 chr m 5.00 1.30 90 amo m 5.20 4.00 91 chr m 1.80 0.90 92 chr m 1.90 0.80 93 chr m 0.70 0.30 94 chr m 4.00 1.40 95 chr m 3.00 1.60 96 chr m 1.70 0.80 97 chr f 15.90 0.07 98 chr f 0.50 0.03 99 chr m 2.30 1.20 100 chr m 2.60 1.10 101 chr m 1.10 0.90 102 chr f 1.60 0.07 103 chr f 0.50 0.07 104 chr b 2.20 0.30 105 chr f 1.60 1.20 106 chr f 1.70 0.03 107 chr m 1.60 1.20 108 chr m 2.40 0.70 109 chr m 2.20 0.40 110 chr f 0.70 0.03 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 4P IWA M6368-4 05/19/91 05/24/91 ms^> i KAYLO EXPERIMENT Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /Ltm2 3 2 7836 /nm2 23508 fjLm2 20000X 1:5.0 Analytical Sensitivity: 7.125 Asbestos Structures/cc 42.539 Asbestos Structures/mm2 Area Examined < 5 /zm > 5 /im No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 32 3 0 41 0 0 1 12 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 2 0 0 2 4 0 0 1 Total Asbestos Structures/cc (All): Total Asbestos Structures/cc (>5 ): 698.273 128.254 Total Structures/mm sq = 4169 Structures/cc < 5 fim > 5 /xm 228.007 21.376 0.000 292.135 0.000 0.000 7.125 85.503 14.250 0.000 0.000 14.250 28.501 0.000 0.000 7.125 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 4P IWA M6368 -4 05/19/91 05/24/91 AIR,- ms ,, / < ` vvv'i.U'V--- fitrk.stcJ' X" (SsXjJt_ KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /xm2 3 2 7836 ]Lim2 23508 jum2 20000X 1:5.0 Length Microns Width Microns Photo ID 1 1-1 chr f 0.90 0.02 2 chr b 4.50 0.40 3 chr f 2.00 0.05 4 chr f 1.10 0.05 5 chr m 1.60 1.00 6 chr m 1.00 0.80 7 chr m 1.80 0.60 8 chr m 6.80 4.00 9 chr m 2.00 0.40 10 chr f 4.90 0.05 11 chr f 1.00 0.05 12 chr f 0.60 0.09 13 chr m 5.60 1.50 14 chr f 2.40 0.10 15 chr m 5.00 2.00 16 chr m 1.50 0.90 17 chr m 7.00 4.90 18 chr m 1.60 1.00 19 chr f 1.00 0.05 20 chr m 1.50 0.90 21 chr m 10.00 4.10 22 chr f 0.50 0.05 23 chr m 6.50 3.50 24 chr m 7.00 4.00 25 chr m 1.80 1.00 26 amo f 2.30 0.25 27 chr m 11.00 6.00 28 chr m 3.00 2.40 29 chr m 4.60 1.00 30 chr m 2.00 0.40 31 chr m 2.20 2.00 32 chr m 2.00 0.90 Types r - Chrysotile -..lO - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophy11ite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc Page: 2 of 3 Client: RICHARD SCRUGGS Sample ID: 4P IWA MAS Log Number: M6368-4 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: AIR, ,,^f Microscoplst: MS ) ifr// 'A-lvitu Reviewed by: X tullh Client Pro]/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 /xm2 3 2 7836 fJ,m2 23508 im2 20000X 1:5.0 Length Microns Width Microns 33 34 1- 2 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 2- 1 71 chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr f m m f f m f f b m m m m m f f m m f m f m f m m b f f m m f f f m f m f m m 0.90 4.60 1.10 1.00 3.00 1.70 0.60 1.20 0.80 5.80 1.20 3.00 1.50 5.00 2.00 0.60 2.90 4.00 2.10 3.50 0.80 2.00 0.70 1.50 1.70 1.50 1.60 3.00 1.20 1.50 7.70 1.00 0.90 2.60 1.60 3.00 1.70 1.60 2.20 0.05 1.70 0.40 0.05 0.05 0.80 0.05 0.09 0.10 3.20 0.40 1.80 0.40 3.10 0.05 0.05 1.00 1.00 0.05 2.00 0.05 0.80 0.05 1.00 0.80 0.20 0.05 0.09 0.45 1.00 0.25 0.02 0.05 0.40 0.05 2.30 0.05 0.40 1.30 Materials Analytical Services, Inc Page: 3 of 3 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Pro^/ref: RICHARD SCRUGGS 4P IWA M6368-4 05/19/91 05/24/91 AIR, , , , MS ' \-t.vv_ KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Volume: Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 40 1 47MM Plastic 1.34E+09 ^m2 3 2 7836 nm2 23508 /^m2 20000X 1:5.0 Length Microns Width Photo Microns ID 72 chr m 2.60 2.30 73 chr f 0.60 0.05 74 amo f 5.20 0.20 75 chr f 4.00 0.05 76 amo f 12.80 0.30 77 chr f 2.10 0.05 78 amq m 5.70 3.00 79 chr m 4.60 3.00 80 chr f 0.80 0.05 81 chr f 2.10 0.05 82 chr m 2.50 0.60 83 chr f 0.70 0.05 84 chr c 49.00 12.00 85 chr m 3.00 0.80 86 amo m 3.00 0.80 87 chr m 7.90 3.00 88 chr m 1.80 1.80 89 chr m 1.10 0.40 90 chr m 4.40 3.00 91 chr f 2.00 0.05 92 chr m 2.00 0.80 93 amo f 12.00 0.60 94 chr m 2.60 1.10 95 chr m 5.00 3.60 96 chr m 2.60 1.00 97 amo f 2.00 0.40 98 chr m 2.00 0.80 HJST SAMPLES MATERIALS ANALYTICAL SERVICES * COPY May 24, 1991 Mr. Richard Scruggs Richard F. Scruggs Law Firm, PA P.O. Drawer 1425 Pascagoula, MS 90564 Dear Mr. Scruggs: Enclosed are the analyses of the dust samples received at our facility on May 19, 1991. The samples were sent under your job/purchase order number: Kaylo Experiment, and were labelled: 1 2 3 Please call our office at your convenience should you have any questions concerning the analyses of your samples. Sincerely, WEL:lac Enc. Ref: M6369 3597 Parkway Lane Suite 250 Norcross, Georgia 30092 (404) 448-3200 FAX (404) 368-8256 CLIENT NAME: Richard Scruggs Law Firm CLIENT JOB NAME: Kaylo Experiment MAS JOB: M6369 MAS SAMPLE NUMBER SUMMARY OF DUST SAMPLE LOCATIONS 2 Tin Can, placed on floor 10 feet from table where Kaylo is; Before, during and after cutting 3 Tin can, sealed blank Summary of Results of Analyses by Transmission Electron Microscopy, (TEM) Client Job Number: Kaylo Experiment MAS Job Number: M6369 MAS Sample Number: Number of Asbestos Structures Counted Asbestos Concentration, Structures per Sa. Ft. 2 121 30 16.2 Billion N/A Asbestos Concentration, Structures per Sa. Cm. 17.4 Million N/A MATERIALS ANALYTICAL SERVICES/ INC. 3597 PARKWAY LANE/ SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 2 M6369-2 05/19/91 05/24/91 DUST , WS&jAL, a,i> CM \| ,, KALO EXPERIMENT Sample Area Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area: Tot Area Examined: Screen Mag: Dilution Factor: 49.2 sq cm 0.053 sq ft 47MM Plastic 1.34E+09 fj,m2 5 2 7533 ]Um2 37665 /im2 20000X 1:200.0 Area Examined Structures/cm2 < 5 /Ltm > 5 jim < 5 fira. > 5 /im No. Free Chrysotile Fibers: No. of Chrysotile Bundles: No. of Chrysotile Clusters: No. of Chrysotile Matrices: 65 5 0 39 4 9.369E+06 5.766E+05 0 7.207E+05 0.000E+00 1 0.000E+00 1.441E+05 3 5.621E+06 4.324E+05 No. Free Amphibole Fibers: No. of Amphibole Bundles: No. of Amphibole Clusters: No. of Amphibole Matrices: 2 0 0 0 0 2.883E+05 0.000E+00 0 0.000E+00 0.000E+00 0 0.000E+00 0.000E+00 2 0.000E+00 2.883E+05 Total Asbestos Structures/1 sq ft (All): 1.620E+10 Total Asbestos Structures/1 sq ft (-5 ): 1.339E+09 Total Asbestos Structures/1 sq cm (All): 1.744E+07 Total Asbestos Structures/1 sq cm (-5 ): 1.441E+06 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MLATERIALS ANALYTICAL SERVICES, INC. Page: 1 of 4 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Proj/ref: RICHARD SCRUGGS 2 M6369-2 05/19/91 05/24/91 DUST WS COtUi.-i-, .v; KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Area 49.2 sq cm 0.053 sq ft Filter Type: 47MM Plastic Filter Area: 1.34E+09 jum2 Grid Openings: 5 Grids Examined: 2 Avg Grid Sq. Area: 753 3 /im2 Tot Area Examined: 37665 pim2 Screen Mag: 20000X Dilution Factor: 1:200.0 Length Width Photo Microns Microns ID 1 1-1 chr f 4.60 0.08 2 chr f 0.90 0.01 3 chr m 1.10 0.30 4 chr b 2.90 0.20 5 chr f 0.70 0.02 6 chr f 0.60 0.02 7 chr f 0.60 0.02 8 chr f 1.20 0.01 i9 chr m 1.60 0.20 - 10 chr f 3.00 0.04 11 chr f 4.20 0.10 12 chr f 0.90 0.01 13 chr m 3.00 1.50 14 chr f 1.20 0.04 15 chr f 1.20 0.04 16 chr m 4.00 1.50 17 chr f 0.70 0.02 18 chr m 0.70 0.20 19 chr f 0.90 0.01 20 chr f 1.20 0.04 21 chr b 0.70 0.12 22 chr m 1.60 0.40 23 1- 2 chr f 1.50 0.04 24 chr m 3.00 2.00 25 chr f 0.80 0.02 26 chr m 1.90 0.30 27 chr m 1.20 0.20 28 chr f 1.00 0.02 29 chr m 2.00 0.60 30 chr m 5.80 1.20 31 chr f 18.00 0.08 32 chr b 2.40 0.10 Types r - Chrysotile ctino - Amosite cro - Crocidolite non - Non-Asbestos ant - Anthophy11ite tre - Tremolite act - Actinolite Structures f - Fiber b - Bundle c - Cluster m - Matrices Materials Analytical Services, Inc Page: 2 of 4 Client: Sample ID: MAS Logf Number: Sample Received: Sample Due Date: Type Analysis: Microscoplst: Reviewed by: Client Pro^/ref: RICHARD ;SCRUGGS 2 M6369-2 05/19/91 05/24/91 DUST ws eat/%u*.. --______________ KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Area 49.2 sq cm 0.053 sq ft Filter Type: 47MM Plastic Filter Area: 1.34E+09 /xm2 Grid Openings: 5 Grids Examined: 2 Avg Grid Sq. Area: 7533 /zm2 Tot Area Examined: 37665 jxm2 Screen Mag: 20000X Dilution Factor: 1:200.0 Length Width Photo Microns Microns ID 33 chr b 2.50 0.15 34 chr ra 5.40 2.50 35 chr m 1.90 0.60 36 chr f 1.20 0.05 37 chr f 2.00 0.06 38 chr f 2.40 0.08 39 chr m 1.00 0.60 40 1- 3 chr m 1.20 1.00 41 chr f 12.00 0.04 42 chr f 2.70 0.04 43 chr m 2.00 1.20 44 chr f 1.20 0.04 45 chr m 1.60 0.80 46 chr f 1.60 0.04 47 amo m 7.00 6.00 M31746 48 chr f 0.80 0.04 49 chr m 3.00 2.00 50 chr f 2.00 0.04 51 chr f 3.00 0.02 52 chr f 1.90 0.02 53 chr m 1.00 0.80 54 chr f 0.70 0.02 55 chr f 3.60 0.04 56 chr m 3.80 2.20 57 chr b 1.60 1.00 58 chr f 0.90 0.02 59 chr f 1.10 0.02 60 chr f 0.60 0.01 61 chr f 0.90 0.02 62 amo m 5.00 4.50 63 chr f 0.60 0.06 64 chr f 0.60 0.06 65 chr c 10.00 0.40 66 chr f 0.80 0.02 67 2- 1 chr f 0.70 0.01 68 chr f 1.60 0.02 69 chr f 0.60 0.04 70 chr f 1.30 0.02 71 chr f 2.50 0.04 K. Materials Analytical Services, Inc. Page: 3 of 4 Client: RICHARD SCRUGGS Sample ID: 2 MAS Log Number: M6369-2 Sample Received: 05/19/91 Sample Due Date: 05/24/91 Type Analysis: DUST Microscooist: WS vui'ili*:, <-/?*-) Reviewed bv: Client Pro]/ref: KAYLO EXPERIMENT Strc. Grid Op Type Structure Sample Area 49.2 sq cm 0.053 sq ft Filter Type: 47MM Plastic Filter Area: 1.34E+09 /m2 Grid Openings: 5 Grids Examined: 2 Ava Grid Sa. Area: 7533 fJ,m2 Tot Area Examined: 37665 ^m2 Screen Mag: 20000X Dilution Factor: 1:200.0 Length Width Photo Microns Microns ID 72 73 74 75 76 77 78 79 80 81 82 83 84 85 86 87 88 89 90 91 92 93 2- 2 94 95 96 97 98 99 100 101 102 103 104 105 106 107 108 109 110 chr amo chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr amo chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr chr f f f f m f f f m m m f f f m m m m f f f m f m m m f m m f f m f f m f f m m 1.60 1.00 0.50 0.60 2.80 2.00 0.70 8.00 1.60 3.00 1.80 0.90 0.90 2.00 1.20 1.80 3.60 2.00 0.70 0.80 1.00 2.60 1.20 1.50 3.20 0.70 1.00 1.50 1.60 1.50 4.20 2.20 1.40 0.70 0.60 0.90 2.20 1.80 5.50 0.04 0.15 0.01 0.01 1.30 0.02 0.03 0.02 0.80 0.20 1.50 0.01 0.02 0.02 1.00 1.50 0.60 1.20 0.02 0.01 0.20 1.20 0.01 0.30 0.60 0.02 0.02 0.70 1.60 0.02 0.04 0.40 0.06 0.02 0.30 0.02 0.02 1.10 3.80 Materials Analytical Services, Inc. Page: 4 of 4 Client: Sample ID: MAS Log Number: Sample Received: Sample Due Date: Type Analysis: Microscopist: Reviewed by: Client Proj/ref: RICHARD iSCRUGGS 2 M6369-2 05/19/91 05/24/91 DUST ws - V- 1 KAYLO experiment Strc. Grid Op Type Structure Sample Area 49.2 sq cm 0.053 sq ft Filter Type: 47MM Plastic Filter Area: 1.34E+09 Mm2 Grid Openings: 5 Grids Examined: 2 Avg Grid Sq. Area: 7533 Mm2 Tot Area Examined: 37665 Mm2 Screen Mag: 20000X Dilution Factor: 1:200.0 Length Width Photo Microns Microns ID 111 chr m 1.60 1.40 112 chr f 2.20 0.02 113 chr f 3.00 0.08 114 chr f 1.20 0.10 115 chr f 3.90 0.10 116 chr m 3.00 1.50 117 chr f 2.00 0.08 118 chr f 7.80 0.02 119 chr m 1.20 1.00 120 chr m 3.40 2.80 121 chr f 2.20 0.08 MATERIALS ANALYTICAL SERVICES, INC. 3597 PARKWAY LANE, SUITE 250 NORCROSS, GEORGIA 30092 (404) 448-3200 05/24/91 TEM ASBESTOS ANALYSIS REPORT Client: Sample ID: MAS Log Number: Sample Received Sample Due Date Type Analysis: Microscopist: Reviewed by: Client Proj/ref RICHARD SCRUGGS 3 M6369-3 05/19/91 05/24/91 Dust^ / / j ____ A 'wy, KAYEO EXPERIMENT Sample Area Filter Type: Filter Area: Grid Openings: Grids Examined: Avg Grid Sq. Area Tot Area Examined Screen Mag: Dilution Factor: 49.2 sq cm 0.053 sq ft 47MM Plastic 1.34E+09 jxm2 10 2 8011 /um2 80110 /im2 20000X 1:3.3 Area Examined Structures/cm2 < 5 /Lim >: 5 m <5 jum > 5 pirn No. Free Chrysotile Fibers No. of Chrysotile Bundles: No. of Chrysotile Clusters No. of Chrysotile Matrices 0 0 0 0 0 0.000E+00 0.000E+00 0 0.000E+00 0.000E+00 0 0.000E+00 0.000E+00 0 0.000E+00 0.000E+00 No. Free Amphibole Fibers 0 0 0.000E+00 0.000E+00 No. of Amphibole Bundles: 0 0 0.000E+00 0.000E+00 No. of Amphibole Clusters 0 0 0.000E+00 0.000E+00 No. of Amphibole Matrices 0 0 0.000E+00 0.000E+00 Total Asbestos Structures/1 sq ft (All): 0.000E+00 Total Asbestos Structures/1 sq ft (-5 ): 0.000E+00 Total Asbestos Structures/1 sq cm (All): 0.000E+00 Total Asbestos Structures/1 sq cm (>5 ): 0.000E+00 Comments : The Analytical Sensitivity is calculated on the probability of analyzing one asbestos fiber or structure in the total area examined. 0.000 display = Below Analytical Sensitivity MATERIALS ANALYTICAL SERVICES SUN 26-MAY-91 09:29 Cur-sol": 0.000KeV = 0 ROI CSIKoO 1.660: 1.810=2014 rj> k MRTERIRLS RNRLYTICRL SERVICES SUN 6-MRY-91 09:42 Cuhsoh: 0.000KeV = 0 ROI CSIKcO 1.660: 1.810=211 fr'i *~( I rl. ^-- MATERIALS ANALYTICAL SERVICES SUN 26-MAY-91 09:44 Cur-soh: 0.000KeV = 0 ROI CSIKoO 1.660: 1.810 = 1194 y lx oh P fU YI ^ "2- H':, MATERIALS ANALYTICAL SERVICES SUN 26-MAY-91 09:47 Cuhsor: 0.000KeV = 0 ROI CSIKoO 1.660: 1.810=4760 fbfrfv P MATERIALS ANALYTICAL SERVICES SUN 6-MAY-91 Cut-sob: 0.000keV = 0 ROI CSIKcO 1.660: 1.810 = 1188 : 09:56 1 M G......, ............... . . . . . . . . . . . . . . . . 0.000 32 r4l4.-nh--:--'yr M 6369-2; CHRYSOTILE J rtf 1 ........ J . . . . . . . j t.............. I 1 Yv`l^Kilrr;'7 VFS = 128 10.240 MATERIALS ANALYTICAL SERVICES SUN 26-MAY-SI 09:57 CuTsot: 0.000KeV = 0 ROI CSIKcO 1.660: 1.810=517 It & jvt HI IIS'' MRTERIRLS RNRLYTICRL SERVICES SUN 26-MRY-91 09:59 Cursoh: 0.000KeV = 0 ROI CSIKcO 1.660: 1.810=2029 i i .............. J............ .............. ......... .... .............. ............. ............. ............. .............. .............. Ifi . : I :. a\ j 1! n :* :& ....... .,,,yT 0.000 39 Ywinj-Wr-.T M 6369-25 MRTRIX VFS = 256 jlJ. 10.240 I? h & h iu mm<r MATERIALS ANALYTICAL SERVICES SUN 26-MAY-91 10:27 Cuf-soh: 0.000keV = 0 ROI CSIKoO 1.660: 1.810 = 1243 /4T 14 MRTERIRLS RNRLYTICRL SERVICES SUN 26-MRY-SI 10:3; Cursor: 0.000keV = 0 ROI CSIKcO 1.660: 1.810 = 1046 j>U~ * )v 'i in') :*jr ''-.ui* MRTERIRLS RNRLYTICRL SERVICES SUN 26-MRY-91 10:33 Cursor-: 0.000KeV = 0 ROI CSIKoO 1.660: 1.810=3688 s I l...........1............1............. \ i "3 j: :: r i1: 1: i i............ ............1..........j M Rj "G""L l .............. JMl \ I'.'T `.".'TTk n.-fctT'fttrag 0.000 35 M 6366-7; MRTRIX ttf ! : ii : fi ! :i% : : ) \ !J z] cL........... L^i VFS = 512 10.24 ..sr f J* * <Y i' i v MATERIALS ANALYTICAL SERVICES SUN 26-MAY-91 10:39 Cursor: 0.000keV = 0 ROI CSIKcO 1.660: 1.810=1033 |'U t( ( l ") x MRTERIRLS RNRLYTICRL SERVICES SUN 26-MRY-91 10:42 Cursor-: 0.000KeV = 0 ROI CSIKoO 1.660: 1.810 = 103 MRTERIRLS RNRLYTICRL SERVICES SUN 26-MRV-SI 10:37 Cuhsoh: 0.000KeV = 0 ROI CSIKcO 1.660: 1.810=854 r_* i I :i >! ! i !t 1! i !i * ............:............:............. 1! C :: i! i; ii h i 1i tY...........V:............V: ............. ) ........ !1 1 ; ''`j? .............1............ j...........s I jI ......... 1i : atadsl ii 0.000 2S M 6366-7; MRTRIX r r ! ? LA VFS = 128 10.240 ,r NAS INC 1141275 lee.'lKV IX10K 5001)1 MAC lUC 114127$ lllMKII 1X2588 2hi V.`:' Y-:''i.- <''<''9. !',.<:? sv:;'->.$? .',Viy ;>v vV.'iW/.f f' T \* '/}';'ti'rV! .>- '''*' ` Mllfcy'J ^J^xvV-Vv^-;v-ft vV/V^;^vt'^VJ^-,''^^'>V'''-'... v.,. :;fvW>' -.v. ;>.*;. 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