Document np0je8kYBNxkpBZ84pQzXGQVw
CG 56
CODE YT-714-D PKG
*SE_PJ 7.1982 ___ KgniO___ '' ''
< *t >a t e: 7l o t ^n u mSe r T-
EST, WT. 18*?* UBS. PREPARATION NOTES
PROCESSES < >YT-714-D- <G)
APPROVED BY: EWK 12/23/81 .
COMTYP JOB NAME: 50YT7i4DMG >; STANDARD HRS. ___TIME ^_^4.Hr
PREP i
J83
- NON-BLEEDING ...
NAME: GREEN GOLD
----
OBTAIN FOR S4 2,4-DIHYDROXY QUINOLINE OBTAIN FOR S9 P-CHLOROANILINE -
1 USE j -. .... | . ACCT I LBS | N-CODE | LBS
44--C | 613-C-. ?
... 1
Rmj&r* < 2037G) WATER INTO V-283 A HEAT
!
85-96 DEG F
...................... I
i
DUMP A RINSE IN FROM Si LOT
166% % !
J
1 2,4-DIHYDROXY
-
SS&-
1 QUINOLINE
i
I
/JfLy______ Wl~- 16etZj~6u2&-\
lyuaJL-- Alt-
LfJkJl____ i/Xl S$JAjfcU-\
i -------------------------------------l----l '
...........l -
44-C | 1678 .... .. i
TO 54* (2836G) AT-85-90 DEG F
DUMP IN S, STIR TO SOL'N FOR Si 2 SODIUM
CARBONATE
-.
i 369 ! ........3--A I 369-
DV Xjr\ RUN \1* <5?5G> WATER. INTO V3 J^*T RlJjsKlN FROM V-324 HYDROCHLORIC _ACID
, \ JpnHEAT TO 68-72 F & DUMP IN~FRM S2
I l NOTE: THE RESOURCE CONSERVATION
1 | RECOVERY BILL HAS CLASSIFIED PARArJ.
i 1 CHLORANILINE (N-613-C) A HAZARDOUS,___
! 1 WASTE MATERIAL. THIS REQUIRES EMPTY N613C
{ t CONTAINERS TO BE GIVEN 3 WATER RINSES WITH
! | 135t 145#F WATER FROM HOT WATER MIXER INTO
}|
BEFORE DISPOSING-, NOTE <2) N-613C IS
j .r EXTREMELY TOXIC DESTROY DRUMS PER STD PRAC
1>er i STIR 30 MIN OR .LONGER TO DISSOLVE FOR SI 3
RECORD: STARTLl7Jka->w
,--v
!
560 796
R]Jir3* (489G> WATER INTO V
r&. in s t a l l i
EMP CHART
,
WHEN S6 STIR COMPUTE, RUJvf IN DV ^THRU SCREEN}
fr* 1 MAKING INSTRUCTIONS:BATCH UNIT-
OF 3
i USE CG 50 CODE YT-714-D <G> 1 LBS
N-CODE I ACC-TI LBS
WHEN S10 STIR COMPLETE, ADJ TO 61 * <21000 (6X330 I '57-A
T 56-40 DEG F. ICE
I -1
SIPHON IN IN 10-12 MIN. SODmM-vNITRi;
M.-.y .. .
5 fey %.
l ! 725-A (:--437.^./
IR 5 MIN 6 RECORD:
-MUST-BE +
725--A
11 STIR 30-45 MIN AT 60-72 DEG F-Mfcf NTAI$N& ,
57-A
+CR, +KI FOR S2 RECORD : - TIME*STARfXS<L
CR_________<*>, Kl__________ ;<+> < '.-> 'J' I
NOTE: <D IF CR-KT-, ADD 20*. *AS IS* INCREMENTS HYDROCHLORIC ACID - - ASSUME 32%; RECORD: CR___ _( + ) KI___,,___<+> <2> IF CR+KI- ADD 20# `AS IS* INCREMENTS
i_______ i
i\ !I
- 28-D I
I-.
'
'
SODIUM NITRUE-
ASSUME 33%
RECORD: CRI____<+) KI____ __<+>
I.*______l 725-A
} - !
15.* C760G) WATER INTO V--283 AND-HEAT- 1
. VT ^TO 6*8 DEG F
..
.|
DUMP IN 6 STIR TO DISSOLVE NICKEL SULFATE^ 4
i>T51PHON IN IN 10-12 MIN'-6 STIR- FOftrSSOte` - l
A^IONIUM HYDROXIDE
v
-839 510
...
l.
-S'.'..--
I - 707-B- t -939fei
I --122-P~ L~-45t0&&=4
WHEN SI6 STIR COMPLETE, TEST OV-?.* RECORD-- -I-
CR_^2fcr_,,<+>,
- *- -- -I-
NOTE: < 1 > IF CR-, KI- ADD 20# -*AS IS*
- -f--
INCREMENTS HYDROCHLORIC ACID - ASSUME. 32%. f __
RECORD-- CR____,_C+> KJ^l L^L.L<
f~-
<2->t*r. CR+, K I- ADD 2# * AS IS" . INCREMENTS f :
$3TUM NITRITE
^ASSUME 33%
RECORD : CR_____._{ + > KI .___< + > - - (
SETTLE 15-3 MIN FOR S24 ^RECORD:
- - (
DV, UART_/5_54^~-
f
-4 I, .*? *v%.<-* I - - - I ...
__( - : -28--A- j
__ _
-f
___ !....725-A
- -1 , - -
-4 - -
i- :-~;~
SLURRY WITH +/- 3 GALLONS WATER IN DRUM S32 SURFACTANT &3300 - " - - -
113 i 892-D | f134
^ _ CV TO 78-82 DEG F 39* <3787&> 6 RECORD (2X330
HT,,i0___DEG F 6 REC__DEG F
|
WHEN S21 SETTLING COMPLETE, COUPLE-DV
I
UfcABERSURFACE IN 60-7 MIN ^ RECORD:................... j
TART_^XX.rTOTAL MIN_Jj L-__
I
AIN IN DVr5 MIN 6 WASH IN LINE ONLY ' I
WHEN S24 COMPLETE, STIR 3 MIN 4. DISCONNECT!
SFER LINE AT CVIMMEDIATELY . ..
i
RECORD; DIA20_^:__<-> ,BASE_X!n<+>/
1
PH_J^L_<8.-9.0)
1*
NOTE:<1> IF DIA20 +, BASE
6 PH'BELOW 8.0 |
(A) ADJ TO PH 8,0-9. SODIUM*CARBONATE 4_____
<B> RECORD PH___ I____
..... -
1
<2) IF DIA20 +> BASE
6-PH-8.0 OR ABOVE:..I
(A) ADD 10# 100% N-44-C -2,4-DIHYDROXY. : }________|
.QUINOLINE <B> ADJ WITH WATER TO +/- 25G
,I
~i I
<C) STIR TO DISSOLVE
-'^-4 .
j
<D) POUR INTO CV
j
<E) STIR lO MIN
:. .
_: |
<3) REPEAT '<1> 6 <2) ABOVE AS NECESSARY TO I
- DIA20, 4 BASE
.. . |
57-A \Lk
3-A
5%.
l Ir?
44,--D I
I
I
I
1
: :'vJt -- '
7
;*
DU P050103922
p.... if
.3 J
rrasp--ftrrgr>"'4" -t L. aQUiP| t-
WENT
MAKING INSTRUCTIONS;BATCH UNIT
PAGE 3 OF 3
-I - USE-- I _ N-CODE -|t--ACCT 1 LBS-
HEAT TO>4 STJR 20-2-fWlN AT
IR.WASH DV TO SEWEf
V RUN IN V2S3 IN 20-25 MIN TiAJNTAIN | STIR 5'MIN J, RECORD: .'PHd$#_ I DUMP IN N-892-B SLURRY FROM-S$2
----- "p- IN BARIUM SOLFA]"-'' i STIR 9Q to A'lJ^I-WP^EG ' RECORD :
oDr
AGITATOR .
k t a k e ; i q t , s a mp l e .
1 S35
V-100
V-i05
\1 -<. 1 SUPERVISOR NOTE:
fa " |<1> IF; BIA'ZO ^ AFTER INITIAL COUPLING <S27) {
> 1*
i Ad v ic e p r o c e s s in g t o : '
"
j (A) LOAD IN BRUMS' @>325* NET AS PRESSCAKE
l\ is , d s ^n o t v b r y * t a k e ,rot- s a mp l e
\
4
L I < B 5 Ht\GH`'! PRESSURE HOSE PRESS AND: BOX AFTER ?.}
1 Dr o p p in g b e f o r e f il l in g n e x t b a t c h
.1I ' V - ''
;.' . .
V'
1 ` SUPVR`:.
k' H \ I BATE:..
K
it
?
1
?
DUP050103923