Document nmma18br287vr0mxE5ejzqkXa
| RT-698-D PKG
< DATE >
<;LSf~NUHBiRT"
EST* WT^'Saliff* l b s :*
PREPARATION NOTES::
pr o c esses
< )RT-698"D (M>
appr o ved by
EWK2/25/82
TYPED BY: KLW STANDARD HRS, _____
TIME of H
NON-BLEEDING
USE N-CODE ACCT
NAME: WATCHUNG RED B
i LBS
LBS
--1
RECORD:
__BATCHES SINCE SPARKLER LAST
I
CLEANED* AFTER 4 BATCHES, CLEAN, DRESS
|. __l 777-A
SPARKLER & PRECOAT WITH 15* DICALITE
|1
FILTER AID
I
OBTAIN FOR S11 2-CHLORO-4-AMINOTOLUENE-5- j
I 740-C I
SULFONIC ACID
-
i
OBTAIN FOR S41 3-HYDR0XY-2-NAPHTR0IC ACID i
I 82-C 1
INSTALL DV & CV RECORDER & CONTROLLER CHART I
NOTE: RUN 15" WATER INTO V-904* PUMP WATER 1
FROM V-904 THRU DISTRIBUTOR* IF WATER DOES I
NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH J
ULL FORCE, NOTIFY SUPERVISOR .
|
. I RUN 20* <415G) WATER INTO V-932 & HEAT-TO
I 'yr 80-100 DEG F
\Jw L, ADD IN 8-9 MIN DRESINATE
*
IR 5 MIN & RECORD: PH__^_._<9 * 5-1 . 5)
.STIR 20 MIN OR LONGER TO DISSOLVE FOR S44
/f Am
NOTE: NOTIFY PRESS ROOM BEFORE ROPING
AREA UNDER V-922
38* (7B2G) WATER INTO V-922
H SODIUM HYDROXIDE IN V-926 & RUN IN
M____ TURN ON AGITATOR t* STEAM DUMP IN' FRCm's ^
2-CHLORO
OT,, *100%,
7-
AMINOTOLUENE 5-SULFONIC? ACID
DUMP'IN ACTIVATED CARBON
DUMP IN FILTER AID
EAT TO 212-214 DEG F WATCH FOAM!i!!
R0RD: BY_.-fe___< + > IF NECESSARY ADJ TO
<BY SODIUM HYDROXIDE
ASSUME 50%
STIR 3 MIN AT 212-214 DEG F, THEN SHUT OFF
STEAM* WATCH FOAM. RECORD: SPARKLER PRES-
URE
_____PSI IF NOT ZERO NOTIFY SUPVR*
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOL *N IS CLEAR. MAINTAIN AT 190-195 F j
FOR SI 9 . RECORD : START^3.1JlCr TOTAUtWNjEP.
CLARITY
F & REC>Sl_ F
7-D 740-C
i 13-B 777-A
7-D
EQUIP i MENT j
PAGE 2 OF 3
i USE CG 32 CODE RT-698-D <M> I LBS
904/CV Ih P
2' <53G> WATER INTO V-904/CV
!
4 1WHEN-SI 7 COMPLETE, PUMP IN V-922 THRU
I
| SPARKLER, MAINTAIN ,%922 AT 190-195 DEG F |
| i RECORD: START jt
TOTAL MIN__^X-_ i
N-CODE
ACCT LBS
902 5
MISC 6
54' (1407G) WATER INTO V-902
I S*f $
|2T t DUMP IN CALCIUM HYDROXIDE h STIR TO SMOOTH. I
N
.URRY
|I
WEIGH SODIUM HYDROXIDE IN V-926 & RUN IN
AND HOLD FOR S41
M U_____,
j 1
33/
laiTi MEASURE^fe?"JUNITS IN V-928 FOR S35. .
|
1^HYDROCHLORIC ACID
|2>*T WEIGH SODIUM NITRITE IN PT FOR S38 ,, /
*r. .
m___ j SL.*, J23e~.-%
I
i I //**
542-0 A e3i9gSutK. ''
7-D i
f 28-D j
I 725-A |
1 66
544 367
922 12gT | UIH+EEN SI 9 COMPLETE, STOP PUMP 6 INSERT V-922I
7 I JrFQQT PLUG
-f
1I RUN IN 15' (309G) WATER & HEAT TO 190-195 F|
RCULATE 15 MlN THRU SPARKLER
|
P V-922 THRU SPARKLER INTO V-904/CV
I
'I
922 128 i RUN IN 9' <177G> WATER INTO V-922 AND HEAT ) 9 1 | TO 190-195 F* CIRCULATE 15 MIN THRU SPARKLR1
904/TV I'^flpUMP V-922 THRU SPARKLER INTO V-904/CV
10 |*S^H^HEN MTY BLOW OUT SPARKLER INTO V-904/CV
I an JHPOUR IN IGEPAL CO-630
-
HEAT TO 165-170 DEG F FOR S34
J
1 1 I
47
s 979-D- 47
CV NOTE:' IF N-740-C SOL'N'WAS PUMPED DIRECTLY
11 M SPARKLER TO CV, OMIT STEPS 33 & 34*
tUN IN 1` (95G) WATER.INTO V--
WHE?i S32 COMPLETE, PUMP V-904 AT 165-170 F
...."`"^GSS^*WIWTOR INTO CV AFAP
p^-TS""MIN) * MAINTAIN 165-170 DEG F IN CV
RECORD : STARTTOTAL MTN___/_:
RUN IN HYDROCHLORIC ACID N-28-D FROM S23
12-15 MIN 3#5<fflR 15 MIN AT 16.5-170 DEG F.
3W1 ADJ TO 48* < 4.536G) AT 32-38 DEG F^
& $'56X330 | L^7-a jL$&6
RECORD: TEMPOS.___ F, VOLUME
RUN IN SODIUM NITRITE N-725-A FROM S24
&FAP (5-10 MIN) 6 RINSE IN PT
STIR 30 MIN AT 32-38 DEG F MAINTAINlN +DR, +KI FOR S40 .RECORD: TIME START_J/CL~L_
CR._*J^l...< + > KI__fc:_< + ) NOTE: <1 ) .IF CR-, KI- ADD 204 'AS IS* INCREMENTS
1 HYDROCHLORIC ACID
RECORD: CR
( + ) KI______( + )
ASSUME 32%
i 28-D [.
(2) IF CR+, KI- ADD 204 *AS IS INCREMENTS
SODIUM NITRITE SECORD: 'CR______( + > KI______ < + > ASSUME 33% DUMP IN FROM S3 6 STIR 10 MIN
______ i
725-A L._*.__ 82-C I 1024
3-HYDR0XY-2-NAPHTH0IC ACID
l_
.....
DUP050102125
BATE PRINTED;
tfiUIP 1 MENT |
l^AGE 3 OF 3
I USE CG 32 CODE RT-698-D (M) | LBS
"n -c o d e
ACCT LBS
902 <#11 DUMP IN AMMONIUM CHLORIDE
12 I
I
I 221 I 165-A |
II
I
CV 1 IMMEDIATELY AFTER S41 COMPLETE', WITH V-902 |
13 1 AGITATOR ON PUMP V-902. THRU UNDERSURFACE |
I DISTRIBUTOR INTO CV IN 18-22 MIN- LET TEMP-!
I RISE FREELY. ^VlY-
,
!
CORD? StART^lJgfes.,_LT0TALJ1IN_r_l______
!
IR 15_MIN & RECORD; PH__^i3L_<9-0-9-8> 1
I TEMP
DEG F .<40-50 DEG F> AND IF-PH I
I IS BELOW 9-0 ADJ TO PH 9-0-9-8
1
1 SODIUM HYDROXiDE
ASSUME 50% |___ ____
7-D
RECORD. PHi--MjffesDIA20__ss?L < -) ASSUME 32% |_;______
ASEJijtjfcr< + ) HYDROCHLORIC ACID
]
28-D
STEAM EJECT V-932 FROM S8 INTO CV POUR IN I OCTANOL I HEAT TO 173-175 DEG F IN 55-65 MIN AND
[ l 30 i
1 588-A 1 30
CDRD: HTto^___DE& F 6 REG________DEG F ' \
IlNG S46 HEATING, RUN10' (268G) WATER
!
|
V-902
I|
ON AGITATOR 6 STEAM 6 DUMP INBARIUM! fiSSk Nj 16-B
CHLORIDE
I|
^ I HEAT TO 155-160 DEG F G STIR TO DISSOLVE 1
1
Y
iHBBl WHEN S46 COMPLETE, STRIKE V-902 AT 155-160F
H' i THRU UNDERSURFACE DISTRIBUTOR INTO CV IN
I 12-3 MIN
-U
I i Jr RECORD : STARTitCI^TOTAL MIN_^.__^.
HEAT CV TO 193-195 DEG F IN 10-15 MIN-
iyy,4
Jff2 J$TIR 60 MIN AT 193-195 F. RECORD START
AFTR 20 MIN S52 STIR RECORD PH_&C8-8-9-35
f , | IF NECESSARY, ADJ TO PH 8-S-9-3 ASSUME 50%
i J AND RECORD : PH_______ _
ASSUME 32%
I'&frn WHEN S52 STIR COMPLETE, FLOOD TO 180-190'
< ! (+/-18000G) AND STOP AGITATOR
j
II
I
I | WHEN INSTRUCTED BY PROCESSING AREA HALF WAY I
I I THRU PRESSING, DUMP I.N 1 OCTANOL, STIR
5 !'
i I MIN G STOP AGITATOR- RESUME PRESSING-
|
10
]I
*][%>
Tlla>
MStou
I
_
7-D i 28-D
588-A
10
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DUP050102126
DU P050102127
DUP050102128
DUP050102129
DUP050102130