Document nmVXK9XLaQKoj4QXwQYdY17Zz

&EPA United States Environmental Protection Agancy Office of Water and Haiardou* West* Washington, DC 20460 SPA 8700*12{Fft) May 19; JNO ` Solid Waste Identification and Listing of Hazardous Waste PLAINTIFF'S EXHIBIT CAP-1816 This package is a complete reprint of the EPA regulations identifying and listing hazardous waste that were promul gated under Section 3001 of the Resource Conservation and Recovery Act (RCRA) on May 19, 1980. If you need a copy of the preamble discussion to this regulation or a copy of other regulations for hazardous waste management that were promulgated under Subtitle C of RCRA please contact: Mr. Ed Cox U.S. Environmental Protection Agency P.O. Bldg. B Dalton and Liberty Streets Dock 14 Cincinnati, Ohio 45214 (513) 684-5362 1 CAPCO JEN 0004822 33119 Federal Regitter / Vol. 45, No. 98 / Monday, May 19, 1980 / Rules and Regulations PART 261--IDENTIFICATION AND LISTING OF HAZARDOUS WASTE Subpart A--Gentral Sec. 26].l Purpose and scope. 281.2 Definition of solid waste. 281.3 Definition of hazardous waste. 261.4 Exclusions. 261.5 Special requirements for hazardous waste produced by small quantity generators. 261.8 Special requirements for hazardous waste which is used. re-used. recycled or reclaimed. Subpart B--Criteria for Identifying the Characteriitlca of Hazardous Waste and tor Llaflng Hazardous Wastes 261.10 Criteria for identifying the characteristics of hazardous wastes. 261.11 Criteria for listing hazardous waste. Subpart C--Characteristics of Hazardous Waste 261.20 261.21 261.22 261.23 261.24 General. Characteristic of ignitability. Characteristic of corrosivity. Characteristic of reactivity. Characteristic of EP toxicity. Subpart D--Lists of Hazardous Wastes 281.30 General. 261.31 Hazardous wastes from non-specific sources. 261.32 Hazardous wastes from specific sources. 261.33 Discarded commercial chemical products and associated off-specification materials, containers and spill residues. Appendices Appendix I--Representative Sampling Methods Appendix 11--EP Toxicity Test Procedures Appendix ill--Chemical Analysis Test Methods Appendix IV--{Reserved for Radioactive Waste Test Methods] Appendix V--(Reserved for Infectious Waste Treatment Specifications! Appendix VI--[Reserved for Etioiogic Agents| Appendix VII--Basis for Listing Appendix VIII--Hazardous Constituents Authority: Secs. 1006. 2002(a). 3001, and 3002 of the Solid Waste Disposal Act. as amended by the Resource Conservation and Recovery Act of 1976. as amended (42 U.S.C. 6905. 6912. 6921 and 6922). Subpart A--General 261.1 Purpose and scope. (a) This Pari identifies those solid wastes which are subject to regulation as hazardous wastes under Parts 262 through 265 and Parts 122 through 124 of this Chapter and which are subject to " the notification requirements of Section 3010 of RCRA. In this Part: (1) Subpart A defines the terms "solid waste" and "hazardous waste," identifies those wastes which are excluded from regulation under Parts 262 through 265 and 122 through 124 and establishes special management requirements for hazardous waste produced by small quantity generators and hazardous waste which is used, re used, recycled or reclaimed. (2) Subpart B sets forth the criteria used by EPA to identify characteristics of hazardous waste and to list particular hazardous wastes. (3) Subpart C identifies characteristics of hazardous waste. (4) Subpart D lists particular hazardous wastes. (b) This Part identifies only some of the materials which are hazardous wastes under Sections 3007 and 7003 of RCRA. A material which is not a hazardous waste identified in this part is still a hazardous waste for purposes of those sections if: (1) In thftpase of Section 3007, EPA has reasomto believe that the material may be a hazardous waste within the meaning of Section 1004(5) of RCRA. (2) In the case of Section 7003, the statutory elements are established. 261.2 Definition of solid waste. (a) A solid wasfe"is any garbage, refuse, sludge or any ,other waste material which is qoi'excluded under 261.4(a). (b) An "other waste material" is any solid, liquid, semi-solid or contained gaseous material, resulting from industrial, commercial, mining or agricultural operations, or from community activities which: (1) Is discarded or is being accumulated, stored or physically, chemically or biologically treated prior to being discarded: or (2) Has served its original intended use and sometimes is discarded; or (3) Is a manufacuring or mining by product and.sometimes is discarded. (c) A malerialis "discarded" if it is abandoned (and not used, re-used, .reclaimed or recycled) by being: (1) Disposed of: or (2) Burned or incinerated, except where the material is being burned at afuel for the purpose of recovering usable energy: or (3) Physically, chemically, or biologically treated (other than burned or incinerated) in lieu of or prior to being disposed of. (d) A material is "disposed of' if it is discharged, deposited, injected, dumped, spilled, leaked or placed into or on any land or water so that such material or any constituent thereof may enter the environment or be emitted into the air or discharged into ground or surface waters. (e) A "manufacturing or mining by product" is a material that is not one of the primary products of a particular manufacturing or mining operation, is a secondary and incidental product of the particular operation and would not be solely and separately manufactured or mined by the particular manufacturing or mining operation. The term does not include an intermediate manufacturing or mining product which results from one of the steps in a manufacturing or mining process and is typically processed through the next step of the process within a short time. 261.3 Definition of hazardous waste. (a) A solid waste, as defined in 261.2, is a hazardous waste if: (1) It is not excluded from regulation as a hazardous waste under 261.4(b): and (2) It meets any of the following criteria: (i) It is listed in Subpart D and has not been excluded from the lists in Subpart D under 260.20 and 260.22 of this Chapter. (ii) It is a mixture of solid waste and one or more hazardous wastes listed in Subpart D and has not been excluded from this paragraph under 260.20 and 260.22 of this Chapter. (iii) It exhibits any of the characteristics of hazardous waste identified in Subpart C. (b) A solid waste which is not excluded from regulation under paragraph (a)(1) of this section becomes a hazardous waste when any of the following events occur: (1) In the case of a waste listed in Subpart D. when the waste first meets the listing description set forth in Subpart D. (2) In the case of a mixture of solid waste and one or more listed hazardous wastes, when a hazardous waste listed 1 CAPCO JEN 0004823 Federal Register / Vol. 45. No. 98 / Monday; May 19, 1980-/ Rules and Regulatibng in Subpart D is first added to the solid W^3) Jn the case of any other waste (including a waste mixture), when the waste exhibits any of the characteristics identified in Subpdrt C. (c) Unless and until it meets the criteria of paragraph (d): (1) A hazardous waste will remain a hazardous waste, (2) Any solid waste generated from the treatment, storage or disposal of a hazardous waste, including any sludge, spill residue, ash, emission control dust or leachate (but not including precipitation run-off), is a hazardous waster (d) Any solid waste described in paragraph (c) of this section is not a hazardous waste if it meets the following criteria: (1) In the case of any solid waste, it does not exhibit any of the characteristics of hazardous waste identified in Subpart C. (2) In the case of a waste which is a listed waste under Subpart D, contains a waste listed under Subpart D or is derived from a waste listed in Subpart D, it also has been excluded from paragraph (c) under 5 260,20 and 260.22 of this Chapter. 261.4 Exclusions. (a) Materials which are not solid wastes. The following materials are not solid wastes for the purpose of this Part: (1) (i) Domestic sewage: and (ii) Any mixture of domestic sewage and other wastes that passes through a sewer system to a publicly-owned treatment works for treatment. "Domestic sewage" means untreated sanitary wastes that pass through a sewer system. (2) Industrial wastewater discharges that are point source discharges subject to regulation under Section 402 of the Clean Water Act, as amended. [Comment: This exclusion applies only to the actual point source discharge. It does not exclude industrial wastewaters while they are-being collected, stored or treated before discharge, nor does it exclude sludges that are generated by industrial wastewater treatment.) (3) Irrigation return flows. (4) Source, special nuclear or by product material as defined by the Atomic Energy Act of 1954, as amended, 42 U.S.C. 2011 et seq. J5) Materials subjected to in-situ mining techniques which are nnL. removed from the ground as part of the extraction process. (b) Solid wastes which are not hazardous wastes. The following solid wastes are not hazardous wastes: (1) Household waste, including household waste that-has been collected, transported, stored, treated, . disposed, recovered (e.g., refuse-derived fuel) or reused. "Household waste" means any waste material (including garbage, trash and sanitary wastes in septic tanks) derived from households (including single and multiple residences, hotels and motels.) (2) Solid wastes generated by any of the following and which are returned to the soils as fertilizers: (i) The growing and harvesting of agricultural crops. (ii) The raising of animals, including animal manures. (3) Mining overburden returned to the mine site. (4) Fly ash waste, bottom ash waste, slag waste, and flue gas emission control waste generated primarily from the combustion of coal or other fossil fuels. (5) Drilling fluids, produced waters, and other wastes associated with the exploration, development, or production of crude oil. natural gas or geothermal energy. 261.5 Special requlrementsldr hazardous waste generated by'small quantity generators. , . (a) Except as otherwise provided in this section, if a person generates, in a calendar month, a total of less than 1000 kilograms of hazardous wastes, those wastes are not subject to regulation under Parts 262 through 265 and Parts 122 through 124 of 1(113,Chapter, and the notification requirements of Section 3010 of RCRA. _ jfit, ./ns to (b) If a person wliqse waste has been excluded from regulation under paragraph (a) of this Section accumulates hazardous wastes in quantities greater than 1000 kilograms, those accumulated wastes are subject to regulation under Parts 262 through 265 and Parts 122 through 124 of this Chapter, and the notification requirements of Section 3010 of RCRA. (c) If a person generates in a calendar month or accumulates at any time any of the following hazardous wastes in quantities greater than set forth below, those wastes are subject to regulation under Parts 262 through 265 and Parts 122 through 124 of this Chapter, and the notification requirements-ofSection 3010 of RCRA: ------ (1) One kilogram of any commercial A product or manufacturing chemical | Jintermediate having the generic name I listed in $ 261.33(e). (2) One kilogram of any off- specification commercial chemical product or manufacturing chemical intermediate which, if it met specifications, would have the generic';name listed in S 261.33(e). (3) Any containers identified in , < 5 261.33(c) that are larger than 20 liters ' in capacity: (4) 10 kilograms of inner liners from containers identified under 5 261.33(c); (5) 100 kilograms of any residue or contaminated soil, water or other debris resulting from the cleanup of a spill,.into or on any land or water, of any commercial chemical product or manufacturing chemical intermediate having the generic name listed in 261.33(e). (d) In order for hazardous waste to be excluded from regulation under this section, the generator must comply with 262.11 of this Chapter. He must also either treat or dispose of the waste in an on-site facility, or ensure delivery to an off-site treatment, storage or disposal facility, either of which is: (1) Permitted by EPA under Part 122 of this Chapter, or by a State with a hazardous waste management program authorized under Part 123 of this Chapter; (2) In interim status under Parts 122 and 265 of this Chapter: or. (3) Permitted, licensed, or registered by a State to manage municipal or industrial solid waste. (e) Hazardous waste subject to the reduced requirements of this section may be mixed with non-hazardous.. waste and remain subject to these reduced requirements even though the resultant mixture exceeds the quantity limitations identified in this section, unless the mixture meets any of the characteristics of hazardous waste identified in Subpart C. 261.6 Special requirements (or hazardous waste which la used, re-used, recycled or reclaimed. (a) Except as otherwise provided in paragraph (b) of this section, a hazardous waste which meets either of the following criteria is not subject to regulation under Parts 262 through 265 or Parts 122 through 124 of this Chapter, and is not subject to the notification : requirements of Section 3010 of RCRA until such time as the Administrator promulgates regulations to the contrary: (1) It is being beneficially used or re used or legitimately recycled or reclaimed. (2) It is being accumulated, stored or physically, chemically or biologically treated prior to beneficial use or re-use or legitimate recycling or reclamation. (b) A hazardous waste which is a sludge, or which is listed in Subpart D, or which contains one or more hazardous wastes listed in SubpaVt D; and which is transported or stored prior 1 CAPCO JEN 0004824- 33121 Federal Register / Vol. 45. No! 98 / Monday. May 19, 1980 / Rules and Regulations to being used, re-used, recycled or reclaimed is subject to the following requirements with respect to such transportation or storage: (1) Notification requirements under Section 3010 RCRA. (2) Part 262 of this Chapter. (3) Part 263 of this Chapter. (4) Subparts A. B, C. D and E of Part 264 of this Chapter. (5) Subparts A. B. C. D, E. G. H. I. J and L of Part 265 of this Chapter. (6) Parts 122 and 124 of this Chapter, with respect to storage facilities. Subpart B--Criteria for Identifying the Characteristics of Hazardous Waste and for Listing Hazardous Waste 261.10 Criteria for identifying the characteristics of hazardous waste. (a) The Administrator shall identify and define a characteristic of hazardous waste in Subpart C only upon determining that: (1) A solid waste that exhibits the characteristic may: (1) Cause, or significantly contribute to. an increase in mortality or an increase in serious irreversible, or incapacitating reversible, illness: or (iij Pose a substantial present or potential hazard to human health or the environment when it is improperly treated, stored, transported, disposed of or otherwise managed: and (2) The characteristic can be: (i) Measured by an available standardized test method which is reasonably within the capability of generators of solid waste or private sector laboratories that are available to serve generators of solid waste: or (ii) Reasonably detected by generators of solid waste through their knowledge of their waste. 261.11 Criteria for listing hazardous , waste. (a) The Administrator shall list a solid waste as a hazardous waste only upon determining that the solid waste meets one of the following criteria: (1) It exhibits any of the characteristics of hazardous wqste identified in Subpart C. (2) It has been found to be fatal to humans in low doses or. in the absence of data on human toxicity, it has been shown in studies to have an oral LD 50 toxicity (rat) of less than 50 milligrams per kilogram, an inhalation LCSu toxicity (rat) of less than 2 milligrams per liter, or a dermal LD 50 toxicity (rabbit) of less than 200 milligrams per kilogram or is otherwise capable of causing or significantly contributing to an increase in serious irreversible, or incapacitating reversible, illness. (Waste listed in accordance with these criteria will be designated Acute-Hazardous Waste.-) (3) It contains any of the toxic constituents listed in Appendix VIII . unless, after considering any of the following factors, the Administrator concludes that the waste is not capable of posing a substantial present or potential hazard to human health or the environment when improperly treated, stored, transported or disposed of. or otherwise managed: (i) The nature of the toxicity presented by the constituent. (ii) The concentration of the constituent in the waste. (iii) The potential of the constituent or any toxic degradation product of the constituent to migrate from the waste into the environment under the types of improper management considered in paragraph (a)(3)(vii) of this section. (iv) The persistence of the constituent or any toxic degradation product of the constituent (v) The potential for the constituent or any toxic degradation product of the constituent.to degrade into non-harmful constituents end the rate of degradation. (vi) The degree to which the constituent or any degradation product of the constituent bioaccumulates in ecosystems. (vii) The plausible types of improper management to which the waste could be subjected. (viii) The quantities of the waste generated at individual generation sites or on a, regional or national basis. (ix) The nature and severity of the human health mitiSrfelttttmental damage that has occurred as a result of the improper management of wastes containing the constituent. (x) Action taken by other governmental agencies or regulatory programs based on the health or environmental hazard posed by the waste or waste qonstituent. (xi) Such other factors as may be appropriate. Substances will be listed on Appendix VIII only if they have been shown in scientific studies to have toxic, carcinogenic, mutagenic or teratogenic effects on humans or other life forms. (Wastes listed in accordance with these criteria .will be designated-Toxic waste*) (b) The Administrator may list classes or types of solid waste as hazardous waste if he has reason to believe that individual wastes, within the class or type of waste, typically or frequently are hazardous under the definition of hazardous waste found in Section 1004(5) of the Act. (c) The Administrator will use the ir criteria for listing specified in this section to establish the exclusion limit referred to in 261.5(c). Subpart C--Characteristics of Hazardous Waste 261.20 General. (a) A solid waste, as defined in 261.2, which is. not excluded.fron; " : regulation as a hazardous waste under'' 261.4(b), is a hazardous waste if it exhibits any of the characteristics "" identified in this Subpart. [Comment: 262.11 of this Chapter sets' forth the generator's responsibility t0--' determine whether his waste exhibits one or more of the characteristics identified in this Subpartj (b) A hazardous waste which is identified by a characteristic in this subpart, but is not listed as a hazardous waste in Subpart D. is assigned the EPA Hazardous Waste Number set forth in-' the respective characteristic in this Subpart. This number must be used in complying with the notification . requirements of Section 3010 of the Act and certain recordkeeping and reporti requirements under Parts 262 through! 265 and Part 122 of this Chapter. (c) For purposes of this Subpart, ths-c Administrator will consider a sample obtained using any of the applicable } sampling methods specified in Appen ` I to be a representative sample withinthe meaning of Part 260 of this Chapt- (Comment: Since the Appendix I sampling methods are not being fort adopted by the Administrator, a pen who desires to employ an alternative, sampling method is not required to demonstrate the equivalency of hie.,; method under the procedures set fort'' 260.20 and 260.21.j 261.21 Characteristic ol IgniUblitty. (a) A solid waste exhibits the * characteristic of ignitability if a representative sample of the waste any of the following properties: (1) It is a liquid, other than an aq< solution containing less than 24 pe: alcohol by'volume, and has a flash. less than 60-C (140`F). as determined,, a Pensky-Martens Closed Cup Tester."* using the test method specified in AJ> Standard D-93-79. or a Setaflash Clr Cup Tester, using the test method specified in ASTM standard D-327* or as determined by an equivalent method approved by the Adminiftra under the procedures set forth in 260.20 and 260.21.1 * ASTM Standards are available from ASO* I Race Street. Philadelphia. PA in. 1 CAPCO JEN 0004-825 Federal Register / Vol. 45, No. 98 / Monday. May 19. 1980 / Rules and Regulations (2) It is not a liquid and is capable, under standard temperature and pressure, of causing fire through friction, absorption of moisture or spontaneous chemical changes and, when ignited, bums so vigorously and persistently that is creates a hazard. (3) It is an ignitable compressed gas as defined in 49 CFR 173.300 and as determined by the test methods described in that regulation or equivalent test methods approved by the Administrator under 260.20 and 260.21. (4) It is an oxidizer as defined in 49 CFR 173.151. (b) A solid waste that exhibits the characteristic of ignitability. but is not listed as a hazardous waste in Subpart D, has the EPA Hazardous Waste Number of D001. 261.22 Characteristic of corrosivity. (a) A solid waste exhibits the characteristic of corrosivity if a representative sample of the waste has either of the following properties: (1) It is aqueous and has a pH less than or equal to 2 or greater than or equal to 12.5, as determined by a pH meter using either the test method specified in the "Test Methods for the Evaluation of Solid Waste, Physical/ Chemical Methods" '(also described in "Methods for Analysis of Water and Wastes" EPA 600/4-79-020, March 1979). or an equivalent test method approved by the Administrator under the procedures set forth in 260.20 and 260.21. (2) It is a liquid and corrodes steel (SAE1020) at a rate greater than 6.35 mm (0.250 inch) per year at a test temperature of 55'C (130"F) as determined by the test method specified in NACE (National Association of Corrosion Engineers) Standard TM-01693 as standardized in "Test Methods for the Evaluation of Solid Waste, Physicai/Chemicai Methods," or an equivalent test method approved by the Administrator upder the procedures set forth in 5 260.20-and 260.21. (b) A solid waste that exhibits the characteristic of corrosivity, but is not listed as a hazardous waste in Subpart D. has the EPA Hazardous Waste Number of D002. , uocumem is available from Solid W Information. U.S. Environmental Protection i a W. St. Clair Street. Cincinnati, Ohio 45268 `Th* NACE Standard i available fromjfri National Allocation of Corroaion Engineers Box M6. Katy. Texaa 77450. 5 261.23 Characteristic of reactivity. (a) A solid waste exhibits the characteristic of reactivity if a representative sample of the waste has any of the following properties: ' (1) It is normally unstable and readily undergoes violent change without detonating. (2) It reacts violently with water. (3) it forms potentially explosive mixtures with water. (4) When mixed with water, it generates toxic gases, vapors or fumes in a quantity sufficient to present a danger to human health or the environment. (5) It is a cyanide or sulfide bearing waste which, when exposed to pH conditions between 2 and 12.5. can generate toxic gases, vapors or fumes in a quantity sufficient to present a danger to human health or the environment. (6) It is capable of detonation or explosive reaction if it is subjected to a strong initiating source or if heated under confinement. (7) It is readily capable of detonation or explosive decomposition or reaction at standard temperature and pressure. (8) It is a forbidden explosive as defined in 49 CFR 173.51, or a Class A explosive as defined in 49 CFR 173.53 or a Class B explosive as defined in 49 CFR 173.88. (b) A solid waste that exhibits the characteristic of reactivity, but is not listed as a hazardous waste in Subpart D, has. the EPA-Hazeedour Wat Numberof DO08* :. 261.24 Characteristic of, EP Toxicity. (a) A solid waste exhibits the characteristic of EP toxicity if. using the test methods described in Appendix II or equivalent methods approved by the Administrator under the procedures set forth in 260.20 and 260.21, the extract from a representative sample of the waste contains any of the contaminants listed in Table I at a concentration equal to or greater than the respective value given in that Table. Where the waste contains less than 0.5 percent filterable solids, the waste itself, after filtering, is considered to be the extract for the purposes of this section. (b) A solid waste that exhibits the ' characteristic of EP toxicity, but is not listed as a hazardous waste in Subpart D, has the EPA Hazardous Waste Number specified in Table I whichcorresponds to the toxic contaminant causing it to be hazardous. Table I.--Maximum Concentration of Contaminants for Charactarlstle of EP Toxicity-- Continued EPA hazardous wilt* number Contamnant Maxmum concentration (mrfbgrame per Mar) 0004 .......... 0005 . 0006 ............ 0007............. 0008............. 0009............. 0010...... - .... 0011............. 0012......... 0013............. 0014 . 0015.............. 0016... 0017____ ArsiruC.......................... .. Banum................................... Cadmium . . ...................... . Chromium....................... ...... Lead........................................ Mercury........ .................... ..... Selenium............. ................... Silver Endnn (1.2.3.4.10.10- hexechioro* .7*epoxy* 1.4,4a.5,6,7,8.8a- octahydro*1.4 -endo. endo* 5,B-dim*th*no naphthalene lindane (1.2.3.4.5.6hexacMorocydohexan*. gamma isom*r. MethoxycWor (1.1.1* TncWoro-2.2-tw (p* methoxyphenyljethane). Toxaphene (Ci*HmC4. Technical chlorinated camphene. 67*69 percent chlorine). 2.4-0. (2.4* DiChSorophenoryacette" acid) 2.4.5-TP S4v*x (2.4.5- Tnchiorophenoxypropionic tod) 50 1000 10 $0 50 02 1.0 50 002 04 100 05 too to Subpart D--Lists of Hazardous Wastes 261.30 Genoral. (a) A solid waste is a hazardous waste if it is listed in this Subpart, unless it has been excluded from this list under 260.20 and 260.22. (b) The Administrator will indicate his basis for listing the classes or types of wastes listed in this Subpart by employing one or more of the following Hazard Codes: tgrvtabt* Wait*................ Corrosive Waste............... Rtactrv* Was1*................ EP Tone Waste-.............. Acuta Hazardous Wane... Toxic Waste...... ...... ........ . 'Appendix VII identifies the constituent which caused the Administrator to list the waste as an-8PJFoxTd-W8e**(BJ orToxRTWraWfFFin 261.31 and 261.32. (c) Each hazardous waste listed in this Subpart is assigned an EPA Hazardous Waste Number which precedes the name of the waste. This number must be used in complying with the notification requirements of Section 3010 of the Act and certain recordkeeping and reporting requirements under Parts 262 through 265 and Part 122 of this Chapter. (d) Certain of the hazardous wastes listed in 261.31 or 261.32 have exclusion limits that refer to 261.5(c)(5). 1 CAPCO JEN 0004.826 '''' . 33123 > '' ;' 'r '""' :' -'7 * ' ' . ' " . i ' Federal RegUter / Vol. 45, No. 96 / Monday. May 19, I960 / Rules and Regulations : $ 261.31 Httardou* watt* from nonapaclfic aoureaa. Industry yid EPA hazardous waste No Generic: P001.. Vf002. ^F003* VF004 \F005.. F006... F00?.. F008... F009... F010*.. F011... F0t2.. F013.. F014... F015... F016. Hazardous waste Hazard code The spent hetogeneled solvents used m degreasing, tetrechloroeihytene. trichloroethylene. methylene eNonde. I.I.l.tncNoroethane, carbon tetrachloride. and the chlorinated fluorocarbons; and ihjdgtt from the recovary ol these solvents n degrees*? operations. The spam hatogenated advents, tetrechtoroethyiene. methytene chfonde. tneWoroethytene. t.l.MncMoroethane. crtorotoenzene, 1.1.2tnehioro-i.2.2-tnfuoroethene. o-ifichtorobenzene. tncNorofkioromethan# and the sM bottoms from the recovery of these soNant*. The spent non-halogenated solvents, xylene, acetone, ethyl acetate, ethyl benzene, ethyl ether, n-butyl alcohol, cyclohexanone, and ihe stN bottoms from the recovery of these solvents. The spent non-halogenatad solvents, cresols and cresyK acid, nitrobenzene, and the sbN bottoms from the recovery of these solvents.......... . The spent non-hatogenated solvents, methanol, toluene, methyl ethyl ketone, methyl isobutyt ketone, carbon &sulfide, tsobutanot. pyndoe and the stilt bottoms from the recovery of these solvents^ Wasteweter treatment sludges from electroplating operations....-............. ---.............r................. ........................... ........--------------- --------------- . Spent plating bath solutions from electroplating operations........................ -................-............................--...... ............ ......... ......... .................... Plating bath sludges from the bottom of plating baths from electroplating operations....................... ------- ------ ------- ------- -....... --........... ... . Spent stripping and cleaning bath solutions horn electroplating operations--...............................................................................-.................. . Quencfeng bath sludge from oil baths from metal heat treating operations...................................... -.............-................................ ........... ........ Spent solutions from salt bath pot cleaning from metal heat treating operations . Quenching wastewater treatment sludges from metal heat treating operations............................................................................................ . Flotation tailings from selective flotation from mineral metals recovery operations....... .........................-........................-...................................... . Cyamdation wastewater treatment tailing pond sediment from trowel metals recovery operations.................. ................... -.............................. Spent cyanide Oath solutions from rrwwaJ metals recovery operations............. Dewatered a* pollution control scrubber sludges from coke ovens and blast ft* naces CD (CD.T) * CD (R.D (R.D (R,TV (R.D (R.D <T) cn m (R.D 261.32 Hazardous waste from specific sources. Industry and EPA hazardous waste No Hazardous waste Hazard code Wood Preservation. KOOI .. Inorgaruc Pigments: K002..................................... K003 ....... ,,........................... KOW............................... .. K005 ..................................... K006...................................... K007...................................... K008,.... ............................... Organc Chemicals: K009................................... KOIO....................................... KO11 KOI 2 KOI 3 K014 KOI 5 K016..................................... KOI 7 KOtS..................................... K01&....................................... K020................................... . K021........... ........................ K022......................... ............. K0?3 K024...,, ................................ K025 K026.............-..................... K0?7 K028...................................... . K079 K030...... -............................. Pesticides: K031 K03&U... ........................... ... K033 -* K034 # *" K03S....... ............................... K036............... -................... K037 _ K033....................................... K039 K040-......... ............. ,,............ K041 K042____________ .__ _____ K043___ Eiptosrven; K044 K045-______ ._________ ..... K04S . . . K047________ -___________ Petroleum Refinm? K04S..________________ ___ K040____ ________________ K050______________ _______ K0S1______ ______ ________ K0S2______ ____________ .... Leather Tanrang Freshing: K053________ ____________ Bottom sediment sludge from the treatment of wastewaters from wood preserving processes that use creosote and/or pentachlorophenot.... (T) Wastewater treatment sludge from the production of chrome yellow and orange pigments......................-.......... Wastewater treatment sludge from me product** o| molybdate orange pigments................................................. Wastewater treatment sludge from the producbbnW zmc yellow pigments....... Wastewater treatment sludge from the productiontrt chrome green pigments... Wastewater treatment sludge from the producboaof chrome oxide green pigments (anhydrous and hydrated).., Wastewater treatment sludge from the production of ron blue pigments........... Oven residue from the production ol chrome oxide green pigments................... ............................. ............. ............. . ............................. ......... .................. ......... .. ................. ............................. ...................... -.... CD CD <D CD CD CD CD Ostdtabon bottoms from (he production of acetaldehyde from ethylene........ ............... ............ --......... ............... DutUatoo side cuts from the production ol acetaldehyde from ethylene............ Bottom stream from the wastewater stnpper m the production of ecrytomtnie... Still bottoms from the foal purification of acrytonrtnte m the production of acrytorntnle --...... ................... Bottom stream from the acetonrtnle column the production of acrylonitrile.... Bottoms from the acetroratnle purification column m the production ol acrytonitrSe................................................ Stilt bottoms from the disUlabon of benxyf cWonde............................ ....................... .... ... ..... ... ---- ............. . Heevy ends or cksbUebon residues from the production of carbon tetrachlonde. Heavy ends (sUi bottoms) from the punfiawon column m the production of epichtorohydnn.......... ...................... Heavy ends from fractionation m ethyf chloride production .... .......... Heavy ends from the distillation ol ethytene dichloode ei ettytene itchlonde production....................................... Heavy ends from the distillation ol vmyt cWoode xt vidyfUUoridalfiUnbmer production.................... .................... Aqueous spent anbmony catalyst waste from nuorocyeffof^r pr^duchon.......... DsbllatJon bottom tars from the production of phenoUacetonf gom/umene.... DsWabon bghl ends from the production of phthabc imhydnde from naphthalene DsUtation bottoms from the production of phthakc anhydnde from naphthalene OuWiabon bottoms from the producbon of ntrobenzene by the ntrabon of benzene................... ......................... Stopping stin tails from the producbon of methyl ethyl pyndmes...... ................... Centrrtuge residue from toluene desocyanato production.............................. ..... Spent catalyst from the hydrocMcnnator reactor in the producbon ot t.t.t-tncMoroethane......... .......................... Waste from the product stream stnpper m the producbon of l.l.t-tnchloroethane....................... ............ .............. Column bottoms or heavy ends from the combined production of trichloroethylene and perchioroethyiene-------- (D (D (R.D (D (R.D m (D (D (T) (D (D m (D (D (D (D (D (D (R.D (D fD (D By-products setts generated n the production of MSMA and ceeodyfcc acd.......................... ...... Wastewater treatment sludge from the production ot ctotdane...................................................... Wastewater and scrub water from the cNormebon of-dydopentarkene the production of chlordane................. Filter aohds from the filtrabon ol hexachlorocyclopenta^erM m the producbon ol chlordane........................... . Wastewater treatment sludges generated m the prediction of creosote........................................ SM bottoms from toluene redamatcn dwblabon in the production of dsuHoton...... .--....... . Wastewater treatment sludges from die production of dotfoton.............. ------------------ --------- --- Wastewater from the washing end stripping of ptorete producbon.................................................. ............ -- fitter cake from the filtrabon of dethytphosphorodthonc aod m the production of phorate...--......................... Wastewatar treatment sludge from the production of phorale... --------- ... . .. Wastewater treatment sludge from the production of toxaphene... Heavy ends or dsMabon residues from the disbttsbon of tetrechlorobenzene n the production of 2.4.5-T... 2.0-Ochlorophenoi waste from the production of 2,4-D........................... ............... ......... ......................... ... (D (D (D (D CD (D (D CD m CD (D CD Wastewater beatment sludges from the manufacturing and processing ot expiosrves Spent carbon from the treatment of wastewater contammg exptosrvee................................. .-- ..... Wastewater treatment sludges from the manufacturing, formulation end toedng of leadbesed mr&ebng compounds.. Pmk/red water frogjJNT operabone___......--------- -------- --------------------- ....---------------------------------...--------- (R) (R) CD (R) Dissolved ar flotabon (OAF) float from the petroleum refining industry______________ ______________ -- Slop oJ emulsion solids from the pebdeum refinmg mdustry.. Heat exchanger bud cleaning sludge from the petroleum reftreng mduefry... API saperetor sludge from the pebdeum refining wdustry.....,,,-------- ------------Tank bottoms (leaded) from the petroleum refining mdustry-. .............. ........ CD (D m CD CD Chrome (blue) tnmmmgs generated by the foaowmg subcategones of the leather Unrwig and firxshmg vidustry; her pulp/chrome tan/retan/ wet fresh; her save/chrome tan/retan/wet finish; retan/wet finish; no beemhouse. through-the-CAie. and shearbng. 3 CAPCO JEN 0004827 Federal RegUter / Vol.' 45. No. 98 / Monday; May l9,'l5aO~/. Rulegfand'RegulaUdria^-, ':' ; 261.32 Hazardous waata from apactflc aourcaa. --Commute - - -v Industry and EPA twzardous waata No KM5... KOSt... KOST... KOSS... Kosg... Iron and Steen K060............ ............ Koet... ... ...... KOW., K063___ Primay Copper KOSa.... Pnmay Lead: K005..,,.... Pnmay Zinc: KOM- K007. KOM_______ _____ Secondary bead: K060... Hazardous wasta Hazard coda Ctvom. (tout) Mvmg g**nt<il! by m* knowing mOeiwgonm ol ttw Kith* umng and tomtong njuuy; tar pulp/efmita Un/rrtn/ MI man tav tiw/ctotm* twt/nun/wwt Kuan; (alan/Mt totals no boambooa^ trvougfvtta-bltjv; and ihaartng. Bulling dual jawattd by tha following aubcalagonaa o( Iba laamar Unmng and towitaig vxtovby; ha pmp/cbnvna lan/tatan/waf totals tav sava/chroma lan/iatan/wat Ivwls ratan/wat Imt/s no baambouaa: and Bvooflh-tha-blua. . Saww> aaaannga ganaatad by tta following aubcalagonaa of fba laamay tannaig and tombing nduaty: tav pulp/cbnana tan/ratan/wat (man. baa aava/cbroma tan/ratan/wat fawn; ratan/wat Imnh; no baamhooaa: tb/ough-tba-blua, and abaanatg. Wastawata Militant sludgas ganaalad by tba following sobcatagonaa of tba laatha tanning and totaling aaXatryi Itaa pulp/cfaonta Un/ ratan/wat town: baa u<a/chroma tan/ratan/wat hwb: /atan/wat town: no baarnhouaa: tbrough-tbaJHoa and ibaartng. . Waatawata Militant akrdgai ganaalad by tba following aoboatagonai of lha laatba lanrang and hwbaig ndutty baa ptop/obroma Un/ ralan/wal towh: baa aava/cbroma lan/ratan/wat totals and tJvixjgb-tbablua . Waatawata traatmant abrdgaa ganaatad by tha following aubcaiagory ol tha laatba tannaig and towhaig industry: baa aava/non-chroma tan/ratan/wat totals (I) (I) (T) (I) (R, T) (R> . Ammonia SUI lana IbJdga bom Coking opaabons.---...-------- --------------------------- ---------------------.-- ------------------------- ------------. Eitwiion conbof dgat/ludga bom tba alactnc fumaca pnxtoction of alaaf.........--------------- ------------- -----------------------------------------------. Spam padda Squor bom alaa towhmg opaabona.-........................................ -......................---------------- ---- ---------------------------------------. Sludga bom tona baalmant ol apant piclila totuot bom ataaf towhmg opaabona......................................................... ............................... . Acid plant blowdown aluny/aludga raautbng bom tba thickamng of blowdown akary bom pnmay coppa production............................ . Surtaca impoundment aebda contained m and dredged bom aurtaco anpoundmanta at pnmvy lead amattmg faobbaa------------- --------- m m (C.1) m m m . Sludge bom boatmen! ol proceas waatawata and/a aed plant blowdown bom primary one production... . Elecbofybc anode abmaa/sludgaa bom pnmary amc prodjcbon.................................... ................... ....... --. . Cadnvum plant laacb raaidua (von oxide) bom pnmary amc production........................................................... . Enwaon conbol duat/aludge bom aacondary lead totalling....................................................................... ..... m. m m (T) 261.33 Discarded Commercial Chemical Products, OH-Speclficatlon Species, Containers, and Spill Reslduea Thereof. The following materials or items are hazardous wastes if and when they are discarded or intended to be discarded: (a) Any commercial chemical product, or manufacturing chemical intermediate having the generic name listed in paragraphs (e) or (f) of this section. (b) Any off-specification commercial chemical product or manufacturing chemical intermediate which, if it met specifications, would have the generic name listed in paragraphs (e) or (0 of this section. (c) Any container or inner liner removed from a container that has been used to hold any commercial chemical product or manufacturing chemical a intermediate having the generic name listed in paragraph (e) of this section, unless: (1) The container or inner liner has been triple rinsed using a solvent capable of removing the commercial chemical product or manufacturing chemical intermediate; (2) The container dr inner liner has been cleaned by another method that has been shown in the scientific literature, or by tests conducted by the generator, to achieve equivalent removal; or (3) In the case of a container, the inner liner that prevented contact of the commercial chemical product or manufacturing chemical intermediate with the container, has been removeeh" (d) Any residue or contaminated soil, water or other debris resulting from the cleanup of a spill, into or on any land or water, of any commercial chemical product or manufacturing chemical intermediate having the generic name listed in paragraphs (e) or (0 of this Section. [Comment: The phrase "commercial chemical product or manufacturing chemical intermediate havingtthe generic name listed in. . .'"refers to a chemical substance which is- manufactured or formulated for commercial or manufacturing use. It does not refer to a material, such as a manufacturing process waste, that contains any of the substances listed in paragraphs (e) or (f). Where a manufacturing process waste is deemed to be a hazardous waste because it contains a substaBeeiluitqd.in 'paragraphs (eljd^ff^jmelfwaste will be " listed in eitherfY61.31 or 261.32 or will" be identified as a hazardous waste by*"' the characteristics set forth in Subpart C"* of this Part.]__ (e) The commercial chemical products or manufacturing chemical intermediates, referred to in paragraphs (a) through (d) of this section, are identified as acute hazardous wastes (H) and are subject to the small quantity exclusion defined in $ 261.5(c). These wastes and their corresponding EPA Hazardous Waste Numbers are: Hazardous wasta No. Substanca/ *060 s*a PO V* 1091 aaa P057 (Acatato)phany1mareury saa P0A2 AcMona cyanohydrin saa PO09 P001_____ 3^a)pht*Acatonyfeanzy9-4-hydroxyeournann salts P002_____ 1*AcatyL2*trouraa P003~____ Aerotan AgannsaaPOO? Agroaan GN 5 aaa P092 Akkcwt saa P009 AfcMan aaa PO40 and --Continued Hazardous wasta No Substanca' P004......... Attm Atgunyan sat POOS POOS........ . AUyt alcohol P00e.,.~.... Aluminum phoaphida (ft) AlVfT aaa P037 Ammoathytana aaa P054 P007.... ... MAmrtomathyfy-Owtsoxazolol P008-....... 4-Amnopyndna Ammonium malavanadata sao P119 P009-....... Ammonum post# (R) ANTIMUON WM saa P092 ANTURAT aaa P073 AOUATHOt saa POM AflETlT saa P020 P010......... Areancaed P011......... Arsanic pantonda P012...~.... Arsanetnoada Athrombm aaa POOt AVUftOL saa P006 Azndana saa P054 AZOFOS saa P061 Azophos saa P061 BANTU saa P0?2 P013......... Banumeyamdt 8ASENITE saa P020 BCMEsaaPOIS P014......... Baraanathiol Daraoapn saa POSO POiS......... Baryttum dust P016 ......... BtstcNoromathyO athsr 8LA0AN44 saa P071 P017m..m.^. Bromoacatons P018.......... Brnona- P019_____ 2*Butanona paronda BUFEN saa P092 Butaphana saa P020 P020......... 2*sac*ButyM.6-tfnrtrophanol P021....... . Caicuneyamda CALOON saa P020 P022_____ Carbon dtsuffida CERESAN aaa P092 CERESAN UNIVERSAL aaa P092 CHEMOX GENERAL saa P020 CHEMOX P.E. saa P020 CHEM-TOL saa POM P023....... .. Chkxoacataldahyda P024_.,,.... p-CNoroanAna P025____ 1*(p-Chtarobanzoyl>*5-rnathO)(y-?'matfiytndo*a-3' eatcaod P020_____ HdCMorophanyl)tNouraa P027___ O-CNoroproponrtnia P028_____ alphaOdorotoAiana P029_____ Coppar cysrsda CREIOX aaa P100 Coumacfen saa POOt CoumaJan saa POOt POM Cyamdaa i CAPCO JEN 0004-828 33125 Federal Register / Vol. 45,' No. 98 / Monday, May 19, 1980 / Rules and Regulations Hazardous waste No Hazardous wait# No. Hazardous waste No. Substance 1 P031 P032-. P033 P034 POOS P036 P037 . P038. P039. P040 P041 P042 P043 . P044. P045 P046 P047 P046 P049 POSO POS P052 P953 P054 P055 P056 P057 P058 P059. P060 P06I P063 . Cyanogen Cyanggen brormdt Cyanogen chloride MAfl-FRlN see P001 CyckxJan see PO50 MARTIN'O MAR-FRIN see P001 2-CyCl0heryl-4 6-dirutrophenol MAVERAN m P001 O-CON see P001 MEGATOX see P005 DETHMOR see P001 P065. .. Mercury futmnate OETHNEL see P001 MERSOUTE see P092 DFP see P043 METACID SO see P071 2.4-OcMoropnenoyyacetic acid (2,4-0) METAFOS see P071 D<worophenytarsine METAPHOR see P071 Dicyanogen see P03t METAPHOS see P071 Oetdnn METASOL 30 see P092 OiELOREX see POO7 P066 . ... Methomyt . 0*etny!arstne P067........ 2-Mathyiazndme 0.0-0ethyl-S-l2-tethynh*o)eihyl)este ol phot* METHYL-E 605 see P071 phofothioc acid P068.. . Methyl hydrazine 0.0 Oiemyi-0-(2-pyraxinyi)phosphoroth'Oate Methyl isocyanate see P064 0.0-Diethyl phosphone aod. O-p-mtrophenyf ester P069..,,.... 2-Methyltactonitnle 3.4-Dihydroxy-aipha-(methyiamno)-rt>ethyi benzyl alcohof P070...... 2-Mfthyi-2-(methyttha)propionaidehyde-o(tnethytcarbonyl) oxime . Di-csopropytfiuoropnosphete OimETATE see P044 METHYL NIRON see P042 P071.. ... Methylparathion 1,4 5.6-Dimethanonaphthaltne. 1.2.3.4,10,10- METRON see P071 hexachioro-i,4,4a,5,8>6a-hexahydro endo, MOLE OEATH see Pioa enoo see P060 MOUSE-NOTS see P106 Ounethoaie MOUSE-RID see PlOa 3.3-0>metnyi-1 -(methyithio)-2-butanone-0((methytamino)carbonyl) oxime MOUSE-TOX see P108 MUSCIMOL see P007 atpha.aipha-Oimethyiphenethytamme Oinitrccycionexylphenol see P034 P072 P073 i.Naphthyf-2-thourea Nickel carbonyl 4 6-Dirwl/0-0 cresol and salts P074 Nickel cyarude 2.4-Dtmtropnenol OiNOSEB see P020 DiNOSEBE see P020 Oisutloton see P039 2.4-Ottuobiuret DNBP see P020 OOLCO MOUSE CEREAL see PJ08 DOW GENERAL see P020 P075. . P076 .. P077 P078.... P079..... . P080. P081., P082.. Nicotine and salts Nitnc oxide p-Nitroaniltnf Nitrogen dioxide Nitrogen peroxide Nitrogen tetroside Nitroglycerine (R) N-Nitn&bdimethylanvne OOW GENERAL WEED KtLLER see P020 P063........ N-Nitrosodiphenytamine DOW SELECTIVE WEED KILLER see P020 OOWiCiDE G see P090 OYANACIDE see P092 EASTERN STATES DUOCtOE see P001 ELGETOL see P020 Endosutfan Endnn Epinephrine see P042 Ethytcyamde Emylenediamne Ethyieneimme FASCO FASCRAT POWDER see P001 FEMMA see P091 Feme cyarude Fluorine 2 Fiuoroacetamide Fiuoroacetic acid. sod<um salt FOLOOOL-SO see P071 FOLOOOL M see P071 FOSFERNO M 50 see P071 fratol see POSfi Fulminate o! mercury see P065 FUNGITOX OR see P092 FUSSOF see P057 GALLOTOX see PQ92 GEARPHOS see P071 GERUTOX see P020 Heptachlor 1.2,3.4. io.iO-He*acworo-i.4.4a.5.8.8a- hexahydro-1,4 5.6-endo, endo-cfcmethenoniph- thaiene . P084 . . N-Nitrosomethyfvwiylamine NYIMERATE see P092 OCTALOX see P037 POflS.. , Octamethytpyrophosphoramide OCTAN see P092 P086. Oleyt alcohol condensed with 2 moles ethylene oxide OMPA see P08S OMPACIOE see P085 OMPAX see P08S I P087 . . . Osmium tetroxide . P088... . 7-OxabiCyCk>(22tlriepttw-2.3-d*^rtooxyhceod PANIVARFIN see P001 ` ' ' PANORAM 0-3feP037 PANTHERINE see P007 * PANWARFIN setfPWi-'5'` POflS .... Parathion ^ PCP see P090 PENNCAP-M see P071 PENOXYL CARBON N see P048 P090.. .. PentecMorophenol Pentachlorophenate see P090 PENTA-KILL see P090 PENTASOL see P090 PENWAR see P090 PERMIC1DE see P090 PERMAGUARO see P090 PERMATOX see P090 PERMITE see P090 PERTOX see P090 PESTOX til see Pfte5 t.4.5.6.7,7-Hexachloro-cyckc-S-norbomene-2.3dimethanol sulfite see P05O Hexachioropropene * Hexaetnyl tetraphosphate HOSTAOUICK see P092 HOSTAOUIK see P092 Hydrazomethane see POOS Hydrocyanic aod ILLOXOL see P037 iNDOCI see P025 Indomethacm see P025 INSECTOPHENE see P050 tsodrm see P060 isocyanc aod. methyl ester KILOSEB see P020 KOP-THfODAN see P050 KWtK-KlLseePIOS KWIKSAN see P092 kumadER see POOt KYPFARIN see POOt LEYTOSAN see P092 LIOUIPHENE see P092 PHENMAO see P092 PHENOTAN see P020 P091......... Phenyl dicWoroarame Phenyl mercaptan see P014 P092......... Phenytmercury acetate P093....... N Phenytttsourea PHILIPS 1661 tee P006 PHIX see P092 . P094......... Phorate P095........ Phosgene P096. Phosphate P097. . .. Phosphorothioic aod. 0.0-dimethyl ester. Chester with N.N-dimethyl benzene sutfonarmde Phosphorothoc acid 0.0-dimethyl-0-{p-mtro phenyl) ester see P071 PIED PIPER MOUSE SEEO tee P106 P096 ..... Potassium cyanide P099 ...... PousMJm s*Ner cyartde PREMERGE m P020 P100 .... i.2-Propenedc( Propargyl alcohol see Pt02 PtOI . .. P/optomtnle Pi02........ 2-Propyn-l-ol PROTHROUAOIN See P001 QUtCKSAM tee P092 OUINTOX tee P037 RAT AND MICE BAIT tee POOt RAT-A-WAY tee P001 RAT-B-GON tee POOt RAT-O-CIDE n see POOt RAT-GUARD see POOt RAT-KILL see POOt RAT-MIX tee P001 RATS-NO-MORE tee P001 RAT-OLA See POOt RATOREX see P001 RATTUNAL tee P001 RAT-TROL see P001 RO-DETH tee P00I RO-OEX tee P106 ROSEX tee P001 ROUGH & REAOY MOUSE MIX tee P001 SANASEEO see P106 SANTOBRITE see P090 SANTOPHEN see P090 SANTOPHEN 20 see P090 SCHRADAN see P085 P103..... Seienourea P104......... SfverCyamde SMITE tee Pt05 SPARlC see P020 SPOR-KIL see P092 SPRAY-TROL BRANO RODEN-TROL see P001 SPURGE see P020 P105........Sodium azide SodKim coumadn see POOt P106 ... Sodwn cyanide Sodium ftuoroacetete see P0S6 SOOlUU WARFARIN see P001 SOLFARIN see P001 S0LF08LACK BB tee P048 SOLFOBLACK SB see P048 PI07........ Strontium sulfide P108 . Strychnine and salts SUBTEX tee P02O SYSTAM tee P08S TAG FUNGICIDE see P092 TEKWA1SA see P071 TEMIC see P070 TEMIK see P070 TERM-1.TROL see P090 P109........ TetraethykJithiopyrophosphatt Pi 10.. Tetraethyllead Pill ... Tetraeihyipyrophosphate Pii2 .... TeUirntromethaoe Tetraphosphonc aod. hexaethyl ester see P062 TETROSULFUR BLACK PB see P048 TETROSULPHUR PBR see P048 Pt13..., Thallcoxxje Thallium peroxide see Pt 13 Pi 14... , Thaikumseiervte P115........ Thallium (I) sulfate THiFOR see P0925 THIMUL tee P092 ThiOOAN see P050 THIOFOR see P050 THiOMUL see P050 THIONEX tee P050 thiOPHENIT see P071 Pi 16-___ Thiosemieerbazide Truosutlan bonef tee P050 P117 ....... Thiuftm THOMPSON'S WOOD FIX see P090 TIOVEL see P050 Pi 16......... Tnchioromethanethiof TWIN LIGHT RAT AWAY see P001 USAF RH-fl set P069 USAF EK-4690 see P002 P119. . .. Vanadc aod. ammonwm sen P120,,.. Vanadum pemoxide VOFATOX see P071 WANAOU see P120 WARCOUMtN see POOt WARFARIN SOOlUM see P001 WARFICIDE see P001 WOFOTOX see P072 YANOCK see P057 YASOKNOCK see P058 2IARNIK see P092 P121......... Znc cyarude P122......... Zinc phosphide (R,T) ZOOCOUMARIN see P001 'The Agency included those trade names of whh it was aware; an omstKm of a bade name does not imply that tt* omned matenai is not hazardous The material 1$ hazardous if <t >s ksted under its genenc name I : ! I 1 CAPCO JEN 0004829 45, No. 98 / Monday, May 19, 1980 / Rules and-Regulations - 331 (f) The commercial chemical products or manufacturing chemical intermediates, referred to in paragraphs [a], (b) and (d) of this section, are identified as toxic wastes (T) unless otherwise designated and are subject to the small quantity exclusion defined in 5 261.5 (a) and (b). These wastes and their corresponding EPA Hazardous Waste Numbers are: Hazardous Waste No. Substance AAF see U005 U001......... Acetaldehyde U002........ Acetone (I) U003......... Acetonrtnle (1,7) U004......... Acetophenone U005....... 2-Aeetytamtnoflourene U006......... Acetyt chtonde (C,T) UO07........ Acryfamtoe Acetylene tetrachloride sea U209 Acetylene tnchionde see U228 U006........ Acryl<c aod (I) U009......... Acrytonrtnlt AEROTHENE TT see U226 O-Ammo-S-lp acetarrd0phen)4}>iH>).2.4.|ft9Z0ie, hydrate see UOil U010 ... 6-Ammo-1.la.2.8.8a8b*hexahydro-8- {hydroxymetnyi)8-methoxy-5-m<>thy)carbamate azmno(2'.3' 3.4) pyrroto(1.2-a) mdole*4, 7-dtooe (ester) U011.........AmrtrtSa 0012....... Arxkne(l) U013.. -- Asbestos** U014...... Auramme U015........ Azasenne U016........ Benz(c)acndme U017..,,. .. Bernal chloride U018..... . Benz(a)antbraeene U019..... . Benzene U020... -- Benzenesuifonyl chionde (C.R) U021...... BertZKkne 1.2-Benzsothazolin-3-one. 1.1-dioxide see U202 Bemotalanthracene see U018 0022...... BenzoCajpyrene U023 , ... Benzotnchlonde (C.R.T) 0024.... 6ts(2-chiofoeihoxy)methane U025........ BiS(2*chloroethyt) ether U026____ N.N-Bis(2-Chtoroethyt)-2-naphthytamine U027....... BiS(2-Chtoroi40propyl) ether U028...... . 8<s(2-e!bylbeifyi/ phthalate U029. Bromomethane 0030, _. 4-Bromophenyl phenyl ether U031.. n-Butyl alcohol (I) U032 Calcium chromate Carbolic acid see U188 Carbon tetrachionde see U2it U033. Carbonyl lkx>f>d* U034 ... Chkxal U03S.. Chlorambocd U036 , .. Chlordane U037 Chlorobenzene U038 . Chiorobenzilate U039.... p-Chtoro-m-cresol U040 Chtorod>bromomethane U041 .. 1*Chloro-2.3 epoiyprdpane CHLOROETMENE NU see U226 U042.. .. Chloroeihyl vinyl ether U043... Chioroethene U044 .,,.. Chlorotorm (I.T) U045. ,. Chloromethane (I.T) . U046___ CMoromethyl methyl ether U047......... 2>Chloronaphthalene U048 ____ 2*Chtorophenoi U049 . - . 4 CWcxo-o-totUKjme hydrochloride 0050 ..... Chrysene Cl 23060 see U073 0051.... Cresote U0S2. . Cresols 0053.. . Crolonaldehyde U054,,, . Cresyfacacid U055 ,,. .. Cumene ._ Cyanomethane see U003 0066 --, Cyclohexane (I) 0057. Cyclohexanone (I) 0058.... Cyclophosphamide OCS9... . Oaunomycm 0060... DOO Hazardous Wasta No Substance1 0061.... . DDT 0062......... DtaBale 0063....... Oberuta.h]anthracene ObenzoCa.hJanthrecene see 0063 0064........ Dibenzo(a.i)pyrene 0065......... Oibrompchioromethene 0066....... 1,2*Dibromo*3-ch>oropropane 006?....... 1.2'0ibrorTpethsne 1)066...... Dibromomethane 0069........ O-n-butyt phthalate 0070........ 1.2-CXhlorebenzene 0071......... i.3-Dichlorobenzene 0072........ 1,4 >0*chlorobenzene 0073....... 3,3**Dhiorobenzidine 0074......... 1 4-DiChkxo-2-buttne 3 3`.Dich)orO`4,4`*diaminobipheny1 see 0073 U075-....... Dichtorodifluoromethane 0076. 1,l-D*chloroethane 0077_____ 1 2*Dichloroethane 0078 ....... 1,1-Ochkxoethyterve 0079-....... 1,2<trans4Jichtoroethy(ene t 0080........ Dchloromethane D*chtoromethydbenzene see 0017 1 0081....... 2.4'Dtohlorophenol 2.6-Dtohlorophenol 0083.... 1.2-Dichioropropane 0064....... 1,3-Oichtoropropene 0085 -.. Diepoxybutane (I.T) 0086. 1.2'Dthythydrazine 0087.. O.O-Diethyt-S-methyt ester of phosphoroddhoc acid 0088 . . Diethyl phthalate 0089. . Diethytstilbestrol 0090 ... Dhydrosairote 0091.. .. 3.3`>Dimethoxybenzidine ; 0092-- . Dimethytamne (i) 0093....,, p-Oimethyfammoazobenzene, , 0094 ,, . 7.12-0<methylbenz(a)anthraeene 0095 .. 3.3 -Dimethyibenzidine U096 .. , aipha.alpha-OmeihyibenzyifiydroperoxKje (R) 0097........ Dimethylcarbamoyt chionde,. U098 1,1-Dimeihythydrazme 0099........ f.r-Omefhy4hydrezme 0100........ Dmethytmtrosoamine 0101____ , 2.4-Oimethytphenol 0102.... Omnethyt phthatate 0103.. ,, Dimethyl sulfate 0104. . 2.4-Dinitrophenol 0)05.... 2 4*Dirvtrotofuene 0106 2 6-Dinitrotoluene 0107 . , D>*n-octyt phthalate 0108 .. 1.4-Dioxane 0109 .. .. 1,2-Dtohenylhydrazme 0110.. .. Dipropytamme (ft . uni____ D*-n-pfopyin*troAmoe EBDCseeUU4 ... i.4-EpoiybutaMisea. 0213 0112 .. UH3. Ethyl aceUte (i) Ethyl acrytate (I) 0114.. , Ethytenebisdithiocarbamate U115-, . Ethytena^oxide (I.T) U116 .. Ethylene thiourea 0117 . one.. Ethyl ether (I.T) Ethylmemacrytate U119 . Ethyl methanesulfonate Ethytmtnle see U003 0120.. Firemaster T23P see 0235 Fluoranthene U121 ... 0122 . FtuorotncNoromethane Formaldehyde 0123 u Formic add (C.T) 0124.. Furan (I) 0125.. Furfural (I) U126 . Glycidylaldehyde 0127... , Hexachtorobenzene 0128 -. . Hexacntorobutad*ene 0129 . Hexschtorocyctohexane U130 . Hexachtorocyctopentadiene U131-. Hexachioroethane U132 . , Hexachlorophene 0133 Hydrazine (R.T) , 0134. Hydrofluoric ac*d (C.T) .: 0135.. Hydrogen suiiide Hydroxybenzene see 0188 UI36.. Hydroxydimeihyt arsine oxide 4.4 .(imidocarbonyi)bis(N.N>dimaihyi)aniline 0014 0137.. 0138. lndeno(t 2.3-cd)pyreoe lodomethane 0139 . 0140 Iron Oextran Isobutyl alcohol Hazardoua Waste Na Substance* 0141_____ Isossfrole U142 ...... Kepone 0143....... Usiocarpme 0144......... Lead acetate 0145........ Lead phosphate U146____ Lead subacetale U147........ Mstac anhydnde U148........ Maleic hydrazide 0149.. .. Matonontnie MEK Peroxide see 0160 0150.... Metphaian U151,,. .. Mercury 0152........ Methacrytomtnle 0153......... Methanethiol 0154......... Methanol 0155........ Methapyntene Methyl alcohol see 0154 0156.. Methyl chtorocsrbonate Methyl chloroform see 0226 U157........ 3-Methytoholanttvene Methyl chtoroformate see U156 0158------- 4.4 Methytene-bis-(2-chloroaniiine) 0159. Methyl ethyl ketone (MEK) (I.T) U160 ..... Methyl ethyl ketone peroxide (R) Methyl iodide see 0136 0161 . .. Methyl isobutyt ketore 0162.. .. . Methyl methacrylate (R.T) 0163........ N-MethySN'-rutro-N-ntrosoguantome U164 . Methyithtouracil M'tomycm C see U010 0165 Naphthalene U166. ,, 1.4-Naphthoqwnone U167.. i-Naphthyiamme U168 2-Naphthyiamme 0169........ Nitrobenzene (I.T) Nrtrobenzot see U169 Ot 70 . 4-Nitrophenol U171 .. 2-Nrtropropane (1) U172 ..... N-Nrtrosock-n-butyiamine U173.,. N-Nitrosodthanolam<ne UI74........ N-Nitrosodiethytamme 0175........ N-Nitrosodi-n-propytamine 0176. ... N'Nit/oso-n-etbyfurea U177........ N-Nitroso-n melhylurea U178 ...... N-Nitroso-n-methyturethane U179 .. .. N-Nitrosopipendme U180-.... N-Nitrosopyrrokdme U181 . 5-Nitro-o-toluidine U182. ... Paraldehyde PCNB see 0165 0163. . Pentachtorobenzene 0184. Pentachtoroethane U185....... Pentachtorontrobenzene 0186...... . l.3-Pentadiene (1) Pere see U210 Perchiorethyiene see 0210 j 0*87. . Phenacetin ! 0188.. , . Phenol I 0189....... Phosphorous sulfide (R) | 0190.___ Phthalie anhydnde I 0191.... 2-Ptcolme 0192 ...... Pronarrade 0193....... 1.3 Propane suttone 0194 ,, ... n Propyiamme (I) 0196....... Pyndm# 0197.. ,, Oumones 0200 .... ,, fleserpme 0201 . .. Resorcinol 0202 ....... Saccharin 0203 ...... Safroie 0204.. .... Seiemous aod 0205 ....... Setenrum sulfide (R.T) SiNex see 0233 0206 .... ... Streptozotoon 2.4.5-T see 0232 0207.. .1.2.4.5.Tetrachlorobenzene 0208.. . 1.1.1.2-Tetfachtoroethane 0209......... 1.1.2.2`Tet/achloroethane 0210.. . Tetrachloroethene TelracWoroeihylene see 0210 0211 ,, Tetrachloromethane 0212 .... 2 3.4.6-Teuachiorophenoi 0213 Tetrahydrofuran (t) 0214 ....... Thallium (i) acetate 0215 .. Thatlxjm (l) carbonate 0216____Tkaftum (I) chionde 0217.___ Thallium (I) nrtrate 0218.. Thcaeetamide 0219 ...... Thiourea 0220 ....... Toluene 0221 ....... Tolutnedmne 0222 ...... o-ToAMfrne hydrochloride * CAPCO JEN 0004830 33127 Federal Regiatar / Vol. 45, No. 98 / Monday. May 19. 1980 / Ruleg and-Regulations U223...... .. Tolutn* dasocysnst* U224...... - Tozaphvns 2.4.5-TP ih U233 U22S. .. Tobcomomathana U226.. . . i.t.MncMoroamana U22?.....- l.l.2'Tnchloro4thar>* U228 . . TncWoroaih#n# Tnchlorosthyton* se U228 U229... . , TncWorotluoromamane U230. . . 2.4,$'Tnchlo'ophno< U231... . . 2.4.&<Tr>chloropt*nol U232...... U233 .. 2,4.5-TnchJoropHenoxyacstic *c*d 2.4.S-Tr>chlorophnoxypropon*c * alpha. alpha- TricMofOtoKwn* s*4 TRI-CLENE se# U22S U23<... . Trvwtxoberuen* (R.T) U235____ , Tns(2,3-<*bromopropyl) phosphat# U236......... Trypan Wua U237....... . Uracil mustard U239....... Uratftana Vary) chtonda saa U043 Vinyfcdana cWonde saa U076 U239....... Xylan# 1 Th* Agency nclud#d those trade names ot winch it was aware, an omission ot a trade name does not imply that it is not hazardous The material is hazardous rf it is listed under its genenc name. Appendix I--Representative Sampling Methods The methods and equipment used for sampling waste materials will vary with the form and consistency of the waste materials to be sampled. Samples collected using the sampling protocols listed below, for sampling waste with properties similar to the indicated materials, will be considered by the Agency to be representative of the waste. Extremely viscous liquid--ASTM Standard D140-70 Crushed or powdered material-- ASTM Standard D346-75 Soil or rock-like material--ASTM Standard D420-69 Soil like material--ASTM Standard D1452-65 Fly Ash-like material--ASTM Standard D2234-76 [ASTM Standards are available from ASTM, 1916 Race St.. Philadelphia, PA 19103) Containerized liquid wastes--"COUWASA" described in "Test Methods for the Evaluation of Solid Waste. Physical/ Chemical Methods," ' U.S. Environmental Protection Agency. Office of Solid Waste. Washington, D.C. 204Qf4Copies may be obtained from Solid Waste Information. U.S. Environmental Protection Agency. 26 W. St. Clair St.. Cincinnati, Ohio 45268) Liquid waste in pits, ponds, lagoons, and similar reservoirs.--"Pond Sampler" described in 'Test Methods for the Evaluation of Solid Waste. Physical/ Chemical Methods." 1 This manual also contains additional information on application of these protocols. 1 These methods are also described in "Samplers and Sampling Procedures for Hazsrdous Waste Streams." EPA 600/2-SO-018. January I960. Appendix II-- EP Toxicity Test Procedure A. Extraction Procedure (EP) 1. A representative sample of the waste to be tested (minimum size 100 grams) should be obtained using the methods specified in Appendix I or any other methods capable of yielding a representative sample within the meaning of Part 260. [For detailed guidance on conducting the various aspects of the EP see "Test Methods for the Evaluation of Solid Waste, Physical/ Chemical Methods," SW-846, U.S. Environmental Protection Agency Office of Solid Waste. Washington, D.C. 20460.'} 2. The sample should be separated into its component liquid and solid phases using the method described in "Separation Procedure" below. If the solid residue 1 obtained using this method totals less than 0.5% of the original weight of the waste, the residue can be discarded and the operator should treat the liquid phase as the extract and proceed immediately to Step 8. . 3. The solid1material obtained from the Separation Procedure should be evaluated for its particle size. If the solid material has a surface area per gram of material equal to, or greater than. 3.1 cm5 or passes through a 9.5 mm (0.375 inch) standard sieve, the operator should proceed to Step 4. If the surface area is smaller or the particle size larger than specified above* the solid material should be prepared fqr,extraction by crushing, cutting or j^nding the material so that it passes tHrolljm;"S.5 mm (0.375 inch) sieve or, if the nfa)enal is in a single piece, by subjecting the material to the "Structural Integrity Procedure" described below. 4. The solid material obtained in Step 3 should be weighed and placed in an extractor with 18 times its weight of deionized water, Do not allow the material to dry prior to weighing. For purposes of this test, an acceptable extractor is one which will impart sufficient agitation to the mixture to not only prevent stratification of the sample and extraction fluid but also insure that all sample surfaces are continously ' Copie* may be obtained from Solid Waite Information. U.S. Environmental Protection Agency. 26 W. St. Clair Street. Cincinnati. Ohio 45268. 'The percent solids is determined by drying the filler pad at BO* C until it reaches constant weight and then calculating the percent solids using the following equation: twiQht ot pad + kM) - (tvs of pad) X too - %sofc* nrtiat wght ot aampta brought into contact with well mixed extraction fluid. 5. After the solid material and deionized water are placed in the * extractor, the operator should begin agitation and measure the pH of the solution in the extractor. If the pH is greater than 5.0. the pH of the solution should be decreased to 5.0 0.2 by adding 0.5 N acetic acid. If the pH is equal to or less than 5.0, no acetic acid should be added. The pH of the solution should be monitored, as described below, during the course of the 'extraction and if the pH rises above 5.2, 0.5N acetic acid should be added to bring the pH down to 5.0 0.2. However, in no event shall the aggregate amount of acid added to the solution exceed 4 ml of acid per gram of solid. The mixture should be agitated for 24 hours and maintained at 20"-40" C (68*-- 104" F) during this time. It is recommended that the operator monitor and adj'ust the pH during the course of the extraction with a device such as the Type 45-A pH Controller manufactured ' by Chemtrix, Inc., Hillsboro. Oregon 97123 or its equivalent, in conjunction with a metering pump anJreservoir of 0.5N acetic acid. If such a system is not available, the following manual procedure shall be employed: (a) A pH meter should be calibrated in accordance with the manufacturer's specifications. (b) The pH of the solution should be checked and. if necessary. 0.5N acetic acid should be manually added to the extractor until the pH reaches 5.0 0.2. The pH of the solution should be adjusted at 15.30 and 60 i minute intervals, moving to the next longer interval if the pH does not have to be adjusted more than 0.5N pH units. (c) The adjustment procedure should be continued for at least 6 hours. (d) If at the end of the 24-hour extraction period, the pH of the solution is not below 5.2 and the maximum amount of acid (4 ml per gram of solids) has not been added, the pH should be adjusted to 5.0 0.2 and the extraction continued for an additional four hours, during which the pH should be adjusted at one hour intervals'. 6. At the end of the 24 hour extraction period, deionized water should be added to the extractor in an amount determined by the following equation: V= (20)(W)-16(W)-A V = ml deionized water to be added W = weight in grams of solid charged to extractor A= ml of 0.5N acetic acid added during extraction 7. The material in the extractor should be separated into its component liquid and solid phases as described under "Separation Procedure." 8. The liquids resulting from Steps 2 and 7 should be combined. This CAPCO JEN 0004831 combined liquid (or the waste itself if it has less than lA percent solids, las noted in Step 2) is the extract and should be analyzed for the presence of any of the contaminants specified in Table I of 261.24 using the Analytical Procedures designated below. Separation Procedure Equipment: A filter holder, designed for filtration media having a nominal pore size of 0.45 micrometers and capable of applying a 5.3 kg/cmJ (75 psi) hydrostatic pressure to the solution being filtered shall be used. For mixtures containing nonabsorptive solids, where separation can be affected without imposing a 5.3 kg/cm3 pressure differential.-vacuum filters employing a 0.45 micrometers filter media can be used. (For further guidance on filtration equipment or procedures see "Test Methods for Evaluating Solid Waste, Physical/Chemical Methods.") Procedure: * (i) Following manufacturer's directions, the filter unit should be assembled with a filter bed consisting of a 0.45 micrometer filter membrane. For difficult or slow to filter mixtures a prefilter bed consisting of the following prefilters in increasing pore size (0.65 micrometer membrane, fine glass fiber prefilter, and coarse glass fiber prefilter) can be used. (ii) The waste should be poured into the filtration unit. (iii) The reservoir should be slowly pressurized until liquid begins to flow from the filtrate outlet at which point the pressure in the filter should be immediately lowered to 10-15 psig. Filtration should be continued until liquid flow ceases. (iv) The pressure should be increased stepwise in 10 psi increments to 75 psig and filtration continued until flow ceases or the pressurizing gas begins to exit from the filtrate outlet. (v) The filter unit should be depressurized, the solid material removed and weighed and then transferred to the extraclion apparatus, or, in the case of final filtration prior to analysis, discarded. Do not allow the 'This procedure is intended to result in separation of the `Tree" liquid portion of the waste from any solid matter having a particle size ?0.45um. If the sample will not filter, various other separation techniques can be used to aid in the nitration. As described above, pressure nitration is employed to speed up the filtration process. This does not alter the nature of the separation. If liquid does not separate during filtration, the waJlfcan be centrifuged. If separation occurs during centrifugation ihe liquid portion (centrifugate) is filtered through the 0.45um filter prior to becoming mixed with the liquid portion of the waste obtained from the initial filtration. Any material that will not pass through the filler after centrifugation is * considered a solid and is extracted. material retained on the filter pad to dry prior to weighing. (vi) The liquid phase should be stored at 4*C for subsequent use in Step 8. ft Structural Integrity Procedure Equipment: A Structural Integrity Tester having a 3.18 cm (1.25 in.) diameter hammer weighing 0.33 kg (0.73 lbs.) and having a free fall of 15.24 cm (8 in.) shall be used. This device is available from Associated Design and Manufacturing Company. Alexandria, VA.. 22314. as Part No. 125, or it may befabricated to meet the specifications shown in Figure 1. Procedure: 1. The sample holder should be filled with the material to be tested. If the sample of waste is a large monolithic block, a portion should be cut from the block having the dimensions of a 3.3 cm (1.3 in.) diameter x 7.1 cm (2.8 in.) cylinder. For a fixated waste, samples may be cast in the form of a 3.3 cm (1.3 in.) diameter x 7.1 cm (2.8 in.) cylinder for purposes of conducting this test. In such cases, the waste may ho allowed to cure for 30 days prior to further testing. 2. The sample holder shopld be placed into the Structural Integrity .Tester, then the hammer should be raised to its maximum height and dropped. This should be repeated fifteen times. 3. The material should be removed from the sample holder, weighed, and transferred to the extraction apparatus for extraction. Anaiytical Procedures, for Analyzing Extract Contamifip&tS * The test me(hQ4fe|53;3paIyzing the extract are as'follows:. (1) For arsenic, barium, cadmium, chromium, lead, mercury, selenium or silver: "Methods for Analysis of Water and Wastes." Environmental Monitoring and Support Laboratory. Office of Research and Development, U.S. Environmental Protection Agency, Cincinnati, Ohio 45268 (EPA-600/4-79020. March 1979), (2) For EndrinrLindane; Methoxychlon Toxaphene; 2.4-D; 2,4,5TP Silver: in "Methods for Benzidine. Chlorinated Organic Compounds. Pentachlorophenol and Pesticides in Water and Wastewater." September 1978. U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory. Cincinnati. Ohio 42568, as standardized in "Test Methods for the Evaluation of Solid Waste. Physical/ Chemical Methods." For all analyses, the method of standard addition shall be used for the quantification of species concentration. This method is described in "Test. '' Methods for the Evaluation of SolidWaste." (It is also described in "Methods for Analysis of Water and Wastes.") BILLING COOE 540-01-M 1- CAPCO JEN 0004-632 33129 Federal Register / Vol. 45, No. 98 / Monday! May 19,1980 / Rules and Regulation! ^ELASTOMERIC SAMPLE HOLDER FABRICATED OF MATERIAL FIRM ENOUGH TO SUPPORT THE SAMPLE Figure 1 COMPACTION TESTER BILUNG CODE $6O-0t-C i CAPCO JEN 0004833 , .. V fiJ? .',>l-'*{ Federal Register / Vol. 45, No. 98 / Monday. May 19, .1980 / Rules and Regulations . .' Appendix HI--Chemical Analysis Test Methods Tables 1, 2 and 3 specify the appropriate analytical procedures, described in "Test Methods for Evaluating Solid Waste" (SW-846), which should be used'in determining whether the waste in question tontains a given toxic constituent. Table 1 identifies the analytical class and the approved measurement techniques for each organic chemical listed in Appendix VII. Table 2 identifies the corresponding methods for the inorganic species. Table 3 identifies the specific sample preparation and measurement instrument introduction techniques which may be suitable for both the organic and inorganic species as well as the matrices of concern. Prior to final selection of the analytical method the operator should consult the specific method descriptions in SW-846 for additional guidance on which of the approved methods should be employed for a specific waste analysis situation. Tibia y.--Analytical Characteristics ot Organic Chemicals Compound Sample handling dass/lraction Non-GC methods Measurement techniques ------- ---------- --------------------------------------Convintionil GC/MS GC Detector Acetomtnte...............-.............. .. Volatile ....................,, . Acrolein ...... .. ........... - Volatile...... ..... Acrylamide.............................. . Volatile ,, . ........ Acrylonitrile ......................... .. .. Volatile.............. .. 8en2ene.......... . .......... - Ben2(e)anthrecene.TM -- - . Extractabie/BN........ 8 10 (HPLC) Benio(a)pyrene.... ......... . . Extrectable/BN ... ____ . . 810 (HPLC) Benxotnchlonde...........-........... ... ExtracUbie/BN,........ ... Benzyl chloride...................... . . volatile or Extracuble/BN - - * * Benzfbjfhioanthene................. ,,.. Extractabie/BN................... ,, B|2-chlOfoethojrymethane) ... Volatile . .. .... ........... Bis(2-chtoroethyl)etbef............. .... Volatile............... ,,..v . Bi$(2-chloroisopropyl)ether....... .... Volatile...... ........................ Carbon disulfide................ - . . Volatile................................ Carbon tetraehionde...... .......... ... Volatile................................. Chlordane................................ .. . ExiractaWe/BN . Chlonnated dtbenzodioxtns - Extracubte/BN . Chlorinated biphenyls............. . .... ExtiactaWe/BN .... .. ChkKoacetaklehyde.................. .. . volatile............................... . Chlorobenzene..................... .. . Volatile . ... --... . 8 10 (HPLC). CWorolorm......... ...................... ,, Volatile.... . Chioromethane...........,,........... Volatile ....... . ............. 2-Chlofophenol........................ . . Extractabie/BN,,. ... Chrysene.........,,,,........... . .. . Ertraetabfe/SN ,, Creosote.. ,,. .................. - Extractabie/BN. . . . . Cresot(s).................................... Extracuwe/A ... Cresyta eod(s).... .................. Extractabie/A .... Dich)orobenzene(s) ...... ... Ext/actabte/BN................. 8 JO (HPLC). ............. - Ochkxoethane(s)........................... VoUWe............................ .. . .. ............ Ochioromethane............. -............. Volatile.............. .............. .. ............ l>chioropheno*y-eceticaod.. ...... Extractable/A.. ....... ....... . .................... Dchtoropropanol.. ............. ....... .. Exvactatne/BN ........................................ 2.4-DwTWthylphenol ....... ... . Extractable/A.......... ............................. Dint/obenzene ..... ......................... Extractabie/BN............................................. . 4.8-Omotro-O-cresot..................... Extractabie/A........................................... .. . 2.4 Omctrotoiuene... ................. .. ExtrecUb*e/BN,,............................................ Endm... ..... ..... ....... . . Extrectable/P,....... ..................................... Etnytether....................... . .. Volatile................................ . ....................... Formaldehyde............. ........... Volatile..................... ..... Forme acd .5...................... . .... Extractabie/BN.................... ....................... Heptachtor. .......... .................. .. Extractable/P ............. ,, .,, Hexachkirobenzene ......... ... Extractabie/BN.............. ....... Hexaehiorobutadiene............_. Extrectable/BN.......................................... Hexachkyoethane ........ .... Extrectable/BN........... .......... . Hexachlorocyclopentadiene.......... Extracuble/BN........... . .- lindane.............................. . ExtractaWe/P....... ..... - . .... Maleic anhydnde............................ Extractabte/BN.......................................... Methanol.,.. ......................... ,. .. - Volatile.... .. ...................................................... Methomyt................ ... ......... Extrectable/BN..................... 8 32 (HPLC). Methyl ethyl ketone.................... Volatile.............. .. ... . .............. Methyl isobutyl ketone.. . ___ Volatile...............,,.. Naphthalene............................ ..... Extracuble/BN................ ... Napthoqmnooe _____ __ _________ CtfMeutXe/BN.................................... ... . Nitrobenzene ........... ............... ... 4.Nitrophenoi... . ,, Paraldehyde (tnmer o( acetaldehyde). ExtrectoWe/BN.............. .................. Extrectabie/A................................ , ... Volatile...... .................................................... 8 24 8 24 8 24 8 24 8 24 8 25 8 25 8 25 824 8 25 8 25 824 8 24 8 24 8 24 5 24 8 25 8 25 8 25 8 24 824 8 24 8 24 8 25 825 ;.;i 8 03 6 03 801 803 8 02 0 to 810 8.12 SOU 812* 8.10 801 6 01 601 801 801 6 06 80S 608 801 801 8 02 801 8 01 8 04 810 '8 25 JitJ 8.10 6 25 1 ;< ,,6.04 8 25 ].' 8 04 8 25 < ' 8 01 8 02 612 8 24 6 24 801 6 01 8 25 6 25 6 25 825 8 25 8.40 8 12 604 600 804 8 25 825 6 24 809 80S 6 01 8 02 8 24 601 6 25 8 25 625 8 25 606 606 6.12 6.12 8 25 6.12 8 25 8 12 825 8 08 8 25 806 8 24 6 01 NSD NSO FID NSD PID FID FID ECO HSD ECO . fjd HSO HSD HSD HSD HSD HSO ECO HSD HSD HSO PID HSO HSO FlD. ECO FID ECO FID. ECO FlO. ECO HSD FlO - ECO HSO HSO HSD ECO FID. ECO FlO. ECO FID. ECO FlO. ECO HSD FlO FID FlO FlO HSO ECO ECO ECO ECO HSD ECO. FlO FlO 6 25 825 625 825 6 25 8 24 8 24 801 8 02 6 01 802 8 10 806 809 609 804 601 ' FlO FID FlO FID FID ECO. FlO FID ECO. FID ECO. FlO FID CAPCO JEN 0004834 33131 Federal Register / Vol. 45; No. 98 / Monday. May 19, 19807 Rules and Regulatlona Tb** i.~~Ane/yt>ce/ Characteristics of Organic Chemicals--Continued Apfwndbc VII.--Said for Listing Hszsrtious Wests* Comp&md Stmpte handtag ctess/fractxxi NorvGC mathoda Maasuramant tacfnquaa ---------------- Convanbonal 6C/MS GC Ostactor EPA hazardous waste No. Hazardous comtitirants for wteeft Mad Pantachlorophanol..................... ... Extractabla/A--.................. rhawi .............................. Extractstea/A Phorat#......... .... Extrsctabte/GN................-.... Phoaphorodrtteoie aod astars.... ... Extractatea/BN...................... PhthaSc anhydnda..... -.............. ... Extractabto/BN...................... 8 25 6 25 ........................ ........... 8.25 Tatracteorobanztoafr)............ . .... Extractabte/BN....................... Tairacteoroathana(s)m....... ............ Voted#_________ ___________ Tatracteoroathana....................... ... Voted#.................................... .......... Tatracteorophanol....................... Extractabte/A......................... Totoana.......... _ ... Voted#.................................... ......... Toluanadiamna.......... _................... Extractabte/BN....................... Toluana fesocyanatafs)....... -.... ... Extracttbte/nonaqusous....... Toxaphsna.... ... Extractabte/P......................... Tnchioroathana.......................... .. Voted#................................... Tncteoroathana(*)....................... ... Voted#.................................... Tncteorofluoromathana............... ... Voted#.................................... TncteorophanoKs)................... ... Extraclabte/A......................... 2.4.5-TP (Srfvax).,........................ ... Extractabte/A......................... Tncteoropropana........................ ... Voted#.-................................. Vnyt cteonda.. ... Voted#.................................... Vjnybdana chlonda...................... .. voted#.................................... Xytena--........................................... Voted#......... ........................... 8 25 6 24 8 24 8 24 8 24 625 625 8.25 824 6 24 6 24 82S 825 6 24 6 24 624 8 24 8.04 6.04 6.22 806 609 822 606 609 609 609 612 601 6 01 604 8.02 8.06 6.06 801 801 8.01 804 8 40 801 8.01 6 01 6 02 ECO ECO.F10 FPD ECO. FIO ECO. FID FPD ECO, FID ECO. FID ECO. FID ECO. FID ECO HSO HSO ECO PID FIO HSO HSO HSO HSO HSO HSO HSO HSO HSO PIO ' Anafyza foe phananthran# and caibazote. if thasa ara praaam in a ratio between 1.4.1 and $ 1. creosote should be conudered present. ECO - Electron capture delator. FID Flame tonaabon detector FPD Flame photometne detector; HSO HaWa specific detector HPIC H<gft pressure kqiW ctwomotography; NSD = Nitrogen-specific detector FID - Photo*onaatn da* Tabk 2--Analytical Characteristics of Inorganic Species Speoes Sample handing class Antimony..-..............-...................... Digatbon............. Arsarac - - ...........-- Hydnda....... -........ Banum........................... ............... oigastxjn............. Cadmum....,,-.... -........... Digsfbon Chromum........................ OgastKm Cyandas ................ Hytfrdytia...... ..... laad.. Digtttion Marcury ............... Odd Vapor.......... NicMI--...... -.................. ................ Oigasbon.............. Satenum--...................... --.......... Hydnda digarbon. S/var. Ogasbon.............. Measurement technique Atomic absortbon-fumece/fieme................ ... Atomc absorbhon-flama-.. Atonecabsorbbon-tumece/ftamev......'........... Atomic ebsorbtion-hmece/name................... Atomc abaorbboo-furnaea/fUma,.^.,.,,____ Atomc abeobbon-apactroacopt tr1 Atorrac abaorbbon-fumaea/flama...... Atomic absorption__________.7.,7.,,*'.!.'.7...... Atomc abeorbborvfumece/name.... .... ...... Atomc abaorboon-fumaca/flama...___ _____ Atomic abaorbbon-fumaca/flama_____ ____ _ Method number 6 50 6 5t 8 52 653 6 54 8.55 6 56 8.57 6 58 8 59 6 60 Table 3.--Semple Prepertion/Sampte Introduction Techniques handing class Physical charactensbcs of waste * a Fksd " "Pasta Sofcd Void#.____ --. Pwgsand trap. Dract mjacbon. Samvotedt and Ovact ryacbon. nonvoteds. Shakaou.. Purga and Hsadip^a. trap. Haadspaca-- Shaka out..... Shaka out Soxteat Soracabon. Procedure and Method Numberfs) Digestion--See appropriate procedure for element of interest Direct injection--*6.80 Headspace--6.82*'' Hydride--See appropriate procedure for element of interest. Purge & Trap--6.83 Shake out--8.84 Sonication--8.85 Soxhlet--6.86 . F001,,____ tatracteoroathytena. mathytena cteorida meteor* oathyftena. 1,1,1*tricMorotthana cteomated J fluorocarbons, carbon tetracteodda v F002-.-- tatracteoroathylana. mathytena cteorida. meteor* oathylsna, t.I.I-tncteoroathana, cteorobarv zana, 1,1^-tnqtjfcn>.l^.tnfluoroath<m. idchlcrobanzana. tncteorofluoromalhteia F003_____ NA. I F004craaota and crasyfc sod. nrtrobanzana > F005-------- mathanot toluana. mathyt athyf katona, mathyt wobutyl kttont, carbon dwulfidt, iaobutanoi. pfsina F008.......... cadmum, chromum, niefcaf, cyarada (comptexad) FO07.......... cyarada (salts) F008......... cyarada (salts) F009.--..... cyarada (salts) FOiO.......... cyarada (salts) F011_____ cyarada (salts) F012......... cyarada (comptexad) F013......... cyarada (comptexad) F014......... cyarada (complaxad) F015.......... cyarada (salts) FQtfl......... cyarada (complaxad) K001......... banzana, banz(a)anthracana. banzo(a)pyrana. chrysana. 4-nrtropritnof. toluana. naphthalana phanof, 2-chlorophaool. 2.4-dmethyl phawl, 2.4.6-tocteorophanot pantachlorophanol. 4.6daatro-ocraad. tatracteorophanol K002......... chromium, tead K003-------- chromum. tead K004......... chromum K005........ chromum. tead K006.......... chromum K007.......... cyanda (comptexad). chromum K008.....__ chromum K009-------- chloroform. formakJahyda. mathytena chlorate. mathyt chlorate, paraidahyda. forme aod K010......... chloroform, tormaJdahyda. mathytena chlorate, mathyt cteorida. paraidahyda. forme acid, cteoroacatatdtftyda KOt 1......... acrytonitnte, aotoratnte. hydrocyanic aod K012......... acrytorxtnte. acatontnte. acroten. acrylamda K013......... hydrocyanc add. acrytonitnte. acatontnte K0Y4......... acatonrtnte. acrylamda KOI 5......... banzyf chlonda. chlorcbanzona. toKrana. banro- K016......... haxacteorobanzana. haxacteorobutadanat carbon tatracteorate, haxacteoroathana. parcb* loroathytena KOI 7......... apeteorohytton. cteoroathars (bo(cteoromathyi) athar and tes (2-cteoroathyf) athars). meteors propana. dKteoropropanots KOI61.2-dcteoroathana, tncteoroathytena. haxacteorcy butatbana, haxacteorobanzana K019_____ athytena dKteonda. l.l.1mcteoroathana. 1.1.2* meteoroathana. tetrachloroathanas (1.1224* tracteoroathana and l.l.l^tatracteoroathana). meteoroathytena. tatraeteoroathytena. carbon tetraeteonda. chloroform, tnnyl cteonda. wry** dan* cteonda miacbort Digaabon..... Oigasbon___,, Digasben. Hycrtda____... Hydnda_____ Hydnda. `For purpoaat of ttes Tabte, flud rafara to raadtfy pouratea Equda, wfxch may or may not contaai suapandad parbetet. Pasta tea matanate. wtste fksd si tha sanaa of flmrabdty, e*i ba thought of as bang ceottcpic or plastie in natura. a g. pants. $ohd matanate art thoaa wastes wtech can ba handted without a contaaiar (la., can ba ptfad up without appro* cutes saggmg). t. CAPCO JEN 0004.835 Appendix VII.--Basis for listing Hutrtow Wsstss--Continued EPA htzerdods waste No Hazardous constituents for wteh S*t#d K020........ ethylene d^htonde, 1.1,1-tnehtoroethane. 1.1.2* tncMoroethane, letrecMoroethanes (1,1,2,2*te* trecMoroethane and 1.1.1,2*tetrachioroethane). tncNoro#thyt#n#, tetrachtoroethylene. carbon tetreehlonde. chloroform, wryl chionde. vwyfc* dene chloride K021......... antimony, carbon tetrachloride. chloroform K022......... phenol, tars (pofycychc aromatic hydrocarbons) K023....... . phthahe anahydnde. mala* anhydride K024......... phthahe inhydnde. polynuclear tar-bka matanats, naphthodunona K025......... meta*dmtrobenzar>e. 2.4-dmrtrototuene K026........ paraldehyde, pyndinas. 2-p>eolir># K027........ touiana Pww^anate. tok>ene-2,4-diamine. tars (benzidirrwdizapor)#) K028......... i.i.i-tnchkyoethane, vinyl chloride K029......... 1.2.*dchloroathane. 1,1,1 -tnchloroethine. vinyl chionde, vmlyiderte chlonda. chloroform K030........ hexaeftorobenzene. hexachlorobutadiane. has* acWoroethane. 1.1.1.2*tatrachloroethar>#. 1.1,2,2-ietrachloroethane, athylena dcMonde K031......... arsenic K032......... hexacWorocydopentadiene K033......... hexachtorocydopentadiene K034......... hexachiorocyciopentad^na K03S......... cresota. benz(a)anthfecene. benz(b)ffuoroan* then#, ben20{e)pyrene K036........ touian#, phosphorodrtNoic and phosphorothioic aod esters K037......... toulane. phosphorodithoc and phosphorothioic aod asters K038 phortt#. formaldehyde, phosphorodrttnort and phosphorothw aod asters K039.. .... phosphorodrthioic and phosphorothioic aod esters K040..... phorate. formaldehyde, phosphorodithioic and phosphorothioic acid esters K041........ toxaphene K042... hexachlorobenzene. ortho-d*chkyobnzen K043......... 2.4.d<chiorophanoi, 2,6-dtchiorophenot, 2.4.6- tnchtorophenot K044... . NA. K045 .. .... NA K046........ lead K047......... N A K04S........ chromium, lead K049..-..... chromium, lead K050......... chromium KOSt......... chromium, lead K052......... lead K0S3......... chromnrm K054......... chromium K055......... chromium, lead K0S6........ chromium, lead K057......... chromium, lead KOM.. ..... chromium, lead K0S9........ NA K060 ....... cyarvde, naphthalene, phenolic compounds, ar* sente K061......... chromum. lead, cadmium K062_____ chromum, lead K063......... chromum. lead K064......... lead, cadrmum K06S........ lead, cadmmm K068......... lead, cadmium K067......... lead, cadmum K066......... lead, cadmum K069......... chromium.4ead. cadmum NA--Wist# is hazardous becausa it moots tithpr tho ignrtabitoy, conowity or reictrwty characteristic. Appendix VII!--Hazardous Constituents Acetaldehyde (Acetato)phenylmercury Acetonitrile 3*(alpha>Acetonylben2yl)*4*hydroxycoumarin and salts 2*Acetylaminofluorene Acetyl chloride l*Acetyl*2*thiourea Acrolein Acrylamide Acrylonitrile Aflatoxins Aldrin Ally! alcohol Aluminum phosphide 4*Aminobiphenyi 6-Amino*t.la.2.8,8a.Bb*hexahydro-&- (hydroxymethyl)*8a*methoxy-5* methylcarbamate azirino(2\3*:3.4) pyrTolo(l,2*a)indole-4,7*dfone (ester) (Mitomycin C) 5-(Aminomethyl)*3*isoxazolol 4-Aminopyridine Amitrole Antimony and compounds. N.O.S.1 Aramite Arsenic and compounds. N.O.S. Arsenic acid Arsenic pentoxide Arsenic trioxide Auramine Azaserine * Barium and compounds. N.O.S. Barium cyanide Benz[c]acridine Benzjajanthracene Benzene Benzenearsonic acid Benzenethiol Benzidine Benzo[a]anthracene Benzolbjfluoranthene Benzojjjfluoranthene Benzo[a]pyrene Benzotrichloride Benzyl chloride * Beryllium and compounds. N.O.S. Bis(2-chloroethoxyjmethane Bis(2*chIoroethyl) ether N.N-Bis(2-chloroethyl)*2*naphthylamine Bis(2-chloroisopropyl) ether Bis(chloromethyl) ether . Bis(2-ethylhexyl) phthalate Bromoacetone Bromomethane 4-Bromophenyl phenyj .ether Brucine *m*.. 2*Butanone peroxide ** Butyl benzyl phthalatt'fj'.^;,. 2*sec-Butyl*4.6-dinitrophenol (DNBP) Cadmium and compounds, N.O.S. Calcium chromate Calcium cyanide Carbon disulfide Chlorambucil Chlordane (alpha and gamma isomers) Chlorinated benzenes. N.O.S. Chlorinated ethane. N.O.S^ . Chlorinated naphthalene. N.O.S. Chlorinated phenol. N.O.S. Chloroacetaldehyde Chloroalkyl ethers p-Chloroaniline Chlorobenzene Chlorobenzilate l-(p-Ch!orobenzoyl)*5-methoxy-2- methylindoIe-3-acetic acid p-Chloro-m-cresol 1- Ch!oro-2.3-epoxybutane 2- Chloroethyl vinyl ether Chloroform Chloromethane Chloromethyl methyl ether 2-Chloronaphthalene 'The abbreviation N.O.S. signifies those members of the genera) class "not otherwise specified'* by name in this listing. 2-ChIorophenol 1- (o-Chlorophenyl)thiourea 3*Chloropropionltrile alpha-Ch/orotoluene Cnlorotoluene, N.O.S. Chromium and compounds. N.O.S. Chrysene Citrus red No. 2 Copper cyanide Creosote Crotonaldehyde Cyanides (soluble salts and complexes), N.O.S. Cyanogen Cyanogen bromide Cyanogen chloride Cycasin 2- Cyclohexyl-4.6-dinitrophenol Cyclophosphamide Daunomycin DDD DDE DDT Dialiate Dibenz(a.hjacridine Dibenzja.jjacridine Dibenz(a,h]anthracene(Dibenzo(a.h] anthracene) 7H*Dibenzo[c,g]carbazole Dibenzofa.ejpyrene Dibenzoja.hjpyrene Dibenzo[a.i]pyrene 1.2- Dibromo*3*chloropropane 1.2- Dibromoethane Dibromomethane Di-n-butyl phthalate Dichlorobenzene. N.O.S. 3.3'*Dichlorobenztdine 1.1- Dichloroethane 1.2- Dichloroethane trans-1.2*Dichloroethane Dichloroethylene. N.O.S. 1.1- Dichloroethylene Dichloromethane 2.4-Dichlorophenol 2.6'Dichlorophenol 2.4*Dichlorophenoxyacetic acid (2,4-D) Dichloropropane Dichlorophenylarsine 1.2- Dichloropropane Dichloropropanol. N.O.S. Dichloropropene. N.O.S. 1.3- Dtchloropropene Dieidrin Diepoxybutane Diethylarsine 0.0*Diethyl*S-(2*ethylthio)ethyl ester of phosphorothioic acid 1.2-Diethylhydrazine 0,0-Diethyl-S-methylester phosphorodithioid - acid 0.0*Diethylphosphoric acid. O-p-nitrophenyl ester Diethyl phthalate O,O-Diethyl*0*(2*pyra2iny])phosphoroihioa!e Diethylstilbestrol Dihydrosafrole 3.4- Dihydroxy-alpha-(methylamino)-methyl benzyl alcohol Di'isopropylfluorophosphate (DFP) Dimethoate 3.3'-Dimethoxybenzidine P'Dimethylaminoazobenzene 7.12-Dimethylbenz[a]anthracene 3.3'*Dimethylbenzidine Dimethylcarbamoyl chloride 1. CAPCO JEN 0004-836 * vV';' 33133 Federal Register / Vol. 45, No. 98 / Monday. May 19, 1980 / Rules and Regulations 1.1-Dimethylhydrazine 1.2-Dimethylhydrazine 3.3*Dimethyl-l*(methylthio)*2-butanone-0* ((methylamino) carbonyljoxime Dimethylnitrosoamine alpha.alpha-Dimethylphenethylamine 2.4- Dimethylphenol Dimethyl phthalate Dimethyl sulfate Dinitrobenzene. N.O.S. 4.6-Dinitro-o-cresol and salts 2.4- Dinitrophenoi 2.4- DinUrotoluene 2.6*Dinitroto)uene Di-n-octyl phthalate 1.4- Dioxane 1.2*Diphenylhydrazine Di-n-propylnitrosamine Disulfoton 2.4- Dithiobiuret Endosulfan Endrin and metabolites Epichlorohydrin Ethyl cyanide Ethylene diamine Ethylenebisdithiocarbamate (EBDC) Ethyleneimine Ethylene oxide Ethylenethiourea Ethyl methanesulfonSte Fluoranthene Fluorine 2-Fluoroacetamide Fiuoroacetic acid, sodium salt Formaldehyde Glycidylaldehyde Halomethane, N.O.S. Heptachlor Heptachlor epoxide (alpha, beta, and gamma isomers) Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclohexane (all isomers) Hexachiorocyclopentadiene Hexachloroethane 1.2,3,4,10.10-Hexachloro-1.4.4a.5,8,8a- hexahydro-1.4:5,8-endo.endo- dimethanonaphthalene Hexachlorophene Mexachloropropene Hexaethyl tetraphosphate Hydrazine Hydrocyanic acid Hydrogen sulfide Indeno(1.2.3-c.d)pyrene lodomelhane Isocyanic acid, methyl ester Isosafrole Kepone - Lasiocarpine Lead and compounds. N.O.S. Lead acetate - Lead phosphate Lead subacetate Maleic anhydride Malononitriie Melphalan Mercury and compounds. N.O.S. Methapyrilene Methomyl 2- MethyIaziridine 3- MethylchoIanthrene 4.4'-Methylene-bis-(2-chIoroaniIine) Methyl ethyl ketone (MEK) Methyl hydrazine 2*MethyllactonitriIe Methyl methacrylate Methyl methanesulfonate 2*Methyi*2*(methylthio)propionaldehyde*o* (methy)carbonyl) oxime N-Methyl*N'*nitro*N*nitrosoguanidine Methyl parathion Methylthiouracil Mustard gas Naphthalene 1.4'Naphthoquinone l-Naphthylamine 2Naphthy)amine l-NaphthyI-2-thiourea Nickel and compounds. N.O.S. Nickel carbonyl Nickel cyanide Nicotine and salts Nitric oxide p-NUroanitine Nitrobenzene Nitrogen dioxide Nitrogen mustard and hydrochloride salt Nitrogen mustard N-oxide and hydrochloride salt Nitrogen peroxide Nitrogen tetroxide Nitroglycerine 4- Nitropheno! 4*Nitroquinoime*l*oxide Nitrosamine. N.O.S. N-Nitrosodi-N-butylamine N*Nitrosodiethanolamine N-Nilrosodiethylamine N'-Nitrosodimethylamine N-Nitrosodiphenylamine N-Nitrosodi*N*propylamine N-Nitroso-N-ethylurea N-Nitrosomethylethylamine N*Nitroso-N*methylurea N-Nitroso-N-methyiurethane N-Nitrosomethylvinylamine N-Nitrosomorpholine N-Nitrosonornicotine N-Nitrosopiperidine N-Nitrosopyrrolidine N-Nitrososarcosine 5- Nitro-o-toluidine Octamethyipyrophosphoramide Oleyl alcohol condensed with 2 moles ethylene oxide Osmium tetroxide 7.0xabicyc!o|2.2.l)heptane-2.3*dicarboxylic acid Parathion Pentachlorobenzene Pentachloroethane Pentachloronitrobenzene (PCNB) Pentacholorophenol Phenacetin Phenol Phenyl dichloroarsine Phenylmercury acetate N*Phenylthiourea Phosgene Phosphine Phosphorothioic acid. O.O-dimethyl ester, Oester with N.N-dimethyl benzene sulfonamide Phthalic acid esters. N.O.S. Phthalic anhydride Polychlorinated biphenyl. N.O.S. Potassium cyanide Potassium silver cyanide Pronamide 1.2-Propanediol 1.3*Propane sultone Propionitrile Propylthiouracil 2*Propyn*1*ol Pryidine Reserpine Saccharin Safrole Selenious acid Selenium and compounds. N.O.S. Selenium sulfide Selenourea Silver and compounds. N.O.S. Silver cyanid^ Sodium cyanide Streptozotocin Strontium sulfide Strychnine and salts 1.2.4.5- Tetrachlorobenzene 2,3.7,8-Tetrachlorodibenzo-p-dioxin (TCDD) Tetrachloroethane. N.O.S. 1.1.1.2- Tetrachloroethane 1.1.2.2- Telrachloroethane Tetrachloroethene (Tetrachloroethylene) Tetrachloromethane 2.3.4.6- Teirachlorophenol Tetraethyldithiopyrophosphate Tetraethyl lead Tetraethylpyrophosphate Thallium and compounds. N.O.S. Thallic oxide Thallium (I) acetate Thallium (!) carbonate Thallium (I) chloride Thallium jl) nitrate Thallium selenite Thallium (I) sulfate Thioacetamide Thiosemicarbazide Thiourea Thiuram Toluene Toluene diamine o-Toluidine hydrochloride Tolylene diisocyanate Toxaphene Tribromomethane 1.2.4- Trichlorobenzene 1.1.1 -Trichloroethane 1.1.2- Trichloroethane Trichloroethene (Trichloroethylene) Trichloromethanethiol 2.4.5- Trichlorophenol 2.4.6- Trichlorophenol 2.4.5- Trichlorophenoxyacetic acid (2.4.5-T) 2.4.5- TrichIorophenoxypropionic acid (2.4.5* TP) (Silvex) Trichloropropane. N.O.S. 1.2.3- Trichloropropane O.Q.Q-Triethyl phosphorothioate Trinitrobenzene Tris(l*azridinyi)phosphine sulfide Tris(2.3-dibromopropyl) phosphate Trypan blue Uracil mustard Urethane Vanadic acid, ammonium salt Vanadium pentoxide (dust) Vinyl chloride Vinylidene chloride Zinc cyanide Zinc phosphide |FR Doc KM4307 Piled 5-16-80- 8.45 amt BILLING COOE 5 j 1 CAPCO JEN 0004837