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PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES^LOUISIANA CONFIDENTIAL: Subject to Protective Order of 14th Judicial District Court No. 91-1145 GENERAL DEPARTMENT Total C12 + C Received fr-rin ? *DC I/TT T/D RPC TTT_________________ T-E II BC_______________________ VC I VC II P/T VDCM Conoco Shell Ga. Pacific Borden's Formosa Plas. (B.R.) ARGO ETHYL (B.R.) ETHYL (Pasadena, TX) Formosa Plas. (P.C.TX) Goodrich 1982 Av<y. 7.0 6.2 25.1 0.8 0.7 42.0 110.1 0.3 5.9 1.5 1.6 0.0 2.4 2.2 JAN. 32 1.7 2.5 19.9 0.2 2.9 9.6 71.9 0.0 4.7 0.0 3.9 0.0 3.0 0.9 FEB. 29 2.4 3.8 14.4 0.0 4.9 34.6 63.8 0.1 10.5 0.0 12.4 0.0 4.5 3.1 MAR. 1 APR. 28 33 4.7 1.0 4.1 0.3 2.1 56.2 69.3 0.1 0.0 0.0 14.0 0.0 5.3 1.9 6.6 0.0 9.9 1.1 1.1 47.5 64.1 (0.1 0.0 0.0 12.0 0.0 5.3 1.5 13.0 7.6 MAY 30 6.3 0.0 18.9 0.0 2.4 53.8 61.5 0.0 3.2 4.7 12.9 0.0 5.9 1.4 1.8 1.8 JUNE 29 5.9 0.0 15.7 1.1 1.4 32.1 75.2 0.1 5.7 0.9 17.7 0.0 7.1 0.6 0.0 2.1 0.6 1.3 JULY 32 5.5 0.0 34.7 0.5 1.1 20.6 58.0 0.3 8.3 6.3 17.3 0.0 9.0 3.9 0.0 3.2 3.1 1.7 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 11.6 0.0 9.9 0.9 1.2 16.2 33.1 (0.1 3.4 8.9 18.6 0.0 6.2 4.3 0.0 5.1 5.0 3.9 3.8 4.0 0.0 0.0 6.5 9.8 0.8 0.0 0.0 4.8 13.6 22.5 33.5 73.0 0.1 0.0 779------ 4.7 3.6 10.5 17.1 10.8 0.0 0.0 5.8 7.0 4.7 0.0 0.0 0.0 5.7 2.1 6.2 8.9 4.7 6.5 2.4 0.0 28. 3 0.9 3.6 24.7 53.2 1.3 3.2 7.4 5.1 0.0 7.0 9.0 0.0 0.0 9.0 0.0 1.7 4.7 0.0 0.6 12.1 15.4 0.6 0.5 1.1 2.2 15.9 28.0 131.6 65.9 4.6 0.7 775------ 7T76------3. i 3.8 2.5 11.9 070------ TJ70------- 6.6 6.1 6.4 3. 1 n.n 1.6 23 33 8. 3 5.9 n.n 2.6 qOii-- 011 4358 _______ Tranq -t-n P/T (TW-ra) 206.4 131.0 178.4 170.9 148.6 139.8 186.1 156.7 110.9 130.5 169.7 139.0 206.3 152.4 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES, LOUISIANA * *' AA 1 Sur>;jeot t. Protect! vc CrMer f 14th JiidicifU District Court Ho. 91-1145 GENERAL DEPARTMENT LOSS__________________________ 1982 AVG. 526.3 JAN. 32 FEB. 29 209.2 288.6 MAR. 28 266.3 APR. MAY JUNE 33 30 29 557.0 432.5 513.1 JULY 32 424.1 AUG. SEP. 29 30 29.5 297.6 OCT. 31 563.5 NOV. 31 486.7 DEC. 31 705.7 1983 397.8 POT TEMPERATURES F No. 1 Kettle Btm 332 No. 1 Second Kettle Btm 312 322 329 278 319 324 330 335 301 278 333 318 311 311 336 337 316 289 284 334 316 260 292 324 321 295 302 No. 2 Kettle Btm 291 283 272 284 786 284 294 297 290 im-- 276 279 280 284 No. 2 Second Kettle Btm 270 246 229 239 259 257 260 226 266 778------ 276 246 266 254 _________yields_________________ Cl 2 92.085 96.754 94.052 95.872 89.999 89.99F 89.999 91.999 99.986 93.480 89.995 89.999 90.00C 92.678 c. 91.995 89.999 96.104 89.268 89.999 92.495 89.999 91.99c 95.325 90.587 89.999 89.999 89.99s 91.314 SL ^14359 BI-305-20 SL 014360 WASTE RECOVERY UNIT PRODUCT Ethyl Chloride Wt. % Vinylidene Chloride t-1,2-Dichloroethvlene 1.1-Dichloroethane c-1,2-Dichloroethylene Chloroform 1,2-Dichloroethane Carbon Tetrachloride Trichloroethylene 1,1,2-Trichloroethane Perchloroethvlene U-Tetrachloroethane S-Tetrachloroethane Pentachloroethane Hexachloroethane Pentachloro Butadiene Hexachloro Butadiene Unknowns 1982 AVG. 0.25 0.10 0.38 0.13 0.56 21.99 0.25 0.49 24.60 8.44 9.27 13.65 8.83 1.84 1.11 2.03 6.19 JAN. 32 0.14 0.12 0.55 0.13 1.20 22.58 0.54 0.90 24.83 6.74 10.01 14.01 9.02 1.84 0.65 1.08 5.45 FEB. 29 0.02 0.09 0.26 0.12 0.58 27.83 0.37 0.39 30.11 4.58 7.03 12.77 5.58 1.31 3.74 1.25 6.82 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES* LOUISIANA MAR. 28 0.09 0.11 APR. 33 0.24 0.02 MAY 30 0.15 0.03 JUNE 29 0.23 0.03 JULY 32 0.29 0.03 0.61 0.56 2.01 28.72 1.01 0.66 25.16 5.81 6.44 12.18 6.78 1.63 0.74 1.21 6.39 0.20 0.16 0.07 0.06 1.36 0.75 17.97 23.08 0.35 0717 0.13 0.16 29.54 32.06 6.88 8.97 8.16 5.11 14.70 1 2.7.0 8.54 5.26 1.62 1.08 0.84 0.70 1.24 1.25 9.65 8.53 0.21 0.09 0.88 24.44 0.20 0.24 31.38 8.35 5.30 13.61 4.21 1.06 0.57 1.08 8.69 0.30 0.12 0.64 23.75 0.09 0.21 31.62 9.44 6.99 10.52 3.81 0.93 0.57 1.17 9.59 Protective Order of 14th Judicial District Court No. 91-1145 AUG. 29 0.29 0.01 SEP. 30 0.29 0.02 OCT. 31 (0.01 0.02 NOV. 31 0.27 0.11 DEC. 31 0.23 1.63 1983 AVG. 0.18 0.19 0.29 0.00 0.27 31.2 5 0.10 0.37 26.61 9.64 5.02 8.13 3.52 0.92 0.64 1.42 11.25 0.58 0.35 0.78 0.18 1.16 1.44 0.33 0.16 0.76 31.21 26.33 20.20 0.38 0.22 0.18 0.53 2.45 0.60 27.36 27.68 29.48 7.55 15.90 11.50 5.98 5773 9.02 8.00 6.61 11.65 3.01 1751-- 5.19 0.44 n.85 0.53 n. 5i 1.33 0.72 1.18 0.98 1.28 9.77 8.43 9.18 0.28 0.26 0.99 18.01 0.27 0.53 22.61 17.91 6.28 10.79 5.01 1.81 n. 75 0.95 7.80 0.34 0.21 1.00 24.61 0.32 0.60 28.20 9.44 6.31 11.47 5. 31 1.24 0.66 1.17 8.46 Specific Gravity 1.433 1.424 BOTTOMS PLANT WASTE Wt. % (INCINERATOR FEED") 1,2-Dichloroethane Trichloroethylene 1,1,2-Trichloroethane Perchloroethylene U-Tetrachloroethane S-Tetrachloroethane Pentachloroethane Hexachloroethane Pentachloro Butadiene Hexachloro Butadiene Unknowns Total 1.06 0.04 4.28 1.61 2.91 9.34 10.99 4.28 5.38 13.11 20.48 Toluene Specific Gravitv 0.15 - 0.57 0.03 5.29 1.67 3.76 10.83 16.97 4.28 4.25 8.83 18.03 0.30 L .44 D.O 6.68 0.76 3.10 11.32 7.7i 3.16 4.15 8.19 24.49 0.31 - - 1.485 - 1.405 1.395 1.78 0.0 5.42 1.32 2.09 10.42 9.39 2.88 5.28 10.48 17.10 0.25 _ 0.81 0.0 5.08 1.08 1.87 10.07 6.51 3.43 4.22 7.68 26.66 0.23 -- 1.19 0.0 7.22 1.52 1.94 11.01 5.01 2.01 5.20 4.74 30.35 0.39 - 1.93 0.0 9.35 2.76 1.45 0.0 7.26 2.91 1.96 2.33 11.65 8.84 6.02 4.43 2.69 2.99 2.92 0.0 2.86 0.70 33.25 36.66 1.34 0.53 -- 1.410 1.381 1.408 1.430 1.400 1.415 1.81 0.0 6.98 3.52 3.30 8.76 4.79 2.95 0.0 1.00 41.69 0.53 - 1.58 2.82 0.01 0.31 6.10 8.93 1.87 4.27 2.58 TM 8.77 9.05 5.06 6.23 3.30 3.75 1.87 2.00 12.31 9.07 32.85 27.73 0.16 0.01 -- 1.81 0.02 5.85 2.59 2.51 10.76 8.35 4.83 2.20 10.98 25.00 0.01 - 0.79 0.03 3.89 3.94 2.02 9.25 7.41 5.42 1.23 11.77 20.91 0.01 1.50 0.03 T750 2.35 2.46 10.06 7.32 3.47 2.78 7.38 27.89 0.34 -- 1 BI-306-10 GENERAL DEPARTMENT VENTS FLOWS MSCF/DAY 1982 AVG. ...VC I___________________________ 25.8 No. 1 EDC 18.0 No. 2 EDC____________________ 84.5. P/T____________________________ 827.Q -QHC-.I__________________________ 181.7 TrirEthane II_______________ 15.8 OHC II 108.4 EDC III CINCIN. FEFD'i 38.9 JAR 32 40.5 57.9 96.3 716.0 35.3 31.4 122.9 30.8 FEB. 29 20.1 35.4 155.4 834.1 6.6 13.9 168.0 38.9 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLESL LOUISIANA INCINERATOR OPERATIONS REPORT C'lNF J OEMT t A1,: Subject f.*. rcobfctiwe Older :f I 4 *: b .Slid i cirri Ob strict Court no. P1-.U45 MAR. APR. 28 33 45.0 49.0 107.0 118.4 126.2 120.6 618.6 888.2 31.4 121.6 6.2 9.5 15.1 123.0 7.5 0.0 MAY JUNE JULY AUC. 30 29 32 29 44.5 19.4 21.7 26.9 47.4 52.4 116.2 116.9 156.6 148.1 196.3 221.9 948.2 1001.4 1140.2 835.1 121.0 121.1 187.7 128.4 29.6 29.7 17.2 22.3 174.9 134.0 110.'3 89.5 0.0 0.0 0.0 0.0 SEP. 30 0.0 30.6 141.2 851.5 177.9 16.9 74.1 U70 OCT. NOV. DEC. 1983 31 31 31 117.3 0.0 0.0 32.2 0.0 0.0 2.5 57.1 179.5 141.3 138.8 151.5 1162.2 1129.1 1311.0 956.5 125.4 150.5 134.4 112.7 46.9 55.0 0.8 23.4 123.0 42.6 104.6 107.2 0.0 0.0 0.0 6.4 Liquid Flow to Incs. from Waste Recovery Lbs./DAY 59275 43203 102832 73234 96091 8684 5 126060 72732 96951 88476 138422 117727 0767#; a/,8i o No. 1 INCINERATOR Waste Gas MSCF/DAY Natural Gas MSCF/DAY Sabine River Water GPM Combustion Air Flow\SCFH ^Operating Hours 398.2 237.3 452 _ 4335 8349 362.6 303.0 411 3732 732 298.0 278.4 37Q 4414 630 711.3 319.3 450 4388 650 312.6 205.0 519 3741 763 510.9 66i -0 275.6 202.0 758 60 3 3853 4786 635 687 752.2 218.6 585 4686 750 411.0 293.9 871 4232 679 279.3 322.1 577 4042 71 L 448.4 474.2 285.8 273.5 538 562 4163 4571 728 735 494. 5 218. 1 528 3411 725 474.7 266. 3 564 4168 702 HC1 in Aqueous Sol. Tons 180 114 60 236 ... 164 Liquid Waste Burned Tons 140 0 0 16 21 No. 2 INCINERATOR Waste Gas MSCF/DAY Natural Gas MSCF/DAY Sabine River Water GPM Combustion Air Flow SCFH Operating Hours 383.0 319.9 478 4463 8276 378.9 536.6 466 1708 726 497.5 461.4 475 3987 679 542.9 353.9 478 4607 664 74.1 117.5 183 4666 243 253 339 587 169 172 315 470 177 255 34 0 0 0 0 00 0 6 150.4 462.2 401.6 415.9 723 559 2422 4379 666 671 515.1 341.4 548 5514 744 158.7 105.3 282 3664 327 1.8 87.2 114 -- 96 86.4 551.9 311.4 308.4 573 543 4466 4730 726 718 628.6 336.5 289.9 310.9 514 455 3260 3353 -- 330 HCl in Aqueous Sol. Tons 400 Liauid Waste Burned Tons 490 62 0 117 154 82 0 117 60 126 304 735 94 60 191 0 28 258 602 1 q5 230 0 O 0 A 31 -- SL 014361 * Tot" a 1 BI-306-20 PPG INuJSTRIES CHEMICAL DIVISION LAKE CHARLESL LOUISIANA INCINERATOR OPERATIONS REPORT COBTIOEMTiALs to Fr(;tcot.iv:; J*n1ici<l t'isfcrici Ccurt 5 No. 3 INCINERATOR Waste Gas MSCF/DAY Natural Gas MSCF/DAY Sabine River Water GPM Combustion Air Flow SCFM ^Operating Hours 1982 AVG. JAN. 32 FEB. MAR. APR. MAY JUNE JULY 29 28 33 30 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 1129.6 1349.7 1022.6 438.4 1094.1 1218.5 1133.0 894.0 1048.2 983.6 1467.1 1154.8 1504.1 1115.2 170.9 114. ft 86.8 61.7 102.6 123.3 111.2 147.2 129.3 168.2 129.fi 67.7 135.2 114.8 192 144 173 105 177 196 197 172 164 283 190 192 187 182 532222 722916 765115 365556 696907 713112 778388 682766 735298 678675 766381 714002 736244 696280 7739 743 661 399 688 593 659 603 670 691 720 546 737 7810 HC1 in Aqueous Sol. Tons - - --- - - -- _- -- -- Liquid Waste Burned Tons* 451 691 1491 892 1564 1263 1828 n55 1406 1327 2146 m3-- "15T4 ' 1426 *Inc. Purchsd .Bottoms Tons 0 - 44 0 00 0 0 0 0 0 47 ~D-------- ~B--------- 175# Steam Gen.(900#Basis] MMLbs. 17.6 22.5 21.2 12. 7 23.2 21.7 18.8 15.0 21.4 20.5 23.4 13.4 73.1 19.7 Wfiflk AriH Recovered T/D _ 42.0 49.6 25.0 40.7 47.5 50.8 45.1 49.9 45.1 * 61.0 41.7 63.0 46.9 qOiw 0w 14362 * Totals BI-306-30 INCINERATOR 1982 AVG. STACK GAS ANALYSIS PPM JAM 32 PPG IiNnPIT^Sj TRIES CHEMICAL DIVISION LAKE CHARLES^ LOUISIANA f? t.t i ?'} t' *; t; * > I* ;*' T; ' * * f- **I .j of ; i ,t t *_'> s'r ici No 2 * ~ M , r3 FEB. MAR. APR. MAY 29 28 33 30 JUNE JULY 29 32 AUC. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 No. 1 & 2 HC1 Cl No. 3 HC1 Cl 93 10 23 (1 6 47 (1 . 4 154 57 108 2 18 2 15 (1 (10 8 17 16 (1 1.3 4 7 19 37 24 27 80 3 68 14 18 (1 (1 31 33 (1 (1 15 22 (1 6 20 22 (1 (1 24 17 22 28 32 17 oL 014363 SEWER SEGREGATION 1982 AVG. Plant Feeds Waste Flow Steam Flow #1 Steam Flow #2 API Separator Flow GPM 581 jSTffiT 14146 #/HR 6736 GPM JAN. 32 901 _ 12182 6675. PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES*, LOUISIANA WASTE TREATMENT COifFID&fTIAt.* Subject to Protect#TO fitter of 14th Judicial District Court No. 91-1145 FEB. MAR. APR. MAY JUNE JULY 29 28 33 30 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 634 385 12267 5337 8102 4702 367 6305 5056 547 843 4549 4165 10117 8633 6 30 IftQflQ -- 757 17 360 6238 727 15811 4457 759 767 18040 17767 3018 4731 852 16567 7215 - 681 12855 6313 - *No. Hours Overflow/Mo. Condenser Feed it 1 Out (Tempi F 7 131 - 128 - 127 - 126 -- -- _ 129 119 127 127 127 127 127 _ -- 126 T77-- ~T26-- Pick Heater #1 Inlet (Tempi Outlet (Tempi Steam Flow F 163 152 156 158 153 1 54 176 165 165 167 173 176 1 6Q 1 64 F 211 206 204 197 205 208 207 204 185 198 200 198 210 202 #/KR 9532 7376 6979 3797 4542 3232 11689 9573 11511 11499 11086 8128 Steam Stripper #1 Overhead (Temp) F 211 214 215 212 210 212 211 211 210 211 211 210 211 212 Bottom (Temp) F 215 217. 216 216 221 211 211 212 213 213 212 21 1 212 214 Feed Flow GPM 385 363 _ 304 183 254 134 308 478 466 436 537 481 418 364 Steam Flow #/HR 4821 4730 3910 2114 2065 998 - - 5524 5574 6045 5859 5545 4266 *Hours of Operation 690 717 533 314 530 222 492 708 640 592 744 708 636 6836 Flow/Steam % 1.63 1.80 1.68 1.86 2.31 1790 - - 1.62 1.69 1.84 1.66 2.14 1.85 Phase Separator Product Plant "B" Outfall (010) (018) GPM 0.0 0.0 0.0 0.0 0.0 o o 0.0 0.0 0.0 0.0 0.0 0.0 GPM 701 GPM 3955 381 3864 299 371 5212 4881 290 423 5010 5109 526 4614 544 4496 466 5524 627 4733 280 487 4469 4921 nn nn 473 ~TTL----50Q3 4827 SL 014364 i 1_____________________ BI-307-20 SEWER SEGREGATION 1982 AVG. Condenser Feed 92 Out (Tenro) ^F- PPG INuJSTRIES CHEMICAL DIVISION LAKE CHARLES, LOUISIANA L'MrFTUWi'l-M.: b : J ;7 c t t <> f* f; ,r , . f i . . , , J , j J. cz e iJ. ifi strict CouVY: No. 9I-U45 JAN. 32 FEB. MAR. APR. MAY JUNE JULY 29 28 33 30 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 _-- 93 _ 88 -- 84 164 170 148 151 -- 128 Pick Heater #2 Inlet (Temp) Outlet (Temp) Steam Flow F F #/HR 185 215 4567 184 211 4156 177 210 4260 186 211 2827 176 214 3134 175 213 5017 179 211 4473 92 194 - 160 200 2740 170 213 2900 165 211 1926 181 209 2404 179 169 212 209 7(179"" 3456 Steam Stripper #2 Overhead (Temp) ``F Bottom fTemn) F Feed Flow GPM Steam Flow #/HR *Hours of Operation Flow/Steam X 213 216 387 2273 8137 3.48 214 215 397 3864 648 2.97 214 215 421 3493 564 3.26 213 215 458 3369 532 4.44 210 2 37 336 4047 571 2.81 210 21 3 482 5375 696 2.78 210 214 325 4321 556 -- 210 214 140 252 -- 211 213 265 3029 368 2.76 209 71 3 251 2290 300 2.90 210 212 185 1572 216 3.17 210 212 277 2429 308 3.44 710 71 L 307 3070 404 2.54 71 1 91 6 390 3351 5415 3.11 Phase Separator Product GPM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 1 SL 0i4oo3 4*<T BI-307-30 WASTE TREATMENT (Sewer Segregation) 1982 AVG. JAN. 32 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES^ LOUISIANA LAB OPERATIONS REPORT tV^IDfcNTJAL* Subject t'. rmeotiv* Orris r of l4th 7iicial Oiittrict Court Ho. Sl~il45 FEB. MAR. APR. 29 28 33 MAY 30 JUNE JULY 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 1983 31 Stripper Bottoms #1 Components: VC Cis/CHCl^ 1,2, - EDC Total C1HC PPM Q. 18 0.04 0.03 0.12 4.38 6.39 4.70 0.97 19.05 6.77 2.04 4.30 29.55 15.69 10.69 9.89 0.30 0.16 0.90 1.64 7.12 3.83 11.60 7.95 o!os 1.78 1.69 6.61 0.12 1.96 3.92 9.51 0.03 0.14 1.77 5.56 0.02 0.73 2.33 4.84 0.01 0.88 3.81 7.06 0.11 0.86 3.15 8.05 0.01 0.93 1.77 4.39 0.08 1.82 3.54 8.19 Stripper Bottoms #2 Components: VC Cis'/CHClq 1.2, - EDC Total C1HC PPM 0.12 4.24 10.33 21.06 ore 7.18 5.06 15.87 0.11 3.80 5.28 12.43 0.12 1.07 7.27 11.97 0.42 0.77 9.65 16.31 n. 14 2.47 8.72 14.11 0.06 3.02 6.68 13.47 0.01 1.90 7.28 11.80 0.03 0.03 3.99 8.76 0.08 0.26 2.25 4.51 (0.01 0.23 3.30 6.38 0.06 0.8? 4.21 8.47 0.04 1.72 4.81 9.39 0.10 1.94 5.71 11.12 "018'' Outfall Components: VC Cis/CHCU 1,2, - EDC Total C1HC TCE PH PPM 0.04 0.98 3.51 6.91 0.45 1.6 0.02 1.11 3.73 7.11 0.17 2.6 0.01 1.03 2.11 4.79 2.30 0.3 0.06 0.35 3.47 6.49 0.91 1.9 o.u 0.88 4.55 7.12 0.27 1.3 OTIS 0T6I 3.18 4.85 1.49 1.7 0.02 0.76 4.88 4.38 0.26 1.9 0.05 0.37 3.22 5.17 0.28 1.3 0.03 0.22 1.66 4.31 0.62 2.4 0.04 0.29 2.06 3.60 0.09 3.2 0.01 1.00 2.31 3.52 0.18 2.6 0.05 0.12 2.07 3.72 0 1.6 0.02 0.35 3.08 5.18 0.05 3.3 0.04 0.59 3.03 5.02 0.60 2.01 014366 BI-307-4O WASTE TREATMENT (Sewer Segregation) Plant "B" Sewer After OHC 1982 AVG. JAM 32 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES^ LOUISIANA LAB OPERATIONS REPORT C(WFIDKNTIALt Subject t.o Protective Order of 14th Judicial lUstrict Court No. 91-1145 EEB. MAR. 29 28 APR. MAY 33 m JUNE JULY 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 Components: VC PPM VDC Trans/EC- MeCl? ___ QL4_________________________ Cis/CHCl^ TRI 1,1, - EDC MC PER 1,2, - EDC TCE Unsvmetrical Symetrical Total C1HC PH 0.13 0.22 0.65 0.28 0.90 0.22 0.80 0.0 0.45 0.02 0.45 0.27 0.65 0.22 0.49 0.03 0.65 0.08 0.17 (0.01 4.46 14.15 0.98 0.38 0.33 0.24 (0.01 0.0 9.82 15.94 6.73 5.9 0.02 0.12 0.05 0 0.45 0.41 0.25 0.30 0.11 0.14 9.57 0.46 0.51 0.01 12.00 6.1 0.08 0.08 0.18 0 17751 0. lij 0.46 0.11 0.58 0.14 7.15 0.34 1.03 0.02 10.51 6.7 0.06 0.05 0.22 0 0.10 0.07 0.04 0.03 0.05 0.04 6.04 0.40 0.37 0 7.17 6.6 0.04 0.11 0.10 0 0.22 1.22 0.53 1 .07 1 .01 0.28 6.41 1.75 0.45 0 8.25 6.9 0.07 0.52 0.49 0 1.18 0: Si 0.72 0.42 0.43 0.24 6.76 0.75 0.63 0.06 12.88 6.7 0.08 0.14 0.18 (0.01 1.54 0.36 0.41 0.25 0.01 0.96 5.20 0.31 0.74 0 10.45 5.3 0.06 0.35 0.28 0 1.81 0.41 0.44 0.18 0.04 0.47 "5703 0.40 0.40 (0.01 8.63 3.5 0.02 0.06 0.71 0.80 0.29 0.86 00 0752-- T793 0.53 0.16 17759 1.90 0.13 0.10 0.83 0.31 0.17 0.78 4.54 38.93 0.19 0.54 0.14 0.56 0 0.03 6.53 29.36 3.2 2.9 0.19 0.43 0.23 (0.01 4.36 0.57 0.60 0.65 0.41 0.87 7.40 0.82 0.59 0.02 18.02 4.6 0.10 0.19 1.16 (0.01 1.45 0.34 2.84 0.84 1.34 1.58 18.13 1.74 1.21 0 31.21 6.8 0.08 0.32 0.36 (0.01 1.16 0.47 0.71 0.40 0.37 0.47 10.69 0.67 0.57 0.01 14.25 5.4 __ SL n0Ui3*i br7/ BI-308-10CENTRAL OHC STRIPPERS OPERATIONS PPG INDUSTRIES CHEMICAL DIVISI N LAKE CHARLES LOUISIANA CENTRAL OHC STRIPPER Plant Feeds Waste Flow Steam Flow Combined Fd. GPM #/HR PH 1982 AVG. 95.0 5087 11.1 JAN. 32 5R.fi 3535 11.1 FEB. MAR. 29 28 101.9 75.8 5146 5143 10.8 10.7 APR. MAY JUNE 33 30 29 110.5 5847 10.8 107.6 4809 11.0 98.2 5728 11.1 JULY 32 86.4 4266 11.7 Steam stripper #1 Ovhd Temp. F Liq.Phase Temp. Feed Flow Steam Flow F GPM #/HR Hrs. of Operation 192 208 58.9 3310 4855 212 229 -- 364 61 193 229 81.6 3783 652 187 226 26.4 1929 324 189 227 31.2 1768 406 197 229 73.9 1221 321 198 227 42.2 2480 461 198 228 48.8 2431 544 P i i h i ; c t. *.f* V r; v t u ` - t i v 41 ir < 13 r of inch .Jiitiioio i i111 r i cr Court Ho. 91-1145 AUG. SEP. 29 .30 OCT. 31 NOV. 31 DEC. 1983 31 88.9 42.95 12.1 63.0 4077 12.0 90.4 471R 12.1 86.2 5701 10.9 58.0 4 336 9. 3 85.5 4758 11.13 200 196 -- 229 229 - 9.6 42.3 - 398 2823 - 74 265 - 193 229 61.6 3661 262 190 230 1.4 136 24 196 228 41.9 1909 3394 Condenser #1 Out Temp. ?F -- - -_ _ - --- _ __ - - Steam Stripper #2 Ov'hd Temp. F Liq. Phase Temp. F Feed Flow GPM Steam Flow #/HR. Hrs. of Operation 210 218 92.7 3780 5470 208 228 2950 581 217 229 0 2818 254 218 227 - 3215 479 222 227 49.5 3992 595 219 277 104.6 4140 555 221 228 81.8 3249 581 222 228 46.6 1898 398 222 229 86.4 4038 628 221 229 51.0 2422 458 220 227 87.3 4718 728 222 225 74.0 3309 547 221 779 50.5 4200 743 219 228 70.2 3412 6547 Condenser #2 Out Temp. F - - --- - - - - - - - - -- - /S-ML nU4114o00 BI-308-20 CENTRAL STRIPPERS 1982 AVG. JAN. 32 PPG INDUSTRIES CHEMICAL DIVISION LAKE CHARLES*, LOUISIANA LABORATORY OPERATIONS REPORT CONFIDENTIAL: r^^r Subject to Protective Orlrer o 14th Judicial District Court Ko. 91-1145 FEB. MAR. 29 28 APR. MAY 33 30 JUNE JULY 29 32 AUG. SEP. 29 30 OCT. 31 NOV. 31 DEC. 31 1983 Stripper Bottoms #1 Components: PPM VC Cis/CHCU 1,2, - EDC Total C1HC n.Qfi 0.21 12.65 16.72 0.09 0.0 1.43 7.04 0.48 0.38 4.58 11.20 0.69 0.16 8.90 14.36 0.72 0.25 5.11 8.82 0.40 1.86 3.64 6.95 0.33 0.61 2.77 5.72 0.07 0.10 2.55 5.50 fO.Ol 0.00 2.43 7.75 10.01 0.15 2.05 2.80 -- - - - 0.01 0.23 3.62 4.47 0 0 3.73 3.83 0.25 0.34 3.71 7.13 Stripper Bottoms #2 Components: PPM VC Cis/CHCl-i 1.2, - EDC Total C1HC 0.87 0.40 5.68 9.59 1.11 0.09 2.88 7.24 0.03 0.52 1.42 3.96 0.16 0.47 4.45 9.58 0.17 0. 90 6. 34 7.99 0.36 2.26 2.15 6.86 0.27 1.40 2.92 6.70 n or 0.16 2.26 5.13 0.36 0.44 1.72 5.47 0.07 0.05 2.09 3.03 0.05 n.n3 2.61 4.60 0.02 0.14 4.35 6.19 0.40 0.18 4.11 7.97 0.26 0.50 3.03 6.23 cqiL 0U 1l 4H 36w9w