Document nkNJ01YneokBKEoYrX8rQ3406

CAM-86 COL 00477 . EXHIBIT I Lthrvinrt LPLAINTIFF'S McCRONE 0001 tune 23., 1976 lit. Zen Stovafl J4cCne Associates 2620 Bcutb MLcM en Avenue E 60616 Zen, aie is to toxf3a a oopl'rgatton 2 M idtb Gene ariege acnoerflizg tut*e T$t-M 9atfl2s t tale to? eelflte-.YaasdLt* CctwInv. To save tile 2 asked Ue* dt ow 5uppU could saM a liwis .*inet3- to 3M% lab tab yen wovid zet sidyn iztdl we bed a ebeaoe to oerssfl Si tr 2abctstsy by s'4'ay .d&taatScn aM' D$ibsl .MtGsdbflb r th* iaterSsx yt *aM Ubestos4ree StSrvs.tu.jesaislg.t%ttOdnUguZot44rdt*tli*stb,on**Syvwet'uhteelAy0os.1au.aat;QtfieletOost.hi1e%s it 2 flat, we mw *3flI4 t. By. the' irpcsii asthot ft. wilt itS thU 2 t! S 4QI ysqub,4 tct tbe aflq be taysi frcfl ala n*my to. Gene itididatid .tIin at nb flcbdn itt thSSntant as tar is Mse Apoflates is encotted. Thu .'W b S CoavesSe*qe for vs4 sad I +43r ina4*te y to work d* this ws. Si-,. jPSzls oat C. B. i.sger 3. 1, i*o COL 00478 McCK.. JUN 241976;. COLGA TB-PALMOLIVE COMPANY A Vd*nr q,retk,, R$SEARCH AND DBV.ELOFMBNT DEPARTMENT POP River Ro . flsteMway. New Jersey 01854 .Tune 22, D$76 Ii'. Gene B. Gfleger Moone &nocjstez 2820 South *cbigezt .&vemte Chicego, U, 60616 Dew Gene, Tbtu is to coxifirt ota telephone conversation ot yesterdey ooucernixig talc lot zwziber 6-13-1k tor our Jeflernoufl2ae j'.tant. Please run TEM-SABD ans1ysie or asbestos on this ssip1e. Z idfl telephone 'ou a Purchase Ordar ne to cover costs. Totre tru3r, 3. P. Slnflco COL 00479 MeCRONE 0003 - 'at4.v..;a. -....- t 1t' Slew ilk &p- 635737 vSr.-war C S-'iai W':i/artI ik 'r-' .*Jcer,paU1n -- frt F - . :1 l. It 1,1 COLCATE.PALMOLWR COMPANY A .XWAN.C6POMTIOK IS.NUDSQN STREET, JERSEY CITY, N.J. 07302 A17SN8 . I.. 41-' - "up" I1 McOrone Associates ? Mid . .. REc.yeo413 2 n IIJtSOGflIRYECEINTSY,ITN. .J. 07302 24 UI flIVfl RD. ISCATAWAY. N-I. 01114 .1I JtSSSY CITY, NO. 07502 IS IIRJSEYCfClRW$IDKCNVITILA&TIEQ,N IIIDOANA 471St L.. DISCOUNT rESINS .1 r]z'io W3Q 2N40 i/IC N/sO 4 Hit Cub S trade SHIPPING TERMS I roe DistlIlItloil 2 POe Shipping fl. PirPvytBfll)Sn&kw 3 0 POflShlppIi,gPL (tolka) City PRods 7/26/$lLbIITEO U? TOs 12/31/76 LSOVC OATS CANNOT St MET NQTIfl STATION [JREKCAtNIVSAINSGCITY, NAN. III IS flsol I IIIsVnCIAcII;Iv.T.OcNst5.1'w. sqio SDOISDH PYAOIRIKK.LNW.Y. . 0028 ATIN: lIcuFvIng Clek .Mt ADINORIZ 0 To YmMI5If TIlt AWTICLcI USXW IIEIEOII Ill ACCOIDANCE WITH 7-IC T&IIMD Alit CONDITIOIIS eli tilE lAOS AND.IACK OF Tills 01011. QIIAIITITY AltO UNit SYIWOLIflINSIR '. PRICE -' yoMne zia],y ._.nPA': :2L.Sausmiszion 2catoiz oosgpw.,q14_$4pjA!9.a mt%x'on Dittriot ion Ana37si 2. .-*re' azElysia -: C. 's..: ' '.. J300ie0b ,: .h' . .: g VENDOR TO PROTECT' ALL METAL PARTS AGAINST CORROSION BY SUTTASLE PROflCTIVE SEALING. kal .Minxk tot. d.th. I wp.,i$cionIiqkS..nThatiss bsj, ,nd'bi #S 4nidbkouas,d.tJy..,#Matp.tosRacsWlao..sw*1i*kst h4n .'4, Land, PAYMeNT WIlL NOT U MADE AGAINST MO ivmA INvola'. WVI UNIU4DIP4G lpfl oS Is. for kavy Tad. L SW'ago 20143243% .ados 100. . flfF Bt' .-i.__'t - ......'........-'MX MUSt LB BILtD TJNLES$ E)OT1(PI By ArJ!aquj IY. . :. ... ( McCRONE 0004 COL 00480 Invoice no. 10175 10246 10287 10363 10376 Colgate Pslnwiive Company MA 5259 Date 81 Mar 76 10 Apr 76 22 Apr 76 14 May 76 24 May 76 Amount 2,000 900.00 600 1,003 875.00 Invoioe 1024.6, 19 Apr 76 1,800 soo.cv \ caD (I :p$ Welter C. Mocrone Associates, inc. COL 00481 MeCRONE 0005 RECEIVED PU0 Auflat 5, Z9$ Ia. Nat *Z!X'O2US Z6ione Msd.stea 2$2O loath Wttfln *venue XL 6061.6 Diar trina T$bpS .gtc ttoo csz3n our tdqbone t-IA(Lfl aMivaiI S' ctaclne viewDpa1ti.iz rosf this det, with gata_!aIsl 1n. W44* Wiov *h 4P$S. .*ex3A. ncW%P bt''g tek ntaa ct thSm aM lts*i pncbsfl sde* awtrn IT- Pabase o*dar w*bqr 65037 ib a bZS*st mtn Sdh wtfl cover td*irde nreeqt *rintaae. tW!*tifaljlga.sUbuflai a l.t,m*ir 6-2a1.2 ter tie we prafle$es aosfl- 4in*4*eao1s2*intatorit rMeqe$s &fl tzot cessi by t be3.tne U$ tide IIXsfl us up to thitu. ThIS yu. !C W. a. ar4ger COL 00482 McCRONE 0Q06 COLGATE-PALZvIOLWB COMPANY 4 Dd.,ct Grfratts RIE4RCH 4ND DEVEZOIMENT DEPARTMENT 909 River Read . Piscataway, New Jersey 02854 August 6, 1976 2*. Gene Uveiflr? M30X012e Aasoci8tea 28O South *cbigan Mwnue Cbicago, 3t 60616 Desr Gene, Eniosed is a ta3.c sample c4e4 0-U for a*btos ata1yais by ltM-SAZD, Charges Thr this sacte s)aoula be n$4e to Pwcmse Order #635737. Thaa,lv you. iT. P. Sizito COL 00483 N COLGATE-PALMOLIVE COMPANY 4 DddcMfl C.rp..Wkn 7tBSRARCH 4?W DRVZLOPMENT DBPAR?MSNT 909 River Read 2'iscflmway, New fern; 08854 R?VE1 .LI August 11, 1976 Mt. Gene $reiger Mone Associates 2820 South Michigan Avenue chicago, z1 6oL6 Dear Gene, This is to conflrm out' telephone conversation oi' August 10 reoyesting TEN- SAED ansqsis of talc lot 8-6-y. nuner to this work. !Dhaa,ka. Please charge our blanket purchase ox'der JPS:la 1T. P. Bnko COL 00484 McCRONE 0008 LVI wafter c, mccrone Ossdates, frc. COWSULTING ULWAMIOROANALYSIS- MIGBOSCOPY SMALL PARTICLE PROBLEMS SOLID-STAn CHEMISTRY 81 August 1976 Dr. Joseph Rhnka, Jr. Cotgate-P&mollve Company B&D Department 909 lttver Road Piscataway, New Jersey Ossot Dear pr. Slmko: Using inrismisslon electron microscopy and selected area electron diffraction, we have analyzed The sample of talc designated as 8-64. We found this talc th be free of asbeetiform minerals, both amphibolea and aerpentSne. This is an excellent quality talc, that is very platy and with a high percentage of flne plates. Thank you for causulthig Mocrone Assoctates If there are any trtber questions ooncernbig this report or the data dontained Therein, please feel free to contaotme. Vezy truly yours, GneR. Gfleger Senior Research Pbystolet ORG tie ref: 5500 22O SOUTh MIOHIGAN AVdNUE . CHICAGO, IWNOIS 50818 82ea42-flQO CAStE CHEMICRONE COL 00485 McCRONE 0009 waiter c. mccrone associates, ho. CON8ULTINGI ULTRAMICRONW.Y$I6 MIOHOSOOPY SMALL PARUCLE PROBLEMS soLrn.STNVE CHEMISTRY 31 August 1076 Dr. Joseph Shnko Wolgate-Palmoltve Compafly Da&D Departhient &O9 River Road t,flseataway, New Jersey 08804 Jar Dr. Stinker ?*Ysthg *ranmlssion electron microscopy and seleoted area electron diffraolaon, we bate snrnThed a Bample designated b' Code 0-IL. a sample was completely free from asbestiforsn materials, both 'ampblbole and serponthie. The material was platy and &iowed a moderate 4 level of fine particles. In general, therefore, it was an excellent sample oflajc. If there Bhouid be any queettnw regardLng these results, please feel tree to contctus. QBthfe rcA 5U0O e B. Grieger Senior Research Pbysiotst 2520 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 60510 512/842.71G0. CASLE: CMEMICRONE COL 00486 MeCRONE 0010 waiter c rncrone assodaies, Inc. CONSULTING: ULTRPMICROWLYS)S MICROSCOPY SMALL PMTIOLE PROBLEMS SCUD-STATS CHEMIStRY - 31 August 1976 Dr. Joseph 81mb, Jr. Colgate-Palmolive Company 909 River Bead Pisoataway, New Jersey 08854 Dear Dr. Bimko; Using transmission electron micros copy end selected area electron dfffraclion, I bate analyze4 a sample of talc designated as 8-10-11. hi this sample we found no ampbthotea end no serpttines. We found this sample to be free of all asbestUorm minerals The sample consisted of a large portion of fines approxImately 15-25% most of wldcb were platy. There was a small portion, 5-7%, which was not platy mid just general irregular particles ctoh were also thin enough to be transparent to the electron beam. The difference here was that they were not thin sheets with well defined crystalline edges. There was also son eWbat less than one percent of tab fibers and shards. this materiel seems to be quite good in general and better than the avenge that we have seen. As I mentioned previously, there was slightly less fines than in Sample 8-8-7 which -we analyzed prevtously Thank you for consulting MoCrone Associates sad if yost should have any qusUo2as con oentg these results please contact us. Veny tiuly yours, p GRGie reA 5500 GzeB. Grieger Senior Bee earth Plsic1st 26 SOUTh MICHIGAN AVENUE. CHICAGO. IWNOIS 60618 312/U2.TIDO CABLE: CHEMICRQNE. COL 00487 MoCRONE 0011 41 /2.. a I. 4' rv- }.#_ S waiter C. mocrofle assOciates, Inc. ;fH'7flr :., J; cflQ - COL 00488 MeCRONE 0012 I -0. V ; - ..A... . bT(50,00C) waiter c. mc drone aEsocIateinc. COL 00489 MCCRONE 0013 t waiter a nicrone associates, inc1 CONSULTING: ULThAMICROMALY$IS MIORO$00PY SMALL FMtGLE PROBLEM& SOLID-STATE CNEMISTT4Y 15 September 1876 Dr. Joseph P. Slake, Jr. cogate-PaimoUve Company 909 River Road Pisoataway, New Jersey 08854 Dear Dr. Birnko: Using transmission electron microscopy and a elected area electron diffraction, we have analyzed a aonple of talc designated as 8-28-29, We found no aabesUfonn minerals In ibis tale. We did, however, And a few extrem sly fine talc ribbons and particles at rolled tale, of which we took electrai plictomiorograhs, and they are Included with ibis report. Again we So'md that there was a feixiy substantial portion of this Mo which was fine in natire, less than 5 sm in general, The talc OOhStItIIteS an cco1lent cosmetic quality tale and is extremely platy. U there are any further qiestioiw concerning this report or the data contained therein, please contact me. Yours sincerely, GeneR. Grieger Seiuior Research Physicist GBGde enclosures ref; 5500 2820 SOUTH MICHIGAN AVENUE. CHICAGO, ILLINOIS 80618 312,442-7100 0*81.5: OHEMIORONE COL 00490 McCRONE 0014 $am$e 8-28-29 - talc (60,000X) -: waiter c. me crone associates, Inc. COL 00491 MeCRONE 0015 I, S 'F 4 I- ft I, 4 / 1./ I t C5. Sample 8-28-29 - tale -J (50, DOCK) waiter c, mecrone associates, Inc. COL 00492 McCRONE 0016 waiter C. mrone associates, Inc. CONSULTiNG: ULTRANICROAMtYSIS' MICROSCOPY' SMALL PARTICLE PflOOLEMS. SOLIO.SThTE CHEMISTRY 5 October 1976 Dr. 3. P. Shnko, J. Colgate-Palmolive Company R&D DeparIent 909 River Bead Piscataway, New Jersey 08854 Dear Dr. Bhnko: using transmission electron microscopy ad selected area electron diffraction, we have analyzed two spmples of talc. These tales were designated as 9-B-a and 9-9-10. These two samples were e4remely in that both showed a high percentage of flues, some rolled talc and flue talc ribbona. In Sample 9-8-9 we found one approximately 1 pm long wbioh appeared morphologically to be similar to cbrysotfle. However, the BLED pattern positively ethnitmted t as a possibility. Di Sample 9-9-10 we also found one particle wbich, although similar in slze to dbxysotlle, was different morphologicafly and gave no diffraction pattern. Both samples were platy and with the exception of the two fibers mentioned (one from each sample) there was nothing which remotely resembled obrysottle or amphibole. U there are any further qjtestlonn concerning this report or the data contained therein, please contact me. Very thily yours, ORG :fa enclosures ref: 5500 4 4o0 Gene B. Grieger Senior l%esearoh Physiolat 29 SOUTH MIIIQAN AVENUE CHICAGQ. IlLINOIS 50615 . 312/542-71X, CABLE: OHEMICI1ONE COL 00493 McCRONE 0017 wallerc. rnccrone associates, hic. COL 00494 MeCRONE 0018 * COL 00495 McCRONE 0019 9-8-S &&EV unknown wailer c. mc crone associates, Inc. COL 00496 McCRONE 0020 ' waiter c. mdcrone associates, inc. PA, CONBULTINa ULThAMICROANALYSIB MICROSCOPY $MAU. PMTICLE PROBLEMS SOLID-STATE OHEMISTAY Z8 October 1976 Dr. J P. Sinko, Jr. Colgate-Palmolive Company 909 River itoad Pisoataway, New Jersey 08854 Dear Dr. 8mko: Using transmission electron microscopy and selected area eleotron diffraction, we bave analyzed a sample of talc designated as Lot 10-7-8. We found this talc to be completely free from ashes fifonu minerals. there were, however, some talc ribbous and some abards. The particles seem to be generally equlaxial and not as platy as some of the talc wblch we have analyzed. This talc generally seemed to be less platy than most cosmetic tales which we bave analyzed, and There were not as many fines In this material as we have found In some previous samples. Thank you for consulting MoCrone Associates. If there are any &rther questions ooxioemsthg this report or the data. contained herein, please contact me. Yours sinoerely, Letct( Qtic4ejj ens B. riegeJ 7] Bbzdor RaSearch'bysit GltQ:fe end. ref: 6500 R820 SOIJ1K MICHIGAN AVENUE CHICAGO, ILutlois soaie 512/842.7100 CADLEt CHEMICRONE COL 00497 MoCRONE 0021 C .2 #1 10-1-8 SAED tale waiter c, mc crone associates, inc. COL 00498 McCRONE 0022 4, I'. 'I er tf IA p 19-74 12, 000q \iajter c. mocrofle assodaies, Inc. COL 00499 McCRONE 0023 wafter c. mocrone associates, Inc. COL 00500 MeCRONE 0024 I F.1 10-1-8 (12,000X) wafter c. mc crone assodalea Inc1 COL 00501 McCRONE 0025 S 10-7-S SLED #2 talc wailer c mc crone assodates, Inc. COL 00502 .McCRONE 0026 S S Wp p p S iI, MA 6500 . 10-v- (50,000X) waiter c, mc crone associates bc. COL 00503 MeCRONE 0027 COLGATE-PALMOLIVE COMPANY A Vilew.,, *rfret*tc RESE4&CH AND DRVHLOPMENr DEPARTMENT 902 Elvu RQH? Piscauway, New firsey 01154 Navter 1, 1976 )4'. Gene Grtger )tirocs Associates 2820 Beuth Mtc)dan Avenue Cbiceo, U, 60616 Dear Gene, DioLosed are tee tale aa3ss for TZM-SAffl) anaata for asbesttora minerals, Please do saniple b%5 thst end as soi an possible. Qhe otber two ore Sorttt but of lower priority. Two are finisbad product tales, both different, and one ta a raw materiel as toflowu: b%5 Plumbed Prodwb 68-130 Meg Raw materiel te3s flI phone purobaso oraers purobase order, may go on ow bleaket Nany th.rnlc5, Enclosure COL 00504 McCRONE 0028 ,AAwaiter c. mcrone dssociates, Inc.CONSULTING: ULTBAMICROANALYSIS MIOROtOPY SMAlL PARTICLE PROBLEMS SOLID-SlaTE CHDAISTRY 18 November 1976 Dr. J.P0 SlmIco, Jr. Colgate Palmolive 909 River Road Plsoataway, New Jersey 08854 Dear Dr. Simko; Using transmission electron microscopy and selected area election dlffraottcn we have anabrzed a sample of talc designated as 10-4021, We tbund this material to be free of MbeStlform minerals; the only non - tajo that we found was some sodium chloride crystals. The transmission electron miorographs and selected area diffraction patterns of these salt crystals are Included with this report. Thank you for constilting Mocrone Associntea. if there are any further questions concerning this report or the data contained therein, please feel free to contRet me. Very truly yoUrs, GBG-Jd Ref. MA 5500 2020 SOUTH MICHIGAN AVENUE . QHICGO, ILLINOIS $0011 M2/542.7100 CABLE: CHEMICRONE COL 00505 McCRONE 0029 10-20-21 SAED #1 NaCI waiter c, mc crone associates, inc. COL 00506 McCRONE ooso ., C. (. J '7- 10-20-21 SLED #1 NaCt waiter c, mc crone associates, inc1 COL 00507 MCCRONE 0031 1' 1 -I iO-20-ZJ. WO,000X) #3. NEll wdler c mocnDne assOcbtes, Inc. COL 00508 McCRONE 0032 10-20-21. 5O, 0O0 flNaCl wafter c, mcrone assock]tes, mG COL 00509 MCCRONE 0033 10-20-21 S2D #2 NaCI waiter c. mcrone associates, inc. COL 00510 McCRONE 0034 LTAVA waiter c. m crone associates, Inc. A A CONSULTING; ULTRAMICHOANALYSIB MICROSCOPY- SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 18 November 1976 Dr. 3.?. Slnko, Jr. Colgate Palmolive 909 River Road Piscataway, New Jersey 08654 Dear Dr. Stmkoz Using transmission electron miorosoopy wid selected area electron difirnotLon 'we have analyzed a sample of talc designated as 1Q.-2021. We found this tnaterLsi to be free of asbestttonn minerals; the only non - talc that we found was some sodium chloride crystals. The transmIssion electron micrographa and selected area dlffriotton patterns of these salt crystals are included with this report. Thwilc you for consulting Mecrone Associates. If there are any further questions concerning this report or the data oontatned therein, please feel free to contact me. Very truly yours, QRG:jd Ref. ma 0500 Gene B. Grieger Senior Beseareli Pk,sioiet / 2820 SOUTh MICHIGAN AVENUE ChICAGO. ILLINOIS 00610 31211424100 CABLE: CHELUCRONE COL 00511 McCRONE 0035 i'A' wafter c. mc crone ossociates, Inc.TA I CONSULTING: IJLTRAMIC$LOAt4AYSIS MICROSCOPY SMALL PAMTICLE PROBLEMS SOLID-STATE CHEMISTRY 18 November 1976 Dr. 3,?, Slmko Colgate Palmolive 909 River Road Piseataway, New 3ersey 08854 Dear Dr. Sknko:. Using transmission eleotron mtorosoy and selected area diffraction we have examined a sample of talc designated as 4915. lh this talc we found one fiber of trenolltB approximateLy 2 nilorometers by 1/2 mIcrometer. Using seleoted area diffraction and zone analysis to give the angles between spots we positively identified this a tremolite. We examined a further preparation from this sample and found no other tremOlite. This particular fiber would not represent wore than a few parts per wEilon, lees that 5 parts per million of asbestitorm minerals and certainly may well just be stray contamination. Thank you for consulting MoCroneL Assocates, It ther& are any further questions concerning this report or the data contained therein please. Liel free to contadt me. Very truly yours, GRG:jd Ref. MA 5560 Gene B. Grieger Senior Beseach Physicist 2O SOLtrH MICNIGAN AVENUE CHICAGO, ILLINOIS 00516 )2p$42.71O0 CABLE: CHEMICIIOWE COL 00512 MeCRONE 0036 a. i's' waiter c. mc crone associates, mc,CONBIJLTINe: ULThAMICflONIALYSIS MIOROSOOPY SMALL PAnTIOLE PROBLEMS SOLID-STATE CHEMISTRY 18 NoVember 1976 Dr. J,P, Slmko Colgate Palmolive 909 River Road Pisoataway, New Jersey 08854 Dear )Dr. Shnkos Using transmission electron microscopy and selected area diffraction we have exanzhtecl a sample of talc designated as 4815. b this talc we found one fiber of tremolite approximately micrometers by ]/2 micrometer. Using aeleoted area diffraction and zone analysts to give the angles between spots we positively Identified this as tremoitte. We examined a further preparation fromthts sample and found no other treniclite. -This particular fiber would not represent more than a few parts per milton, less than C parts per million of asbestiform minerals and certainiy may well Just be stray contamination. Thank you for consulting MoCrone Associates, if there are any further questions concerning this report or the data contained therein please feat free to contact me. GBG:jd Ref. MA 5500 Very truly yours, no B. One br Renear Physicist 2820 SOUTH MICHIGAN AVENUE CHICAGO ILLINOIS $0816 812/042-nOD CABLE: CUCIUCRONE COL 00513 McCRONE 0037 4 'I waiter c, mc crone assodates, Inc. COL 00514 McCRONE 0038 4915 no, 1. SA1tD Tretnotite waiter a mc crone associates, inc. COL 00515 MCCRONE 0039 ORJGIN4L PURCHASE ORDER "on,.Show thu M#fl&fl' 6361S5 SILL TC -- - - COLGATB-PALMOLWB COMP? n6 A DflAWARZ coRtO1ON' 1OS.uUOSO STREET, JERSEY COflO2 ADNj SHIP TO .LJL_1....J...LJ-.--------___ Me0roo Associates 29 Jet GREENE ST. IJensty CITY, N.J. 07302 IOU RIVER ItO. FISCATAWIJ.V, N.J. 01554 In1 P IJERGIERYANCDITBYr,.N.J. 07505 0}iieago, Illinois 60616 -J. 161 I I$RJESCFEFIRYlSNOONSVTIALTLIEO,N INDIANA, 47150 TiRRCKEAIVNSINASBCSITTYA, TSAION,NSeioD wscouirr TERVS 1 2/10 1(/30 2 NISG 3 1/ID H/3D 4 Net Cash 6 Trade SHIPPING TERMS 111 FOB Disthmtlon 2j,FODSbIppl.s Pt (4"I*.P&yt 81195'.. Below 3 JFUDShlppllIgPt. (Cotkcfl city WANT RD fly AZAP ASOVE DArt CMINOT BE ME? NOtIPY 22 1IS1E1R0 ICCAERLLSTYO. MCASLrIF. 04710 Ito. PARK AVE. 1115w YOtIC. N.Y. 10022 23 A'TTPt Recelvins Clark YOU Mt UT 121010 FI*PIlSIf THE ARTIClES 115110 IJIREON III A000RUAHtE WITH rIte Tails AC COIOITIOHS ON THE tACt AltO BACK OfT IS ORDER, QUANTITY AND UNIT SYMBOL NUMSER P2IICE antssion 4ectron Y4DVOBCAW and 8eleetod Area fleotron Diffraction Aafl8i5 ot u'c Ta p1es flabefled as fo]tq: -- .......6B-o ,. ............... .......- .... ....... ----------------- ........ ...: ........... ._,_..t_.j ..,Thisieaonet5*eflqueot: ...., ............................. NOTE; ,Samples sent under separate covet to )fr. Gehe Gr.eger ot Mocrorie on 11/1/76 ...........AXEXEM' . :. : MALVENDOR TO PROTECT ALL. AINSTCCRRON BYSLIITABLE PROTECTIVE SEALING. EttIRS invoias Hid TnMJs e..tJ,mt.d romportoWot, &orqe Mast ba nppeda by pr.pSJ fnt;bt bill or copy .f oulgl..4 bW ci Iai.g. hUlK PACEAS willi pwdai oSr nb*br, pymb.I un*.r. wdnls ted q.onMy. M..plo*t* .1*1. c.d.t Isle b, .tnd ..dlb.fl.. Ike flB ha tad ord award It th. Ins. sal .oScms Sc lb. baa I.r..d, PAYMENT Wilt NOT IC MAD! AGAINST P20 FORMA INVOICe. -F4LMOLIVB COZIIPAN7 sswr JEESBI !.X S 5flj COL 00516 ZEMflisD B tZi McCRONE 0040 -. - cvati-er c. mdcrone associates, mc: CONSULTlNG ULTRAMJOROAHALY$IS MICROSCOPY. SMAU. PARTICLE FRO8LEMS S0UD-ATE CHEMIStRY 2 December 1976 Dr. Joseph P. Simko, Zr. Colgate-Palmolive Owupany 909 River Road Piscataway, New Jersey 08864 Dear Dr. SIxD; Using transmission electron microscopy and selected area electron diffraaUon, we have etmnlned two samples of talc which were shipped to us as special lots. These tales wore designated as MAhG 11-1-18 and 68-130, dated 11/1/76. The first set ot these two tales, MAG U/i/ia, was an excellent example of talc. It wa extremely platy, bad an excellent particle size distribution and no asbeaWorm minerals. We did, however, find some slight traces of sodium chloride in this material, but that was the only extraneous material which we could find In this sonple. The second sample, 68-130 dated 1V1/76, showed some rolled talc, isle ribbons, talc fibers and an extremely high percentage of fines, but otherwise was extremely platy and again did not show amy asbeeWorm minerals, nor was there arj platy antigorite. 'This did not look as good a sample of talc as the RAG 11-1-76 sample in that it bad a lot of Abers, even thongh they were talc. Thank you for consulting MoOrone AssocIates. If there are any further questions concerning this report or the data contained herein, please feel free to contact us. Yours sincerely, ORG :1C ref: 6600 - P.O. 63618 Gene B. Grieger Senior Research Physicist 2820 SOUTh MICHIGAN AVENUE -cHICAGO, ILUNOIS 60815 $12a42-7100 CABLE: OHEMIORONE COL 00517 MoCRONE 0041 waiter c.tno crone ossoclales, Inc1 .4 r-4 b 1 I Mag 1/1/16 12,000% - waiter c. motrone associates Inc. COL 00519 McCRONE 0043 COLGA TB-PALMOLIVE COMPANY 4 Ddawn G4nN RRSE4RCJI 4ND DEVELOPMENT DEP4RFMENT 909 River Read Piscataway, New J,r.r,y 08851 Deceer 7, 3.976 Gune Gz'ieger ?t%ona Aeaoaatea 2820 South MLcbigan Avenue Chicago, th 606t6 Dear Gene, Enclosed is a talc seaple labeled ABE. flease do PEM and BRED on St. Charge to our blabket pme2ztae oraer. Thanks. UPS: is Enc1oame c nil-a U. P. Sako COL 00520 MeCRONE 0044 waiter c mc crone associates, mc, CONSULTiNG ULTRAMIOROANAZXSIS MIC8OSCOPY SMALL PARTICLE PAOSLEMB - SOUD$TAT cj,y 3 January 1971 Dn Joseph p. Rtmlcn, Jr. Oolgate-Pabnolive Company 900 mver Itoad Placataway, I'ew Jersey 08854 Dear Dr. Slmko; tathg trazsmtaston olttron zotoros copy and selected area electron. diffraction, we bate analyzed a ample of talc identified as talc ABE and dated 1.2/S/TS. We Itnud this talc to be completely free of asbestiform mhrn'als. We did, however, find that ft had a few fine talc ribbons and some Mo fibers. We also found thin to be fairly low to moderate in fines and not as platy as the ganpie designated as MAG whtoh we prevtunly anaiyzed, Thank you for consuithig MoCrone Aseooiate and if there axe any further questions concerning slits report or the data contained herein, please feel free to contact me. 4.. Very truly yours, Gene it. Grleger Senior Itesearob 'bysicist GBthfe end. ref: 5500 28W SOUTH MICHIGAN AVENUE- CHICAGO. IWNOIS 6081n . 512/8424100 CASLa CIIEMICRONE COL 00521 McCRONE 0045 F .' 0 a 9-8-9 (5O,000X) , waiter c, mocrone associales, Inc. COL 00522 MoCRONE 0046 Waiter c. mccrone associciles, inc. CONSULTING; ULTRMILOROANALYSF$ MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE OHEMISThV_ it January lOT! Pr. Joseph P. Slmko Colgat -Palmolive 909 U Lver Road Pisoataway, New Jersey 08854 Dear Dr. Sinico: Using transmission electron microscopy and selected area electron diffraction we have analyzed your latest sample of talc designated as Lot 1-5-0. The Mte on this 'sample was erroneously gtven as 1-5-78 and should be 1-8-77. In this talc we found no Indication of asbestiform thineala. This talc La extremely platy, and In general better than the average talc which we have aeon from this supplier. Because of Its platinesa we find some fine thlo ribbons and Line roiled talc fibers which appear InevLtthie on grinding such pla' material. Thank you for consulting 3iccrone Associates. If there are any irther qizestlona oonoemftg this 'report or the data contained therein, plese feel free to contact me. Very truly yours, GRGdd Ref. MA 5500 Gene B. Grteger Senior Research PIysLolut 232080UTh MICHIGAN AVENUE.CH!OAGQ, ILLINO1S 806ts $1V842-?100 CAflLE: ONEMICRONE COL 00523 McCRONE 0047 LII waiter a mc crone assodates, Inc. CONSULTING; ULTRAWCROANALYSI$' MICROSCOPY SMAI.L PARTICLE rBOBLEMS 'SOLID-rATE CHEMISTRY 21 Jauaay 19'?? Mr. .1. P. Blmko, Jr. Colgate-Pabuolive Conpan 909 River Road Piscataway, New Jersey 08854 Dear Mr. $bnlco: We have completed our determination of the asbestos content of the tale samples which you submitted to us (Tale .kBE), using the Scbnlquee o s-ray diffraction and ligb microscopy. The results are given In the attached sheet and the x-ray diffraction patten. U there should be any questions concerning these tesults please contact us. Yours sinoeroly, Ralph 3'. much, Jr. Research Chemist attach. ref: 6500 2020 SOWN MICHIGAN AVENUE CHICAGO ILLINOW OIIe 1/6lZ-TIO0. CASLE CHEMICRONE COL 00524 McCRONE 0048 Date Client rnle1-a Pezlv.toJtie Sample Description ten roaMA Projqot X-BAY DIflBACTION Serpente Cuntent 72 07?t de /tc$cA Aanpbiboiecontent'pp_dai'eSej If?roeComments 0//0i,Ye eZtA 4nqe ,c ,zS'.'o.. LIGHT NflCBOZCOPY 8erpentlne Content ',st Ampbibole content - vi.oAS Comments (at tc, A0L4L tt t.t q tCSO kb'Q...a waiter i Fnccrrine assodde Inc. 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Ni.fUlUMstfl.l0S.U0000fl1*l* JJ IIWII'I.pu......1-n1L:0LblNf1a0.1..f.ldJaL.I-pnfNllLIJltInUIto0fln0Q.0?ob,nr*nNNInU.s,0wfl0nk0ftl0_. .0NEN0SN.._I5US.._US0p0tI!.SN.np,,.p4INCU*lN.: Ii Piuiugi s__..s.I .s si s.tPllOlNP'nOuSfl%f.lp.U0o5:1:t1ncflna.paI.IUIll.*nP0.*flu U t*flnaOlnnanp.asn... .NN..aN.U..Un a0 SMV02 SLInPflSlI(I gINUflTu Unoig. ______ i t :;!JJ:llJI!:!!IIIflhIllffl1011IJIIlI1IIIIIIIllflhifthIftIftflJJfllljftDet 8ggnn.*nnMuen.nu.isn.flffliflNfifNl INIflIfl**N *iNt*aa.Ih,Araa."nfnlnfnlN.nn,nnNflsi Ei"il __i1 asII s'ainni rfnli n.1n1*lin_.pa.!-_'frlfinfiIl:--,JiiISamjfIaii.N.aanIiiU1aif4fanrfillWl-.nNJinMln.-tjm.Ii.rIN.lnNmarkitu2Iffn,lflNffNalr.fla{NlSl-aaffL.NVlilNfmfIJealnfrtNltlaMff.alini.lIalnIngf_9nilf.nnnnhl.IpifmNi,.kNNljfl.iaa.Jl.S.amf.fNia.N.JSl.lhfin..tPflmtNi{WmannIihlf.tafLffl.mffmfal'aml.hall.NlflIsaa.nn5ZIlnNm..C.m:aa.uf.,htnlTtnla1j..in.nznasrI,.Ihlfaf'n,hi1J.lhtiilfrn.LaIn.i.lIjfrjlaa.III..fHNalW"Ni.f_flWnfFWNnIllVla,NUmNCaIn.,amnn,to_mfatnfinSalaInWniWiaiaIfair.anfnNaaan.nl_f.lannIhihlifaII1nC.kafFhialiflrmuNtllfjilfiaIiNfCfnlIli,Uil:tqnllfiiSVn,tf,irif.lpafjlmtltIk.hlhf.liU81:lN:h.N1-,lNltn._.tnt.laiiafe*jfs?f.n,llaaNlsIalzfsf1nhh.-lnilN,Un.N,anfh.hii.:a.Zial.utf*.fnif,NlSa,nllnwlfl.snnatnlti.,WfiiSn,n.aif.lf.n.,lliLl.hfNInfafin.lS*lllfi.faiaw,.tfliit*:uilJa$,f.nfrn,l!lMliiIs{NnIIinNSsitnlnhIISIJautauNaiiIfif.Pfi!if.NlllinlxNiflafWlaNNialhStia!5antW.i.ifz.i.hNtmlnafISnuaINlN:iNa.stW*t...NIPNaaNnIif.uLiNNPEl.ntMlIfPnl!NNig*IasalfiNN*WNIII_W.JfnItIInlifxhIU.JaiInlfn$r_kiiNtlfNitnfhiMf*IffMhllt!lllsSapi._.Na!.,NkNana!SIan!,f.,RS.'flm.u,l*.Es.k.lN*afu.a.NtflS!fWt._i.tn$Ill9.i,htNl.i.ns,.Wa,imanin!ffilnaLINNnil!inllfNpj,fI.!M,i.fiuml'l.Xa.l!...m.g.lsiIj.iPiI*niNim*nPfjsai!lfnlMlf**la.i$RPllnINNRntnNn.I%,.fff.a*.Enln.ifla.lffNf.ffaflllul.llUflffuvwW$f.N.iNlNhinflmuia,.NPl*NilUn.n.siiijaiIfififiiinllilil!lj.l.liI- 1US5an.Jflsatfln2ana.a.ni.iiin.i.nn.ann, Nflflni,a.-P?f.PIn.nS1LN!l0W.l.WILfri*fnnNtlf_I.s*fNltfll.IaWlNfasiIn.hNlnSflirao.Nnhlli.M.NaNaSf..aXfotannll*NNtlatNt*filI,Iiflnn.llMnMalaf.itNnft.cNPfl,llnlElnoWniift.nNf.tanfiInflj.ltJ*l.LnI.,uliI*5hwISIkaNf!afas.Nma,rinilf'lhIa.oiimlhnnutm:.fnlSnOINmrinlaf.afaaut.fnmlJ.nln.ual..I,fiaiannNWtfaflnt..gnfpnll.fa.alWm.up..nl.l.aslnhha,.Niaj.:nn,fapN,nNhaIa.islLa..sjfi1N*niljU.lflanInLnnnka**IlN;IaIIh1snf5IifmilNNiin.l1Illa1Nph.a.Sst*flIi.plf.S5:KfILirSlttnfallfi1.*.NLi1,1nILl5lnKUnflHuiS*1Ufae,I'jlci10,l,l.lh,P1lEhnlN.NaJ.,HrnnNI.in.tNjia.9IlnIIi..nhaiE.NiatSni.nat..SnNimn.a.nN.iiNnn.f.wpunN2lunihihar.Nlffuatfzsl..fllarlNfNNl.h.h.Ifh.l..U.lNmtl*i,lN.IPII.hfL*I.$ln5,hNinf,I.NmlnL5nf.aIllIlmmImf,N.nlI..fiifaIlnhia.l.ph..ii.N..n.,4n,Nnf.j.nijlh..1ii.*i.nI..Ipa0s..0N,IJnIIa.I.g.afn.luI..Jun_Nni;:NINL.L.n;n.2pahNILIN9nnSI1.nnINi.n.nn.fi.uinJlIiSI#allm.ia.hNLIahn.M.nm:NNhn51rnI.iIn1j.nin!_n.t.ai*9N.1.Sin,5ai.n.fn1n_hpihnIncl,.ihfN.IlnWlaSntalnn1fE.l1nuNSN:a_nls...na%nai.f:a.aNIt.SaUnj.NuSilc.i.m,siNs_u.I,.*ue*I..IIIi..f.ii.fpsIsi.JiI.1iiil.u.i!l.r.lI.Nl',.rnnVr..p.-_iIaaIJi.i.iini.INI.h.a,i-mNisu..siuftyftfilpjI-abwlhtlurEf.Nhl.iNlStaialdAlfiifla.i.nL.-nil..adhiw.ish_W.i.amnC..u.nh,.ia..pA!a..t.ll..ifs.fuaNtpL.il.i.Li_h$lnn.5ail.i:h..aa_..a_n1if*sniI.lI..utnn.lilh0.A.t..sli..ia..mP.ifiN.tif...lIa.nI1nli..ff!nmI..l,l-.!W,npn!i.&.l1b.l -- . iluinji- - l,lNifilI$NIaNNI1NN5aNf1ElW1uN5LYuafIiUJl*.tk.JPhlfllhIllSlitIlirISNN9.fNIlnSlhS!nIml.isifNN.ullaaslfmhDilgnhli,f.i.rn.lls.aNInNnsiU.ianiaiLNI,i.sf.fnfllulnsJflilLihlNst9pInN.IuINfn{lI.Jn.uNIf.nliIaNnNJ:ssSlNIaS..Jl.IuIa-.naII.n.nnInaXs.n.I.r.Nintai...N.Izfi.l,tIn.if.Jln.rwnnc,a.,a,.a.,.,atnuNa,.Wi.k,aNIvLII.N*IlL.le.LaIUf.aiNNtnk.uNf1lli.Mt.Idui1ilEn0.l.i.1N.1aif,ull..h'.NpN.ur..il.:Iiu..l-II.l 1. :jJ -1 tit n-rt; T*rn tSt3IJ-4:-.14 en CC 0 C) F VE F COLGA TB-PALMOLIVE COMPANY A Ddna fV4th RESEARCH 4Nt DEVELOPMENT DEPARTMENT 9Q9 Rio,, Znd PitU41M91 N,w firny 08854 $ )teb?uey 1, 1977 Jr. Gene wieger Mtrone Associates 28O 8outh Mtcbigan Avenue chicago, u1 GaGiG Dew Gene, Bttc1ose is a samfte of talc xabelea #266. flease do flM-BZD av1ysia for asbestos ndnerata. Ctsrge to our open ptwobsse. order number. Thanks. JpBsls Enclosure C .j. p imko COL 00532 McCRONE 0056 waiter c mc crone associates, Inc. CONSULTING: ULTRfl.IICRQANALYEIS MICROSCOPY SMALL PMTICLE PROBLEMS SOLID$TATE CHEMISTffi' 10 February 1977 Dr. Joseph P. Blmko Colgate Palmolive Company 909 Blver Rogd Pisoataway, New Jersey 08864 Dear Th. Blmkb: Using transmission electron microscopy and selected area eleott'OA diffraction we have analyzed a talc designated as lot 121-fl from the 1877 serIes. We found no athsstlform minerals In this talc and the talc was not extremely p1 sty. What plates there were, were rather thick. We did find some sbaxds, some sodium chloride, and a moderate to high leni of fines. Thank yo' for consulting Mocrone 4suoclates. If there ar any further questions concerning this report, please contact me. Very truly yours, GBGjd Ref. M.4 5500 Gene Larieger Senior Besearch Scientist 2120 SOUTH MICHIGAN AVENQE CHICAGO, ILLINOIS 80518 812/542-7100 CABLE: CHEMICRONE COL 00533 McCRONE 0057 3 Ai waiter c. mccrone assocbtes, Inc.IYA CONSULTiNG: ULTRA$IICR0ANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SQ1.ID.$TATh CHEMISTRY 11 February 1977 Dr. Joseph P. Slmko, Jr. colgatePeintoIive Company 909 RiverRoad Piscataway, New Jersey 086b4 D.ar Dr. Slmko: Using transmission electron microscopy and selected area elecitin diffraction, we bays anaiyzed a sample of tal designated by the number 4166. In this talc we found no asbestiform minerals. The plates which we found were rather thick and the material was not very plat'. There were some shards and moderate to high fines. we did find three fibers In this sample. Two of these were organic and did not dlffraet, The third was quite obviously not chrysotfle but did give a weak ring pattern consisting of one ring whiob could nut be positively identified. 'Thank you for consulung Meorone Associates and IL you should hive any questions concerning these zesulis, please contact us. Sincerely, GltOfe. ret: 8500 S or Research k,Ist 2820 5OUTh MICHIGn1 AVENUE. CHIOAOO, ILLINOIS OaSIS .312/342-7100 . OAB.E OHWIOROHE COL 00534 McCRONE 0058 MA 5500 SAED #1 - utown waiter c, mccrbnbssocis;inc: COL 00535 MeCRONE 0059 1:. 5500 4166 (50,000X) #1 c wolfer . moclorie dssocicttOs, Inc. COL 00536 McCRONE 0060 MA 5500 SAED #2 - orgame waiter c. mc crbne tissodas; Inc. COL 00537 McCRQNE 0061 COL 00538 McCRONE 0082 ras' waiter C. mc crone associates, Inc.COMSULTINa ULTRAMICHOANALYSIS' MICROSCOPY' SMAU. PART1CLB PROBLEMS SOLID.STATE CHEMISTRY 12 August 1977 Dr. Josepbp. Shuko Colgate-Paimolive Company 909 River Road Plecataway, New Jersey OBBM Dear Dr. Sl3vkoI Using transmission electron microscopy and selected area electron diffraction, we have analyzed a sample ef talc desiprn*ed as Lot 7-24-25 from The 1977 serIes. Morphologloafly, this na a poor quality talc In that it seemed to have a lot of fibrous material in it. However, none of tide fibrous material was an aSbestiform mineral, but was talc fibers, rolled talc, talc rda and talc ribbons. The pereenage qf fines present were moderate t2othoi3ghnwraitnhgsoem. e platy talc, but mostly email equ.ezlal particles in the Thank you for consulting Mocrono Associates and if you should have any hirther questions acnenridng these results, please coutst us. Very taily yours, Gene R. Grieger Seidor Research PhyMelet GRGde end. roft 5000 2e2000UTh MCHI3AN AVENUE CHICAGO, ILLINOIS 60518 312/*424100 CAULLi CNEMIORONE COL 00539 MaCROME 0063 .13. I tI:: ? - -" A' :' -. * r '- I.' -3'.. -'-3.. Walter c mocrons assocfatS,lnc,.:.. .3 . . MCCRONE 0064 COL 00540 4' Lv 4 - -. '*' 4 -I Lot 7-24-25 O, 000X) wailer c, mocnne associates, Inc. COL 00541 McCRONE 0065 V kYTA $A' waiter C. mc crone associates, Inc. I COHSLJL11NG: ULThAMICHO4WALYSIS MIOROSCOPY SMALL PAflTICLE PaOBLEMS 6OUD8TATE OHEMISTI3Y 8 March 1977 Dr. Joseph P. Slm]co,Jr. colgate-Palmolive Company 909 River Boad Placataway, New Jersey 08854 Dear Dr. Bunko: Using tranhmisston electron microscopy and selected area electron diffraction, we have analyzed a sample of talc designated as Lot 2-10-fl of die 1977 series. In this sample we found moderate fines, somewhat thicker plates sad also a tine inorganic znaterial which was tco widely dispersed to allow for electron dlffraotlai ideutiflcstlon of, but is believed to be NaCt. We did not find any ash estiform minerals in this sample. flank you icr consulting Mocirone Aesoci$es. If there are any further quo stions concerning this rsport please feel free to contact me. Very truly yours, GoneR. Griegr Senior Research Plsioist - GX%G:te ref: 5500 2620 SOUTH IIOKIGM AVENUE.. CHICAGO, WNOI$ 60618 S12/$4Z41O CABLE QHEMFCRONE COL 00542 McCRONE 0066 $ wailer c mc crone associales, Inc. CON$IJCflNG: ULTRNlICROAt3Al.YEIS MICROScOPY SMALL PARTICLE PROBLEMS SOLID4TATECHSMISTAY 10 March 1977 Dr. Joseph P. Simko, Jr. Colgate-Palmolive Company 909 Wver Itoad Bscatway, New Jersey 08854 Dear Dr. Siniko: Tistig tr,inn1saion electron microscopy and setecte&erea electron dlffracllon. we have analyzed a sample designated as Lot no. 2-22-23 from the 1977 seie. In this t*Io we found no asbestiform minerals. The talc seemed to have moderate to high Levels of fines and the plates were a little lit pu the thick side. We also found a few ribbons and shards, bttt,jrom their diffraction Dattern, these were undoubtedly talc. If there should be any thrther questions please feel free to conta4t sue. Very truly yotn4s, GBete ret: 5500 Gene E. Grieger Senior Research P*aibist 2520 SOUTh MIOPIIOAN AVaNUE' HIwSO, ILLINOIS aoeie- 312/842-7100 QABLE CHEMIOROI4E COL 00543 MeCRONE 0067 4. waiter c. mc crone associaies, inc. CONSULTING: ULTMMICROANALY$IS MICROSGOPY. SMALL PARTICLE PROBLEMS - SCUD-STATE CHEMISTRY 13 April 1977 Dr. Joseph P. Slmlco, Jr. Colgate-Palinoltve Company Doe mver Road Piscatawa3r, New Jersey 08854 Deer Dr. Bimko: tJsIng tranemise Ion electron microscopy and selected area electron diffraction, we ban analyzed a sample of talc designated an Lot 8-81-4-1, and found no asbeatlfoxn minerals in this sample. Mthouglz the talc did include a high percaitage of lines and some shards, it was c*tremoly platy but did not show large thin platen. Instesa, small almost round equmdal particles were the predominant talc form pros out. If there axe any further queetis ooncextlng this report or the ta contained herein, please coi4nct me. Very truly yours, Gene B. Grieger Senior Research Physicist ORQ;fe ret, 8500 2820 SOUTH MICHIGAN AVENUE CHICAGO IWNOIS 60616. 312/842.7100 CASLE; OHEMICRONE COL 00544 MeCRONE 0068 /4 waiter c. mccrone associates, Inc. a a CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMML PARTICLE PROOLEMS. SOLIO-STAT CHEMISTRY 12 July 1977 Dr. Joseph $lmko Colgate-PalmolIve 909 mver Road Plsoaway, New Jersey 08864 Dear Dr. Simko: Using transmission eleotrca microscopy and a4ected area electron diffraction we bays analyzed a sample of talc designated as M 0 N 6, 040, dated 6/18/Ti. in this sample we find no aebeatiform minerals. The particles geworally seem to be oqubdal with moderate tines. Some oX the material is platy and there is a fins fiber which may be organic In nature. This fiber is very similar to a ribbon. This Is not baoterM debris. Tbankytrn for consulting MoCroneAssoolates and if there are ax farther questions concerning this report, or the data oontained therein, please feel free to contact me. Vez truly yours, GRajd Ref. MA 5500 Usne B. Grieger Senior Research Thysloist 2820 SOUTH MICMIGAI1 AVENUE CHICAGO, IWNOIS 60816 812M2-7100 CABLE: CHEMIORONE COL 00545 McCRONE 0069 waiter C, mc crone assodates, inc. CONSULtIMa: UCTThMICROANALY$I6 . MIClIOSCOPY SMALL PARTICLE PROBLEMS. SOLID-STATE CIIEMISTWV 13 October 1977 Dr. Joseph P. $ftnko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 0886t Dear Dr. Simkog Using transmission eletron microscopy and selected area electron diffraction, we have anaiyd a sample of talc designated as Lot 9-21-fl from the 1e7l series. We did not find any aabestform minerals in this sample. We did find, however, that there were moderate fines with emno of the talc pIai and a rather blgh percentage of sodium chloride in this sample. This suns sample was also analyzed by x-r diffraction and in it we again (amid no asbestlioran nthierale. We did find, however, that there was present chlorite and se alpha silicon dioxide (quartz). Thank you for conanttlng Mocrone Associates and if you should have any cueslions oonernlng this aaiella please contact no. Shioer*, Gene B. Grieger Benior Besearoh Physicist GRthXe ret; 5600 fl20 SOUTH MICHIGAN AVENUE CHICAGO, ILUIJOIS 50015 812/5Z-71OO CADtrn CHEMIORONE COL 00546 McCRONE 0070 Date CZ',tJjev 1W77 ClLeut ofaM- pa)istnlru'e MA Proj ect 3Cc. Sam$e Description 44r'. To/ce tbaL j114470-L-L0* S-I-zt X-RAY DWmCTION Sez!penthle Content- e eMxtpbiboie Coxitent k Comments rec'es.J' r,AInrt4'e 4'oi-S:n LIGBT MtCRQSCOPY SerpenUne Content Amphibole Content Comments wailer c. mione assocbtea Inc. COL 00547 McCRONE 0071 :=Ir..'-.'.!.'.-.'.f.lm...t.r.'.5..".r.n..a..a..a.......a..n.a...gl.a...v.l.ta.,.r.k.................1....d...._..H...n..'.na..nI.atunuarlaHtalilh.n,w..snw.5ggggggaw 45a...nnn.n.tIS.an4s.aana..ua.-snn.aftn.a.-af..l__ssirnfa.sl..an.l$..-nlaa..aan...9n.t-ln5s.smaan*...5s-.anWn..fs.n.I$-Slskn.a.__Jn-aSlnnU$a._.s-P.1akmiatnfaa5AnsnslI*a.n..af5wn.f*nalslaS5aafIf.alvll{al5*snnlnaTafa5f%nnl.n.al,anhI.nanal.5*aa..aa.nama..s.aanR...fj0.nn.lka.al.lsn.aLs#a.n.A!-.a.a.nf..rafn.nsnnslnllaaSnUasn...p...1.sn.tism.....SmI.a15NntutuaIIia..sIannja..n.ln!fa...aIfa.sllan!.Sfaa.n..lmaanll.fI.-...l..nff-la.a..I.nlslana.l5llSl*E.Snf*n.n..-l..lwaa..nfa.a-.._sknllnannnn.Ian.na.Sn_sa.gon.ts.lI.na.S..a..*.rs9tsa...ak.._naansssa..tn.n...annlI..Slninlalnaan.nl..n.nnw_k.na.assnU.a.t.ataans_.tI4a'lnt.U-IIIIIpamkfsIasC...Ulnfl-5nI*nnna.tt.sn.lsna-l1afn...lannUll57-aa.a.aas.s.f.an5a-.,naaarla-fnfl.t---sns.s,.l5n.lsla,anas-.m-a-s,t,annnn-l.I.am..Ila_.9s!t.,nl.ta.a...an.aa-s.f-E..j.ae.n-kal,._a.*.sif.ss.-_v.*aSnl_fInsn.n.,taS..ltan5na,f..sa.aaisa:-5al.nannnfmaa-aS..a.gla-.l.....f.aiswf*.,..s.ngnalaanlanf-w*..al.nalf.*.afal..nln..l-.nkgS5nsaa*...-a.aa{aAan..sf-nSsaa.U...lR-..s.sfI.jUfs.Sa..a*lnt,.f.nlnaaal.j.nSWff.li.nl.sn.lln.'ia.EfVaI*aSanf.tma..snlgnl.at.aamjatsn.mf7.faa.:a_.aVl.ai.fnil,s.f..aV.S.a.st.l.ln._.5.,FIIsI.a..I.a.--ififtLlItZScf*,xtif:aaa*5ift15al5Is4;m.ilaalntg:IjWN.I.nl*f;s..st,l,t!?.sat.:rf.atflIuaanmL.S.-smuaIl;ursl.a-l,k_aI.,a.Ia.ah,jk,s-sa.a.n.l!Snu,,_a.a*aa.f.-.ns..-.aS...aLnslia-U.fN.s.a__*n.Saa.innl.f-.-nsan.c_'..fnt_.alln:n-ra.._nal.an*aaasstan-__--$rh,.a.,_a.shaaat-lnSn_Sa-aan4-atnnly.In_._nairr'S*SI4f..aiss',.ntalann..rsf.n5i..S.-r?ala-ralf..in.l4W-a.-.f5.aSn_nnli.9n..sfn..,lln'.n.n-nnaf-,.s,nalS'f,n_nfnlf.f..ri-.lla*l..tll.n.allnnaf-.SM.aa-f:nf.s.a..wn.nl.l-{-*sl-us.E.nsJ...l.g.ff,a-n.na..n...san,l.l..R,nS.U*aarnnn.,anS;-nnS*nar.l-r..aZn-J.nl:lc.a.*n.rrn.a.Saa..MSnaZnLa.l..'r..ts-.a.no.paa.rn.*.-anW.fzM-Sfa*lna,-al.al-alaSt..fao-.p-n'.sl!v-nsSs-asnla,--.I.-n1Pt..,'HS'-is-raf5a.----n.j-'ramaSr-laa.-as2-a-lnran-.r,---i-sWmW-mfa5_-n.a'.t-Y.fsD-?sl.-U,f---lS.*4-aS.ns.,.ln,.f--La'S'-.a.afl.5cn-_ftm.nUS:dIllnnnalI-anta',ama,_a,nffM:anni-aHral.qsaalaaf.n.qn$Sna.wnnl..fa.a.ss.lj..afl..sw..zlH.a1.nfnla-.n...U.,atal.fan.s.5f.aa.ilga.snlf.a.fnt.m,.1sananfl..l.ssfanll.nW...nil.nnan..UffU.t,..lf..lannlaa.l.a.al.l.uaa-aa.1...I.aR...t.t.l.n.Sn..5n.*.a-sa9.n.a'n.la45aU...anT.f.a9.W.anu.lp0,..nn.n.m,nnh.nusn.n,5t.n.n.i.as1nna.naansnnnniU1wa.an.U.a's.ifa1Hs1ol.tanss1..:a.nfln..n-tkn.nna.f.fsnsaatlna.haw.a..a.sa,n.ssIsn..aw..s.aaaa..sr:*..n.5anaSnI..aa.-.I,H.w*.SaU..nS.asnaaannUamw.pUlan.a.*.c_aknnaan.Inanaas.sHsa.an.a4nSa*ns.as.n.1H.i..,aa,nas...a..rS.,tn,tI...... lnk*5S IstI'I -EfIlIa-f,l.'" 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(C (CCC C C C I ,tf,9-bSdO COLGATE-PALMOLIVE COMPANY 4 Dii. wn d.*miki RESRARCH AN)) DEVELOPMENT D.BPARTMRNT 909 Rint Ro . Pircataway, Ncw Jirny 08854 November 7, 19T1 Mr. Gene Grieger l4oCrone Associates 2620 South lacbigan Avenue Chicago, XL 606i6 Dear Genes I'm enclosing two samples of t&.e for opticaa microscope examination. We re not certain abo(at the composition for the following reasons: (a) we see a Prsible weak aapbibole Line by s-ray at W.5 an lines at 20 10.35 and 10,15 in sample 1635. 'biat none of these in the Trench Talc. Cbt) asaperaio stang shows proper colors fl-an tremolite in both cases bxb the morholo' isn't right. We nnt to ow more about what these materialCe) might be. Charge our open purchase order number tor thia work. Sincera3, .JPB: is Enbiosure a. P. Simko, Jr. C 1fl-a COL 00549 MoGRONE 0073 Pb wafter c. mc crone associates, inc. CONSULTING: ULTRAMICRQANALYSI$ NIOR0300P? SMALL PARTICLE PFIOSLWS SOLJD-$TATE CFLEMISThV 15 November 1977 Dr. 3usephP. Slink,, Colgate-Palmolive B & D Department 909 Idyer Road Pisoataway, New Jersey 08854 Dear Dr. $lmko: I bays completed the analysis of your sample hoMing the deMgtatiou: MflTalc-Code M-6670-2, tot No.-1O-26-77, 10-27-77, presldpmstt sample, Xorthe deterinThtlon of this asbeatUom material content. This speainen wae found to consist, primarily, of platy talc ranging from email to moderately large (>10 pm) sizes. Talc shards, talc ribbons, Mreqtzent uneven fibrous aspect nona abestiform silicate, material and cocasional chunky Inorganic particles are to be noted In This sample. This electra microscopical exambiafion did not reveal the presence of asbesUform material In the sample. Thank you for oonsulting us once again. If any questions should arise ccncemxlng this analygis, please do not hesitate to conlaot me direotly. Sincerely, BJS:5d Ref. 5500 mchardj. Bbimps 4esearch chemist asao SOUTh MICH(GAPJ AVENUE CHICAGO, IjL9OI$ 806*8 8fl/842-7100 CASLE: OHEMICRONE COL 00550 McCRONE 0074 wafter c. mcrone associales, inc. - COMSULI1Na ULTAMIIOROANALY$I$ MICROSCOPY SMALL PARTTCLE PROSLEUS SOLIO-STA'TE OHEMISThY 16 November 1977 Dr. J. P. Slmko, Jr. Colgate-Paimolive Company 909 River Road Piscataway, New Jersey 05854 Eeerflr.Slmka: This letter cojftrma the telephoned results of our microscopical : ../.......e,nnnb.1ioji of your two samples, French Talc - Lot 5954 -11/3 and Talc 1615 -Lab #4811 - 1113. . you had noted In your letter of November 7 that both Ban)plee contain particles wbich show the right microscopical dispersion statnThg colors for tremolite but the wrtg morphology. We have ident1ed these P*d65 Mlipftttte. . .. ..tWhe. SIBOIDUnd asmafl amountoitremoliteinTalo j6lObu$nonein tin nis Is consistent witS your flD results. The-other minerals Identified are noted on the enolosea Iaboratofl report sheets. .0 you have y questions please let the lotow. . - ., With. best wishes, LBN fe end. ret: 5500 tuoy B. MoCrone Senior Research Scientist !8O SOUTh MICHIGAN AVENUE - CHICAGO ILLINOIS 60616 8121*42-iwo CABLE: CHEMIOROHE COL 00551 McCRONE 0075 I. Date 9 client COLQArE-. PAL-nba's (!Ot4P4NY Sample Desoz'tptton PRIENCH TEAt Zor sss.i. jq MA Projept 5500 X-RAY DIfltR ACT ION SeronUne Content Amphthoie Content Cotnments - r'LIGHT MICROSCOPY .. '.. Serpfltne Content ,4*4 Ampb1boe Content ami Comments *4., 4%q L,1 Mi,. . s.d ftt4aMwJl'rk 4p wafter , mocSe assocIafe Inc. COL 00552 MoCRONE 0076 Date 9 /tYXMS4t.E' qyy Client 00L0477- Pgu.wuve OCWP,IMY MA Project 5500 Sampis Description Tha Ia' is, L46 ha,',, si/s X-RAY DIFFEACTION Serpithae Content Mnpbiboie Content Comments LIGHT MIOBOSGOPY $erpenUne content ,one detseid Amphibole Content ti'msw/i/ ddttd Comments Aimil 4(gagct 4,1&t $MS* now4 .0 4t;' ;amtptkae .aJ - a*h( It. tF OSt9I '1 / k:.i! ( waFter c. mccrone asocbte Inc. COL 00553 MeCRONE 0077 waiter c. mccrone associates, Inc. CONSUCflNG ULTRAMICIqOANALYSIS. MICROScOPY. SMALL PMTJCLE PROBL2MS SCUD-STATE CHEMISTRY 5 January 978 Dr. Joseph P. Sbtko1 Jr. Colgate-Palmolive Company 909 River Road Pisoataway, New Jersey 08854 Dear Dr. Slmko: Using transmission electron mloroaoopy and selected area electron diffraction, we have analyzed a sample of pre-bipmeut tale designated as Lot 13-27.28 of tbe 1277 sertes. In this sample we found no asbeatiform minerals, In this sample we Mmd moderate levels of fines arid the aanpIe again indicated predozninantly equiwdal. particles which were not extran4i platy with some Indtoatton of shards. Some sodium chloride was ajao present. The anple however, did not exhibit any ftbera that we could detect. 'Vhank yi for consulting McCnne Associates and if you should have aa' trther questions cone erthng this analysis please contact me. Sincerely, Gene B. Grieger Sailor Research Physicist GRG;fe ret; 5500 282080UTh MICHIGAN AVENUE CHICAGO, IWNOIS 60616 312/842.7100 CABLE OHEMICRONE COL 00554 McCRONE 0078 waiter c. mc crone associates, inc. CONSULTIWB, ULTMMICROANALYSIS - MICHOSOOPY SMALL PMTICLE PBOBLEMS SOLID.8TATE CHEMiSTRY 25 January 1978 Er. S. P. Slmko, Jr. Colgate-Palmolive Company 909 Biverfload piscataway, New Jersey 08854 Iear Dr. Simitot I have finished the *namission eleotron microscopical nram4naUon of your sarple, designated as tOt 1-5-6, for asbeattorm material content. This sample was found to contain platy material ranging from the submiorometer size ranges to plates in excess of 20 pm. Little material of any other motphologtoai type was found to be present. No asbeatflorm material was detected. BepresentaUte eiedtron mictographe of the sample are aended. Thank you for consul Ung us once 4am XE any questlos should arise concerning the analyses we are performing for you, please do not hesitate to call. RJSfe end. ret: 5500 Richard J. Shimpe Research Chemist U20 SOUTh MICIIIGAN AVENUE CHICAGO, ILLINOIS 60618 312/842.7100 OASL OSEMIORONE COL 00555 McCRONE 0079 C. 2-24-24 Lo 1-5-8 diffraction patten of typical matetial waiter C. mcrone associates. Inc. COL 00556 MoCRONE 0080 LAwafter c mccrone associales, Inc.OONSULflNG: ULmAMICROANALYSIS M0R0SOOPY SMALL PARTICLE PROSLEMS SOUP-STATE CHEMISTRY 23 February t978 Dr. Joseph P. Slmko, Jr. Colgate-Palmolive Company 009 River Road Piscataway, New Jersey 0884 Dear Dr. Bhnko: I have completed my transmission electron microscopical erninaUon of your sample, designAted Lot -8-7, for asbeetiform material. The ample contains material ranging from the subinicrometer size ranges to particles In wroass of 25pni. Although the predominant material is basically platy it occurs mainly in ohiml masses. No asbesUform material is found to be present although fibrops aspect inorganic partlolea are conamon and range in morphological types from shards to an erent flbc bundle. Repros enthve electron micrographa showing the semple iaterlai lypical fibers and electron diffraction patterns are appended for your further information. flank you for consulting us ozice again. If any questions should arise concerning this data, please do not hesitate to call. E3s de etiol. ret; 5500 RichardS. smmps Research Chemist 2320 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 6O16 12/842-71OU CASLE CHEMICRONE COL 00557 McCRONE 0081 2-25-10 2-6-7 32,000X DiffraoUon pattera of 2-26-U. wafter c. mcrone associates, Inc. COL 00558 MoCRONE 0082 .:. .. -'.a.:t.-:7.:. : .::t ? 'Ic. .3- 'F: .t:fl, 'tp '..' ''ri4 ?z&fl .'L. p, .. .1 2-28-31 2-8-'? 20,000K fiber waIter o. mocrone associates, Inc. COL 00559 MoCRONE 0083 waiter c mc crone qssociates, Inc. CONSULTING; UL7HAMIOROANALY$IS MICROSCOPY SMALL PMTIOLE PHOBLEMS SOUO-STME OHEMISTflY 7 Apill 1978 Dr. Joseph X'. Siruko, Jr: Coigath-Palmolive OompaT 909 River Road Pisoataway, New Jersey 08854 Dear )DT.Sl3nJcot Using transmission electron microscopy and selected area electron dlffracuon, we have analyzed a saznpliof talc, designated as 3-16-17, for asbesttform minerals. . We did not find any asbesWorm ninerals In this talc and it appeared to be quite 1&pical of the previous tale which we have examined for you in that only some of the talc was platy and there wne moderate fines. Thank you for consulting UcOrone Associates and if you should have any further questions concerning this report, please feel free to call me. Yours sincerely, GROtto ret: 5500 Gene K. Qriegr Sailor Research Physicist 2820 SOISrH MICHIGAN AVENUE OHOAGO, ILL!NOIS LOSIB 811842.71OO CABLE; CHSMICRONE COL 00560 McCRONE 0064 rrAnsw,Tezc AGENCIES Sodnz talco 3 Unifta Vol Obliose PEAnIO (NflII Italy) Sodna Anota Talco But Tha & 0. Lqlawu. Italy 0. A, Baldracco El Ripe Torino MATBUOAR" CHARLES MATHIEU, Inc. P.O. BOX AM 18-22 BANZ STREET STJM?flT, NW IEB8BY 07901 REPEE$Efl'flTTh Di USA. OF FOREIGN M]]qEs Nay 17, 1978 (201) 277-0510 Hr. Ian i4. dtewart Walter C. Mactone ISsoc., Inc. 2C8h2ipca8g. Mo,iIclhliignaonisAve6n06u1e6 Dear Mr. Stewart: CworintifnirgMtnogreoquuretsetletphhato,neeffceocntivveersiartaimonsdoifatthelyo, tyhoeur dpaeyrfworemaroen taablsceinacaeploefsfsibearot utos,yaosubetshteosfopfalortwicilnegs:tests to determine the x-ray defraction optical microscopy TEM - S?aED These samples will be forwarded to you from either our plant in Alpine, Alabna or South Plainfield, New Jersey and marked for (IrcteooelugosartatstPiPtat.lOmd.uoBlpiovlxiecAaCMtoer,i.pSaunmy.mitT, NheewteJsetrrseeysu0l7ts90s1h.ouPldlebaesetoswenadrdthede as you remee*ber, you have been performing the TEM tests for Colgate Palmolive Coiany and the' have now asked us to perform Tthheewrehfoorlee,tepslteapsreocuesaeutrheiasnldetcteerrtaasfya tbhleanvkareitooursdleort,satuoththoermiz.ing yoa to perform the tests above so that we may cartL'fy the absence of asi5estiform minerals to Colgate Palmolive Company. Thank you for your cooperation '4th the above. Very truly yours, CHARLES MATEIEU, INC. DflF tab *s ta$.i4bh Sty 4ita inssis.& by uninz. Jl.qootaion asj a,Sos awb)cct t cozjltrom beyond mit cono4. E*a so isod upon exissttg rail! nra end Clutonncgtmm. COL 00561 MeCRONE 0085 ia. PM waiter c. m crone assocbfes Inc. TA ai CONSLtTING: ULTRAMICROAMALY$I$. MiCROSCOPY SMALl. PAWHCLEpRQSLEMS. SOLID-STATE CHEMISTRY 2 Jtxm 1978 Mr. Donald K. Ferry Charles Mathien, Inc. E. 0. Boz} 18-22 Bank Street, Sizrnrit, New Jersey 07901 -.Dear W rry: - We have t1eted r Saalnatiu of your ts.c eaile identified ass. Talc RbWS, W6670-9, Tht 5-2-3 using the CTEA J4-1 ethod su p1 natal by tranamiseica electron microscopy with selected area electron diffraction. Ne.tther method indicated the presence o5 aebeatiform minerals present. The 34-1 results eve presented on the attached atnary sheet. The elecb?ctt thcrosropicai. flilwtn4ticn sha,al the talc tol,epreaait as equi-ased grains rather thaa as ectra3sely thin plates. There was little or to indication of fibrous or roiled talc present. manic you for consulting bbOzcne Associates an if you ehojld have ay questions concerning these results please contact us. Very thu7 yours, G!Thfe awl. ref: 5500 cc: J. P. Siathx', Jr. Olgate-Pab1Sve Co. Ge$e K. Orieger S SaUor Researach Physicis 2620 SOUTH MICHIGAN AVENUE CHIcAGO, ILLINOIS 80516. 31VU42'TlOQ CABLE: CHEMICRONE COL 00562 McCRONE 0086 Client Cc, Pcta.wc,/ive MA Proje.ct SCao Sample Description flJ Epipc m-,.6zn-c L,,t ,3t X-RAY DIFFBACTION Serpenthe Content ')tniei Amphibole Content d- p%,,%,4 Cotnments a 6 lo ,-; $ o1 S,v9., tIaRat MXCBOSCOPY Serpentine Content Amphibole Content Comments x-4-.-< jq waiter c, mocrofle associates, Inc. COL 00563 MCCRONE 0067 00r00a I_n ll l*ltn5ffllfIllW551la.lllnI5I_as-----1-fllSSalal0t.5IInIf-,l-aa.ma_*fa__-I_at-s_Wr"l_la.-aWma_nsIf.sSstf5-__-laliWSsssSsS--slI-S4T_-lsS-SSSnSSt5S_s-_aYSI1ti5.lla-_Ss-5l-sTSnl5tInlW-lllllfftlaal1Izi:.tCWi.rz..._JL1!fJ.rrtiI.at.ff.i.ll--finUai a.l-aia-nnlSrn.rI.J--_aaiaEulklanI a...-.--=1an=as5s=p5s-i=_S5sIa. lIatass.sa-nWItnatas..naP.flc.fal!1!I6n9,(g1p an slWa.trlIia..1nasWanWannann_!iaIn_..n('I nWW*a.m_fllWunn_fWlttaJA - iWanSnsaWauuWklWfIWltnsWwlW.WtfnslI.fiI.l '-1.4s.afIlf_IiWa_nfl_fl-.Sln5._ln.Unaa.Iia.Inn_ufItf.'nlInaanlilnsniI_laalII*a.Sa_ii.Wfaasanl.SxaWW.fnIt.*alSnI.a1Inu.I.ll. 5la1S5t5 fIaPsl-_aianagl SSI ata1ItaWn.S1_W5SISnflWalfInllfialfsll. an-_aI 1'aW5aa1laI5-_u1ai -I*l5la_7I Si I sanI5_I1lII*ISht5tII1i;i(n.I ) iS1aI1asl1Iu1aI[1la1i9ltaaISt - i_al_I 11111 ISa[slSIa5_a_allUnl1Saaatllau1Il.gas.l1".I,flI1'lIINl5Tl-SSa- S l.un_a_na. IfallI alIanWll. li_In 55._a l'5aS"PaIWa1aalsU.la1ala.l_a WISIA. -. 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Ii II, i.! iii .Ii' . Ii I hal I, I I II I II I' r tf/ // COLGATE-PALMOLIVE COMPANY A Th'wm, Citmain ZBSE4RCH AND DRVliLO2'2CENT D,EP4RTMJINY 903 Rivrr Real . Piscn.nvay, New fern2 0fl51 Septeter a6, 1978 Ian Stewart Melirone Associates 2820 South Michigan Avenue Chicago, it 6063.6 Dear Ian, As discussed., I have enclosed two ttllipore filters containing particulate matter thich we want identified. The sarples were obtained by filtering a liqui& product followed, by washing with water. Photomiorographe of each are also enclosed. Codes are 10033 amd. 6000'r, please give priority to 10033. Specifically in sample 10033 we are interested. in identi4iag the black-appearing particles. By light microscope those appear to be hsld in a yellowish mass or material whose identity is also Unknown. Information concerning the yellowish mass is dSire,l but is secondary to the black, I suspect the black material is amorphous carbon If so the surface layers will be contaminated with a. variety of organic sad inorganic cozonente. I have had BEM with ZSrgy dispersive x-ray run with the following resultat Black Particles oohtain; aAAl,tM.flg, ' Ca, Si, U, a Cl, Background fliter contains: Al, M, Ca, Si., Na Kv,*Na A second possibility for the source of the blSack'Vcon7toamiInt.ant'"iFs a dye used in the product. This is an organic containing C, U, 0, N, S and Na, Sample Coopr has black pe.rticles together with what appears to tts a crystalline substance. In this case we are btarested. in the identity of the crystalline phase. The millipore is 0.22 micron GB. A purchase order will follow under separate cover. If I cu be of any help please call, Sincerely, JPS: is Enclosures , P. Binko ..c 5137-, COL 00565 - McCRONE 0089 COL 00567 McCRONE 0091 COL 00568 McCRONE 0092 C waiter a mcrone assodates, Inc. S CONSULTING; ULT.RAMICROANALYSI$. MICROSCOPY SMA4.L PARI1OLE PROSW4S SOLID-STAIE CHEMISTRY 17 October 1978 Dr. J. P. Sinko Co1gate-Plnvil tve Oorxpaay R&D Deparbc3t 909 River Road Piscataway, New Jersey 08854 Dear t5r. SbLco This letter tI.1 confirm and sutmrize the results we obtained on the particles fa.ai the filters you sent us on 26 September and identified as 10033 and 60007 low -letter Indicated that the black rticles on filter 10033 were of bisjtes't priority and you were particularly Interested in determining cthether these black particles were asorphous carbon. During the analyses we were 1n frequatt contact and I shall therefore Just briefly ewmarlze oim conclusions here. San1e 10033. Black yarticles are a aixttze of asorphous carben and StaPtate. O3neLusion is based on electixn Lldcroprcbe analysis of black particles tch shos approthately 80% C and x-ray diffraction tcbich shows a mi*u.re of 3 phases, one arphous, one graphite and the third Sairple 60007. YeJ1wiah umsa This iraterial is very togateoua and contaists approximately 3% Si, 12%C, 35% Cii, 4% Fe, 3%A1, 2%P and 2%Na. Based on x-ray diffraction t1iis phase probably contains about 50% Cal? and 20% CuLX)3 The Ca? shows, however, at Inversion of the relative Intensities of the 3.15 and 1.93 lines and very broad diffuse lines Indicative aunil paiticle size. Yello4ah nsas. Consist oF ny fine particles, electron probe shows 20% Si, 8% C, 10% Ga, 12% Fe, O.8%l 12%Al and 0.8%?. flectrbn probe data suggested possibly a clay but x-ray data again indicates Ca? predrxjthant 2020 SOUTh MIOHIGAN AVENUE CHICAGO. ILLINOIS GQ61 312842.7100 QABLE: OFIEMCRONE COL 00569 McCRONE 0093 Dr. 3. P. Sbico Page two At this point you indicated that you did aot wtsh any further work performed on these saxxples. We shall discard your sanpies in two qeeks imiess we hear otherwise fran you. Yours sincerely, tan N. StaQart Manager, Electron ptica Group IMS:fe ref; 5500 COL 00570 MeCRONE 0094 --- aS-5$4$6t# e'- 02t' 'ajL4jLthL4s -2 _ _-. 4. 7 S e misL4rrertfr I. 1 - - -I c," - COL 00571 McCRONE 0095 '' -- - e-v r /t -. -( r-:c: '24- '-. 4 .. .: . JL -t - .- -. .. - I . . - -- .. . . :,. .. dr?% " -' t4 -', -"-, ak...::: .. .. - .r,, - . / ,. M? - 1''.-, -' .: 1 ' ' "t-' :e : ks'' "4'JIC ......2- / & Jd '. _:s ., _( .s, '%1k' I- / I J_ -' '' .3) ' SVL- -t _.s ..,' ' - -.. - ?P*k - -:;;,: :4';.- r,' COL 00572 McCRONE 0096 POSITION OF PARTICLE ON PLATE ZJ(#'t ywrV,c?wo C7%r?r'. r '# .t.# .J -. Sample No. lOO(flS/a. 2.. L-001umn no. 1 I-i O Beryllium plate no. L PARTICLE MOUNTED ON o Carbon plate 0 Aluminum stub no. ./1 o Xraypin,boxno. o Copper grid no. PHOTOGRAPH P102 X-RAY DATA Data /n-/r7? X-va'tlImno Sample size Description of sompie /LExposuretlme.SIt EnvlronmentAOtt Ccmero U ' nun KY. ma z.r TubeflCi tUter' SAMPLE 7.7 1 3%.q31 Cl I.q tA ., A$TM No C.-/aic, d 1110 .3 #8Th No d !Th L14- Cl Z.fl Cl z_,p .ci 2i.t*i$ 'CIf 1h.461 oCrI hJf- s.li C t.U- I ,.IG Cf 4.Z.i 2.. a.. -3 (2.. 2.. .1 i-j.-,Comments p4II _et/.C-fl7 4, Conoiqelons .4t..pAa ,psi C a. ci it fl,, 4a gs',, p COL 00573 McCRQNE 0097 POSITION OF PARTICLE ON PLATE norflJ-kcoiumn PHOTOGRAPH NQ I SampLe No. PARTICLE MOUNTED ON o BeryllIum plate no. o Carbon plate no. 0 AlumInum stub no. o Xroypin,boxno. o Copper grid no. X-RAY DATA Dote Sample lao X-rayfilmno . Description of sample Exposuretlme_Ir. Environment KS. ma Tube Comsra filter mm SAMPLE ASTM No d 1"to ASTM No d ii 4 a4f I. * t I, * 169f PHOTOGRAPH NO.2 esi4t qL4 JiG- ,tn -taC /1-$5i /01 )o.o ,o. e4 /j/q, 3e, 217s, s;s8 (Pb (Lt ,ot Comm B Co no Iusio 'a COL 00574 McCRONE 0098 POSITION OF PARTICLE ON PLATE, r rColumn norlII L Sample No. PARTICLE MOUNTED ON OC2 7 _.7 (U Beryllium plots no. 0 Carbon plate no. 0 Aluminum stub no. Dxroyn,boxno. 5 Copper grid no. X-RAY DATA Dote / 'M X-ray film no Sample size Description of sample Expoeuretimq&hr. Environment a.4' Camera tZLrnm Ky. ma Tube tPS filter. el/f SAMPLE d ASTM No t5 d fto ASTM d Xo - - .11 -C r,tpsitentsfl '//0.i0f g.l: :0 - sat 7 *0..S?(t .7 PHOTOGRAPH NO.2 ConvnentS 4(/-1-4 .- .Jnao( a.- .tti1Conciiel0ne S ' cf--' COL 00575 McCRONE 0099 rn '1c Ky tD b1ce.k 1,oj-J'Mo.. 10033 c,000; jM(omiS3 S &"44 QYj*4)#... - 3 $ 3- of io 2.. I 'U Igt jig oaieOCT4 Sampteor particle it. Size Shops Co to r(T.) (R ) Ag Al Ba Co -4'"+ CI Cr Cu Fe 1< Mg Mn Mo NI Pb S 1 ".k Ti Zn C lo-9a F Na 0 / 7MICROPROBE DATA SHEET 1978 Corrany OBSERVATIONS MI?COPIC 6 ELECTRON MICROPROBE DATA, % COMPOSITION 4-4- I- jfl_$J5 30-44 .a-4i i- j-.c 0,6-I 7,j..4A i-4 i-a Cal-i .t-4 J5 14-.x5 id-is /4-1,5 4-Jo i-'J MA No. 5C3 Lt5,3 lt5 0.8 comments aJ io,.a... ik.? /a.4 pr 91,4 4g,o 14 49 eflA31 e/3 COL 00577 MeCRONE 0101 ''I (4tnkrh'a. A1k o4 Wed - u--yettwa* nn4i's -JL 4}Wt 0cc 4?ve COL 00578 MeCRONE 0102 EED$-u RU1HflL SIP S CIK CAFE PSI; ff5: 437 ET 83$ flT: 9 1K ZBEWCH 00.08 EOe.08C= 00-10fKl5EUI COL 00579 McCRONE 0103 :zezrt.:,.:..=1..ra..E.. irie-C53aj jnLrt=r; - a=.1Rair EZrZ. :::::::: = - -. :S -F -c r. t:--=-- t",.C - -a-.-: I COL 00580 MeCRONE 0104 C FtU'ALSIP CAFE .t:A1 ET= 39$ 1K 526 Z131'W 2EWCH ee-is icEv 362 1= 18.22 COL 00581 MeCRONE 0105 - .. ;t:j; - .-. ErjEc#gL Jr:. TrAm igiaiiiiiCE Lt!jfl :razce J[;1-; .-. . . - .- C C C COL 00582 McCRONE 0106 10:1 R'S1 CA fflTl':ALTi 100$ ET= 1flS $12 aus-n P$' 142 ZUT; 9 20 LU/CIt tee e-teinv 48.88 t= 1088 1 * COL 00583 McCROI4E 0107 - - .-.. .-..J..-. r; ... - . -.. -_ - ? - .rr Mi: 5 -- r C "1 C ...._ pt.,.... "2:: COL 00584 McCRONE 0108 tO2 P$T.LT: 1028 9:At E1 512 lOGS Ens-it cFsI .76 UTt 7 20 EWCH tee E'20.O0 C es-t1o* 1 * COL 00585 McCRONE 0109 - nZ;:r 2 rarE t-Th ;; - &.ilL=i1flr= a .i;j:z. ic:.........._$_._. zt:rt 7- a- z_.YE rh- a--..- --.-m - -. -. '7 - -. - a-- '- -' a aJE - - COL 00586 McCRONE 0110 F.. R16:f5l:t$IP CAFE PDI:A1 Er 356 1K EEDS-1I $: 624 D1:12 a. 42.20 C 318 12.22 * COL 00587 McCRONE 0111 ... . a... .....................*r:.. .{....4 ,..,.. .j .....................I1:::2r2n - -. ............. lb rE.J!J ........... ..................................................................,.t r ...... iru: I:: ... :;::::::::::::._ ............... { ............ '103 sscoo 3NOdOVJ 3140 a 'op I!! ii ill II III II 'H I'' HI 'II Ill t COL 00589 MeCRONE 0113 oi'7 COL 00590 McCRONE 0114 ,j' waiter c. mc crone associates, Inc.V I OCN$UL'fINa uLTRM,jICHOANALYSIa MICROSCOPY. SMALL PARTICLE PRoSLEMS 'SOLID-STATE CHEMISTRY 22 Nvather 1978 It. I). R, Ferry charles thien, [no. P.O. Box AX 18-22 Batik Street Swmit, New Jersey 07901 Dear Mr. Ferry: Using tzansaiss ion eleabni ntcroecopy and selected area electrai diffractint, we have' analyzed a sauile of talc dasebseinsatltfeodmams "hLioetra1i1.s-2i-n3,ti1d9e7e8aSleeroiefs"ta. 2cWaenfdoutnhdemplaty talc and talc flne were both tmderately distributed statistically. There were a faq abards in this ta3 tch are qaite typical. We also analyzed the sauple using x-ray diffraction and in this we fow4 no serpeneinee and no anhibolea. We did however, find acne thiorites aid sane sljiha-Si02. Thank yoti far consulting thcrone Associates and if there are any further questions cncerrdng this report or the data contained berein, please feel free to contact ne. Very truly ynurs, CRC :jd Ref. MA 5500 cc: Th. Joseph P. Sinicc, Jr. Gene R.. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE. CHICAGO. ILUNOIS OX1S 512;842-7tU). CABLE; CHEMICROtIE COL 00591 McCRONE 0115 Date ji-7-78 Client CMa-(e'c j1ec.+A5et.c MAProject SCbc Sample Description 1iT it Ia it 4.1,t it--. fr/ -#4?o-I. 4 Z-RAY DIVF2ACTICT Seruentine; Detected Amphibole: Detected Other Thaees Present: Chlorite Dolomite Calcite Other: Not Detected Not Detected L-' a-SIC2 Magnesite L- Mica, Oominenta: LIGHT 4ICBOSCOPY Chrysottle Tremolite,Aottnoltte Nonuibrous Serpentine Others Comments: toIal %. a-Sb2 % ilbroas waiter a mccrone associates. Inc COL 00592 MeCRONE 0116 :J1 I.:. . - IJL.-LTh LJ - ...... ---. : -.-- ..J_.- .'-. .4 I.. . .:. ............. - ..... r:[4g.pS.tL.JtLtI! Till H W4 ___ : I __ - .:-j 1 - --. --- - - F----t-- ' -: --------------_--_-_--_______ ... - J2UtZJ -- - a- __. - ._L_. t- I- ------------------------ -- -------------- I.'---FH-+. I ... . - COL 00593 McCRONE 0117 1 wafter c. mcrone assodates, inc. CON8ULI1NG: ULTRftMIORQfrVALYSIS MICROSCOPY SMALI. PARTICLE PRO8LMS SOLID-STATE CHEMISTRY 22 January1979 i-fr. 1). 1k. Ferry charles Nathteu, Inc. P. 0. Box AM 18-22 Bank Street Sumnit, New Jersey 07901 Dear bfr. F&L7I Using transmission electron ud.croscopy aid selected area electron diffraction, we have analyzed a sarple of talc designated as Lot #12-19-20 of the 1978 series. We fond this talc to be ccqletely free of asbestos minerals, both aibibolea and serpaitines. We found this talc to be slightly platLer than the previous tales tcli we have examined skid it was an excellent talc. We also atied this naterial using x-ray diffraction. The results of cur x-ray diffractlm analysis indicates that * could not detect any amphibole or serpatine minerals in this talc using x-ray diffraction techniques We did, 1wever, fini aUght traces of chlorite and alpha-5102. We could detect no other minerals In this talc. The x-ray aiffractfrn data are included with this We thank you for consulting thcrone Associates and if you have any questions ccncerning this report or the data containth herein, please call n, Yours sincerely. Gais 1k. Griega- Saxior Research Ptsicist G:fe attach. ref: 5500 cc: Dr. S. P. SIt - Col.gate-Palirolive 28W SOUTH MICHIGAN AVENUE CHICAGOrIWNOIS 60816.312/842-7100 CABLt C*IEMICEOVIE COL 00594 McCRONE 0118 Date 1 2-79 Client Ck.ww/ec p1ct-IAt.t5 j... MA Project Scar, Sample Description TJe L,n' No. fl-it-va; X-RAY DXflBACTION-- Serpentlne Detected Amphthole: Detected Other Thases Present: Chlorite Dolomite daloite Other: Not Detected Not Detected L-" a-8102 l4agneslte w -'' Mica Comments: LIGHT MCR0SC0PY Chrysotite Tremoltte-Acttnollte Nonftbrous Serpentine Others: Comments: total % a -SIO % fibrous waiter c, mccrorie ossodiates, inc COL 00595 McCRONE 0119 S Se :e ... .. ..e. ...-s.c.S.3. ' iiI 'li I: i i:; ;;h ;J . 1H 1:1 '1:-tHiiIi . II.1II ,. I I! 1 1.1; .i . II.. N ..flfl ....in It 10::::.:.::::::::::::.u::n'9::u::I::I. :i0 L uaviiutwui i.:iiLiuph..:::.it_I1i.iiui:I. fi. S .AJdS"4IMt I!! ......... :flt, S... 0 S. I I -j .......I m ti ig:i'n:guui zr: . 1t.0ij1).:......'q.i..........P...oP....O SW ii V V PflflSSS EU WIpLIflWt4.*.ps ci EIMI3 gzui:iarr.W :4- .... E. -'.hPtI':I.:.:::5il:.::-':;: r. ......r..n..m.. !i9rrI.. ..rn.I.:m.u;:uV::.:V!nn 9 II fl f.dthrL' r. er-: 'I1::r:.hn:r:.:.:.I..:rt S ans U ji;uflij Vn wp. n flJflSS WVPP4 Iflp. P rr '!J........- . - . - ;!. . njrmm :. 11UflIfl11I -fi **_J . - U- VU Puu..PS0.5.. ...zmfl{zPntPmS nn-lHI 41 ptqj:Jj4jiVTS&SSkIIfOlpViipSg3ixSpM r1 p. I P U P.IUa..PVInp.lfl. IU S0nVilSP.pOopP - ::::::1inPI;h rInIaIllhia1arEr:: I ' .uh.;Ii;L. .14a111L111111 llt.itltHtIiliil. ? IillhIftI1 - - -! . .................'PU: :'.Va.;.-i1Ia! teaUouInI.PUIpAn.U._1E1.P1..l.p.1I1.P.ar.Il.I)ts4f..d.l..sr.:..I.L5..u...V..1SI.l4Im.rnU.sn.-t..:SP..Jf.plI.Ilanf.l.pUf.l.S.c...II...I-h....U...f..l..nU.....i.-......U.p..t.-....-4..ti..JIIr..I.U'..I.I...fIVpl.rtII.-IsLrS:pIq.fmjIlst.Ial.OII:i.IftOf.U.l1lTr_TP.0U.in1uUflIfiItlPtu'lIJPItft.UilJIIIhUqln'MM.In.ItU.InIIIOP&I.OL4'II.I1I: 1 RI'&r1 :- 4 a en.. p b 11 ;iu,I -P :IIg.J..1.I1.El l,:?IP:P::jP:I:.I.u.:1ihJ".ait.J1 b . I IIJUflIUflIUfllMMIUiJK$I -$-S$Isi$I$lI$aII$$III1IIII_I_I_S_ $ 1111(1' roC."1 0 0wz CU-) Date FZc97? Client ?a/)*c n/lye MA Project SS'Oc i0rSample Decr!ptIori 2ttlfl, ftl-(e277 Rz,goo X-RAY DIFFRACTION Serpenthie; Detected Not Detected Amphibole: Deteoted Not teoted Other Phases Present: Chlorite i-" ft-3102 Dolomite ..- balcite I' Magnesite " Other: (4nr.) Mica Comments; LIOfl 3\UCROSO Ofl Chrysotile Tremollte-.Aotj.nojite Noafibrous. Serpentine Others; Comments: total % a-SIC2 % fibrous waltero. mocrone associates, Inc COL 00597 MoCRONE 0121 V V V V V V V. V I U.'' UUIIIIII1$j4.$\ llmllq I iii Lllll!F traannn fl1$%flfl**WTPgIfal.t.l.aap...qm,.....u.a tS.n-a x&flmu.*.-na.. flE -r't .4k w as UWrOrI - lit U' 8:1 'r'I.. nab..: a: -' a' 51 I In .a. in III:.iii:! !1i :hIIIIllaIIrdnuuJI Ii %riWI& tiIillliztiiI1 dllqiifflr iisiIJIIIMas.f..fnlnInI. u- -" lal1nfif.Elu.inf.d.aiflflkltsh.1nIi1qff a . I: 1 nSfl*iIliIi IIfSl tSI*SISIn51In1S1151I1InInfl5f*l5I*lSl aSW ____ F i-s.. ia i Zfl:r8m:U:qutm vnmgar_aifilfrlPntEianLin4nnmannlfilfllinmnIniENnun. fl*.l.U.*a. n3s NSLAUnE-&--f-Hi-n--s-f_i-I-ra :-. . ii T- ij' illi3''IWIB-riJ-- ktasnnassn. .I.ni S itfl. 1it51*nalna.nSnwaInsnusInIshuIatfIlanWiw*nnna..n fl tI ::itjr1 ra..UI5flilsUn.mm.wnn.... mzi jffulianliiaIEdl I1Wflnu5*flf4l$11m1f.l3a...nn.nnna..nJlnu.a.n.nsia .a. saunas 1S1A&na Ifl U r' -4um.1nn.rS!arr.-.t1(8laSwaaa.*aasmu LI!.naansaatu_____________________ In..I S tIns 1*IISIflI rn.flIan.InI.f.i.pIana.l k.5*..w afi*sn5*a*5I nluullt Lta.______________W__iI___ uiuIII&Za I., fliI!bn8$ . ,iraui- i-f--. - -: I: - rj ____ .- -lIi'JIOi 1111111 !!IilltIIIffhIIjJllQflhIIJI!j{IjlJ i-i!!; hllIoii! !.:;NIJJJtIIIIJII fl - ?e S s'-s"e.--e .. l -ii reaw.rawrararcssrauwsrg,rawJfs,aJsrs1arSaw/ '. asrsreessgsistra a COLGATE-PALMOLIVE COMPANY 4 V:kwm 4e4#n R.ZSE4RCH 4N1' DRVRLOPMENT DRP4RThIBNT 909 Rii'.r RosA . flsc.vtewa2, Now Jersoy cnn 1a.otL' Ir," February 2, 1979 Mr. 1a21 Stewart MeOrone Associates 2820 South Nichigan Avenue Chicago, 2. 60616 Dear 'an, Thlosed. are tic saiqles coded 6003,6. end 10016. fox' mioroprobe ead microfttfraction studies. These are, residues trapped on 0.22 micron mil.ipore fliter discs and are siii1ar to sample 10033 I sent you September 26. We want the sand 1formation on tbese as on 2.0033 (reported in your letter dated a.o/iT/TO). We are concerned it any toxic elalleits are presents idtet are the black spects, and what other crystals are present? I iould gg5 the two naples are sSmilar and zniBht differ in the proportions present. A purchase order has been sent under separate cover. Ser sly, .TPS1s Bn210 sure cc P. A. Z&iger 3. P. Bauscbild Jr. COL 00599 MeCRONE 0123 - A.. 43 j,z-C 5 /4, 'er 3J /37- In L-/4, COL 00600 McCRONE 0124 I- ------#WL - -' -------- ftlrAs 'nr?I4..A4lHAs44 11 4S4,_i -t - .L t---------- i.h41 $ Jta*L. :1 >1i4 t4 4w_-Lo41$i.4L!ij 4' aii.c..*, J1bQ..*i42..l.4 .bL_j.h34s....L. flk.s . .,4 \ t-..t..-...........t..-.-.--- . - SuGa...+.f 44 I 7t I. . ...................................... . r&. JR - 4 .:... - . .. - - 0 .flfl, I :':-f-slf-li.l.lfl1$(:fl... .. IJ(flU .... . :.'. .,. H :.0a*n'.a.' . /-4.. I .tt,,_ r Ru- .*fl0$ :' flfl: a. iaann. F I- r,.fl0EflwNr, -- - - -:$ -. .. .- :zi 0.T' -. IL --.... ..***aflPnTT fl5 &SI r*asrenwatnion.p-g. r--.i3txn2f*aW-la$$s3r3ns*SSNnfVN'wl4E!fSnlS*an**-fSBwls*f*MalnN;*nsL.Mat-w.aU.5$0. : . .-': - - -. - -_ .: McCRONE 0125 COL 00601 P .Teesov MICROPROBE DATA SHEET Company Z4in Samcl.Qr,7 Particle . Size' .L Shape Color(13 :3 g6cMICROSCOPIC M 5- 6 OBSERVATIONS -? uD (R) ELECTRON MICROPROBE DATA, % COMPOSITION Ag Al j..,, 1-4 Ba Ca , oj-as o.o-, '6-go CI 4..i.',5 d.et'4& i..j a4 .td..4.3 14 as-i rn-i sn-so T-M i-a do-SO Cr Cu Fe I-. O..I-t. , - A K Mg Mn '-a Mo NI P I-A Pb S i-a 4-6 St 1-14 i-. l-j Ti in C ,i-'M co-ca .10-40 ,-,s1 ,,.ej. 4-. Na 0 0.5-I ,5-ao A - At 'd'5 4o-i-o. a -4 . 14 "4t,J-A6 / A - - ...4 4-1 0-O.5 In- i. 0.5-I o.a-o.5 ?fl.40 aa-ja '-I--I f-ia 77.1.. nd 4- .6-5 * s 4. ' /5.f 40 l.A. UT MTItO ,a.1.( 475.'i ,g,q .4.a 'kg- Comments .LO,jA.n) / flat dtAdn.bh'. + $a Q.4 .5.i4,q '#t. t9.t 3a.3 ,04,.q S?.o is.s J.ts,q Aa 7 54.! .h. 41.R. 5.1 35.1 72J. f4 COL 00602 McCRONE 0126 z COL 00603 MeCRONE 0127 W -Bavek4#4flt I) COL 00604 MeCRONE 0128 waiter c. mc crone associates, Inc. CONSULTING; ULTRN.IIQRQAMLYS)6 MICROSCOPY SMAU. PABT1CLE PROBLEMS SOLID.STATE CHEMISTRY 9 Februery 1979 Mr. Daiaid Ferry charles Mathieu, Inc. P.O. Box P24 Stnoit, Naw Jersey 07901 Dear Mr. Ferry: Usesliencgtxed-raayredaiefflreaccttriuoxndanfd snstdseiaz electron microscopy with acticn, *e have analyzed a sarle of tale designated as bitai 100, Lot 851800. Both techniques show this talc be ccaip].eteiy free fran ashes tiform minerals. Electrcu microscopy thawed this talc is extremely piety. Because of its platiness there were wxs rolled talc shards, but this e normally find 'with piety talc. The results of our x-ray analysis also fnlfrated that no anpbiboles and serpeitinee ne presant We did find sane chlorides and txaces of alpha-8i02 dolazd.te, ral cite and znamesLte. The results of that investigatiat axe fncicded with tWa report. That you for consulting *Crcne Associates and if there are any further questions concerning this report or the data contained herein, please feel free to citact we. Very truly yours, Getie R. Grieger Senior Research Thysicistr G1: fe mci. ref; 5500 cc: Jo Belt Slito - Colgate-Palnoliw Co. 2820 SOUTh MICHJQAN AVENUE. CHICAGO, ILUMOIS W81S 512/842.7100 CABLE: OHEMIORONE COL 00605 McCRONE 0129 wolfer c mcrone assochies, Inc. GON5UL11NG ULTRAMICROANALysI MIOROSCOPY SMALL PARTICLE PROBLEMS SOlJD.STATE CHEMISTRY 9 February 1979 a it. Donald Ferry Charles )tldeu, Inc. P.O. Box AM Simid.t, New Jersey 07901 Dear Mr. Ferry: Using x-ray diffraction and transmission electron n oscor with selected area electron diffraction, we have analyzed a sariple of talc designated as thnital 100, tot 881800 Both techniques show this talc l be cailetely free fran sabeatitorm ndner4a. Electron uil.croscopy showed this talc is atrsiiely platy. Because of its there were axie rolled talc shards, but this we normally find with plty talc. The results of our z-r' analysis also indicated that no kaphiboles and serpentixes we present. We did find some chlorides aid traces of s].$a-8102. dolomite, calcite and gnesite. The results of that investiatiai are included with this report. Ths&lc you for consulting &Crone Associates aid if there are any further questions concerning this report or the data contained herein, please feel free to contact n. Very truly yours, Gene R. Orieger Senior Research Physicistr Ga1idG.fe ref: 5500 cc: Joseph Slit - Colgate-Pabnolive Co. 202050UTh MICHIGAN AVeJUR CHICAGO. ILLINOIS 60616 3t2/8t27100 GA5tE OHEMIORONE COL 00606 McCRONE 0130 Date 1-29-7? cuent i moeot s-rao Sample Description Zinc's, P1-6277 Ant RJIQDO X-RAY DXPFRACTION Serpenttn.e; Detected Amphibole: Detected Other Phases Present: Chlorite z- Dolomite .- Calcite I- Other: Not Detected Not Detected '.'a-SIC2 C+vnre) Magnesite Mica Comthents: UGHT MICROSCOPY Chrysottle Trexnolite-Acttnojtte Nonitbrous Serpentine Others: 77 /LrcJ' total % a-sio2 % fibrous Comments: waiter c. mcorone associates, Inc COL 00607 --McCRONE 0131 u...,.,,u,t uuululvi 'II 'Is $ I 5 1 1 $ U S 55$ S-S V I 'U. fI'flWliW ......nrL..:'..;1: jie'nfln EliIIIWIMIH___________ u. nfl.n' S n..,fl.fl. 1W" :fl5- e24*SflflflflflWasfl.W..mt.tfflltssZ.tw.cnPnillfi'lWaTnflSn.5I1:'l5l::Sh:5:255:5S:5;kIl:.p::S:!t'.Es..:..S-..p Sr CinXsSw.flI.rk.,i.f.a!Et5j".(C5SEj.ILft' ,.ss.cri ElflflWrInI..f-luT. -fl- S:":n:4;:: ..n,I.ll..... n5p4.sl... 51 55r.5.5..h...h.Sn.S..r.....,..a,..i.n...S......lS....S.1.f..l.f..l.e...fl i . ;.WI!.fnlrf.l..M, Iflrf'lIT_'f_i?lIl' i.' '!I IIn=stt1iw1irn'ini . S ....SI 5 iIi.w.!lli9I I..nIIZlSiolIb-fltIfHHg-IlseIiIz.hIS:I.!IZlf-::l.h1.r.u..Ia.i.ILlI.fil..w.....fd..l..:..:.r..1.gI.S.. 1I..I..l...i..SIn.cn....1..l..x.t....nI. ..si..!f.'.t..l..52i.5I.if.SidI.!Il.I.S..grIi..IIl::-1b.I:..'ls.ngt..St-..&un...a...l.:..ifIi..;-.rlS!.:....,..r...:.uSW.w.:....:l..-.ts;-...f;....nIlu...JnhJl.I;urt.Pn1.:....1:..Vn.1..E.5.:.r1S...ff1...llt.fi.fnVLl.lSl5_'tWzfTPSl.:flrES- 1 . . lu j4je -e 'I .flny, aa-. sw. p uS.1 ....s..Irs'. - . r ':1. q2HSftuI.i.w, uiI. 'sie. -vr,- I , -. I aww.anaaeNU i lit:'K.; iJ:ll::dPN!I:ffj:!! IRsiLSZ______ Ti WWIt !ic!:h:. tIRiiThlliiii :!:::::::::::::.:I._ 2 rb. :::g:!i!i ;::. IPIHI .. . i. I ........... Ii TU- .....:*i"t:tUiI ......r.:::w IflhiJH H '4: :: . --ig- ----- IMI ..,,..,. J Ill fl ! : ?fl:? -tt.t.fli i.!uIi. 73 mflifl'itjq. r' [iilL1.!:1hTg:M$lti9,Ilti!a - .J'-1::StS5 ine5ttc4r jflJ I,S _ _,. :;:::::::ui#.r.::i .. '...t'-Z 9 3 3 . .'z:'-.':. - ., 555%-S USSJ 55555 IW*i 55fl tI. . I. flfl fli*SflflS Sn I fltii.Tfr&rr wM .S l5 I 'A taup. 1,u'r$I i inq tq&'.lJfll ,i' .' i;j uS: 1I;tllIIIK' ; I' S S S S S S S S S S .5 5* S SS - 'I 'ihr1:r.12-:J:!E.."...................9..:.I.:.;;.. ''i '''K'' , :! .-.jt' .,'VI't i iI ii :S Speed Letters To l4'M 7T4 c. 2z1"c*s ,&SVC, -C'ct tra.ZJp-O &ncZ' ei.)/w 41FS, a From c. cnflflFh, ,Z'c, // &,td* J7. RLC4 6 Subject Ccfl )fljx'c9t IdIbt&ilPD Message cesana'VAM &Jc mE 4,9 Mmez.F /f 74tC frc 6h,( ,fz7E :2ev.Et7:;yflJ of ftiy?>,A,, fdflJ.'Fj/C cc2.$nr- PALm 'IV' Ct Az Syt EjQafa )..n. , &mif.ac.V1 v..'att i*t $44,flt i Cg,,q,qC 7/4r,rFprnf7 y r (cr',)' S/.nPCo) Date_'2" 17Stgned 'Z2 '.n Reply VWscnjaies nC Date Signed fletain while copy, return pink copy tie COL 00609 McCRQNE 0134 walterc mocrone associates, inc1 CONSULTING: LJLTRAMIOROfrNALYSI$ MICR0800PY SMALL PMTICLE PROBLEMS SDLID4TATE CHEMISTRY 4 May 1979 Ifr. Donald Ferry Oharles Xathieu, 'DC. P.O. Box JiM Stmnuit, New Jersey 07901 Dear Mr. Perry: Using transmission electron microscopy and, selected area electron diffraction, we have analyzed a sample of talc designated as l5onotel 6040, lot #492400. Vs found this talc to be platy and of excellent quality. Then were no aebestitorm minerals contained in this talc, neither aphiboles nor serpentines. -. thank you for conss1ting McCrone Associates and if you have any questions regarding this report please teel tree to contact me. Gene L Gtteger Senior research Physicist GRS:fe ref: 5OO CCX 3.2. Siwlco - Colgate me 5OUTH MICHIGAN AVENUE CHICAGO1 IWNOIS SOSTS $1V542-7I00 CASLE CHEMICRONE COL 00610 MeCRONE 0135 Bate 4-zo-z Client C Mt.+k j' u.. MA. Project rroo Sample Descripttnn Taifr G04o ftiny tJ lot 4t400 jX-BAY DTh'PRACTION Serpenttne: Detected Amphibolet Detected Other Thaeea Present: Cblprtte Dolomite V rCalcite Other: Not Detected Not Detected a-SIC2 Magnesite .- Mica Comments LXGW2 ivIlOROSO OPt Ohryaotile Tremolite-Acttnoltte Nonflbrots Serpenttne Others; Commente; . . total % a-SiC2 % fibrous waltero. mocrone associates, Inc COL 00611 McCRONE 0136 COL 00612 McCRONE 0137 ware/( C ,% CQjy 4crc,Speed Letter. From C. ri.or. r - zfl' Va..7& 47$. /.u3- tciVk ST CA4,j4 f44 #r'. tek Subject MESSAGE :z; ,cCe.7I-t,i,rnJ: Jwccswfa /1 It .S>t3i,rs"Lt ac ,* c,t, 1.# Li $N,. ,qro'.tr,cpe e9Ja1F1iOC.f fq,q -a C -m - - - na%Z'r j41C2F CtA'4n 7W 1ro"-a 7 4! ,t Wlon Semi conlny Date Signed REOIPIS1fTRETAJN WHWE COPY, RETURN PIM( COPY COL 00613 MeCRONE 0138 00 I00 C' a C, C) 0ziii 0-a C,, Co aT.o.t4n_ 'I"If"I'IItIIftipaa'tllaa-.is-s-.ianf,IIIa.t..l ::mnp:ilS#z;it;t"S:.tr-1r."-fr'1"r1'rtrcztt. aaa" one0o0t0ct0' 002959000 iaal._itpa l-ii 'a-Icr1:aLHt:xl.lf's. nanKttiallalaaa.xracr4.atej.snla&l .I-- 000 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I' ii IiI iIl iii i Ii II I,! I.i I I I I I I I liii II ii ill! Ii III wafter c. mcrone 'assodafes, Inc. CONSU.1NG: ULTRAM1CRQANALY8IS MICROSCOPY SMALL PARTICLE PROBI.EMS SCLW'STATE CHEMISTRY 9 May 1979 Mr. Donald Perry Charles Natbien, Inc. 18-22 BaDk Street P.O. Box AM Sutait, New Jersey 07901 Pear Mr. Ferry: Vsing x-ray diffraction and traumtlaeion electron microscopy wIth selected, area electron diffraction, we have analyzed a sanpie of Monital 6040 talc designated as Lot #590300. We found this talc to be completely free frota asbestiform minerals both amphibole and serpentine. There were, however, a few talc shards in this sample but the bulk of the talc Lu predominantly platy If you should have any questions concerning this analysis, please contact me. Sincerely, Gene R. Gfleger Senior Research Physicist GRO ft ref; 5500 cc: Joseph Simko -. Colgate 282D SOUTh MICHIGAN AUSNUE CHICAGO, ILLiNOIS 815 312/14S7100 . CABLE: CHEMIORONE COL 00615 MeCRONE 0140 I rOli Date lets I jn Seanpieflesoription (flnn;t4 cn4oYaJr MA Project SCOc j11_aX17 ,t-sqowo X-RAY DIFFRACTION Serpentine; Detected Amt*lbole: Detected Other Fthases Present: Chlorite Dolomite Calcite Other: Not Detected Not Detected a-SIC2 Magnesite MIca____ Comments: IIGwr nICgOSCoPY ChryaotUe - a-si02 Trernolite-Actinolite toM % Nonfibrous Serpentine Others: Comments: To fibrous wcflterc, mccrone associates, Inc. COL 00616 McCRONE 0141 Dear Ms. Palenik: Attached plase find the letter from Dr. a. P. Sirtiko whteh. was to accompany the 4 samples he sent you yesterday. There was a slight mix-up and the letter was left behind, Sorry for the inconvenience, Haryanne Bechtold Secretary to Dr. Simka COL 00617 MoCRONE 0142 It/f LCA XE-PALMOLIVE COMPANY 4 Vwgn cwivwthu X1,EtEARCH AND DEVEZOPM.ENT DEPARTMENT 909 'Rivur Rgw . Piscatawa$', Nnv Jim; 08854 August 18, 1983 Ms. Deborah Palenik Mccrane Assp.htes 2820 South Michigan Ave. Chicago. it 60615 Dear Ms. Palenik: Enclosed are 4 samples of Talc for analysis for Asbestos by TEM-SAED. Lot Nos; are: 12873, 12877 13080 and 13081. Lot 12873 has been previously anafyzed by your laborators' but we want to theck ft again. I understand cost$r analysis will be approxfmately $350. I am havtng a pureMse order sent under separate cover. Sincerely, .3; P. Stmko, Jr. Sr. Section Head Analytical Department JPS:meb cc: H. Schubert 3. H. Callahan COL 00618 McCRONE 0143 r0C) o0 Dr. j P. Simku, Jr. COIGATh - PALMOLIVE COMPANY fl flew S.d a Pit.naq. New f.t.c - USU C Sic.. - .. S..4c,.... tcj P- Ms. Deborah Merit Mccteie AsoItates 2820 SOUth Mtcfitgan Ave. Ch1cao, 11 60616 Ails 22 83 - 7g.' PROJECT TITLE: SPONSOR 09O4&O ADDRESS; flJU LU A ,tJt AILJl.,VSfld I. ESCA COLGATE -PALMOLIVE COMPAEY 909 RIver Road Piscataway, New Jere ey 08B54 (ofl)') PROJECT NO.: MA 55QQ DATE RECEIVED: 7 3d 76 P.O. N0.r COMMITMENTS: $ Contact: Telephone No. (201) 463 1212 SUMMARY Q)i PROBLEM: Lab Notebook References: No. pp No. pp No. pp Photomioro " "d ,nn.Wnr --?1e dispoaal: med (where) arded thividuai Date S+ or iC N V\ a qai.90 AI,1.3%%EJflt\ 4nr+ 1 Ic&g U tka\ .u%tstku3 .... ai' C.Cet t3.kp& /M'4,5Jtox OIV. - Charge Summary oat mdtviduals $ / Ins trunient Travel Other Cost Total Chant S OR for billhig Project TAr GroupLdr PBOcux juwujsea ROUGH DRAFT REPORT RECEWED oo .tettS teCoU'3. 1. BThLD To CLNT $ INVOICE NO. (5) COL 00620 MeCRONE 0145 kilL r$A1 waiter c. mccrone associates, Inc. CONSULTING: ULTRAMICROAMALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STAlE CHEMISThV 27 October 1983 Dr. 3. P. Stfro, Jr. Colgate-Paimolive Company RW Depathnent 909 River Road PSecataway, New Jersey 08854 Dear Dr. S; This letter concerns the asbestos amalysis of three talc samples labelled 12873, 13080 and 13081. Sample 12877 was frund broken 'when the sample bac was opened end coul.d txt be analyzed. The samples 'were analyzed by trwasad.ealon electron microscopy. thrysotile atheatoe was detected n all Uwee saripl.ee. The was not done quantitatively so no attnt of athestoa can be determined. Thank yvu for consulting MeOrone Associates. If you have ar qusatiens please do not hesitate to call. Siacerety, Deborah P. Palenfic Mgr., RI "tron Optics Gi.uw P:fe Ret: 5500 2620 SOUTH MICHIGAN AVENUE CHICAGO. LLJOI5 00616 3121042.7100 CABLE CHENICRONE COL 00621 ,McCRONE 0146 Yt7a -r !Sc/O-osVC)-C I *\1t -% -7Zvo .-t4 4Ltfl ;tr?y /3cm -9j3o?/, S4.np&/fl7& A?-V&O ctj a-wiI - d7tA&t1 nSr tec TIC trc7tt -"- COL 00622 MeCRONE 0147 COLGATE-P4ZMOLIVE CO]MPANY.. 4 Vt/nm Cfl.r.14s RBSLIRCR AND UEYELOPMRNT DEP4LTM liNT 909 River Road Pi:cotaway, Ncw Jsrssy 0t84 'Qatob'er 31, 1983 Ms. Deborah Palehjk, MoCrond Associates 2620 outkJltchigan Ave .CMcago, 'FL. 6G616 v. .M;s,;.p.a.leiilL. . . .. "nciosed.tsa i1.ngle talc swnple.Lot Wo S09063 for analysis' (by..TM-SAED.for'asbestos. Pe4se expedite. thit *nrt,. A..PWtM!4 :ft.er?No.; is.belng'sent separately. .. . .. .; .Mapy.thanics Stncerely .1flL44!t. Dr. O.'. Stm /t ar. 'cc? W. S,bhubert C...' Sthwarz E-1-5 COL 00623 MoCRONE 0148 ORIGINAL PURCHASE ORDER unm05fl742 1- /&4f4L tc"':'.T C,, COLGATflAZNOL!V4ffj47( . Shots ,ii numbr CiG42! ftc'% DAYE/,/3/fl HIP 10 1M; bIJitiie 4tcbfdd ' '2oa. stut eltgd1t AW&tt cMpn% 1t9 4,' iii POtwIflyI D. PISCATAWAY, N.J. *0554 II ltP.MaNnfl. I V CITY,N.J. 071*2 I IJRJItCflEER,VPmOoNSYTIALTLIEO,N. INDIAWA O'I20 I I iI$KtACNtVPIANSDCSITtAYT, IXOMNl. (Pill - DISCOUNYTERMS 4IPflNG TIRMS WANTED DY 2/il) N/al) 2 0 i/to N/3O 3 N45 504 N/30 S NETCASH 1 FOB Putln*%Ion 2 OB6hWlIIPt Th.#yflM) &. &row 3 U FOB Supping Pt. (CactI OILy MaIS R.c. Pit! Code P103se Bush IP ABOVE DATERNNOT BEMETNCTIfl 1nucwfllAi%iooa; :A'n: ug Cled you IAftHOIIIIIO TO PIJINISII tIlt ANTICICI LISEO I3I!*$ IN ACC0OANCE WF1*T12 flR4S *1W COICITIIIf0N.TIE FACE AID PAtIO TIlls 050CR. .........................................QUAMTItY MID WIlT SYMBOLNUMPCR . . PRICE 1 ca. Tale Sanpte for anabvais for abostoss a '-. " ' tst apj'rox. $35" tfetco Thib to a one ttfle reueat., Bamptea sent uaer separate "#<.. '66 14 flebt1fPaIeuLk et Mdroue MsocXates. 1 TAX EXEMP1 VEMOOR IC PROTECT ALL METAL PARTS AGAIHST CORROSION WY SULnSL,E PROTECTNE SE&LD4G. SEUZRS INVOICES that h,dvd. autlrnriad Iran.poltafloo d.org miS be auppori.*y propald freIghi billorCOLGM'E- py ef erlpkol WV 0 Iodlnp. MARX PAWOE$ wIit p.1db,. order number, symbd nsb.r, cds.qfl ad untIIy. AwpIntP of tMs aid.. Is be dennd a cwtlflcaftop that you Mv. rood aid apn.d I. Jim I.s.o cad coitdllloeis an 'Ii. Miii hereof. PAYMENT Wilt N0 SE MADE ACAINET PRO FORuM INVOICE. ..DNc ...............t...i.gt3-,;SERA By t:t-i3k-1 ' 4s r ?"'rit- 1'1"M4iftf&r44&-l' COL 00624 McCRONE 0149 MA: tEtEP&ODUCtD I--I0.e-%d' ...Nfslt.md-a&'WflwtJ.tsbbyWMiiawa#d0"e1. I nu*sec..w, ucma MisAYina tilt ul Nm; 3,rny PMPWk 0 tAnnaw SIMS TAX mtn'T usu tUZACA1I FSM ST4 Put DM11. 1$PWAII iw 011105,,, tlI'M* 131- 815 -ufoo Da 1/13/13 ............. a The uae.susd ,..Aiar ,,dts, iS Ii 4 nut veqvksd Ia pip thu Sew Jay bbs ndfw Us. rci the pitt. at ,...S. .4 k# ihk CIvIIISNhreis Iii isilk pvqpiy .ihuesdw*hsvwdfw.r tp_.... 5nc.ldopsssWtdapstsl*qodfnlfIl'&d4pSWieapIc.Stts3y:SweiMlIt ebeJwfa1ladsilOniT3tyheis .at ss.w for ua naav* aM Mn3zus.. a or the rTh. .asvipan ii, Sis uS. .1 spud iuifl'. pepetip ii he used foe the abs.. deoSbed e*smp putposeh iw -t NJ.LA. 5Mfl.$j a's.. inn. dSp # pad p"kinnd gas if suiupuSs asud 1 M Ms US WA pepw .s'be.cfIsa eNsNs.Z I, the undwslgn.d purdiaisr, have reed cad isnyhid wiWi the lasirawice, and rules pwaaed put. sueS Ii the P4.w Jsnu' 5.1.. end Use las Ms w4tk ruped I. the as of the larnaipi U.. Csqttfleaps, and life my.WIIV thee the ,sn4r nun'S Scala I. net ruked I, saInt 11* Sn av us. Pan an ike Ironict lIen es VQSSOISeIs wcnd 1' Wile Coam_i,.. 1k. 'se.decsjapd purduusse husky swim (imS., ii,. pIa&I5s fee psrfury ad Vole. swsnIag Its ultef 5h MfIvn,eltse, pliewn In this CatIft,atj Is Ito.. uir,nI 5'. / ajanrENIOR BUUR CkITBAt, : t I' :c411, a X05 BDDSCSI at'., iXBt CZTY, N. 3. 07302 (Equaerr WRCThABmG BSCTION) I COL 00625 MCCRONE 0150 . I -.--. ttiHJHTtttIT4 h..js V 4..;.,. :..' II, -4).....Ii r -'---k+-i---------- F---i----i-- .4............ r-_--- .i t---J--i-I 4 1-H}-1 Li -.......4..............................i.......-.H.L--.-.HL-.1..--*t-H....4..L.H.t.."'..:.tL+..!-..t..*..n................... -I--f -H--- .f.Ii.?_---------._t L LJ_ -- I ...i.. I COL 00626 McCRONE 0151 LYYA TA4A! waiter c. mccrone associates, inc1 t a CON8I.ItjING ULTMMICROANALYSIS MICROSCOPY SMALL PABTIaE PROBLEMS SOLIPSTATE CHEMISTRY t6 Novatjber 1983 Dr. 3. P. Sinko, Jr. Colgate-Poimoltve Catipany Research & Develornt Departnezxt 909 River Road Pisoataway, New Jersey C885I Dear Dx'. 8*o: This report stmnarizes the asbestos analysis ot one talc saawle labelled tot #809063 which was sent to us under P.O. #633715. The sample was examined by trananission electron microscopy and no aabestcm was detected. Zis technique has a detection 1 lmtt ot 0.1% by weiit. Thank you tot' conaulthg Mcdrone Associates It you have any quentions, please do not hesitate to cell. Sincerely, Deborah P. Palenik Manager, fleutron Optics Group Dpflcb Ret: 5500 2520 SouTh MuCHIGAN AVENUE. UIICAGO. ILLINOIS 6C518 51V842.7100 CABLE CIIEMICRONE COL 00627 MoCRONE 0152 4znzt&= 4&-ao tsu 2cA' S -it5 ooS am4& Qlri-</C4LAs-cAIa% s2'/ t.tt4 .3? o9 b' CL9a4C. (C COL 00628 McCRONE 0153 I M. Jj ka . I COL 00629 MoCRONE 0154 COLGA TB-PALMOLIVE COMPANY 4 Ddmon nth,s ZBSE4RCH AND DEVELOPMENT VEP4.RTMRNT 90? River R#4d Fiscat.watj', Nw Jerst 3$4 RECEflD NOV 2 1 isis November 18, 19711. Br, lati Stenai MeCrone Associates 2820 South Niohigaxt Avenue Chicago, n 6o6i6 Bear Ian: Snc1oae are tbvee aaavies ot talc I wou34 like anai.yzea for ebrysotils aM tramolite using T$}( eM SAED. Sazwies 'e iabele& A, eM S. Charges tcr this work shotad caray our pttroh&se order No. 6s768. Sincere .1 cT. P. Sirko, Research Associate COL 00630 McCRONE 0155 I .31, 13 It r-"A" PL A& A44+Mo.az& L' % .. '1 fl'LtAJ4&4,&3. aa2fl I :. ;..' ORIGINAL PIJR.CKASE OP.DER 0S2174 . 'bow this ss,w6sr nivolcn, ching xZifr.z 6)2760 COLG4TE-P4LMOLWE COMPANY A DElAWARE CORPORATION J1p-',cceiV,105 HUDSON STREET. JERSEY CITY. N.J. 07302 ATTENTIONPCI KoOrone Associates 2820 South Michigan yenue 4 Ubicag, Illinois 60616 I. InsCO U NT TER MS ShIPPING TERMS I */10 Nt'30 - I [lyou u;tIoatIoo, 2 N/aG 5 3/10 It/3D I alOash 2 I'OS Shipping Pt, .' (A-..Pty& Blll)So.B.kw 3 0 rue ShlppingPt. (Collect) WANTED BY LW' C V , Tr*de CII)? YOU ARC LOT 117CC TO PWIIOSN Tig ARTICLES USICU IIERCON IN ACCORDANCE 111TH TIlL Tfl115 ApID CONDITIONS Oil 1' IMN1'ITY AND UNIT SYMBOL NUMBER ' SHIP 'TO 25J JI. OISEENK ST. CR5EY CITY, N.), 57305 l4It ID*PRIOICVAETRAWRADV.p NJ, 05514 is.I Iijsmoi.LVtM; NJ, 07102 161 !IRJEEFCFEEIVRINSOONSTVAILTLIEO. N IMUMNA 470Db, I RECKIVINO STATION I KANSAC CITY, NAN, 0*05 22) J1I7E*R0IcflERLLETYO,SCSATLIF. t4710 Rot 1In)0N0 YPOARRKKA. NVEfl.. 10057 2511 A'rrN: It,c.iV ig Curt PACE AND PACK OF TIllS ORDER PRICE - TranStission Electron m'roaoo1q arid electron dtftraction j anatysis of three tale saapies for ehrysotile wid tvo1ite - NOTE: This Ls a one Ujue ordS for A specific 4o3s - address as above: - , / ... - Attention; Dr. x; StoveS . g TAXEXEMPT ' 1 / MENOOR'TO PROTECT ALL METAL PARTS AGAINST CORROSION ST SUITABLE PROTECTIVE SEAt.lt'JG, $EttEIRVOICIS*ct rads. arIt.rtadfmmpbda5oi cLasses, mat beLnppolted $ pupdflrsleld LW o CO cMeodApwy(heMtFoQ.dbgc.l4adqu.!.EnWSdUwuolilwtahdflMp.ewa5d.n.et,axtJ).tjujjolesaibvn,Ey.e7Sm.5boetgEv;.m.dbt.ol.te.ibaTZdci aods-i,-ioMsci.poMaatheslSa BY PAYMS4? NOT U MACS mAJPar PlO ?o!M INYOICL -, VT 3v' 1-v -. NEW -fly - -- SAtES TAX WJST US BILLED UNLESS Xgz4E'TED B! AnACIIBD CERTIflCtTE. COL 00632 MeCRONE 0157 1']tOJ1CT COST RECOI1D PROJECT TITLE; 3 tale samples SPONSOR: COLGATEPALMOLXVE COMPANY ADDRESS; 909 RIver Read Pisoataway, New ersey 08854 PROJECT NO.: MA 4426 DATE RECEIVETh 2 74 P.O. NO,; 632768 co1aflTTaENTs:$ ConLact: 3. WItrak Telephone No. (201) 468 1212 SU1WIsIARY 01" PROBLEM; Lab Notebook References; No. pp.____Initfals_ No.____ pp.____ InitIals No.____ pp.____ InitIals Photoinlorographic record no. Sample disposal: returned med (where) discarded Individual time (Exclusive ci oper. time on that. below) Date Name Hours Charge DIRECT COSTS Travel bate Traveler Destination .. Instrument time Date SEM TEM iCB3) EMP IMP ESCA f-l.ours Char:: Outside Services Ite Thoth Photo teriats Supplies Co . . Charge Summary Cost Individuals $ Ihetrunient Travel Outside I Other Cost Total $ OK for bilftng I Project Ldr Group Ldr I PROJECT LEADER ROUGH DEAn REPOBT RECEIVED IMS TOTAL CHARGE $ BaLED TO CLIENT $ INVOICE NO. (8) COL 00633 McCRONE 0158 4' - 10 Desen*br 1874 Dr. J. P. almko,Jr. Ceg.t-Pabn.1tn Compaq 00*flkirfloS .Piucalaway, New 3r087 OS 154 Deer Dr. maSt UsiSsbegpthees4eAofttlo$a&to*ns. we bay. flalysid thrO safltpsu of tale ldee.tIMd !"t"'' be4SSfMtlmuS. Atuhef$nl*tf*llA*astdhtwtno f$ib0e tN%If jatbItt.flsa tw1d4 are mtoj.flnAt.w -! Sle Ma ner.s5 three 1*00 atIat Thin trS$.SS. s*ri4 then s $* *t'iP ehowM film m$nl*lnthS ibu*Ie *Mbi*tS*tI**eabn*. *IiUitttsK be0Ht1*$fl co&flfltflUDn oXitwna ps. *, flth no thUS. z*$sb& S *athtrfelulS*adMksfl. -s fr4.7* L- a$ft#? Wit aitd_g-e'*t were ig eM flbntg, - 'Ss aUiSML; S 1*0*. Thu ' m$nS tu a fllbw fl *Zb.* were snm$s S 'uflc - cont4er the. arcs we Wk$ at. *nti,. it *pe be I *1*4 Ioaf* *1 sapbth$n COL 00634 MeCRONE 0159 I Dr. J. P. Slnilco Page Lwo 4D the tal, mine. Sample. P and 8 showed no ampbite*e. mt did show larger plate, of ta2q than sampLe A, whiob nmpie P elsa SWfrg Wfl amounts of oqaidc EaM.dt1n.. 'j%anc jot for caaeultifl NeUrons Asscui*ln. U there ire aiy qflptoes ecnqenI this repast it the dda ooat*thfl hera, pisaso Mt ins to Vt! truly ,ttta, S enelestres re*MA44S8 GQ*L tier 51*5 *toS*.b Pbyelobt COL 00635 McCRONE 0160 MEMO FROM GENE GRIEGER. co)cx r0CD 00 C' MEMO FROM GENE GRIEGER c t COL 00637 ft McCRONE 0162 C, McCrone Associates, Inc. swnple A-I ShED COL 00638 MeCRONE 0163 Walter C.. Mocrone Associates, Inc. Sample A, o. 1 (5GI) COL 00640 McCRONE 0165 9, Walter C. McCrone Associates, ific. sample A, no. 2 (5OiC) COL 00641 McCRONE 0166 00 COL 00642 ,McCRONE 0167 COLGA TB-PALMOLIVE COMPANY 4 Pdsa* G'frethn RZSE4RCJI AND DBVRLQPMBNT DEPARTMENT 909 Ricer Read Piscataway, Now for::; 9fl54 January 28, 197b Th. Ian Stewart }6cCrone Associates 2820 South MtoUga* Menus Chicago, flhinois 6o6i6 Dear Dr. Stewart: nctose are three samCLes of talc tick vs want ans3rzC for cbrysotfle and treinonte. X have discussed thcse with you by telephone and I went traastssion electron inioroacoy awli .ectron dit(rsotion 'analysis done. Charges for this work should car o purthase order ro. &95% yIf I can be of amy aanistaace pLeas ontact me tncereZy, (2m4 1t63-1212 ext. 379. 3. P. i43*o, Zb, Research Associate v S. Dr. $chneiber of our carany Las not received prcwised flberat,re. .t 51374 COL 00643 McCRONE 0168 PROJECT COST RECORD PROJECT TITLE: Talc 11S1'81H PRO3ECT NO. MA 3805 SPONSOR; COLGATE-PALMOLiVE COMPANY DATE RECEIVED: 13074 ADDRESS: R&D Department P.O. NO.: 614958 900 1tive? Road COMMZFMENTS$ 2-800/san Contact: J. P. Simko, Jr. Pscatany, New Jersey 08884 Telephone No. (201) 468 1212 X 379 SWMARY OF PROBLEM: Lab Notebook References: No.____ pp.____ IniUals_ No.____ pp.____ InlUais_ No.___ pp. IuiUais_ PhoInmcrographfc record no. Sample dthpoaal: returned filed (where) discarded Individual time (Zxotus lye ot apex. ime on Inst. below) Date Name H Charge DIRECT COSTS Travel fl Trivejer Destination Charge Summary Cost Ilidividuala $ Instrument time Date BEM TEM XE]) EMP Thil ESCA PROJECT LEADER BOUGa DRAPT REPORT RECEIVED ifours . 1MB Obarge Outside Services Date Photo Photo 1&ter!ath Supplies Company TratBi Outaide Other Cost Total rh.-a $ I DXC for billing Project Ldr Group Ldr "I TOTAL CHARGE $ jS V BILLED TO CLThNT $ INVOICE NO. (5) COL 00644 McCRONE 0169 Mr. j. P. S$,s, J1 cd$ate-Palm.Un Coapny S and I) Dip 000 RiVet Ro*4 flstsw*y. NJ OSM Dr Mr. Sln*os ,4awe bs$ ftoibed our analj'ais of your nmptn dSjlpatsd 5$. Caibmera Suegist, C. EaflI. lb the sn.fi,E S we. it Ma$1$s Lw*',ur. akis*l. Wa debctad tfl 41 of thot. W io% a*paa o**t a de$ vM*as.aet present btbi$tnywbatniItm1 a*iak r#s.rI'-$$t*a,aio$4*vz#$S:IOksOo$fplt.ttosstg0M1t%s0h0ea bOWL CSnte*S IWI**I44*SL 4* C. 0.0CM to t..001%. SuIg_os thaetosvg*#s t WS*I tbt'hi.s*I.niatt$o. Rspre%S*- you *lr flw$tl$g Mocroms Anoeles. if you bs,e say q*ssMa please do ,aatbuitt. to.dIL Sans' SW. neZ *ISeII*C1I t1e4ittja COL 00645 McCRONE 0170 p L4 COL 00646 McCRONE 0171 Walter C. Metrone Associates, !ne. Casbmere BOUQUBt Chrysotlle then (51,000X) Walter C. Mccrone Assooates, lnc. COL 00648 McCRQNE 0173 Walter C. MoCrone Associates1 Inc. COL 00649 McCRONE 0174 &A' ,a. I' !. 4, 1 a .: .. . St "S N.C. Regal, g oral 1ew (51,000X) 0 .,-,-w---,..----. ---.----.-.. .-..- ..__._....-,. -..4.._..2..__,._._.....;....,..._. :t. -. Walter C. Mqcrone Associates, Inc. COL 00650 McCRONE 0175 Walter C. MoCrone Associates, fnc Wafter C. Meemne Associates, Inc. h - '4 4 r. . sw:;, V. .. . - fl* 4 _44 - 1' Wafler C. MeCrone Associates, Inc. 5,-. a. MCCRONE 0178 COL 00653 k. a 516Chrysotile fibers (t,OoOX) Walter C. MeCrone Associates, Inc. COL 00654 A MoCRONE 0179 ITAUAN TALC AGENCI3$. / Sot t.Zco B GnAt Vii aao. $odes. tlws T&c !ndco Thou $ 0. PinsaS (Roles biy) Iegbni. ttafr 0.4. Baldaccu & bliposo Todno C.ats MDnss "MAflUOAR" A. LC.GODZ UJSD CHARLES MATHIEU, in ED. BOX AM 18.22 BANK STREET SUMNIT, NEW JERSEY 07901 ItSPRESENTATWE ZR IJ.S.A. OP POBMON CW!B (Z01) 277-0510 January 10, 1979 Mr. Gene it. Grieger Senior Research Physicist Walter C. McCrobS Associates, Inc. 2820 South Michigan Avenue Chicago, U. 60616 Dear Mr. Griager: Confirming our telephone conversation of today, enclosed please fisd a sample of talc marked "Monital 100, Lot 881800" which is a new source for the Colgate Paimolive Company, their specification No. M-6277. Please test this sample with the 'anal CTPA J4-i. method and report the results to us and Dr. Sinko Sn the usual manner. Thank you for your cooperation with the above. Very truly yours, CHARLES ?IATUIBU, INC. DEF Sb cc; Dr. ti. P. Simko atflos cn$u$bb in Jdmsfls Isi.nd by rinks. Mswiato,w tnt CIItfl i*tUt. SofidSons hyind or inn,!. Vista l'isrd len wdatMg tcfIf is nd aistnl nph$kns. COL 00655 McCRONE 0180 wafter c. mcrone associates; inc. COWSULtNG: ULTRAMICIOMALYSIS MICROSCOPY SMALL PARTICLe PRO8LEMS SOLID-STATE CHEMISTRY 6 July 1979 Mr. Donald flrry Cbariss $atthieu, Xnc. 2. 0. Box AM Bumsit, NJ 07901 Dear Mr. !erry: Using x-ray diStraction, tranmisaion electron microscopy and selected area electron diffraction, we have analyzed a sample ot Colgate talc, designated as tonotal 6040, Lot 592200. X-ray diffraction 43.4 tiot detect either amphibole or serpentine. We did, however, find that some chlorite, a trace of c-Si00, some dolomite, calcite and a trace of 7nAguesite vats present in This talc. The results at our electron microscopic exmnination confln tht there are no asbestiform minerals, amphibole or serpentine, present In this sample either. The talc is platy and has a wefl-characterised crystal structure. manic you for consulting MoCrona Associates. Very truly yours, GEG: 5mg enclosures X&-5500 Gene P.. Grieget Senior Bssaarch Physicist 420 SOUTh MICKIGAN AVENUE. CHICAGO, ILLINOIS 61616 512/842.7100 OABI.E; OHEMIOR0N COL 00656 McCROME 0181 ;Jw79 .?A 5QQ )A; Pen Q$xies **eIS'c. a ,.ke. rii I '--/ S '4 - I C - -- . 1- -I -* -C I 'c-: '. - .r- -.'--. .. I, r '.'.Vt?-,A -"I - ' --I'-' --_' 'I I I- .1 I "I - -k,'-- r - r1. I, -I . I - II I.,- t.F' 5 -' ' I-I_I - I '_-, 'I - 11I,1r ?Y'Y :, -' r :- COL 00657 McCRONE 0182 cizent SampleDescription a Date - 71' MA Project croc ,V0;+0 1 4Mo; 't.,t Senoc X-RAY DIFFRACTION Serpentine: Detected Anphtbole; Detected Other tases present: Chlorite Dolomite k Calcite 1e Other: Not Detected Not Detected V v a-sb2 w" Magnesite '(hity.itoa Comments: LIGBT MICROSCOPY Ohrysottle Tremolite-Aottholite Nonfibrous Serpentine Others: - - 2d total % a-SiC2 % fibrous Comments: wciiterc. mocrone associates, inc COL 00658 McCRONE 0183 4-. rn waiter a mcrone associates, inc. I CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PMI1QI.E PROBLEMs SOLID-STATE CHEMISTRY 6 July 1979 Br. Donald Feny Charles Natthieu, Inc. 1'. 0. Box AM Sinnit, NJ 07901 Dear lit. Ferry: tsbg x-ray Aiftraction, trannUseton electron microscopy and elected era electron &tffraction, we have analyzed a sample of Colgate talc, deeSsnated as tacactal 6040, Lot 592200. X-ray diffraction did not detect either amphibole or serpentine. We did, however, find that some chlorite, a trace of a-SiC , some dabmite, calcite and a trace of rsagnesite were present in his talc. The results of our electron xnicroaca'ic examinetton confirm that there are nc asbestUon minerals, amphibole or serpentine, present in this sample either The talc is piety and 1158 a well-characterized crystal struettire, Thank you for consulting Nctrone Associates. Very truly yours, CRC: smg enclosures m-5500 Gene B. Grieger Senior Researeh Physicist 2820 SOUTH MICHIGAN AVENUn. CHICAGO ILLINOIS 50018 312/342-7100 CASLE: CHEMICRONE COL 00659 McCRONE 0184 :Ctc jj/ Ad /0 cf 0 c7b49pCA'ra-nt'-rc-a-s'*Icri/a4te i2c ,4Z c.ra t atta-A te-M&- &f t>/4( -w-nn g F 27' K-47 tan.p ae-ea4# ,a4rsue2 ...%'>tf$L .s-cLcc 0 - - -t sC. A- .j 47 '-'I- &,&a Or str2 17 4-cC. gc tl a-d-t S.-, ta.'4 e- (V r3. COL 00660 McCRONE 0185 riwaiter c. mcione associates, Inc. ACONSUtThG ULTRAMIGROANALYWS MICROSCOPY. SMALl. PAETIOLE PROBLEMS. SQUD.STATE 6 September 1979 fr. D. K. Ferry Charles Mathieu, Inc. P. 0. 8n Summit, New Jersey 07901 Dear Mr. Ferry: We have completed our analysis of ta].c Monital #6040 Lot 791000 received 1 August, and find it free from asbesiform udnerats. The talc was examined first by x-ray diffraction which showed neither serpentinea nor aiaphiboles present. An examination was then performed by electron aicroscpy combined with selected area electron diffraction. %lUs exaaipation showed little evidence of fibrous naterials present. High aspect ratio particles observed in this talc wets identified by electron diffracd4n as ri'bbons or shards of talc. The majority of the talc consisted of good, piety talc. As usual, it you have any q'*esticns on this work, please feel tree to ca1 ins. Tours sincerely, Ian N. Stewart Nauager, Electron Optics droup flfS:fe Bef: 5500 cc; Dr. J. Siako - Colgate 2520 SOUTh MICHIGAN AVENUE. CHICAGO, IWNOIS 00615 EZ'542-7100 CABLE: OHEM1OROtIE COL 00661 McCRONE 0186 II Ir . Ij- : -1Milr- !!R!t ?r. -- fl_ flatSi J S$*U 'PsqIn9huu: nia 2PfflffEIrrn5 at_a .ial -tt tji4Lupma.a.p5n nflSS S Va-ti /, . it_a MU. ant- _:-- ..a* -.!I n ,,a*a.*r.insa. aMfl.an..wanwasa n-I. -.dflanNn..Sinaaansaun..i*ja Irqsnaansj.antnascasats.I aFtan.*.nflflIflnaaan- Na4aFn flaNagan -. an a__n !ff3rt 0. isa.....: U5:. ..---- .---------. 'ft fl5Ft..... ins- fl_S. an iip*5 ISS5SflSfl :'La. Cr--. .i.o,ia a n . fl-aSIa -* - --..a....I. ..a.... . a.....I .iSSaaanafl i.fltflfl55S .5aia45flflfl 5fli55 ......s_na ......_.fl_._.aa .. t_ -. In 0 a SO _. . ................. . 5- .. .3- 4 . Saa4StlflflM - . mitt-E-'- .-,_. -- -------------Ia O'4 . .... .0 . ,- 4 .) ... A 5 '5.ao t.4 - 'a , 0 "' S !1ph lasar Sa55flOaa a................5 Ia...... I.I.4-in... I.............a :j::::::::q3h. . 'ai- .......... ............r N .saIs.aan5q5......................... aas-...................- a- .. . .......SaUaaa._ ..----....a... 4 SI p I ..."a SS isa .a. Sa.. a I ..::: 4kvunu a a: .. ala 141.....IaI-saI ............a. .aaa :a' :,aV Sir ass flNN '5 It .5.55 aaaSai a.*a.aa0.n fli Si 145 S5'.......saua.aac, noaai..... ....- anal. .....is ...S *Piia.5N55515..a - F_:cua.. Eff ir. ibr 5 555 all.. S5I ... r I.. 1 :::u:!' aS a I........a5 I I a. Ufl ,....... iu.uiNIiIIIrn.,!. :.uuAnz:: :::::n:.u:% a5ta. !npSasa ....Sn .a rE a9aaa an............a.-.l.i.S....n.s.a... S ...nani.l . -......n ... .0 anu._.nal ..a. 55 ................nflaaa ..aalliflsSaafl-fl.b4...an a. ...4-.a5S.....- a.....n.as aasflOaiflaSaaaaiSn Ia-ia .......ii..in....., S 5a.g 55 rnaI,1Iw:::IIMl.1., ai a-ai. a. Ufl.fl..uinfl.P.a.l 5..as....-a. ......,.,...n .....fl..nflfl.fl.nS,flfl......lahk.t_n_jafla. .e...5.....aS.. 1::::::i:u1i$8.j5pt9 - .....a.a.....n..i.. ..........a...-a . E - -& -. N'I !S 111k . ......sqil -.......a. -sa.. 45 nS a flflncj..1.-a-n p.5S bflfluct. a'sa ......I ...a-..nI S. ...in. .nS.iss .nnsaan..flifl . nsa.. .a.- bafl.N.nSofl4alS . .......ct-u.n ---------,..........,........a...fl........n.. Saiflfl..fl.Sflfl.flWI...flh..II.P.iI .4$44........ I.. . ..an'.n.nS...n....afl..nflSn.. . ..IEF!i!!-ail!!.r.rt . -. ... -. - .. . . a. .. fl - a. s. UI1 i a .............-a- Ira......in. 5r'giri. aSIUI - ...a. SSflSi ,155&n.PSI5 : ., -a . S..Ia .......I.p 15 si 4I a- rIua. .............S ..... iLrI! en a alan a Ia-. I-i-a SIibNraa :;::::!IL:.v:;:::E:: a59.5 'p.........Sisa..fi.........55_a.- ............ .......5 S 5 SaSSi.a..... Sail r U.' 91..l...............1....... i:11 !:_; .--;va;;p;....ih;:T:...:.. I .............................5S a a S ...ia.i a a a..',. .a ni.aa.s...na .....a-.ia... ..a. ....a..................In. ............4 ............................a .Jn ...... a I.........aSfliaSnflSt. ii ..055. .aa....a..aan...flhlaiuli..l......i#aia...ai. a In. ............h...a.I1..................Lnj Lp. .11I.4Sa..alfl.lai.flSS%.lS.k.ia - lanai U{UlZaIU9fl{a 15adLhn!! a;;:;;Rl!kihXirf:z!:::::piEna!..h...i.u..aj1..unna.g#au .SSS a..- ..... n_.sea .n.. I5SWt55S ..ttai..ail 9IjflhIIHui -.. .::Ia--a...........- usa - p .1 Sn . na.. '.1- - a. L. 55. ar ....ai.n.a. ns.n.- a... .i.n a... au 5SflaflflSal ssSssaS 555...S.aS. . .. a-.. ... -. z...r -- . . . . 1.. . a I L91.O JWOUOV'J Z9900 '103 Date Client C fla+it 1 e, /S-i c. MA Project CS"Oo - Sample Desortjtton Talc, }ti nst +aJ 6o40, I,,tiioon X-RAY DIFFRACTION Serpentine: Detected Amphibole: Detected Other Thasee Present: VChlorite VNot Detected Not Detected a-St02 DolomIte Calcite Magneette Mica Other: Commentst LIGHT MICROSCOPY Chrysntile Tremolite-Aetinoilte Nonfibrous Serpn Otherat Comments: a-sto2 taM % % fwrow V wailer c. mccrone acciales, ho. COL 00663 McCRONE 0188 WALVZR C MCCa!)N ASSOC. XNI z8a0 soum NICEGAN AVE CHICAGO, ILL. Gt$16 SpeedLetter. I LE*Ao From CYPRUS XNDUSTRLAL HINEBLL$ 631 NEtUCHEN RAD SOWN PL*XIWXBtSD, N.J. 07080 SubjoG -j.nhi.rmo MESSAGE jc'L Gentlemen; flialesed is a eai1e ef Monoblena Talc 14-6277 (Nonital mis) for cct19 sour routine Snycatigation Lor suborn ainerats for Colgate-Palms- live Co. Pleeae piefozt your usual work Dfl tkis z&mp3e aM rornrd the results to us with a copy to J. Sbnpoo. nspw atw Datu Slgrwd RETMP1 WHflE OOPY RET1! FIN PINK cop? 676 COL 00664 MeCRONE 0189 Date /O-fR-79 Client ivo(ttc1i?o,f ut1flie,o/c MA Project .rrOo Sample DescrLptlon flk.. (}7-C,t77, 2,fr /OI3oO X-RAY DIFFRACTION Serpentine: Detectec Not Detected Amphibole: Detected Not Detected Other ThaaS Preaent Chlorite i.- a-Sb2 DomIte L- Calcite i.- Magneette &- Other zMica Commenta: LIGHT MICBQSCOPY Chrysottic . Tremolite-Acttnollte Nobroua Serpentine Others: rt . % fibrous Comments: waiter c. rncrone associates, Inc COL 00665 McCRONE 0190 '49 Figure 1 - General flew of talc C22,500x) wafter c. rncrone associales, Inc. COL 00666 McCRONE 0191 L.;.1JJ .IU HJI) Li pa.fl-S.. nnnaSn.a.ft5JIl7,InSff;l.,l.a..nS.#*.Enn.-t.frl.a...-S-.rn..StP.s.lIWapf*l.lnlf.ls.n*.s*.sI.nrfnnla.,.anhns.s.r..nInSI.PsC) 000 ...t. nst ltl.a. nuanlpI1J555J1C' inu'"0 IU5t5t5 S...;C-a' 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$*_l)5Il.sSgII1Ilfa*.lEjlIInLsiSntIk-illtF!aSl11I5St05-l,t'*I.ItPSlVJul1fIf5ISlIt.fta-'in_!Itlpia.n5I*f,1*N1I5d,1tStIaWaltl5l!IPu..nSSlltia.5I_IJ5iOns15.t_IihfnI..JSnIlPP.I5.{t.Slttp1iIfnnl,f%.5iaJII*S5mn.ulf*fI.aiSlfIgtflii15s*Pl.i*S.f1f*5Ikl.lpIf0.5JS.l.lIl.SfsI.5pS.ahwa5SlnlStfitlnO1,hSSnasfIS..nnllf5lfa5PpIh1lw*-*n.5iSIIfl_IJlIlf..*.'Saf.Iillnnt*5w5kiflwP.nmlEa5-nPflS_.awI5flpnliSSf.nSffI.Snslnl01fwln*f4nSSs5Ifltf.sSfn..lln_.h*n.5nS5illnla!aS5Iin.lsunlfalnis-...nS*nsEllI.t.tf*.!iWnS5nalPnl*ffSo*fSa.naW.5nPfnfpSn;fsPlPfS5nS5lxlinWIl*tnlrsIlpl.$snifalf5ISlfaCI05*IainfIltliSfnSlrffIftfnlSifaniS*I1anI.ttaSn..iS*IiiRnlllsfSll-.W1aI*nfstU1tP0lI.hstnPSI.nhtlsiSa5s.Il!jO.1fnf*t.SiI5..Psttnf.In.sIlnW..l,in.cln.5:.sIf-SaPlm1*tnl5IWIIInna.nf.s.ZIU.lIifaPif.SaI11ft*5P.xPI5nlS_u5nnl-ftaISfnnlnl.ntf5.l15.n:nrtal.tlsSlfUt5SnafulUnIanf0af.m5n-tIMnSu*..aapSnnnrhllnas1fsi1pl.l*.5aII5.1.n.Pnnnnfl.ntItI.:*nIIn.Pl.nnwnf.fnfS-i-5Pn.l:tIiln0SsSn,f;.rSisllaU15ipfs8.fi.scnfnanwiS!..f*5tiln.Un.d4tf.*lIlst_tOln*5u*ns.i.f9ifSf:*n15iLl.l{fwdfnngaif.lfl*atf..-.5nis*wYl-f5lxi,nIStapflf.ifnf.llip55f5n-n3IWna.n.Lh-t..1nlI5la*rnifSlnlfSlp.olw1fsn.fSSflfI0na_.s*ts.Ia*.lfsaTi_..Sl5f1flfS5s.!nlln.tIl.1RS0S.a..nfKS.n.aSn5I5.lntlStflfiISnnif..-5Pln.POi.ItI1Pf15ln_.s.!!flIat.,lam-O.ffsnSulS.fmt!lw1a15.ll5fffS*.aslun..l!*-_itf.{a.Il._5nf15lWfflu.f.5nafnssl.f*.alnw;5lS55Il5.t85i-nar5alII.silPSl*sh.t2555,i5!_lPP-f.uaifiMnin.n**s!.a3155.I1*!.1_.s.lIfli.s.-iI IdI I III III IT hi III lPiili.!1.fl I! Iii I.- - t94 -ssoo I... &fli ;r T s-4 (Caj i2.&I .44v42. .. I .: LijI.ILZ.iII.1I.LthIt :L:kIoLT kTh. . I)s .4aiLtdZet.. .aiat.. . 1LALI.i:dLLbAt;h:I .oZnj): ofUtcu -, t COL 00668 McCRONE 0193 9 . c:.. c6tae2%4-. COL 00669 McCRONE 0194 0 waiter c. mc crone associates, Inc. CONSULTING: ULThAMICI$QAMt.YSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CI4EMISThY 12 November 1979 Hr. John P. Shift Cyprus Industrial Minerals 651 Metuchen Road South Plafttfjeld, New Jersey 07080 Dear Mr. Shift: We b completed our analysis of the sample of talc labeled "Mono- blend Tale M-6277 (MonitalTaic) tot 1O l3oo. No asbestiform minerals were detected using x-rsy dtftraction mid transmission electron miqroscopy. The talc showed typical blocky and piety particles and talc ribbons. The ribbons ware differentiated trofl asbastiform minerals by selected area electron diffraction. A TEM totomtcrograph taken at 2,50OX is enclosed. Thank you for consulting Mecrone Associates and it you have any questions concerning this work, please contact us. touts sincerely, - Richard M. Ellis, Jr. lesearok Hioroscopiot R1!S :6 End. Raft $590 cot Dr. Joe Shako, Jr. - Colgate-Paimolive Co. 2820 SOUTH MIOI4IGAN AVENUE CHICAGO, ILLINOIS 80615 312/842-7100 CABLE: CH!MICRONS COL 00670 .'McCRONE 0195 Speed Letter. Walter MoCrone Associates mc. From Cnslzs Industrial Minerals Co. a828 South Miahiga Ave. 651 Metuohen Road Chioago, Ut. 60607 South_PlMnfield,_N.J. _07080 Subjeot 1 rOW MESSAGE Teat Lot Asbestos Pibara - Sample Monoblend Code 1(6277 Lot # 129U00 "1 tsc.1S fleass run your regular test for asbestos tibers en I enclosed sample. PLease send an additional copy of your rerort to 7. Si'nko. CoZgate Palraoljve Co. Researfl Center 909 River Road, Pisoataway, N.J. 0885k S/ REPLY Date Signod ESThJN WHITE COPY, RETOaZI PINI( GOP? 070 J COL 00671 McCRONE 0196 a waiter c. mc crone associates, Inc. CONSULTING: ULTRAMICRQANALYSIS MCROSOCPY. SMALL PARTICLE PROBLEMS. EOL!D.STATE OHEMISThY 8 January 190 Mr. J. P. Stiff Cyprus Industrial Minerals Company 651 Matuchea Zoad - South Plainfleld, New Jersey 07080 Dear 14r. Stiff: We have completed our asbestos analysis of talc sample Mocoblend Code $6277 Lot #L291100. The rray diffradtion ana1sis showed no detectable asbestiform minerals. The TD1 analysis Likewise showed no detectable asbeatiform minerals. The sample was a typical talc and contained a few fibrous ribbons. Please contact us if you have any questions concerning the work. Thank you for consulting McCrozze Associates. Sincerely, Ref. NA 5500 EnctosureB cc .1. Siuto Richard H. Ellis Research Nicroscopist 252080U1H M}CHIOAN AVENUE CHICAGO, ILLiNOIS 60510 S12,eZ42T10U oA5LE OHEMICIWNE COL 00672 McCRONE 0197 Date Client (/3ai Pa'khn/ive, Cc, MA Project vCbn Sample Description /Wok.Mt je&J ,11-4177, L0t jz qj io X-RAY PTPFflACTION Serpentine: Detected Amphibole: Detected Other Thaseg Present: Cblrjte L- Dolomite V Calcite v Other: Not Detected i- -'Not Detected a-Sb2 -' Magnesite t/ Mica Commeits: LIGET MICROSCOPY Cbryaotlle Tremolite-Actlnoltte lronzbrons Serpentine Others: Comments: totni % aSbO2 % Throne V waiter a. mecrone associates, Inc COL 00673 MeCRONE 0198 !!...I7TTTT T :i :4T;z 7 TT'p 1 U rf'-'t;i..,Pbj,qThC k.. - ,TV _ .,;i.. - E4 n 4 -i:+F ' F 1 b suxsafl.nfl... 'Via 0 C) 0 0 000. a .3 ' ''c a'" io - o a - o.a ..c - _ae_ 4aO i.$ c _. mc cc..-Ot,J ,a OC, **4 *40 i,t P 0 0 0 00. I.aI!n! qiI!& qjuiz;t :tE': !!2 Lead IR * ieteee - a .r. 21 .4 eiQt .ei 61 *1 en :v: 7 trP1 EtI t-.. fcrth a gln:-..s flJflfslfi;ffllf=l .: -. 1'l qg-cw, /4q12 TE/tl {s 44&dJflMc S44Mfr& PVJ44fJA A44 _T cY COL 00675 McCRONE 0200 Cyprus Industrial Minerals Company 861 Meluohen Road South PISnIlaid. NA. 07080 Telephone (201)754-4830 TWX 710-097-9628 August 28, 1980 Walter C. Mactone Associates, Inc. 2820 South Michigtur,Avenue Chicago, Xl 60614 Gentlemezi: Enclosed is a sample of monoblena talc Zor your routine investigation of asbestiform minerals for Colgate Palmolive Co. Please perform your usual work on this sample and forward the report to us. (tot No. 802509) Yours truly, CYPRUS INDUSTRIAL MINERALS P. Stiff JPS/cr AC CYPRUS COL 00676 McCRONE 0201 waiter c mcrone associatea Inc. CONSULTING: ULTflilCROfl4ALy$ls MICROSCOPY SMAIJ. PABTICLE PROBLEMS SOLID-STATECHEMISTRY 2 September 1920 'C Mr. 3. L stiff Cyprus Industrial Minerals Company 651 Metuchen Road South Plainfield, Wew Jersey OYOBO Dear Kr. stiff I We have completed our asbestos analysis of a talc sample labeled Lot #601809. The siasple was examined with the tranarsission electron microscope. The sample contained no detectable asbeetiform minerals. Thank you for consulting Meurone Associates. If you should have any questions concerning this analysis please contact us. Sincerely, Richard 14. ELlis, Jr. Research Microscopist ME; 6 Ref; 5500 .1. P. Simico3 Jr. 26Z SOUTH MICHIGAN AVENUE CHIcAGO. IWNOIS 60615 312/542.7100 CABLE; cHEMICRONE COL 00677 MCCRONE 0202 waiter c. rnccrohe associates, Inc. AA CONSULTING: ULTUAMICROANAI.YSIS MICROSCOPY. SMALL PARTICLE PROBLEMS SCUD-STATE CHEMISTRY 19Sotembar 1980 Nr. U. P. stift Cyprus Xndus trial itharals Company 651 Matuchen Road South Plaintield, New .lexSey 07O8 aar Mr. Stift: z have oompletbd' aty asbestos analysis on a talc sample labeled. Lot #802509. Who sample was examined with the tranatssion electron mior000pe and selected area nletron diffraction. Tha. sample contained no detectable asbestit9rm minoxals. - Thank you tar consulting Racrcne Assoothtsa fleasa contact .me if you have any questions. Sincerely, Bfflo gb Ret: 5500 Cc; U. P, Bp]co, Fr. RtchaXd)S, Eflis,qr. Research Sicroscopist' / 2UOSOUTN MICHIGAN AVENUE CHICAGO, ILLINOIS BOSh 5124424100 OAOL& CHEMICRONE COL 00678 McCRONE 0203 Cyprus Industrial Minerals Company 651 Metuthen Road South Plainflhid, N.J. 07059 Tetephofle (201) TM-4880 TWX 710-907-9528 axtuary 13, 1981 Walter C Mccrone Associates, Inc. 2820 south Michigan Avenue Chicago, In. 60616 Gent imen; oyEnfocualrsobuseessdutaiifloswrmatrksmaominpnleterhaiolssfsamfomonrpobCleolleagnnadtdetafolPcarw2afaoorlrdivyteohueCror.eropuoPtrliten, aetsoeiunpvsee. rsftoirgmation Loft l].D865 Yours truly, CflRUS NDU$TRtAZ }4I$RALS Co. ,flc,i deiLL_- BEXUH B. TaEMnq CYPRUS COL 00679 McCRONE 0204 wafter c, mc crone' associates, Inc. CONSLfl.TINO: ULTRMIICROANALY6IS MICROSCOPY SMALL PMTIOLE Pfl081043 SOUDsTATE CHEMISTRY 16 March1981 Mr. Lou Marina C nsa Industrial Minerals 555 South Flower Street La Angeles, CaLifornia 90011 Beat Mr. Murino: t have completed my asbestos analysis of a sample of Cyprus Monoblend Talc lot fl10865, submitted with K. Lehman1s lettet of 13 January 1981; The sample was anatyaed with the transmission electron microscope (rEM) and electron diFfraction. The sample contained chrysotile asbestos at a level less than 0.1% by weight. The chrysotiLe was identified by its lectron diffracUon pattern. Thank you far consulting Mecrone Associates. Please contact us if you have any usstions. Sincerely, Richard K. Zllis, Jr. Research Microscopist RHEofe atE; 5500 cc Vetu M.ttuo - Cyptus Induetria, LI 2520 SOUTh MIONIOAN AVSNUE 01110A001 ILLINOIS 80518 312/842.7100 OABI! CHEMIORONS COL 00680 McCRONE 0205 Pleat 4th **'z-/ &i1 4 ,(44 6OO COL 00681 McCRONE 0206 RECEtVED AIlS0 S iS1. Gypnis Industrial Minerals company Talc Division 555 South F'ower Sheet Los Angeles. CaliFornia 90071 Telephone (213) 48$3700 TWX (91 321.5753 July 30, 1931 Mr. Richard A!. Ellis, Jr. Research Mioroscopist Walter C. -McCrode Associates, Inc. 2820 South Michigan Avenue Chicago, illinois 60616 Dear Mr. Ellis: In response to your January 1981 letter addressed to Mr. Lou Murino, we would like to receive the diflraction pattern of the chry-sotile asbestos fibers which you observed in the Monoblend sample, Please send the diflradtion pattern to me at: Cyprus Industrial Minerals Company 2485 Military Avenue W. Los Angeles, CA 90064 Thank you Thr your assistance. cerely, MMX :mc Technical Services Manager CYPRUS COL 00682 9- McCRONE 0207 j waiter a mccrone associates. Inc. * QQN$VLTINQ: UL.TRNICROANflXSIS MICROSCOPY SMALL PARTICLE PAOSLEMS SCUD-STATE CHEMISTRY 26 August 1981 Mt. Maral )L Kazasian Cyprus Industrial Minerals Company Talc Division 555 Soutb Flower Street Los Angeles, California 90071 Dear His. ltazazian: In response to your letter of 30 July 1981; I have enclosed the diffraction patternof the inonobleud talc sample #110865. The diffraction pattern is of a chrysotits single fiber taken at 200 kV. The sample contained a very small aunt of chrysotile and may have been a cgntaminant. The very small size of the eingle fibers ('340 .6. diameter) make it difficult or impos- sible to get a diffraction pattern using Less than 200 IcY. ton bad meitioned that you were using low ICV. I feel that this could. be the problem vitlt seeing the pattern. Pleape coittaut ie it you have any questions. Siizcerely, Richard U. ElliS, Jr. Research Bicroscopiet RME: fe Inch Ref: 5500 28W SOUTH MICIUGAN AVENUE CHICAGO. 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I ( (( I Si i J14111 S ,j__1_.1_j__I I I..L.,1..L (i. i I,- I COL 00687 McCRONE 0212 ORIGINAL PURCHASE ORDER 0 0*-?. a 1 II H t1 2' 9JERSEY CITY, N.J. PURCHASE ORDER NO. TV,' plo 'TAX PCRCt NT j ta at Oh Te a In - a. OiI&I IL'I a YtNOOR NUMSII at - 0003 1 S HIP 1 CODE 2 CODE S CODE 4 SILL TO ICQU S CODE COOS SPEC. RAT 11111' SHIP 'TO 120 1) L. 547 - 'OS .1 01 OS JUt MORRIS ST. K 5753 JJuERsSuEtYstCxIsTYt..cNs.Jn. t07502 .ICRSEY CITY, N.J. *730Z IJ?ECRRSEAYNDCISTTY., KN.5J1. 10*7102 COLGAT&PALMOLWE COMPANY DCLAWARS CORPONATION 300 PARK AVRHUE, Nfl YORK, N.Y. 1*022 CITY 5 ci I, - LL'J) I Wk l4vj?jt ('vne tr,1*hsc3 6 DILL 'TQ 99 .5 bUchi'y-i Ave. r4kfr1n,tLL-. /91') 1.1/. coW4Tg?4LMOUfl COMP4tJY U p.o. sax zie* ::IiflWflAflIRRCNEII.TIAL ..ITATIO1J $ II 150X401 4 CITY. N.J. 01192 24 ATTN. 2 GRANO ST. X $s - JERSEY CITY, N.J. 07202 In GREENE ST. K Ill. CITY. N.J. 07192 Ia CRANO ST. K ZIG, IJURSEY CITY, fl.J, 07102 IIJIStfYlgOYIC!KITSYT,.2N2.J7.39, 7*05 IIDJEURRSSEIOYINcadvP,RNIt.JN. 29575)051 so GuANO IT. KillS U CITY, N.J. 07302 I4flSENC IT. K ZflW JERSEY CITY, N.j. 97*05 I DIsCOUNT TflM$ SHIPPING TERM5 so rou DunhiWiva 2FJ PO SInppIug Pt. AT%RoAC,h erflk,. (Pi..Pcy a BU S.. Sekw 30 POD flipping Pt. (CeHecti CI PIETPANTONIO 201.547.2592 ESTIMATE CARRIER MUST ct l - - oi CALL24 HRS. _________2 PRIOR TO DELI VERY. 'SW. ..4fl'SI'!PflS -31 I-I ii- It is 11CC. PLANT 00031 JERSEY CITY itS Iw.on In socoIdara with the tenis aid ooimdltisn. en thi tact mId ban sUM. aid... ROD TYP 4IIANTITV oSa COWERSION COLCATS NIJMIEII IIT FACTOR IVIROt, JOASIt PESCIS rPt ION CL udPI. S IU.LDOLLAR*I PIER 'I!24VUtItilrIPPING 900UMUNU MUST COKTA NAN APPLICASL.E NINYVCICSYE*PTRNSAPTAIOINCrnLEUrOqCs*Ay UmYi.I4tRct TRANOSFPOQRRITCAINTAIOLNBCIL1,AVAtMU. 154..? *-t. lID? Si M&OE ASAIKIT PRO FORMA IRVOtCE, ?.ctc HEREOF. COL 00688 COLG4TE P4LMQLWE COMPANY N.IgotnYcatwnd. unless Signed by outho,gn.j MCCRONE 0213 HoJEcr flitS: U1SIOH. tt.: SPONSOR: ADDRESS: E8ahln WST REcORD talc RCT 1004C ytA1wBWfl1VE iXtIPAW Cet PROJECflQ.: 12917 DAlE EECEflzj: 5 25 8 D)3 326242 Contact:: SUMMARY OF PSOBLEM: Lab Notebook Reterencest No. pp. InitIals No. pp. InitIals No. pp. InUIals_ Phototnlvrognphtc record no. Sample dispotat: returned tiled 4where) dis cat ded DU1ECT COSTS Exclusive o oper. Individual time time on Inst. below) aie laxne Hours Charge A2Q&L.. E Travel Charge Suuimarv rate Trateler Destination Cost I Individuals S Travel Oixtstde Other Instrument time Date TE2SI CRb MI' IMP ESCA E.\IMA ?IOLE RouS Charge i Date Company Photo I Pitoto Materials Sppites I TCohtaal e $ Cost Olt for bIIlIIIg Project Ldr Group Ldr__ TOTAL ChALICE $ BLLLED TO CLIENT $ INVOICE NO. ) ,SLQfl.. T/&.7/J .,%o - WDJECT LEAD itfE COL 00689 McCRONE 0214 1 waiter C. mccrcne associates, inc. y CONSULTING; Ut.TRAMICROANALYSIS MJCROSCOPY SMALL PARBOLE PO8LE?4S $OI.ID-GTATg CHEMISThY 26 July 1953 JtrU RQa wlgate-PaluioliVe Caany 300 Petit kviue New Y4c, New York 10022 IV(5. Dear t Roach I have ccapleted ur asbestos analysis o a talc sa1e 1abele BCTIOO4C, Lot /)22873 ana subnitted under purchase order 096142. The sax1.e s sejeoted area wcamtwd e].ectzcg with the ttansmsston e1eca' microscope ax5 dif&actit. fle sile was fruna to contain a wry low level of chrysottle asbestos, probably less than 0.12 by weight. Brane of U exated in preciwie the low gxttmt, possibility a o second saple was amtamfratien. Iptretopaored ath. contained cbrysotfle. plxtadcrograpbs of chrysotile fthera are enclosed. Thanic 'ou r csu1ting McOrone .Msoc fates. fleaee tact me i )CU have any quesUuis tegerding this analysis. Sincerely, Richard N. Ellis, Jr. search Microacopist W4E:fe Thai. ReE: 12917 aego SQUTH MICHIGAN AVgMJE 03110A00, CLUNOI Qc8 3W84t-?tOO GSLE CHEMLORONE COLI 00690 McCRONE 0215 'Yt wafter c. mccrQne assodofes, Inc. COL 00691 McCRONE 0216 waiter a mccrone associates, inc flA1 Sfl1flSi:f.l'fflfl! S. ,qi( ILW AL' at ski j Ak. & ku a A aL eat. A iL I A .V / ..A.' L.LIt LSLWfl!flLLflZPflflW!rL1 AS.' . V 1 '. A AM I:)L.s-..'..tiJL-. LL2>a.L: .. . :;L. j;j;. a!iLL. IP &AL..a..i t-&A .a A. COL 00693 McCRONE 0218 COL 00694 McCRONE 0219 C ERWCT COST RECORD 1 NOJECT TIThE: 6 anpls talc for at( PROJECT ?Ojl87j GUS IDMEt w. SPcSCR; OME RECEIV2D1 84 P.O. NO. 35L4/7 AD1RESS: Pistmmwey )%1 o'Zr4- Contact: P cc repOrL to. Te epI-(GIeI.87R 76sc Individual ticte Nra Sarole disoosat: returned discarded consuted DIRECT COS1 (ExelusLve of cper. on inst. below) Hours Cherge Ch.re Surttar', Ir4ividuals instn1tenc TraveL Outsice Other $ Tote1 ch.are Xztitr.zcnt U:re Ditto Ilourn 1' Chnrcc OK for bijlir.2 Project leader Group leader Cos ;up Iie$ Wt\I. OLV4CE stIfl LVOI ;X).jpr oL\ ntcerr \TX( COL 00695 MCCRQNE 0220 waiter c. mccrone assp'piates, mc; T CONSULTING; ULTRM.IIORQAFJALYBI3 MIOROSOOPY SMALLPARTJCtE PRO8LEMS SDLID.STATE oaicsmv 27 April' 1984 Dr. .J. P. Sfrc, Jr. Sr Section Read, Analytical lgate".Pa1nolive company 909 Ricer Road Piscataway, New Jersey 08854 Dear Dr. S3nkot This report concerns the asbestos ana].ysis by JTh of six talc aamspes sthS.tta1 under your P.O. 634617. ttysotile asbesthe was detected in saspies 0613W, 2713Z a3 1813AX. b asbestos s deteceed in samples 89073, 2283]. and At 13032. Slits this tectmS.que is not quantitative, no asbestos caacenation can be assigned. &tThank you consulting ZdcCrone Associates. If you have aty questions, please do not hesitate to call. Sincerely, Deborah P. Palenlk flecon Microscopist RaE: 11871 0 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 80816. $12/84-71O0 CSLECNEMICRCNE COL 00696 MCCRONE 0221 TLt 214. S,e4v2 / Y' -tJ. v.-7' C,1 .t bG2tr&41 ac.#'j A?O'>1''C37,7 s -.44 0 C' 4J &7/3tY ov'J ///diFX. ,M aLt- z# So 73) C1e.--rj z'4r td1tctL, g Co c csiwaeJ 7%ti ,dt.c ra o&#t2c&'tS74fr'ar, Ciac4 p COL 00697 MeCRONE 0222 C COLGATE-PALMOLIVE COMPANY Re search and Development DMsion 1O9R,CfROid piwaaw'.NJ S4 4 .7 January 24, 1984 Ms Deborah Palenik Recrono Associates 2820 Booth Michigan Avenue Chicago, IL 60616 Dear Ms. Palenik: Enclosed are 6 eanples of talc tor analysis for asbestos by TEM and SAED. The three coded 0613B1t, 1813AX and 2713EZ are finished products and contain 1% magnesium, carbonate, 1Z zinc stearate and perfume as addUives. The remaining three so9073, A113031 and Al22831 are raw material, talc with no additives. Please analyze these as soolt as possible. A purchase order to cover costs will follow. If there are any questions, my telephone number is (201) 878-7566. Thank you. Sincerely yours, JPsnneb cc: P. A. Mi&ger W. Schubert Dr. .1. P. Sirako, Jr. Sr. Section Read Mialytical Department )(g-y P C5I37.5 COL 00698 ,McCRONE 0223 J o 74&4, COL 00699 McCRONE 0224 1101.1* 0)1 r1.. r--... I* N i14 ..S*itd W isS. *..4 lnMSSW t. 1.4 4 SN NIStUIMCAIV MAY NO! - .0 IL gEnoouc&a. 1'*.tr uf Nra' IPIIU wiiios o. t*x*tlON VAX m'n Un cs*MtI FORM ST4 nil. HAHfl flhllitAlt 4* MIIIIs)hptl t4IMQl 315-59 M'S LI, nhs.d_, . Tho uS4...1iilodqI4&. M 0* i I. not r.qvlmd I. psy $ii Sw JorNy ash. soWn U.. on ths'piHdISW W ,S.A..... avail by sl,M CslftkS. brine duo Juna*h paissi p.spsty p.,.. duad wil S ...4 tsr Lt1 Sold NnqlbJ. p.n.as$ p$peIy Wifli vad forth. Mowing easnupt papon for gj or. cosiat Scm dszstlp Mt. *s1ia.Lve* ts niflrS eM dnC.va a the sifl*dntIl CS' 2SL.*LLJ Mel. . liw 0ISIIRIb0 tethoS. ci .011 teflL nonl profly us ho used it, she ahoy, dnalbed IflP! PwP0flhI r.444d jjS..L.j NJS.A. 5d42S. vioi itijWi pOtI001I r4 end *W 1. f*q MS (Zoo tsvv dli fib.9 of ptMc4& vwpw &a&.. ekisnA I. the wsduSqn.d purd.sw.r, hay, nod and ...,Ls with St l'wfrwulon. and ruin p eivl9nped pvc uses to flue New Jwny kin ed U.. Tan Ass With 'S.fld to II.. vie at *1 EnatS U.s Csctlftw and U it my b.lI.f thes if.. vendor nomed honin S oat r.qvfrsQ I. Shet ib, tab.. or use to* fl tho Ira none 1001! Ct "r'' usynd by Nil. C.nN..l,. The vndonlpnsd pwduss wishy .wa.n (undo, the penalfi,. or p.ury and ohs ewnflaq) tint uflolS*11 inVscsaN.0 shown In thu CwfI$.o9. Ii hut A v.00* Itn. as a cozasz-apwnr C '4410 rt tNhItwI '4 tt.M4.n & Li 8UXER CNT1WL GD42BRThG 'DEPAKIThWiT 103 UJDSCtT ST., JEMEy aiwY, N. J. 07302 (nimimqt BYBCABw szcnar) COL 00700 McCRONE 0225 ? fl..p -.0. TERMSaNDC0ND,ttoNs SItVO1C$S thillod The qu the SeU*r'flntlae logethermiuirthe 0z day of sfdpmeot Is the Purchesir. lblsofi.Sgorekjie receljti ppilt ligated by canler, slafla thvld4 lavblths chaR be Sued toy shipments appifl ephast each putchasa ordu. Monthly statement, must be maIled 0i SOOn as possible tot the tint of ceeb month. WARRANTf - The SeYier txpreriy warrant, and agrees that there ha. bruit, tomplianee with and no violation of any lradema& ihts, patont rIiirco1syrhl,orof any nib law or n'gulatlori of tin. Pcdpral Governtnent orof any Stain or any of their rcspecttvo agencies or poIlLlj.'al itiibdlvbioaw, in and told Purcl.asr.r hannloye (1w muuacturo. (ron, any or nil prodvctlon.aaie eoia,, damages, fainnderoor ritehxippiennoenet.o(fInthcelugdoinogdsehonunntau,iIidre.r:saannddthfeeeSseollfeerxwpiolrltIwsiidtehmeansirfiys) aidilcl, may be Incurred by (he Ptgthnnr by reason of any claim or suIt aath out of the Infritigemenl of any iradanirit, patonl rlht or copyright andlorby aaron of city cilatlon. claim or suit fordameges and/or pmstlln brought ugahirl the Purchaser l.astd upon any Injuricn,dsmesclil or vlolttioinrcaulllngor ClaiITWd to havrreiqdtcd From any alleged infringement or dofeet In auth good. or Ingredients or parts thereof EQUAL. EMpLOYMENT OffORTUMITY -. Tiic Equal Employment Opportunity Clauen Sni'tlon 202 of Executive Order I 1246 as *mcndcd related toEqial Employnwntflpportunitins and lmpIerncntizr Hula and Regulaulonsof the Serroisry of Labori SectIon 503 of the Itnhthilllalloat Act cr1973; SectIon 402 oF the Ylotham Era Yatcr.ds Readjustment Aalaja,,cr Act of 1974; and Erocotive Order I 1625 ndating to minority buttansi enterprises are Inco,po,uted herein by cecilia refvrn,ce.. CHANGES in ORDI1R - llalsordercannot bechariged, maCflied ordlacharged many maunerexcept by agreemetatin mithig Spied bya duly authorized reprcsontallvo*IIhe Purchaser. 'The Parcbuerregzves the right to (1) make ctaaps In the ordar (2) cancel ill or any past of the order at orn' ilme, by notice In welling. The Puachai*s shall not bb reeponalblefor cost bicwTad by the Saaerlaa connection with this ordce arm, thc date of receipt of the change cc casedetlon notice. U Mesa tire Sefler pxessnUto the Pusdiaser an liemlead statement of claim qalest thePerchIaniwIthIn twenty (20) daYs after (lie tecdpt of notice of such change or canceflallon, the Sebr 'lieu be coacludvly dSsed to have tIred all Calms Against (lie Purchaser with *cct thereto. CANCELLATION ror SElLER'S DEPAULT - Shoillil the Seller rail (1) to effect delivery on or before the wedded dellyeiy date (a) (2) to dotivor goods In nil respects conforming with lbs requIrements (3) in the due performpce of each .d alt of the terms and conditions of till order, she Piudasnes n.y cancel this order tq whole or I, pert. Without psejudice to the foregolrt the Seller agrees to ropoet prompttx to the Pittc%ntr any aoOt apecHied daltyshi shipment of the panda covered by ttajs order. SPIECtI'IVATIONS. DRAWINGS. etc. - All .pedfleallona, drawings, plan; dsgna, rptes, or oIlier descylpdoh$fqnd loin this order shaG bedeerned an Integral pitt ofthla orderu tuflyaelfsetoutbfidlhezth,aswlsellerwnnntathatalldsltvcrleshercmtshall conform thereto, oath delIvery beIng aubject to the inspection and upproval of the Punhaeer, whother or not any - payment shall bays been u,ade thereonby thu Pwaaer. NQNCONPORMTh4G MATERiAl. - If Sinai deliver. defective mattel.) or mated.) not oonformlmr to the reed'upon ,pecllkailona, Purchase may (1) hold such inatedal at Seller's expn pendIng InstructIons as to disposal, 2) Mum It to Seller at LelZer'a expanse, or (3) utIlize It Pa the form received or alter uppading or other operations art performed on ft, or tithe It in a different mariner or In different p.opoctlona wish other products thin vii Intended, and SeSer will be Hat), for any dbelraartloti In the nine to Purchaser of ti material and for any incIdental o, other damages uttered by Purchaser rwldng from such Wectiyegias or nonconformity. No replacement of defective a, nonoonfonnlrag material will be made by Seller unite. autltmtied by Purdiaser PACKING - The Purchaser edt atow no chirps for boxing, pac*aglag or uadn unless by written aptament. Malarial muse be packed, tipped and billed In conformity to tia.dflc.tionreqnlrom,ata necemery to secureMlnlmum frelalit rates. OUR cOUNr - The Purchuefl count win be accepted as haul and conclusive on all shipments not aecompenled by a paddag ticket. LIABILITY for DAMAGES - Whenever Seller shall, by vksue hereof, have properly of the Purchaser In Its poeseasloat, the Stile, theft be deemed an Insurer thereof end Sail bersepana)ble for Its safe eileen to the Purchaser. ASSIGNMENt - This order diet not be aseigned or Datisfened without prior waltaca consent of the Purchase,. WMVER - Purchases dull no) be deemed to have wa)#esl say of Its eights bermaasder uSia such waiver slut have been Sped bye duly authozlaed repreeantattvi of the Pureha air. No auth walvee, valise expressly naiad therth. ahalt to effective er to any delIvery or other flaneactigu whIch occurs subseqisnt tome date of the waiver, nor as may sonth,ianee oft delault after retch data. SHIPPE9 MANIFEST JER5EY CITY TRUCK DELIVERIES - DELIVERY INSTRUCT%ONS kSHIPPBRSMANIiE$T Isprovlded breach load sad meat eocbMpan,ach eltipanent. REERVE UNLOADING PACE AND TIME bytelephonlnp 0t'S47'2G1U, they city RAfI. D4IiYdtS - 1prlvatt.ur.ctic(olmatl. .j$ronrQ 0ev ars :..,JEFPETISONYP.L.fL.@ R4It,pqAVEFlS......i:lP4ty(tbRIOdAtnDgt'.9pOfLflAtTJ:.M'" ORO}tlO -KANA5 CITY 8AILDEUVth1I l')' AI0irt4RK ISCrfYSOUTHEf3N I9AJLROAD Co sERgaEv RAIl. DELfYtRIES sourHERsnctFacn..ILRCIAP: .. . .- COL 00701 MCCRONE 0226