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BIODEGRADATION (BOD/COD) AR R26 -- 0777 Identity: A mixture containing perfluorooctanesulfonate, which `may also be referred to as PFOS, FC-95, or as a `component of FC-206 or L3243. (1-Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot numbers were 501 and 895. The test sample PFOS, 1is7.F5C%-2d0i6e.thyCluernreengtlyicnoflorbumtaytlioenthienrd,ic7a8t.es91it%iswaatemri,xt1u.r3e3o%f 0.67% Sultone foamer, 1% sodium octyl sulfate, 0.04% sodium lauryl sulfate, 0.5% polyoxyethylene monooctylpheny! ether, and 0.05%benzotriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data does notaccurately reflect degradation test sample. potential of the fluorochemical `component of the Method: Not noted. Type: BOD Ultimate and dichromate reflux COD GLP: No Year completed: 1976 Contact time: 20 days Inoculum: Source not given. Lot 501 Chemical Oxygen Demand (cop): 500,000 mg/L. Biochemical Oxygen Demand (BOD): 5-Day: 45,000 mg/L - 11-Day: 218,000 mg/L. 15-Day: 304,000 mg/L. 20-Day: 319,000 mg/L. Lot 895 Chemical Oxygen Demand (COD): 480,000 mg/L Biochemical Oxygen Demand (BOD): ~ 5-Day: 45,000 mg/L. 11-Day: 263,000 mg/L. 15-Day: 20-Day: 270,000 mg/L 263,000 mg/L 001411 tSRhueebmsfatiruakonsrco:echTReeemsmitciaanrlgkwsprafosipeolcrdo.tnioTdnuhceatlveoandleo.unestrheepmoirxtteudraepapslydetosctrhiatbemdixitnutrheeTaensdtnot No conclusions given. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 p0 araQ0 uary00000000 mReeltiahboilditfyo:llKoiwiemdi.scThhreaniknioncgul3.umSitsundoyt lparcokpserdleysccrhiaprtaicotnerainzdedr.ecTohrdessoafmtphle.e cpourniftiyrmwaatsionnootfptrhoepearmloyucnhtaroafctfelruiozreodchaenmdictahlepsrtoupdoyrtliaocnksinatnhaelystoilcuatlion. R0 EFER0 ENCE0 S 00000000 STth.ePasutlu,diMeNs,weLraebcRoenqduuecsttednubmybtehre 332M59C,om19p7a6n.y, Environmental Laboratory, ow0 er000000000 Last changed: 6/28/00 001412 . or sna EES SOR te se ester o----_____ REQUEST FOR LABORATORY WORK Lab Request No. 3259 TO: ENVIRONMENTAL ENGINEERING LABORATORY -- BUILDING 53-6N Requestor PName:g00 oOCaGAfneesepurs6s-o2m27e6 Lab Personnel ARD 7/5 oTwerheacs.simpie: __(e Tl=_T_ re ------ SampleDate: _____ DateNeeded: A OateCompleted: [ ___r=32- --7p Sime Decipion E ear s E 3eSot [WWe 21T ehBeTm 2E0---d-- Total Hardness, mah as CaC03 Be rrr TP Alkalinity, mg/l asCaCO3 A Re 1 oH Ee Sulfate, aSOs" NM-- TT T TT 1 17 H--H--F--H-- I AI | py] fay te p -- f Silica, moll as S102 Tuoride, mg/l as Ortho Phosphate, mg/l asP_ Total Phosphate, mg/l as P "Total Chromium, mg as Cr Hex_ Chromium, mg/ as Cr. Feo ren: Total Cyanide, mg/l as CN rr rr T T1 T-- 111 1 rTTT rT rr TTT H rr F rTTT 1 Tron, mg/l as Fe. langanese, mg/l asMin TTT H------F-- tH BOhDen,oml,go PY anol UIE j NI[Wx 1 TVCooOtlDaatl.iSluesmSpouiesnSphdeoenrddtSe.odLlSioodlsgi,d" sO,lmgmsgt/le) ~~ [T XI00o ,0~ 00T|rX5200,00r 0 N1e ,07r 0X|,=0e 050 0,000 Turbidity, mg/l Silica rr Tr Total Solids, mg Toa ree Total VolatileSolids, mg I Hee IT Zs rT TT 11 Ee [1237 1 rzrel #8 1122|7 Total Bacteria, No./100 mi Total Coliform, No./100mi Fecal Coliform,No./100ml Fecal Streptococcus, No./100 mi Ammonia Nitrogen, mg/l 3s N KiedidahiNitrogen, mg/las N Oland Gress,mgt Crew See aflaihed eee <heed = a rTrT rT T r Tr FrTF2 TTT H--H-- 3 = | | 11 TT blo TTT] TT TT 111 : pS eee le Env Es. 1s Sc -- EnvronmEasn.at i ~ 001 Errnog.rLonGots JE T-- rwumepr = - I dr FC 206 set. ~~ -- 5. I= rr 45000 000 wm>g/2 --18- 304000 ~~ --20- 31300 ulbonalz s- a TS 26- creer ---- --S- FC 206 Usd gas AS,000 mg 2s,000 : -- 210,000" 263,000 + sessmmpegs ----eeee FM-3222 131000 mye 000 --s- 859000 - 20 563,000 000 hsm 5- 53 000 mele ] _ 1- 485,000 203000 * Is (8800 + --R- 203000 Td NSeBsRe001414