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Miscellaneous Mechanical Equipment E 12 - 2.1
engineering
STANDARD
PLAINTIFFS | EXHIBIT
I^'VCEL'2'26`5"?-'
PACKING MATERIAL GASKETS And
THREAD LUBRICANTS
CELANESE CORPORATION OF AMERICA
Central Engineering Charlotte Office
000009
APPROVED NOVEMBER 2, 1961
Celanese Corporation of America MISCELLANEOUS MECHANICAL EQUIPMENT PACKING MATERIALS, GASKETS AND THREAD LUBRICANTS
Sponsor - Belvidere
Engineering Standard E 12 - 2.1
Issued Rev. No. Date
11/2/61
PREFACE
Packing and gasket materials of numerous types and shapes are avail able from a large number of manufacturers. There are individual preferences in specific applications. Where several materials overlap in suitability it is not sensible to arbitrarily prescribe one only, since availability and cost may favor other materials in many localities.
Therefore this standard, as concerns packing and gaskets, is designed to assist the plants of the Corporation in solution of difficult problems rather than to attempt to tabulate many materials versus many applications.
The thread lubricant section catalogs available material with comment where facts are known.
000010
(1)
Celanese Corporation of America MISCELLANEOUS MECHANICAL EQUIPMENT PACKING MATERIALS, GASKETS AND THREAD LUBRICANTS
Sponsor - Belvidere
Engineering Standard E 12 - 2.1
Issued Rev. No. Date 11/2/61
1. SCOPE
This standard is limited to problem applications within the corporation. Compilation is made of uses where difficulty has been or is experienced. Against the problem applications are shown a.) the material and form that solved the problem or b.) the best material known to date where problem is not considered to be solved.
This standard also tabulates applications where thread lubricants are used and opinions given.
2. GENERAL
Data submitted by several of the plants is contained in the accompanying tables.
Table 1 - Lists applications where original packing methods were not satisfactory. Against each entry is shown a treatment deemed satisfactory or the best found to date by individual plants.
Table 2 - Lists similar information about gasketing.
Table 3 - Is essentially a list of thread lubricants and sealants in general use at several plants. No attempt has been made to list all of the uses of all of the sealants.
000011
(2)
TABLE 1 - PACKING MATERIAL
Engineering Standard
Misc. Mechanical Equipment Nov. 2, 1961
000012
(3)
TABLE 1 - PACKING MATERIAL
9 /1 /6 :
Engineering Standard
Misc. Mechanical Equipment
000013
w
TABLE 1 PACKING MATERIAL-
Engineering Standard
Misc. Mechanical Equipment
(5) 000014
TABLE 1 PACKING MATERIAL-
Engineering Standard
Misc. Mechanical Equipment
(6)
TABLE 1 - PACKING MATERIAL
Engineering Standard
Misc. Mechanical Equipment
000016
(7)
TABLE 1 - PACKING MATERIAL
Engineering Standard
Misc. Mechanical Equipment
000017
(8)
I TA13LE tL' '-l- 'Atwi'NG1 'm}\1(1!,'RIA Ll
Engineering Standard
Misc. Mechanical Equipment
000018
(o)
Engineering Standard
TABLE 1 - PACKING MATERIAL
(10) '
000019
TABLE 2 - GASKETING MATERIAL
Engineering Standard
Misc. Mechanical Equipment
000020
L. (U)
TABLE 3 - THREAD LUBRICANT
Misc. Mechanical Equipment
(12) 000021
INSULATION SECTION 1977 Edition
000022
SECTION PREPARATION The Insulation Section was prepared by Ray Hearon, Cl Weldon Wallace, Bay City; Jim Beasley, Bishop; and Jc
Pampa.
DISTRIBUTION Each plant will be supplied three copies of the Insul Section. Use one of these copies to reproduce your i number of copies. The Clear Lake Plant will be respc distribution to Chemical Company Purchasing and othe: Divisions requesting copies.
PROCEDURE FOR REVISIONS AND UPDATING To .<eep tr.is section open ror improvement arm tne cis of new Engineering know-how, it is important that met additions or revisions to the Standard be readily ava atoacked 10m letter should be us^d r,/ 0 -- = v efeasible be reviewed by the Insulation Standards Committee and the Plant Engineering Superintendents at their meetir accepmance. All holders of the Insulation-Standard w the revised material and new oubiications as ohev bee
000023
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-: '
Ray Hearo
i N ane anj .sea: cn i
Clear Lake
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SUBJECT: Recommended Revisions to Insulation Section
(1) State changes or additions you feel with improve or uodate this section.
(2) State justification.
ng Super! Citv
aisnc C'aa'" Lake Pam. a
3/
000024
SCOPE
Celanese Chemical Company E.mc 1 necr 1 ng Practices for Insulation
CRITERIA Fcr Writing This Section
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--
r vATEPIAL PECO IPEVENTS
SE GIVEN TO THE '/ENOCH a PERMANENT REOUIREMENT
I r or MATER IALS.
i<
j APPLICATION PECUIPEySNTS ]
| "or Celanese It Contract
1 Insulation Workers ano I Engineers. Ai;s field I in kncving i1j A! rPJSPU'.UICAATITsC.'Ni, C" Tm
1
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ENGINEER S' GO ICE
I Tor Celanest. it Contract
j Engineers. Aios Engineer I IN T'H AREA cr SCSI ON AMO
PR CCUR E.MENT OF materials : WITH A minimum Of I'VC.
3 /` / / -/ V
000025
CRITERIA FOR WRITING INSULATION SECTION
1. Provide conformity of insulation between Chemical Company Plants to allow Chemical Company Purchasing to obtain the most economical agreement with the suppliers and applicators of insulation.
2. Provide a training manual for the Engineer becoming involved with insulation.
3. Establish guidelines for the application of insulation materials in the Chemical Company Plants.
Sr CfnH.vilCAL CC.yFA.N'rTTrT
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000026
3/1,
NOTES TO USERS
The Insulation Section consists of three basic information packages: requirements for vendors, guidelines for engineers, and requirements for application of the insulation.
The first two sections will be supplied to a potential vendor for his consideration and to aid in his supplying of materials and expertise for Chemical Company jobs.
The third section will be supplied to a contractor when bids are being obtained for job-site maintenance or construction.
The Section should be used strictly as a guideline and may be
changed consistent with good Engineering Practices and
approval of the Project Engineer. This Section should
oe
construed to prohibit continual testing and evaluation insulation material.
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.ickr.esses pres nted in Tables 1 through 4 were T-2 013, "Econo: .ic Insulation Thickness Computer 5 lists the pr cess and economic conditions
the recommend d thicknesses in those cables. agreed-to average conditions at
our.d chat olart-to--olart ckr.ess differences to justify
The Computer Applications Croup
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000027
I 3/1 1.
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Ml SCOP-
f M2 INSULATING MATERIALS - HCT SERVICE
M2.1 CALCIUM SILICATE (KAYLO) M2.1.1 DESCRIPTION M2.1.2 SERVICE M2.1.2.1 Temperature Ranee M2.1.2.2 Components Insulated M2.1.3 THICKNESS
M2.2 MINERAL WOOL M2.2.1 DESCRIPTION M2.2.2 SERVICE M2.2.2.1 Temperature Ranee M2.2.2.2 Components Insulated M2.2.3 THICKNESS
M2.3 CELLULAR GLASS - (FCAMGLASS) M2.3.1 DESCRIPTION M2 .3.2 SERVICE M2 . 3.2.1 Tem.cerazure Ranee M2.3.2.2 Cc-zor.er.t3 Insulazez
M2.4.1 DESCRIPTION
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z.
MZ 1 Z
M2.4. 2. 2 Ccm.rcr.enz3 Insulated
2'1 '*'
ELANESS CHEMICAL CC.MPANYr
000028
3/:/r
M2.5 INSULATING CEMENT M2.5.1 DESCRIPTION M2. 5.2 SERVICE M2.5.2.1 Temoerature Ranee M2.5.2.2 Components Insulated M2.5.3 THICKNESS AS BESTCiS TAPE M2. S. 1 DESCRIPTION M2 .6.2 SERVICE M2.5.2.1 Temperature Range M2.6.2.2 Components S U ^ 58 *" O M2.6.3 THICKNESS JGAMED PLASTIC M2. 7.1 DrSCR'"?'7'ICN M" " ? SERVICE M2.7.2.1 Temperature Rar. - e
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OiE.vICAL COMPANY-:
000029
3/1/7'
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M5.3 WIRE NETTING M5.3.1 DESCRIPTON M5.3.2 SERVICE
M5.4 BANDS M5.4.1 DESCRIPTION M5.4.2 SERVICE M5.4.2.1 Aluminum Jacketir.c M5.4.2.2 Pipe Insulation M5.4.2.3 Vessel Insulation.
>15. 5 WIRE M3.5.1 DESCRIPTION M 5.5.2 SERVICE
>15.6 SCREWS >13 .5.1 DESCRIPTION >15.5.2 SERVICE
>15.7 NEED PINS >15.7.1 DESCRIPTION
m= 2
CDI-S
>15.5 c:-:il-s?rinc-s MS .9.1 DESCRIPTION
!SiCT:CN: INS1
ELAN ESI CHEMICAL COMPANY
000030
3/1/T7 i
Ml SCOPE
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This section describes the minimum requirements for the purchase of exterior thermal insulation materials for pipe, instruments and equipment. A summary of this section is attached in Table 7.
M2.1.1 DESCRIPTION
Insulation shall be a rigid hydrous calcium silicate pipe covering of sectional or segmental form. The insulation shall contain an inhibitor to reduce
the possibility of stress corrosion cracking of stainless steel. CAUTION--calcium silicate containing asbestos will net be used.
M2.1.2 SERVICE
M2 2.1 Temperature Range - Calcium silicate is normally used for components operating in the temcerature rar.ee of 451 = F to 1300?.
M2 2.2 Components Insulated - Calcium silicate is used for the insulation of carbon steel and alloy piping and equipment.
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Table 1 gives
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000031
M2.2.1 DESCRIPTION
Insulation shall be a segmental, mat faced, felted refractory fiber pipe covering such as mineral fiber pipe insulation.
M2.2.2 SERVICE
M2.2.2.1 Temperature Ranee - Mineral fiber pipe insulation is normally used for components operating in the temperature range of 451? to 1000F. Mineral wool in special cases can be used to 1800.F.
M2.2.2.2 Components Insulated - Mineral fiber pipe insulation may be used on any cylinaerical equipment 36" in diameter or less and it may be used on stainless steel items.
M2.2.3 THICKNESS
Table 2 gives the insulation thickness for components using mineral wcol. For applications above 1000F, thickness should be determined with vendor assistance and/or use of the T-2013 program at CCCTC.
ELAN
M2.3.2.1 Temper at'ire Range - Cellular glass is used
for components operating in the ranee from 90F to'SOQ'F.
M2.2.2.2 Components Insulated - Cellular glass may be used for the insulation of piping or equipment of any material of construction oceratinc in the 90 to 3003F ranee.
M
Thickness of cellular glass and equipment should be dete
sulation used on dned from Table 3
000032
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MATERIALS
8/1/77 |
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M2.4 . 1 DESCRIPTION
The insulation shall be sectional pipe covering of 6# density or rigid sheets and blankets of 3# or 6# density fiberglass.
M2.4.2 SERVICE
M2.4.2.1 Temperature Range - Fiberglass is used for components operating in the temperature range of 90F to 450F.
M2.4.2.2 Components Insulated - Fiberglass may be used for piping, instruments, and equipment.
M2.4.3 THICKNESS
Table 4 gives the insulation thickness for components insulated with fiberglass.
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M2.5.1 DESCRIPTION
Insulation shall be a high temperature mineral wool type insulating cement such as Ryder Thermckate irl-MWP or equal.
M2.5.2 SERVICE
M2.5.2.1 Temperature Range - Insulating cement is used for components operating at temperatures of 71F and above with upper limits depending upon the material used.
M2.5.2.2 Components Insulated - Insulating used for the insulating of irregu such as pumps, turbines, valves. Insulating cement is also used to and smooth the surface of fabrics ccverinc,,
M2.5.3 THICKNESS
The thickness of insulating cement shall be as shewn for mineral wool in Table 2. For irregular surfaces use the thickness shewn for 35" diameter.
000033
IsscmcN: insuiaii:::
^SSlAiNSSZ CHEMICAL COMPANY*
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3/1/77 ! 7
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M2.6.1 DESCRIPTION
Insulation shall be a woven asbestos cloth tape 1" wide x l/*8" thick.
M2.6.2 SERVICE
M2.6.2.1 Temperature Range - Asbestos tape is used for components operating at temperatures of ISO-? and above.
M2.S . 2 2 Components Insulated - Asbestos tape is used on irregular surfaces such as bent pipe and tubing where the use of rigid insulation is considered impractical.
M2.5.3 THICKNESS
Tape shall be wrapped to a thickness of 1/2 inch. If thicknesses greater than 1/2 inch are required, consideration should be given to alternate materials
M2.7.1
n>7
Insulation shall be flexi ci.cs i.ns'uici'iioc
earned clastic oucurar
M2.7.2
M2.7.2.1 Tern; .s usee :cr ccnccn:f 130 = ? and below.
M4
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usee or. bene
cf ricid ins
cIss Ccceracir*?
ns uistiion tenoeracures
2 ----^
s
knass shall be 2/4
mini
'HSc C MJCAL
000034
I S/1/77
\
M2.8 HIGH TEMPERATURE SERVICE
For services in the 1800 to 2300F range, Babcox and Wilson "Kaowool1^ 8-lb density blankets or equal should be used. Insulation thickness should be determined with vendor assistance and/or use of the T-2013 program at CCCTC.
Insulation shall be a rigid cellular glass material in flat block, beveled lags, or pipe covering of sectional or segmental form. M3.1.2 SERVICE
M3.1.2.1 Temperature Range - Cellular glass is used for components operating in the ambient to -350F range.
M3.1.2.2 Components Insulated - Cellular glass shall be used for the following:
a. Piping, instrument or equipment with a diameter of 36" or less.
b. Equipment with diameters greater than 35".
c. Irregular surfaces.
thick smooth. Jackecinc bcth with and without attached moisture carrier are used. Aluminum elbcw covers shall be 0.020" thick.
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LAN=2= CHEMICAL CCMPANV- r-T -^
insulatic:: MATERIALS
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000035
M4.1.2 SERVICE
M4.1.2.1 Moisture Barrier - Aluminum jacketing with attached moisture barrier shall be used over calcium silicate insulation when wet conditions' are anticipated.
M4.1.2.2 Components Jacketed - All straight run piping insulation shall be jacketed with smooth or corrugated aluminum. The following components may be jacketed with aluminum if specified:
a. Insulated elbows.
b. Vertical vessel and exchanger shells with corrugated aluminum.
c. Horizontal vessel and exchanger shells with smooth aluminum.
Mastic shall be a polyvinyl acetate emulsion such as Benjamin Foster Sealfast mastic with ar. aluminum color, or a solvent cutback type such as Lion Nokorode "Sealkote" or a vinyl acrylic such as Childers Vy-CRYL, or Pittccat 300 for cold service.
M4.2.2 SERVICE
Mastic weather barrier shall be used over all insulated components such as pumps, turbines, insrrumencs, valves, exchanger and vessel heads where aluminum jackeuinc is impractical. Mastic shall also be-used for elbows and ecuicment for which aluminum jackeuinr is net soecif
sc: be used whe a service aluminum cr T12.5 1. C .
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2ELAN=3-3 CHEMICAL COMPANY". tl;-.
materials
000036
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10
'M5.1.1 DESCRIPTION
Joint sealer shall be an aluminum gray vapor barrier sealer such as 3enjamin Foster's No. 30-45 or an asphalt base sealer such as Lion Nokorode "Low Temp"
M5.1.2 SERVICE
Joint sealer shall be used on all butt edges of sing layer insulation or outer layer of multi-layer applications.
M5.2.1 DESCRIPTION Glass cloth shall be 10 x 10 thread count or IC x 20
LAN532 CH2M1CAL CCMPA.NYt
! CN: lN SI MATERIALS
000037
8/1/77
l
M5.4 SANDS
M5.4.1 DESCRIPTION
Hands shall be 3/8", 1/2", or 3/4" wide x .020" thick stainless steel with matching double prong seals.
M5.4.2 SERVICE
M5.4.2.1 Aluminum Jacketing - 3/8" wide bands on 9" centers are used to secure all aluminum jacketing.
M5.4.2.2 Pipe Insulation - Bands 1/2" wide are used on 9" centers to secure insulation on pipe greater than 12" in diameter and equipment with a diameter of 36" or less.
M5.4.2.3 Vessel Insulation - Bands 3/4" wide are used on 12" centers to secure insulation on ecuipment or Dice with a diameter greater than 36".
M5.5 WIRE
MS.5.1 DESCRIPTION
Wire shall be 16 gauge stainless steel or galvanized.
MS. 5.2 SERVICE
Wire is used on 9" centers to secure pipe insulation on lines through 12" diameter. Stainless steel wire is used at high humidity locations and galvanized wire is used at lew humiditv locauior.s.
MS.6 SCREWS
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Screws s aluminum screws.
e Me. 8 x 1/2" long ed HEX head or oar.
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CHEMICAL CC.VIFANYrnmcTT
000038
8/1/7' t '/ . \c.
M5.7 WELD PINS
M5.7.1 DESCRIPTION
Wei'S pins shall be 12 gauge minimum 304 or 316 stainless steel and of sufficient length to project through the insulation being secured for attachment of speed clip.
M5.7.2 SERVICE
Weld pin spacing is optional depending on service and type of insulation. Project engineer should specify. Generally, spacing should never exceed 2'0" c-c. At edges and projections such as nozzles, spacing should be closer.
MS.8 SPEED CLIPS
MS.8.1 DESCRIPTION
Speed clips shall be push-on type of 30 gauge sheet metal of either round or square type. They shall be a minimum of 1-1/2" diameter or 1-1/2" square.
MS.8.2 SERVICE
All weld pins shall be topped with speed clips. If weld pins and speed clips are used in conjunction with wire netting, the weld pin should protrude through the netting with the speed clip on the outside of the nettinc.
MS. 9 CHIL-SPRINC-S
H'-AN
bands on larce diamerer ecuitmer.t to allow for expansion or ccncracricn. One Chil-spring should be used above everv 30 feet of strapeing if excessive expansicn/ccncraction is expected (i.e., >2" grower.)
000039
3/1/77
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