Document nevrdKd8kB7rM9gzpN9M9BL6
*
J4f* <03y.M4 (Automated-. --------
CGf)3 COPE KY^Qn7-n
PKO.
- m>~fp 33672
EST. wet, 1080______ LBS.
STD. HRS.
TIME
7x ?m
14 YC-2-B 93 4 Lot
1 \3w a
14 YC-2-B 93 4 LotlW?
14 YC-2-B 93 4 Lot ______
MAKING INSTRUCTIONS: BATCH UNIT
D.V.
PROCESSES
APPROVED BY
( ) KY-907-D (ft ;WK 12/12/77
(J _ ( ) 5C6''12/13/77
( ) M MW 12/15/77
() ()
TYPED BY Tj 2/3/78 "------
/j -'J1'
`7
Total Weig1 ht - 3480#
EQUIPMENT
fc?*EH9KR0L0tSS) - YELLOW MEDIUM
203 Run 33"-(560"6r) water into V-203
& Pour In
205 <5^3 Dun in
1 Record: Start ///*Sjpptl. -- ..........` ...
----,1 ____ ____ Fin /*'* SO.HTX______________
.y ___ (tskP-0^ __'
* Lot , % <y.7 f
NON-BLEEDING USE N ACCT. LBS. CODE LBS.
320 32-D 320 48 x 50 YC-2-B 24G0
.
Pj*rrtTV-203 thru Homoa,,i:Lat IrBOO-ggOfr psi into V-205______,,
When \b203 MTY, waffR' colorNthru Homoq at 1800-2200 d s t usind
__tlffhimum water/ 3^
l(>2
:rRecord V-305- VolL-tfAfiT1 ,JrInspect Homoq strainer &
& ad.i clean
to if
60" (2100 necessary
G)
Tl sv
JO-
Run 10" (514 S) water into SV & start agitator___ _________ POrfio V-205 thru Homoo at 4800-5200 iwsi- into V* ..lA"
Record: Time Start /2L **%"Total Min t 3T2* '
NOTE: ' If Homog pressure rails below 4800 psi, 3-way valve
will recirculate slurrv to V-205
.
WRen V-205 MTY, run in 5" (240 G) water and nun thru Homoq at^4800-5200 osi
s*..
SP 42^SP Step 01 - Set Formula Selector to position #2 (V-24.3) or
& y-'
#7 f V--2441
CP Pressr SV Cam Reset PB-set 22TC in Auto Remote
3 ^(Temperature is set at 19Q-194UF)_____ __________ ______
ir
Record levels^and
^llLG
.%
set Raw Materials Counter - preset #1 80 Gal
#1
as
follows!
*rSet strike flow controllers as follows:
__3BC10 (N-27-D Controller! in Manual
0.83 GPM
b^3E20 (N-27-D Walter) in Manual Local
5.28 GPM
(N-27-D/wai :er Ratio) ________ __ 0.64
-'cL.^ClO (N-32-D Controller) in Manual
1.08 GPM
L_-g>g&C2n (A1-32-D WaterV in Manna! 1 oral _____4.47 GPM.
1 /'fc^EePo .(n -3?-b.. Mater.!, in. Remote
j
1 J^-SFRIO (N-32-D/Water'Ratio)
0.83 1
1. V' .. ... .... ___ ___ i '....... SV i^ [Jberator Steo PB . ~
-___ .
. ... . J
...................
SP 17"|Record Level 2 LG
%. If below 35% follow solution
& make-up procedure for N-27-D
CP p^ t.n 48u (2470.6)
4 Keeord:__d H
_______ ______ !___ ^______ _____________
2TETdi to 11 1-11 3 using N-7-H diluted to 5%
Assume 50%___I
i___ 1 J (10 parts water to"! part N-7-D)___________________ !_____J
L__Slohon into SV__Record:.pH'&fe.;_________ 21- Operator Step PB
; 13829 REV.
------- ----1
15-A 160 . 27.n 275
32-n 1840. _
1
Wq ~ 7-D Quj: f *<
-
EQUIPMENT
pag e 2 c g 03 c o d e KY-9Q7-D (D) es t .w g t . 3480
l bs . use n
ACCT.
LBS. CODE LBS,
,2*sv ,-pp" "SP Step 06/39 - After heat op Records pUTf.T, (9.5-10,0)
SP
Switch 3FC20. 8FC20.8FC2G to Auto
"
***QS&r'& ^ 24- ODerator Step PB
CP "SP Step 10/43 - When 3FC20. SFC10. 8FC2Q water flows In limits
' Switch 3FC10' to Auto, Operator Step PB
'SP Steo 11/44 - When 3FC10. 3FC20 flows in limits, switch
'*****.
- T
p>23
3FC20 to Remote Operator Step PB During strike. Record
pH
&
time
as
follows!
SP Step
.
!
& im
V-243/V-244
pH
13/46-(30 rain)
#7
: 14/47: 60 min)
215/48 ( hrsl v ,&16/49 ( 2 hrs 25 mTn ) 9 )f__ 17/50 ( 3 hrs Final
Range 9.0-10.0 9,0-10.0
9.0-10.0 9.0-10.0 7.5- 8.5
Time -- --
3,2 .
la L <*&
TlAS 'TI iO
Xtk.i.seA Af-27
NOTE:(1) If d H not as specified notify Supervisor & note
in log (2) If final pH is above 8.5, adi pH to 7.5-8.5 & 1
)/ V 29 Sift in
Recordr d H ^
Assume 78% ------------ y
.v-.'-. 50
27-D 128-A
50
***; Sr Add 17" (208 6) water to V-302 Add & stir 2 min for S58
- Assume 50%
FT
7
3JK*
.............. Mrinq strike
. .. Dump
... into. PT............
iWin.
. ... . .
in ............. ..................
Stir IQ: min with lightning mixer for S39
.'. /< * . . ...
..
356 ,*ar Iturinq strike run .20* (244 G) water into V*356
26JS8 , "Turn on steam to (317 G) at 478-182-QF-
___________
Pump PT mixture from S35 thru undersurface JHstrthutor AFAP
-rftf Jlinse PT with hot water from hot water mixer & pump In.
*r<r .Shut..off pump__:___________________________________________ ... ^Sttr 30 min at I78-18PF for S49
"he -not shut off agitator
100
318 36 36
7-0
169-A 155-A 160-A
50
318 36 36
' ,
SV &
\J V
yflltS4L
When s?Q comolete, Close water line &
heat SV to 198-2Q0F in 5-10 discharge valves at stearate
min pump
SP J ^46 Open V-356 Discharge valves to stearate Dumo inlet 9 ^ Sl Open water valve at stearate pump 8 run water thru
/: ' Homog at 29O0.-3100.psi. to sewer
1 ^ / 48 While Homog water at 2900-3100 psi. open homog
/ Mtichange valye to ..-SV ft rloce valve to sewer ....... Immediately Den stearate Dump discharge valve.
Turn on pump & Homog V-356 to SV at.2900-3100 psi .......
f Maintain SV at 198-200F
N> 50 while Homog V-356 to SV, shut off water valve at
SBl Stearate pump ASAP When Homog complete, rinse in -356 with hot wafer
From hot water mixer
DUP050093106
EQUIPMENT
pag e 3 CG 03 c o d e KY-907-D (D) es t . w g t . 3480
l bs.
USE LBS.
SV 1 &V
When. $51 complete turn off Homoa & stearate pump, Stir 5 min at 198-200 'F
SP \ ^54- Shut off steam
9l. Con'T
2
When.S54 complete, Operator PB
SP Steo 23/53 Record d H 3*%
(3,3-3.71
*'"57 If necessary adj pH to (3.3-3.7) (DOWN ONI Y) Record' pH
: NOTE: Dissolve extra N-15-A in water at 110-12OF in drum
Use. + 30 qal of water to 50# N-15-A. Sti r. SV 5: min
after each addition
U- ^ 58 Run in N-7-D from. S31 in
min A stir 5 min
_ ...
u Record- pH tf,if (4,2-4,41 & if necessary add d H 4.2-4.4
& Record-" hH
Assume
(Dilute 10 parts water to 1 part N-7-fl) ^"`'Siphon N-7-) into SV
Assume 1WL -... K
.............
iterator Step PB_________________ ___________________
Upanartor Step PB.............. .. ...... _.................. ........ ,............... .
?P Step fiO - Batch complete 'P<4*Hffp 7j ? t/-' *J-0
N CODE
15-A
... ?7-n ..... '.. .'
ACCT. LBS.
START
FINISH
OPTR
.Tuie 71'f Step Time /i SP Step
~~^TZT~~. .
J/Ieb !*>
... . .. '
7l.ef&A...... %
&
x7-72r
P
"9
7j 4'im
ym 1
\
:
. \\ *
DUP050093107
t
l
DUP050093108
DUP050093109
sLjrnwnsVy
NOON
DUP050093110