Document nNmkLmZEebOd5qjQ2OvNQjORa

AR 426 -- 0717 ACUTE AQUATIC TOXICITY IESTSUBSTANC 000E 000 Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1- Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot numbers were 4 and 6. The test sample is FC-203. Current information indicates it is a mixture of 1.34% PFOS, 35% diethylene glycol butyl ether, 37.85% water, 20% ethylene glycol, 2.66 % Sultone foamer, 3% sodium octyl sulfate, 0.1% sodium lauryl sulfate, and 0.05% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrationsof impurities. Data may not accurately reflect toxicity of the fluorochemical component of the test sample. M-- ETHOD:e-- ee ------ Method: Not given. Type: Various static and Continuous flow screening GLP: No Year completed: 1973 -- 1974 (5 studies conducted) Species: Not given. Supplier: Not given. Analytical monitoring: Temperature, and DO Exposure period: 96-hours, 10 days, and 18 days `Statistical methods: TLso/L.Cso values calculated using Test organism age: Not given. Pretreatment: Not given. Test conditions: Various. Lighting: Not given graphic interpolation. Concentrations dosing rate: Various Stability of the test chemical solutions: Not noted - Exposure vessels: Notgiven NNuummbbeerr ooff roerpglaincaitsemss: p1er replicate: Not given. Number of concentrations: five plus a blank control Water chemistry during the study: Various RESOLTS OOOO Nominal concentrations: Bk control and various concentrations Element values: Study 1 (wk3% concentrate Lot 4}: 000520 96-hour LCso = 0.75 mL. Study 2 (w/3% concentrate Lot 6): Study 3 (Lot946):-hour LCs = 0.075% conc. 96-hour LCso = >1000 mg/L Study 4 (Lot946)-:hour LCso = 0.061% Study 5 (Lot 4): 96-hour LCso = 0.1875% Study 6 (Lot 4): 4-7 day LCso = 1875 mg/L. 8 day LCso = 1525 mg/L 9-10 day LGso = 1250 mg/L Study 7 (Lot 4): 96-hour TLso = 0.0438 (no units, assume % concentrate) Element values based on nominal concentrations Remarks: Testing was conducted on the mixture as described in the Test tShuebsftluaonrcoechReemmicaarlkpsrfoipeolrd.tioTnhealvoanle.ues reported apply to that mixture and not conclusions The test sample LCs, varied among the studies depending on the test type and duration. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 patAQuANTY Reliability: Kiimisch ranking = 3. Testing lacks record of methodology used. Scoanmfpilrmeatpuirointyofwtahse naomtopurnotpeorflfylcuhoarroacchteemriiczaeldparnopdotrthieosntiundythleascoklsutainoanl.ytical - REFgReNCes This study was conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, Lab Request number 2002 and 2009, 1973-1974. o0 mwe0 R 00000000000 Last changed: 6/27/00 000521 Ste stutted; 2-27.73 DBiohsey "Fozos af2one. 2%4Ws j= I asws| % uve]0 P Ee Surat wll Sorvall P EeTaTH Bx 7 . SCAN EEE EAEER = +] p 3 ie Joo Js EN sul ele ql Lot-4 3/Comepttile) | 3 = T&M Cg IM Sorvivat . Abs] hl4% 7IT Surya i LL : 7H > of - +H] 0/ E-- Ee =E: o 2 | oo | fea s2t m1 oeehps " wal -- - 04 1 bn ol "-~ . fe Er Th Se pS IPA I I OT el ge SE "EEFeehing Test E- idml onege . lioll MLcOat" i - od ww aU SeSeaadd Bl TTEYVIVAY AdOD Ls38 = 4d bey rFpad 1 LAB REQUESTBOOK -- 4250 oo Water andWestewater. A008 ( REQUEST FOR LABORATORY WORK Lab ReqJ uest No. : TO: ENVIRONMENTAL ENGINEERING LABORATORY -- BUILDING 53-6N Reams Las Fosorne PRR Name: DALE RACK Requestoste pant --i------ HSoelmdplSeamDaptlee: For D-- aysDatEexN.esTdedi: me:ir |e Date Rec'd. 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Bo A aly FR Fa dE io ol ps To 0 1] rl OTH BC WME PE EER. RBCYH Ou a its Bik eh hE Le SEH OE ped RAH E g Sa Priel EA TE Soolom m Soop Lod: de 3 itLh AAT Fir a }Fi stip te Pk +d HE TC onCICy QNIDA TgEReE)l, choaotke firRtdiH aRA hPlA oaJ d 1Lx deSHRIESRdY LR Tr CET 00% air Wo Ded Ao Dead TiavINAY KioSiE | e] Lol les 2h ALL oad ALL Ded ho yop i500 THE een , o wFL IyERlb EE SE ae iS eokee e E y E = Lna = == Tore 3La mnh TEEr n Te a LidEe EE REEEEEeeE Io ln SEH Ht Sante EEE haa ( GHoiEEAiTEsHnT S nLE B Ee R E EEa Eales a L ng E sE CHEa ER {a ETESS G EE iE RfEEnaaa l giHl INGE I En Geel Hl JERIE E pE uiimE Ees fE e l hfH i si fig RE ER NM E L HSE e SLae he rE Lin eee HERE ApH HRY a ; C V| aoT i1p E A CER TE ENE N NEGt EE f E R T eH HeCE C or |oi ni ' Ls H fiiry roEEn ld didi hihGt [Ha ETDHIU NG Si ET Fp H SE nFH Fo Cae STAs Lihat] celia SET Hi avin) CEE fi 000525 ce: LAB REQUEST BOOK -- 42H oo WaandtWasetewarter REQUEST FOR LABORATORY WORK Lab Reauest No, E 0a30000! TO: ENVIRONMENTAL ENGINEERING LABORATORY -- BUILDING 536N [-- [-- ume: DON BOCA Aecueoste Duero pr-- I EE I Description: NC--203 LaF#4 HSoolmdplSeDuamtep:F_or___DatBeoNyseEsstd. Teidme:: He. Y DHaotseCSopemnptl:ete d: 5 _30_./A = 20-78% PS ~~ Tota Hardnas, ml 5 CaC03 mTTr 11 Calcium Hardness, mg/l as CaCOa TTT 711 TAP AAlksalilniity., mgm/l l35s CCaaCOC3O H--H-- r-- r --H oSmHgEsor [r r r r ] r Nitrate, mg/l 35 NO3 Tr rr Tr Chioride, mg/l as CI Silica, mg/l 355107 TTT 11 rr rrr SiTutorhidPer,oms/plhatose| TTS H ---- -- -- T-- TH T ----H ( Total Phosphate, mg/lasP_ TTioota.lCChhroommiu,m, mmg/giaassCCrr rr TTTr--17 T H r H uy Total Cyanide, mg/l as CN rrr rT 0 Ferrocyanids, mg/l 3s ON 11rrr g Tron, mg/l as Fe. 1rr TrT1 = Wanganese, mg/l as Mn rrr 11 < Surfactant, mg/l ss LAS 1 rrr 11 ZL Phenol. mg! rr rr rr BOD, mg rr rr rr x TOD, mg/l (Short, Long, Dilute) rrr rr Tot SuspendedSolids, mg Tr rr Tr 3 Volatile Suspended Solids, mg/l rrr Tr" Turbidity,mg/lSitica rrr Tre = Total Solids, mg 1rrr TT B Total Volatile Solids, mg/l TTT on Conductivity, mhos Total Bacteria, No./100 ml Tr rrr rrrrr Total Coliform, No./100 ml 11 rr Fecal Coliform, No./100 mt Fecal Streptococcus, No./100 ml 1 rr Tr rrT r r Ammonia Nitrogen, mg/l as N rr Tr liemdidahGi Neitrogen,p mg/i as N rrr rr rr (CoBmlmooessaEno.CATbwopuil dLCe5o/bgRoo708f71 5 | [TTT T11 1 -- TT TT i Enna En a Gna Eoviromanal Eng, Lib ink -- Eien En La.De0de05Re2v79sm COPSY Ma e CU ightodd FE _205 Sah pail ltkulo iT r CohtTol SCYeerivg Yest : ul | Mo Seed . dl Ne, 5 No wl : i ool oawm vo pead woread ' 0.1, AoW No pead . aval . Lol mow ALL ped MLpeat i 10 / aoe Rr ALD gg jaML Pend rE ITN TREE Ee Tad PPM loo [ae rt Goo setatooo": 3 ool 0ois aes oors_ ol. p Mild 16 .4 7 i J. ae : Evely cycle :- | Ave. Tom stk Solution 700rol DOifedlich watel514! 5 / ha siting Skt Ce ole b APs E LE oseR Ad eeCR J stock sian] es ARATE RCRA | VeLe le are \oo, 600 CPM \oos PPI herd Sotcal WPA RE s Re i Ty Ek "BEST COPY AVAILABLE vett= e 4eliiy Sinfso|vaahio l e D5 001sAR00aS i Oo Jon ie . PPM 2)ths 2'stec SooT l rReEleES hsLee a ll TE ne i en Ee RE SRR Faas Co Light wer Fe-2o3 Lob *4 - . leering test wl [XIWA Lemlfe Aeads2 To Jesutienl GL 2H hou!" 1007. Chow tools. wu o.| 16m! IA EY ws Lo reoml 2 yA . e Hal l en Ba AER Le BEST COPY AVAILABLE Ta ( . TM TLEI a TT i Ge ae SE CE CetelaY on pe E Re Rn R O Cl Gpe R ate E ghei eSR ChLlEC E aH n R SRRRSaE a aT CPoE E psigMSEOA O A RE DEREfeiBee hg ET She en ed OS e L Le l sara RE 8s 000551 = Pore starftleed; pe2.31a*s3 hokQu ssAyssy -- FFee--220033-:. g Ib HT E i [oeJoo] wrJoe] Jo]| = Fl Conc.. bs .0\ 24Ws Suv%ual [asve] Tool cans] iP=f Surv%ival (ef PP Sorvivat luof 2658 oon Soru7waE TT G 11S [1 1 vo |oleof1 loo ssa) veo Rlee] , FEE {og | [418 | N 0035| veo 0 |Goferf 100 T las] vee gli TIT top Hdl | Qos ER ve [60 54 \oo vee] ER veo glo ER Ar 06 4 } Sail - SFeehing est! He . TA S 2 \ # Flow vest -- TIAVIVAY Ad0D 153g c= (of stock solution fo stalr with + - Vo per H & oo 250 Soo, 1Se Mess eM ER HE pate staffed; @)day Conc. 22b . Soruwal Biohssy - eX LT 1 Cdk beBh. dno] ABFE s endo] oe5 ANY Nem | iis wl Survwal PP Sorvivar - 1s fi Control Veo [6s 55) Joo [1] 100 i ad ; loo iH wowoo= [ orL[Hl=eo T[a TTrf ode feiiig Tt 5 00 | >|f loo fin re wo ied 4s) FE i al afer J TT | lis 3 Te RE pir 4 SQeeningTest s : | * CFlowtest TERE ec NS = SL EE BN ! sav sion15dg8 | beet pate started;d; ""SlSoiokhsssysy - WT gpm pdDiEds] Tas 2 et |F TLL he } aan] [1I Am Conc. | sw%ont | AD[OPl sevzen fTe ao: l -- 0.025 wo ler I veo 0 vo [67Sof wo ed; | Soru%uat Plow Q ow] LE13 rast CL1i7 a= wo lil Iso TL Voo df waa) Fed CH EE dept LH a a1 005 wo |67]50f ENee veo E= |E[so] Ei fEobE IBHrG | TTT 7 IE SCF leenine q Test: - LE. . CF test il 3 Bos Tr FIEVIYA.Y AO. DIS- IE. CTI Ti Ty rhebh f .F rtreme]hiSie| OTT ER Psartee csrtaatffeedd; Soke Tohssy CT LR Re J Fini ELL ir. Ce) Conc. i veo + ie IE E E EREc= an ad]ed[TaCgae] elTool Sorvwal | Sorvval PP Joo 70 |5;2] foo Joo # {20 caCwvaPeDh Suruivat Sei mi LH Survival. 00L;a in LEH3 EFC 100. ils Csr 2] 3.2, Joo B foo [ ACH alee] 100 | THEE = = 5 4 Fe Er A fot 56 po 106 o \as| . 100, A "Ed IoSizEe: TT S `eeniingnqTTeesstt: L ie Toa :Hat H he h beet avAi donLsv 3d. Tn ET EE Date stalfedts 12-1975 IOASEY = EA pt Bos: Ttowed|wn[uf] = [HIN N[1] L.one. : rd Ea 24%Wws[ef Sorowal Pl Tosa] i 487 es. Sumival tee J q PE |7elE4 a ToFtla Lad OdBE p> Sorat] 1 TPT SorvivAWE LEE [4T 5 EE Sti ER Lens wo [70]So # |4s BN LAR : a Le el] 0LRT PHT A 0 ee wai |ee fol 0 [fd TIN TH 3751. o 0 EYi "7 - AN EEdER [A 5 / EEb al fo fell J oy . ' SGl2eehing Test: 3 Now -- So) (Soommppy) + Gg TIBVAdIODVLsAHSopYnY. L422550" D. [SOeoA.S re - PR ! I K N ELECES SCotock Sclubion tostCaltUwiLth,TTee ||.0337755 QSEanfALb0Y wal AED Ro Pol hid pr Sia Pte staffed;1 2.4.1274-75 OViONSSY --=f/Ce- . 203 Ladho.gs idFL)]fd = tod| 0 Joe] wo Jule ve Jelod wo Jiig x Conc. ON Troe l : bol 244s % Soruwal wo > Pf s3e | |35]f asm| [ool 7 [ey Sorvval PP ee oz z |S 52] we | oso] cane]? Ce Re Survival Mw Log Tami = y) Fle v0 . of . 100. > losh]a4d owi=]eS us) o[oEE{JGEERE : 0025 | veo | 32 oo 0.05 \0o. o " 53 |L 100 TER Sls] vee [e%[aal dor LE oeJel] TR , 50! Voo ole6s5 34] = 00| FJORS EEN Bi 0015 | ves | [52 \oo 50 o lesan Ee ot fe [elo ow ld 0 dled] 0 |H BEST COPY jAVAILAB fee aie StFechingTest: ggn eglaictest a ~ - I 100 aso 7y 20) aos willed= nE i ooo Seo 750 Jose 1d ..a0S i oars. alAiieing Egrr a i itf EeLo CBE onads I aia dt_ewnm alfiaernp .TRes bT a a TS e hh fFs e y e Si e hy ) TT ates fie a ! 5oRtheed:eeskgaz CP TEET HEEEATE ~~ S ak welcs uGrig wooobil Li Mesd- LiCsa= Te i [oT re LL Lal ;5 2 IRE ! ala H + E i a1ah HE 4 Doe EE eSl i Quo f S HE Eo |i giol a. n CRIES ai Ebi ae Li Seal ea Fo inn Ely Sian Pai iVOTH lat; Hip sie ERE hh lean , J! 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A009 REQUEST FOR LABORATORY WORK Lab Request No._EEF TO: ENVIRONMENTAL ENGINEERING LABORATORY -- BUILDING 53:6N Recussor Lab Peon -- ad wd [75]| orion TB TR NParmoej:et N0o.. [SALOF)Fo_nmNowequeCsotodnetde Sample Date: Date Needed: ______ Hold Sample For _____Days Est. Time: _______ Hrs. ? DE OAsntaevRencdSgmples Date Complewed: S \= J -- Hrs.Spent: _ ~ \S ~~ CTaTolttalaAlHaHkradanleirs,sd, nmimgte52s5CCsaacCC0O5s.003 H r It I Er -- r 0 4 TMT Alkalinity, mg/l as CaCOs 3Seemme------------ HF -- Tr rT 17 7 | CNihtrratie,,mgm/alfas3N6O1. r rr T T r T =LT SiFlica,emomll 3102 TrTr z TOrotahoPPhhoosspphhaattee,mmagT/l aassP H--H-- rJTr x Tioot.alCChrraommiu.m,mma/TlCas Cr H--H I -- --F -- 1 -- QO FiiTsouelysCyiadneid,e.mmoylseseOnN r rr r rr r r bWoul oSFPmahientngoili,cenuemeni,:nlnotTessiLAmS E H t TH S t E E-- 1 2OTo0DtD.a,SorusggpeSnderd SCoogy amih r r Ir E EE S r rI r r E---- VTToooltratbiSiloedtiSsuyms,,opeminadSeidteSsolids, mg/l r H rrr r r r r r TToounldaVciavaiyl,mSholoisds mal Tort SacerNoTOT r r Ir r r T rr r TFeoctaalCCoolfrouem,NNooT0000 amT r TT n TTT FeQARcimraeloaaorSGauaenmptsNNoiimcrsooocmpcgunesT g.,,mm,Nagloa.s/10m0i r r T rrrT r " rr Bisassay, 25s PPA [J75[1/535 [Jase 11 Le 7J "117 =~ T117-- 1 _-- ee05a1 tE e Enon ra. Li Gary Enrol Er. Lub BkE -- Esra En, Ls Sd--en vr Coy oo A 3 . (FemestaMali Rio assay study --C.Fhw Hest 5 7d les [eis ppm hbke I 8. 2dy LisestSosper Foo 9-lody lesos Laso ppM. a Lisgov338,0 Jan dL i + Ny aE : 1 ! ;|; Ee Woepm 2 =o EN 8m x wy : AN bo 24 swowal : ; Vo i | " So, SN \ a bl : . : . |: ; Ce Ko de ee TT TR TTT ge TT or 000542 owes fied pane #B2iopsy -T 220% Lot 4 ConA c. ped of w= of eas E7N [enfIbDeOm}). SamiTezal feng PY EA Serva I 4 : wy dflap [Tio] fee] ol % bias Soruial x .e S2 TF So JpPe 425 fo | w|So] Joo [HY Ligpps bh So Ty fat| So. LY So:f loo PREY] BRT TX Fd : Th So fv E50L,odHgekd 2,500 a. ; Ii e) TOi T HiY; TT SotemnmmTest | # C Yop test Ea 7 [ire oi Pop 5] .y To. Ye 25 solution to. shalt WINETBAYdIo1V8A3gY 4 2asz hi oo0ase 00k25 0laSe 0\RIS 9ASoo Te ETI Pathodds . Biohsey - ~ Sozod La a CONC. 2A SSC orunl AB ||. Sirw=wal Eo on 7M Dies EEL > PP Survival PP sorvmt |P atloret|e oo|Je [LTN HHe SN TAL ] A] 625 Ios 4s] oo l.2, Ne aGe {aR[1E= |BN AT H Ce fe T HEe ATTN Flows test :g L? 23 ! FIBVIVAY AdOD 1538 . m EEE Be eee SEE een DE smn ! 2 HEFH EEE HE Ti T LTT LL r F-- t Esobm gHEmHEHE Hisntls HlHH FH :#5 EEErEEbE HE T E EE E e3E eiTH H| EiEFgEA D11 E L HEh EE EEEeEe HH HH HH RE ETETT eR ETHHE HH - HHT EE ee REE r 5 tH i Lp PR EH TE OEE pe ii EE EEgE aE t ee TR nH nH Ee Bi EH fits, EH a HH ERG THT Te TT Ty Bi HEE HEEL Lm nn TE sir LETTERED LT a HOE a PE HEmERRESRR ESTEE HTOEREEEEREHE ERE E Hann EHH RR EE nn Th . He grb ag E PET HER STE ETRE : [REEbY ERR HH HERE SZH =F EEE OE ET rr TT TT TT Ta a Ln subi I SHtH ti ha bia LH i HHH 2 wie wie le 000