Document n9j7pD5bvYYJN6dX6515d9E8X
Interoffice Communication
(conoco)
TO: FROM: DATE: SUBJECT:
Brandt Butler, Lake Charles Refinery Paul Steele, PED, Ponca City
January 31,1990
SARA Title Ml, Section 313 Documentation 1988 and 1987 Reporting
Attached is the documentation supporting the 1988 Toxic Chemical Release Inventory for the Lake Charles Refinery as required by SARA Title HI, Section 313. This information must be kept readily available for a minimum of three years from the reporting date (until July 1,1992).
Also included is the documentation supporting the submission of updated rqlease estimates of 11 chemicals for the 1987 reporting year. This should be kept with the original 1987 doc umentation.
To avoid confusion during future reference to 1987 documentation, please remove the first page from the new 1987 binder and place it at the front of the old 1987 binder, this will redirect attention to the new binder when inspecting the data and calculations for the aforementioned chemicals.
Please contact me (ext. 5903) if you have any questions.
Paul E. Steele Process Engineer Environmental Group Technology Section
Process Engineering Division
Ik
cc w/att: cc w/o att:
J. E. Cearley, Houston DFM/LES, LWC Clyde Rhodes, S&T, Lake Charles
File EV-1040.1
SAL 000005621
SARA TITLE XII, SECTION 313 1988 TOXIC CHEMICAL RELEASE INVENTORY
REPORTS AND CALCULATIONS LAKE CHARLES REFINERY
SAL 000005622
LAKE CHARLES REFINERY TABLE OF CONTENTS
I. LIST OF CHEMICALS REPORTED
XI.
1988 RELEASE SUMMARY FOR REFINERY
III- 1988 REPORT FORMS ( FORM R )
IV.
CALCULATIONS
1. Calculati onal Methods and Assumptions 2. Sample Calculations 3. Chemical Specific Calculations
a) Release Inventory i> Amount Released per Medium ii) Percentage of Total Release Breakdown
b) Waste Treatment Methods and Efficiencies c) Release Calculations
V. AFPENDICES
A. Reportable Toxic Chemical List Development i) Technical Services List of Chemicals API Refinery List ii) Threshold Calculations for Reportable Chemicals iii) MSDS-HISS Computer Scan
B. Emission Factors i> SOCMI Emission Factors ii) AP-42 Hydrocarbon Emmision Factors iii) Wastewater Release Table <EPA Guidance Document) iv) Chemdat 6 Land Treatment Emission Model v> Vapor Pressure Data
C. 1988 Operating Expense and Yield Data (Blue Book)
D. Maximum Amount On-Site Calculations
i) Calculations
ii) 1988 Louisiana Tier Two Inventory Forms
Instructions
E- Process Stream Composition Data i) Gas Stream Composition Data and Calculations i. i > Liquid Stream Composition Data and Calculations
000005&23 SA^
Solid Waste Release Data and Calculations i) Solid Waste Disposal Summary ii) Solid Waste Release Calculations iii) Chemdat h Land Treatment Model iv> Solid Waste and Spent Catalyst Analytical
Data
Wastewater Treatment Release Data and Calculations i) Wastewater Secondary Treatment Release Calculations ii) Wastewater Analytical Data iii) Wastewater Discharge Self--Monitoring Reports iv) Wastewater Treatment Release Table (ERA Guidance Documt) v) Wastewater Primary Treatment Release Calculations
Storage Tank Release Data and Calculations i) Storage Tank (Point) Release Summary ii) Storage Tank Release Calculations (Spreadsheet) iii) 1988 Equipment Inventory Survey (EIS) (Tank Capacities,
Throughputs, and VOC Release)
Process Equipment Fugitive Release Data and Calculations i) Process Fugitive Chemical Release Calculatiohs ii) Process Fugitive VOC Emission Calculations iii) Process Drains Fugitive Release Calculations iv) Cooling Tower Fugitive Release Calculations v) Bailers & Heaters (Fuel Gas) Fugitive Release Calcs vi) Fugitive Emission Source Count in Process Units iv) Fugitive Source Leak Frequency Data
Product Loading Release Data and Calculations i) Loading Loss Release Summary ii) Loading Loss Release Calculations (Spreadsheets) iii) Product Loading Records (1988) iv) Product Specifications
SAL 000005624
LAKE CHARLES REFINERY 1988 SARA 313 REPORTING
LIST OF REPORTABLE TOXIC CHEMICALS (26)
Aluminum Oxide (u) Ammonia <u) Benzene (m,p) 1,3-Butadiene < m,p,u) Chlorine (u) Cobalt compounds (u) Cumene <m,p) Cyclohexane (p) Ethylbenzene <m,p) Ethylene (m,p,u> Hydrochloric Acid (u> Lead compounds <p) Manganese compounds <p) Methanol (p,u) Methyl t-Butyl Ether (p) Molybdenum Trioxide <u) Naphthalene <p,u) Nickel compounds <u) Phosphoric Acid <u) Propylene (m,p,u) Sodium Hydroxide soln. <u> Styrene (p) Sulfuric Acid (m,u) Toluene (m,p) 1,2,4-Trimethyl benzene (m , p) Xylene (m,p>
m manufacture the chemical P process the chemical u otherwise use the chemical
SAL 000005625
1988 RELEASE SUMMARY LAKE CHARLES REFINERY
RELEASE, LBS/YR
AIR
NON-PT
POINT
WATER
LAND ON-SITE OFF-SITE
Aluminum Oxide Ammonia Benzene
13 Butadiene Chlorine Cobalt Compounds * Cumene Cyclohexane Ethyl Benzene Ethylene Hydrochloric Acid Lead Compounds ** Manganese Compounds * Methanol MTBE ** Molybdenum Trioxide Naphthalene Nickel Compounds * Phosphoric Acid Propylene Sodium Hydroxide Styrene Sulfuric Acid Toluene
1,2,4 Trimethylbenzene Xylenes
910 2200 18000 1300 2000
15 13000 12000
9000 14000
610 400 250 1500 1 100 120 7200
11 NA 140000
0 880 <499 41000 8400 51000
44000 NA
1 7000 NA NA NA
570 8500 1600
NA 16
0 0 760 8700 NA 1200 NA NA NA 0 27 460 14000 170 7700
NA 3100
39 NA NA NA 39 39 39 NA
0 0 0 0 2 NA 47 NA 0 NA 0 39 0 39 39 39
NA NA
0 NA NA NA
0 0 0 NA NA NA NA 0 NA NA 0 NA NA NA NA 0 NA O 0 0
1100000 NA NA NA NA
2700 NA NA NA NA NA NA NA NA NA
21000 NA
1900 0
NA NA NA NA NA NA NA
TOTAL
325395
104703
3461
0 1125600
NA = Release is not applicable * - Not reported as compound in 1987
= 1988 -first year reported * = A cal cul ati onal error was made in estimating point release of
cyclohexane. See cyclohexane calculations and Appendix H.
SAL 0Q0005626
(conocoj
North American Refining
Conoco Inc.
P.O. Box 37
Westlake, LA 70669
(318)491-6211
CERTIFIED MAIL - RETURN RECEIPT REQUESTED (P 845 189 239)
CERTIFIED MAIL - RETURN RECEIPT REQUESTED (R 845 1$9 ZW
54.
June 30, 1989
U. S. Environmental Protection Agency P. 0. Box 70266 Washington, D.C. 20024-0266
Mr. R. Bruce Hammatt, Emergency Response Coordinator Office of Water Resources Louisiana Department of Environmental Quality P. 0. Box 44091 625 North Fourth Street Baton Rouge, Louisiana 70804-4091
Dear Sirs:
1988 Toxic Chemical Release Inventory Conoco Lake Charles Refinery
The Toxic Chemical Release Inventory Reporting Forms for the! Conoco Lake Charles Refinery are attached. If you or your staff hpve any questions regarding this report, please contact Brandt iButler, (318)491-5599.
Manager Lake Charles Refinery
DEK/ds att bcc w/o att:
PFM/ESJ SHD/LTW PBB RDT/AJN DEK Jack Cearley - RMT-RM-NA, TA 3042, Houston Terry Thoem - MA 1142, E0HS, Houston Paul Steele - 220 ST, PED, Ponca City
bcc w/att: File: 54.73 EPA11: DEK-06-23-89
SAL 000005627
rorm Approvoa OMo ro.:__^
Approval Expires:____01/92
^ P/\ U.S. Environmental Protaction Agency
TOXIC CHEMICAL REUEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Plannhng end Community Rlght-to-Know Act of 1986. else known es Title HI of the SuperimJ AmentSnoms end Reeuthortzetlon Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION INFORMATION
(TNe space for your optional use.)
wPvoatoiAtrhMyHfeoraocnmtirieoMpforMairsrtiaanongMahahtobtoafumnrdiesenaasrhtriotamawsrapsotantdaphaatios,r
rinseipfraunosttsa.nstt]obsdsnsrgefttabnmalaotratrtanvotadmantga daoattaecans,aaoda$bdm, taagndandamomoipnftatatinnsangathnad SoaaatMnlmdseaotttoaanmomroefanntsIynwfeofrmhmaar tiiaoganp.eesetsInocSlfuuddthianings
SgfeSKK
WBaMRWnueaaadrdnssduahhecgiinHnnteiggooamttnnqooedunnnl,.ttjotoOOPtar.hyrn.CoCad.j.eOA2cB0f2ftffu00aicd04ierg80se.0o,(t2f A0MPO7tat^0fnnfe-i:0ohrw0aa0otTt3raRo)fnc.fI
1.1 Ara you claiming tha chamieal Identity on paes 8 trade eeerott
l * Jt. 1 1 Vas (Anahor question 1.2;
No (Oo not amw 1.2;
Attach substantiation forms.)
Oo to position 1.3.)
1.2
tt "Yes* in t.t, is this copy: [ ] Sanitised [ ] tlnsanitlaod
1.3 Rooney* 19 88
2, CERTIFICATION (Reed and sign after completing al tactions.)
I lawny eartlfy that I hma reviewed the MticM dacunmif and that, to tha MM o( my inomlidpe and MM. tha submitted information is trua and complete and that tha amounts and valuat in this report are aeeurata based on reasonable astimaias using data available to thha Bnpaift pi this report.
Naim and eHMai Mila of owner/operator or ssnior
Don R. Unruh, Refinery.Manager
Official
Signature
Dat* signed
FACILITY IDENTIFICATION
Facility or EstabUshmonC Moms
Conoco Lake Charles Refinery
________________________________________________ WHERE TO SEND COMPUTED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Streot Add ass
Old Spanish Trail
3.1
City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-02^6
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendflt E)
This rsport oontains Information tar (Chacfc one):
3.2
a. [X ] entire facility
[ 1 Part of a faculty.
Technical Contact
3.3 Brandt Butler
Public Contact
3.4
Don R. Unruh
SIC Coda (4 digit)
3.S a 2 911
b. NA
3.6
030
latitude
Minutes
14
Dun a Bradstraat Nunba(<)
3.7 . 00-842-7692
e.
Seconds
36
CPA Uantiftoatton Nurrfear(s) (RCRA I.O. No.)
3.8 aLAD990683716
NPOES Permit Nuntta|t)
3.9 aLA0003026
rtsoaMno Straams or Water SMs (antar ona nama par boa)
,3ayou Verdine
Telephone Number (Include area coda)
318-491-5599
Telephone Number (Induce area eodt)
318-491-5222
d.
Degree*
093 NA NA NA b. NA
a.
Longitude Minute
16
f.
20
3.10
SAL 000005628
LtadargrwM hfacttan Wail Cods <UC) UantHicattan Nurrfcerts)
3.11 NA
4. PARENT COMPANY INFORMATION
Mama of Parsot Company
4.1 E. I. DuPont de Nemours
4.2
Parant Company's pun ft Bradstraat Niertaer
00-131-5704
EPA Form 93S0-1 (1-69) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
. PUBLICLY OWNED TREATMENT WORKS (POTWe)
1.1 POTW nm
1.2 POTW nam*
M______________ ______________________________________________________________________________________
Street Address
Street Address
City
Coutty
City
State
Zip
Stele
Pag* 2 of 5
County zip
Z- OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHCH WASTES are SENT ONLY FOR RECYCUNQ OR REUSE).
2.1
Off-site location name
BFI
EPA tdentllestian Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Comy
Calcasieu
State
Louisiana
zip
70664
Is location under control of reportlno taoMtty or parent company?
2.2 Off-sit* location nam*
NA
EPA idenlllloetMn Number (RCRA D. No.)
Street Address City
County
State
ZIP
Is location teeter control at reporting (acuity or parent company?
| [ ]vw [xl*0
[ ]v- [ u
. Off-tit* location name
2.4 Oft-sit* location nam*
EPA MenCHIeetlon Mites (RCRA O. No.)
EPA WentIdeation Member (RCRA O. No.)
Ctreat Address city Stele
County zm
Street Address City Stele
County Zip 1
ft locetfen under control of reporting facility or parent company?
2.5 Off-sit* location nama
( ]ve*
[ ]no
fs location under control of reporting facility or parent company?
2.6 Off-sit* location nam*
[ lv,, [ ],,
EPA UentHicallon Number (RCRA D. bto.)
EPA Identification Nun Sin (RCRA D. No.!
Street Address
Street Address
City
County
City
County
State
Zip
State
Zip
location inter control of reporting tedNty or parent eonwany?
[ ]v,, [ u [ ] Cheek IT additional papas of Part t we attached, ibw many?
Is location wider control ot reporting facility or parent company?
SAL 000005629 , Jl Yes
l
J No
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form,)
-ft EPA
REPA FORM
PART |H. CHEMICAL-SPECIFIC INFORMATION
Page 3 of 5 (Tills space for your option*] use.)
1. CHEMICAL IO ENTITY{Do not complete tM* section If you complete Section 2.)
1.1 [Reserved]
CAS Number (Erftar th* number exact* es tt appear* on the 313 list. Enter NA If reporting * chemical category.) 1.2 1344-28-1
Chemical or Chemical Category Name (Enter the name exact* as It appears on the 313 list.)
1.3 Aluminum Oxide Generic Chemical Name (Complete only if Part l, Section 1.1 is cheeked "Yes." Generic name must be etruelturai* descriptive.}
1.4
MIXTURE COMPONENT IDENTITY 1Do not eorrwiete this section If you complete Section 1.) 2. Generic Chemical Name Provided by Oippllcr (Limit the name to a maximum of 70 characters (e.g., numbers, tetters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check a* that aoolv.)
Manufacture the chemical:
3.1
ti
a.l J Produce
If produce or import:
f 1 For on-site C-L J use/processing
f .l
1 For sale/ J distribution
b. [ ] Import
e.[ ] As a byproduct
f.[ ] A* an Impurity
process the 3.2 chemical:
,f * 1
d.[
1 wa-mem
J As a reactant
] Repackagtng onfy
h f 1 A* * formiiatton
-l J component
[ 1 As' an article J component
3.3
Otherwise use the chemical*
f vlAs a chemical
*-l AJ processing aid
r 1.
^^
b.l J As a manufacturing aid
fl!
c.l J Anpftary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OUR1NG THE
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Reiaasa (tos/yr)
You may report releases of less than 1,000 fee. by checking ranges under A.t. (Do not use both A.l and A.2)
A.l Reporting Ranges
0 1-496 900-099
A.2 Enter
Estimate
5.1a {][][]
910
5.2 Stack or point air emissions
[S.2a I [ 1 [ 1
44,000
5.3 Discharges to receiving
11
streams or water bodies 5-3-1 L_J
(Enter latter cod* from Part I
Section 3.10 lor stream(s) m
in* box provided.)
j1 5.3 2 1 1
5.3.3
5.3.1a {][][] 5.3.2a [][][] 5.3.3a [Hill
NA
B. Basis of | Estimate] (enter code]]
ES.lb
;
5.2b El
5.3.1b O 5.3.2b O 5.3.3b E)
5.4 Underground in]ection 5.5 Releases to land
S.S-1 On-sit# landfill
5.5.2 Land Yreatment/apolicatton farming
lS.4a ] [ 1 [ ] 5.5.1a [][][] 5.5.2a [][][]
NA NA NA
*.* 5.5.1b D 5.5.2b C3
5.5.3 Surface impoundment
5.5 3l [][][]
NA
5.5.3b | |
5.5.4 Other disposal
5.5.4a [][][]
NA
5.5.4b Q
[ ] (Chac* H additional information * provided on Part rv-Si^plamontal Information.)
EPA Form 9350-1(1-89) Revised -- Do no; use previous versions.
SAL 000005630
(Important: Type or print; read instructions before completing form.)
gpA
EPA FORmR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 of 5
--
r --------------------------------------------1
(This sp4ce for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
of teas than 1 ,000 lbs. by checking ranges under A.1. (Do not use both A.1 and A.2)
(tos/yr)
A.1 Reporting Ranges o t-aoB soo-eeo
A.2 Enter
Estimate
Oltcftarp* to POTW
,-------. ,-------,
tamer location number I . | I
[]{][]6.1.1 from Part I. Section 1,) 1 ' 1 \____J
HA
(enter code!
CDi.I.lb
Other off-ttta loeatlon (antar location numb#)
J00 ffrom Part I, Section 2
]f
][
1 1,100,000
Other off-tlla locationf* | |
_ - _ (enterr, location nnuummbo^ ^ | ; | 6-2.2 from Pan a. Section
1 LJLI J HA
Other fi-iite location (enter location mantoer
6.2.3 from Part I, Section 2.,
[Mill
6.2.1b
O6.2.2b
6.2.3b
[ ] (Check if additional Information Is provided on Part IV-Snaplemental Information.)
Dispose)
16.2.1c M iJ 2-
6.2.2c 6.2.3c M
7. WASTE TREATMENT METHODS AND EFFICIENCY
A- General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Ranoe Of
influent Concentration (enter code)
D. Sequential
Treatment? (cheek If applcabie)
E. Treatment Efficiency Estimate
F. Based on Operating Oata? Yes
No
7.1a
7.1b ZEE
7.1c 0
7.Id [* ]
7.1a
7.2a
7.2b
ZEE
7.2c
7.2d lx 1
7.2e
7.3a 7.4a
7,3b 7.4b
n|a
7.3c 7.4c
7.3d 7.4d
[1
l1
7.3# 7.4#
7.Sa 7.6a 7.7a
7.6a
7.9a 7.10a
7.5b 7.6b 7.7b 7.8b 7.9b 7.10b
7.5c 7.6c 7.7c 7.6c 7.9c 7.10c
7.5d [ 1
7.6d [ 1
7.7d t 1
7.6d
l1
7.9d [ 1
7.10d [ 1
7.6# 7.6# 7.7# 7.8# 7.9# 7.10#
[ ] (Check If addibonaJ Information It provided on Part IV-Supplemental Information.)
99,9.
7.,, 7.2,
[ ] [X ] [ ][X]
7.3f [ ] [ ]
7.41 l ] l ]
7.Sf ,7.6f 7.7f 7.8f 7.9f
[ ][ ]
MM
[ ][ 1 till
[ 1[ ]
l 1[ 1
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actions taken to reduce the amount of the chemical being released from the fscftty. Items and an explanation of what Information to Include.)
T See the Instructions for coded
A. Type of Modification (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action Center code)
Current reportktg
year (fca/yr)
Prior year (Ibsfyr)
Or percent change
M
fcKA Form 9350-1(1-89) Revised - Do not use previous versions.
SAL 000005631
(important: Type or print; read instructions before completing form.)
-SEPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section if you need addMonsf space tor answers to questions In Part Ml. Number the ines used sequential? from Cnes In prior sections (o.g.. 5.3.4. 6.1.2. 7.11)
Page 5 of 5 (Thrt space lor your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III. Section 5.3)
You may report releases of less than 1.000 tos. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Rsisase (fes/yr)
A.! Hsporth>g Ranges
0 Jrsss _ sop-ess _
a.2 Enter
Estknate
S.3 Discharges to receiving streams or
water bodies
5.3..
(nt tetter coM front Pert I Sectton 3.10 lor ttroim(t) in 5 3 the boa provided.)
5.3.
. 5.3_____.[Miff
. 5.3. .[][][]
J[ 1 [ ] [ ]
5.3.____
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of iess than 1,000 lbs. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (Ibs/yr)
A.1 Reportktg Ranges
0 I-4S0 soo-seo
A.2 Enter Estimate
B. Basis of Estimate
(enter code in box
provided)
C. Type of Treatment/ Oisposal
(enter code in box
: provided)
_. 6.1. _
Otsenaree to POTW
_ ___
tenter location lumber 1 . 1 1 1
win Pan 1. Section 1.) 1 1 M____)
[][][]
6.1._______b O
Other oh-erte teeatten <
e9
(enter toeation number 1*11
6-Z -----------Jmm Pert . Seetton 2.) 1 * 14
1 1
[][][]
Other eW-elte toeation j-- f i 6.2._______issTpiStVass?? i * _____1
- IfOM Pin ft, SiCUOA 2.1
Other oil' eHe location
, ----
e9
(enter location number 1 * 1 1
6-2------------iron* Pan a, Sectlona.il *14
1 1
[][][] (][][]
6.2._______b 1 1 6.2._______b 6.2._______b
6.2._c|M| | |
*.2.
e|M| | |
*.2.
eM | |
ADOmONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III. Section 7)
A. General Wastestream
(enter code In box provided)
8. Treatment
Method (enter code kt box prorided)
C. Range of Influent
Concentration (enter code)
0. Sequential
Treatment? (check tf sopacabis)
E. Treatment
Efficiency Estimate
F. Based on Operating Oata? Yes
No
7-- 7--b LL1J
rrri7.
.Q
7.
b
7.
c Q 7------------o[ ]
7.
e
7.
c0
7.-----------d[ ]
7.
e
%'i 7-
% 7.
[ ][ ] f ff 1 1
J. l ] If ]7.
7._c
7----------- [
7.______e
% 7'[
7.
dlU- > 7. 1 1 1 i | | ||7. .D 7-_______b
7- b IJJJ 7. 7- b | | | |
7. ,, cm
7-----------
7.------------ [ ]
Q7-_______c e Q7-----------
* 7. e Q 7----- < Q
7.-----------d[ 7. d[
7. d[
---- -I 7----- <>[
]
]
] 1 ]
7.______e 7.______ e 7. e 7.______ e 7.______ e 7.______ e
*
'[ If 1
-f% '-- H 1 % ' [ If ] % <[ ][ ]7-----------
% :* `MM % >--M H 1
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005632
(Important: Type or print; read instructions before completing form.)
horm Approved OMB No.: 2070--0093
Approval Exp*r*s:_--2i2L
Page 1 of S
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1966.
also known as Title HI of the Superfund Amendments and Reauthorteatlon Act__________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public reOertlnQ burden (or this collection of Information la aatlmaiad to
voy Own 30 to 34 hourt par wipanw.
with an avaraoa of 32 hours par
time tar rentawnng
aaanjdlnti existing data
_ , arlno and matataVuno tha data nudkd. and eomptatlne
_ ' oodaction of intormaltan. Sand eomntants regarding tM bwden
stimata o# any other aspact of ins
oofiactto of Information, indudirv
wgaHona tar raductao ttaa burden. to
Chief, Information Policy Branch
(PM-223), US EPA, 401 M St.. SW.
Washington, D.C. 20440 Attn: TRI
Burden and to tha Offica of Information
and Papulatory Attain, Offica of
Manaqaman and Budget Paperwork
Adduction 1 Project
(2070-0083).
W O.C. 20603.
====
1.1 Are you claiming tha chemical identity on page 3 trade secret?
1.2 If *Yea* in 1.1. Is this copy:
1.3 Reporting Year
[ ] Vas (Anvar question 1.2:
[ ^ ] No (Do not answer t.2;
Attach substantiation forms.)
Go lo question 1.3.)
1 1 Sanitised 1 J UnsarVtiaed
13 88
2. CERTIFICATION (Reed end sign efter completing ell sections.)
l hereby certify that l have reviewed tha attachad aoeunwM and that, to tha bast of my knowledge and belief, tha aubmHtad intarmatian is trua and eametata and that tha amounts and values In this report ere accurate based on reasonable estimates uskta data available to tha preparers pi this report.
Name and official title of owner /operator or senior management official
Don R. Unruh, Refinery Manager
Signature'
lata signed
3. FACILITY IDENTIFICATION Facility or Establishment Name
Conoco Lake Charles
Street Address
Old Spanish Trail
3.1
City
Westlake
State
Louisiana
Refinery
County
Calcasieu
ZIP Code
70669
______________________
WHERE TO SEKlD COMPLETE!D FORMS:
t. U.S. ENVIRONMENTAL PROTECTION AGENCY P<0. BOX 70266 WASHINGTON, DC 20024-0266 ATTN: TOXIC CHEMICAL RELEASE INVENTORY
2. APPROPRIATE STATE OFFICE (See instructions Appendix E)
This report oontalna Information tar (Chock one):
o.2
Technical Contact
3.3 Brandt Butler
Public Contact
3.4
Don R. Unruh
..[x] An antIr* facility
[ ] Part of a ftaHtr.
Telephone Number (Inches
318-491^5599 j
Telephone Manber (include area code)
318-491-5222
SIC Code (4 dtaft]
9.3 .2911
b. NA
c.
d.
a. f.
3.6
Bayess
030
Latitude Minutes
14
Osoaiii
36
Degrees
093
Lonoltude Minutes
16
Seconds
20
Dun A Bradstreel Number(s}
3.7 . 00-842-7692
b. NA
EPA Identification Number(t) (ACKA I.O. No. >
3.6 .LAD990683716
b. NA
3.9
fs*>OES Permit Ntmbar(s)
.LA0003026
rteoehnnQ Stream* or Water Bodies (enter one name per dox)
..Bayou Verdine
b. na
b. NA
3.10 c.
a-
a.
Underground Section Well Code (IRC) tdentHieatlon Number (s)
3.11 aUA
PARENT COMPANY INFORMATION
Name of Parent Company
4.1 E.I. DuPont de Nemours
4.2
Parent Company* s Owi A Bradetreet Number
00-131-5704
EPA Form 9350-1 (1-69) Revised--Do not use previous versions.
t.
b.
SAL 000005633
1
(Important: Type or print; read instructions before completing form.)__________________________________page 2 of S
**
rf--cOPAA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
(This space for your optional use. j
1. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name
Street Address
City
County
City
County
State
Zip
State
ZiR
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHCH WASTES ARE SENT ONLY FOR RECYClmO OR REUSE).
2.1 Off-slte location name
BFI
EPA tdentltieetion Number (RCAA O No.)
NA
Street Address
Cities Service Hvy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
b location under control of reporting facility or parent company?
2.2 Off-slte location name
NA
O.CPA UtMfffeaUon NunW (ACftA
NO.}
Street Address City
County
State
Zip
is location undsr oontroi el reporting facility or parent company?
[ ]vea [x]n
[U [U
2.3 Off-site location name
2.4 Off-slte location nams
EPA Identification Nwnbar (RCAA O. No.)
EPA UsnMHcatlen Nwwoar (RCAA D. No.)
Street Address City
County
Street Address Ctty
Cowty
State
Zip
Stste
Zip
Is location under control of reportmg facility or parent company?
[ ]v
[u
2.5 Otf-site location name
Is location under control of reporting faculty or parent company?
2.6 Off-slto location name
[; ]v..
[ ].
EPA tdemiliealion Number (RCAA O. No.)
EPA Identification Number (RCRA O. No.)
Street Address
Street Address
City
County
City
County1.
'tate
Zip
State
zip '
S location under oontroi ot reporting (entity or parent company?
[ ] Yes
[ ] No
Is location wider control of reeertlng facility or parent l company?
[ ] Chock tf additional pages of Part are att served. Hew many?
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
Pag* 3 ot 5 (This space for your optional use. |
1. CHEMICAL IDENTITYfDo not complete this section H you complete Section 2.J
1.1 1.2 1.3 1.4
(Reserved] CAS Number (Enter the number wMtly it wai on the 313 ut. Enter NA II reporting a chemical category.)
7664-41-7 Chemical or Chemical Category Name (Enter the name exactly a* n appears on the 313 Hft.)
Ammonia Generic Chemical Name (Complete only H Pert I, Section i. i le cheeked 'Yes. * Generic name muet be structurally descriptive.)
MIXTURE COMPONENT IDENTITY (Do not complete this section tt you comoiete Section 1.1 2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum pi 70 characters (e.g.. numbers, letters, spaces, punctuation).)
3. ACTIVITIES ANO USES OF THE CHEMICAL AT THE FACILITY (Check al that asolv.)
Manufacture the
if produce or Import:
chemical: 3.1
rt
a.l J Produce
f 1 For on-site c.l J usa/processktg
.f d-l
1 For sale/ J cSitrtbutlon
b. [ ] Import
e.[ ] As a byproduct
f.[ ] As1an impurity
Process the 3.2 chemical:
f a* l
d. [
1 J Ae a reactant
] Repackaging only
. f 1 As formulation b.| J component
f 1 As) an article c-l Jco^nponent
Otherwise use 3.3 the chemical*
fv 1 As a chemical a* LX J processing aid
.f 1
.
b.l J As a manufacturing aid
Jf 1 :
c.L AnCMary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENOAf Ol 4 I (enter code!
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (fcs/yr)
You may report releases of less than 1.000 t>s. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l Reporting Ranges
0 1-4SS 500--90S
A.2 Enter Estimate
5.1 Fugitive or non-point elr emissions
5.1a [][](]
2,200
5.2 Stack or point air emissions
5.2a (][][] NA
5.3 Discharges to receiving
LI
[][][]streams or water bodies a-3-1 LLJ
5.3.ta
(Enter letter code from Perl l
Section 3.10 for stream(s) In the box provided. >
1|
S.3.2 1___1 -----
5.3.2a [][][]
n5.3.3 5.3.3a [][][]
3,100 NA
5.4 Underground Injection 5.5 Releases to land
$.5.1 On-elte landfill
5.5.2 Land freatment/applicatlon farming
5.4a [][][] 5.5.1a (HIM 5.5.2a [][][]
NA NA NA
5.5.3 Surteoe impoundment
5.5.3a [][][)
NA
5.5.4 Other diepocal
5.5.4a (][][]
NA
B. Basis ol I Estimate: (enter code)
5.1b to 5.2b [I
5.3.1b D3 5.3.2b O 5.3.3b O
$.4b J___1 5.5.1b P 5.5.2b Qi 5.5.3b G] 5.5.4b O'
1i (Cheek 11 addition*) information is provided on Pert rv-Supp*emeniaf Information. >
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005635
o EPA
EPA FORM^
PART Ml. CHEMICAL-SPECiRC INFORMATION (continued)
(This spice for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfer* of less than 1,000 bs. by checking ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfers
(bs/yr)
A.1 Reporting Ranges
0 1-400 500-009
A.2 Enter Estimate
B. Baa)* of Estimate (enter code)
OlteMrgi to POTW
Ienter location number I .If
6.1.1 from Pert , Section 1.) Mil
,
1 [][][]
NA
(.1.1b
i
I. Type of Treatment/ Disposal
Other efl-site location __ . . , (enter location number I * II
6.2.1 from Pen . Section 2.) I z l |
| [][][]
NA
.1b 6.2
Other ff-elte location
^
6.2.2
[!][
][
l[
1
6.2.2b
Other ort-ilte location _. ....j
6.2.3 aarpM`aa,[I].g[
][
][
1
i.2.3b I I
[ ] (Cheok If editions) ^formation Is provided on Part (V-Supplamenta! Information.)
7. WASTE TREATMENT METHOOS ANO EFFICIENCY
A. Genera! Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Ranoe of Influent
Concentration (enter code)
O. Sequential Treatment? (cheek If applcable)
E. Treatment Efficiency Estimate
F. Based on Operating Data? Yes
No
.7.1
7.2a 7.3a 7.4a
GO
0
7.1b 7.2b 7.3b 7.4b
rTi
EE EE
7.1c 7.2c 7.3c 7.4c
7.Id 7.2d 7.3d 7.4d
[1 [1 [1 [1
7.le 7.2e 7.3e 7.4a
36 % 98
7.1f TM
[ 1 l X1
[ ] [X ]
7.3f [ 1 [ ] 7.4f ( ] [ ]
7.6a 7.6a
7.Sb 7.6b
[
7.Sc 7.6c
7.Sd 7.6d
[1 []
7.5e 7.6e
f 1[ 1
[ 1[ 1
7.7a 7.6a
7.7b 7.6b
[
7.7c 7.6c
7.7d [ 1 7.8d [ 1
7.7a 7.8a
T-" [HI
*" l 1 [ ]
7.9a
7.9b
[
7.9c
7.9d [ 1
7.9e
17.9f [ ] [
7.10a 7.10b
7.10c
7.10d [ 1
7.10a
{ ] (Check If addKJona! Information la provided on Part IV-Supplemental Information.)
r.,o, [ ] [ ]
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
A. Type of Modification (enter code)
u
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
Current reporting
year <b/yr)
Prior year
(Ibs/yr)
( Or percent . change ,
1 1% i
EPA Form 9350-1(1-89) Revised - Do not use previous versions
C. Index
O. Rekson for Action (enter code)
LrJJ
SAL 000005636
(Important: Type or print; read instructions before completing form.)
Page S of 5
St PDA
EPA FORM R
^ trM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need adrftionaf space for answers to questions In Part III. Number the tines used sequentiatiy from tines tit prior sections (e.Q.. $.3.4, 6.1.2. 7.11)
(This tipace lor your optional use.|
--i
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
(Pan HI, Section $.3)
You may report releases of less than 1.000 fcs. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Releasa (tos/yr)
A.1 Reporting Ranges o i-w soo-ess
A.2 Enter Ettknate
5.3 Discharges to
.------
receiving streams or
[][][]water bodies
$-3--------1------I 5.3.____a
8. Basis if Estimate
(enter code In box'
provided!
5.3______bQ
C.% From Stormwater 5.3_______c
lrter tetter coda from Pan <
II
Section 3.10 tor *treem| In c ]
II
[][)(]ihe boa provided. J
---------------
S.3_____a
[][][]5.3_____a
5.3.
b!T~ 5.3.
c
bS5-3-_____
S3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1,000 lbs. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (fasfyr)
A.1 Reporting Range#
0 i-ese too ess
A.2 Enter
Estimate
8. Basis of Estimate
(enter code in box
provided)
C- Type of Treatment/ Disposal
(enter cotie In box
provided)
PUcherge to POTW
,, . .
6i wi
iJfIS*atk2J5E?T > N
_ kffnrtfi l SAOliQn 1*)
[][][]
6.1._______b O
Other oft--ette Wrilhn f --^ p--1 -*_______ttpfrttS2&,
Other oft atte location r--j i 1 i
6.2.
(enter location nwvWer 1*11 1
-----------tram Pert i. Section?. 11--1*1_____1
[][][] [][][]
Other eff-she Inc alien *--
f$
(enter location number | * 1 1
6-z------------(ramPet a. Section 2.| 1*1.1
1 [llltl 1
__ ns.2.
b
6.2._____to
6.2._____b
.?
e|M| 1 1
.*.
e |m| | |
M
c|m| | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Pert HI. Section 7)
A, General Wastestream
(enter code
in box orovidedl
8. Treatment Method
(enter code h box provided)
C. Range of intoent Concentrattor
(enter code!
0. Sequendai Treatment? (check If
aoptieabiel
E. Treatment Efficiency
Estimate
F. Based on Operating
Data? Yes
No
* * i n i>_______ rm7. . Q 7. -
| | |7. . Q 7. b
|
7 --'* 7---e 7---e
7. <,[ ]
d [7---------[7-----------d
1 ]
7. 7. 7.
e e e
% ? ' t ] [ -[% 7- H ] % 7- [ H
1 1
11 i i [ ] ? '[ J[ 17.
7---e
7----------- d
7.______ e
%
7-- 7. .Q
> ra'i 7.--b l LL.,1
7--- 7---e
d[7----------7. d[
] ]
7.______e ^ 7. e
[% 7---
H
]
* * '[ J[ 1
7.
7- 6 1 LL.I 7--- 7-----d( 1 7.e
% '(HI
7 b||| |
7--- 7-__ -[ ] 7.______e % 7---[ H 1
7. .Q 7---> Mil 7--- 7 d( 1 7. e % 7- ? 1 H 1
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
SAL 000005637
Form Approved OMB iNo.: 2070-0093
Approval Expire*
(Important: Type or print; read instructions before completing form.)
Paoe 1 of S
^pyy U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency PlanNng and Community Rlght-to-Know Act of 1986.
also known as Title III of the Superfund Amendments and Reauthorization Act
EPA FORM
R
PART I,
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public fiporttng bwden tor thi*
eeUoctlari ot information M ttUmitad to
vary from 30 to 54 hnn par ropan**. wtth an, average ot 32 hour* par
taduoing time tar ravfewInQ i. searching eidstlng Oat*
. _ ithertng ana matmalrung the Oata nadad. and completing and
raataaOngi tha coOeetton of Manhattan.
Band oorhmanta regarding thi* burden estimate or any other aspect ot this
oottaction ot information. Including
suggestion* tor reducing this burdan. to Chief. Ihtormeitan Policy Branch (PM-223), US CPA. 401 M St.. SW.
Washington, O.C. 20460 Attn: TO Buroan arid to tha Ottie* el information
and Regulatory Affairs. Oftioa of
Management and Budoat Paperwork
Reduction
Project
(2070-OOS3).
Washington. O.C. 20603.
1.1 Are you claiming the chemical identity on page 3 trade secret?
1.
[ 1 Ye* (Answer question t.2:
[ No (Oo not answer 1.2;
Attach substantiation lorms.)
Go to cueslien 1.3.)
1.2
ft *Yes* In i.t. Is this copy: [ ] Sanitised [ ] Unsanittaed
1
1.3 ftaocrtlng Year
19 88
2. CERTIFICATION (Read and sign after completing afl sections.)
andt hereby canity that I have raviawad tha attached documents and that, to tha boat ot my knowledge and batlot. tha submttiad Mtarmattan is trua r raport.complete and that tha amounts and vaiuas in this raport ara aocurata basad on raaaonabla aatlmatas using data avallabia to th^ praparars of this
Name ard official title of owner/operator or sanior managamant official
Don R. Unruh, Refinery. Manager
Signaiura
Oata
3. FACILITY IDENTIFICATION
Facility or Establishment Nemo
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1
City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu 2. APPROPRIATE STATE OFFlck (See instructions
Zip Code
70669
Appendix E)
This raport contain* Information tor (Choc* one):
3.2
Tachnlcal Contact
3.3 Brandt Butler
Public Contact
3.4
Don R. Unruh
-.[x] An anttra taciHty
b. [ ] Part ot a facility. Telephone Number (Incjuds
318-491-5599
Tsiaphona Nmbar (tndyde mm
318-491-5222
SC Coda (4 dgitl
3.5 *2911
b. NA
c.
a.
m.
3.6
Degree*
030
Latltuda
Minutes
14
Second*
36
Degree*
093
Longitude Minutes
16
Second*
20
Oun a Bradstreet Nurrber(s)
3.7 . 00-842-7692
NA
EPA Idantlficatlon Number'*) (RCAA I.D. No.)
3.6 * LAD990683716
NA
NPDES Permit Numbar(t)
3.9 .LA0003026
rteoahing Stream* or Water Podia* (enter one nama par boa)
aJJayou Verdine
NA b. NA
3.10
Undergram
3.11 aHA
actIon Wail Coda (UIC) tdanttflcation Number(t)
4. PARENT COMPANY INFORMATION
Name ot Parent Company
4.1 E.I. DuPont de Nemours
Parent Company* s Oun 6 Bradstreet Number
4.2 00-131-5704
EPA Form 9350-1 (1-89) Revised--Do not use previous versions.
SAL 0000a563F
(Important: Type or print; read instructions before completing form.)
A r-r-1A
O' trA
EPA FORM R
PART 11. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
t. PUBLICLY OWNED TREATMENT WORKS (POTWa)
1.1 POTW name
NA
Str#t Address
1.2 POTW name Street Address
Page 2 of 5
{This spice lor your optional use.)
-------------- J-
City
County
City
County
Slat*
Zip
State
i Zid
\
2. OTHER OFF-SITE LOCATIONS (OO NOT REPORT LOCATIONS TO WMCH WASTES ARE SENT ONLY FOR R6CYCUNG OR REUSE).
2.1
Off-site location name
BFI
EPA Idemideation Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Cowity
Calcasieu
State
Louisiana
Zip
70664
la location under control at reporting facility sr parent company?
1 [ ]y~ [xl**
2.2 Off-site location name
NA
EPA identitieation Number (RCRA D. No.)
Street Address City
Cowtty
Stale
Zip i
Is location tMer control at reporting facility or parent company?
[ ]v-
f ]
Off-site location name
2.4 Off-site location name
EPA Identification Number (RCRA O. No.)
EPA identification Number (RCRA O. No.)
Street Address City
County
Street Address City
County
State
Zip
Stale
Zip
1* location under control of reporting (acidly or parent company?
2.S Olf-skte location name
[ ]y
[ ]no
Is location wider control of reporting facility or parent company?
2.6 Off-site location name
Uv-
[ ]*
EPA tdantltteation Number (RCRA C. No.)
EPA Identification Nunfear (RCRA O. No.)
Street Address
Street Address
City State
County Zip
City State
County 1
Zip
|
- location under control of reporting tecMtty or parent company?
[ ] Yes
[ ] No
Is location wider oontrpl of reporting faculty or parent Company?
[ ] Check If addmonej pages of part 1 are attached. How mww?
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
-&EPA
REPA FORM
PART IM. CHEMICAL-SPECIFIC INFORMATION
Page 3 of 5 (tJ space for your optional uss.)
1. CHEMICAL lDENTTTY(Do not complete this taction K you complete Saction 2.)
|
1.1 (Reserved)
CAS Number (Enter the number exactly * ft appear* an the 913 ni. Enter NA it reporting a chemical category.)
1.2 71-43-2
;
Chemical or Chemical Category Name (Enter the name exactly at >t appears on the 319 list. |
1.3 Benzene
Generic Chemical Name (Compiata only H Fart t. Section 1.1 rt checked "V**.' Generic name must be structrealty descriptive. | 1.4
.
1------------------------------------------------------------
MIXTURE COMPONENT IDENTITY (Do not comdete tHt section if you comdete Section 1.)
2. Generic Chemical Name Presided by Supplier (Limit the name to e maximum of 70 characters (e.g.. lumbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check l that apply. >
Manufacture the
If produce or import:
chemical: 3.1
ri a.l XJ Produce
T c.l
yA1J
For on-site usa/procassing
\
b. [ X] import
.( ] As a byproduct
f. [
1 For sale/ J distribution
As; an impurity
Process the 3.2 chemical:
Otherwise use 3.3 the chemical'
r 1 . .. * l XJ A# * r#acum
d. [ ] Repackaging only
f 1 As a chemical *'l iprocessing aid
. f 1 As a formulation bl J component
f1
b.L J Aa a manufacturing aid
f 1 Aslan article c.l Jcotlnpcnent
fl' c.l iAncMary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURINQ THE CALENDA
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than 1.000 bs. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l Reporting Ranges
0 t-4 S00-CM
A.2 Enter Estimate
5.1 Fugitive or non-point air emissions
S.la (][][]
18,000
B. Basis of
I
Estimate I (enter co^ejl
5.1b
i1
Tj j
5.2 Stack or point air emissions
5.2a [][][]
17,000
ol
5.2b
5.3 Discharges to receiving ... j a 1 streams or wster bodies S-3-* 1--1
5.3.1a [][][]
39 S.3.1b (M
(Entor iottar cod* from Part I Section 3. to tor treem(t) tn
the box provided.)
|1 5 3 2 1____1
-------
5.3.3 Q
5.3.2a [)[][] 5.3.3a [][](]
NA
5.3.2b |____1 5.3.3b Q
5.4 Underground injection
5.5.1 On-t(ie landfill 5.5.2 Land traatmant/applicatien farming 5.5.3 Surface impoundment 5.5.4 Other d<potal
5.4a [][][]
5.5.1a {][][]
5.5.2a [
1t
1l
1
S.5.3a [][][]
5.5.4a [][][]
NA NA
0
NA NA
5.5.1b ! 5.5.2b Q| 5.5.3b []] 1 5.5.4b n
[ ] (Check It additional information is provided on Part tv-Supplemental Information.
EPA Form 9350-10-891 Revised--Do not use previous versions.
SAL 000005640
u
(Important: Type or print; read instructions before completing form.)
Pag* 4 of s
o EPA
EPA FORM^
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of lass man 1.000 bs. by checking ranges under A.1. (Do net use
both A.1 and A.2)
A. Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-499 SOO-999
A.2 Enter Estimate
8. Basis of Estimate (enter code)
Discharge to POTW
... .
(enter location number { . 1 |
[][][]6.1.1 from Fen I. Section 1.| 1 1 M___j
HA
6.1.1b O
d.Type of Treatment/
Disposal
j (enter code)
Other otr-elte location . .-------, - - , (enter location number 1 | (
[6-2-1 from Pen a. S*ctkm2.)| f |-|. .. |
i
Other off-eite location . . ----
,
[6.2.2
f(reonmterPlaorct aat.ioSnencutinoSnjZsr .\lLo_Z_lMl ___1
Other oft--site localion
---J
6.2.3 tarp2h?Kss?.) 130 f
'i l
r f f
][ if 1t
i HA i l
6.2.1b Q 6.2.2b CH 6.2.3b
$.2.lc lMl
^.2.2c |m| 6;.2.3c [m| 1
[ ] (Check if addttlonal Information la provided on Part IV-Stppiemental Information.)
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of
influent Concentration (enter code)
D. Sequential Treatment 7
(cheek tf appleable}
E. Treatment Efficiency Estimate
F. Based on Operating Data? Yes
No
7.1a '.2a 7.3a 7.4a 7.5a ?.6a
0 0
7.1b 7.2b 7.3b 7.4b *.Sb *.>
1 B11 I1 1
1 Job 1 l U 1
1 .1 1 1 1111
7.1c 7.2c 0 7.3c 7.4c 7.5c 7.6c
7.1b [ ]
7.2d [ I
7.3d [ ] 7.4b [ ]
7.5d [ 1
7.6b [ ]
7.1e 7.2a 7.3a 7.4a 7.5a 7.6e
N
00
95 % 100
%
7.1f ?.2f
5k t.3f
% t-4f
* 7.5f
% 7.6f
[ im [ ] [x]
(x j t t 11
i ]
[ 11 i l 11 )
7.7a
7.7b
|| 1 1
7.7c
7.7b [ ]
7.7e
% 7.7f [ i [ ]
7.6a 7.6b | | | |
7.6c
7.6d [ 1
7.8e
% 7j.8f [ 11 i
7.9a 7. rrn
7.9c
7.M [ ]
7.9e
% 7i9f [ 11 i
7.10a 7.10b | | | |
7.10c
7.10b [ ]
7.10a
[ ) (Check If addKtonal Information la provided on Part IV-Supplemental Information.)
% 7,10f [ i [ ]
8. OPTIONAL INFORMATION ON WAST MINIMIZATION
(tndtoate action* takan to reduce tha amount of the chemical balng ralaaaad from tha facflty. Saa tha Instruction* for coded
Itama and an explanation of what Information to Include.)
______________________
A. Type of Modfflcation
(enter code)
8. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
(m0
Current reporting year <be/yr|
Prior year (bs/yr)
( Or percent . change {
\ 1* t
:N 1
EPA Form 9350-1(1-89) Revised - Do not use previous versions.
SAL 00000564,1
(Important: Type or prim; read instructions before completing form.)
Page 5 of S
^A rI-nfVa-V
PART IV.
REPA FORM
SUPPLEMENTAL INFORMATION
ITtas fpace tor your optional use.)
Use this section If you need addhionai space for answers to questions In Part HI. Number the Snes used sequentU*y from Ines in prior sections (e.g.. $.3.4. 6.1.2, 7.11)
-4- --
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE {Part III, Section 5.3)
You may report releases of less than 1.000 lbs. by checking ranges ixtder A.1.
(Do not use both A. 1 and A.2)
A. Total Release (*>s/yr)
A.1 Reporting Ranges
0 >-499 $00-999
A.2 Enter Estimate
B. Basis {of Estimate
(enter code in bo^
provided)
5.3 Discharges to receiving streams or waterbodies
.--.
[](][]11
--------*--* 5.3_____*
C.% From Stormwater 5.3. --.bljZI
5.3.._ c
(Eniw letter code lr" P*rt 1
J1
Section 3. to tor etree/n(c) n c ,
1)
[Millthe boK provided.)
--------'------1
5.3_____a
[][][]S.3. -- D 5.3_____a
5.3._____bL 5.3._____c
jns.3._____
S.3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1.000 trs. by checking
ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-4S0 SOO-999
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
.. 6.1.
Discharge to POTW
.-------- __
(enter loctilon nertwr 1 . 1 1 tram Port 1. Section 1.) 1 1 |.)
1 I
[][][]
8.1._____b Q
Other ort-eite tocetlon <--. r - -i
e 3 (enter toealton number 1 1 1 1
--------Vom
*. Section Z.) 1 * U 1
Other ert-efte loeetlan r--i i --i
-2---
Lil-U
[Hill [][][]
6.2._____b I"! 6*2._____b Q
;2.____c|M| 1 1 8^2. c|m| | |
Other off-eHe tocetlon
i
e n (enter location number 1 - 1 1 --------from Pert A Seelton 2.) 1 Ml
1 1
l
11
1[
1
6.2._____b Q
e|Ml | j
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III. Section 7)
A. General
Wastectream (enter code In box provided!
B. Treatment Method
(enter code In box provided)
C. Range of Influent Concentration (enter code)
O. Sequential Treatmet*? (checstf apoteatotel
E. Treatment Efficiency Estimate
F. Based on Operating Data?
Ves
7, 7.
7.
-[ 1
7,
7. [ H
7. 7.
7.
--[ 1
7. I ][
No
1 1
7. 7.
7.
.-[ 1
7.
7. I H 1
7. 7.
7.
.-[ 1
7. { ][ ]
7. 7.
7. 7. 7. 7. 7. 7.
7.
[1
7.
--[ 1
7. 7. [ 1
7.
1
7. I H 1 7. [ ][ 1
7. [ H 1
7 . [ ][ 1
7. 7.
7.
EPA Form 9350-1 (1-59) Revised--Do not use previous versions.
-[ 1
7. [ If
000005642 SAL
1
Form Approved OMB Njo.: 2070-0093 Approval Expires:. _ 01/91
(Important: Type or print; read instructions before completing form.)
Paoe 1 of s
o-EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1986.
also known as Title 111 of the Superfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
vary from yWn an
ting txaean tor this Information ta estimated io
34 howtpefMponM.
ot 32 hours par
KfiStor
owe data
tuna tar reviewing
wwdna existing data MrtaQ and maintaining tha
completing and
. ., eoltaeitomn of information.
Send
estimate or
eoitaettan <of Information, InduOM
suggestion^ tar reducingthis burden, to
Chief, Intarmaitan Policy Brawn
us epa. aoi m st.. sw.
Washington, O.C. 20480 Attn: TRi
Burdsn and to tha Offiea of Information
and Regulatory Attain, Office ol
Manogomeril and 8udoat Paperwork
Reduction
Protect
(2070-0093).
1.1
Are you claiming the chemical identity on paoe 3 trade secret?
1.
[ 1 vea (Answer question 1.2;
[ No (Do not answer l.2:
Attach substantiation forms.)
Go to ouetitan 1,3.)
1.2
tf 'Vea* In 1.1, ta this copy: ( ] Sanitized [ ] Unaanitlzed
1.3 Reporting Year
19 88 J
2. CERTIFICATION (Read and sign after completing a> sections.) 1 hereby certify that 1 have reviewed the attached document* and that, to tha best of my knowledge and beiief, tha submitted httmaiion is true and complete and that the amounts and values in this report are aeorate based on reasonable estimates using data available to the preoarers of this reoort.
Name end official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
77^77
Date signed
fr?
3. FACILITY IQENTIFICATi
Facility or Establishment Name
Conoco Lake Charles Refinery
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Addres*
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report eontalne Intarmattan tar (Check 3.2
..[x] An entire facility
>. [ 1 Part of a facility.
3.3 Technical Contact Brandt Butler
3.4 Public Cantset Don R. Unruh
3.5
6C Code (4 digit)
.2911
3.6
030
b. na
Latitude Minute
14
Oun & Bradatreet Number(s)
3.7 . 00-842-7692
EPA identification Nwnber(s) (RCRA I.O. No. )
3.6 .LAD990683716
NPOES Permit Numbar(a)
3.9 ..LA0003026
Receiving Streams or Water Oodiss (ants
..Bayou Verdine
c. Seconds
36
box)
d.
Degrees
093 NA NA NA b. NA
Telephone Number (Include area code)
318-491-5599!
Telephone Number (Include area code!
318-491-5222 !
Longitude Minutes
16
f.
Seconds
20
3.10
SAL 00000564-3
Underground bisection Weil Code (LSC) UMHieiUan Nt*rtaer(s)
3.11 ..NA
PARENT COMPANY INFORMATION Mama of Parent Company
4.1 E. I. DuPont de Nemours
Parent Company* a Out & Bra
4.2 00-131-5704_____________________________________
EPA Form 9350-1 (1-69) Revised--Do not use previous versions.
u
(Important: Type or print; read instructions before completing form.)________________________________ ___________________Pag2of 5
O' CtKDAA
11. RPART
EPA FORM OFF-SITE LOCATIONS to which toxic
CHEMICALS ARE TRANSFERRED IN WASTES
(Thrt apace for your optional use.)
1. PUBLICLY OWNED TREATMENT WORKS (POTWt)
1.1 POTW name
NA
Street Address
1.2 POTW name
Street Address
City
County
City
Cpwtty
State
Zip
State
ZIP
i-- -
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHK5H WASTES ARE SENT ONLV FOR RECYCLING OR REUSE).
2.1 Off-site location name
BFI )EPA Identification NurrOer (RCRA O. No.
NA
Street Address
Cities Service Rwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
h loeatien under control of reporting (adUty er parent company?
2.2 Off-slte location name
NA
EPA Identllicattan Number (RCRA C. No.)
Street Address City State
County Zip1
It location under control at reporting facility or parent company?
[ ]y- [xJm*
ru [u
2.3 Off-slte location name
2.4 Off-alta location name
EPA Identification Nuitir (RCRA O. No.)
EPA tdantlfteation Number (RCRA O. No.)
Street Address
Street Address
City
Oenty
City
County
State
Zip
State
Zip
is location under control of reporting facility or parent company?
2.6 Off-site location name
[ ]v~ [ ]
K location under control of reporting facility or parent oonwany?
2.6 Off-site location name
[ ]v,, [ U
EPA Identification Numb*- (RCRA O. No.)
EPA identification Number (RCRA O. No.)
Street Address
Street Address
City State
County Zip
City Slate
Cowity |
Zip
Is localIon undar control of reporting facility or parent eowyny?
[ ] Ves
[ ] No
M toeatlon wider control of reporting tadltty or parent jeompany?
[ ] Check if addKIenai pages o< Pvt are attached. How many?
EPA Form 9350-1(1-89) Revised--Oo not use previous versions.
(Important: Type or print; read instructions before completing form.)
pnA X* C"M
EPA FOBM R
PART III. CHEMICAL-SPECIFIC INFORMATION
Page 3 of 5 (Tt^is space for your optional use.)
1. CHEMICAL IDENTTTY(Do not complete this section If you complete Section 2.)
1.1 1.2 1.3 1.4
[Reserved) CAS Number (Enter the number exactly as it wm on the 313 list. Enter NA if reporting a chemical category.)
106-99-0 Chemical or Chemical Category Name (Enter the name exactly as ft appears on the 313 ust.)
1 . ^ - Riit-sHIftne Generic Chemical Name (Complete only It Pen l. Section 1.1 >* checked "Yes.* Generic rwme must be structurally descriptive.)
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1. t 2. Generic Chemical Name Provided by Stppflar (Limit the name to a maximum of 70 characters (e.g.. numbers, tatters, space*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check a that apply.)
'
Manufacture the chemical:
3.1
rv i
a.lA J Produce
If produce or import:
fX 1 For on-site c.L J use/processing
. f 1 Fflr sale/ " l J distribution
b. [ ] Import
e.[ ] As a byproduct
f. [X ]a^ an impurity
Process the 3.2 chemical:
fv 1 a. IX J Aa a reactant
d. [ ] Repackaging only
JK \ 1 As a formUatton
b.L component
Jf 1 Aai an article
c.l component
Otherwise use 3.3 the chemical*
f 1 As a chemical *- t J processing aid
Lf ]4 b.L J As a manufacturing aid
TV1 e.LXJ AnbMary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SfTE AT ANY TIME DURING THE CALENDAI
(enter code)
5. RELEASES OF THE CHEMICALTO THE ENVIRONMENT ON-SITE
A. Total Release (tos/yr)
You may report releasee of lees than 1,000 toe. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 t-499 500-099
A.2
Enter Estimate
5.1 Fugitive or non-point air emissions
5.1a [][](]
S.2 Stack or point air emissions 5.3 Discharges to receiving
,streams or water bodies 5-3-
5.2a [][][]
5.3.1a [][][]
1.300 NA
NA
(Eottr tatter code from Peri l
Section
tre*T'l) *n
the box provided.)
I 5.3 9 I
I I
0S.3.3
5.3.2a [][][] 5.3.3a [][][]
B. Basis of
Estimate (enter code
S.lb
5.2b i.3.1b Q
i.3.2b O
C. % From Stormwater
5.3.ic
NA
5.3.2c
5.3.3b
5.4 Underground injection 5.S Releases to land
5.5.1 On-sfie landfill
5.4a [][][]
5.5.1a [][][]
HA NA
S.4b 5.5.1b
5.5.2 Lend treatmeni/epplicetion terming
5.5.2a M11.M
HA
5.5.2b
5.5.3 Surface impoundment
5.5.3a [][][]
HA
5.5.3b
5.5.4 Other disposal
5.S.4a [][](]
[ J (Cheek If additional Information i* provided on Part IV-Supplementa I kntormation.)
NA
S.5.4b
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005645
(Important: Type or print; read instructions before completing form.)
^ FPA
EPA formR
Pag* 4 of 5
(This spaeje for your optional use.)
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
1
You may report tranefer* of leas than t .000 to*. by checking ranges under A. 1. (Do not use
both A.l and A.2)
(b*/yrj
A.l Reporting Ranges
0 1-409 SOO-999
A.2 Enter Estimate
Otoeharg* to POTW
,,
Temsr location number [.If
>.1.1 from Port I. Section 1.) I 1 II
[][][] NA
Other off-elte location ,-------, _ _ . (enter locatlen nuiear I - II
6.2.1 from Part a. Section 2.| ( * (1
.
[|
Other f1-*Ke location (enter location ntmbe
.BOfrom Part I. Section 2
Other oh-Ue location (enter location number
BQ[6.2.3 from Part I. Section 2
1C
1[
i[
1f
1[
lr
I NA
1
1
(enter code)
1.1.1b n
6.2.1b 6.2.2b 6.2.3b
[ ] (Check if adrfftionai Information ( provided on Part IV-Supplementaf Information.)
Disposal
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
6. Treatment Method
(enter cede)
C. Range of
Influent Concentration
(enter code)
7.1a
7.1b
01
7.1c
Q7.2a
7.2b
7.2c
7.3a
7.3b
7.3c
14a
Q
7.4b
[.
7.40
7.5a
7.56
7.6a 7.eb rr
7.7a 7.6a 7.9a
7.7b 7.6b 7.9b
Q
Q
Q
7.5c
7.6c
7.7c 7.6c 7.9c
7.10a
7.10b
7.10c
O. Sequential Treatment 7 (check If appteabfe)
7.1d [ 1
7. [ 1
7.3d [ 1
t7.4d
1
7.5d [ 1
7. " [ ]
7. 7d [ ]
7.6d [ ] 7.9d [ ] 7.10d l 1
E. Treatment Efficiency Estimate
7.1* 7.2* 7.3*
7.4*
7.6*
7.6* 7.7* 7.6* 7.9* 7.10*
[ ] (Check H adtftionaJ Information te provided on Part IV-Supplementaf Information.)
P. Based on Operating
Data? Yes
No
7.if [ 1 [ ] 7.2f [ ] [ 1
7.3f [ 1 f ]
7.4f (111
[ni
t-* t n i
7.7f
[ ][ 1
7.6f [ ] [ ]
t 1[ 1
7.10f [ ] [ ]
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
A. Type of Modfflcation (enter code)
10_ 1
B. Quantity of the Chemical in Wattes Prior to Treatment or Disposal
Current reporting year (bs/yr)
Prior year (bs/yr)
| Or percent
j change
4
1 11 *
EPA Form 9350-1(1-89) Revised - Do not use previous versions.
C. Index
D. Reason for Action (enter code)
|r|. J
SAL 000005646
(Important: Type or prim; read instructions before computing form.)
o EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section H you need addflional space tor answers to questions In Part hi. Number the Ines used eequentlaiy from 8nes m prior sections (e.Q.. 5.3.4. 6.1.2. 7.11)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
(Pert III. Section S.3)
]
You may report releases of less than 1.000 bs. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (bs/yr)
A.1 Reporting Ranges 0 MW 500-099
A.2 Enter Estimate
5.3 Discharges to
--
receiving streams or
[][][]water bodies
5.3.--L-J 5.3_____a
B. Basis of Estimate
(enter code In box!
orovkiedl
C.% From Stormwater
5.3_______c
(nw letter coo* Imm Pert l
Section 0.10 tor itream(t| m c 3
1 I
1 I
5.3_____a [][][]
the oo provMod.)
-----------
s.3._n 5.3_____a [][][]
5.3.____b[jl 5.3_______c
5-3._____b[p 5.3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL tN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6)
You may report transfers
A.Total Transfers (bs/yr)
B. Basis of Estimate
<t. Type of Treatment/
Oisposal
of less than 1.000 bs. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 i-m sotheee
A.2 Enter Estimate
(enter code In box
provided)
(enter code
' In box provided)
,. 6.1.
Oteduqt to POTW
,.
* |.|(enter location urrter 1 . 1 |
from Port 1, Cectlow t.) 1
.
1 I
[][][]
tf~l6-1._______
Other oft-Me location
* |a 9
fontor location number 1
*<J-`------------irom Part I. SectionJt.| 1
1 1.1
,
[1
1
1[
1[
1
Other ott-slte location 1 1 p-e
! |6.2.
(enter loeatlm number
21 1
[][][]-----------Lem Part a. Section*.) LU I-------1
*> 1 16.2._______ O.2._______b
c|M|*2._____ | | 6-iz. c|m| 1 1
Othar oW-ellt toeatlon - <--*
c9
(enter location number 1*11 1
* [][][]b z*-----------from Part 1. Section 2.) 1 I Ij
O6.2._______b
6f 1 Ic|m|
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Part HI. Section 7)
A. *G**e--n--e---r-a-l*
a8. TTrreeaetlment
^C. RfteainMgae moIf
f0t. ^Se- q---u- e---nt*ia-*l
CE.^Treatment '
CF. CBased on
Wastestream
Method
Influent
Treatment?
Efficiency
Operating
(enter cede
(enter code
Concentration
(check If
Estimate
Data?
In box provided)
In box provided)
(enter code)
applcable)
Yes
No
--'
f ] 7.
t ][ ]
7. t ]
[ It 1
l1
.'l H 1
A]
[ H1
-`I ]
-'[ H ]
]-*[ 7.
[ It ]
--o
[ ] 7.
?--'l U ]
7. 7. f 1
[H1
--
A]
-'[ ][ ]
EPA Form 9350-1(1-691 Revised--Do not use previous versions.
SAL 000005647
Form Approved OMB NO.: 2070-0093 Approval Expires:_____2im
(Important: Type or print; read instructions before completing form.)
Page 1 of S
o-EPA U.S. Envlronmantal Protection Agancy
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 319 of the Emergency naming and Community Rlght-to-Know Act of 1&B6.
also known as TMe HI of the Stsxrfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
tag burpen tor tN* Informalton m tlnuia to
34 hart par i
o( 32 hour*
time tar rovtaw'tno
iaarching aictaltna data srtng and mafcitalntng the
and comptstluj and
, coftaettan of Information.
Sand eenvTfanta ranardino this btsden estimate or any oathear masupect of Ms ceollteacetilon CMrf Itnnftoarrmmatitoan. Muidfing
suggestions tar reducing this biurden, to C(PhMie-f,223I)n, foVrSmaEtPioAn. 40P1olMicy*St.B7 raSrWvf,t
Washington! O.C. 20490 Attn: TRI
Burdai and to the Offlea of Information
and Regulatory Affairs. Office o'
Management and Budget Paperwork
Reduction i Project
(2070-0093).
Washingtons O.C. 20903.
1.1 Are you claiming the chemical identity on page 3 trade secret?
1.
1 i Yes (Answer question 1.2:
1^1 No (Do not answer 1.2:
Attach substantiation forms. 1
Co to Question 1.3.1
1.2 tf 'Yes* in 1.1. Is this copy: [ ] Sanitised [ ] UnsanKUed
*ff Reporting Year
19 88
------------
2. CERTIFICATION (Read and sign after completing aN sections.)
I hereby certify that i have rents wed the attached documents and that, to the best el my knowledge and belief, the submitted information Hr true and complete and that tha smomtt and wlust In this repori are accurate based on reasonable estimates using data available to the preparers of this report.
Name and official title of owner/operator or
Don R. Unruhy^g^flj
management official
iger
facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND C0MPL^TED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1
City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See Instructions
70669
Appendix E)
This report eonfaine information for (Cheek one):
3.2
.-[x] An entire facility
b. [ ] Part of a facility.
Technical Contact
3.3 Brandt Butler
Public Contact
3.4
Don R. Unruh
Telephone KhcrPor (tacluia"
318-491-55>9999 |'
Telephone Number ('include.
318-491-5222
SIC Code (4 dtott)
3.$ .2911
NA
3.6
Oegrees
030
Latitude
Mlnulee
14
36
Oun & Bradstreet Number(s)
3.7 . 00-842-7692
EPA Identlfieattan Numper(t) (RCAA I.O. No.)
a.a .LAD990683716
3.9
NPOES Permit Number(s)
.LA0003026
neceiving Streams or Wat:er Bodies (enter one name per bos)
..Bayou Verdine
Degrees
093 NA
NA
NA
b. NA
Longitude Minutes
16
Ssconds
20
3.10
d.
Underground Wecttan Weil Cede (UlC) tasntMicattan NterPer(s|
3.11 mXA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Out A Brs
4.2 00-131-5704_____________________________________
EPA Form 93S0-1 (1-89) Revised--Oo not use previous versions.
(Important: Type or print; read instructions before computing form.)
3-EPA
REPA FORM
PART HI. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (This space for your optional use.)
1. CHEMICAL IDENTITY(Do not complete this section If you complete Section 2.)
1.1
1.2
(Reserved]
CAS Number (Enter the rxanber weedy It appear* on the 313 list. Enter NA H reporting a chemical category.)
7782-50-5
Chemical or Chemical Category Nam# (Enter the name exactly as it appear* on the 313 list.}
t .3 Chlorine
1.4
Generic Chemical Name (Complete only if Pan l, Section t.t la chectted *Ye*. * Oenerte name muet be structurally descripttva.)
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1A 2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (*.., nenbera. letters, space*, punctuation), j
3. ACTIVITIES ANO USES OF THE CHEMICAL AT THE FACILITY (Check ll that apply.)
Menufecture the
if produce or import:
chemical: 3.1
ri
a. L J Produce
f 1 For on-site c.l J use/processlng
.f d-l
b. [ ] Import
e.[ ] As a byproduct
f.[
1 Fdr sale/ J dtttribution
] A* an Impurity
Process the 3.2 chemical:
3.3 .Oth.er.wi.se.use tne cnemicai:
ft
_
* l J As a reactant
d. [ ] Repackaging only
L J[ 1 As a chemical
a. processing aid
. f 1 Asformulation b.[ J component
Lf .J1.
b.l As a manufactiatig aid
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE
f 1 AS an article c-l ic^mponent
c.flXlJ AncMary or other use
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (fae/yr]
You may report releases of less then 1,000 be. by checking ranges under A.1. (Do not use both A.1 and A.2|
A.1 Reporting Ranges
0 MM 500-009
A.2 Enter
Estimate
5.1 Fugitive or non-point eir emissions
5.1a [][][]
2,000
5.2 Stack or point air emissions
5.2a [][][]
NA
5.3 Discharges to receiving
{1
streams or water bodies 5*3*' i--I
(Enter letter code from Part 1 Section 3.10 for ctream(s) In the box provided.)
1]
5.3 2 1____1
S.3.3 1 1
5.3.1a [][][] 5.3.2a [][][] 5.3.3a (][](]
NA
5.4 Underground Injection 5.S Releases to land
5.5. 1 On-*ite landfill
5.5.2 Land treatment/application (arming
5.4a (][][] 5.5.1a [][][] 5.5.2a t 1 [ 1 [ ]
NA NA NA
5.5.3 Swfaoa impoundment
S.5.3a [][][]
NA
8. Basis of J Estimate (enter code)
5.1b La] 5.2b LJ 5.3.1b C 5.3.2b L 5.3.3b C] 5.4b C l'
5.5.1b 5.5.2b 5.5.3b
6.5.4 Other dlieotil
5.5.4a [](][]
NA
5.5.4b
t]
(Cheek It additions! Information provtded on Part (V-Suppiemental information. >
EPA Form 9350-1 (1-89) Revised--0o not use previous versions.
SAU 0000056*9
(Important: Type or print; read instructions before completing form.)
-8-EPA
REPA FORM
PART I!. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
t. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name
Street Address
City
County
City
Slate
Zip
State
Page 2 of S
(TNs space for your optional use.)
County Zip:
2. OTHER OFF-SITE LOCATIONS (DO HOT REPORT LOCATIONS TO WHCH WASTES ARE SENT ONLY FOR RECYfjuNG on REUSE).
2.1 Off-site location name
BFI
EPA tdentilieatien Number (fiCAA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
Slate
Louisiana
Zip
70664
Is location under control of reporting facility or parent company?
2.2 Off-site location name
NA
EPA Identification Number (RCRA D. No.)
Street Address City
County
State
ZIP :
Is location infer control of reporting facility or parent oompeny?
L [ ]vee [xJn*
[U
[u
t.4 Off-site location name
2.4 Off-slte location name
EPA MentMieatien Akpnber (RCRA O. No.) Street Address
EPA Identltieatlan Number (RCRA D. No.) Street Address
1
City
County
City
Caxky
Stete
Zip
Slate
Zip.
Is location under control of reporting facility or parent company?
2.S Off-site location name
[ ]v-
[ ]n.
Is location tfde eontrot of reporting facility or parent company?
2.6 Off-site location name
[U
(U
EPA Identification Number (RCRA . No. >
EPA identification Number (RCRA D. No.)
Street Address
Street Address
City
County
City
County;
| Stale
Zip
Stete
Zip
jcatlan under eontrot of reporting facility or parent company?
[ ]v~
[ ].
[ 1 Cheek N addttlonal pages of Pert > are attached. How many?
ts location under eontrol of reporttng facility or parent oompany?
liu [ u
EPA Form 5350-1(1-89) Revised--Do not use previous versions.
SAL 000005650
(Important: Type or print; read instructions before completing form.)
SEPA
EPA FORmR
PART til. CHEMICAL-SPECIFIC INFORMATION (continued)
Pag* 4 of 5 (This spaa* tor your optional use.)
6. TRANSFERS OP THE CHEMICAL IN WASTE TO OFF-SfTE LOCATIONS
You may report transfers of less than 1.000 lbs. by checking ranges under A.t. (Do not use both A.1 and A.2)
Oisetwe* to potw ,--. .--. lentor location number (.If 6.1.1 from Parti. Section i.j [ 1 |-|___
A. Total Transfers (fes/yr)
A.1 Reporting Ranoas 0 t-*oe soo-eog
A.2
Enter Estimate
[ ] [ 1 [ 1 HA
8. Basle of Estimate
(enter code) 6.1.ib O
Other off-stt* location ,------, . -- _ _ ,, (entor toeatJon number 6.2.1 from Part l, Section 2.) | _\ |
t
]
Other ott-eh* location . - - - (enter location number 1 j 1 6-2.2 (rent Part l. Section 2.) ]..*J |
[J
Other off-stte location .-----, , <mr location number 1*11 6.2.3 from Part 1. Section 2.) | 2 | |
.
t
1
[ ]f 1 LH 1 III!
HA
6.2.1b O 6.2.2b O 6.2.3b 1 |
[ ] (Check tf additional Information it provided on Part IV Supplemental Information.}
C+Type of Treatment/ Oteposal
(enter code)__
6.2.1c lMl 1 1 6.2.2c 1 M| j | 6j.2.3c | mJ ) )
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of Influent Concentration (entar code)
O. Sequential Treatment?
(check If appIcabU)
E. Treatment Efficiency Estimate
l"_L*J J7.1a
7.1b
1 1- 2a
7.2b
11
7,lc 7.2e
7.,< [ ] 7.2d [ ]
7.1e 7.2s
% %
7.3a
7.3b
||||
1 1 1 17.4a
7.4b
Mil7.5a
7.Sb
7.3c 7.4e
7.5o
7.3d [ ] 7.4d [ ] 7.5d [ ]
7.3e 7.4e 7.5e
% % %
7.6a
7.6b
||||
7.6c
7.6d [ ]
7.6#
%
7.7a
**>
I | |1
| | | |7.6a
7.8b
M 1 17.9a
7.9b
| | | |7.10a
7.10b
7.7c 7.6c 7.9c
7.10C
7.7d [
7" [ [7.9d [7.10d
]
] ] ]
7.7# 7.6# 7.9# 7.10#
% % % %
[ ] (Check If additional Information it provided on Part IV-Supplemental Information.)
F. Based on Operating
Data? Yes
No
[ 1 [ ]7.lf
l
[ 17.2f
1l
( ] ]T.3f
l
[ ] [ ]71 .4f
[ 1 [ ]7.5f
[ 57.6f
l 1
1 [ 17|.7f
l
[ ] [ ]71.8f
[ ] [ 17j.9f
l 1 1 ]7L10f
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
I
(Indteat* actions taken to reduce the amount of the chemical being released from the factity. See the Inatructtoai for coded
hems and an explanation of what Information to Include.)
,
A. Type of Modification (enter code)
8. Quantity of the Chemical In Watte* Prior to Treatment or Oftposal
C. Index
0. Reason for Action (enter code)
HU
Current reporting year (fet/yr)
Prior year (bt/yrj
Or percent change
EPA Form 9350-1(1-A9I Revised - Do not use previous versions.
SAL 000005651
(Important: Type or print: read instructions before completing form.)
EPA
REPA FORM
PART CV. SUPPLEMENTAL INFORMATION
Uso this section if you need addhtonal space for answers to questions In Part III. Number the Ines used sequantlafy from Ines In prior sectlone (e.g.. 5.3.4. 6.1.2. 7.11)
Page S of S (This space for your optional use.)1
AOOmONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
(Part III, Section S.3)
I
You may report releases of less than f .000 bs. by checking ranges under A.t.
(Oo not uso both A.1 and A.2)
A. Total Release (bs/yr)
A.1
Reporttrig Ranges O 1-400 00-09*
emir Estimate
S.3 Discharges to
,--.
receiving streams or waterbodies
II 5.3.--1--1
5.3_____a
[][](]
B. Basis of Estirriats
provided) \
5.3______lO
C.% From Stormwater 5.3_______c
(Enter letter coca trom Part 1
1J
Sacnon a. 10 tar tlraamfsl In e a
II
lha boa provided-)
---------------
5.3_____a
[][][]
5-3--------bO S.3._____c
5.3_____a [][][]
S.3._c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part III, Section 6)
________
______
You may report transfers of less than 1.000 bs. by checking ranges under A. 1. (Do not use
both A. 1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
o t-aoe soo seel
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
Olfeharpt to POTW
.. -
_.
(amor location nunOar I . I I I
6.1._____from Pont. Section 1.11 1 II____|
[][][]
1.1._____b I I
6.2.
6.2.
6.2.
1,00Other off-eite location
lanter location nui* from Part A factIon
[][](]
Otnor oft '4f location (antatr.location lurta
LED [](][]-- fromi Part . 6actIon
Other eft-eHe taoedon (entw loeailon numba
.mo [nui. bom Part t. Section 2.
.2._c[mi n
Ml
6.2. 6.2. M
AOOmONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Part III, Section 7)
A. General
Wasteetream (enter code
In box provided)
8. Treatment Method
(enter code
In box provided)
C. Range of
Influent Concentration (enter code)
0. Sequential
Treatment? (check If oppicable)
E. Treatment Efficiency Estimate
F. Based on Operating Data? Yes
No
7. L_Q 7.
7.
--"[ 1
7.
7. [ ][ 1
7. 7.
7.
--[ ] 7.
7. [ ][ 1
7. 7.
r-----------
1--[ 7.
7. I ][ 1
7. 7. -> L
7.
A ] 7.
7. [ H ]
7. 7. 7. 7.
7._* '
r---a[
A
]
)
7. 7.
7. I H 1 7. I H ]
7. 7.
7.
-*[ 1 7.
7. [ ][ 1
7. 7.
7.
.-[ ] 7.
7. ( H 1
7. 7.
7.
EPA Form 9350-1(1-69) Revised---Oo not use previous versions.
---[ ]
7. 7. [ ][ 1
00000&65Z
SAL
horm Approved OM8 Nii.: 2070-0093
Approval Expire*-- - 01/91
(Important: Type or print; read instructions before computing form.)
Page 1 of 5
o-EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Right-to-Know Act of 1966. also known as Title III of the Superfund Amendments and Reauthorfzation Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
rep irtmg Uraen tor this coliteilen of Momatign N ittknalM to
veiy fremac to 94tanpoipc with an m woo* of 32 hours por reepane*. to duJng time lor reviewing
Instruetiens. soaring existim data
cures*, o*1 hsrtng and matortatowne th* data needed. and completing arwl reviewing th* eoHectlon of Mormatton. Sand oontitibiu regartmg this &urd*n
sstlmata or any other aspect of this
ooflection of information, indudim Mjesstion* lor reducingthis burden. lo Chief, Information Policy Branch
(PM-223). VS EPA. 401 M St., SW
Washtoteton. O.C. 20460 Attn: TRt Burden and to tha Offiea of Information and riagutitory Alfa**, Olliee of
Management and Budget Paperwork
1.1 Are you claiming the chemical Identify on page 3 trada sacret?
1.
1 j Ye* (Amwr question 1.2;
1 ^ 1 No (Do not answer 1.2;
Attach substantiation forms.)
Go to Question t .3.1
1.2 if "Yes* tot 1.1, Is this copy: [ ] Sanitised [ ] Unsenttlced
'1.3 Raportinfl Year 19 88
2. CERTIFICATION (Read and sign after completing afl sections.) 1 hereby eertlfy that 1 hare reviewed the attached document* end that, to th* best Of try knowledge and belief, ttw si^nHted tntoimalien is true and compiate end that the amounts and values toi this reoon ere accurate based on reasonable estimates using data available to th* cyepa/ers of this report.
Nam* and official title of owner/operetor or senior management official
Don R. Unruh, Refinery. Manager
Data skgnad
Fedllty or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPL :D FORMS:
t. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Wesclake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL REljEASE INVENTORY
Calcasieu
2ip Cod*
2. APPROPRIATE STATE OFFICE! (See Instructions
70669
Appendix E)
Thf* report eontalne Information tor (Check one): 3.2
..[x] An entire teetttty
[ 1b. Part of a facility.
Technical contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
etc cod* (4 dwt)
3.5 .2911
NA
3.6
Oegreee
030
Minutoe
14
Oun & Bradstreot NumDer(t)
3.7 . 00-842-7692
Second*
36
ERA identification Number () (RCf\A i.C. No.)
3.6 ..LAD990683716
NPOES Perniil NwrOerlil
3.9 .LA0003026
Receiving stream* or Water Bodies (antor on* name per boa)
..Bayou Verdine
d.
Degree*
093
NA
NA NA b. NA
Telephone Number (Induce
318-491-5599 1
Telephone Nurrfeer (Include are* code)
318-491-5222
Longitude Minutes
16
Second*
20
3.10
Underground Infection Well Code (UIC) Identification Number(s I
3.11 .NA
_ PARENT COMPANY INFORMATION Nam* of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company a Oun I Bradstreet MjnOv
4.2 00-131-5704_______________________________________
EPA Form 9350-1 (1-69) Revised--Do not use previous versions.
u
(Important: Type or print; read instructions before computing form.)
tHA*% r-l-l A
O
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC
CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
1.2 POTW name
_____________116______________________________________________________________________________
Street Address
Street Address
City
County
City
State
Zip State
Page 2 of 5 (This space for your optional use.)
1
1 County
1 4
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WMCH WASTES ARE SENT ONLY FOR R6CVCUNQ OR REUSE).
2.1 Olf-slte location name
BFI
2.2 Oft-slte location name
HA
1_________________________________________________________
EPA Identification Number (RCRA O. No.) NA
EPA tdentlfieaiion Numeer (RCRa O. no. )
Street Address
Cities Service Hwy at 1-10
Street Addrets
Ctty
Sulfur
County
Calcasieu
City
Co)jnty
State
Louisiana
Zip
70664
State
Is location under oontrol of reporting facility or parent company?
la location wider control of reporting faculty or palrent company?
[ ]v* [xl***
i[ Jve [ U
2.3 Ofl-ilte location name EPA Identification Number (RCRA O. No.)
2.4 Off-site location name EPA Identification Number (RCRA O. No.)
1
Street Address City State
Cowity ZIP
Street Address City State
County Zip ;
b location under oontrol at reporting tacuity or parent company?
2.5 Off-site location name
[ ]ve [ ]
is location under control of reporting facility or parent company?
2.6 Off-site location name
t Jv..
[U
EPA tdentttieatien rtanbar (RCRA O. f*>.)
EPA Identification hfcjmber (RCRA O. No.)
Street Address
Street Address
Ctty State
Cowrty Zip
City State
Cowrty ii
zip ;
* location Wider oontrol Of reporting taeUHy or parent company? [ ]v,, [ ]
is location wider oontrol of reporting faculty or parang company?
[ ] Cheek ft adOttonal page* of Pan t are attached. Mow many?
EPA Form 9350-1(1-69) Revised--Do net use previous versions.
(Important: Type or print; read instructions before completing form.)
A ... XV tPA
REPA FORM
part 111. CHEMICAL-SPECIFIC INFORMATION
Page 3 of 5 (This space for you* optional use.)
1. CHEMICAL IDENTITYIDo not complete this section If you complete Section 2.)
-1
1.1 {Reserved)
F)CAS Number (Enter the number exactly aa it appear* on tha 3t3 list. Enter NA 11 reporting a enamieal categor
1.2 NA
Chemical or Chemical Category Name (Enter the name exactly a* it appear* an me 313 ifet.)
1.3
Cobalt compounds
)Generic Chemical Name (Complete only If Part 1. Section t.t !a checked "Ye*." Generic name mat be trudha-eiiy descriptive.
1.4
i
)MIXTURE COMPONENT IDENTITY (Do not complete this section If vou complete Section 1. ,2. Generic Chanttcai Name fYprided by Supplier (Umrt the name to a maximum of 70 character* (e.g, number*, lettWs, spaces, punctuation).)
_____________
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check el that apply. I
Menufeeture the chemical:
3.1
r
La. J Produce
if produce or import:
f 1 For on-site c-l i use/processlnq
.f
<*-l
Process the 3.2 ehemleal:
Otherwise use 3.3 the chemical*
[ ]b. Import r
l J As a reactant
[ ]d. Repackaging only
Jft 1 As a chemical
-l processing aid
]e.[ As a byproduct K J\ 1 As a formulation
b.{. component
.r 1
b.l J As a manufacturing aid
f.[ f
c.l
[
c.l
1
1 Fdr sale/ J attribution
] As an Impurity
J1A4 an article component
1 i AncSary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR
( ^1 (enter code)
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (fea/yrj
You may report releases of less than 1.000 bs. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
o t-aea 500-400
A.2 Enter Estimate
B. Basis of
j
Estimate
(enter cods)
5.1 Fugitive or non-point elr emissions
5.1a Mill)
5.2 Stack or point air omissions
5.2a [][][]
5.3 Discharges to receiving
II
streams or water bodies &>3-l 1--1
(Enter letter code from Perl l
)Section 3. to tor *tream() In
tha box provided.
|[
5 3 2 1____1
S.3.3 Q
$.3.la [][][] 5.3.2a [][](] S.3.3a (][][]
15
NA NA
5.1b LQJ i 5.2b tl I
5.3.tb CD
5.3.2b a
5.3.3b [4]
5.4 Underground injection
5.4a [ J t 1 t 1
NA
5.4b LJ
5.5 Releases to land 5.5.1 On-site landfill
/5.6.2 Land treatment appilealkxi farming
5.5.3 Surface Impoundment
5.5.4 Other disposal
5.5.1a [][][]
NA
5.5.1b |_J
5.5.2a [ i [ n ] 5.5.3a [][][]
NA NA
UA5.5.4a [][][] ____ _______
5.5.2b L ]
5.5.3b [C3 S.5.4b (C1
(U (Check l* Additional information is provided on Pan IV-Supplemental Information )
EPA Form 9350-1 (1-89) Revised--Do not use previous versions.
000005655
SM-
& EPA
EPA FORM^
PART m. CHEMICAL-SPECIFIC INFORMATION (continued)
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers Of lost than 1,000 bt. by chocking ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfart (fes/yr)
A.1 Reporting Ranges
0 1-49 800 000
A.2 Enter
Estimate
6. Baals of Estimate (enter code!
,,,sST.,Qn[ i t i t i
Other off-cfte location , . , (enter bocetkon number 6.2.1 from Pen . Section;
Other oft-site location _ . * (enter loeetton number 6.2.2 from Pert t. Section 2.)
Other off-elte location tenter loeetion number 6.2.3 from Pert l. Section 2.)
M 1r 1 [MM!
[][][]
NA
2,700
HA
6.1.1b 6.2.1b 6.2.2b
D
[ ] (Cheek K addMonal information Is provided on Part (V~Supptemental Information.)
i
C.Type of Treatment/ Disposal
7. WASTE TREATMENT METHOOS AND EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(ontor code)
C.Ranoe of influent
Concentration ____(enter code)
D. Sequential Treatment?
(chock If
applcabfo)
7.1a 7.2a
7.1b
n 7.2b
IN
7.1c 7.2e
r.id 7.2d
[i []
7.3a
7.3b
7.3c
7.3d l 1
r*4a
Q 7.4b
7.4c
7.4d [ 1
E. Treatment Efficiency Estimate
7.1#
7.2a
7.3e
7.4a
7.Sa 7.6a
7.5b 7.6b
7.6c 7.6c
7.5d 7.6d
[1
[1
7.6a 7.6e
7.7a 7.6a 7.9a
7.7b 7.8b
7.9b
[
7.7c
7.6c
n7.9c
7.7d [ 1
7.fid
[]
7.9d [ 1
7.7o 7.fte 7.9e
7.10a
7.10b [
7.10c
7.10d [ ]
7.10#
[ ] (Check If addMonal Information is provided on Part (V-Supplemental Information.)
F. Based on
Yes
NO
7.1f 7.2f 7.3f 7.4f
[H]
[ ]( ] [ ][ ] [ ][ ]
7.6f [ ] [ ]
7.6f [ ] [ 1
7.7f
[ ][ ]
7.8f
[ ][ ]
7.91 [ 1 l ]
7.10f [ ] t ]
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indteate action# taken to reduce the amount of the chemical being released from the faeftty. See the instructions for coded hems and an explanation of what Information to Include.)
A. TJSdHieattan (enter code)
B. Quantity of the Cherroeal in Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action [(enter code)
Current reporting
year (fce/yr)
Prior year (tos/yr)
Or percent change
1M
SAjL 000005656 rT
EPA Form 9350-1 (1-89) Revised - Do not use previous versions
(Important; Type or print; read instructions before completing form.)
rpA 0 C-tVA
REPA FORM
part IV. SUPPLEMENTAL INFORMATION
Use this section If you need additional space for answers to questions In Part HI. Number the Ines used quentialy from Hnea St prior sections (e.g.. 5.3.4, 6.1.2. 7.11)
Page 5 of 5 (Ttn space for your optional use.)
additional information on releases of the chemical to the environment on-site
(Part HI, Section S.3)_______________________
i
You may report releases of less than 1.000 lbs. by checldng ranges under A.IT (Do not use both A.1 and A.2)
A. Total Relsase (toe/yr)
A.1 Reporting Ranges 0 MW SOO-OM
A.2 Enter Estimate
S.3 Discharges to
,----.
receiving streams or waterbodies
I1 5.3--------'--*
5.3..--* [][][]
6. Basis Of Estimate
(enter cods in box!
provided!
5.3______bD
C.% From Stormwater 5.3_______c
(mr letter code from Pen 1
I|
Section 3.10 tor etreem(<) in e \
I___I
trte box provided.)
--------------------
S.3_____a [](][]
S.3.____bf|~1 S.3._____c
5.3_____a [)(][]
5-3-_____bQ 5.3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part III. Section 6)___________________________________________________________________________________________________ |
You may report transfers of less than 1.000 Os. by checldng ranges under A.1. (Do not use both A.1 and A.2)
A.Total Transfers (fes/yr|
A.1 Reporting Ranges
o i-ese soo oss
A.2 Enter
Estknate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(entsr code to box
< provided)
Piacherge SO POTW
-
(][][]s.i._____tttSSVTZSZFr.,
.i._____b n
e-2---smstwsa, 0O
Other off elie toeetlon i----i i--"i
6.2.
(enter toeetlon nuibe I *11 1
---------Wn Pen t. Snctton2.ll_H____1
Other gtl eMe location
i
g;
(enter toeetlon number 1 * 1 1 1
6-z-----------from Part 1. Section 2.) I * l.l 1
[][][] (][][] [](][]
6.2._____b O 6.2._____b Q 6.2._____b n
6f2. c|mi n 6(2. _c|M| | |
lII
i
*_ to
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Pert III, jetton 71
A. General
Wastestream (enter code
to box provided)
B. Treatment Method
(enter code to box provided)
C. Range of
WlNRt Concentretfor (enter code)
D. Sequential Treatment?
(check If aodcable)
E. Treatment Efficiency Estimate
F. Based on Operating
Data? Ye*
No
, .D
* LI.X1
7.
c 7.
d[ ]
7.______e
% 7- [ ][ ]
7. 6 1 1 1 1
7- =
7.
d[ 1
7.
e
% 7.
f[ l f l
7. *1111
n7. c
7.
dr 1
7.
e
% 7.
f\ i r i
2. .Q
UJ 17- b
7. b | | | |
| |7-_b
J. )
- - cm
7. = Q
7-_e
7. e Q
7- =
7. d[ ]
7----------- <[
]
7-----------0 [ ]
7. d[ ]
7. e 7.______ e , 7.______ e 7.______ e
% 7-
% 7.
% !7'
% ,7-
[][ ]
'[ ] [ ]
'(HI <[ ][ ]
-- 7 - I.IJ 1 2. 7. b rrn
7-----<= 7. c
-[7-_______
7. d[
] ]
7.______ 7.______e
[ ][ ]% !7-_______ % i*- '[ ][ 1
PA Form 9350-1(1-69) Revised--Oo not use previous versions.
SAL 000005657
Form Approved OMB No.: 2070-0093
Approve! Exp*re:___2ii__
(Important: Type or print; read instructions before completing form.)
Pago i of S
S-EPA U.S. Envfronmemal Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Pfenning end Community ftght-to-Know Act of 1986.
also known as Title III of the Superfund Amendments end Reauthorization Act___________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
PubUe rapArthq bidden ter this aametlan * Internalion H wilmttad to vary trum 30 to 34 hnn par responds,
________
of 32 hours par
reepon**, Hadng time tar revtewinq
nwtWtaa. esarchkig --Istinp data . _ , Mtng and maintairMng the
data naadsfl. and eomptatlng and revtawhng 0*4 dottedton ofIntormattan.
a raoerdtag thta bvdan estimate lany outer asa*paet of thta ooiteetten if information, itnr cluding
suggestions tar reduetno Ihia burban, to
Chtef. bttahnalion Policy Branch
(PM-823), US EPA, 401 M St., SW.
WaaWnghinJ O.C. 204S0 Attn: TPl Burdan and lb the Office of Infarmallon and Regulatory Affair*, Olfte* of
Management and Budget Paperwork
Reduction ! Profad
(2070-0003),
1.1 Ar* you claiming the chemical Identity on peg* 3 trade secret?
1.
F ^1[ I Yes (Answer question 1.2:
No (Do nd answer 1.2;
Attach substantiation tarms.)
Go to Quasiten 1.3.)
1.2 if *v*' in i.t. (a this eepy: [ ] Sanitized [ ] Unaanmxed
jfT .-^==q 1.3 Reporting Year
19 88
2. CERTIFICATION (Reed end sign after completing el sections.) 1 hereby canity that 1 have rertewod the attached documents and that, to the beat et my knowbdo* and belief, the submitted information is true and compteta and that the wnouUi and values In ttv* report are accurate based on reasonable estimate* using data available to the preparers of tnis rapon.
Nam* and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
3. FACILITY IDENTIFICATION Facility or Estabflshmant Nam*
Conoco Lake Charles
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
Refinery
County
Calcasieu
Zip Code
70669
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY P.O. BOX 70266 WASHINGTON, DC 20024-0266
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
2. APPROPRIATE STATE OFFICE (See instructions Appendix E)
This report contains information tar (Check one): 3.2
.[x] M entire facility
- I ] Part et a facility.
Technical Centad 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
Telephone Number (IncM*
318-491-5599
Telephone Number (include
318-491-5222
code)
SIC Coda (4 cftgtt}
3.S ,2911
b. NA
e.
d.
e. f.
3.6
Oagraas
030
latitude Mirutes
14
Seconds
36
Degrees
093
Longitude Minutes
16
Seconds
20
Don & Brsdttraet Numbarfs)
3.7 00-842-7692
EPA taanllfieation Ntembar(s) (RCRA l.D. No.)
3.6 ..LAD990683716
b. NA b. NA
NPOES Permit Number(*)
3.9 ,LA0003026
NA
ReoeMng Streams or Water Bodes (antier one name par tax)
*ayou Verdine
b. NA
3.10
d.
Lkteergrotate vyectlon Wait Coda (U)C) Identification Nurreer(i)
3.11 .NA
Name et Parent Company
E.I. DuPont de Nemours
Parent Company* s Out 4 Brad*treat hMnber
00-131-5704
SAL 000005658
(Important: Type or print; read instructions before computing form.)
a r-m a tJ-'A
EPA PORM R
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTW*)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip State
P>Q6 2 Of s
(This space for your optional use.)
County
zip
j 2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WVeCH WASTES ARE SENT OhtY FOR RECYCUNQ OR REUSE).
2.1 Oll-slte location name
BFI
EPA Identification Number (RCRA D. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
is location under control at reporting facility or parent company?
2.2 Oll-slte location name NA
)EPA identification Number (RCRA O. No.
Street Address City
County
State
Zip
is location under control of reporting facility or parent company?
c.a Off-site location name
[ JY- [xl**
.
2.4 Off-slta location namo
U[ ]y (
EPA Identification Number (RCRA O. No.)
EPA Identification Nwnber (RCRA O. No.)
Street Address
Street Address
City
County
City
CouWy
State
Zip
State
Zip 1
Is localUn under control of reporung tecHIty or parent company?
2.S Off-site loeetlon name
[ ]ves
[ ]no
Is location under control of reporting facility or parent company?
2.6 Oll-slte location name
t U1 ]y
EPA Identification Number (RCRA O. No.)
)EPA Identification NunOer (RCRA D. No.
Street Address
Street Address
City
County
City
County
State
Zip State
Zip
, location wider control of reporting faculty or parent company?
[ ] Yes
[ ] No
is location under control of reporting facility or parent company?
| ] Yes
[ 3 No j
Cheek
pages Part are attached. How many?
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005659
(Important: Type or print; read instructions before completing form,)
S-EPA
REPA FORM
PART II!. CHEMICAL-SPECIFIC INFORMATION
Page 3 of 5 (This spacs for your optional usa.)
1. CHEMICAL IDENTTTYfOo not complete this sectiontf you complete Section 2.)
1.1 [Rasarvad] CAS Number (Enter the number exactly a* it appear* on me 313 u*t. Enter NA If reporting a chemical category.)
1.2 98-82-8
ChamicaJ or Chemical Category Name (Enter tne name exactly as h appears on me 3ia net. j 1.3
Cumene Generic Chemical Name iconwtete only n Pert . Section l.ti* checked Ye*.' Oenerte name must be structurally descriptive.) 1.4
"
t
2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 character* (e.g.. mxnber*. letters, apace*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that apotv. 1
Manufacture the chemical:
3.1
a.[x ] Produce
If produce or Import:
fY 1 For on-site c.LA J uee/processlng
1 Fpr sale/ J diftrlbution
b. [ ] Import
]e.[ As a byproduct
#-[x3^ an Impurity
Process the 3.2 chemical:
a. [^ ] As a reactant d.[ ] Repackaging only
K f 1 As a formulation D,l J component
1 1 Aa an artleie c.l J component
Otherwise use 3.3
the chemical:
f 1 As a chemical a.L J processing aid
b.[ 3 Aa a manufacturing aid
c.[ ] AncdUry or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SFTE AT ANY TIME DUPING THE IQ I7 I (enter coda)
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SfTE
A. Total Release (fcs/yr)
You may report release* of less than 1,000 toe. by checking ranges under A.1. (Do not use both A.1 end A.2)
A.1 Reporting Ranges
0 1-400 500-009
A.2 Enter Estimate
5.1 Fugitive or non-point air emissions
5.1a [][][]
13,000
5.2 Stack or point air emissions
5.2a [][][]
570
6. Basts of i 1 Estimate i (enter code}
13s.ib
5.2b 0
5.3 Discharges to receiving
Ik I
streams or water bodies 5,3< 1 --*
(Enter letter code from Part 1 Section 3. to tor tream(t) in the box provided.)
|] 5 3 2 I___
-----
5.3.3 | |
5.3.1a [][][] 5.3.2a [][][] 5.3.3a [][][]
39 NA
5.3.1b 0 5.3.2b 0 5.3.3b Q
5.4 Underground injection 5.5 Releases to lend
S.S. 1 On-*lte landfill
5.4a [](][] 5.5.la [][][]
NA NA
5.4b O 5.5.1b 1___1
6.5.2 Land treatment/application farming
5.5.2a [][][]
0
5.5.2b 12J
5.5.3 Surlaca impoundment
5.5.3a [ ] [ ] f ]
NA
5.5.3b 0
5.5.4 Other disposal
5.5.4a [][][]
NA
5.5.4b 0
[ 1 (Cheek If additional information is provided on Part (V-Supplemental Information.)
EPA Form 9350-1(1-89) Revised --Do not use previous versions
SAL 000005660
(Important: Type or print; read instructions before completing form.)
o EPA
EPA formR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 of S (This space for your optional use.}
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1.000 toe. by checking ranges under A. 1. (Oo not use
both A.1 and A.2)
A. Total Transfers (tM/yr)
A.l Hsporting Ranges
0 1-480 soo-oee
A.2 Enter
Estimate
B. Basis of Estimate (enter codel
Discharge to POTW
__ __
(enter location number jT1 6.1.1 framParti, Section i.)i 1 1-1___ ]
[][][]
NA
6.1.1b n
Otter off-tlt* location
.
. , , (antar location number 1 * | (
[Mill6.2.1 from Pan S. Section 2.) L2J l_l
Other off-tile location . . ___
, . , (enter tocation number 1 9 l 1 6.2.2 from Pert 1. Sectkm 2.) I ll
I[
1t
1[
1
Other efl-ehe location ---- , -1 J 6.2.3 )STp|SV`?SSf?.)[I|.n[
][
][
]
NA.
6.2.1b o 6.2.2b o 6.2.3b
C.Type of Treatment/ Oisposal
1 (enter code).._______
6.2.1c lMl 1 1 6.2.2c |m| 1 | 6.2.3c M | |
[ ] (Chock If additional information la provided on Port IV-Suppiemental information.)
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent
Concentration (enter codel
0. Sequential Treatment? (cheek If appleable)
7.1a
0
7.1b
mi
7.1c
7.Id [ ]
'.2a
0
7.2b
I'M1!
El7.2c
7.2d { ]
7.3a
7.3b
1 aI 0 I7 1
7.3c
7.30 [ ]
7.4a
7.4b
1 NIAI 1
7.4o
7.4d [ ]
E. Treatment
Efficiency Estimate
F. Based on Operating
Oata? Yes
No
7.1e
95 % 7.1,
] tx]
7.2s
100% 7.2,
] [X1
7.3e
87.5* 7.31
x] [ ]
7.4e
% 7.4,
till
7.5a 7.6a
7.5b
||||
76b | | M
7.5c 7.60
7.5d [ ] 7.60 [ ]
7.5e 7.6e
% 7.5f % 7.6f
[ ][ 1 [ 1[ 1
7.7a 7.6a 7.9a
7-7b 7.b 7.9b
|||I ||M ||||
7.7c
7.6c 7.9c
7.70 [ ] 7.60 [ ] 7.M [ ]
7.7e 7.6e 7.9e
7.10a
7.10b | | | |
7.10e
7.100 [ ]
7.10e
[ ] (Chock If additional ^formation It provided on Part IV-Supptomontal Information.)
% ?.7f
[ 1[ 1
% 7.8f
[ ][ 1
(HI% 7.9f
% 7.10f ( 1 [ 1
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indteato actions taken to reduce the amount of the chemical being released from the factity. Kerns and an explanation of what krformatton to Include.)
A. Type of Modfflcation (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Oisposal
C. index
; See the Instructions for coded
-- 1--------------------------------------0. Repson for Action (enter code)
1
M|
Current reporting year (ft>s/yr)
Prior year (fcs/yr)
} Or percent { change ,
1 1*
|r| .1
EPA Form 9350-1(1-891 Revised - Do not use previous versions.
SAL 000005661
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART IV, SUPPLEMENTAL INFORMATION
Use this section it you need Additional space for answers to questions In Pan IU. Number the Roes used sequential/ from arms In prior sections (e.g.. 5.3.4. 6.1.2, 7.11)
Page 5 ( 5 (This tpace lor your optional use.)*
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part lit. Section S.3)
You may report releases of less than 1.000 fci. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (ts/yr)
A.1 Reporting Ranges
o \-499 soo-ese
A.2 Enter Estimate
B. Basis lot
Estimate
(ehteTcode ktbo*
provided)
S.3 Discharges to
..
receiving streams or
II
[][][]water bodies
5.3--------1------l 5.3_____a
C.% From Stormwater S.3______bC
5.3________c
totter CM* Irom Pan 1
!}
Sections. 10 lor stream/*) In r
(Millthe boa proceed.)
3
II J---------'-------1
S.3_____a
[][][]S.3_____ 5.3_____a
5.3._____bO S.3.
c
tJD S-3-_______C
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Pan ill. Section 6)
You may report transfers of less than t .000 tos. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (tos/yr)
A.1 Reporting Ranges
0 1-409 500-000
A.2 Enter
Estknate
6. Basis of Estimate
(enter code m box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
.. 6.1.
Oitdwg* to POTW
,. ^ , .
(enter location nantor 1 , 1 ] |
[][][]from Pert i, Section t.) | 1 |.|____J
6.1._____b O
-- Bu [](][]e-2-
Other offtotte location .
--
Other eff-elte location i i i * *
6.2.
(enter location number | 2 1
[][][]---------from Pert 1. Section 2.1 LU'I____\
Other off-sMe location --
kn
(enter location mrter 1 | 1
(][][]*z*--. tram Pen , Section 2.) 1 * l.l
I 1
6.2._____bCH
n6.2._____b
6.2._____b O
!*-____c|M|
1
6,2. c|m| | |
6.2. c|M] | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Part III, Section 71
A. General
Wasteetream (enter code tn box provided)
B. Treatment
Method (enter code In box provided)
C. Range of
influent
Concentration (enter code)
0. Sequential Treatment?
(check If appteabie)
E. Treatment
Efficiency Estknate
F. Based on Operating Data 7 Yes
No
n ---i i
ini
---i i
[ it i
.b [
7. -- 7.
.-( 1
[H1
-- L
.b L
7.-- ---
7. ---[ .-[
1 1
[ It 1
(H1
.-l 1
[H]
--
--`=
EPA Form 6350-1(1-69) Revised--Do not use previous versions.
[1
[} .-[ 1
7.
7. [ H ]
7. [ ][ 1
7. [ H
SAL 000005662
1
rurm >vpproveG OMO Ho.; Approval gv0W61
(Important: Type or print;, read instructions before completing form.)
Page lolS
EPA U.S. Environmental Protaction Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of tbo Emergency Planning and Community Right-to-Know Act of 1986.
aiso known as TWe III of the Stperfund Amendments and Reauthorization Act________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Pubtie
Ing turban for thi*
collectton information is aattmated to
vary Iron
le 94 hour* par <
with an
of 32 H
OSSU searchtilnmgawtoilrtirnegvtacwtr^
Oltl
ouneas^QAjharlng andmaJntadnno tha
. . and oomptatlng and reviewing thea ooopMsaection ofInformation.
Sarto cenwsnti ragi Ms aburden estimate or any other aspact of thii
burdanl'iScollectton | of information, inefc
suggestion^ tor reducing this
Chief, Information Policy Brawi
(PM-223).'uS CPA. 401 M St.. SW.
Washington, O.C. 20460 Attn: TRI
Burden and to tha Office of Information
and Regulatory Affairs, Oftiea of
Management and Budget Paoamwk
Radueiion : Projact
(2070-00931.
Washington, O.C. 20S03.
1.1 Are you claiming tha chemical Identity on page 3 trade secret?
1.
[ ] Yes (Answer question 1.2;
[ ^ } No (Do not answer 1.2;
Attach substantiation terms.1
Co to Question 1.3.)
T.2
tf *ves* in i.i, is this copy: [ ] Sanitised [ ]uns*itl*ed
1.3 Reporting Veer
19 88
2. CERTIFICATION (Read and sign after completing ai sections.) . hareby cartlfy that I have i an levied tha attached documents and that, to tha best of my knowledge and belief, tha submitted information is true and eompiaie and that the amounts and values In this report are accurate based on reasonable estimates using data available to tha [preparers of this report.
Name end official title of owner/operator or ssniar management official
Don R. Unruh, Re finely. Manager^
Signature
Pate signed
3, FACILITY IDENTIFICATION
Faculty or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLlEeTtE! D FORMS:
1. U.S. ENVIRONMENTAL PROJECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
Cotatty
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains infor mation for (Check one): -.2
[x] An entire feetuty
[ ].. Part of a facility.
Technical Contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
SfC Coda <4 digit)
3.S ,2911
b. NA
3.6
Minute
030 14
Pun A Bradstroet Number(s)
3.7 . 00-842-7692
c.
Second!
36
Telephone Nurrfeer (Indyda
3X8-491-55991
Telephone Ntartoar (include area code)
318-491-5222
d.
Degree*
093
NA
-1---------------------------------Longitude
Minutes
16
Seooods
20
CPA (denttftcatton Mnbe(i) (RCRA LD. No.)
3.8 ,.LAD990683716
NA
NPDES Pend hkenber(s)
3.9 ..LA0003026
nsaoMng Streams or Water
a3ayou Verdlne
(enter one name par boa)
NA b. NA
3.10
d.
Ltodargreund faction WaH Coda (L9C) tdentificatiQn Number (s) 3.11 aHA
PARENT COMPANY INFORMATION Name of Parent Company
4.1 E. I. DuPont de Nemours
Parent Canpuy'l Oun A Bradstfeat tfiiisi
4.2 00-131-5704_______________________________________
EPA Form 9350-1 (1-89) Revised--Do not use previous versions.
SAL 000005663
u
(Important: Type or print; read instructions before completing form.)
a r-n A X* CrA
EPA PORM R
PART 11. OFF-SITE LOCATIONS to which toxic CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBUCLY OWNED TREATMENT WORKS (POTWs)
1-1 POTW name NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip State
Pape 2 of 5 (This space for your optional use.)
Cbunty zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WUCH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE).
2.1 Off-site location name
BFI
EPA IdentHieatton Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
ZIP
70664
Is location under control of reporting faculty or parent company?
2.2 Off-site location name
NA
EPA Identification Number (RCRA O. No.)
Street Addrwt City
County
State
la location wider control at reporting facility or parent company?
[ ]v [xl**
[ 3 Yes
[ ] No
2.3 Off-site location name EPA tderwMcatton Number (RCRA O. No.)
2.4 Off-site location name EPA Identification Nwnbar (RCRA O. No.)
Street Address City State
Cowtty Zip
Street Address City State
County Zip !
Is location undar oontroi of reporting lacillty or parent company?
2.S Off-site location name
[ ]v~
[ In.
Is location under oontroi of reporting facility or parent company?
[ ]v,,
[u
2.6 Off-stte location name
EPA WentHieatton Number (RCRA . No.)
EPA Identification Nwnber (RCRA O. No.)
Street Address City
County
StfMt Addrmt City
i County
State
ZIP State
Zip
M location undar oontroi of reporting facility or parent oompeny?
[ ] Yes
[ ] No
is location under control of reporting facility or parent company?
[ ] Yes
[ 3 No
[ } Ctieek If eddtttonal pages of Part I are attached. Mr* mew?
EPA Form 9350-1 M-89) Revised--Oo not use previous versions
(Important: Type or print; read instructions before completing form.)
nrnA era
epafohmR part III. CHEMICAL-SPECIFIC INFORMATION
Page 3 Of 5 (TH* space for your optional use.}
1. CHEMICAL IDENT1TY(Do net oomptote tN# section If you complete Section 2.)
1.1 {Reserved}
CAS Number (Enter the ma-nbar exactly a* H tppsari on the 313 list. Enter NA H reporting e chemical category.) 1.2 110-82-7
Chemical or Chemical Category Name (Enter the none exactly as it appears on the 313 ust.) 1.3 Cyclohexane
Generic Chemical Name (Complete only it Pert U Section 1.1 la checked *Yas, * Generic name nun be etrueturaHy descriptive.)
1.4
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1.1
2. Generic Chemical Name Provided by Oiopfler (Umrt the name tee maximten of 70 characters (e.g.. numbers, tetters, spaces, punctuation).)
3. ACTIVITIES ANO USES OP THE CHEMICAL AT THE FACILITY {Check el that epptv.1
Manufacture the
If produoe'or Import:
chemical: 3.1
rt
a.l J Produce
f 1 For on-sKe c.l J use/processktg
. T 1 Far sale/ c.l JdwtHbutlon
b. { ] Import
e.[ ] As a byproduet
f.[ ] As an Impurfty
Process the 3.2 chemical:
3.3
Otherwise use the chemical'
fx 1 .
__
* l* i As a reactant
d. [ ] Repackaging only
{ 1 As a chemical
i processing aid
. r 1 As a formulation
b.l J component
. f 1.
. ____ ,.
b.l J As a manufacturing aid
\ 1 As an article J component
f]
c.l J Ancftary or other use
4. MAXIMUM AMOUNT OP THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR
(enter cod*)
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Raleass (toa/yr)
You may report releases of less than 1.000 fee. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l Reporting Ranges
0 MW 500-000
A.2 Enter
Estimate
S.1 Fugitive or non-point air emissions 5.1a [][][]
12,000
5.2 Stack or point air emissions
5.2a [][][]
8,500
5.3 Discharges to receiving
1 aI
streams or water bodies 5*3-' L--j
(Enter letter cod* from Psrt 1
Section 3.10 ter stream(s) In
the box provided.)
II 5 3 2 1____I
5.3.3 n
5.3.1a [][][] 5.3.2a [][][] 5.3.3a [][][]
39 NA
B. Basis ofl 1
Estimate (enter c^des
5.1b Gl
5.2b G}D
5.3.1b QD 5.3.2b 0
C. % From.Stormwater 5.3.1c ^A
5.3.3b
r j
5.4 Underground injection 5.5 Releases to land
5.5.1 Ov-*lt* landfill 5.5.2 Lend treatment/application farming
5.5.3 Surtaee impoundment
S.S. Other disposal
S.4a [Hill
5.5.1a [][][]
5.5.2a [][][]
S.5.3a [][][] 5.5.4a [][][]
NA NA 0 NA NA
a&.4b
5.5.1b LJ 5.5.2b La
5.5.3b Q 5.5.4b P
iLi (Check if additional Information It provided on Part lV-Ouctilnanlil information. |
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005665
(Important: Type or print; read instructions before computing form.)
A PDA
EPA formR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 Of 5
-- 11
' i
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1,000 lbs. by checking ranges under A. 1. (Do not use
both A. 1 and A.2)
A. Total Transfers (bs/yr)
A. 1 Reporting Ranges
0 1-499 500-999
A.2
Enter Estimate
8. Baals of Estimate (enter code!
C.Type of Treatment/ Disposal
Discharge to POTW
.-------, ,-------,
<ntr location numbor
.1
6.1.1 from Port I, Soetton 1.) [ 1 1-1____
[][][]
HA.
6.1.1b n
Other otl-slls toeatlen
,, .
- - . lemor location numbor 1 , |
f0-2.1 from Part . Section 2, 1 Mil 1
Other off--ilt location .------,
-
6.2.2 <^Tp!sY.l<ags??., HO [
1[
][
1[
M
1 NA
1
1.2.1b I 1
6.2.2b
6.2.1c 6.2.2c [Ml
Other oft--alt# locationi
isrpSff&sst., SO [ ] [ ] [ 16.2.3
.----------. _. ______I
n6.2.3b
_______ iwi t i
{ ] (Check If additional information Is provided on Part fV-Sipplemontal Information.)
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wasteetream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent
Concentration (enter code)
D. Sequential
Treatment? (cheek If appScabie)
ill U7.1
0
7.1b
7.1c
7.Id [ 1
7.2a 7.3c '<*
0 0
7.2b 7.3b 7.4b
IE D
a|o u
El
7.2c 7.3c
7.4c
7.2d
7.3d
[1
[1
7.4d [ 1
E. Treatment Efficiency Estimate
F. Based on
Operating Data?
Yes
No
7.1e
7.2c
95 % 7.,, 100
[ ] [X] [ 1 [X]
7.3e
87.3* 7.3f [X ] [ ]
7.4e
7.4f
(HI
7.Sa 7.6a 7.7a 7.8a
7.9c
7.Sb
7.6b
7.7b
7.6b
Q
7.9b
7.Sc 7.6c 7.7c 7.6c 7.9c
7.5d 7.6d 7.7d 7.fid
[1 [1 [1
[1
7.9d [ 1
7.Se 7.6e 7.7e 7.6e 7.9e
7.Sf [ ] [ 1
7.6f [ 1 [ ]
7.7f [ ] t ]
7.8f [ ] [ ]
7.91 ( 1 [ 1
7.10a
Q7.10b
7.10c
7.10d ( 1
7.10e
[ ] (Check if addHional Information la provided on Part (V-Suppiemental Information.)
7.10f [ ] [ ]
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indteate actions taken to reduce the amount of the chemical being released from the faeflty. See the Instructions for coded Items and an explanation of what Information to include.)
A. T Modfflcctlon
(enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
O. Reason for Action (jenter code)
Current reporting year (tbs/yr)
Prior year (bs/yr)
Or percent change
sal. 000005666
M 0D
EPA Form 9350-1 M-89) Revised - Do not use previous versions.
(important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Um this section if you need addhlonal space lor answer* to questions In Part HI. Number the Hoes used sequential? from Ines In prior sections (e.g.. 5.3.4. 6.1.2. 7.11)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON^SITE
(Part III. Section 5.3)
,
You may report releases of less than 1.000 lbs. by checking ranges under A.t.
(Do not use both A. 1 and A.2)
A. Total Release (l>s/yr)
' A.1 ReportHq Ranges o 1-S6E soo-eee
A.2 Enter Estimate
B. Baste 3f
Estknats
(enter code In box
provided!
S.3 Discharges to
receiving streams or
water bodies
$
" n(Emir tetter coo* IrOm Part
Sreiien 3.10 for nr4m|t| 5.3_____I____I the boa provCed.)
5.3.. 5.3..
[][][] [][][]
5.3. 5.3.
5.3..
5.3..
[ ][ 1[ 1
5.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1.000 lbs. by checking
A.Totaf Transfers (t>s/yr)
B. Basis of Estimate
cL Type of Treatment/ Disposal
ranges under A.1. (Do not use both A.1 and A.2)
A.t fleporOnfl Ranges
A.2 Enter
(enter code in box
(enter code ki box
0 1<4M S00 SBC Estimate
provided)
provided)
Discharge to POTW
,
e. i._____ttTplSffMEtt, [][][]
6.1._____b n
e9
Other eh--site location (enter location number
1
f
1--Ii
6 Z----- from Pan i. Section2.) LD l__)
Other eft-site location i i [ 1 i
6.2.
(enter location number III 1
------- iron Part 1. Section 2.1 L--J-L_J
e9
Other eff-eite location (enter loeetlon number
1--- I Ir--1
--------from Part a, Section 2.) 1 * 1 1 1
[](][] [ ][ 1 [ 1 [Kill
6.2._____b 1 1 6.2._____b n 6.2._____b tD
._,ran
*4- c|m| | |
6.^. c|m| 1 1
AOOmONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Part III. Section 7!
A. General
Wastestream (enter code
In box provided)
B. Treatment Method
(enter code In box provided)
C. Range of Influent Concentration (enter code)
O. Sequential Treatment?
(check If appiceWe)
E. Treatment Efficiency Estimate
F. Based on Operating Data? Yes
No
7.
7.
-l 1 7.
[H]
7. 7.
---------[ 1 7.
-[ 1
7.
[ ][ ]
I7-. H 1
7. 7.
-"[ ] 7.
t J 7.
[H1
[ H]
7.
7.
.<[ ]
7.
[H1
7. 7. 7.
7.
[ ] 7.
7.
----------[ ]
7.
---[ 1 7.
[H1 [H1
[n]
EPA Form 9350-1(1-6) Revised--Do not use previous versions.
SAL 000005667
Form Approved OMB No.: 3070-0093 Approval Exp*os:_21'22____
0. EP/Y U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of tha Emergency Planning and Community Rlght-to-Know Act of 1966. also known as Tide III of tho Suparfund Amendments and Reauthorization Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION
INFORMATION
(This space for your optional use.)
Paoo 1 of S
burden tar this Informalion la MtkntM to
Sdhoweperi
of 32 tam
eeerchhM wdettng dele
ring MflHMaNng tha
and Lonolaiing and
_ . .. ,, ooMacttan of Manhattan.
Sand ocmmenu naadina Mt tun HkMto dOrr any Mhar aeesppaect oi ttti
collection i of information. Including
gtaQasttanfc for rodudno tNa burden. to
Chd,___Information Policy Branch
(PM-223), US SPA. 401 M St.. SW,
Washington, D.C. 20400 Attn: TW
Burdan and to the Offled of tnformatlm and ftogiaatory Affair*. Office of
ManoeamafK and Budget PipowM
noduction | Project
(20HHJ093),
WaaNngtoii. D.cTkWCD.
1.1 Am you etslmlne Uo chemical Identity on page 3 trad* sacref?
1.
\ j Yoa (Answer Question t.2;
[ No (Do not tmwar t.2:
Altacn substantiation terms. 1
Go to question t.3.)
1.2
N "Yes* In 1.1. la th [ ]sanitiaed[ ] UrwdWtlaad
1.3 Oapnrtlnq Yoa 19.98,,
2. CERTIFICATION (Road and sign aftor completing al tactions.I I haraby certify that (have rationed tha attached doeianants and that, to tha boat of my tawatdga and boliaf, tho auOnVttod MarmatMi 1is true and complete and that tha amounts and value* in this report are accurate based on reasonable estimates using data available to tihhae preparers of this report.
Nam and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
Signaur*
Date signed
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Wesclake
State
Louisiana
P.0. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See Instructions
70669
Appendix E)
This report contains Information for (Check < 3.2
.[x] An entire facility
t ] Part of a teMIty.
Technic *1 Contest
3.3 Brandt Butler
Pitalic Contact 3.4
Don R. Unruh
C Code (4 dKjit)
3.S .2911
3.6
030
b. na
Latitude Minutes
14
e.
Seconds
36
Dun a Bradstreel Number(s)
3.7 . 00-842-7692
EPA Uanttfiealten Number(s) (RCRA I.O. No.J
3.8 .LAD990683716
f#>0S Permit Numtoer(s)
3.9 .LA0003026
nsoelytng Streams or Water Bodies (enter one name per ms)
..Bayou Verdine
d. Degrees
093 NA NA NA b. NA
Telephone Number (taduda erea code)
118-491-5599
Telephone fkartaer (Include am. code)
318-491-5222
e-
Longitude Minutes
16
t.
Seconds
20
3.10
Underground infection Wed Coda (LAC) identification Niartaarlsl
3.11 aNA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Out a Bradstreet Nwiteer
4.2 00-131-5704
EPA Form 9350-J (1-69) Revised--Oo not use previous versions.
(Important: Type or print; read instructions before completing form.)
O' EPA
REPA FORM
part n. OFF-SFTE LOCATIONS TO WHICH TOXIC
CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Addm
Pag* 2 of 5 (This space for your options) use.)
City
County
City
County
Stete
Zip
State
Zip
2. OTHER OFF-SITE LOCATIONS (OO NOT REPORT LOCATIONS To WHCH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE).
2.1 Off-slte location name
BFI )EPA UentHicaiian Number (RCAA O. No.
NA
Street Address
Cities Service Hwy at 1-10
CHy
Sulfur
County
Calcasieu
Stele
Louisiana
Zip
70664
H fecetidn under eontrol ot reporting lecUlty or parent company?
2.2 Off-site location name
NA
EPA tdentdicetion Number (RCRA O. No. I
Street Address
City Stete
County zip
Is location utdar control ot reporting facility or parent company?
[ ]y* [xJn
[ U [ ]
s.Z Off-slte location name
EPA tdenUtteaMon Number (RCRA C. Ne)
2.4 Off-slte location name EPA identltteatton Number (RCRA O. No.)
Street Address
Street Address
City
Canty
City
County
State
Zip
State
Zip1
Is location under control of reporting facility or pb-ant company?
2.S Off-site location name
[ ]v~ l ].
is location under control of reporting facility or psijent company?
2.6 Off-site location name
1 ]v,, [ ]
EPA Identuicetlon reanber (RCRA O. No.)
EPA Identification fkanbb- (RCRA O. No.)
Street Address
Street Address
City Slate
County Zip
City stats
CourSy -----------------------------------------
a location inoer control of reporting ledkty or parent company?
[ ] Yes
[ ] No
is location tmdsr control of reporting facility or paroht company?
[ ] Cheek If eddrttonei pages of Part we attached. How many?
EPA Form 9350-1(1-09) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART til. CHEMICAL-SPECIFIC INFORMATION
Page 3 of $
(TwJ space for your optional use.
CHEMICAL lDENT(TY(Oo not complete two taction If you complete Section 2.)
1
1.1 [Reserved) CAS Number (Enter the number exactly as it lopsin on the 313 list. Enter NA H reporting a chemical category. |
1.2 100-41-4
Chemica) or Chemical Category Name (Enter the name exactly as tt appears en the 313 Utt.)
1.3 Ethylbenzene
Generic Chemical Name (Complete only If Parti. Section l.i is checked *Ves.* Generic name mat be structurally daecrlpOve.) 1.4
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1.1 !
2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (e.g.. numbers, letters, epeees. punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check l that aootv.l
Manufacture the chemical:
3.1
r a.l gj Produce
If produce or Import: f 1 For on-site
C-L XJ use/proceosing
T d-L
1 Fori sale/ J distribution
b. [ ] Import
e.[ ] As a byproduct
f.[x ] As pn Impurity
Process the 3.2 chemical:
f1
__ _
* 1 XJ Ae a reactant
d.{ ] Repackaging only
. f V1 As a formulation
b-l XJ component
r 1As an article c-l Jcoiftonent
3.3
Otherwise use the chemical'
f 1 As a chemical a-l J processing aid
.T 1 b.l J As a manufacturing aid
f1 c.l J Anc^Ury or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURINQ THE CALENDAR 1VEAR
1 n 17 1 {enter coda)
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Reiease (bs/yrj
You may report releases of less than 1,000 tos. by checking ranges under A.l. (Do not use both A.l and A.2)
A.l Reporting Ranges
0 1-409 500-000
A.2 Entor
Estimate
5.1 Fugitive or non-point air emissions
5.1a (][][]
9,000
5.2 Stack or point air emissions
[][][]S.2a
1,600
5.3 Discharges to receiving ... 1 A| streams or water bodies 5.3.1 1------l
(Enter tetter code from Pert 1 Section 3.10 (or ctreem() in the box provided.)
1 '1 5.3.2 1___1
5.3.3 O
5.3.1a [][][] 5.3.2a [][][] 5.3.3a [][][]
39 NA
5.4 Underground injection 5.5 Releases to land
5.S. 1 On-*ite lendtiii
5.4a [][](!
5.5.1a [][][]
NA NA
S.S.2 Land treeiment/apptication farming
t5.5.2a 1 [ 1 [ 1
0
8. Basts of , { Estimate (enter eo^
L Jq5.1b
j
l1
5.2b LoJ !
5.31b GD 5.3.2b Cl
C. % From Stormwater 5.3.1c NA
5.3.2c NA
5.3.3b
LJ5.4b
5.5.1b |___H
5.5.2b C3j
5 5.3 Surfece Irr^oundmeni 5.5.4 Other di*poel
S. 5.3a [][][] 5.5.4a [][](]
NA NA
5.5.3b 5.5.4b Q
[ 1 (Cheek (f additional information is provided on Part rv-SuotMamanial Information.)
EPA Form 9350-1(1-89) Revised--Do not use previous versions
oooo056?
SAL
(Important: Type or print; read instructions before completing form.)
^ EPA
epa formR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 ol 5 (TN space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfer* of lest than 1,000 to*, by checldna ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfers (tos/yr)
A.1 Reporting Ranges
0 1-40B S00-BBQ
A.2 Enter
Estimate
6. Basis of Estimate (enter code)
Discharge to POTW
__
(enter localton number 1.1)
6.1.1 worn Pert Section t.) L_J l__ 1
[][][]
HA
6.1.1b O
Other off-ene location
------,
. (enter location number ] 2 6.2.1 from Pan a. Section 2.) j f |-{
][
1r
it
]
NA
6.2.1b C]
Other oll-slte location
__
e i e !'t*r localIon ntanbor I 2 1 I 6.2.2 from Part l. Section 2.* 1__iL _ 1
6.2.2b Q
Other ofT-*lte tocatton (enter tocatton number
,1-----,,dt
j
6.2.3 from Part 1. Section 2.) ( *_
t
6.2.3b 1 ]
[ ] (Check If addWonal information it provided on Part IV-Supptemental Information. |
b.Type of Treatment/ Disposal
(enter cart*)_________
6.2.1c lMl 1 1 6.2.2c |Mt 1 1 6.2.3c |Mf 1 I
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General
Wastestream
(enter code)
6. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
D. Sequential
Treatment? {check if
applcabfe)
7.1a
7.1b
1
1
7.1c 0
7.,d [ ]
'.2a
7.2b
kiiJi 1
7,2c 0
7.2d [ ]
7.3a
7.3b
I *l0|7|
7.3c 0
7.3d [ ]
7.4a
7.4b
1 "UU
7.4c
7.4d [ ]
7.1e 7.2e 7.1e 7.4e
7.5a 7.6a
' 1 1 1 1 7> 1 J.I.I
7.5c 7.6c
7.Sd [ ] 7.6d [ ]
7.Se 7.6e
7.7a 7.6a
7n> 1 1 1 1 7.eb | | | |
7.7c 7.6c
7.7d [ ] 7.8d [ ]
7.7e 7.Be
7.9a
7Sb 1 1 1 1
7.9c
7.9d f ]
7.9e
7.10a 7.,0b | | | |
7.10c
[7,0d
]
7.10e
[ } (Chock tf addWonal information Is providod on Part tV-Suppiemonta) Information.)
ill
111
F. Based on
Operating Oata?
Yes
No
95 % 7.If 100 % 7.2f
[ 1 ( x] [ 1 ( X1
%87.
7.3f
% 7.4f
[ X1 t ] [ J[ 1
% 7.5f % 7.6f
[ 1l 1 [ 1[ 1
% 7.7f
[ 1l 1
% 7.flf
[ 1[ 1
% 7.91
I 1( ]
% 7.10f [ 1 t 1
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(tndteate actions taken to reduce the amount of the chemical being released from the faeffty. See the Instructions for coded
Hems and an explanation of what Information to Include.)
____________________________________ ____________
A. Type of ModMcation (enter code)
B. Quantity of the Chemical In Waste* Prior to Treatment or Disposal
C. Index
0. Besson for Action (enter code)
1 |m| 1
Currant reporting
year (tos/yr)
Prior year
(tos/yr)
{ Or percent , change (
l !* 1
|r] I
EPA Form 9350-' m -89) Revised - Do rot use previous versions
SAL 000005 671
(Important: Type or print; read instructions before completing form.)
3 EPA
EPA FORM R PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addhtonal spec# for answers to questions in Part m. Number the fines used sequential^ from fines In prior sections (e.g.. S.3.4, 6.1.2. 7.11)
Page S of 5
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III, Section 5.3)
You may report releases of less than 1.000 lbs. by cbecMng ranges under A.1.
(Do not use both A.1 and A.2)
5.3 Discharges to receiving streams or water bodies
5.3..
A. Total Release (fas/yr)
A. I Reporting Ranges _2________MW MO-BW
A.2 Enter
Estimate
(enter in box
provided
[][][]
5.3..
C.% From Stormwater 5.3----------c
ier tetter code from Part*" S.3_____
K [lion 3.10 tor ctream<| the Doa provided.)
S.3_____a
1[
1[
1
S.3.
S.3.
5.3..
[][](]
S.3.
5.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6) ________
You may report transfers of less than 1.000 tos. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
o i-tee 6oo eee
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C, Type of Treatment/ Olsposal
(enter code In box
provided)
_ 6.1.
Otacharg* e POTW
--,
tenter location tamper I . I I I
[][][]famPetl. Section 1.1 < 1 1| I
1.1._____b O
6.2.
6.2.
6.2.
Other ofl-ette tacaticn
t EOenter location number rom Part t, Section L|
Ojetnhteerr^oiWoc-asHtlcentaracmatibce?nr ,aa
i Part . Cactien
Other oW-Wte location tenter tauttoMinSw worn Pert I. 6action
IHH1
[nit]
(][][]
6.2. 6.2. 6.2. Ml
6.2.
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III. Section 7)
A. General
Wasteetream (enter code In box provided)
B. Treatment Method
(enter code
In box provided)
C.RanQe of Influent
Concentration (enter code!
D. Sequential
Treatment? (check If appicable)
E. Treatment Efficiency Estimate
F. Based on Operating
Data? Yes
No
7. 7.
7.
[)
l ][ 1
7. -* 7.
7.
[]
( ][ ]
7. 7.
7.
--[ 1
7. [ H ]
7. 7. 7. 7. 7. 7. 7. 7.
7.
-0[ ]
-
---[ 1
7. -t 1
---I ]
MM
[ It J
[ 11 1
[H1
7. 7.
(1
7.1 ( ][ 1
7. 7.
7.
-I ]
7., .[ H 1
EPA Form 9350-1 (1-69) Rerised--Do not use previous versions.
SAL 00000$672
(Important: Type or print; read instructions before completing form.)
Form Approved OMB Wo.: 2070-0093 Approval Expiree:. 01/91
Peoe 1 of S
5EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Commtmky Rlght-to-Know Act of 1986. also known ae Title IH of the Supecfiatd Amendments and Reauthorteatlon Act___________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This apace for your optional use.)
Public
ting burden tar this
eoltacttan < ' Mormattan ta MMatM to
vary earn
3< noursper response,
wttn an
of 32 hour* par
time lor revtaeinq
aaafUdng witting data
rtng ano maMatrang the
oompletlnq and
letion of Mormatton.
Band
tom* regarding this burden
MlktwM ' any other aspect o1 Uvs
ooltaettan at Mormattan. inotudino
suggestions tar reductao this burden. to
Chief. Mormattan Policy Branch
(PM-S23). US EPA 401 M St.. SW.
Washington. D.C. 20460 Attn: TRi
Burdan and to mt Offtoa of Mormattan
and napjatacy Atlaira. Otftca of
Managemtait and Budget Ptpaaarh
Raduettan
Protact
(2070-0003).
WasN^tah. O.C. 20603.
1.1 Ara you claiming the cnamteaf Identity on paga 3 trada acral?
1. [ ] Yes (AnswerQuestion t.2; ______________ Aitacn substantiation forma.\
No (Oo not antiwar 1.2: Go to Quasi tan i ,3.)
1.2 H -Yaa* In 1.1. ta this copy: [ ]sanKtaad[ ]unaanitlaad
1.3 Reporting Year 19-86--
2. CERTIFICATION (Read and sign after completing al sections.)
1 hereby canity that I turn* reviewed tha attached dooumantt and that, to tha batl of my hnovrladga and baltaf,. tha submitted InfiniMttttaann Ita true and
complete and that tha amounts and valuaa in thta raport ara aecurata basad on reasonable asttmatas using data available to tihhaa|praparars of this reeort. Nama and official lilta of owner/operator or senior management official
Don R. Unruh, Refin^xy. Manager
Slgnatura
Data slgnad
Facility or Establishment Nama
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PRO 5CTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
Slate
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-02 66
County
ATTN: TOXIC CHEMICAL RE LEASE INVENTORY
Calcasieu
Zip coda
2. APPROPRIATE STATE OFFICSf (See instructions
70669
Appendix E)
This report contains Mormattan tar (Ctaet one); 3.2
Jfv 1
a. [X An entire faefttty
Jf 1
b. 1
Part of a facftfty.
Technical Comact 3.3
Brandt Butler
Public Comact 3.4
Don R. Unruh
Telephone Nwnfiar (Inchide area ooda)
318-491-5599
Telephone Number (tadtita area ooda)
318-491-5222;
SIC Coda <4 digit)
3.5 .2911
3.6
Oagreaa
030
b. NA
Latitude Minutes
14
Seconds
36
d.
Degrees
093
#.
Longltuds Minutes
16
1 i.
Seconds
! 20
Dun & Bradstraat Number(s)
3.7 .. 00-842-7692
EPA Uentlftaatton Number(t) (PCAA LO. No.)
3.8 .LAD990683716
o. na b. NA
NPOES Permit tAanber(s)
3.9 .LA0003026
rteoelvtng Streams or Water Oodles (enter one nama par (mm)
.Bayou Verdine
b. NA b. NA
3.10 e.
d:
a.
Underground ejection Walt Coda (UtC) Uamifieattan Nurrtaer(t) | 3.11 a.NA
PARENT COMPANY INFORMATION Nama of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Out l> Bradstraat Njnbsr
4.2 00-131-5704
EPA Form 9350-1 (1-89) Revised--Do not use previous version*.
f. b.
!
]
^SAL 0000056173
1
I
i
0*t
u
(Important: Type or print; read instructions before completing form.)
tPAe\ rriA
9
REPA FORM
PART II. OFF-SITE LOCATIONS to which toxic CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMEf"
1.1 POtW n*m
NA_ .. .
Street Address
1.2 POTW name Street Address
(This sp4ce for your optional use.)
1
|
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHCK WASTES ARE SENT OM.V FOR R(CvjxMO OR REUSE).
2.1 Off-site location name
BFI
EPA tdentifteatton NurrV>er (RCRA O. No. I
NA
Street Address
Cities Service Hwy at 1-10
2.2 Off-site location name
NA
EPA toenttfieation Number (RCRA O. Na.\
Street Address
1i
------i-r
It location under control of nportlng (acuity or psrM 1
| [ ]vee Ixl'**
i u]v
t
2.3 Off-(te location name EPA UentilteeUon Number (RCRA E>. No.) Street Address
2.4 Off-tile location name EPA loentMieetion Nwnber (RCRA O. No.) Street Address
!
Ctty Stete
County Zip
City State
cowity zip !
tt location under donuts e1 reporting facMHy or parent company?
2.5 Off-site location name
[ ]v- [ ].
EPA UentlOoatlen Number (RCRA D. No. 1
is location under control el reporting facility or parent company?
2.6 Oil-site location name EPA ttwitifteatlon Nuntv (RCRA . No )
[j ]y~
' |
|
[ ]
Street Address
Street AdOest
City Stale
County ZIP
City State
Cowtly] Zip
ea|lon wider control d reporting facMKy or parent company?
[ ]. [ U
ts location wider comet of reporting facility or parent jcons>any7
[jlv-
l ].
[ ] Ctwefc It addMonel pages of Pert I are attached. Mow many?
PA Form 9350-1 M-69) Revised--Do not use previous versions-
(Important: Type or print; read instructions before completing form.)
S-EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S
nt
(Thta space for your optional uss.)
1. CHEMICAL IPgNmV(Do not complete this section If you complete Section 2.)
1.1 (Reserved)
CAS Number (Enter the numb*
1.2 74-85-1
,ty a* tt
en the 313 list. Enter na H raportho e eernteal eat
Chemical or Chemical Category Name (Enter the name exactly as tt
on the 313 Ust.|
1.3
Ethylene
structural
Generic Chemical Name (Complete ety tr Part I. Seel ton J. t ts cheeked *Ye.* Generic name must be
Ry descriptive.)
1.4
MIXTURE COMPONENT IDENTITY (Do not oomotete this section If you complete Section 1
.2 Generic Chemical Mama Provided by
(Umtt the name to a maximum of 70 character* (e.g., luibei,
, space*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aooN.)
Manufacture the chemical:
3.1
a.[x] Produce
If produce or import:
L 1 For on-site c.P- J use/processlng
<*-[
IdEtiSuftion
b. [ ] Import
e.[ ] As a byproduct
f.tx] a! an Impurity
Process the 3.2 chemical:
a. [ x] As a reactant d. [ ] Repackaging only
f 1 As a formulation '-l * component
f 1A4 an article *.l J component
Otherwise uss the ehemieel:
^ J J At a chemical
or other use
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total RtMease (tos/yr)
You may report releases of less than 1.000 be. by cheeking ranges under A.1.
(Do not use both A.i and A.2)
A.I Reporting Ranges
0 1-496 500-990
A.2 Enter Estimate
B. Basis of
Eetimatd
(enter cede
S.t Fugitive or non-point air emission#
5.1a Mill]
14,000
5.2 Stack or point air emissions
5.2a (HIM
5.3 Discharges to receiving
I
streams or water bodies 5*3-* I--J
(Enter teller cede from Part I Section 3.10 for stre*m() in (he pox provided. >
j| 5.3.2 I____1
-------
I5.3.31
5.3.fa [][][]
5.3.2a [][][]
(HIM5.3.3a
5.4 Underground injection 5.5 Releases to land
5.S.t On-site landfill
5.5.2 Land treatment/application farming
t5.4a 1 l 1 [ 1
5.5.1a [][][]
[5.5,2a 1 l It 1
NA NA
NA NA NA
5.3.1b 5.3.2b 5.3.3b
5.5.3 Surface impoundment
5.5.3a [][](]
NA
.5.4 Other disposal
5.5.4a [][][]
NA
S.S.4b
tU (Chack if additional information is provided on Pari tv-Supplement*1 information.
EPA Form 9350-1(1-89) Revised--Do rvol use previous versions.
SAL 000005675
(Important: Type or print; read instructions before completing form.)
0 EPA
epaformR
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
page a i 5 (This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfer* of less than 1.000 to*. by cheeking ranges under A.1. (Do not use
both A.1 and A.2)
A. Total Transfer* (toe/yr)
A.1 Reporting Ranges
0 1-4S8 SOP-COS
A.2 Enter Estimate
B. Baals of Estimate (enter code!
Discharge to POTW
1 .
(enter location nuntter f . 1 1
[][][]8.1.1 from Pert 1. Section l.| [ 1 11____
NA
6.1.1b O
Other off-site location
. ..
, . . (enter location nunttor 1 9 1 i 6.2.1 from Pert a. Section2.) | .* |-(
[][](]
Other off-site location
-
[_ . _ (enter toealton nunOw ] !
it
1r
i
NA
6.2.1b n 6.2.Zb n
Other efi-ette looation r. (enter location runtter 9 1 6.2.3 from Pan a. Section 2.) * ]
.
M[
M
1
6.2.3b n
[ ] (Check If addMonal Information la pro*dad on Part IV- Supplemental Information.)
C.Type of Treatment/ Disposal
(enter code)
6.2.1c 1 1 1 6.2.2c M| | | 6.2.3c M |
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code!
B. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
7.1;
7.1b
Ql
7.1c
7.2a
7.2b
7.2c
D. Sequential
Treatment? (check If appteabte)
7.Id 7.2d
[1
[]
E. Treatment Efficiency Estimate
7.te
7.2e
7.3a
7.Sa 7.6a 7.7a 7.6a 7.9a 7.10a
0
7.3b
7.4b 7.Sb
[
7.6b
[
7.7b 7.8b
C
[
7.9b
Q
7.10b
7.3c 7.4c 7.5c 7.6c
7.7c
7.6c
7.9c
7.10c
[ ]7.3d
t 17.4d
7.5d [ 1 7.6d [ 1 7.7d t 1 7.8d [ 1 7.9d [ 1 T.IOd t 1
7.3e 7.4e 7.5e 7.6e 7.7e 7.6e 7.9e 7.10e
[ ] (Check If addttlonal formation is provided on Part IV-Si^ptcmcntal Information.]
F. Based on Operating
Oata? Yes
No
7.1f (111
7.2f [ ] [ 1
7.3f tit]
7.4f till
7.Sf tit]
7.6f t 1 t 1
7*7f tit]
7,8f
tltl
7.9f tltl
7.lOf t 1 t 1
6. OPTIONAL. INFORMATION ON WASTE MINIMIZATION (Indtoate actions taken to reduce the amount of the chemical being released from the facSty. See the instructions for coded
A. Type of Notification (enter code)
H1
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
Current reporting year (tos/yr)
Prior year (bs/yr)
j Or percent ( change ,
1 f* 1
'EPA Form 9350- -69) Revised - Do not use previous versions
C. Index
D. Reason for Action (enter code)
lt- 1
SAL 000005676
(Important: Type or print: read instructions before completing form.)5 of 5
a PDA
EPA FORM R
v CrM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addttlonal space for answers to questions to Part Ml. Number the Hnes used sequentialy from Ines In prior sections (e.g.. S.3.4. .1.2. 7.11)
(This space for your optional use.)
AOOmONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part HI. Section 5.3)
You may report releases of less than 1.000 fes. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (t>s/yr)
' A.1 Reporting Ranges 0 S00-999
Estimate
5.3 Discharges to
,--.
receiving streams or
|1
[][][]water bodies
5.3--------L--) 5.3_____
B. Basis of Estimate
(enter code prodSell
C.% Prom Stormwater 5.3______bD
S.3_______c
(Enter totter cod* trom Pert 1
11
Section 3.10 tar tirttomtt) in c n
I__1
[][]{]the bo* prowded.)
-----------
5.3_____a
[][][]S.3_____a
5.3.____JO 5.3._____c
S3._____bC 5*3-_____c
AOOdTONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part HI. Section 6)
You may report transfers of less than 1,000 tos. by checking ranges under A. 1. (Do not use
both A.1 end A.2)
A.Totat Transfers (bs/yr)
A.1 Reporting Ranges
0 1-4SS 600 ess
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(enter code to box
provided)
I
**
.. 5.1.
Diacharv* to POTW
r--.
tamer location iwnter f . I I 1
[][][]tram Pan t. Section l.j 1 1 M 1
Other etf-ette ioeetlan > i i e (enter location number 1 I 1 1 6*z---------from Pwi . Section 2. > 1 * M___|
Other an olte location r--j i "*i
6.2.
(enter location nuittor 1 3 1 1 1
---------from Pens. Section 2.\ LZJ-I--J
Other eff*eHe location *-- , 6-2._____^pfiWE3S, Q3.U
[][][] [][][] [][][]
6.2._____b 1 1 6.2._____b O 6.2._____b CD
6.2.____c|M| | | 6.1. c|M| | | 6.1. cIm| 1 1
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part ML Section 7)
A. General Wasteetream
(enter code
to box provided)
B. Treatment
Method (enter code to box provided)
C. Range of
Influent
Concentration (enter code!
D. Sequential Treatment? (check If
aooteable)
. Treatment
Efficiency Estimate
F. Based on Operating
OetaT Yes
No
7--
67--- l_l.)J
7. - M I I
*g
-[7--- ]
7.______ e
-[ 17. o Q 7---
7.______ e
% 7 [ H 1 [% H 1
,
.D
_______b I 1 I I
7-----------=
7------------* [ ]
7.______ e
% 7- 1 H 1
7.
. Q 7...
| | | |
7-----------*
7. ,D
7.
7.>> 1 1 1 1
7- - LLU 7._b LLU
' * 7---b LlJ j II 7' * '--1 7. b II II
7-----------= 7-----------* [ ]
7-_c
7-----------b
= 7-. Q7. c b 7-----------
7------------b[
[7 b
7------------b[
0 l7-----------
7. df
]
] ]
]
1
7.______ a 7. e 7. e 7. e 7. e 7. e
% 7-- Mil <[% 7-- H ] % 7- '( H 1 % 7- '[ ][ 1
% 7-[ ][ 1 % 7- ' [ ] [ ]
ERA Form 6350-1(1-49) Revised--Do not use previous versions.
SAL 000005677
{Important: Type or print; read instructions before completing form.)
Form Approved OMB No.; 2070-0093 Approval gvpknee-- 0W9I------
Pago 1 ol S
'S'EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planntaa end Community Right-to-Know Act of 1986,
also known at lute 111 of the Superfund Amendment! end Reeuthorizetton Act__________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
nolle (reporting tmrcMn lor 1N
collection ol Mermetion la aMlmiMe to watryy tfrank 30 to 94 hoiry par response,
wrftn ani varan* of 92 hours par
. inrSudvifl lima tor rMawwe
Instruction*. eawnhlng wasting data
aoureaa. garnering and maintaining the
data needed, and oomniatlng and
reviewing the eeUaetion at information.
Sand carinont* regarcNng this birden
astlmata or any other aapnet ol this
osIMetion ot Viformation, including
suggestions ter reducing this burden. to
Chtet, information Policy Branch
(PM-223), US EPA 0I M St., SW.
Washington, O.C. 20460 Attn: TP)
Burdan and to tha Olfie* of information
and nagulatory Affairs, Office of
Management and Budget Paperwork
Reduction
Project
(2070-0003).
Washington, O.C. 20603.
1.1 Are you claiming the chemical identity on page 3 trade secret?
1.
[ J Ye* (Answer question 1.2;
1 ^ 1 No (De net answer 1.2;
Attach substantiation terms.)
Go to Question (.3.)
1*.2
tt *Yes* in 1.1. Is this eepy: [ ] Sanitised [ ] UnswVtlxed
1.3 flapming Year 19 88
2. CERTIFICATION (Read and sign after completing aM sections.) 1 hereby certify that t have reviewed tha attached documents and that, to the beet of my knowledge and belief, the submitted information is true and oempieta and that tha amounts and values in this report are accurate based on reasonable estimate* using data available to the preparers of inis report. Name and official title of owner/operator or senior management official
Don R. Unruh^ Refinery. Manager
1 Oats signed
lerzk/tf
i
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROtECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0jZ66
Cotedy
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Speeds
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report eantalna information tor (Cheek ana): 3.2
.[X j An entire facMty
.. I 1 Pvt of a facility.
3.3 3.4
Technical Contact
Brandt Butler
Public Contact
Don R. Unruh
Telephone Number (Include area coda)
318-491-559^___________
Telephone Nuntar (include area code)
318-491-522^
StG Coda (4 dW)
3.S a.2911
b. na
3.6
Oeyaei
030
latitude Minutes
14
Dun a Sradstreet Number(t)
3.7 . 00-842-7692
EPA IdentHieatien Number(s) (PCftA i.D. No.)
3.6 .LAD990683716
e.
Seconds
36
d.
Degrees
093
NA
NA
*.
Longitude Minutes
16
Seconds
20
NPOES Permit Numbar()
3.9 .LA0003026
HeoeMng Streems or Water Bodist (enter one name par boa)
Bayou Verdine
NA b. NA
3.10
d.
Underground |action WeU Cede (LSC) Uentifieattwi Number(s) 3.11 HA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Poront Company's Out 4 Bradstreat Number
4.2 00-131-5704
EPA Form 93?"-i (1-69) Revised--Do not use previous versions.
SAL 000005678
(Important: Type or print; read instructions before completing form.)
O. EPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
t. PUBUCLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip State
Page 2 of s
Cpunty
i 4i p
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHKX WASTES ARE SENT ONLY FOR RECVCLtUG OR REUSE).
2.1 Off-site location name BFI
EPA Uentllieatioft Nunder (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Cotetty
Calcasieu
Slate
Louisiana
Zip
70664
e location under control at reporting faculty or parent company?
2.2 Off-slte location name
HA
EPA tdentilicattoA Number (RCRa D. No.)
Street Address
City
County
1l
State
Zip
i
Is location under oontral at reporting faculty or patent company?
[ 1Y~
1x1**
;[ ]v
[ Jh.
*.3 Off-slte location name EPA tdsntlflcstlen Number (RCRA O. Me.)
2.4 Off-slte location name EPA uentldcation Nurrtter (RCRA D. No.)
Street Address City State
Coiaity ZIP
Street Address City State
i
County !
Zip i
Is location taider control o( reporting ledHly or parent company?
2.S OH-site location name
[ ] Yes
[ ] No
Is location (aider control of reports facility or paraftt company?
f ] Yes
[ ] No
2.6 Olf-slte location name
EPA Identification Nwitber (RCRA O. No.)
EPA
ton NMht (RCRA D. Mo.)
Street Address
Street Address
City
County
City
County
State
ZiP State
Zip
location under control of reporting faculty or parent company?
[ ]v
[ ]h.
is location under control of reporting foelttly or parent company?
{ ] Chsdt H eddtUonei pegss of Part t are attached. How newt
EPA Form S350-in-89) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART 1(1. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (This kpace for your optional uas.)
1. CHEMICAL IDENTfTY(Do not complete this section If you complete Section 2.)
1.1 1.2
(Reserved) CAS Number (Enter the number subtly as It appeem on tha 313 Hat. Enter NA K reportmo a chemical catepory.) 7647-01-0
1.3 1.4
Chemical or Chemical Category Name (Enter the name exactly ee it appears on the 313 Ust.)
Hydrochloric Acid
i
Generic Chemical Name (Complete omy if Pert 1. Paction 1.1 ie Cheeked "Yea.* Generic name muet be structurally descriptive.)
1 ---------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------- 1-------------------------------------------------------------
MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) 1 2. Generic Chenseai Name PioniJed by Supplier (Umft the name to a maximum* 70 character! (e.g.. numbers, lottersL spaces, punctuation).)
a. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aootv.1
Manufacture the
If produce or Import:
chemical: 3.1
ry a.l J Produce
f 1 For on-elte e.L J use/prooessing
^T d.L
Jb.[
Import
e.[ ] At a byproduct
f.(
Process the chemical: 3.2
r l d.[
1A _ J As a reactant ] Repackaging only
. f 1 As a formulation J component
f
1
1 For kale/ J distribution ] As an impurity
1 As ajn article Jcomponent
3.3 Otherwise use the chemical:
3 proSweSg*^ ^
b.l ] As a manufacturing aid
c.[x ] AncRery or other use ;
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURiNQ THE CALENDAR YEAR
m (enter code)
8. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yrj
You may report releases of less than 1,000 be. by chocking rangos under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-409 S00-909
A.2 Enter
Estimate
B. Basis of Estimate (enter codb)
S.1 Fugitive or non-point air emissions
5.1a [][][]
610
5.1b
5.2 Stack or point air emissions
5.2a (][][]
16
5.2b
5.3 Discharges to receiving _ , I I
[][][]streams or water bodies s.j.i LA-J
5.3.1a
(Gntr lettar cods tram Partm Ssction 3.10 lor stram(s) in tha box provided.)
r*i S.3.2 1___I
r~iS.3.3
5.3.2a [][][] 5.3.3a [][][]
5.4 Underground injection S.S Releases to land
5.5.1 On-site landfill
tS.4a i r i r ]
5.5.1a [Hill
NA
NA NA
5.3.1b * 3.2b n
5.3.3b 5.4b i.S.lb I I
5.5.2 Land treatment/application 1arming
5.5.2a [][][]
NA
5.5.2b
5.5.3 Surface impoundment
5.5.3a [][][]
NA
5.5.3b
S.S.a Other disposal
5.5.4a [][][]
[ ] (Cheek if additional Information i* provided on Part (V-Supplementa! information. )
NA
5.5.4b
EPA Form 9350-1(1-89) Revised --Do not use previous versions.
SAL 000005680
u
(Important: Type or print; read instructions before completing form.)
O EPA
'
EPA FORmR PART 111. CHEMICAL-SPECIFIC INFORMATION
(continued)
Pag* 4 of S
(This spaces for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1.000 lbs. by cheeking ranges under A. 1. (Do not use
both A.l and A.2)
A. Total Tram ifers (tes/yr
A.1 Reporting Ranges
0 1-499 500-909
A.2
Enter Estimate
8. Basis of Esdmats (enter code)
(enter location number . | j
[][][]e.1.1 from Part 1. Section t.)
___|
KA
Other eft-tte localhan .-----. _ _ ,, looter location numoer i - I ]
(Mill6.2.1 from Pans, Section 2.11 2 !( |
Other otT-stt* location --. r --... . , . (enter location number 1 e 1 1
L r6.2.2 from Part , Section 2. J I _J J
]f
ir
]
Other off-*He location
J
(enter location number 1 *1 I | T 1 f
6.2.3 from Pen 1. Section 2.) j
|] ( |
1T j|
1 J
NA
6.1.1b 6.2.1b 6.2.2b n 6.2.3b |"1
[ ] (Check if addtlonal information is provided on Part IV-Supplemental Information.)
C^Type of Treatment/ Disposal
(enter code!
6.2.1c lMl 1 1 6f2.2clMl 1 1 6.2.3c |m| | |
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code}
C. Range of Influent
Concentration (enter code)
D. Sequential Treatment?
(check if appScabte)
E. Treatment Efficiency
Estimate
F. Bated on Operating Data?
Yes
NO
7.1a 0 7.1b IfJfcUl
T.2a
7.2b
|N|A | |
7.3a 7 1 1 1 1
7.4a 7<b 1.11. J
7.1c 7.2e 7.3c 7.4o
7.1b [ ] 7.2d [ ] 7.3d [ ]
]7.4d J
7.le 7.2e 7.3e 7.4e
100% r.if % r.2f % 7.3f % 7.4f
[x ] [ ( ][ [ 1t [ 1[
1 1 1 1
7.Sa 7- I 1.J 1
7.5c
17.Sd [
7.5e
% 7.5f [ ] [ ]
7.6a
7-b
||||
7.6c
7.6d [ 1
7.6e
1 1 1 17.7a
77b
7.7c
17.7d [
7.7e
| | | |7.6a
7.8b
7.6c
[ ]7.8d
7.Ce
7.9s 19* 1 I II
7.9c
[ ]7.8d
7. Be
| | | |7.10a
7.10b
7.10c
[ ]7.10d
7.10e
[ ] (Chock if addhtonal Information is provided on Part fV-Supplemental Information.)
% 7.6f [ 1 ( 1
% 7.71 [ 1 [ 1 % 7.8f l 1 [ ] % 7.9f [ 1 [ ] % [7.10f 1 f 1
. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(kxSeat* actions taken to reduce the amount of the chemical being released from the facftty. See the instructions tor coded Kerns and an explanation of what Information to kidudo.l
A. Type of
Modification (enter coda)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
1 I M|
Current reporting year (toi/yr)
Prior year (tos/yr|
f Or percent t change ,
1 1* l
EsD
EPA Form 9^c'* * '-69) Revised - Do not use previous versions
SAL 000005631
(Important: Type or print; read instructions before completing form.)
&EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section if you need addKionaf space for answers to questions m Part HI. Number the fines used sequontlaly from fines h prior sections (e.Q.. S.3.4. .1.2. 7.11)
Page 5 of 5 (This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
(Part 111. Section 5.3)
_________________________________________________________________
__________
You may report releases of less than T.000 fos. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Rsieata (tos/yr)
A.1 Raportkig Ranges o i-*e soo-eee
A.2 Enter Estimate
5.3 Discharges to receiving streams or water bodies
,--
}J
I
5*3--------L--1 5.3_____a
1t
]t
I
B. Basis ofi Estimat*
(enter code in box i
provided) i
5.3________bCj
C.% From Stormwater 5.3______ c
[Enter tetter cod* Irem Pert l
(1
Seeiton 3.10 ter streemts) in e n
1___1
the bO> provided.)
--------
5.3_____a [][][]
5.3.____bQ S.3._____c
[][][] 5.3______ a
JJ5-3-_____
5-3-_____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Pert III, Section 6);
You may report transfers of less than 1.000 B>s. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.Total Transfers (K>s/yr)
A.1 Reporting Ranges
o t-4ss coo-ees
A.2 Enter
Estimate
B. Basis of Estimate
(enter code Inbox
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
_ . (enter leuU iwntar 1.1 1 1
[][)[]5.1._____from Parts. Section t.) |_JJ|___J
Other off-site locition < 52_____J^p!^X3E?)
[][][]
Other ctt-ette location i i i
[][][]6.2.--(freonmterPleorctaAtio6neneuttnoWn e2r.1
| 21 1 I L__H___1
Other aw efte ioeetlan < - .
I3.U [][][)-- tSTp!sa?,ssr?.l
6.1._____b 6-2-_____h O 6.2._____b O 6.2._____b C]
6-2-.__c|M| | | 6.2. c|m| |_ ) .z; c|m| 1 1
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Fart fll. Section 71
A. General Wastestream
(enter code In box provided)
7- * 7-
7. . Q 7.
B. Treatment Method
(enter code In box provided)
1 1 I I him
C. Range of Influent Concentration (enter code)
7--c
D. Sequential Treatment? (check If appfioabte)
-[ 17---
7.
cQ
7.
d[ ]
E. Treatment
Efficiency Estimate
F. Based on Operating
Data? Yes
No
7. e 7. e
% *
% 7-
`Mil 1 l t )
-[ '[ If 1,
7- b | | I |
7----------- =
7-----------
1 7.______e
%, 7---
7. . Q
- err i*
-I ]7. c Q 7----------
7.______ e
*[% 7-- If ]
!u
*|
7. . 7- b | | | |
b U-t. J7----------7--* b | | | | 7--* 7- 1 1 1 1 *7-- 7- Q1LI
7-_-
, c
Q7. c 7- C Q7. c
of7-----------
7----------- <*[
<[7----------d[7. -[7------------
]
]
] ] ]
7.e , 7.______ e 7._______e 7._______e 7.______
*[ H 1% 7--- % 7 '[ If ]
--[% 7- If 1
% 7---<f If 1 % 7- !l If 1
EPA Form 9350-1(1-59) Revised--Do not use previous versions.
sM_ OOOOQ56S2
(Important: Type or print;read instructions before completing form.)
Form Approved OMB
2Q7Q--OQ93
Approval E^jlTd*:. 01/91
Page 1 of 5
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency PUnring and Community FUght-to-Know Act of 1966.
also known at Title HI of the Suparfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION
INFORMATION
(This space for your optional use.)
tag tauten tor tN< information is animated to
34 hours par responei,
of 32 hour* par
_ time tor tmtaMno aaatxhini) atOtatag data ring anomaHtairing '
containing and
Sand wtlmtte
ocliaction el tatormatim. regarding this burdan
any other aapaet of tM
cotteetton ! of tafcrmatlon, including
suggestion* for radielngthto Otadan. to
Oilal. Information Policy Branch
(PM-223), US CPA, 401 MSI., SW,
Washington, D.C. 204S0 Attn: TRl
Burdan and te tha Ohtoa el information
and Regulatory Affairs. Otttoa ot
Management and Bidgii Paperwcrk
Reduction i Protect
(2070-0003).
Washington, O.C. 20603.
1.1 Are you cialmino the chemical Identity on page 3 trade secrsf?
1.
f ] Yes (Answer question 1.2;
[ ^ 1 No (Oo net answer 1.2:
Altaen substantiation terms. I
Go to Question 1.3.1
V.2
fl 'Yes* In t. 1. is this copy; [ ]sanitUad[ ] Unianltlaed
1.3 Reporting Year 19.82____
2. CERTIFICATION (Read and sign after completing al sections.} I hereby earthy that f haw leitan'ed tha attached documents and that, to the best of my knmfedge and belief, the submitted information is true and complete and that the amounts and vatuas m this raport are accurate based on reasonabto estimates using date available to the preparers o< this raoort.
Nama and official title el owner/operator or senior management eiticial
Don R. Unruh, Refinery. Manager
Signature
Date signed
Facility or Establishment Nama
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
County
ATTN: TOXIC CHEMICAL RE^-EASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See Instructions
70669
Appendix E)
This report contains Sdoimatton tor (Checfc one): 3.2
[x] An entire facility
[ 1 Parte! atacUhy.
Technical Centact 3.3
Brandt Butler
Mile Coitact 3.4
Don R. Unruh
SIC Coda <4 digit)
3.5 4.2911
3.6
0grm
030
t>. na
Latitude Minutes
14
c.
Seocndi
36
Dw A Bradstree! Number(s)
3.7 00-842-7692
6PA Identification Nurrtaar(s) (RCRA LO. No.)
3.6 .LAD990683716
NPOES Permit Mjmber(t)
3.9 .LA0003026
naceiytag streams or Water Oodlss (enter pne name per boa)
Bayou Verdine
Telephone Nurrtaer (inctuta area coda)
318-491-5599|
Tetophone Nuitber (induce area coda)
318-491-5222
d.
Degrees
093 b. NA b. na b na b- NA
a.
Longitude Minutes
16
f.
Seconds
20
3.10 c.
d.
.
Undaryoung tan+actton Weh Cods f\J)C) tdsntificatton Number)*)
1 3.11 aNA
PARENT COMPANY INFORMATION Nama ef Parent Company
4.1 E. I. DuPont de Nemours
Parent Cempwty*s Oun * Bredstreet fdjmbar
4.2 00-131-5704
EPA Form 93c'1- ' M-89) Rdtdsed--Do not us* previous versions.
f.
b.
u
(Important: Type or print; read instructions before completing form.)
a r-riA 0 ERA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PU8UCLY OWNED TREATMENT WORKS (POTWt)
1.1 POTW mma
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip Stata
County Zip
2. OTHER OFF-SfTE LOCATIONS (OO NOT REPORT LOCATIONS TO WCH WASTES ARE 8&tT ONLY POR R6CYQLMO OR REUSE).
2.1 Off-sita location name BET
EPA Idsntlfieaiton Number (RCRA O. Ns.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
6tete
Louisiana
Zip
70664
* b location under control o1 reportbig facility or parent company?
2.2 Off-sita location nama NA
EPA IdsntHicatian Number (RCRA O. No.)
Street Address
City State
County ZIP 1
is location undsr oontrol ot reporting 1acMty or parent oompanyT
I [ J Yea [x]
[U [U
2.3 Olf-stte location namo EPA Identlticatlen Number (RCRA D. No.)
2.4 Off-slta location namo EPA MamNleatlan Msnber (RCRA D. No.)
Street Address
Street Address
City
County
City
County
State
Zip State
zip
Is location under control of reporting facttity or perent company?
2.S Oil-site location name
[ ] Ye. [ ] No
Is location undsr control at reporting facility or parent company?
2.S Oil-site location namo
[ ]v
t ]n.
EPA tdenttllealion Number (RCRA O. No.)
EPA Identification Number (RCRA D. No.)
Street Address
Street Address
City
County
City
County
State
Zip State
Zip
jcatlon under aontrei el reporting facility or parent company?
l
t ] Yes
[ ]no
Is location wde central el reporting faetfity or parent company?
[U
[u
( 1 Cfwok If oddKIonal papas of Pvt *c WKWd, tour many?
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
SrEPA
RERA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (Thle space for your optional us*.
1. CHEMICAL IDENTITYIDo not complete this section tf you complete Section 2.)
1.1 1.2
1.3
{Reserved)
CAS Number (Enter the number exactly a* it appears on the 313 llet. Enter NA If reporting a ohewkeal category. |
NA
Chemical or Chemical Category Name (Enter the mm exactly a it appear* on the eta Met.)
Lead compounds
t .4
Genetic Chemical Name (complete only H pen 1, section 1.1 i* merited Yes.* Qenerto neme muet be stroctwaity descriptive. \
MIXTURE COMPONENT IDENTITY (Do not complete this section K vou complete Section 1.) : 2. Generic Chemical Name Provided by Steadier (Limit the neme to e maximum o< 70 characters (e.g., nuntaii, tetters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check el thet aootv.)
Manufacture the chemical:
3.1
r1 a.l J Produce
If produce or import:
f 1 For on-site c.l J use/processing
.f d*l
b. [ ] Import
e.( ] As a byproduct
f. [
1 For sals/ J cfsfrftxrtion
] As on Impurity
Process the 3.2 chemical:
f1 a-l J As a reactant
d. [ ] Repackaging only
K f T1 As a formtiation b l X] component
f 1 As jan article c**> J consonant
Otherwise use 3.3 the chemical-
f 1 As a chemical J processing aid
r1
__
b.l J As a manufacturing aid
f1
i
c.l J AndMary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURINO THE CALENDARJYEAR. ' 0 15 I |enter code)
5. RELEASES OP THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than 1.000 fcs. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l Reporting Ranges
0 1-409 500-066
A.2 Enter
Estimate
5.1 Fugitive or non-point air emissions
5.1a [][][]
400
5.2 Stack or point air emissions
5.2a [][][]
0
5.3 Discharges to receiving c . . { A 1 streams or water bodies -3 ` 1--1
(Enter letter code from Pert l Section 3.10 for stream(s) in the box provided.)
1] 5.3 2 ____i
5.3.lD
5.3.la [][][]
5.3.2a [][][] MMM5.3.3a
5.4 Underground infection
5.4a t H H 1
0
NA
NA
5.5.1 On-lte landfill 5.5.2 Land treatment/application farming 5.5.3 Surfaca Impoundment 5.5.4 Other dispotal
S.5.1a [][][]
S.5.2a {][][!
[ ] ]5.S.3a
f ][
S.S.4a [}[][]
NA NA NA NA
B. Basis of 1 1 Esttnate 1 (enter eo^ei
S.lb 0 5.2b d j 5.3.1b P 5.3.2b D 5.3.3b Q 5.4b [J
5.5.1b P 5.5.2b P 5.5.3b P 5.5.4b P'
[ ] (Check if addiiton*i information >s provided on Part tV-SuPPlamontal kiforrrvatlon.)
EPA Form 93S0-1 H-69) Revised--Oo r>ot use previous versions
SAL 000005685
(Important: Type or print; read instructions before computing form.)
pp/\
EPA formR
PART III. CHEMICAL-SPEC1RC INFORMATION (continued)
Pag* 4 of S (This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less man 1.000 tbs. by checking ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-409 500-090
A.2 Enter Estimate
B. Basis of Estimate (enter codel
CMeetwge to POTW
{enter location mvnber (
6.1.1 from Part I. Sactton 1.)
][
][
1 NA
6.1.1b CH
Other off-*It# location
, __
_ _ _ (antar location number 19 11
t6.2.1 from Part K Sectwn 2.> ( 2 ||
1f
1[
1 HA
i.2.1b I 1
Other off-ette location
(enter location number
:BG[from Part I. Section 2.
O{ethneterroloffc-aatlito*nloncuamtiobnerBd[
6.2.3 from Pan I. Section 2
It
ir
1(
it
3
i
1.2.2b | I
a6.2.3b
[ ] (Check If addWooal information ts provided an Part IV-Supplemental Information.)
.Type of Treatment/ Disposal
7. WASTE TREATMENT METHOOS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
D. Sequential Treatment? (check If
applcable)
E. Treatment Efficiency
Estimate
7.1a 7.2a 7.3a
'.a
7.1b 7.2b 7.3b 7.4b
Em
7.1c 7.2c 7.3c 7.4e
7.Id [ I
7.2d 7.3d 7.4d
[1 [1
(1
7.1* 7.2* 7.3* 7.4*
7.5a 7.6a
7.5b 7.6b
7.5c 7.6c
t 17.5d
7.6d [ 1
7.5* 7.6*
7.7a 7.6a 7.9a
7.7b 7.8b 7.9b
Q
7.7c 7.6c 7.9c
7.7d [ ]
7.fid [ ] 7.9d [ 1
7.7* 7.8* 7.9*
7.10a
7.10b
7.10c
7.10d [ 1
7.10*
[ ] (Check If additional information is provided on Part (V-Suppl*mental Information.)
F. Based on Operating Data?
Yes
No
7.If 7.2f 7.3f 7.4f
[ ]f ]
[ ][ 1
[ ][ ]
[ ][ ]
7.5f t 1 l 1
7.6f [ ] I 1 7.7f [ ] [ ]
7.8f M [ 1
7.9f [ ] [ ]
7.10f (HI
fi. OPTIONAL INFORMATION ON WASTE MINIMIZATION (tntfeate actions taken to reduce the amount of the chemical being released from the facftty. See the instructions for coded Items end an explanation of tehat Information to Include.)
A. Type of Modification
(enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Olsposaf
C. Index
fO. iaeon for Action enter code)
Current reporting year (toa/yr)
Prior year
(bs/yr)
Or percent change
Ml
EPA Form 9350 f H-69) Revised - Do not use previous versions.
SAL 000005686
(Important: Type or print; read instructions before completing form.)
A rnA
'O' CrM
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section H you need addhlonai space for answers to questions In Part HI.
Number the Hnes used sequentlaiy from flnes ki prior sections (e.g., S.3.4, 6.1.2. 7.11)
pQq S of 5
(This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III. Section S.3).
You may report releases of less than 1.000 lbs. by checking ranges under A.t.
(Do net use both A.1 and A.2)
5.3 Discharges to
receiving streams or water bodies
,
II 5.3----------L--J
A. Total Release (bs/yr)
A.1 naporttog Ranges o i-*ss 500-ass
A.2 Enter
Estimate
[Mill5.3_____
B. Basis tof Estimate
(enter code InboxT
provided)
5.3______tO
C.% From Stormwater 5.3________c
(Enter tetter oMf from Pert 1
(|
Section 3.10 tor <treem(<) in ct
1___1
the boa provided.)
3 J-----------'
5.3_______
[][][]5.3_____a [][][]5.3_____a
5.3.____bQ 5.3-______c
_bCS-3-
5-3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS'
(Part 111, Section 6)
_______
You mav report transfers of less than 1.000 lbs. by checlolng
ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 nsportlng Ranges
o i-4so boo see
A.2 Enter
Estimate
B. Basis of Estimate
(enter code in box
provided)
C. Type of Treatment/ Disposal
(enter code in box
provided)
Diecnero* to POTW
,,,,
.,
(enter location nanbar [.If 1
[Hill6.1.from Pari 1, Section 1.) | 1 |.|]
6.1._____b n
e5
Other off*Pie location t H r~t (enter location luntar 1 * I 1 |
[][][]----------from Partfl. Secttean 2.) 1 * 1.1____|
Other oh eha location i t >
6.2.
(enter locationnunSiei 1 S 1 1 1
[][][]----------frwn Part . Section 2.) 1_____H___1
Other oh olta location -- . --
(][][]62-----------
6.2._____b 1 1
ns.2._____b
.2._____b n
. n.*.
h
6.2. c|M| t 1
6.2.
c|m| 1 1
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III, Section 71
A. General Wastestream
(enter code in box orovidedl
B. Treatment Method
(enter code
in box provided)
C. Range of
Mkient
Conranti itton (enter code)
D. Sequential Treatment? (checkK apolcabtel
E. Treatment Efficiency
Estimate
F. Based on Operating Data? Yes
No
7--` Q7. .
77-
1 1 1 1
t 1 1 1 1
7.
c
7.
d[ ]
7.
e
n7. c
7.
df ]
7._______e
% 7 '[ H ]
[ ] [ ]% 7-
'
| | | |, 7-
- - cm7. . Q
7.
CQ
7.
d[ ]
7.
e
7.
cQ
7.
d[ ]
7.
e
% 7 '( ][ ) % 7- 'I H ]
7- * 7- b 1 1 1 1
7. . Q
| | |7- b | , . 7- > LL.J 1
* 7--n 11
I7--* 7-. _b | | | |
7- . b
7-----------= 7- . 7- c7.
7.
7-
7. 7. 7.
d[ ]
-[ ] d[ ] ]d[
d[ }
7._______e , 7. e 7._______e 7.______ e 7.
% 7-
%7
% 7-
% 7-
% 7.
'MM
'MM
<[ H ] <[ H 1 [f 1 [ ]
EPA Form 93S0-1(t-89) Revised--Do not use previous versions.
SAL 000005687
Form Approve OMB Nd.:. 2070-0093
Approval Expires:. 01/91
Paoe 1 of S
u'5, Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Flaming and Community Wght-to-Know Act of 1966. also known as Title III of the Super-fund Amendments and Reauthorization Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public reportlrw burden tor this
collection of Information la MllmtMd to
very from 30 to 34 hours par rtipoui.
with an nsrag* of 32 hows par
raiponaa, btouafinq lima for reviewing
Instructlone, eeerching oalHwa data
sources, gathering ara maintaining the
data needed, and completing and
rertewkig the collactlen elInformation.
Sand owwfcnb regardtog this burdan
estimate or any outer upaet of this
oollection rl Information, hxskjdtng
suggestions lor reducing this burdan. to
Croat, Monriattan Policy Branch
(PM-223), US &A, 401 M fit.. $W,
Washington. D.C. 20460 Attn; TRI
Burdan and to the Oifioa of information
and Regulatory Affairs, Office of
Management and Budget Paperwork
Reduction
Protect
(2070-0003).
Washington, O.C- 20609.
1.1 Are you ctalminQ the chemical Identity on page 9 trade secret?
1.
I J Yes (Answer Question 1.2;
I *1 No (Do not answer 1.2;
Go to Question 1.3.)
[ ] Sanitised [ ] Umanitlasd
1.3 Reporting Yea
IQ 88
2. CERTIFICATION (Road and sign after completing al sections.)
I hereby certify that I have reviewed the attached documents and that, to the beet of my knowledge end belief, the submitted Mormetien is irue and complete and that the amounts and value* in thie report are accurate based on reasonable estimates using data available to the preparers of this report.
Name end oflidal title of owner/operator or senior management official
Don R. Unruh, Refinery.Manager
Signature
Date signed
Facility er Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street AdQws
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
CotaMy
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See Instructions
70669
Appendix E)
This report contains Information tor (Check one): 3.2
.[x] An entire tacMtty
[ 1b. Part of a faculty.
Technical Contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
Teta^wne Nuvher (Indole area code)
31B-491-5599
Telegtone Nutbv (Include ns code)
318-491-5222
SIC Code (4 digit)
3.5 .2911
b. na
e.
d.
e. 1.
3.6
030
Lalltuoe Minute
14
Seconds
36
093
Longitude Minute*
16
Seconds
20
Own A Bradstreel Number(s)
3.7 .. 00-842-7692
NA
CPA Identification Numher(s) (ACAA I.O. No.)
3.6 .LAD990683716
NA
NPOCS Permit Number(s|
3.9 .LA0003026
ReeeMng Streams or W.u
..Bayou Verdine
(enter one name per box)
NA b. NA
3.10
Underground Infection Web Cede (UC) identification Number(s) 3.11 aNA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E. I. DuPont de Nemours
Pact Company* e Out A Bradstreet
4.2 00-131-5704____________________________________
EPA Form 9350-1 (1-69) Revised--Do not use previous versions.
SAL ; 000005688
(Important: Type or print; read instructions before completing form.)
9a frc-nHAA
REPA FORM
PART il off-site locations to which toxic CHEMICALS ARE TRANSFERRED IN WASTES
<. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name NA
Street Address
1.2 POTW name Street Address
City
County
City
Stats
Zip Stale
Page 2 of
County 2ip
2.1 Off-site location name BFI
EPA identification Number (RCRA O. No.) NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
ZIP
70664
' location under control ot reporting tadUty or parent company?
L I ]v-
Ixl No
Off-slte location name
2.2 Off-slte location name
NA
EPA Identification Number (RCRA O. No.)
Street Address
City
County
State
ZIP
Is location under control of reporting faculty or parent company?
[ ]v t u
2.4 Off-elte location name
EPA Uentiflcatien NunMr (RCRA O. No.)
EPA IdantlflcatiOT Number (RCRA ID. No.)
Street Address
Street Address
cay
County
cay
County
State
Zip
State
Zip
is location under control ot reporting facility or parent eencciy?
2.5 OH-slte location name
[ ][ ] Ye*
No
is location wider control of reporting facility or parentlcempany?
2.6 Q((-*tte location name
[ ]v,,
[ ]
EPA identification Nunev (RCRA O. No.)
EPA Identification Number (RCRA *>. No.)
Street Address
Street Address
City State
County ZIP
City State
County i
Zip
1
jeation under control of reportMg facility or pwent eon^any?
[ ][ ]v~
NO
[ 1 Cbedt If addltipnai pagM at Pan t era attached. Hew mayf
Is location wider control of reporting (acuity or parent Company?
[U
u [
EPA Form 9350-1(1-89) Raised--Do not use previous versions
(Important: Type or print; read instructions before completing form.)
&EPA
REPA FORM
PART t(L CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (ThM space for your optional use.)
1. CHEMICAL IDENTTTYfDo not complete tNa section If you complete Section 2.)
1.1 1.2 1.3 1.4
[Reserved} CAS Number (Enter the number erectly ae it appear* on the 313 list. Enter NA If repdrtMQ chemical category.)
NA Chemical or Chemical Category Name (Enter the name enact* at it appears on the 313 list.) Manganese compounds Generic Chemical Name (Complete enty W Part 1. Section 1.1 is Checked *Yes.* Generic name muet be structurally deeoriptlve.)
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1.1 2. Generic Chemical Mama Prodded by Supplier (Limit the name to a maximum of 70 character* (e.fl. numbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Cheek al that aootv.l
Manufacture the chemieai:
3.1
ri a.l J Produce
If produce or Import:
r 1 For on-sits c.L J use/proeestlng
.f *l
b. [ ] Import
s.[ ] As a byproduct
f.[
1 For sale/ J distribution
]As an tmpurtty
Process the 3.2 chemical:
r * *
d. [
] A- . JAa a reactant
] Repackaging only
.[ V1 As a formulation "*l XJ component
f 1 As *n article c-l J component
Otherwise use 3.3 the chemical*
F 1 As a chemieai * L J processing aid
. f 1.
_
b.l j As a manufacturtog aid
[1 c.L J Anoilary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SrTE AT ANY TIME DURING THE CALENDAR]YEAR
^RELEASES OF"THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (tos/yr)
You may report releases of less than 1.000 bs. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l Reporting Ranges
0 1-4SB soo-eso
A.2 Enter " Estimate
S.1 Fugitive or non-point air emissions 5.1a [][][]
250
S.2 Stack or point air emissions
5.2a [][](]
0
S.3 Discharges to receiving _ _ 1 pA streams or water bodies 5-3`i 1 1
5.3.1a [][][]
(Enter letter cods from Perl 1 Section 3. to lor stream(s) In the box provided.)
] 5.3.2 1
1 1
5.3.2a [][][]
l ] [ ] 15.3.3 n 5.3.3a
[
5.4 Underground injection 5.5 Releases to land
5.5.1 On-alte lendTIH
[5.4a 1 [ ] f 1 Mini5.5.1a
5.6.2 Lend treatment /apehca! ion farming
1 [ 1 15.S.2a [
[
6.5.3 Surteoe impewtdment
5 5.3a Mini
S.6.* Other disposal
5.5.4a [itit]
0
NA
NA NA NA NA NA
B. Basis of
1
Estimate,
(enter codeM
5.1b Gill
5.2b 0
5.3.ib 0
05.3.2b
5.3.3b Q
0S.4b 05.5.1b 0,5.5.2b
s.5.3b 0:
5.5.4b 0
[ ] (Check H additional information it provided on Part IV-Supplementai Information.)
EPA Form 9350-1(1-89) Revised--Do not use previous versions
SAL 000005690
(Important: Type or print; read instructions before completing form.)
ft EPA
EPA F0RM^
PART HI. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 of s
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1,000 bs. by checking
ranges under A. 1. (Oo not use
both A.1 and A.2)
A. Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-490 500-990
A.2 Enter Estimate
B. Basis of Estimate (enter code)
DMWfp* to POTW
(enter location number
,---,-1| |r --.i
[](][]6.1.1 from Part i. Cectton 1.1 i * H I
NA
6.1.ib
__ . 6.2.1
Other off-elte location
l.(enter toeatlen number
from Pan Section 2.)
--| --
1*
|I
II
t i [ i r i NA
6.2.1b
Other ot1-ne localion -- |---- -
, . , (enter location number 1 1
f6.2.2 from Parti. Section 2.1
M
if
ir
i
6.2.2b CD
Other oft-slte location
HO [ ] [ ] [ 16.2.3
-, J
6.2.3b | |
| ] {Cheek if eddMonal Information is provided on Part IV-Supplemental Information.)
(t.Type of Treatment/ Disposal
l Jantercode)_________
6.2.1c ra i i 6.2.2c |M| | | 6.2.3c |M| | |
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent
Concentration (enter code)
| T4 17.1a
n7.1b
7.1c
Mil"T.2a
7.2b
7.2c
D. Sequential Treatment? (check If apptcable)
[ 17.Id
7_2d [ ]
11 1 17.3a
7.3b
7.3c
7.3d [ ]
7.4a
7.4b | | | |
7.4c
[ 17.4d
E. Treatment Efficiency Estimate
F. Based on OperatinQ Data? Yes
No
] [ 17.1e
% 7.If l
[ 1 f 17.2e
% 7.2f
t 1 [ 17.3e
% 7.3f
[ 1 [ ]7.4#
% 7.4f
7.5a
htj
7.6a 76b LLl. .1
7.5c 7.6c
?.Sd [ ] 7.6d [ ]
7.5# 7.6#
% 7-Sf % 7.6f
[ 1t 1 t 1[ 1
7.7a
77b lJ,._L J
7.7c
[ ]7.7d
7.7#
7.6a 7te U.i 1
7.6c
[ ]7.6d
7.6#
| | ||7.9a
7.9b
7.9c
[ ]7.9d
7.9#
| | | |7.10a
7.10b
xx_ [ ]7.10c
7.10d
7.10#
[ ] (Chock if addttlonai Information Is provided on Part IV-Supplemental Information.)
% 7.71
% 7.8f % 7.9f
[ 1[ 1 [ ]1 ] [ 1[ 1
[ ] 1 ]% 7.10f
a. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actions taken to reduce the amount of the chemical being released from the facSty. See the Instructions for coded items and an explanation of what Information to Include. I
A. Type of Modfflcatkxi
(enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current reporting year (bs/yr)
Prior year |bt/yr|
. Or percent I change
I [
I SPA Form 9350-1(1-89) Revised - Do not use previous versions.
SAL 000005691
(important: Type or print; read instructions before completing form.)
-S'EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addttlonaJ spec# for answers to questions fet Port III. Number the Bnes used sequent!sly from Inti In prior sections (e.g.. 5.9.4. 6.1.2. 7.11)
ADDITIONAL INFORMATION ON RELEASES OP THE CHEMICAL TO THE ENVIRONMENT ONSITE
(Pert 111. Section 5.3)
You may report releases of less than 1.000 bs. by eheddng ranges tnder A.1.
(Do not use both A.1 and A.2)
5.3 Discharges to
receiving streams or
water bodies
5
5.3..
A. Total Release (bs/yr|
A.1 Reporting Ranges o i-aee soo-ees
A.2 Enter Estimate
[][]()
B. Basis of Estimate
(enter code in box ,
provided!
C.% From Stormwater i.3______J^] 5.3.
.c
(Enter letter cod* from
[][][]tiaetion 3.10 (or
Pan"
*"
5.3_____I_I ___II
the bo provided.)
5.3_____a
5.3.. 5.3..
[][][]
LS._Q 5.3.
5.3. op5-3-------
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part 111. Section 6)
___________
You may report transfers of less than i .000 bs. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Totol Transfers (bs/yr)
A.1 Repot Uig Ranges
o t-ese <oo esc
A.2 Enter
Estimate
B. Basis of Estimat#
(enter code in box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
1
*
_ 6.1.
DIMS*wee to POTW .. .1--
,
(enter tacattan iwrear 1,1 1 I
[][][]from Pert 1, Section t.J I * M 1
Other o(f-ilt ioeatton i--^ . .
e9
tenter location number 1 11 1
6-z-----------tram Pert S. Section2.) I I.1 1
t
n
]i
i
6-2._____b | |
||
Other off elte location f--t i--i
6.2.
(enter tocetton mrUr | 2 | | 1
-- from Pert I. Section 2.) L_H___1
re
Other off 'Bite location
(enter tocetton number 4 211 l
-- JrwfiPert t. SectionS. 11 * I I___)
1
H
][
1
6.2._____b Q] 6.2._____b 03
c|M| | | .. c|m| | |
AOOITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III. Section 7!
A. General
Wasteetreom (enter code
in box provided)
B. Treatment
Method {enter code In box provided!
C. Range of Influent Concentration (enter code
D. Sequential Treatment 7 (check if
PP**bel
E. Treatment
Efficiency Estimate
F. Based on Operating Data? Yes
No
n
--* --
-*[ ) 7. --[ 1 7.
--' l H ] --[ H 1
--*
7.
A1
A]
--[ 1
7. 7. 7.
-<[ H 1
till
--[ ][ ]
--
---
.A 1 ---[ 1
7. 7.
[H1
][ ]
7.
'---[ 1
7.
-[ It 1
---
--4 ] 7.
/[ H J
EPA Form 9350-1 (1-69) Revised--Do not use previous versions
SAL 000005692
(Important: Type or print? read instructions before completing form.)
Form Approved OM8 No.: 2Q7Q-0093 Approval Expiree:. 01/91
Pace 1 of S
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Right-to-Know Act of 1986.
also known as Title III of the Superfund Amendments and Reauthorteatlon Act___________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public rvetrtlng
tor iNt
coHecttsn of Mormiilen i* mwmm to
very from 30 to 94 hours per response,
with an Mreaa of 32 hour* per
ssss&r ssaruniiai wmim eat*
source*. gathwering Mandm*mimainitMainning me
date needed, and complellno and
rerteetnq th cchectiun etlnformatto.
Send oommirtt regarding IN* burden
estimate or any otter aspect of this
celteotion at information, Inehdine
uagwllont tor reducing this burden, to
Chief, Information Policy Branch
IPM-223). US EPA. 401 M St.. SW.
Washington, O.C. 20460 Attn: TPI
Btvdan and to the Office of formation
and Regulatory Affairs, Oltiee of
Management end Budoet Paperwork
Reduction
Project
(2070-0083).
Washington, O.C. 20603.
1.1 Are you claiming the chemical Identity on page 3 trade secret?
f1. [ ] Yes (Answer question t.2:
No (Do not answer 1.2;
Atfach substantiation forms.)
Go to Question 1.3.)
1.2 it Yes* in t.t. Is this copy: [ ] Sanitised [ ]unaanftized
1.3 Deportmo Year 19 88
2. CERTIFICATION (Read and sign after completing el sections.) 11 hereby ewtffy that have reviewed the attached document* end that, to the best of my knowledge end belief, the abdUsd information is true end
correlate and that the amounts and values in this report are aecurat* based on reasonable estimates using data available Id the preoarers of this report.
Name awl official Mile of owner/operator or senior management Official
^Don R. Unruh, Refinej^. Manager
Date sloped
/n
Facility or Establishment Name
Conoco Lake Charles Refinery
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
Stale
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
Gaudy
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Cede
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains information for (Chock ono): 3.2
.[*] An entire leeUity
K[ ] Part of a faculty.
Technical Contact 3.3
Brandt Butler
^jbfte Contact 3.4
Don R. Unruh
Telephone Number (include
^18-_44i-_5599_
Telephone Number (Include eree coda)
318-491-5222
SIC Code (4 <*gft)
3.S .2911
3.6
Degrees
030
b. na
Latitude Minutes
14
c.
Seconds
36
d.
Degrees
093
e. Longitude
Minutes
16
Seconds
20
Dun & Sredstreet Number(s)
3.7 . 00-842-7692
NA
EPA Identification Number'*) (RCRA t.O. No.)
3.6 .LAD990683716
NA
NPOES Permit Ntanber(s)
3.9 .LA0003026
HsoeMno Streams or Water Bodies (enter
Aayou Verdine
boa)
NA b. NA
3.10
d.
Undergrotnd ejection Well Code fUtC) tdemifieatlon Number(s)
3.11 NA
PARENT COMPANY INFORMATION Neme of Parent Company
4.1 E.I. DuPont de Nemours
Perenf Company's Oun 4 BrsdtVsM Number
4.2 00-131-5704
EPA Form 9350-1 (t-69) Revised--Do not use previous versions.
SAL 000005693
LJ
(Important: Type or print; read instructions before completing form.)
oA
rn.
trA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC
CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWa)
1.1 POTW name
___ ____ NA_____
Street Address
1.2 POTW name Slraet Address
City
County
City
Stele
Zip State
Pag# 2 of (This apace for your optional use.
County ZIP
2.1 Off-site location name
BFI
EPA identification Number (RCRA D. No. |
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Cowity
Calcasieu
State
Louisiana
Zip
70664
iis location under central o reporting taeMIty er parent company?
[ ]v
2.2 Off-site location name
NA
)EPA identification Number (RCRA O. No.
Street Address City
County
State
Zip
aIs location undar control I reporting lacdity or parent company?
I ]v,, [ U
2.3 Off-slt# location name
2.4 Off-glte location name
EPA MantMeatlen Number (RCRA C. No.)
EPA identification Number {RCRA O. No.)
Street Address
Slreel Address
City
County
City
Cow*y
State
Zip
State
Zip
Is location undar central o< reporting facility or parent company?
2.5 Off-site location name
t ]ves [ ] Mo
Is location wider control of reportInq facility or parent eempany?
2.6 Oft-site location name
[ ]v,,
[U
EPA Identification Nwnber (RCRA O. No.)
EPA Identification Number (RCRA O. No.)
Street Address
Street Address
City
Courtly
City
County
State
Zip State
ZIP
i location under control o< reportinQ ladttty or parent eorv^any?
[ ] ves
[ ] No
is location under control pf reporting facility <ir parent company?
[ ]v
[U
[ ] Check If addHtonal pages ef Part are etteetwd.
iMMt
EPA Form 9350-1(1-89) Revised--Do not use previous versions
000005b'**
(Important: Type or print; read instructions before completing form.)
-ft EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
u
Page 3 of S
(This space for your optional use.)
1. CHEMICAL IDENTITY | Do not complete tNe section H you complete Section 2.)
1.1 1.2 1.3 1.4
(Reserved! CAS Number (Enter the number exactly a* It appear* on the 313 net. Enter NA. H reporting a chemical category.>
67-56-1
Chemical or Chemical Category Name (Enter the name exactly a* it appear* wt the aid Hat.)
Methanol
Generic Chemical Name (Complete only Fart I, Section i.i la checfcea 'Yet.* Generic name mat be *tructuraity oeccriptive.)
MIXTURE COMPONENT IOENTTTY (Do not complete tNa eectlon If you complete Section 1.1 2. Generic Chemical Name Provided by Supplier (limit the name to a maximum of 70 character* (e.g., number*, letter*, space*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that OOtV.)
Manufacture the chemical:
3.1
ri
La. J Produce
If produce or Import:
f 1 For on-stte e.L J use/processlng
f
b. [ ] import
e.[ ] As a byproduct
f.[
7 For sale/ * attribution } As an Impurity
Proce** the 3.2 chemical:
c * l
d.[
s J Aa a reactant
] Repackaging only
r i a* a formulation
b lX J component
r 1 A an article c-t J component
Otherwise use 3.3 the chemical'
f * l
J1
As a chemical processing aid
Jb.l
1j A, *
a
_ manufacturing
aid
c.flyA lJ AncSary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR
(enter code)
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (toe/yr)
You may report releases of less than
1,000 be. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-490 500-999
A.2 Enter
Estimate
5.1 Fugitive or non-point air emissions 5.1a [][][]
1,500
B. Basis of
1
Estimate
(enter epde)
5.1b CsD
5.2 Stack or point air emissions
5.2a [ ] [ 1 [ ]
5.3 Discharges to receiving streams or water bodies
1* | 1 .1
5.3.1a [](][]
(Enter teller code irom Pert 1
Section 3.10 for *treem(*} In the box provided.)
[1
5,3.2 1___1 5.3.2a [][][]
5.3.3 0 5.3.3a [][][]
5.4 Underground Injection
5.4a [ ] [ ] ( ]
$.5.1 On-ite landfill 5-5.2 Land ireeiment/appiieelion (arming
5.51a [ 11 1 [ 1
5.5.2a [ ] [ ] [ ]
760 0
NA
NA NA
0
0*.
5.3.1b 0 5.3.2b 5.3.3b Q
C. * From Stormwater 5.3.1c NA.
5.3.2c NA
5.4b Q
5.5.1b
5.5.2b Q
6-5.3 Surface impoundment 5.5.4 Other disposal
5.5.3a [][][] 5.5.4a [][][]
NA NA
5.5.3b Q 5.5.4b 0
[ ] (Check if additional information is provided on Part fV-Sueolemental Information.)
EPA Form 9350-1 (1 -89) Revised--Oo not use previous versions.
SAL 000005695
(Important: Type or print; read instructions before completing form.)
*epa
,,,,,,
EPA FORmR
CHEMICAL-SPECIFIC INFORMATION
(continued)
Page4 of 5
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1.000 tot. toy checking ranges under A.1. (Do not use
both A.1 and A.2)
toOlacharo* POTW
, r--,
(enter location number {ill
1.) |$.1.1 from Pan 1. Section
1 1 H____
A. Total Transfers (*>s/yr)
A.1 Reporting Ranges
0 1-409 500 ass
A.2 Enter Estimate
[][][] NA
S. Basis of Estimate
(enter code)
(Z36,1.1b
Other off-fit* location .-------, ---- . , . (enter location number 1 9 1 )
| 2 |6-2.1 from Fan , Section 2.) | j
Other off-*ii iocaiion .
| 1 )_ _ _ | zJ l 16.2.2
a,(enter tocetion ntanber
from Fart Section 2.)
____
f ][ (It
1f 1(
] NA 1
CD6.2.1b
- 6.2.2b nn-
Other off-*He location
ran r i [ i [ i6.2.3
--- . J
1 I6.2.3b
[ ] (Chock If additional Information It prodded on Part IV-$uppiemental Information.)
C.type of Treatment/ Disposal
(enter coda)
M | |6.2.,6 | |.2:2c|m| | |6.2.3c |m|
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wastestraam
(enter code)
B. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter eede)
D. Sequential Treatment? (cheek If appieable)
E. Treatment Efficiency' ' Estimate
F. Based on Operating Data?
Yes
No
7.1a 7.1b IbIiTiI
7.1c
7.,d [ ]
7.1e
100% 7.,, : ] cx i
7.2a El 7.2b l.li t J
07.2c
7.26 [ ]
7.2e
100% 7.2f
]i tx
7.3a
7.3b
|n|a| |
7.3C
7.36 [ ]
7.3e
% 7.3, [iti
7.4a
7.4b
||| |
7.4c
7.46 [ ]
7.4#
% 7.4, [ i [ i
7.5a
7.5b
||(1
7.5c
7.S6 [ ]
7.6e
7.6a 7.6b 1 1 1 1
7.6C
7.66 [ ]
7.6#
7.7a 7-7b || | J
7.7C
7.76 [ ]
7.7#
7.8a 7.6b [J XI
7.6c
]7.66 [
7.6#
7.9a 7Sb 1 1 J. 1
7.9c
[ ]7.96
7.9#
7.10a
7.,0b | | J |
7.10c
]7.,06 [
7.10a
[ ] (Check if addWonal Information It provided on Part IV-Supplamantai Information.)
% * [ i [ i
% 7.6f
i[ i
% 7.7,
i( ]
% 7.8f
i[ ]
% 7.9f t i [ i
% 7.10f [ i [ i
a. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate action* taken to reduce tha amount of the chemical being released from the faedty. Sea the instructions for coded hams and an explanation of *hat information to include.)
A. Type of Modfflcation (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
M1
Current reporting year (tos/yr)
Prior year (tes/yr)
j Or percent i change {
1I %
(
r*n
fcPA Form 9350-1(1-39) Revised - Do not use orevtous versions
SAL 000005696
(Important: Type or print: reed instructions before completing form.)
& EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section if you need additional space for answers to questions in Part til. Number the Hoes used sequential? from Ines in prior sections (e.q.. 5.3.4. 6.1.2. 7.11)
Page 5 of 5 (TWs space lor your optional use. )
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part Ml, Section 5.3)
You may report releases of less than 1.000 bs. by cheering ranges under A. 1.
(Do not use both A.1 and A.2)
A. Total Release (bs/yr)
A.1
Reporlino Ranges 0 i-s soc-ess
A.2 Enter Esttnate
5.3 Discharges to
.
receiving streams or waterbodies
I 5.3--------1--1
5.3_____a [][][]
B. Basis of Estimate
(enter coda In box ;
provided1
C.% From Stormwater 5.3______tO
5.3----------c
(Enter teller cede from Pert
j1
Section 3. to or ttrn(t| in c 3
J___1
the bon provided.)
a **----------1------
5.3_____a
[][][]
5.3_____ 5.3____a [][][]
5.3.___' bl~] S.3._____c
S-3-_____bD 5.3._____ c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1.000 lbs. by cheering ranges under A. 1. (Do not use
both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-460 500 SOS
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
_ 6.1.
Diectierga to POTW (enter knltan rwmbtr
. I
,
1, 1
tram Pet C. Section 1.11 1 |.|
1 1
[111(1
6.1._____b O
Other etf-ehe location p - . -*--- srwsit-ssiss.i 0Q [
11
It
1
6.2._____b 1 1
.*.<= M 1 |
Othereff-efle location f"" 1 |* 1
6.2. --------
fr(oemntePr elortoSe.tloSnecntuiomnb2e.r1
( Z1I I LZJI----I
[][][]
f 9 (enter toeetlon mettoer 1 1 1 1 [][][] *z---------tram Pert I. Section J.l 1 *1.1___J
6.2._____b HU 6.2._____b O
.*. e|M| | | 6.2. e|M| 1 |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part ill. Section 7)
A. General
Wasteetream (enter code
In box provided)
B. Treatment Method
(enter code
In box provided)
C. Range of Influent
Concentration (enter code)
D. Sequent!* Treatment? (check If appicabie)
E. Treatment Efficiency Estimate
F. Based on Operating
Qata? Yes
No
7.
a 7._---------b
I11
7.
c
7._--4 1
7.______e
% 7.
4H]
7._______a 7.
111 b
7.
c
7.__--4 1
7.
e
% 7. - 4 11 3
7.
a 7.
111 b
7.
c
7.
df 1
7.
e
% 7.
*[ H 1
7._______a 7.
b
7._______a 7._---------b
111 111
7._______c 7._______c
7. 4 1 7.__--4 1
7. e 7._ e
% 7._--4 It 1
% 7.
4H3
7.
a 7.
111 b
7._______c 7.__4 1
7.
e
% 7.
4 ][ 3
7.
a 7.
111 b
7._______c
7._--4
]
7.
e
% 7.
4 ][ 3
a 7.
11 1 b
7.
a 7.
_L1J *>
7. c 7._______c
7._--4 7._--4
1 ]
7. 7.
e e
% 7._--' ( J[ 3
% 7.
4 ][ 3
EPA Form 9350-1 (t-69) Revised--Do not use previous versions.
SAL 000005697
(Important: Typg or print? read instructions before completing form.)
Form Approved OM6 NO.:
Approval Expires
2070-0093
01/91
Page t o< 5
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Wght-to-Know Act of 1986.
aJso known a* Title III of the Stoerfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public reckoning burden tor mis
wiieclioii oil tatoiMiion ntmittd to
ry tram 3# to 34 hour* per response,
with an average of s how* per
raipuia*. tararfnq time tor ravtavdcu
Irwnjotiana. searching eclating data
sources. gathering andmalrtiafeung the
data nmeaeddeidd,. ai nd eomptatino and
sSEs?collection of Morvnation.
flOnVIfHEe. regarding tMa tartan
estimate or any other aipani ef thia eolleetton of Information. Including
Mneactiorta iter reduclnqthls tartan, to
wet, niermatlon PoHcy Brareh
(PM-223), US EPA. 401 M St.. SW.
Washington, D.C. 20460 Attn: TRl
Burden and to tha Offlea of Mermatian
and Regulatory Affair*, Offlea ef
Management and Budget Paperwork
Reduction Washing*
Project
(2070-00031.
D.C. 20603.
1.1
Are you claiming the chemical Identity on page 3 trade secret?
1 1 Yea (Anawer question 1.2;
I ^ J No (Do not answer i.2;
Attach substantiation forms.}
Go to oueation t.3.1
t .2 tt 'Yes* In 1.1. la this copy:
j
1j
1.3 rieporUng Year 19 88
2. CERTIFICATION (Reed end sign efter completing el sections.) I hereby certify that I have isrlewed the attached doownem* and that, to ihe beat of my Knowledge and belief, tha aubmNted information la true and complete and that tha amounts and value* in this report are aocwaia based on reasonable estimates using data available to tihhaa preparer* of thi* report.
Name and official title of earner/operator or senior management ottleial
Don R. Unruh, Refinery. Manager
Signature
Date signed
--FACILITY IDENTIRCATION Fatality or Establishment Name
Conoco Lake Charles Refinery
WHERETO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
state
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
Cowtty
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Cede
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
Thf* report oentaint Information for (Check one): 3.2
P.[X ] An entire facility
b. [ 1 Part of a fadUty.
3.3 Technical ContwS Brandt Butler
3.4 RPMe Contact Don R. Unruh
STC Coda (4 taglt)
3.5 .2911
b. na
Latitude
3.6
Minutes
030
14
Dun t BrMtUwt Mwnper(s)
3.7 .. 00-842-7692
EPA Identltteation Nunber(s) (RCRA I.O. No. |
3.6 4LAD990683716
c.
Gscondt
36
d.
Degrees
093 NA NA
Telaphona Number (k elude area codal
*18-491-5599
Talaphona Nwrber (inctuda area coda)
318-491-5222
a.
Longitude Mmutet
16
f.
Second* 20
M3OES Permit Number(e)
3.9 4LA0003026
Receiving Streams or Water Sodiaa (enter ana name per boa)
.Bayou Verdine
NA b. NA
3.10
Uhdargrowxj ta|eetton Weil Code <WC) idantfficatien Nurtwtt) 3.11 aNA
4, PARENT COMPANY INFORMATION Name ef Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Dw> A Bradatreei hkenber 4.2
00-131-5704
EPA Form 9350-1 (1-69| Revised--Do not use previous versions.
SAL 000005698
(Important: Type or print; read instructions before completing form.)
oA EPAf-nA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWa)
1.1 POTW nama NA
Straw! AMtu
1.2 POTW name
Street Address
city
County
City
State
Zip State
(This spaCc for your optional use.)
County 2ip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHCN WASTES APE SENT OM.V FOP RECVCUNO Oft REUSE).
2.1 Off-site location name
BFI EPA Identification Number (RCAA O. No. )
HA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
la location under control of reporting (acuity or parent company?
2.2 Off-site location name
NA
EPA Identification Nienber (RCRA O. No.)
Street Address City
County
State
Zip
is location under control of reportlnQ UdUty or parent company?
I [ Jvoa [xl***
[ hm [ U
s.,4 Off-site location name EPA fdantifteatton Number (ftCRA D. No.)
2.4 Off-alte (ocation name EPA identification NwrSaer (RCRA D. No.)
Street Address City
Coioty
Street Address City
County
State
Zip State
Zip
to location wder control Of reporting facility or parent company?
2.6 Off-site location name
[ ]~ [ u
Is toeation under control of reporting facility or parent company?
2.6 Ofl-site location name
[ ]v,,
[u
EPA demllicatlcn Number fftCRA O- N. 1
EPA Identification Nunbw (RCRA C. No.)
Street Address City
County
Street Address City
County
State
Zip State
ZIP
ocation under control of reporting facility or parent company?
!
[ ]v~
[u
to location under control of reporting ledWty or parent company?
[ ]v-
[U
[ ] Chick H addnbntl pqi at Part a are ittaeM. How many?
EPA Form 93S0-1 |t-89) Revised --Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART lit. CHEMICAL-SPECIFIC INFORMATION
Pag* 3 of 5 {TN* space for your optional us*.)
1. CHEMICAL IOENTTTYIDo not complete this action ff you compiata Section 2.)
1.1 1.2 1.3 1.4
[Reserved] CAS Number (Enter the number exactly as K *ppears on tn* 313 list. Enter NA H reporting a chemical category.) 1634-04-4 Chemleai or Chemical Category Name (Enter the name exactly as tt appaare on the 3t3 o*t.) Methyl tert-butyl ether Genetic Chemical Name (Complete onty H Part 1. flection 1.1 is checked "Yes. * Generic name must be structurally descriptive. >
MIXTURE COMPONENT IDENTITY (Do not oomolete this section If vou oomolete Section 1.1 2. Generic Chemical Name Provided by Supplier (Umlt the name to e maximum ef 70 characters (e.g., ntenpart. tatters, spaces. punctueiion).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Cheek al that aooN.I
Manufacture the
If produce or import:
chemical: 3.1
ri
a.l J Produce
f 1 For on-site c.l J uee/proeessing
f
b. [ ] Import
*.[ ] As a byproduct
f.[
1 For sale/ J distribution
] As an Impurity
Process the 3.2 chemical:
f d.[
1^ J A* a reactant
] Repackaging orty
. [ XI As s fomrndatton b.|. "component
f 1 At an article
c* J component
Otherwise use 3.3 the chemical*
f 1 As a chemical *'* -J processing aid
J ].
. ___,
b.l J As a manufacturing aid
f1 c.L J AncJHary or other use
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than 1.000 bs. by checking ranges under A.l.
(Do not use both A.l and A.2)
A.l neportkig Ranges
o t-499 soo-em
A.2 Enter Estimate
S.1 Fugitive or non-point air amissions
5.1s [][][]
1,100
S.2 Stack or point air emissions
5.2a [][][]
8,700
S.3 Discharges to receiving
1a 1
streams or water bodies &*3-` i 1
(Enter letter cede from Pert l
Section 3.10 for ctream(t) lr me box provided.)
11 5.3.2 1 1
5.3.3 n
5.3.1a [](][]
5.3.2a [][][] [5.3.3a 1 [ ] ( 1
2 NA
5.4 Underground Injection
5.4a [][][]
NA
5.5.1 On-fit* landfill 5.5.2 Land treaiment/eppiicetfon farming
5.5.3 Stelae* impoundment
5.5.la [][][]
[5.5.2a 1 [ I [ 1 S.5.3a [][][]
NA NA NA
5.5.4 Other disposal
S.$.4a [][][]
NA
[ ] (Check If addioonai information is provided on Part rv-Suppl*mental Information. >
B. Basis of ! 1 Estimate (enter coden
5.1b Col
5.2b G>)
5.3.1b 0
EH5.3.2b EH5.3.3b EH5.4b EH5.5.1b EH5.5.2b EH5.5.3b
5.5.4b O
EPA Form 9350-1 i 1-89) Revised --Do not use previous versions.
SAL 000005700
(Important: Type or print; read instructions before completing form.) .
O EPA
pA formR
FART III. CHEMICAL-SPECIFIC INFORMATION (continued)
Pag* 4 of S (ThEt space for your optional use.)
. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers
.of lee* inan 1.000 b*. toy checMng
ranges under A.1 (Oo not use
both A.1 and A.2)
__Otaetwpe to POTW 1lantv toeriton nunew 1, | j.| |6.1.1 from Pert Section 1.)
-IT 1 ____
,Other off-slte location .____ ... f 1(enter location number l. | |.|6.2.1 from Pan Sections.) 2
1|-
_Other off-eite location i 1 1... (enter location number 1, 2.) 1 _2 _l6.2.2 from Part Section
____. |*L
A. Total Tranifera (bs/yr
A.1 Raportlng Range*
o i*4oe soo-eos
A.2 Enter
Estimate
[][][] NA
[][][] NA
[ 1 f 1 f-I
B. Basis of Estimate
(enter code)
6.1.1b CD6.2.1b 6.2.2b
Other off-eile location
-- ,J
s.2.3 izzrr`s-:!%sz.l FlO f
1f
1f
1
6.2.3b
C.Type of Treatment/ Disposal
^_^(*mereode^^^^_
IMI.2.lc 1 I 1 16.2.2c |M| | |6.2.3c |M|
[ ] (Cheek If addKIonal Information la provided on Part IV-Suppiamental Information.)
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
D. Sequential Treatment? (cheek If applcable)
. Treatment Efficiency Estimate
F. Based on
Operating''
Oata?
Yee
No
7.1a 7.2a 7.3a 7.4a
7.1b ca 7.2b 7.3b
|b|i 111 Ulo M
In| a| |
till
7.1c 07.2c 7.3c 7.4e
7.,d [ ] 7.2- [ ] 7.3- [ ] 7.4- [ ]
7.1* 7.2e 7.3e 7.4e
95 % /.if 98 % 7.2f
% 7.3f % 7.4f
( 1 fx 1 [ 1 lx ] ( 1( 1 [ 1[ ]
7.S* 7Sb l I.J 1 7.6a 76b 1 Jj.l
7.5c 7.6c
7.6- [ ] 7.6- [ ]
7.5e 7.6e
7.7a 7-7 1 1 1 1
7.7c
7.7- [ ]
7.7e
7.6a 7-8b L1._LJ
7.6c
7.6- [ ]
7.6*
7.9a 7-3b till
7.9c
7.9- [ ]
7.9*
7.10a 7.,0b | | | |
7.10c
[7.10- ]
7.10*
[ ] (Chock If addKional Information Is provided on Part (V-StaapiementaJ Information.)
% 7.5f [ 1 [ ]
% 7-6f [ 1 [ ]
% 7.7f
% 7.8f
[ 1[ 1 [ ]( 1
'% 7.9f l 1 t ]
% 7.10f [ 1 [ ]
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(tndteat* actions taken to reduce the amount of the chemical being released from the facBty. See the instructions for coded Items and an explanation of what Information to include.1
A. Type of Modtftcatton
(enter code)
B. Quantity of the Chemical m Wastes Prior to Treatment or Disposal
C. Indax
0. Reason for Action (enter code)
(mQ
Current reporting
year (bs/yr)
Prior year
(bs/yr)
, Or percent | change ,
l 1* i
EPA Form 9350-1(1-89' Revised - Oo not use previous versions.
m
SAL 000005701
(,important: Type or print; read instructions before completing form.)
6 EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section tf you need addttlonal space for answers to questions m Part til. Number the Snes used sequemtaly from tries in prior sections |.g.. 5.3.4. .1.2. 7.11)
Page 5 of 5
additional information on releases of the chemical to the environment ONtSITE (Part III, Section S.3)
You may report releases of less than 1,000 *>s. by checking ranges under A. 1.
(Do not use both A.1 end A.2)
A. ToUi Release (bs/yr)
A.1 Reporting Ranges
0 MW 500-099
A.2
Enter Estlmats
5.3 Discharges to
.
receiving streams or
)I
(][][]
water bodies
5.3.--.1--1 5.3-------a
B. Basis Of Estimate
(enter code in box
provided)
5.3______bO
C.% From Stormwater 5.3_______c
(Enter letter ccoe from Pert I
11
Section 3.10 lor tirm(t) met ' 1 __1
the boe prchCed.t
--------" *
5.3_____a
[][][]
S3_____ 5.3-------a [][][]
5.3._____bT~1 5.3._____c
S.3._____JI
5-3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III, Section 6)
You may report transfers of less than 1,000 fes. by checking ranges under A. 1. (Do not use
both A.1 and A.2)
A.Total Transfers |t>s/yr)
A.1 Reporting Ranges
o mm soa seel
A.2
Enter
Estlmati
8. Basis of Estlmats
(snter code In box
provided)
C. Type of Treatment/ Disposal
(enter code in box
provided)
OIdM9* to POTW
- . ,-------,
..
(enter location number I .11
6.1.______Wn Part a. Section 1.) | 1 |.|
I I
[][][]
1.1._____b
6.2.
Other fT-**te location (enter location nufSe . from Pan a. Section 2
[][][]
6.2.______
Other ott-ette location (enter location numbeir
,(H.D
--------from Pert B. Seel Ion 2.
[][][]
6.2.
iOther oil-elte location
(enter location nurrber | | | | from Pert , Seakn 2.) 1*1.1 I
n
it
i
6.2. 6.2. 6.2
II
62.,
6.2..
A. General Wastestreem
(enter code In box provided)
7--
B. Treatment Method
(enter code In box provided)
-nil
7--* 7---* U-U
, - -cro
7. . Q 7- * au
i.M. I
7- b U...J.I
7. .Q 7- "fill
7. .Q 7- - Q. 1J
7. .D 7. J> 1 1 1 1
hi
o
C.Renge of Influent Concentration tenter code)
O. Sequential
Treatment? (cheek If appieatolel
7. c Q 7. d[ ]
7. c Q 7--c
7`-------- -[ 7--------- -I
] ]
7--' 7---------[ ]
7_______e 7`--------[ 1
7--c 7--------- [ 1
E. Treatment Efficiency Estimate
F. Based on Operating
Oata? Yes
No
7.______ e
% 7--'[ It ]
7.______ e
% 7_______[ ][ 1
7.______e
% 7-_____ *[ )[ ]
7.______ e
%7
>[ 11 1
7._______e v
%7
[ 111
7.______e
* 7---*[ H 1
7. d[ J
7--- 7--------- -[ 1 7- <= 7. d[ ]
7.______e 7.______e 7. e
% 7-______[ 11 1 % 7-_______'[ 11 1 * 7-------- ?l 11 1
m
hi
EPA Form 9350-1 (1-69) Reused--Do not use previous versions.
SAL 000005702
(Important: Type or print: read instructions before computing form.)
Form Approved OMB NO.: 2070-0093
Approval Expires:. 01/91
Page i of S
o'EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1936,
_____also known as Title HI of the Superfund Amendments and Roauthortzation Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION INFORMATION
(TNs space for your optional use.}
PwOHc reporting ttrotn tor this
ooiMeUanioi Mgnration is estimated to
very from 30 to 34 hours perrespo with an twreoe of 32 hours
itochriing time for revtoxing
searolitou extolIng tijti
ring ana matotetomo the
i oomclallnQ and
.. - . .Sion of tntarmation.
Send wtoiwMs regardtog mto tartan
estimate or any other aepeet ef this oeltoetlan of information. Intodim
(UNHUm for raductaqthts burden, to Wei, Information Policy Brerch
(PM-223), US EPA. 401 M $t.. SW, Washington. O.C. 20460 Attn: TRI
Button and to the Office of Information
and Regulatory Affairs, Office of
Manaw*'toil and Budget Paperwork
Reduction Project
(2070-0093).
Washington. O.C, 20603.
1.1 Are you Claiming the chemical Identity on page 3 trade secret?
1.
[ 1 Yes (Answer question 1.2;
[ ^ ] No (Do not answer 1.2;
Attach substantiation forms.)
Co to Question t.3.1
1.2 ff *Yes* to t.t. Is this copy: [ ] Sanitised[ ]uneenK4aad
1.3 naporttog Veer 19 88
2. CERTIFICATION (Read and sign after completing al sections.) I hereby certify that I have reviewed the attached documents and that, te the best el my knowledge and belief, the submitted information is true and comptote and that the amounts and values to this report ere aeaaate based on roasonabto estimates using data available te the preparers ef this report.
Name and official title ef owner/operator or senior management official
Don R. Unruh, Ref inp^ry. Manager
Signature
; Oate signed
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 Ctty
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
2lp Cede
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
TMs report contains Information ter (Chech one): 3.2
.[x] An entire facility
>. [ 1 Pan of a tacuity.
Technical Contact 3.3
Brandt Butler
PitoUe Contact 3.4
Don R. Unruh
OC Coda <4 d&t)
3.S .2911
b. na
3.6
030
Latitude Minutes
14
Dun 6 Bradstreat Number(s)
3.7 . 00-842-7692
c.
Seconds
36
Telephone Mntor (tndyda area eeda)
318-491-5599
Tslsphgna Number (toctjids am* eoda)
318-491-5222
d.
Degress
093
NA
Longitude Minutes
16
t.
Seconds 20
EPA identification Nwnbar(s) (RCRA l.O. No.)
3.6 ..LAD990683716
______
NA
NPOES Permit Number (s)
3.9 .LA0003026
Receiving Streams or Water Bodies (enter one name per box)
.Bayou Verdine
NA b. NA
3.10
d.
Underground ejection Welt Cede (UC) Identification Nuntoer(s) 3.11 aNA
PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Out 4 Bredstreet Number
4.2 00-131-5704
EPA Form 93S0-1 (1-fl9| Revised--Do not use previous versions
SAL 000005703
LJ (Important: Type or print; read instructions before computing form.)p<0< 2 of s
-
0
EPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC
CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Address
City
County
City
Stete
Zip State
(This space for your optional use.)
County Zip
2. OTHER OFF-SITE LOCATIONS (OO NOT REPORT LOCATIONS TO WVSCM WASTES are sent only for RECYQLMG OR REUSE).
2.1 Off-site location name
BFI
EPA Ueitiiieitien Number (RCRA D. No.)
NA
Street Address
Cities Service Rvy at 1-10
City
Sulfur
Cautty
Calcasieu
State
Louisiana
zip
70664
ts tocalion under control of reporting facility or parent company?
1 [ ]v- [x]-
2.2 Off-site location name
NA
EPA IdentHieatian Number <RCAA . No.)
Street Address
City
County
State
Zip
Is location under control of reporting facility or parent company?
[ ]v~
[U
2.3 Off-site location name
2.4 Off-alte location name
EPA tdentifleatlon Number (RCRA D. No.)
EPA identification Nun bar (RCRA O. No.)
Street Address City
Oounfy
Street Address CHy
County
State
Zip Slate
Zip
is location under oentroi of reporting facility or parent company?
2.5 Off-site location name
[ ]v [ ].
it location under control of reporting facility or parent company?
2.6 Off-site location name
[ ]v,,
[U
EPA identification Number (RCRA D. No.)
EPA IdentHieatian Nunber (RCRA O. No.)
Street Address
Street Address
City
County
City
County
State
Zip Stale
Zip
location under oentroi of reporting faotfty or parent company?
[ ]v [ U
is location under control of reporting taefiity or parent company?
] Cheek if additional pages of Part ere attached. How many?
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
... ** trH
REPA FORM
pARj hi. CHEMICAL-SPECIFIC INFORMATION
u
Psq* 3 of S
{This space for your optional use.)
1. CHEMICAL IOENT(TY(Do not complete this section If you complete Section 2.)
1.1 (Reserved]
1.2
)CAS Number (Enter the number exactly a* It aooears on the 3l3 list. Enter na if reporting a chemical category. 1313-27-5
Chemical or Chemical Category Name (Enter tne name exactly as u appears an uw 313 n*t.) 1.3 ftolvbdeniun Trloxlde
!
Generic Chemical Name (Complate only if Part 1, Section 1.1 Is chair*ad "Yes, * )Oanerte name must be structurally descriptive.
1.4
MIXTURE COMPONENT IDENTITY IDo not complete this section If you convict* Section 1.) 2. 70 )Oanerte Chemical Name Pruvided by Supplier (Limit the name to a maximum of characters (e.g., numbers, tatters, spaces, punctuation).
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aootv.)
Manufacture the chemical:
3.1
ri
a.l J Produce
If produce or Import:
f 1 For on-site c.l i use/proceesing
T c.l
1 For sale/ i distribution
b. [ ] Import
e.[ ] As a byproduct
f.[ ] As an Impurity
3.2 :=r
[ ]*..
d. [ ] Repackaging only
b.[ issues"1"
c.[ isj^sss1*
3.3
Otherwise use the chemical-
f,, lAs a chemical a.lX Jproeesskig eld
kf 1,
. _____
b.l J As a manufacturing eld
fl. c.l J ApeBary or other us*
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR BE (enter cod*)
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (tos/yr)
You may report releases of less than 1.000 be. by checking ranges under A.l. (Do not use both A.l and A.2)
A.l Reporting Ranges
o i-4S soo-egg
A.2
Enter Estimate
5.1 Fugitive or non-point eir emissions
5.1a [
1[ 1[
1
120
S.2 Stack or point air emissions
5.2a [][][]
5.3 Discharges to receiving ,
jJ
streams or water bodies &-3- '--l
(Enter Miter code from Part 1 Section 3.10 tor siream<s) In
the box provided.J
Fj
5.3.2 1_____1
5-3.3
5.3.1a [][][] 5.3.2a [][][] 5.3.3a [ 1 [ 1 [ 1
NA NA
5.4 Underground injection
5.4a [][][) NA
5.5.1 On-site landfill 5.5.2 Land treatment/aoplieatlon (arming
]5.5.1a [ 1 t 1 [
S.5.2a [](][]
NA NA
5.5.3 Surface Impoundment
5.5.3a [][][]
NA
5-5.4 Other disposal
5.5.4a [HU!
NA
B. Basis of Estimate (enter codejl
S.lb 0 5.2b Q 5.3.1b Q 5.3.2b O 5.3.3b Q 5.4b 0 5.5.1b Q 5.5.2b 0 5.5.3b QJ 5.5.4b Q
[ 1 (Check w
Information > provided on Part IV-Supplemental tntormatvon.)
EPA Porm 9350-1(1-891 Revised -- Do not use previous versions
000005705 SAL
(Important: Type or print; read instructions before completing form.)
o EPA
EPA FORM^
PART III. CHEMICAL-SPECIFIC INFORMATION
Continued)
Pag* 4 of 5
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfer* of lets than 1.000 toe. by checking range* under A. 1. (Do not use both A.1 and A.2)
A. Total Transfers (fes/yr)
A.1 Reporting Ranges
o i-4ss soo see
A.2 Enter
Estimate
B. Basis of Estimate (enter code)
Discharge to POTW
, ----i _
(enter location number I .\ I
f
6.1.1 tram Part CactIon 1. | I * I
Il
]t
1[
] HA
6.1.1b o
Other oft-eit* location .. . .
6.;.i
,[[] [
Other e<t-*He location -- .. . j
LXIlj [
Other aff-elt# location r--~
^
6.2.3<t^1^.,B[j[
1[
1[
1[
1[
}f
1[
1 21,000
1 NA
1
6.2.1b
i.2.2b tu
I"!i.2.3b
[ ] (Check ff addMonal Information is provided on Part IV SipplwieniS Information.)
C.Type of Treatment/ Disposal
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Rang* of Influent
Concentration (enter code)
D. Sequential Treatment?
(check if appfeabte)
E. Treatment Efficiency Estimate
7.1i 7.2a 7.2a -.4.
7.1b 7.2b 7.3b
7.4b
Ta
7.1c 7.2o 7.3c 7.4c
7.Id 7.2d 7.3d 7.4d
[] [J [1
[]
7.1e 7.2* 7.3* 7.4*
7.5a 7.6a 7.7a 7.6a 7.9a
7.Sb 7.6b 7.7b 7.6b 7.9b
7.60 7.6c 7.7c 7.8c 7.6c
7.5d [ 1
7.6d [ 1 7.7d I ] ?.6d [ 1
7.9d [ 1
7.6* 7.6* 7.7* 7.8* 7.9*
7.10a
7.10b
7.10C
[7.10d ]
7.10*
[ ] (Chock if addMonal Wormation Is provided on Part fV-Suppiem*ntal Information.
F. Based on ' Operating
Data? Yes
No
7.If [ 1 [ ]
7.2f [ ] t ]
7.3f 7.4f
[ 1[ ]
(Ml
7.5f (111
7.6f I ] [ ]
MM7.7f 7.8f { ] [ ]
7.9f [ ] [ ]
7.10f [ ] ( ]
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actions taken to reduce the amoiait of the chemical being released from the facSty. See the Instructions for coded
hems and an explanation of what Information to Include.)
__________
A. Type of Modification (enter code|
B. Quantity of the Chemical In Waste* Prior to Treatment or Disposal
C. index
D. Reason for Action (enter code)
Current reporting year (Ibs/yr)
Prior year (Ibs/yr)
Or percent change
M
EPA Form 9350-1(1-89) Revised - Do not use previous versions
SAL 000005706
(important: Type or print; read instructions before completing form.)
A rna ^
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section if you need addttlonal space for answers to question* In Pert III. Number the fines used eequendety from fines In prior Motion* (e.g.. S.3.4. 6.1.2. 7.11)
Pa?* 5 of 5 (This space for your optional use.)
'
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE <Part III. Section 5.3)
You may report releases of less than 1.000 fes. by checking range* under A.1.
(Do not use both A.1 and A.2)
5.3 Duiisschiiari^gvess tov
receiving streams or water bodies
|| II 5.3.^--L--J 5.3..
A. Total Release (bs/yr)
A.1 naportkig Ranges
O MW _ SOO-S99
A.2 Enter
Estimate
[][][]
8. Basis of Estimate
(enter code
In box _ provided
5.3.
n C.% From Stormwater 5.3_______c
(m Wte cede irem Pert l
II
Seciton 3.10 lor stream(s) in c
II
the boa promded.)
3.J.--.1--J
5.3..
[][][]
_a 5.3.
5.3______ 5.3..
(](][]
5.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part III. Section 6)
________
_____
You may report transfers of less than 1.000 fes. by checking ranges under A.1. (Do not use
both A.i and A.2)
A.Total Transfers (bs/yr)
A.1 neportktg Ranges
o i-ese soo see
A.2 Enter Estimate
6. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
Otecfuro* to FOTW
__ --
.,
(enter leeatian rmmt 1 . I 1 1
6.1.______font Pert . Section t.| 1 ' I I 1
(][][]
_ D'
>
I^KV"aS5SiiOther oft1 site leeatlon p-- --
-2_____
LUO
Other oW-she location r--j r-- i
6.2.
(enter leeaUen nartw 1 X j I I
----------from Pert 1 Section X. 11 I'L--J
[ 1[ 1 [ 1
[][](]
_ n.2.
t>
6.2.______b O
c|M| 1 1 S.2. e|M| | |
Other efPOMe IbciSw 6 2-______
[][][]
fi.2.______b CD
6.2. c|Mj | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Fart III, Section 71
A. General
Wastestream (enter code In box provided?
8. Treatment
Method (enter code In box preddad)
C. Range of Influent Concentration (enter code)
0. Sequential Treatment? (check IT
appteabie)
E. Treatment Efflefamcy Estimate
F. Based on Operating
Data?
Ye*
No
n
7.
7.
l1
--[ 1
[H1
lH1
7. 7. .-[ 1
[H1
--<
1
(H1
7. 7. -I 1
[U1
7. .-[ 1
[ H]
r---c D 7. [ ]
7. ( H ]
7. ]
[ ][ 1
(]
[H1
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
SAL 000005707
Form Approved OMB No.: 2070-0093 Approval F01/^1
u-s- Envlroomdnui Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1966. also known as Title HI of the Superfund Amendment* and Reeuthodzatkxi Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION INFORMATION
(This apace for your optional use.)
Ptbiie reporting burden tor this collection at bdormetlon Is estimated to very Siam to 34 hours par response, with an average of 32 hours per raaporaia. Mcfudvig 11ms ter reviewing
Instruction., sowchira existing data aouroaa. gathartng and maintaining the date needed, and eomoielino and
Send eontmtanu reoereHna this burden
eatknete or any other aapeet ol this
collection ot Wvmation. including
suggestions ler reducing this btvdan. to
ChfSt,___Information Policy Branch
(PM-2Z3), US EPA. 401 M St., SW.
Washington. D.C. 20460 Attn: TRi
Burden end to the Office of Mermatlon
end fleguletory Affairs. Oltioa ot
Menegenwnt and Budget Paperwork
Deduction Prefect
(2070-0093),
Washington. O.C. 20603.
1. 1 Are you daMng the chtmleal Wantlly on page 3 UMt eacret?
1.
1 i Vh (Answer question 1.2;
[ ^ J No (Oo not .newer 1.2:
Attach substantiation form*.)
* Go toquesHon 1.3.)
V.2
tr -Yea* in 1.1. la thisoopy: [ j Sanitised [ ] UnmHItM
1.3 Deportbiq Year 19 88
2. CERTIFICATION (Read and sign after completing al sections.)
t hereby evilly that I have reviewed the attached documents end that, to the beat of my knowledge and belief, the submitted information ia true and complete and that the amoien* end vetuee m this report ere accurate baaed on reasonable eattmatea usine date evelleble IP the preparers of tins report.
Nan and official title of owner/operator or senior management oMicial
Don R. Unruh, Refinery. Manager
Signature
Date signed
<Z/z-?/g7
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
We sclake
State
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report oomakne information for (Cheek one): 3.2
..[x] An entire laduty
>. [ 1 Perl of e faculty.
Tsctheal Qontaet 3.3
Brandc Butler
Public Contact 3.4
Don R. Unruh
SIC Coda (4 (Pott)
3.$ .2911
b. na
e.
3.6
Degrees
030
Latitude Minutes
14
Seconds
36
Dun A Bredatreet Number(s)
3.7 . 00-842-7692
CPA identification Number(s) (RCRA t.O. No.)
3.6 ..LAD990683716
NPOCS Permit NunOerls)
3.9 4 LA0003026
nscetvlnq Streams or Water Bodies lenter one nan* per boa)
..Bayou Verdine
d.
093 NA NA NA b. NA
Telephone Number (tockxJe
318-491-3399
Telephone Number (tnetudo
318-491-5222
e.
Longitude Minutes
16
Seconds
20
3.10
Underground VVection Well Code (UC) Identification Number(s)
3.11 eNA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Dun A Bredatreet Number
4.2 00-131-5704
EPA Form 93S0-1 (1-89) Revised--Oo rvot u* previous version*.
f.AL 000005 70B
(Important: Type or print; read instructions before completing form.)
-o-EPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Addreet
City State
County Zip
City
suta
County tip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO VWeCH WASTES ARE SENT OMV FOR R6CYCUNQ OR REUSE}.
2.1 Of (-site location name
BFI
EPA Ueniifiealien Number (RCRA O. Ns.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
Stet#
Louisiana
Zip
. 70664
t It location under control at reporting facility or parent company?
2.2 Off-site location nama
NA
EPA WeniMiealion Number (RCRA O. No. |
Street Addrete City
County
State
Zip
it location wider control of reperUng faculty or parent company?
[ Jve. lx]1**
[U
(U
... Off-slte location name
2.4 Off-slte location name
EPA tdentifteatian Number (RCRA D. No.)
EPA identification Number (RCRA D. No.)
Street Addreee
Street AddHi
City
County
City
Canty
State
Zip State
Zip
a location under central of reporting facility or parent company?
2.6 Off-site location name
[ ]v [ U
Is location under control of reporting facility or parent oompany?
2.6 Off-tite location nama
[ ]v,, [
EPA tdOTtlticatttn Number (RCAA C. No.)
EPA Identification Number (RCRA D. No.)
Street Mlreee
Street depress
City
County
City
County
State
Zip Stale
Zip
acation under control of reporting facility or parent eerreany?
[ ] Ve.
[ ] No
is location wider central el reporting leditly or parent company?
[ ] Yea
[ ] No
[ 1 Cbcrtc If addMienai paoee at Part are attached. How many?
EPA Form 93S0-1(1-69) Revised--Do not use previous versions
SAL 000005709
(Important: Type or print; read instructions before completing form.)
-&EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (This space for your optional use.)
1. CHEMICAL IDENTTTY(Do not complete thi section If you complete Section 2.)
1.1 1.2 1.3 1.4
(Reserved) CAS Number (Enter the ixmber exactly as ft appears an the 913 Mst. Enter NA II reporting a chemical category.)
91-20-3
Chemical or Chemical Category Name (Enter the name exactly at it appear* on the 313 list.)
Naphthalene
Genetic Chemical Name (Complete onty If Pan l. Section l.l H checked *Yea.` dearie name muet he structurally descriptive.)
MIXTURE COMPONENT IDENTITY (Do not comoiete this section If you complete Section 1.1 2. Generic Chsmleal Name Provided by Supplier (Limit the name to a maximum of 70 tharaetm (e.g., numbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY 1 Check afl that apply.)
Manufacture the
If produce or Import:
chemical: 3.1
ri a. L j Produce
r 1 For on-sits c.l J uae/processlng
_f 4.L
b. [ ] Import
#.[ ] As a byproduet
f.[
1 For sale/ J (Attribution
] As an Impurity
Process the 3.2 chemical:
r ,4 l* A* a reactant
d.[ ] Repackaging onfy
r b.[
i1 As formulation component
f 1 As an article J component
Otherwise use 3.3 .....
me chemical:
T 1 As a chemical a. 1 J procetstog aid
b.lJ 1
_
J As a manufacturing aid
fv 1 e.LA J AneEary or other use
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than 1,000 bs. by checking ranges under A. 1.
(Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-499 500-099
A.2
Enter Estimate
5.1 Fugitive or non-point air emissions
[][][]
5.1a
7,200
5.2 Stack or point air emissions
5.2a [][][]
5.3 Discharges to receiving _ streams or water bodies
[)[][]I a]
'--& 5.3.la
(Enter latter cede from Part l Section 3.10 lor stream(s) in the box provided.)
[][][]1 1
5 3 2 I___1 5.3.2a
Minis.3.3 n 5.3.3a
1,200 47
NA
5.4 Underground injection 5.5 Releases to land
5.5.1 On-slte landfill
f5.4a n 11 i 5.5.1a [][][]
NA NA
5.5.2 Land treatmerrt/appltedtion farming
5.5.2a [][][]
0
5.5.3 Surface Impoundment 5.5.4 Other disposal
5.5.3a [nit]
[ l [ i5.5.4a [
]
NA
NA
[ ] (Check if additional information is provided on Part iV-Suoptomentai tiformation.>
0. Basis of
1
Estimate:
(enter code)]
5.1b 0 |
G>]5.2b
5.3.lb 0 S.3.2b O
5.3.3b H3
C. % From Stormwater 5.3.1c NA
5.3.2c NA
54b Q
5.5.1b C3
5.5.2b Qj
5.5.3b Q 5.5.4b Q
EPA Form 9350-1 11 -89) Revised--Do not use previous versions
SAL 0000057X0
u
(Important: Type or print; read instructions before completing form.) .
1 oEPA
epaformR
PART III. CHEMICAL-SPECIFIC INFORMATION (continual)
Pag* 4 of S (This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers
ranges under A.1. (Do hot use both A.1 and A.2)
A. Total Transfers (bt/yrl
A.1 Reportkig Ranges
0 1-400 SOO SOS
A.2 Enter Estimate
B. Basie of Estimate (enter code)
Dteehare* to POTW
__ __
(enter location manbar 1.(1
[][][]6.1.1 from Part 1. Section 1.) 1 1 1-1 1
NA
6.1.1b
C.Type of Treatment/ Olsposal
^^^fente^ode^^^^
Other oft-ette location
.-------.
_ ^ . (enter loeatlon manner j , 1 1 6-2.1 from Part 1. Section 2.) | 2 |.[_ J
[
Other off-ette location , . . - - - (enter location number J 1 6.2.2 from Part l. Sections.) 1 * I I-
,
1f
1[
t ] NA itl
6.2.1b CU
n6.2.2b
6,2.1c lMl I 1 6.2.2c |M| j |
Other ott-eUe location
6.2.3
(enter location manber from Part I, Sections.)
a
I Lt ] JLi
6.2.3b 1|
[ ] (Chock If iddMoml Information Is provided on Part IV' Supplemental Information.)
6.2.3c |M| 1 |
7. WASTE TREATMENT METHOOS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent
Concentration (enter code)
O. Sequential
Treatment? (check If appteaMe)
E. Treatment Efficiency Estimate
F. Bated on
Operating "
Data?
Yas
No
7.1a '.2a
0 0
7.1b 7.2b
|b |i 111 li1 b |l |
7.3a 7.3b LlIlLI 7.4a 7.4b In|a| 1
7.to 0 7.2c 0
7.3c 7.4c
7.,d [ ] 7.*d [ ]
7.3d [ 1 7.4d [ 1
7.1e 7.2* 7.3e 7.4*
95 % 7.If
100
% 7.2f
%87. 5
7.3f
% 7.4f
[ ] fx ] ( 1 [x 1 ]fx [ ] t ][ ]
J7.Sa
1 1 1
7.6a *> LLi-l
7.5c 7.6c
7.Sd [ 1
7.Sd [ ]
7.5# 7.6a
% 7.Sf % 7.6f
[ ][ ] [ 1t ]
7.7a
**
111 1
7.7c
7.7d [ ]
7.7e
till7.6a
7.b
7.6c
[ ]7.M
7.6#
7.9a
1111
7.9c
[ ]7.9d
7.9e
7.10a 7-,0b LI ! 1
7.10c
[ ]7.,0d
7.10#
[ } (Chock If additional Information Is provided on Part IV-Supplemental Information.)
[ [ )% 7.7f
1
% 7.8f [ ] [ 1
% 7.9f [ ] t ]
% 7.10f [ ) [ ]
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(tndeato actions taken to reduce the amount of the chemical being released from the facMty. See the Instructions for coded Items and an explanation of tehat Information to Include.)
A. Type of ModMcation
(enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current
Prior
. Or percent
reporting
year
J change
year (fes/yr)
(Oa/yr) I
Ml l
SAl 0O00571!
1
EPA Form 93S0-1(1-891 Revised - Do not use previous versions
(important: Type or print; read instructions before completing form.)
<& EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addftional space for answers to questions In Part Ml. Number the fine* used sequential? from fines In prior sections ji.g., $.3.4. 6.1.2. 7.11)
Page S of S
AOOtnONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part Ilf, Section 5.3)
You may report releases of less than 1.000 to*, by cheddng ranges under A.1. (Oo not use both A.1 and A.2)
A. Total Release (tos/yr)
A.1 Reporting Ranges
O 1-Wf SOO-999
Estimate
B. Basis of Estimate
(enter code in box
provided)
S.3 Discharges to receiving streams or water bodies
5.3..
[][][]
5.3.
[Enter letter code front Pert t
II
Section 3.10 tor ctream(s) in r t
I___I
the boa provided.)
a.-.--- --*
S.3..
5.3_____CD S.3..
I 1l ][ ]
[][][]
5.3. 5.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS" (Part III. Section 6)
You may report transfers of less than 1.000 lbs. by checking ranges under A.1. (Do not use both A.1 end A.2)
A.Total Transfers (bs/yr|
A.t Reporting Ranges
o t-eee goo see
A.2 Enter Estimate
B. Basie of Estimate
(enter code In box
provided)
C. Type of Treatment/ Olsposai
(enter eode In box
provided)
6.1._____BBttrSSSfT.i
[ H J[ 1
6.1._____b 1 1
OtlwrdMiM tooatlan i--i1 i 6 2 (enter location wnesr 1 1 1 1 ----------iicnhftl, finuent.) 1 M___]
other oh-ehe location r--"1 i--*
6.2. -------- ((raemntePraloncaatioSnecmtioantt2e.r)
Ifill 1 LJ`L-J
Other off site location r --i r--1 6 2 (enter location number I 1 1 1
--------from Part , Section 2.11 z 1.1 1
[][](] [][][]
[][][]
6.2._____b I I 6.2._____b O 6.2._____b CD
*.Z._c|M| | | .*. c|M| | | 6.*. c|M| | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part HI. Section 71
A. General Waetestream
(enter code In box provided)
B. Treatment Method
(enter code
H box provided)
C. Range of Influent Concentration (enter code)
O. Sequential Treatment?
(check If
aopficabtel
E. Treatment Efficiency Estimate
F. Based on Operating Oata? Yes
No
7.--*
[1
lH1
7.
[]
7. ( H 1
---I 1
7. t n i
7.
-->
[) --------[ ]
_____ <[ 1
( it j
[H1
[U]
7.
7.
-"[ ] -"[ ]
[ ][ ] [H1
--`
---[ ]
[H]
EPA Form 0350-1(1-69) Revised--Oo not use previous versions.
SAL 0QQQQ5712
Form Approved OMB No.: 2070-0093
(Important: Type or print; read instructions before computing form.)
Approval Expire*:
01/91
Pag* 1 of S
S-EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community FVoht-to-Know Act of 1966.
also known a* Title III of the Superfund Amendntent* and Raauthorization Act
EPA FORM
R
PART 1.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public raportira burdM lor IN* 'CollectIan A information I* wtlRUMd to
very from SO to tour* par
with an average et 32 (nn .
feapanee, include*) time tor revleman*
Instruction*. aedchinfl eadating data
eureea. gathering ainfmairrtalrwwi tie
data needed, and completing and
reriewAng die willaction o< Information.
Send eamments reoardta-g this tudon
eetimate dr any ether expect el this
collection cl Information, inekjdtno
suggestion* tar reducingtN* burden, to
Chief, Information Policy Brorwn
(FM-223), US EPA. 401 M St.. SW.
Washington, O.C. 20460 Alin: TRI
Burden and to the Office of Information
end naputatory Affaire. Offtae of
Menagemeof and Budget Paperwork
Reduction Project
(2070-0063).
Washington. O.C. 20603.
1.1 Are you claiming the cnonVcsi identity on page 3 trade secret?
1.
11 Yes (Answer question 1.2;
1 * 1 No (Oo not answer 1.2:
Attach substantiation forms.)
Go to Question 1.3.)
1.2 ff * Yes* in t.l. is this copy: [ ] Sanitized [ ] UnsenltUsd
1.3 - Reporting Year 19.83.
2. CERTIFICATION (Read and sign after completing al sections.) 1 hereby certify that 1 Iwn reviewed the attached dsamntt and that, to tha beet of my knowledge and belief, the submitted information is true and complete and that ths amount* and values tot this report ore accural* based on reasonable estimates using data avallabia to the preparer* et ihti report. Name and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
Oats signed
Facility or Establlahmant Nome
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
Cetaity
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
Thi* report eentalne Information tar (Cheek one): 3.2
>tx] An entire (acuity
.. I 1 Pert of a facility.
Technical Contact
3.3 Brandt Butler
Pubtie Contact 3.4
Don R. Unruh
Telephone Number ftnefcate area coda)
318-491-5599
Telephone Nuntaor (induce area coda)
318-491-5222
SIC Coda (4 digit)
3.S .2911
b. na
e.
d.
a. f.
3.6
030
Latitude Minutes
14
SaffnnrU
36
Degrees
093
Longitude Minute*
16
Second*
20
Dun 6 Brsdstreet NumOer(s)
3.7 . 00-842-7692
NA
EPA Uenttficatton Nwnberfs) (RCRA I.D. No.)
3.8 .LAD990683716
NA
NPDES Permit Numbers)
3.9 ,.LA0003026
NA
Heelvino Stream* or Water Bodies <ent
*3ayou Verdine
boa)
b. NA
3.10
d.
Undergrawid ejection well Code (UC) Uontification Nurr*er()
3.11 *NA
PARENT COMPANY INFORMATION Noma of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Oui A Bradiuset Mmber
4.2 00-131-5704
EPA Form 9350-1 (1-A9) Advised--Do not use previous versions.
SAL 000005713
(Important: Type or print; read instructions before completing form.)Pag* 2 of S
a
A FPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PU8UCLY OWNE0 TREATMENT WORKS (POTWs)
1.1 POTW nm
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip State
(This space for your optional use.)
County Zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHKH WASTES ARE SENT Of*.Y FOR RECVtLMO OR REUSE).
2.1 Off-slte (oeation name
BFI
EPA Identification Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
zip 70664
la location under control o< reportIno ladilty or parent company?
2.2 Off-slte location name
NA
EPA Identifleattam Number (RCRA D. No.)
Street Address City
Coutty
State
ZIP
fat location inter control of reporting facility or parent company?
[ ]vee [xIn
[ lv,,
[u
2.3 Off-slte location name EPA MentHteallon Njmber (RCRA D. No.)
2.4 Off-slte location name EPA Identification Nimbar (RCRA D. No.)
Street Address
Street Address
City
County
City
County
State
Zip State
Zip
Is location under control of reporting facility or parent company?
[ ]ves
[ ]no
2.5 Off-slte location name
Is location under control of reporting facility or parent company?
2.6 Off-slte location name
[ ]v
[u
EPA Identification fWmber (RCRA O. No. |
EPA identification fkjmber (RCRA O. No.)
Street Address
Street Address
City
County
City
County
6tale
ZIP State
Zip
location under central of reporting faculty or parent oompany?
Is location under eontraf of reporting facility or parent company?
[ ]v-
[u
_________________________________________________________[ ]v-
[U
[ ] Check H additional paper of Part are attached. How many?
EPA Form 9350-1(1-09) Revised--Oo not use previous versions.
(Important: Type or print; read instructions before completing form.)
3-EPA
REPA FORM
PART lit. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (Thi spac for your optional us.
1. CHEMICAL IDENTITY(Do not complete tHa aaction If you complete Soetion 2.)
1.1 (Reserved] CAS Number (Entar tha mautar auetly aa it apoaara on tha 313 Hat. Enter NA M tsporting a dwnlul eatagofy-)
1.2
SA Chemical or Chemical Category Name {Enter tha nama axaetty aa it apgaara on tha 313 Nat.)
1.3 Nickel compounds
Generte Chemical Name (Campiat only it Part I. Soetion u a chacad V,` oanartc namo mutt ba ctruettaaUy eascriptiva.} 1.4
MIXTURE COMPONENT IDENTITY (Oo not complete this section If you comoiete Section 1.) 2. Oanarie Chomical Nam Providad by Suppliar (Limit ttia namo to a maximum of 70 ofiaraetora (.g.. numbars. battora. tpacas. punctuaiion).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Cheek al that aoNV.I
Manufacture the chemical:
3.1
ri a.i J Produce
If produce or Import:
r 1 For en-atte
c l J use/processing
^f d-l
b. [ ] import
e.[ ] Aa a byproduct
f.[
1 For eale/ J distribution
] As an impurity
Proceasthe 3.2 chemical:
r ** l
d.f
1 i Aa a reactant
] Repackaging only
1 Aa a formulation bl i component
T lAs an article c-l icomponent
3.3
Otherwise use .. . . .
the chemical:
f v 1 At a chamteal a.i XJprocessing aid
^f 1
___
b.l J As a manufacturing aid
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE
r1 c.i J Anctiary or other us
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than
1.000 be. by checking ranges under A.t. (Do not use both A.i and A.2)
A.I Reporting Ranges
0 T-4SS S00-9W
A.2 Enter Estimate
5.1 Fugitive or non-point air emissions 5.1a [][][]
11
5.2 Stack or point air emissions
5.2a [][][]
NA
5.3 Discharges to receiving streams or water bodies 5.3.1 1--1
(Entar lattar coda from Part l SacHon 3. to for straam(a) m tha box providad.)
([ 5.3.2 !___1
5.3.3 Q
5.3.1a [Hit] 5.3.2a [][][] 5.3.3a [][][]
5.4 Underground injection
5.4a [][][]
NA NA
5.S. 1 On-atta landfill 5.5.2 Land traatmanifapplicalion farming
5.5.1a [][][] 5.5.2a t ] t ].[ 1
NA NA
5-5-3 Surfaca impouiwmaii
S.S.3a [][][]
NA
5.5.4 Othar disposal
5.5.4a [ ] [ ] f ]
NA
B. Basie of 1 Estimate. (enter code|
5.1b I-]
5.3.1b cn
5.3.2b
C % From Stormwater 5.3.1C NA
5.3.2c
5.3.3b O
5.4b ;
5.5.1b O
5.5.2b CD
5.5.3b 1 1
s.5.46 n
t ] (Chae* H additional information <* provioao on Part iv-Sueplamantal information.)
EPA Form 9350-1(1-89) Revised -- Do not use previous versions
SAL 000005715
(Important: Type or print; read instructions before completing form.)
o EPA
EPA F0RM^
PART HI, CHEMICAL-SPECIFIC INFORMATION (continued)
Pag#4 of S (TWs spade for your optional use. |
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfer*
of test than 1.000 b*. by checking ranges under A.1. (Do not use
both A.1 and A.2j
A. Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-409 500 OOP
A.2 Enter Eotlmate
8. Basis of Estimate (enter codel
Ottoharg* io POTW r--. ----
(enter location number | 6.1.1 (ram Pen >. Section i.) I
.1I 1 1-1____
[][.][]
KA
1.1.1b
Other otl-eile location
(enter ioeetion numbei
(1from Pert , Section 2
'BE
fltl
1,900
!.2.1b 0
Other oft-4te ioeetion
. LUO [6 2.2
,-------. ...
3
Other ofl-eite ioeetion
6.2.2
(enter ioeetion menber tram Pvt a. Section 2.
Bur
][
]r
][
i[
1
]
NA
6.2.2b 6.2.3b
[ ] (Check If additional Information Is provided on Part IV Supplemental Information. |
G.Type of T reatment/ Disposal
.2.1c ImT7T2 I
R6.2.2c
6-2-3cfMT I I
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
O. Sequential
Treatment?
(check If appScable)
E. Treatment Efficiency Estimate
Ma
7,2a 7.3a
7. -
7.5a 7.6a
CU
7.1b 7.2b 7.3b 7.4b
7.5b 7.6b
7.1e 7.2c 7.3c 7.4e 7.5c 7.6c
7,1d 7.2d 7.3d 7.4d 7.Sd 7.6d
[1
t]
[]
[]
t1
[]
7.1a 7.2* 7.3* 7.4e 7.6* 7.6e
7.7a 7.6a 7.9a
7.7b 7.6b 7.9b
7.7c 7.6c 7.9c
7.7d 7.6d 7.9d
[] [1 [1
7.7# 7.6* 7.9*
7.10a
7.10b
7.10c
[7.10d ]
7.10*
[ ] (Check If addttlonai ktformatlon Is provided on Part IV-Supplemental Information.)
F. Based on Operating
Data 7 Yes
No
[ 1[ 1
7.2f [ ] [ ]
7.3f [ 1 [ ]
7.4f [ ] [ ]
7.5f [ I [ 1
7.6f Mil
7.7f [ ] [ ]
7.6f [ ] ( )
7.9f ( 1 [ 1
r.iot [ ] [ ]
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indteat# actions taken to reduce the amount of the chemical being released from die facEty. See the instructions for coded hems and an explanation of what Information to Include.)
A. Type of MooddHhtlecaatton (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current reporting year (tos/yr)
Prior year (bs/yr)
Or percent change
Ml
SAL 000005716
EPA Form 9350-1 (1-891 Revised - Do not use previous versions.
(Important: Type or print; read instructions before completing form.)
A PDA O UrM
EPA FORM R PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addHIonal space for answers to questions in P* tu. Number the Mas used sequential/ from inea In prior section# (e.g.. 5.3.4. 5.1.2. 7.11)
Page S of 5 (This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part 111, Section 5.3)
You may report releases of less than 1,000 lbs. by chocking ranges under A.1. (Do not use both A.1 and A.2)
S.3 Discharges to receiving streams or
water bodies
5.3..
A. Total Release (bs/yr)
A.1 naportttg Ranges
0 _ J-496 500-009
A.2 Enter Estimate
[][][]
B. Basis of Estimate
(enter code In bos
provided)
C.% Prom Stormwater
5.3.
n 5.3_______C
(Enlar totter eoto from Part*" 5.3_____
Section 3,10 tor *lream<c) the bOK provided.)
5.3..
5.3..
S.3..
[][][]
f ]f J[ 1
.JO5.3.
S.3.
5.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE L3O3CATIONS
(Pert 111. Section 6)
You may report transfers of less than 1,000 bs. by cheddng ranges under A.1. (Do not use
both A.1 and A.2)
A.Totaf Transfers (bs/yr)
A.1 Reporting flanges
o 1-ese too asa
A.2 Enter
Estimate
B. Basle of Estimate
(enter code inbox
provided)
C. Type of Treatment/ Disposal
(enter code ki box
provided)
Discharge to POTW
__
_,
(enter location iwnbw 1,1 1 |
6.1._____ten Pen R. Section 1.) | 1 M____|
[][][]
6.1._____b Q
Other cd-tlf toeatlon f-- 1
6-2-_____tt&nss&t
Other eW alia location j--j i--i
6.2.
(enter location number 2
1
--------fom Part a. Section 2.) L--J l____1
Other oti-tlte localIon
s.2.-- SSOSrSXSSSt,
[][][] [][][] [][][]
6.2._____b n 6.2._____b O 6.2._____b C]
6-2.____o|M| | | .2. c|m| 1 1 .2. c|m| 1 1
AOOmONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Pert lit. Section 7)
A. General Wastestream
(enter code
In box provided)
8. Treatment Method
(enter code
in box provided)
C. Range of Influent
Concentration (enter code)
D. Sequential Treatment? (check If appScabiei
E. Treatment Efficiency
Estimate
F. Based on Operating Oata? Yes
No
-lU
--*
[ ] 7. f1
[H] .'[ H 1
--
7.
.-[ ]
.*( H 1
--<( ]
--'[ H 1
--1 I 7.
-'[ H 1
.-[ 1
7. --<[ H ]
M
1
7. .*[ H ]
7.
7.
.-[ 1
.'[ n i
J 7.
'---l H ]
EPA Form 9350-1(1-59) Revised--Do not use previous versions.
SAL 000005717
(Important: Type or print; read instructions before computing form.)
Form Approved QMS No.: 2Q7Q-0093 Approval Expires:. 01/91
Page 1 of S
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Wgtrt-to-Know Act of 1086.
also known as TWe III of the Superfund Amendments end Reauthortzatton Act___________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public reporting burdon lor this
collection o< fofomution Is estimated to
vary wtth
from on
30 to 34 awrags
hoefu"aj3TiSR
respansa, Mousing lime tar reviewing
Instructicne. --arching --Isting data
sources, gathering ana matntakvnc the
data needed, and completing and
reviewing trid oodocttan of information.
Send eommgnta regarding this burden
estimate or any other -r--** of this
COlMetion of Information. Ineluding
suggestions tar reducing this burden, to
Chief, Mopnattan Policy Branch
(PM-223), US EPA. 40l M St., SW,
Washington, O.C. 20460 Attn: TRi
Burden and to the Office of ntarmation
and Regulatory Affairs, Offiee of
Management and Budget Paperwork
Reduction Project
(2070-0093).
Washington. O.C. 20603.
t. 1 Are you claiming the chemical identity an page 3 trede secret?
1.
1 1 Yes (Answer question 1.2:
I * | No (Do not answer 1.2;
Attadi substantiation forms. \
Go to Question t .3.)
1.2
ft - Yes- in 1.1. Is this copy: [ ]senlttaod[ ] Unsanitlnd
1.3 Reporting Year
19 88
2. CERTIFICATION (Read and sign after completing al sections.)
t hereby certify that l have reviewed the attached documents end that, to the best of my knowledge and belief, the ndsnfeted Information is true and eomptata and that the amsutlt and values In this report are accurate based on reasonable estimates using data available to the preparers of this report.
Name and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
Signature
Date signed
K /
Conoco Lake Charles Refinery
1. U.S, ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
Slate
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains Information for (Check one): 3.2 '
..[x] An entire facility
[ 1 Part of e facility.
Technical Contact 3.3
Brandt Butler
Publte Contact 3.4
Don R. Unruh
etc Code (4 dfoft)
3.S 2911
b. NA
3.6
Degrees
030
Latitude Minute
14
Dun a Bradstreet Number(s)
3.7 . 00-842-7692
c.
Seconds
36
Telephone Number (bekds area code)
318-491-5599
Telephone Nwtfoar (Include area code)
318-491-5222
d.
Degrees
093
NA
e. Longitude
Minutes
16
f.
Seconds 20
EPA Identification Number(s) (RCRA I.O. No.)
3.6 .LAD990683716
NPOE5 Permit Number(a)
3.9 .LA0003Q26
Receiving Streams or Water Bodies (amier one name per box)
.Bayou Verdine
NA NA b. NA
3.10
Undargroww Inaction Weft Cede (LSC) Identification Number(t) 3.11 HA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Compeyi Out t Bradstreet
4.2 00-131-5704
f 9350-
4s
^Toopoosti8
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC
CHEMICALS ARE TRANSFERRED IN WASTES
I. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
Zip Stale
Page 2 of S (This space for your optional usa. j
County ZIP
2. OTHER OFF-SITE LOCATIONS <DO NOT REPORT LOCATIONS TO WteCM WASTES ARE SENT ONLY POR RECYCLfMO OR REUSE).
2.1 Olf-slte location name
BFI EPA tteniHication Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
SUte
Louisiana
zip
70664
Is location under control of reportHo faculty or parent company?
2.2 Off-site location name NA.
EPA Identification Number (RCRA O. No.)
Street Address City
County
State
Zip
Is location under control of repertlno faeNIty or parent company?
f ]y [x]no
[ ]v [ U
Ofl-slte location name
EPA Identlfleatlan Nwrbar (RCRA D. No.)
2.4 Off-site location name EPA identification Number (RCRA O. No.)
Street Address
Street Address
city State
County Zip
City State
County Zip
Is location under control ot reporting facMity or parent company?
Is location under control of reporttrig facility or parent company?
2.S Off-site location name
[ ] Ye*
[ ] No
2.6 Off-site location nemo
t ]v,, [ u
EPA Idsntitieatian Number (RCRA O. No.)
EPA Identification Number (RCRA D. No.)
Street Address
Street Address
City
County
City
County
State
ZIP State
Zip
location under control of reporting fwtitty or parent company?
Is location inner control of reporting facility or parent company?
[ ] Yes
[ ]ns
I 1 Owed If tMUoml pign of Part aro attached. How manyT
EPA Form 9350-1(1*89) Revised--Do not use previous verstons.
[ ,]. [ U
SAL 0000057X9
(Important: Type or print; road instructions before completing form.)
o-EPA
REPA FORM
PART 111. CHEMICAL-SPECIFIC INFORMATION
Psq* 3 of $ (This space for your optional use.) j
1. CHEMICAL IDENTTTY(Do not complete this section If you complete Section 2.)
1.1 {Reserved)
1.2
CAS Number (Enter the number exactly as It appaan on tha 313 list. Enter NA H reporting a chemical category.)
7664-38-2
Chemical or Chemical Category Name (Enter m name exeetty a* it appear* on the 313 lift.)
1.3 Phosphoric Add
Generic Chemical Name (Complete only if Pen l. Section 1.1 is Checked "Yes.* Generic name must be structurally descriptive.) 1.4
MIXTURE COMPONENT IDENTITY (Do not complete ttiie section If vou comoiete Section 1.) 2. Generic Chemical Name Provided by 6ufelter (Limit the name to a maximum ot TO characters (e g.. numbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check el that apply.1
Manufacture the
If produce or import:
chemical: 3.1
ri a.l J Produce
f 1 For on-site c-l J use/proeessing
t
b. [ ] Import
e.[ ] As a byproduct
f.[
1 For sale/ J distribution
] As an Impurity
Process the 3.2 chemical:
r * l
d. [
] Am - r*~*,-* J Ae a reactant ] Repackaging only
K T ] As a formulation *L J component
f ] As an article c-l Jcomponent
3.3
Otherwise use .....
the chemical:
fv 1 As a chemical a. IX J procaeskig aid
.f 1
. _____ t.
b.l j As a manufacturing aid
f1 e.t i AncSary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR YEAR
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Rolease (tbs/yr)
You may report releases of Vess than
1.000 bt. by checking ranges under A.l. (Do not use both A.l and A.2)
A.l Reportmg Ranges
0 t-*9 500-909
A.2
Enter Estimate
5.1 Fugitive or non-point air emissions
5.1a [][][]
NA
S.2 Stack or point air omissions
S.2a [ ] [ ] [ ]
5.3 Discharges to receiving _ ,, [7| streams or water bodies 5.3.1 lLJ
5.3.1a (][][]
(Enter letter cod* from Part 1 Section 3.10 lor *iram<J m tn* pox provided.)
[][][]1 I
5 3 2 1 5.3.2a
[][][]CD5.3.3
5.3.3a
5.4 Underground Injoctlon 5.5 Releases to land
5.5.1 Ovill* landfill
[5.4a If 1 [ 1 [HIM5.5.1a
5.5.2 Land trealment/appiication farming
5.5.2a [][][]
5.5.3 Surfee* impoundment
5.5.3a (][][]
5.5.4 Other dtapoaal
5.5.4a [](][]
NA
0
NA
NA NA NA NA NA
{ ] Check if additional Information is provided on Part tv-Supplemental information.)
6. Basis of 1 Estimate 1
(enter eoctyM
[D5.1b
j
5.2b
5.3.1b [3 5.3.2b
C, % From Stormwater 5.3.1c NA
5.3.2c NA
5.3.3b 1 1
s.<t> !
CD5.5.1b
I
CD5.5.2b
CD5.5.3b
5.5.4b n
6PA Form 9350-1(1-891 Revised--Do not use previous versions
SAL 000005720
u
(Important: Type or print; read instructions before completing form.)
O EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 of S (This spade for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers
of less than 1.000 tos. by checking ranges under A. 1. (Do not use both A.) and A.2)
A. Total Transfers (fcs/yr)
A.1
Reporting Ranges
o t-sse soo-ess
A.2
Enter
Estimate
B. Basis of Estimate (enter code)
Otaeherp* to POTW
[][][]6.1.1
(enter location mute (ill from Pert . Section 1.) 1 M l
,
\ \
NA
6.1.1b O
Other eff-stte location
. r.--
6_.2..1.
(enter location number 1 - I from Part a. Section 2.) ( _
11
[
1[
1[
10
6.2.ib 0
Other off-^He location
. .
t6..2A.2. f(reonmtePr laorctaIt.ioSnencutimonbe2r.) lLoJl-li. J1
Other off--die localIon , .. r--J
e.ntrpSisa.HOi
1( 1(
1 ( 1 1[ 1
HA
O6.2.2b
C.Type of Treatment/ Disposal
(enter code!
| 2!
6.2.2c |M| 1 | 6.2.3c |M| 1 |
[ ] (Chock If additional information la prodded on Part IV Supplemental Information.)
7. WASTE TREATMENT METHODS ANP EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent -
Concentration (enter code)
O. Sequential
Treatment? (cheek If applcable)
7.1a 0 7.1b |c|i|i| 7.2a 0 7.2b |c|i|i|
7.1c 7.2c
7-,`1 7.2d
(1
[]
7.3a
7.3b
|n|a| 1
7.3c
7.3d [ ]
E. Treatment Efficiency Estimate
F. Based on Operating Oata? Yes
No
[x] [ 17.1e
100% 7.1f
[ ] (x ]7.2e
100% 7.2f
[ ] [ ]7.3e
% 7.3f
7.4a
7.b
1 11 1
7.4c
7.4d [ ]
7.4e
[ 1 [ ]% 7.4f
- 7.5a
IJJ 1
IJ_1 17.6a
T-*
7.Sc 7.6c
7.Sd [ ] 7.6d [ ]
7.5e 7.6e
% 7.5f % 7.6f
MM [ ][ ]
7.7a TM 111 1
M 1 17.6a
7.8b
7.7c 7.6c
7.7d 7.8d
[]
[]
7.7e 7.8a
M 1 17.fla
7-9b
7.9c
7" [ ] 7.9e
| | | |7.10a
7.,0b
7.10P
[ ]7.,d
7.10s
[ } (Check If addftlonaJ Information la prodded on Part IV-Supplemental Information.)
% 7.7f
% 7.8f
% 7.9f
% 7.10f
[ ][ ] (111 I 1[ 1 [ 1[ ]
8 . OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actione taken to reduce the amount of the chemical being released from the faeftty. See the Instruction* for coded Item* and an explanation of what Information to Include.)
A. Type of MotMcatlon (enter code)
6. Quantity of the Chemical In Waste* Prior to Treatment or Disposal
C. Index
D. Reason lor Action (enter code)
Current reporting year (tos/yr)
Prior year
(toa/yr)
. Or percent I change
I I I* I
EPA Form 9350-1(1-89) Reused - Do not use previous versions.
SAL 000005721
(Important: Type or print; read instructions before completing form.)
EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section if you need additional apace for answers to questions In Part in. Number the Bnes used sequential from anes ki prior sections (e.g.. 5.3.4, 5.1.2. 7.11)
Page S of S {This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III, Section 5.3)_________________________________ _____________________________
You may report releases of less than 1,000 bs. by cheering ranges under A.1.
(Do not use both A.1 end A.2)
A. Total Rariase (bs/yr)
A.1 noporing Ranges 0 HR 500-ess
A.2
Enter Estimate
5.3 Discharges to
.
receiving streams or water bodies
,_ 1 1 S.3-------1--1
S.3___ a
[](][]
B. Basis of Estimate
(enter code kt box
provided)
C.% From Stormwater S.3______bO
5.3______ c
(Enter letter cod* from Pan 1
1I
Section 3. to tor iMamtl) in r i
|___1
mo bon provided.)
-----------
5.3_____a [](][]
S.3_____O S.3_____a [][][]
5.3._____bf~1 S.3._____c -_tP S.3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Pert HI, Section 6)
You may report transfers of less then 1.000 bs. by cheering ranges under A. 1. (Do not use
both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reportkig Ranges
0 1-40S too sss
A.2 Enter Estimate
B. Basis of Estimate
(enter code Inbox
provided)
C. Type of Treatment/ Disposal
(enter code In box
provided)
_, 6.1.
Otechwgc e POTW ,-----, . (enter toeouon toft liar 1 . 1 I 1 trerf' Port t. Section 1.1 | 1 |.)___J t
][
]I
]
6.1._____b Q
g9
Other
o location |-- *--*
(enter location number 1 * 1 1 I
[][][]--------from Part a. Seetlcnl 1 * U _ 1
6.2._____b O
|6-2-____c|M| |
Other eft-one tocihon i--t | -- i 6.2.--------tfroanmtoPr elorlcaLtioSneicwtinonb*c.) Ll*J|-|LJ1
Other ofl-sHo iuualiow i
t5SSMKii MM*-*_____
[][][] [ 1[ ] [ ]
o6.2._____b
6.2._____b
!. c|M| | | S.2. c|M| | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHOOS AND EFFICIENCY (Pert Ilf, Section 7)
A. General
Wastestream (enter code in box provided 1
B. Treatment
Method (enter code In box provided)
C. Range of
Mhjent Concentration (enter code)
0. Sequential Treatment? (check If appleable)
E. Treatment Efficiency Estimate
F. Based on Operating Oata?
Yes
No
7. a 7. b 1 J.L i
7.
c 7._---[ 1
7.___ e
% 7.
r 11 ]
7.
a 7._
. (IT i
7.
c 7._---[ 1
7.___ e
% 7.
.<r ] i 1
7. a 7. b r r i i
7.
c 7.
dr i
7.
e
% 7.
f [ 11 1
7. a 7. b ITT i 7.___ a 7.___b TT i
7. e 7.
fi
7.
e
7.
c
7._---i ]
7.
e
% 7.
f [ 11 ]
% 7,___-<[ n ]
7, a 7. b rrr i
7. a 7..
rrr i
7. c 7. d F 1 7.
7.
c 7.
-[ ]
7.___ e
% 7.
% 7.
f[ ] i 1 r 11 ]
7. a 7._
rrr i
7.______c
7.
-[ ]
7.______e
% 7.
r ]i 1
7. a 7. - CLL i
7.
c 7 --<( ]
7,______e
% 7.
<[ n ]
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
SAL 000005722
Form Approved QMB No.: 2070-0093 Approval Expire* :_93/91
(Important: Type or print;, read instructions before completing form.)
Pago 1 of i
SEPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning end Community Hght-to-Know Act of 1986,
also known as Title 111 of the Superfund Amendments and Reauthorization Act___________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
PubUc reporting burden tor this
collection m Information M winittM to
vary Obowmn S3O0 to 34 tMtauurra par i
with an swaps of 32 how* par
msaonas. tncknfing time tor renews^
mauuctlona. tsaniiWgj existing data
ouroaa, gatharbig and maintaining the
data naidaa. and completing and
reviewing tha eoltaetlon o< tntormatleri.
Sand comments regarding iMs burdan
estimate or any other asscpact of this causation o< Information, tnetudir^
suggestion* for reducing ihia burdan. to
usChiaf, Information Policy Branch
(P*A-223).
EPA, 401 M St., SW.
Washington O.C. 20400 Attn: TPi
Burdan and to tha Otlioa of Mormalion
and Ragulatory Affair*. Offioa ol
Management and Budgal Paperwork
Raduetion Project
(2070-0003).
Washington, O.C. 20603.
1.1 Ara you claiming tha chemical Identity an page 3 trade secret?
1.
[ ] Yas (Answer Question 1.2:
[ ^ ] No (Do not answer 1.2;
Attach substantiation forms.)
Go to Question 1.3.)
1.2
tt *Yee* in 1.1, is this oopy: [ ] Sanitized [ ] UnsaNtlaod
1.3 fl sporting Year 19 88
2. CERTIFICATION (Read and sign after completing al sections.)
I hsrsby earthy that I hava ra viawad tha attached decunantt and that, to tha boat of my knowledge and ballaf. tha admitted information i trua and complete and that tha amount and vetoes In this rsport ara accurals based on reasonable estimates using data avaUabia to tha proparors of this report.
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SE^D COMPLETED FORMS:
1, U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
Cotarty
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report eomaine Information tor (Check ana): 3.2
..[x] Ait antIra fecHIty
[ 1 Part of a facility.
Technical Contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
StC Coda (4 digit)
3.S .2911
b. na
Latitude
3.6
Degree*
Mirwtes
030
14
Dun & Bradstreet Number(<)
3.7 00-842-7692
EPA Identification Number (*) (RCAa i.D. No.)
3.6 ..LAD990683716
e.
Seconds
36
Talaghona Number (Include area cods)
-J18-A91-5599...
Telephone Number (include area code)
318-491-5222
d.
Dagraas
093 NA
NA
a.
Longitude MMutas
16
Seconds 20
NPOES Permit Numpar(s)
3.9 .LA0003026
Receiving Streams or Water Bodies (enter one
*.Bayou Verdine
bOK)
NA b. NA
3.1 d.
Underground Pfaetton Wall Coda (UtC) Idantlffcation Numbar(s) 3.11 aHA
Parent Company'* Ow 4 Sradcueat fWmbar
00-131-5704______________________________________
EPA Form 9350-1 (1-69) Revnsoo--Do not use previous versions
SAL 000005723
L_l (Important: Type or print; read instructions before completing form.)
a rriA
o trA
EPA FORM R
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBUCLY OWNED TREATMENT WORKS (POTWs)
1.1 POTWnam# NA
Street Adores*
1.2 POTW name Street Address
City
County
City
Stete
ZIP State
Page 2 of S (This space for yotr optional use.)
County Zip
2. OTHER OFF-StTE LOCATIONS (90 NOT REPORT LOCATIONS TO WMCH WASTES ARE SENT ONLY FOR RECYCUNG OR REUSE).
2.1 Off-slte location name
BFI
EPA Ueniihcation Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
Stete
Louisiana
ZIP 70664
' is location under control d npenire faculty or parent eompanyT
2.2 Off-slte location name
NA
EPA (dentHieatwn Number (RCRA O. No. |
Street Address
City
Canty
State
Zip
Is location under control of reportkv facility or parent company?
1 [ 1Y~ [xJ"
[k
[U
2.3 Off-slte location name
2.4 Off-site location name
EPA identification NunCer (RCRA D. No.)
EPA tdentffteailot Number (RCRA O. No.)
Street AddreM
Street Address
City
Cotady
City
County
State
Zip State
Zip
Is location under oontrel ot reporting facMtty or parent company?
2.S Off-site location name
[ ]v [ U
1* location under odrtrol ot reporting facility or parent company?
2.6 Olf-slte location name
[ ]v,, [ U
EPA Wentllicatlon Number (RCRA D. No.)
EPA Identification Number (RCRA O. No.)
Street Address
Street Address
City
County
City
County
State
ZIP Slate
Zip
ocation unM control art reporting itdmy or parent company?
[ ] Yes
[ ] No
[ ] Cheoh additional pages of Pert are attached. Hew mwiyT
Is tocatien under control art reporting facility or parent Company?
i ]v- [ U
EPA Form 6350-1(1-89) Revised--Do not use previous versions.
SAL 000005724
(Important: Type or print; read instructions before completing form.)
n EDA CrM
EPA FOBM R PART III. CHEMICAL-SPECIFIC INFORMATION
Pag* 3 of S {This space for your optional use.)
1. CHEMICAL |DENTTTY(0o not complete this section If you complete Section 2.) 1.1 {Reserved]
CAS Number (Enter the *nber exactly a* ft appears on the 313 Wat. Enter NA It reporting chemical category.) 1.2 115-07-1
Chemical or Chemical Category Name (Enter the name eaeetiy as it appears an the 3t3 list.) 1.3
Propylene
Generic Chemical Name (Complete only If Part 1, Section 1.1 is Cheekeo 'Yes.* Generic name must be structtraliy descriptive.) 1.4
MIXTURE COMPONENT IDENTITY (Do not complete this section If vou complete Section 1.)
2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (e.Q., rajmbers, letters, tpaoes, punctuation),)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aooiv.l
Menufecture the chemical:
3.1
ri a.lxj Produce
If produce or import:
f v 1 For on-sKe c-l^Juee/processinQ
Jf
1 For tale/ i (attribution
b. [ ] Import
e.[ ] As a byproduct
f. [ ^] As an impurity
Process the
3.2 chemical:
3.3
Otherwise use .....
ins cnemicsi:
*
flxA Jl
a. As
.
Mueue reactant
. d.[ ] Repackaging only
f
a.L
lJAprsocaecshsienmg iacaidl
*f
b\
1J
As a formulation
component
.f b.l
1J
. As
a
manufacturing
aid
f 1JAcoamapnoanretnictle
f1 c.L X-l AncSary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENDAR!YEAR lO I 7l (entar coda)
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
You may report releases of less than 1.000 tos. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (tos/yrj
A.1 Reporting Ranges
0 1-499 500-999
A.2 Enter
Estimate
B. Basis Of | Estimate (enter codeH
S.lb 1
S.1 Fugitive or non-point air emissions
5.1s [][](]
140,000
5.2 Stack or point air emissions
5.2a l ] [ ] [ ]
NA
5.2b
S.3 Discharges to receiving _ .
1
streams or water bodies o-3*1 l--1
(Entr laitar cods from Part l
Section 3.10 for ttraam(s) In the box provided.)
1[ 5.3.2 1 1
5.3.3 n
5.3.1a [][][] 5.3.2a [][]{] 5.3.3a [][][]
S.4 Underground ln|eetion
5.4a t ] [ 1 [ 1
NA NA
S.3.1b n
.""Mtormwater
5.3.2b 5.3.3b Q
5.3.2c
5.4b [j i
5.5 Releases to land 5.S. 1 On--*lia landfill
5.6.2 Land traatmant/application farming
5.5.1a (][][] 5.5.2a [][][]
NA NA
S.S.Ito O 5.5.2b Q
5.5.3 Surtaea impotndmant 5.5.4 Olhar disposal
5 5.3a [][][] 5.5.4a [][][]
NA NA
5.5.3b 3 5.5.4b Q
[ ] (Chacfc If additional Information providad on Pan iV-Suopiemantal Information.)
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005725
(Important: Type or print; read instructions before completing form.)
o EPA
EPA FORM^
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
Page 4 of s (This space for your oottonal use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of lot* than 1,000 lb. by chocking ranges under A.1. (Do not use
both A.1 and A.2)
A. Total Transfers
(bs/yr)
A.1
Reporting Ranges
0 1-499 fi00 909
A.2 Enter Estimate
B. Basis of Estimate (enter codel
Dtecheipe to POTW
---- ---
(enter location number I, I J 6.1.1 tram Part I. Sectten
[][][]
NA
6.1.1b
Other
tecatten
--
. , (enter location number ] i) | 6.2.1 from Part I, Sectten ;.)| * ||
f
1[
II
1
NA
i.2.1b I I
Otner otf-ett* tecatten . - -j s.z.2 tsrp5tgasa!?,[j].D [
1I
][
1
i.2.2b I I
C.Type of Treatment/ Disposal
Other off-ette tecatten
ienter tecatten iwanbei'.][ 1 [ rom Part S, Section 2
1[
1
'2.3b d]
[ ] (Check H addWonal Information Is provided on Part IV-Supplemental Information.)
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wasteetream
(enter code)
B. Treatment Method
(enter code)
C. Range of Influent Concentration (enter code)
D. Sequential
Treatment 7 (check If appttcablel
7.1 7.2a
7.1b 7.2b
7.1c 7.2c
t 17.Id
r-" [ 1
7.3a r.4a
7.3b 7.4b
7.3c 7.4c
7.3d 7.4d
[]
[1
E. Treatment Efficiency Estimate
7.1i
7.2#
7.3e
7.4e
F. Based on Operating Data? Yes
No
7.If [ ] [ ]
7.2f t ] [ ]
7.3f [ ] { ]
7.4f [ ] ( 1
7.6a
7.6b
7.7a
7.7b
7.8a
7.8b
7.9a
7.9b
7.10a
7.10b
7.6c 7.7c 7.8c 7.9c 7.10c
7.6d ( ] 7.7d t 1 7.6d [ ] 7.9d [ ]
7.10d [ 1
7.6e 7.7e 7.fie 7.9a 7.10*
7.6f [ ] [ 1
7.7f [ 1 I 1
7.8f [ 1 [ ] 7.9f [ ] [ ] 7.10f [ 1 [ ]
8. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actions taken to reduce the amount of the chemical bektg released from the faeftty. See the Instructions for coded Items and an explanation of what Information to Include.)
A. T Modification (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current reporting year (fes/yr)
Prior year (Ibs/yr)
Or percent change
M it
EPA Form 9350-1(1-09) Revised - Do not use previous versions
SAL 000005726
(Important: Type or print; read instructions before completing form.)
a EDA ^ urM
part iv.
Repa form
supplemental information
Use this section If you need addftlonal space for answers to questions In Part III. Number the fries used sequentlafly from fries in prior sections (e.g.. 5.3.4. 6.1.2. 7.M)
Page 5 o< S (This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III, Section S.3)
You may report releases of loss than 1.000 hi. by checking ranges wider A.1.
(Do not use both A. 1 and A.2)
A. Total Release (bs/yr)
A.t Reporting Ranges 0 \~499- S0Q-Q9B
A.2 Enter Estimate
0. Basis olf Estimate
(enter code in box
provided!
5.3Discharges to receiving streams or water bodies
_
5.3.
5.3..
[][}[]
(Effltf letter code tram Part Section 3. to tor stre*m<s) the boa provided.)
5.3..
5.3..
5.3..
[][][]
[][][]
i-3-_bCJ
ADOtTIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1.000 bs. by checking ranges under A.1. (Oo not use both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-4SS BOO S90
A.2 Enter
Estimate
B. Barts of Estimate
(enter code in box
provided)
C. Type of Treatment/ Disposal
(enter code kt box
provided)
Dtseftaroe to POTW .------. .-----,
_ . (enter todaUen nuitor 1.1 f | 5.1.___wm Part i. fiwtloii t.| I 1 M_____|
(Hill
O)l
*
Other ett Uto location <-->
SO [][][]
6.2._____b H
6.2.------c |m| | |
Other off-afte toeattan i ~i r- i
6.2. --------
fCroamntoPr laoctaLtioSnandwtainto*r.
1
( Z11 1 LJ'LJ
[][][]
6.2._____b
.*. e| M| | |
-*--- ts,*rp5fj`,asiEf?.i LlI.LJ [][][]
6.2._____b S
S.*. c|M| | |
A. General Wastestream
(enter code In box provided 1
7--`
*
7. . Q 7.
B. Treatment Method
(enter code kt box orovided)
- rm
bllll
7-. bllll 7.
7.
*---n
7. .
- - rm * - 1 Q.J 7- * 1J _L J
7- - 1 LU 7---b | |_j |
7' b|||)
C. Range of Influent Concentration (enter code)
7--- 7---
D. Sequential Treatment? (check tf appBeabiel
7- -[ 1
7. df 1
7---=
7
e[ ]
7--- 7
a[ ]
7- .
7-
7-_______= 7- 7-
7` -[ 7 -[ 7---- -[
7-__ -( 7- [
] ] ]
1 ]
E. Treatment Efficiency Estimate
7. e
%
F. Based on Operating
Data? Yes
No
'[7--- 11 ]
7.e
% 7-
'fill
7.e 7. e 7.e 7. e 7.S
s7.
7.e
H )% 7-'l
% 7 '( ][ 1
'[% 7-- ][ 1
* 7 >( ][ 1 % 7- [ ][ 1 % 7--<( H 1 % 7 [ H 1
j
e
fs.
EPA Form 0350-1(1-09) Hevised--Do not use previous versions.
SAL 000005727
Form Approvod OMB No.: 2070-0093
Approval Expire*: 01/91
(Important: Type or print; read instructions before completing form.)
Paoo 1 of S
6-EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Flaming and Community Wght-to-Know Act of 1966.
also known a* Title HI of the Superfund Amendment* and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
nubile reporting brn ter thi is
collection of MermaUon is estimated to
very tram 30 to 34 hoin par response,
erfth an emrege of 32 hours per
response, mplutfing time tar reviewing
Instruetlons. --rchiiM existing cats
mnat, gathering andmainlainng lha
data needed, and oomcistlnq and
rortowtag the ooOecttoi eflntarmattan.
Sand comments regarding this burdsn
estimate or any ether aspact of this
eoltaettan of information. tncVjdtng
suggosttans tar reducing, this burden, to
Chief, totertnation Policy Branch
(PM-223). US CPA. 401 M St.. SW.
Washington. D.C. 204*0 Attn: TRI
Burden and to the Office of Information
and Oagulatary Affairs, Office of
Management and Budget Paperwork
Reduction Protect
(2070-00*3).
Washington, D.C. 20*03.
1.1 Are you claiming the chemical Identity on page 3 trade secret?
1.
[ 1 Yea (Answer question 1.2;
[ ^ J No (Do not answer 1.2:
Attach substantiation forms.)
Co to Question 1.3.1
1.2
If *Yet* in 1.1. is this copy: [ ] Sanitized [ ] UnswVtUed
1.3 Deportlog Year 19 88
2. CERTIFICATION (Reed and sign after completing al sections. |
I hereby certify that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true and complete and mat the amotmts td values In this report are accurate based on reasonable estimates using data evailtbli to the preparers of this report.
Name and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manage^_____________
Signature
Date s
3. FACILITY IDENTIFICATION
Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 Clly
Westlake
Slate
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains Information for (Cheek one): 3.2
*.[X ]an entire facility
.. t 1 Part of a feedtty.
Technical Contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
Telephone Nwtaer (include
318-491^5599
Telephone Neibir (include area
318-491-5222
sic Cede (4 digit)
3.5 .2911
b. na
e.
d.
e. 1.
3.6
Degrees
030
Latitude Minutes
14
Sspends
36
Degrees
093
Longitude Minxes
16
Seconds
20
Dun & Bradstreet Nu-nber(s)
3.7 00-842-7692
EPA Identification Number(s) (RCRA I.D. No.)
3.8 .LAD990683716
b. NA b. NA
NPOES Permit Number(s)
3.9 .LA0003026
Receiving Streams or Water Bodies (enter one name per box)
aJJayou Verdine
b. NA b. NA
3.10 c.
d.
.
Undargroune bisection Weil Cede (LHC) Identification Nurrtoer(s)
3.11 *NA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
Parent Company's Out 4 Bradstreet Number
4.2 00-131-5704
EPA Form S3S0-1 (1-89) Revised--Do not use previous versions.
f. b.
(Important: Type or print; read instructions before completing form.)
A r-r-IA trA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW n*m
____ _ . NA_______________________
Street Address
1.2 POTW name Street Address
City
County
City
Slat*
Zip State
Page 2 of 5
County Zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WMCH WASTES ARE SENT ONLY FOR RECYCLfMG OR REUSE).
2.1 Off-sita location name
BFI
ERA identification Number (RCRA <D. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Ceiatty
Calcasieu
State
Louisiana
zip
70664
K location under central el reporting teciuty or parent company?
2.2 Off-sito location name
NA
EPA Idemiticatton Number (RCRA D. No.)
Street Address
City
Courity
State
ZIP
a location under contra! at lepcnlno facility or parent company?
L
2.J Off-sito location namo
[ ]y-- Ix]n
2.4 Off-sito location namo
[ ] Yes
[ ] No
EPA tdentMhcaUon Ngrvtoar (RCRA O. No.)
EPA Identification Number (RCRA O. Mb.)
Street Addrosa City
CaMy
Strwt AAlrttf City
County
State
ZIP Stale
Zip
a location under control et reporting facility or parent company?
2.S Off-sito ioeation namo
[ ]v [ u
Is location under control of reporting facility or parent company?
2.6 Olf-sito location name
[ 1* [ U
EPA identification tOenfaor (RCRA D. No.)
ERA identllicatlon Ntanber (RCRA O. No.)
Street Address
Street Address
City
County
City
County
State
Zip
location wtdor central of reporting facility or parent company?
I____________________________________________
[ ]v~ [
]
State
Zip
a location under contra! of reporting faeMIty or parent company?
[U [u
EPA Form 93SO-1(1-09) Revised--Do not usd previous versions.
SAL 000005729
(Important: Type or print; read instructions before completing form.)
o-EPA
EPA FORM R PART 111. CHEMICAL-SPECIFIC INFORMATION
Pafle 3 of 5
(This apace for your optional use.!
1. CHEMICAL IDENTTTYfOo not complete this section If you complete Section 2.)
1.1 (Reserved) CAS Number (Enter the number exactly a* It appears on the 313 list. Enter NA If reporting a enemies) category.)
1.2 1310-73-2 Chemical or Chemical Category Name (Enter the name exactly as it appear* on the 313 list.)
1.3 Sodium hydroxide (solution) Generic Chemical Name- (Complete only if Part I, Section 1.1 is checked *Ye." Generic name mutt be structurally descriptive.
1.4
MIXTURE COMPONENT IDENTITY (Do not complete this section if you complete Section 1.) 2. Generic Chemical Name Provided by Supplier (Limit the name to a maxMsan ol 70 eharaetars (e.g., numbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aootv.l
Manufacture the chemical:
3.1
rt a. L J Produce
If produce or import:
f 1 For on-site C-L J uee/processing
.f d-*-
1 For sale/ J distribution
b. [ ] Import
e.[ ] As a byproduct
f.[ ] At an knpurtty
Process the 3.2 chemical:
f ** l
d. [
1 J A* a reactant
] Repackaging only
w f ) As a formulation *L J component
f ] As an article c.l J component
Otherwise use 3.3 the chemical*
T -.1 As a chemical a. L XJ processing aid
, f 1.
...
b.l J As a manufacturing aid
f1 c.l J Ancillary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURINO THE CALENDAR YEAR
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (be/yr)
You may report releases of less than
.1.000 fes. by checking ranges under A. 1
(Do not use both A.1 and A.2)
A.1 Reporting Ranges
o i-ass soo-eee
A.2 Enter
Estimate
5.1 Fugitive or non-point air emissions
5.1a [][][]
5.2 Stack or point air emissions
5.2a [][][]
S.3 Discharges to receiving
[][][]streams or water bodies
. ("7") *3-1 L*sJ
5.3.1a
3.(Enter letter coo* from Part 1
Section to lor streamfs) in the box provtoed.)
[][][]) |
5.3.2 1 I 5.3.2a
[][](]5.3.3 5.3.3a
0 0 0
NA
5.4 Underground injection 5.5 Releases to land
5.5.1 On-site landfill
5.4a [)[}[]
5.5.1a [][][]
NA NA
5.5.2 Land treatment/application farming
[ [ [5.5.2a
1
1
1 NA
5.5.3 Surface impoundment
5.5.3a [][][] NA
5.5.4 Other disposal
5.5.4a [][)[] NA
[ 1 (Cheek M aOOii'onai inlormalion i* provided on Part IV-Suppiementat information.
B. Basis of I
Estimate ,
(enter codeM
05.1b 05,b
5.3.1b 0
CZ!5.3.2b
5.3.3b O
5.4b Q
5.5.1b (ZD|
o5.5.2b
5.5.3b | |; 5.5.4b Q
EPA Form 9350-i(f-69| Revised --Do not use previous versions
000005730 SAL
(important: Type or print; read instructions before completing form.)
Page 5 of S
SEPA
EPA FORM h PART IV. SUPPLEMENTAL INFORMATION
Use this taction U you need additional space for anawere to questions In Part Hi. Number the toes used sequentU#y from toes in prior eectione (e.g., 5.3.4. 6,1.2. 7.11)
ADDmONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON^SITE
You may report releases of less man 1,000 bs. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (bs/yr)
A.1 Reporting Ranges
0 1-499 S00-999
A.2 Enter
Estimate
5.3 Discharges to
|--.
receiving streams or
II
[water bodies
5.3--------1--1 5.3_____a
3[
1(
3
8. Basis at Estimate
(enter code Inbox
provided)
5.3______tC
C.% From Stormwater
S.3.
c
(Enter letter cede from Pan 1
1]
Section 3.10 lor
[the fee* oromded-l
In c 3
II
--------------'
5.3_____a
3[
3[
3
[][][]5.3_____ 5.3_____a
s.,_a 5.3.
c
a-n -2*____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6)
You may report transfers of less than 1.000 lbs. by checking ranges under A.1. (Do not use both A.1 and A.2>
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
0 1-4SS too sos
A.2 Enter
Estimate
8. Basis of Estimate
(enter oode In box
provided)
C. Type of Treatment/ Disposal
(enter code h box
provided)
6.1.
PIMieia to POTW lanter location nurteMr
[][][]from Pan I. Soottaw
6.1..
6.2.
Othar eft-eite location (mar location runsa . (rum Pan a. Cootion 2
[][][]
6.2.
O(ethneterrolfotc-aUttioenloMcantiOonr,,a.p
[nil]----------tram Pan i. flection 2
6.2.
?,soOther off-etta location
(enter location nuntt . from Pan i. Section
[
iiii
i
(.2._____b rn i.2._____b n 6.2._____b
6.2.i
AODmONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part W1. Section 7)
A. General Wastastream
(enter code
in box provided)
8. Treatment Method
(enter code In box provided j
C. Range of
Influent Concentration
(enter code)
0. Sequential Treatment 7 (check If
applcablel
E. Treatment Efficiency
Estimate
F. Based on Operating Data?
Yes
No
7.
7.
( 1 7.
i n3
7.
_<= ---I ] 7.
ni
7.
3J
.*[ 1
7.
-<l H 1
7. 7.
-- --
I1 (3
7. 7.
H3
-*[ 1[ 3
7.
--* 7.
_<=
7.
A3 [3
7. 7.
-'{ 3 3 3 -<[ ][ 3
--
7. 7.
--'>
--<=
7.
[3 (3
7. 7.
.'[ J[ 3 -'[ 3 3 3
EPA Form 9350-1 f 1-A9) Revised--Do not use previous versions.
SAL 000005732
(Important: Type or print; read instructions before completing form.)
O EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION (continued)
Pago 4 of 5 (This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of lass than 1,000 bs. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A. Total Transfers (tos/yr)
A.1 Reporting Ranges
0 1-4SB 500-098
A.2 Enter Estimate
8. Basle of Estimate (enter code)
Otteiwst to POTW
,
1 | I(enter location number
,
| [][][] NA6.1.1 from Part 1, Section |.) I'M
.\
cd6.1.1b
C.Type of Treatment/ Disposal
^^^(ente^wde^^^^
Other oft-site location . 4 , (enter location rw*ar j 2 1 1
[6.2.1 from Part S, flection 2.) (__r|__
]f
1(
] NA
Other otf-elte location ___
Me . . (enter location nunMr 1 * 1 *M . . [6.2.2 from Part I. Section 2.1
.
1[
Jf 1
Other otl-aite location f.
| 1 j i(enter location number , (. *_M_ [][][]6.2.3 from Part I. SeetlmZ. \
-
6.2.1b CD 6.2.2b O 6.2.3b 1j
6.2.1c lMl 1 i 6.2.2c |M| 1 1 6.2.3c |m| 1 1
[ ] (Check If addtoonal Information Is provldad on Part (V-Supptemental Information.)
7. WASTE TREATMENT METHODS AND EFFTCIENCV
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter code)
D. Sequential Treatment? (check If applcabio)
E. Treatment Efficiency Estimate
F. Based on Operating Oats? Yes
No
7.1a
0 7.1b
|C|1 |l|
7.2a 7.2b I|aI 1
| j |7.3a
7.3b
|
7.1c 7.2c 7.3c
7.,d [ ] 7.2d [ ] 7.3d [ ]
7.1# 7.2e 7.3e
100% 7.If % 7.2f % 7.3f
[(X1 [ 1[ [ 3[
1
] 1
7.4a 7.5a
7.4b 7.5b
m'i
M||
7.4 7.Sc
7.4d [ ] 7.Sd [ ]
7.4e 7.Se
% 7.4f % 7.Sf
[ 3[ 3 [111
7.6a 7.7a
7.6b 7.7b
||||
Mil
7.6e 7.7c
7.5d [ ] 7.7d [ ]
7.6e 7.7e
% 7i.6f % 7.7f
[ 3[ 3 [ 1[ 3
7.6a
7to
till
7.6c
]7.3d [
7. fie
|| 1 17.9a
7.5b
7.9c
[ ]7.9d
7.9e
| | | |7.10a
7.,Ob
7.10c
7',0d [ 1 7.10e
[ ] (Chock if addKionat information te provided on Part IV-Stplemental Information.)
% 7,6f % 7.9f % 7.10<
[ 3[ 3 [ 3[ 3 [111
. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(tndtoate action* taken to reduce the amount of tha chemical being ralaaaad from the facSty. Saa the Instructions for eodad items and an explanation of what Information to Include.)
A. Type of Modfflcatlon
(enter code)* I
Q. Quantity of the Ciiendoal In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current reporting year (tos/yr)
Prior year (tosfyr)
( Or percent , change ,
[M I
l
R
EPA Form 9350-1 (1-89) Revised - Do not use previous versions
SAL 000005731
(Important: Type or print: read instructions before computing form.)
Form Approved OMB No.: 2070-0093 Approval Explrds:. 01/91
Page 1 of 5
EPAo
U.S. Environmental Protection Aoeney
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community fVght-to-Know Act of 1986,
also known as Title HI of the Stperfund Amendments and Reauthorlzahon Act_________
PwWe reporting burtm for tht eoMtetloi of information m Mdmttad to very ton M M 34 how* par ntpone. with an Mrm ot az hours par
nuponaa, IrtotuJng lima tar reviewfno
tonmettonaj eaarcNng eetara data " --"--1---------^maMaMng the
PART I.
FACILITY IDENTIFICATION INFORMATION
estimate or anv oner aspect of this
coiteeitan at Information, including fugga*tkau ler reducing this burden, to
Chief, Information Polkey Brawn
(PM-223). US EPA. 401 M St.. SW.
Washington. O.C. 20460 Ann: TRi
Burdan and to lha Offlea of Information
and Regulatory Affair*. Office of
Management and Budget Paperwork
Reduction Project
(2070-0063).
Washington, O.C. 20600.
_______
1.1 Are you claiming tha chemical Identity on peg# 3 trade secret?
L 1 Ye* (Answer question 1.2;
[ ^ j No (Do not answer 1.2;
Attach substantiation forms.)
Go to Question 1.3.)
1.2 tf'Yes* m l.t. it this eepyt [ ] Sanitised [ ]unsanttled
1.3 Deponing Year
Ifl 88
2. CERTIFICATION (Reed end sign after completing al sections.) t hereby certify that I have reviewed the attached document* and that, to the beat ot my knowledge and betlet, the eutsrVtted Infonnation is true and compfeta and that the amounts and value* tn this report are accurate basad on raasenabia estimate* using data available te fha preparers ot this report.
Name and official title of owner/operator or server management official
Don R. Unruh, Refinery. Manager
Date slgnad
3. FACILITY IDENTIFICATION Facility or Establishment Mama
Conoco Lake Charles
Street Addre**
Old Spanish Trail 3.1
City
Wesclake
Refinery
Cowity
Calcasieu
1...............r
i
vvncnc iu oenu vumruicu runme.
1. U.S. ENVIRONMENTAL PROTECTION AGENCY P.O. BOX 70266 WASHINGTON, DC 20024-0266 ATTN: TOXIC CHEMICAL RELEASE INVENTORY
2. APPROPRIATE STATE OFFICE' (See instructions
Louisiana
70669
Appendix E)
This report eontalne information for (Check one): 3.2
Tv 1 *.l^ J An entire facility
f1 b. [ J Pert of e feclhty.
Technical Confect
3.3 Brandt Butler
Public Contact 3.4
Don R. Unruh
SC Code <4 digit)
3.S a 2911
b. NA
e.
3.6
Degree*
030
Latitude Minute*
14
Seconds
36
Oun 4 Bradstreet Numbar(s)
3.7 00-842-7692
EPA Identification Mumber(t) (RCRA i.D. No.)
3.8 a LAD990683716
NPDES Permit NurTtter(s)
3.9 .LA0003026
Deceiving Stream or Water Oodles (enter one name par boa)
.Bayou Verdine
Teiaphone Number (IneMf area coda)
318-491-5599 :
Talaphona Number (include area coda)
318-491-5222
d.
Degree*
093 b. na b. NA b. na b. NA
e.
Longitude Minute*
16
f.
Second*
20
3.10 c.
<s.
e.
Underground k*eetion Weil Cod* (UfC) identification NurTttar(s)
,3,, aNA
PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.I. DuPont de Nemours
4.2
Parent Company's Out 4 Bradstreet Nwitbar
00-131-5704
EPA Form 93S0-1 (1-89) Revised--Do not use previous versions.
t.
b.
SAL 000005733
U
(Important: Type or print; read instructions before completing form.)
r% rnA
x* trA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBUGLY OWNED TREATMENT WORKS (POTWt)
1.1 POTW nm
NA
Street Address
1.2 POTW name Street Address
City
County
City
State
ZIP State
(This space for your optional use.)
County Zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WMCH WASTES ARE 9&MT ONLY FOR RECYCUNG OR REUSE).
2.1 Off-slto location natno
BFI
EPA Identification Number (RCAA O. NO.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
IS location under centre! of reporting facility or parent company?
2.2 Oll-slia location name
NA
EPA Identification Number (RCRA . No,)
Street Address City
County
State
Zip
Is location under control of reporting faculty or parent eampany?
[I
[U
[u
2.3 OM-slto location name EPA identification Number (AGRA O. No.)
2.4 Off-alto location name EPA Identification NumOor (RCRA O. No.)
Street Address
Street Address
City
County
City
County
State
Zip State
Zip
Is location under control pt reporting facility or parent company?
2.5 Olf-sito location name
1 ]v [ ]no
Is location under control of reporting facility or parent con^any?
2.6 Olf-slto location name
f ]v,,
[
EPA Identification Nurttwr (RCRA O. No. |
EPA Identification Number (RCRA O. No.)
Street Address
Sireel Address
City
County
City
County
Stale
Zip Slate
Zip
location under control of reporting lacWty or parent eampany? [ ]v,, [ u
Is location under control of reporting facility or parent company?
[ ] Yes
[ ] No
[ ] Cheek if additional pages of Part are attached. How mewt
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
SM- 00000513*
(Important: Type or print; read instructions before completing form.)
a rnn EPA
EPA FORM ^ PART HI. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S (This space for your optional use.)
1. CHEMICAL lDENITTY(Do not complete thle section If you complete Section 2.1
1.1 (Reserved] CAS Number (Enter the number exactly u it appear* on the 313 Hst. Enter IMA rt reporting a chemical category-1
1.2
100-42-5
Chemical or Chemical Category Name (Enter the name exactly a* it appear* ot th* 313 n*t.) 1.3
Stvrene
Generic Chemical Name (Complete only It Part U Seelion 1.1 i cheeked "Ye*. Ganarie name mutt be atrueturatly rHwrrlplli* ) 1.4
MIXTURE COMPONENT IDENTITY (Do not comolete tNs section If vou complete Section 1 .V 2. Ganarie Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (.g.. nun*er*. letters, space*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check el that aootv.1
Manufacture the chemical;
3.1
r1 a.L J Produce
(f produce or knport:
f 1 For on*the c'l -1 ute/proeeeting
T
b. [ ] Import
e.( ] At a byproduct
f.[
1 For tale/ J (Attribution
] A* an Impurity
Proeea* the 3.2 chemical;
fr 1 * J At a reactant d. f ] Repackaging only
Kf 1 As a femviatfon b.l i component
f 1 Asian article Jcofnponent
3.3
Otherwise use the chemical'
f 1 At a chemical * ^ 1 processing aid
1 , ^ ,__. b.l 1 As e manufacturing aid
fl c.l i Anc*ary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANYTIME DURING THE
S. RELEASES OP THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (tos/yr)
You may report releases of lets than
1.000 tot. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-400 500-000
A.2 Enter
Estimate
5.1 Fugitive or non-point elr emissions
5.1a [][][]
880
5.2 Stack or point air emissions
S.2a [][][] 27
5.3 Discharges to receiving streams or water bodies
fTj i_J
(Enter letter coda from Part 1 Section 3.10 for ttream(s) In tn* box provided.)
fI 5,3 3 1 1
5.3.3
[5.3.la 1 f ] I 1
l 1 15.3.2a
[ ][
5.3.3a [][][]
39 HA
S.4 Underground injection 5.5 Releases to land
6.5.1 On-*he landfill
6.5.2 Land treatment/application farming
(5.4e 1 f IT 1 (5.5.la 1 1 11 1 5.5.2a [][][]
NA NA 0
6-5.3 Surface Impoundment
1 l 1 15.5.3a [
[
HA
5.5.4 Other ditpotal
(HIM5.5.4a
NA
B. Basis of . I Estimate; (enter eode}|
s.ib (il
5.2b 0 5.3.1b 0 5.3.2b
5.3.3b 0 5.4b Qj
5.5.1b 0i 5.5.2b 0j
S.S.3b | |1 5.5.4b 0 1
(Check It aoditiona) inlormation is orov'ded on Part tV-Suppiemanta! Information.)
EPA. Form 93S0-1f1-69) Revtsed -- Do not use previous versions
SAL 000005735
(Important: Type or print; read instructions before completing form.)
oEPA
EPA FORmR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
Pag# 4 of S (This space for your optional use.}
6. TRANSFERS OF THE CHEMICAL (N WASTE TO OFF-BITE LOCATIONS
You may report transfer* of tece than 1.000 lb*, toy cheeking range* under A.1. (Do not use
both A.1 and A.2)
A. Total Transfer*
(fes/yr)
A.1 Reporting Range*
0 1-4*0 500-0*0
A.2 Enter
Estlmati
B. Baal* of Estimate (enter code!
DiMhorpe to POTW ,-----, (*mar taMtion (iimr M} t 5.1.1 from Part I. Section t.J I ' l-l
,
[][][] NA
6.1.1b ED
Other ort-*lte location . ,, (enter toeatiort numoer 1*11 6.2.1 from Part t. Section 2.) 1 * 1-t
MMI
I
r. J
Othar off-elte location (enter location numeai from Pan *. Section 2
111) M
Ottw oH-altt location
S(antar location number
L-lJ-Li-J6.2.3 from Pant. Sactlon 2.
3
NA
!.2.1b
6.2.2b
n6.2.3b
[ ] (Check W addWtonal Information 1* provided on Part IV-Supplemental information, j
C.Type of Treatment/ Disposal
L J6.2.ic Ml I F Fm6.2.2c I
6.2.3c )ML f |
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
B. Treatment Method
(enter code)
C. Range of influent Concentration
(enter code)
M*
Q 7.1b
b|i ll I
7.1c
El D7.2*
7.2b EE
7.3a
7.3b
NA
r-4*
n
7.4b
Q
Q7.5a
7.Sb
a7.2e
7.3c 7.40
7.5c
D. Sequential Treatment? (check if appteabie)
[ ]r.id
7.2d [ 1
7.3d [ 1
[ 17.4d
( 17.6d
E. Treatment Efficiency Estimate
7.1* 7.2* 7.3* 7.4* 7.5a
90 %
100
7.6a 7.7a
7.6b
T-7b
Q
rr
7.6a
7.8b
Q
7.9a
7.9b
7.10a
7.10b | |
7.6c
7.7c
7.6c
7.c Q
7.10c
[7.6d [7.7d I7.6d l7.9d
7.l0d I
1 ] ] ]
1
7.6* 7.7* 7.8* 7.9# 7.10*
[ ] (Cheek If edtftional Information la provided on Pert IV-Staspiemental Information.)
F. Based on Operating Data? Ye*
No
7.1. [ ] [X]
7.21 l 1 lx]
7.3f 7.4f
lH] MM
>-5' [HI
t 1[ 3
7.7f [HI ?.6f MM
7.9f [ ] [ )
7.101 MM
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate action* taken to reduce the amount of the chemical being released from the facty. See the Instructions for coded Items and an explanation of what information to include. I
A. Type of Modfflcation (enter code)
6. Quantity of the Chemical In Waste* Prior to Treatment or Disposal
C. index
0. Reason for Action (enter code]
Current reporting year (Ibs/yr)
Prior year
(ti#/yr|
Or percent change
LaLM O .CD
EPA Form 9350-1(1-891 Revised - Do not use previous versions.
SAL 000005736
(Important: Type or print; read instructions before completing form.)
Page 5 of 5
3-EPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section W you need addHJonal spec# for answers to questions In Part III.
Numbor the fries uitd sequential/ from Itws in prior aAction*
5.3.4. 6.1.2, 7.11)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ONSITE
(Part III. Section 5.3)
You may report releases of less than 1.000 lbs. by checking ranges taider A. 1. (Oo not use both A.1 and A.2)
A. Total Release (tos/yr)
A.1 Reporting Ranges 0 1-400 5OO-0M
A.2 Enter Estimate
5.3 Discharges lo
.-------
receiving streams or ,, ,,
II
twater bodies
5.3.-- 1--' S.3_____a
3t
3f
3
B. Basis of Estimate
{enter code In box
providedl
C.% From Stormwater 5.3______bQ
5.3_______c
(Enter latlar coea from Part t
11
Section 3. JO tor iirMm(i) Pci
II
[tha boa prcwwMd.)
9-*--------u~1
5.3--^.a
3[
3[
3
5.3._____bl 1 5.3._____c
[ 3 [ 3 [ 3S.3_____a
_] S-3-______c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Part III. Section 6?_________________
You may report transfers of less than 1.000 bs. by cheddng ranges under A. 1. (Do not use bofrt A.1 and A.2)
A.Total Transfers (ba/yr)
A.1 Reporting Ranges
0 I-400 0Q OQQ
A.2 Enter
Estimate
B. Basis of Estimate
(ontor code in box
provided)
C. Type of Treatment/ Disposal
(enter code tn box
provided)
6.1.
Oiacnarpe to POTW (enter location mans , runt Part f, ffaetlan
[][][]
1.1._____b
6.2.
Other eft site tanuun -- (mer location iwnMr I - I I I from Pan a. Section a.) I *_l-l J
Other off-site lafiilkw 6.2._____ tamerr location mattee f
L.0O1 worn Part f. beettan
6.2.
Othar off altc location
r. -
tenter location nunW I - I I I
irem Part i, Saetlon 2.) I * I t I
[](][]
(][][]
[][](]
6.2.
e.2._dM| | 1
T I6.2.
6.2.____c|m!
6.2.
.--c|m| I I
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part 111. Section 7)
A. General Wastestream
(enter code In box provided)
8. Treatment Method
(enter code
In box provided!
C. Range of Mhient Concentration (enter code)
D. Sequential
Treatment? (cheek tf appteablef
E. Treatment Efficiency Estimate
F. Based on Operating
Data?
Yes
No
n7. 7---6 l
7.
7.
r---c
[1 -[ ]
[ ][ 1
[H]
7.
'------ "
7--- cm
7. 7.
ED
7.
A1 --I 1
[ ][ ] [ ][ j [H]
7. 7. 7. 7.
7.
cm
7. 7. 7.
A1
3
A1
7.
[U3
[ 31 3
[ 11 3
7. 7.
7.
1
t It 1
EPA Form 6350-1(1-69} Revised--Oo not use previous versions.
SAL 000005737
(Important: Type or print: read instructions before completing form.)
Form Approved OM8 No.: 2070--0093 Approval Expires:. 01/91
Paoa 1 of S
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Right-to-Know Act of 1966.
also known as Title III of the Stxwrfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public reporting burden lor ifw*
OoUecttan of information t* estimated to
vary from 30 to 34 howl per wponn,
with an average of 32 hours par
naspanae, pehiang time tor reviawtng
existing data
fouroat, oathanng and maintaining the
data nated. and compfstma and
reviewing the oottection of Mormatlon.
Send comments regardthtt burden
ettlmata or any ether aspect of this
collection t information. Includirw
suggestion* tor reducingthis burden, to
CMef. Mbrmation Policy Brsrah
(PM-223), US EPA. 401 M St.. SW.
Washington. D.C. 20460 Attn: TRl
Surdsn end'to the Office of Information
and Reguiptory Affairs. Office of
Management and Budget Paperwork
Reduction
Project
(2070-0063).
Washington, O.C. 20603.
1.1 Are you claiming the chemical identity on page 3 trade secret?
1.
1 ] Yea (Answer Question 1.2;
1 ^ I No (Do rwt answer t.2:
Attach substantiation forms.)
Go to Question 1.3,)
1.2
If *Yes* in l.t. Is this copy: [ ] Sanitised [ ] Uneantiized
1.3 Reporting Year 19 88
2. CERTIFICATION (Read end sign after completing el sections. | I hereby certify that I have reviewed the attached documents and that, to the bast of my fenewtadgs and belief, the submitted information is true end oompiete and that the amounts end values in this report are accurate based on reasonable estimates using data available to the preperers of this report.
Name and official title of owner/operator or senior management official
Don R. Unruh, Refinery. Manager
3. __FACtHTYJPENTIFICATION Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
Slate
Louisiana
P.O. BOX 70266
WASHINGTON. OC 20024-0266
Canty
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Coda
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains Information for (Chad* one): 3.2
fv 1
Jd. 1.7C An entire taeHIty
ri
Jb. [
Part of a facility.
Technical Contact
3.3 Brandt Butler
PubHC Contact 3.4
Don R. Unruh
SIC Coda (4 <dgtt)
3.S .2911
3.6
Degrees
030
b. NA
Latitude Minutes
14
c.
Seconds
36
Dun & Bradstreet Number()
3.7 .. 00-842-7692
EPA Identification Number(s) (RCRA i.D. No.)
3.6 LAD990683716
3.9
hPOCS Permit Nwnber(s)
.LA0003026
Receiving Streams or Water Bodies (enter one name par box)
*3ayou Verdine
Telephone Nwnber (include area cade)
318-491-5599
Telephone Number (include area coda)
318-491-5222
d. Oagrees
093
b. na
b. NA
b. NA
b. NA
a.
Longitude Minutes
16
f.
Seconds
20
3.10 c.
d.
#.
Undergromd Infection Wail Code (UiC) tdentHtcation Number(s) 3.11 aNA
4. PARENT COMPANY INFORMATION Name of Parent Company
4.1 E.1. DuPont de Nemours
Parent Company* Ow & Bradstreet Nuntwr
4.2 00-131-5704
EPA Form S3S0-1 (1-69) Revised--Do rvot use previous versions.
t. b.
SAL 000005738
(Important: Type or print; read instructions before completing form.)
& EPA-- r-r- m.
REPA FORM
PART 11. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWs)
1.1 POTW name NA
Street Address
1.2 POTW name street Address
City
County
City
State
Zip State
Page 2 of S (This space for your optional use.)
County ZIP
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WtCH WASTES ARE SENT ONLY FOR RECYCLMQ OR REUSE).
2.1 Off-site location name BFI
EPA identification Number {RCRA . No.) NA
Street Address
Cities Service Hwy at 1-10
etty
Sulfur
County
Calcasieu
Stale
Louisiana
zu
70664
is location under control gi reporting faculty or parent company?
2.2 Off-site location name NA
EPA Identification Number (RCRA C. No.)
Street Address City
County
State
Zip
is location wider control of reporting faculty or parent company?
[ ]y#s txl**>
[ lv-
[ ]h.
4.3 Off-site location name
2.4 Off-site location name
EPA tdantifleatlen Mjmber {RCRA O. No.)
EPA tdantltteailon Number (RCRA . No.)
Street Address
Street Address
City
County
City
County
State
ZIP
State
Zip
Is location under control of reporting facility or parent company?
2.S Off-site location name
[ ]ves
[ ]no
Is location under control of reporting facility or parent eompeny?
2.6 Off-sfte location name
[ lv..
[ ].
EPA identification Nwnbv (RCRA O. No.)
EPA Identification Nuntoar {RCRA . No.)
Street Address
Street Address
City
1 County
City
County
State
Zip State
Zip
< location under aontiol of reporting faculty or parent company?
U[ ]v~ [
[ ] Cheek tt eddlttenat pages of Part 1 are attached. Hews many?
is location under control of reporting faefttty or parent company?
[ llv-
U[
EPA Form 93S0-1 (1 -69| Revised--Do not use previous versions.
SAL 000005739
(Important: Type or print; read instructions before completing form.)
&EPA
EPA FOAM R
PART III. CHEMICAL-SPECIFIC INFORMATION
Page 3 of S
---------; ---
-------
(This spaca for your optional use.)
1. CHEMICAL IDENTITY(Do not complete this section if you complete Section 2.)
1.1 [Reserved] CAS Number (Enter tha number exactly as it appear* on tn* 313 list. Enter NA if reporting a chemical category. >
1.2 7664-93-9
Chemical or Chemical Category Name (Enter the none exactly e* n appear* on the ata Net.)
1.3 Sulfuric Acid
Generic Chemical Name (Complete onty h Pert l. Section l.l I* cnecXed 'Ye*.' Generic name muet be structurally descriptive.> 1.4
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1.1 2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum of 70 characters (e.g.< mender*. tetter*, apace*, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Cheek el that aootv.)
Manufacture the chemical:
3.1
ri a. IXj Produce
If produce or import:
f vl For on-rite c-l AJ use/processlng
J f yl For sale/ t distribution
b. [ ] Import
e.[ ] As a byproduct
f.[ ] As op Impurity
Process the 3.2 chemical:
r ].
.
*-1 J As a reactant
d.[ ] Repackaging only
hf 1 A* a formiiatlon b-L J component
r 1 As an article
*l J component
3.3
Otherwise use the chemical'
f lAs a chemical a. L XJ processing aid
f1
,,
b.l J As a manufacturing aid
f1
,
c.l gjAnc^ary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURING THE CALENOAR YEAR
|0 1 ?! (enter code)
5. RELEASES OF THe'cHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (bs/yr)
You may report releases of less than 1.000 b. by checking ranges under A.1. (Do not use both A.l and a.2)
A.l Reportlnq Ranges
0 1-490 soo-eoe
A.2 Enter Estimate
5.1 Fugitive or non-point air emissions
5.1a f
J I xJ I
]
5.2 Stack or point air emissions
5.2a [][][]
460
5.3 Discharges to receiving ... I* | streams or water bodies 5-3.1 1--1
5.3.1a [][][]
(Enter l*tler cod* from Pari 1
Section 3.10 lor (Um|t) In the box provided.)
11
5 3 2 1___1
5.3.2a [][](]
5-3.3 | | 5.3.3a [][][]
0
NA
B. Basis of
1
Estimate !
(enter cod4)
5.1b 0, 5.2b S']
5.3.1b 0| 5.3.2b Q 5.3.3b O
C. % From Stormwater 5.3.1c NA
5.3.2c NA
5.4 Underground injection 5.5 Releases to land
5.5.1 Orv-*lie landfill
5.5.2 Land treatment/application (arming
S.4a [
][
11
]
5.5.1a [][][]
S.S.2a [][](]
NA NA NA
5.4b 0 f 5.5.1b 0 | 5.5.2b 0
5.5.3 Surface wnooundment 5.5.4 Other discos*!
5.5.3a [][][] 5.S.4a [][][]
NA NA
5.5.3b 0 5.5.4b 0
[ ] (Check If additional information is provided on Part fV-Suppiemonfal information.)
EPA Form 9350-1(1-691 Revised--Do not use previous versions.
SAL 000005740
u
(Important: Type or print; read instructions before completing form.)
gDA
epa formR
PART M. CHEMICAL-SPEC1RC INFORMATION (continued)
Pag* 4 of 5 (TNe space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of teas than 1.000 *>s. by checking ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfers (fca/yr)
A.1 Reporting Ranges
0 1-400 500*000
A.2
Enter Estimate
8. Basis of Estimate tenter code!
Oischarps to POTW <--, --*, (amer toestlen number ) . 1 |
[6.1.1 from Pan I. Section i.j 1 1 |.|____
anOther ott-ette location
_ _ . (enter location number 6.2.1 from Pan I. Saettai 2
[
Other otf-ette location
-BD I(enter location nunSaor
from Pan I. Section 2.
Other eft-eltei location tamer toeatii
ssff?,HO6.2.3 from Pan A
.-------.
]{
1\
]l 1f
1 t 1 NA
1 [ 1 NA
MJ
][ 1
6.1.1b 1.2.1b I I
6.2.2b i.2.3b | 1
[ ] (Cheek If addKtonal Information Is provided on Part IV-$uppiemental Information. )
C.Type of Treatments Disposal
T. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of
influent Concentration (enter code)
0. Sequential Treatment?
(cheek If applcable)
. Treatment Efficiency Estimate
F. Based on Operating Data? Yes
No
7.1a 7.2a 7.3a 7.4a
0
7.1b 7.2b 7.3b 7.4b
lc 03 [F A| f
1111
11 1 1
07.1c 7.2c 7.3c 7.4c
7.'d [ ] 7.M [ ] 7.3d [ ] 7.4d [ ]
7.1* 7.2* 7.3* 7.4*
100% 7.If % 7.2f % 7.3f % 7.4f
[ *1 [ [ ][ ( 1t [ ][
1 1 1 1
7.5a
7.5b
||||
7.5c
[ ]7.5d
7.5*
7.6a 7.7a 7.6a
7.6b
||| |
7.7b
||| |
| |7.6b
||
7.6c 7.7c 7.6c
[ ]7.6d [ ]7.7d
[ ]7.d
7.6* 7.7* 7.6*
| | | |7.9a
7.9b
7.9c
[ ]7.9d
7.6
| | | |7.10a
7.10b
7.10c
[ ]7.10d
7.10*
[ ] (Check if additional Information Is provided on Part IV-Stqiplemental Information.)
% 7.51 I 1 [ 1
1 [ 1% 7.6f
t
% 7.71 [ 1 [ 1
% 7.61 [ 1 [ ]
% 7.9f [ 1 [ 1
l ] [ ]% 7.lOt
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indeate actions taken to reduce the amount of the chemical being released from the facftty. See the Instructions tor coded Hems and an oxplanatlon of v*hat Information to tnckido.)
Modification (enter code)
B. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
0. Reason for Action (enter code)
0
Current
reporting year (Ibs/yr)
Prior
year (tos/yr)
. Or percent I change
I l
EPA Form 93S0-1 (1 --69) Revised - Do not use previous versions.
SAL 000005741
(Important: Type or print; read instructions before computing form.)
a PDA
Xy CrM
EPA FOBM R
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need addHkxiaJ space for answers to questions in Part HI. Ntsnber the lines used sequentially from ines fen prior sections (e.g.. 5.3.4. .1.2. 7.11)
Pag 5 of 5 (This space lor your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III, Section 5.3) _________
You may report releases of less than 1.000 tos. Oy cheeking ranges under A.1.
(Do not use both A. 1 and A.2)
A. Total Release (tJs/yr)
A.1 Reporting Ranges
O 1-400 5OO.00B
A.2 Enter Estimate
5.3 Discharges to
.--------.
receiving streams or water bodies
II 5-3- --1--1
5.3_____8 [][][]
B. Basis Of Estimate
(enter rode ki box
provided)
C.% From Stormwater 5.3________b(~]
5.3_______c
tenter eilr eoM tram Pan 1
1|
Section 3.10 tor *tream(c) tj
1____1
the boa provided.)
--------------------
5.3_____* [][][]
5.3_____a [][][]
5.3.
bj 5.3.
c
s.3.n _____C
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part III. Section 6)
__________
_____
____
You may report transfers df~tess than 1.000 lbs. by checking
ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (fes/yrj
A.1 Reporting Ranges
0 1-400 too 909
A.2 Enter
Estimate
B. Baste of Estimate
(enter code ki box
provided)
C. Type of Treatment/ Oisposai
(enter code In box
provided)
[][][]6.1._____ISrp^53SfT-.
Other oft-eite toeatlon i-- --e
69
(enter location number 1 1 1 1
e,z*--------from Part . Section 2.) lM.j J
Other (MMe localton t j i--i
Lil-LI-- tSTpEfV^SSf?..
Other off tNi location <
SOe-2---
i
--
[][][] [][][] [][][]
6.1._____b Q
b|~~l6-2._____ n6.2._____b
*2._____b
6-2-------c | m| | | 6,2. c|m| | |
| |*.*. c|M|
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS ANO EFFICIENCY (Part HI. Section 7)
A. General
Wastestream (enter code
in box provided)
B. Treatment Method
(enter code
In box provided)
C. Range of
Influent Concentration (enter code)
D. Sequenttef Treatment?
(check If apptcabiel
m
mmj
F. Based on Operatkig Oata ? Yes
No
T--' 7-
"Mil
= 7.
d[ ]
7.
e
%
111]
,
7-... b | | | |
7-
c
7.
d[ ]
7.
a
% 7--[ H ]
7. 7--* 7-
b n 11
b| | | |
, .Q 7-______b f|||
7. b mi
7. b 1 1 1 1 7. ^ rm , .n 7. b m i
7-
..=
7.
7.
cQ
7.
d[ ] -[ ]
7- , c Q
7-------------[ 1
7.
=
7.
d[ ]
7-_______e
7.----------*[ ]
7.
c Q 7-
- [ 3
7. c 7-______1 ]
7. e 7. e 7. e 7.______e 7.______e 7. e 7. e
% 7-[ If ]
*1
'[ ][ )
%
'( If 1
% *
1 1[ 3
% 7-
-[ ][ 3
% 7-
[ J[ 3
%*
! ( 31 3
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005742
(Important: Type or print; read instructions before completing form.)
Form Approve*] OM6 No.: 2070-0093 Approval Fvplrw 01/91
^PagsJjjtJSp
EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1966. also known as TWe III of the SuperfundAmendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION INFORMATION
(This space for your optional use.)
Public rationing burden tor mil ooilaoiluaiMJMamwtion is estimated to
very from 30 to 04 hew* per reeenii.
with en average el 32 hours per
response. Metudeig time lor reviewing
Instructtone. scat Thing existing data
sourest. oaSterWj and maintalnind the data needed, end completing and
rovtoadng the eoNeettan of Mormetton.
Send conenants regarding this burden
estimate or any otnar aspect ot this
ooltaelten dt Information. inetudina
suggestions tor redudna this burden, to
Chief, Information Policy Branch
(PM-S23), US EPA. 401 M St.. SW,
Washington. O.C. 20460 Attn: TRl
Burden and to the Office ol totormatton
end Regulatory Affairs, Office of
Management and Budget Paperwork
Reduction
Project
(2070-0003).
Washington. O.C. 20603.
1.1 A/e you claiming the chemical Identity on page 3 trade secret?
1.
1 1 Yes (Answer Question 1.2;
[ No <0o not answer 1.2:
Attach substantiation forms.)
Go to Question t.3,1
1.2
tf *Yes* in i.t. Is this copy: [ ] Sanitised [ ] Unsanittmd
1.3 Reporting Year
19 88
2. CERTIFICATION (Road and sign after completing al sections.| 1 hereby oertlfy that 1 have reviewed the attached documents and that, to the oast of my knowledge and baiiaf. the submitted information is true and complete end that the amounts and values in this report are accurate based on reasonable estimates using data available to the preparers of this report.
Name and official title of owner/operator or ceniar management official
Don R. Unruh, Refiij&py. Manager,
Signature
Oats signed .
.
3. f*ALiiinT lueminwiiufi____________
Fadllly or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-02Q6
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
2. APPROPRIATE STATE OFFICE (See Instructions
Zip Cede
70669
Appendix E)
j.2 This report oontatoe totormatton ter (Chech one):
a. [x ] An entire facility
b. [ ] Part of a facility.
Technical Genteel 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
SIC Cede (4 digit}
3.5 .2911
3.6
Degrees
030
6. NA
Latitude Minutes
14
c.
Seconds
36
Dun & Bradstreat Number(s)
3.7 . 00-842-7692
EPA Identlfleatun lsiumber<s) (RCRA I.O. No.)
3.6 .LAD990683716
3.9
NPDES Parmit Numbar(s)
.LA0003026
Receiving Straame or Water Bodies (enter one name per box)
..Bayou Verdine
Telephone Nwnber (include
.318-491-5599 ,
Telephone Number (toctudp area code)
318-491-5222
d.
Degrees
093 NA NA NA b. NA
.
Longitude Minutes
16
Seconds
20
3.10
d.
Undergruwu traction Well Code (UIC) IdentHicaticyt Number(s)
aUA
EPA Form 93S0-1 (1-89) Revised--Do not use previous versions
SAL 000005743
(Important: Type or print; read instructions before computing form.)
CrA/> r-nA
O'
Repa form
PART II, OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTWt)
1.1 POTW name
NA
Sires! Address
...................
1.2 FOTW name Street Address
City
Cotetty
City
Stats
Zip State
Paoa 2 of s
(This space for your optional usa.J
County zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WhfCH WASTES ARE SENT ONLY FOR RECVCUNG OR REUSE).
2.1 Otf-slta location name
BFI
EPA Identification Number (RCAA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
Cotatty
Calcasieu
Slate
Louisiana
zip
70664
1* location under control of reporting feetttty or parent company?
2.2 Off-pslte location name
NA
EPA Identification Number (RCRA D. No.)
Street Address City State
County Zip
is location under central of reporting facility or parent eompenyT
[ 1Y-*
[ ]v
(U
2.3 Off--slto location nama EPA Identlficatton Ntanbsr (RCRA O. Na.)
2.4 Off-slto location nama EPA tdemltteatton NMaer (RCRA D. No.)
Street Address
Street Address
City
CaMy
City
Coaly
State
Zip
State
Zip
Is location trtder control of reporting fedUty or parent eompany7
2.S OM-sita location nama
[ ]v,, I u
Is location under control of reporting fadUiy or parent company?
2.6 OH-sita location nama
[ ]v,,
[ ]*
EPA Identlfieatipn Number (RCRA O. No.)
EPA Idamlticaiion Number (RCRA D. No.}
Street Address
Street Address
City
Cotetty
City
County
State
Zip
State
Zip
t location under control of reporting facility or parent company?
is location under control of reporting facility or parent company?
( ] Y*
[ ] No
______________________________________________________________[ ,lv-
[U
[ ] Check If additional pages of Pert 1 ere attached- How nunyt
EPA Form 9350-1(1-89) Revised--Do not use previous versions-
SAL 000005744
(Important: Type or print; read instructions before completing form.)
PDA 'O' Crn
epa form r
PART III. CHEMICAL--SPECIFIC INFORMATION
u Page 3 of 5 (Thii space for your optional use.)
1. CHEMICAL IDENTTTYIDo not complete tN section If you complete Section 2.)
LI 1.2 1.3 1.4
(Reserved) CAS Number (Enter the mender exactly a* it appear* eh the 313 list. Enter NA II reporting a chemical category.)
108-88-3
Chemical or Chemical Category Name (Enter ew name exactly at it appaar* an the 313 w*t.)
Toluene
Generic Chemical Name tCompleie only n Fart t, section l.l it Cheeked *Yea.* Generic name muat be structurally descriptive.)
MIXTURE COMPONENT IDENTITY tDo not complete this section If vou complete Section 1A ^ 2. Generic Chemical Name Provided by Supplier (Until the name to a maximum at TO character* (e.g.. numbers, letters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY {Check al that aootV.I
Manufacture the chemical:
3.1
rt a. IX J Produce
If produce or Import: Fy 1 For on-eite J use/prooeseing
.T *-l
1 For sale/ J distribution
b. [ ] Import
e,[ ] As a byproduct
f. [x 3 As ian Impurity
Process the 3.2 chemical:
rx 1
rmme+Mnt
a. lA J As a reactant
d. [ ] Repackaging only
h f 1 As a formulation b.l J component
f 1 As an article e.l J component
3.3
Otherwise use the chemical*
[ 1 As a chemical * l i processing aid
. f 1.
. ,,___. _
b.l 1 As a manufacturing aid
f1 c.l J Ancillary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME OURING THE CALENDAR YEAR
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Relaase (bs/yr)
You may report releases of less than 1,000 fee. by checking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-4M 500990
A.2 Enter
Estimate
S.1 Fugitive or non-point air emissions
5.1a [][][]
41,000
5.2 Stack or point air emissions
5.2a [][][]
5.3 Discharges to receiving ... la 1 streams or water bodies *-3-i l--1
(Enter letter code from Part i Section 3.10 tor stream!*) in
the box provided.)
j] 5-3.2 I
5-3-3 n
5.3.la [][][]
5.3.2a [][][]
5.3.3a [][][]
14,000 39
NA
B. Basts of 1 Estimate l (enter code)!
5.1b Q 5.2b G3 5.3.1b QD 5.3.2b 0
5.3.3b O
5.4 Underground Injection 5.5 Releases to land
5.5.1 Orv-slte landfill
5.5.2 Land treatment/appiieaUon farming
5.4a [][][]
5.5.la [][][] 5.5.2a (][][]
NA NA
0
5.4b 1 1| 5.5.1b 1 11 5.5.2b Q
5.5.3 Surface impoundment
5.5.4 Other disposal
S.S.Sa [][][] 5.5 4a (][][]
NA NA
s.s.sb o! S.5.4b Q
[ ] (Check it Additional information is provided on Part IV-Supplamental Uiformatiorv)
PA Form 9350-1(1-891 Revised--Oo not use previous versions
0000051*5
stf-
u
(Important: Type or print; read instructions before completing form.) ,
EDA
epa
PART III. CHEMICAL-SPECIFIC INFORMATION {continued)
page 4 of s
(This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of lets than 1.000 to*. by cheddnq ranges under A. 1. (Do not use
both A. 1 and A.2)
A. Total Translate (tw/yr)
A.1 Reporting Range*
0 1-409 S00-909
A.2 Enter Estimate
B. Bests of Estimate (enter code)
Oteeherge to POTW
r--.
(mar Meatier* number 6.1.1 from Part , Section
I \
.1I ' } |___j
[][][]
HA
6.1.1b
Otf*ar off-tHe toeetlen r---,
- - , (enter leeetion number | 9 ( 1 6.2.1 from Part 1, Section 2.11 2 j-|
J [](]{]
HA
6.2.1b n
Other ott-eUe toeatton . . , . (enter location number 1 9 1 | 6.2.2 from Part l. Seetten2.il *1-1
1[
1t
I f -1
6.2.2b
Other otf-*lte location ---- ...J <enter location ntanber j 91 | T f 6.2.3 tram Pert *, Section2.) 1 2 M II
1f 1[
1r Jl
1 J
6.2.3b fj
[ ] {Cheek if addMonal information is provided on Part IV'Supplemental Information.)
C.Type of Treatment/ Olsposai
(enter code)
6.2.1c |m| | | 6.2.2c |m| | | 6.2.3c M| |
7. WASTE TREATMENT METHOOS AND EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of
Influent Concentration (enter oode)
D. Sequential Treatment?
(cheek If apptcable)
7.u
a
7.tb
lB I1 1 M
7.1e Q
7.10 [ ]
7.2a
Q
7.2b
|B (l | l|
7.2c QI
7.20 [ J
7.3*
Q
7.36
|A|0 | 7|
7.3c Q
7.30 [ ]
7.4a
Q
7.b
|n|a| 1
7.4*
7.40 [ ]
E. Treatment
Efficiency Estimate
F. Based on Operating Data? Yes
No
7.1#
90% 7"
t 1 [X )
7.2e
100% 7.2,
[ ] [* ]
7.3e
87.5% 7.3,
[X] [ ]
7.4#
% 7-4,
[ ][ )
7.S.
Q
IJ.J..I
7.6.
Q
7sb
LJ.JLJ
7-Sc Q 7.6c Q
7.6d [ ] 7.6d [ ]
7.5# 7.6e
% 7"
[H]
% 76t
Ml]
7,7.
Q
77b
I..J..1..I
7.6.
Q
7.8b
||||
7.7e 7.80 Q
7.7d [ ) 7.M [ ]
7.7# 7.8#
% 7"
[ ]( 1
% 7M
[ 1[ ]
7.9.
Q
7.9b
||||
7.90
7.90 [ ]
7.9e
% 7-9<
[ ]l ]
7.10. Q 7.10b | | | |
7.100 Q
7.100 [ ]
7.10#
[ ](Cheek If additional ^formation is provided on Part IV-Supplementai information.)
% 7.10, [ ] ( ]
6. OPTIONAL INFORMATION ON WASTE MINIMIZATION
'
(indicate actions taken to reduce the amount of the chemical being released from the facftty. See the Instructions for coded Items and an explanation of what information to include.j
A. Type of
Modification (enter code)
0. Quantity of the Cherricaf In Waste* Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
KU
Current reportkig
year (Ibs/yr)
Prior year
(Ibt/yr)
j Or percent . change (
1 1*
ED
EPA Form 9350-1(1-89) Revised - Do not use previous versions
SAL 000005746
(Important: Type or print; read instructions before completing form.)
'S-EPA
EPA FORM R PART fV. SUPPLEMENTAL INFORMATION
Use this section if you need adtftional space (or answers to questions In Pert III. Number the lines used sequenttafiy from fines m prior sections (e.g.. S.3.4, 6.1.2. 7.11)
Page 5 of 5 (This Space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part M. Section S.3)
You may report releases of less than 1,000 K>s. by checking ranges under A,1.
(Do not use both A.1 and A.2)
A. Total Release (fcs/yr)
A.1 Reporting Ranges 0 1-499 soo-oss
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
S.3 Discharges to receiving streams or water bodies
s-5.
(mar tetter cooa from Pan I Section 3-10 (or tum(t) in t 5 the ton provtoed.)
5.3..
. 5.3.
S.3. 5.3..
[][][]
[ II 1 [ 1 [][][]
5.3.
.3.__ bT~l
i-3-_____bQ|s.3.
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS (Pan in. Section 6)
You may report transfers of less than 1.000 fi*s. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Totsf Transfers (tos/yr)
A.1 Deporting Ranges
0 I-4S9 soc
A.2 Enter
Estimate
B. Basis of Estimate
(enter coda In box
provided)
C . Type of Treatment/
Disposal
(enter code In box
provided)
BBPlacharpa to POTW
j j jtwwr eawkp iMi*r i Part I. Gaelton 1.)
(Hill
6.1. o_
Othar off-*Jta location
*9
(aniar location numMr
BO [][][]----------from Part I. Sacttoi 2.)
6.2.
BOOthar oti-ttU location
J aniar location martoar tram Part t. fraction 2.)
[Hill
__ BBOthar
location
antar location nomflar
es; Parts. Sactlon*.J
[][][]
6.2. _
||
. . _6 2
e.z. c|m[ | |
6.2. 6.2. cl Ml |~|
ADOmONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part IH. Section 7)
A. General Wastestream (enter code
In box provided)
B. Treatment Method
(enter code
In box provided)
C. Range of Influent
Concentration (enter code)
O. Sequential
Treatment? (check if
aoofeabto)
E. Treatment Efficiency Estimate
F. Based on Operating
Data? Yes
No
, .a
-1111
,11117. , 7.
7. . Q 7-----------c Q
7. 7.
<[ ] d[ ]
7.______e 7.______e
% 7-
H ]<1
% [* 1 f 1
7- 1 1 1 1 1 7 [ ] [ n j,
----------
7--
7.______e
% 7---
n ti l 1 '[ H ]7. 7. b
7. c Q 7-----------0
7. e
% 7--
n ri7. b
---[ ]7-. = O 7-
7.______e
% 7- <( n ]
0
n
7. .D
LLU77. b | | | |
[ ]7. e <---------0
7.______e
Q 7----[ ]7- c
7.______e
% 7- '[ n ] % 7-t ][ i
- * 7- >MM ' > 1]
Q ]7. c
7. d[
7.______e
7. Qc 7----d [ ] 7. e
% 7- <[ it i % 7- '[ n ]
EPA Form B3S0-1 (1-69) Revised--Do not use previous versions.
SAL 000005747
(Important: Type or print; read instructions before completing form.)
Form Approved OM8 No.: 2070-0093 Approval Explras:---1121.
Paoo t of S
EPAO'
U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning end Community Rght-to-Know Act of 1936, also known as Title HI of the Superfund Amendments and Raauthorizatlon Act__________
EPA FORM
R
PART I.
FACILITY IDENTIFICATION
INFORMATION
(This space for your optional use.)
ftAMe reporting burden tor this
eotlacUanbt MermUen ts mimuim to
vary (ram90 to 34 hour* par erponri.
with an {average of 32 hours par
rasponao. Including ttma tor renewing instructtom, amihinp existing ui*
ouroaa, gathering and maintaining tha
eau nssnsa. and completing and
reviewing P*> ooHocilon ot Marmation. Sand eonananu cogerdtnQ tM* burden
catenate Sr any other aapaet ot this
eottaettan at Mformelion, inetudlng
eogasttona tor caddUnqtMa tureen. to
Chwt. formation Policy Branch
(PM 229), US EPA. 401 M St.. SW,
WasMngleh. O.C. 20460 Attn: TRl
Bcadan and to tha Offica ot Information
and Reguitatory Affairs, Otfioa ot
Management and Budgat Paperwork
Reduction
Project
(207H-OOH3).
Washington. O.C. 20600. ______________
1.1 Are you claiming the ehamieai Identity on page 3 trade sacral? -
1.
[ ] Yes (Answer question 1.2;
f No fOo not answer 1.2;
Attach substantiation terms. I
Go to Question 1.3.1
1.2
tt "Yes* In 1.1, Is this espy: [ ] Sanitised [ junaanttlsad
1.3 Hsporting Year 19.S3.
2. CERTIFICATION (Read and sign after completing all sections.) < hereby certify that I hava reviewed tM attached documents and that, to tha bast el my knowledge and ballet, tha submitted Mamuibn is true and complete and that tha amounts and values in this report are accurate based on reasonable estimates using data available to tha {preparer* ot this report.
Name and official title of owner/operator or senior management official
Don R. Unruh, Re finery. Manager
Oat* ibrad.
3. FACILITY IDENTIFICATION Facility or Establishment Name
Conoco Lake Charles Refinery
WHERE TO SEND COMPLETED FORMS:
1. U.S. ENVIRONMENTAL PROTECTION AGENCY
Street Mdrsn
Old Spanish Trail
3.1 City
Westlake
State
Louisiana
P.O. BOX 70266
WASHINGTON, DC 20024-0266
County
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
Zip Code
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
Tble report oontalne Information (or (Check one); 3.2
1A Jfv 1 An entire facility
Jf 1
b. [
Part ot a faculty.
Technical Contact 3.3
Brandt Butler
PubUe Contact 3.4
Don R. Unruh
3.5 SIC Code (4 dfeit)
.2911
b. NA
Latitude
3.6
Degrees
Mirutes
030
14
&Dun Bradstreet Nurtwr)
3.7 , 00-842-7692
.
Seconds
36
EPA Identification Numbers) (RCRA I.O, No.)
3.8 .LAD990683716
NPOS Permit Number(t)
3.9 .LA0003026
Receiving Streams or Water Bodies (amor one name par box)
aJJayou Verdine
TeMphone Number (Include area code)
318-491-SS99
Telephone Number (inchips era# cade)
318-491-5222
d.
Oagrees
093 b. NA b. NA b. NA
NA
a.
Longitude Minutes
16
f.
Seconds
20
3.10 c.
d.
+.
Underpound h)eclbn Weil Code (UIC) tdentificalion hhanber(s)
3.11 .NA
4. PARENT COMPANY INFORMATION
Name ot Parent Company
4.1 E.I. DuPont de Nemours
4.2
Parent Company's Dun 6 Bradstreet Number
00-131-5704
ERA Form 9350-1 (1-89) Ravtsoo--Do not us previous versions.
f. b.
SAL ooooo5-r
(.Important: Type or print; read instructions before completing form.)
EPA
EPA FORM R
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
. PUBLICLY OWNED TREATMENT WORKS (POTWs)
Pape 2 of 5 (This spate for your optional use.)
City State
County Zip
City State
County Zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT LOCATIONS TO WHCH WASTES ARE SENT ONLY FOR RECYCLING OR REUSE).
2.1 Off-site location name
BFI
EPA Identification Ntanbar (RCRA O. No.)
NA
Street Address
Cities Service Hvy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
k location under central of reporting facility or parent company?
| [ ]ve* [xl1**
2.2 Off-site location name NA
EPA IdanlHieetien Number (RCRA O. No.)
Street Address
City
County
State
Zip
IS location undar control of reporting faetUty or parent company?
tU
[
u
Off-tUe location name
2.4 Off-slte location name
EPA Identification Number (RCRA C. No.)
EPA Identification hfcenbar (RCRA *5. No.)
Street Address City
County
Street Address City
County
State
ZIP
State
Zip
Is location under control of reporting ladlily or parent company?
2.S Olf-stie location name
[ ]ve*
[ ]no
Is location under control of reportmg facility or parent Company?
2.6 Ofl-*Ue location name
[ ]
[u
EPA Identification Number (RCRA D. No.)
EPA Identification Number (RCRA D. No.)
Street Address
Street Address
City
County
City
County
Stale
Zk> State
Zip
ocatlon urwier control of reporting facility or parent company?
[ ] Ves
[ ] No
t location wider control of reporting facility or parent company?
[ 3 Yes
[ ] No
[ 1 Cheek It addilionei pages of Pert ere ittektd. How mwtyT
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000005749
(Important: Type or print; read instructions before completing form.)
&EPA
REPA FORM
PART III. CHEMICAL-SPECIFIC INFORMATION
Pag 3 of 5 {This apace for your optional use.)
1. CHEMICAL tOENTfTY(Do not complete this section W you complete Section 2. |
1.1 {Reserved]
CAS Number (Enter the number exactly at It appears on the 913 Oct. Enter NA it reporting a chemical category.)
1.2 95-63-6
1.3 1.4
Chemical or Chemical Category Name (Enter the name exactly as it appears an the 30 list )
1*2,4 - Trimethylbeazeue
1.1Generic Chemical Name (Complete only if Par? l. Section
* Checked 'Yes.' Generic name must be structurally descriptive.)
MIXTURE COMPONENT IDENTITY (Do not complete this section If you complete Section 1.) .2. Generic Chemical Name PnwMefl by Supplier (Limit the name to a maximum pt 70 Characters (e.g. numbers, tetters, spaces, punctuation).)
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that apply.)
Manufacture the
If produce or Import:
chemical: 3.1
ri a.lX ] Produce
f y 1 For on-site
F.lA J use/processing
.f
1 For sale/ 1 distribution
b. [ ] Import
e.[ ] As a byproduet
f.[^]As an impurity
Process the chemical: 3.2
[vl
. __,,
a. 1* J Aa a reactant
d. [ ] Repackaging only
. f 1 As a. formulation
b.l J component
f 1 As an article c.l J component
3.3
Otherwise use the chemical'
f 1 As a chemical J processing aid
J 1.
_
^
b.L J As a manufacturing aid
f1 c.L J Ancillary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE
S. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (Ibs/yr)
You may report releases of less than 1.000 tos. by cheeking ranges under A.1. (Do not use both A.1 and A.2)
A.1 Reporting Ranges
0 1-499 500-999
A.2 Enter
Estimate
5.1 Fugitive or non-point air emissions
5.1a [][][]
8,400
5.2 Stack or point air omissions
5.3 Discharges to receiving
[T|
streams or water bodies 5-3-' Ui-J
(Enter latter code from Pert t
Section 3.10 for treem() in
the box provided.)
li
5.3.2 1___)
05.3.3
S.2a [HIM $.3.1a [][][]
S.3.2a l ] l ] l ]
5.3.3a [}[][]
170
39 NA
5.4 Underground ln)eetion 5.S Releases to land
5.5.1 Oo-slte lendfllf
S.4a [Hill 5.5.1a [](][]
NA NA
5.5.2 Lend tre<ment/appilcetian terming
S.5.2a [][][]
0
5.5.3 Surfece impoundrnant 5.5.4 Other dispoeel
5.5.3a [][][]
S.5.4a [][][]
NA NA
[ ] Chock M additional inlormatKan s provided on Part fV-SuopJementel Information )
8. Basis of ] Estimate i 1 (enter code)]
5.1b 5.2b
0
[H
5.3.ib GO
C. % From Stormwater 5.3.1c NA
5.3.2b
5.3.2c
5.3.3b 1 1
0;s.4b
5.5.1b 1 I1
5.5.2b 0 1
5.5.3b 0
05.5.4b
1
EPA Form 9350-1(1-89} Revised--Do not use previous versions
SAL 000005750
(Important: Type or print; read instructions before completing form.)
6 EPA
EPA FORmR
PART III. CHEMICAL-SPECIFIC INFORMATION
(continued)
____________ _______________Page 4 of s (This spado for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1.000 lbs. by checking ranges under A.1. (Do not use
both A.t and A.2)
A. Total Tramifers (bs/yr
A.1 Reporting Ranges
o i-*ee soo eee
A.2 Enter
Estimate
8. Basis of Estimate (enter code!
Oitehtfoi to POTW ...--, r -
(smer location number j , | I 6.1.1 from Part 1. Section l.l I'M
1 [][][)
NA
6.1.1b
Other o-*lte location
_ _ . (enter location number 1 9 1 1
6.2.1 UnPani. Sectton 2.1 )
___]
flllll
HA
6.2.1b O
Other
location ,____. .. --.
. . . (enter location number I * 1 1 6.2.2 from Part 1. Sections.) 1 .J-l _ J
[
Other off-eite location , , - . J (enter location numbar ( .1 T 1 T 6.2.3 from Part 1. Section2.11 *)! II
i[ 1f 1[
ir i
tr j|
1 J
6.2.2b 6.2.3b 1 1
[ ] (Chock If addfttonal Information Is provided on Part IV Supplemental Information.)
C.Type of Treatment/ Disposal
i _ (enter fan/4*)
6.2.1c lMl 1 1 6.2.2c M -- 6.2.3c |m ~3
7. WASTE TREATMENT METHODS ANO EFFICIENCY
A. General Wastestream
(enter code)
8. Treatment Method
(enter code)
C. Range of Influent Concentration (enter code)
D. Sequential Treatment? (check If
appleabie)
E. Treatment Efficiency Estimate
F. Based on Operating
Data? Yes
No
7.1a
0
7.1b
rm
7.1c
7.1d [ ]
7.1e
95 % 7-If
[ 1 [ XT
7-2a
0 7.2b
F'i in
07.2c
7.Jd [ ]
7.2e
100 % 7.2f
[ 1 [X1
7.3a
0 7.3b
ft on
7.3c
7.*. [ ]
7.3#
87.5 % 7.3f
( xl t 1
7.4a
7.4b
1 4*1 1
7.4c
7.4d [ ]
7.4e
% 7.4f
[ ][ 1
7.5a
7.5b
M II
7.5c
7.Sd [ ]
7.5e
% 7.Sf
[ ]( ]
7.6a
*<*>
1111
7.6c
7.6d [ ]
7.6e
% 7.6f
[ 1[ 1
7.7a
7-7b
|| | |
7.7c
7.7d [ ]
7.7e
% 7.7f
[ 1[ ]
7.6a
7.8b
||||
L1..U7.9a
7-9b
7.6c
7.9c
7.8d [ ] 7.9d [ ]
7.8e 7.9e
% 7.8f
111]
% 7.9f
[ 1[ 1
7.10a
7.10b | | | |
7.10c
f1
7.10e
[ ] (Check If addftionai Information Is provided on Part IV-Supplemental information.)
% 7.10f 11(1
a. OPTIONAL INFORMATION ON WASTE MINIMIZATION
(Indicate actions taken to reduce the amount of the chemical being released from the facSty. See the Instructions for coded Items and an explanation of what Information to Include.)
A. Type of
Modification (enter code)
6. Quantity of the Chemical In Wastes Prior to Treatment or Disposal
C. Index
D. Reason for Action (enter code)
Current reporting year (Ibs/yr)
Prior year (Ibs/yr)
Or percent change
M
EPA Form 9350-1(1-89) Revised - Do not use previous versions
SAL 000005751
(Important: Type or print; read instructions before completing form.)
oEPA
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need additional space for answers to questions in Part HI. Number the ines used seguemialy from flnes In prior sections (e.g.. 5.3.4. 6.1.2. 7.11)
Page of 5 (This space for your optional use.)
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part 111, Section S.3)
You may report releases of less than -1,000 bs. by checking ranges under A.1.
(Do not use both A.1 and A.2)
A. Total Release (B>s/yr)
A.1 Reporting Ranges 0 WW 500-009
A.2 Enter Estimate
S.3 Discharges to
,--.
receiving streams or waterbodies
II S.3--------L_1
5.3_____* [][][]
B. Basis of Estimate
(enter cod* in box
provided!
C.% From Stormwater S.3______n
S.3______ c
(Enter letter code (ram Pen l
{1
Sectton 3. lO lor tvwm(d in c e
11
the bow provided.)
a.3.-- --i
S.3_____*
[][][]
A rtRITlPtsi a i IS keAAs 4 *
S.3_____a [][][]
S-3.____tQ 5.3._____c
-Q - --_____-
You may report transfers of less than 1.000 be. by checking ranges under A.1. (Do not use
both A.1 and A.2)
A.Total Transfers (bs/yr)
A.1 neportbg Ranges
0 1-4SS SCO SOS
A.2 Enter Estbnate
Disehwge to POTW
_ , (enter location number 1 , I 1 6.1._____from Pert A Section 1.) 1 1 !!
| 1
[][][]
Other (t die location
e-2-______XttSfiftZSXZi L3Q
Other eff-ahe location p -i t >
6.2.
(enter location number 1 t
1
----------from Pan 1. Section 2.) 1-------M____1
Other off alto location r--^ ..
en
fontor location nunWor 1*11 |
*z-----------from Part A Section 2.>1 *1 1 1
[][][] [][)[] [][][]
B. Basis of Estimate
(enter code In box
provided)
6.1._____b Q
6-2-_____b j |
6.2._____b n
6.2.______b d]
C. Type of Treatment/ Disposal
(enter code In box
provided)
S.J._c|M| | |
6.2.
c|m| | 1
6.2. c|Ml | |
ADOmONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part ML Section 7)
A. General
Wastestream (enter code
In box provided)
B. Traatment Method
(enter code In box provided)
C. Range of
Mhient Concentration (enter code)
D. Sequential
Treatment? (check If aooleablel
E. Treatment Efficiency
Estimate
F..Based on Operating Oata 7
Yes
No
7. , f-]
- rn i7 --
7.
eQ
7-----------d[ ]
7.
% 7- [ ][ ]
7. . 7- b | | ||
-[ ]7. e [] 7-----------
7. e
% 7- ' [ ] f ]
7. .Q
1 I 1 17-_*
7- _<= 7.
d[ J 7.
e
% 7 -[ H 1
7. . Q
- rm
-I ]7- c
7-----------
7. e
%7
-l H 1
7. .D 7. b | | | |
7.> l_LJ I
* 7-----------
7-
bill!
7-_c
7. c Q
Q7-_______c
7-----------d( ] 7. d[ ]
7. ,,[ ]
7. 7. 7.
e e e
[% 7--- If ] * 7 '( H ] % 7- 71 It ]
7--* 7* 7.
b||| | rb 1 1 1
7- = 7. d[ ] 7. e
]7. c
7. d(
7. e
% 7 <[ H 1 % 7 <A It 1
EPA Form 9350-1(1-69) Revised--Do not use previous versions.
SAL 000005752
(Important: Type or print;, read instructions before completing form.)
Form Approved OMB No.: Approval Expires:
2070-0093 01/91
Page 1 of S
S-EPA U.S. Environmental Protection Agency
TOXIC CHEMICAL RELEASE INVENTORY REPORTING FORM
Section 313 of the Emergency Planning and Community Rlght-to-Know Act of 1966.
aiso known as THie HI of the $ts>erfund Amendments and Reauthorization Act
EPA FORM
R
PART I.
FACILITY IDENTIFICATION
INFORMATION
{This space for your optional use.)
F*uWtc reporting bureon tor true collection at information Is estimated to vary from SO to 34 ne<^response, with
time lor reviewing
searching existing data
. w tthertno end maintaining the date neaped, and completing and
revieednq the ooileellen of formation
Send comment* regarding this burden estimate or any ether maspect of this edteetlen el Vtiermaiian. Including
suggestion* tor reducing Ihls burden, to Chief, information Policy Branch
(PM-223). US CPA. 40t M St.. SW. Washington. O.C. 20460 Attn: TRl Burden and te the Office of Information
end Regulatory Affairs, Olfice of
Management end Budget Paperwork
Reduction
Project
(2070-0093).
Washington, O.C. 20603.
1.1 Are you claiming the chemical Identity on page 3 trade secret?
[ 1 Ye* (Answer Question |.2;
f ^ 1 No (Do not answer 1,2:
Attach substantiation forms, |
Go to oueslton t .3.)
1.2 tf *V#s* in t.t, is this copy:
1.3 Reporting Year
19 88
2. CERTIFICATION (Read and sign after completing afl sections.) I hereby oertily that I have reviewed the attached documents and that, to the best of my knowledge and belief, the submitted information is true end complete and that the amounts end vatuea b this report are aecurete bated on reasonable estimates using data available to the preparer* ol this report,
Name and official title of owner/operator or senior management official
Don R. Unruh, Refinery Manager
Signature
X
IfTry^
3. FACILITY IDENTIFICATION ' Facility or Establishment Name
Conoco Lake Charles Refinery
wncnc iu oenu v/umrixicu runivib.
1. U.S. ENVIRONMENTAL-PROTECTION AGENCY
Street Address
Old Spanish Trail
3.1 City
Westlake
Louisiana
P.O. BOX 70266
WASHINGTON. DC 20024-0266
Cotaity
ATTN: TOXIC CHEMICAL RELEASE INVENTORY
Calcasieu
2. APPROPRIATE STATE OFFICE (See instructions
70669
Appendix E)
This report contains Information for (Check one):
<
JS. An entire feeillty
-
[ Jb. Pan of a facility.
Technical Contact 3.3
Brandt Butler
Public Contact 3.4
Don R. Unruh
SIC Coda (4 digit)
3.S .2911
*. NA
c.
3.6
Degrees
030
Latitude Minutes
14
3,7
Dun 6 Bradstreet Numberfs)
. 00-842-7692
EPA Identification Number(s) (RCRA l.O. No.)
3.8 ,LAD990683716
Seconds
36
NPDES Permit Number(s)
3.9 .LAQQ03026
Receiving Streams or water Bodies (enter one name per box)
a3ayou Verdine
Telephone Number (Include area code)
31 8--491 -5599,
Telephone Number (include wm code)
318-491-5222
d. Degrees
093 b. NA b. NA b. NA b. NA
e.
Longitude Minutes
16
f.
Seconds
20
3.10
d.
Underground traction Weil Code (UiC) Identification Nun*>ar(s)
3.11 .NA
PARENT COMPANY INFORMATION
Name of Parent Company
4.1 E. I. DuPont de Nemours
Parent Company' a Om A Bradstreet lWnber
4.2 00-131-5704
EPA Form 9350-1 (1-89) Revised--Do not use previous versions.
t b.
SAL 000005753
(Important: Type or print; read instructions before completing form.)
a rna
tPA
REPA FORM
PART II. OFF-SITE LOCATIONS TO WHICH TOXIC CHEMICALS ARE TRANSFERRED IN WASTES
1. PUBLICLY OWNED TREATMENT WORKS (POTW*)
1.1 POTW name
NA
Street Address
1.2 POTW name Street Address
City
County
City
Sleie
2ip State
Paqa 2 of s (This space for you* optional use.)
Courtly Zip
2. OTHER OFF-SITE LOCATIONS (DO NOT REPORT locations to wmch wastes ARE SENT ONLV for RECYCUNG OR REUSE).
2.1 Olf-slte location name BFI
EPA Identification Number (RCRA O. No.)
NA
Street Address
Cities Service Hwy at 1-10
City
Sulfur
County
Calcasieu
State
Louisiana
Zip
70664
Is location under control c< reporting lacttfty or parent company?
2.2 Off-site location name
NA
EPA tdentificattoA Number (RCRA . No.)
Street Address
City
County
State
Zip
Is location under control of reportIno facility or parent oompany?
[ ]ve* [x]
[ 3 3Yes
[ No
2.3 Off-site location name EPA tdentllicalion Number (RCRA O. No.)
2.4 Off-elte location name EPA tdantifteatton twmber (RCRA O. No.)
Street Address
Street Address
City
County
City
County
State
Zip Slate
Z4
Is location under control ot reporting facility or parent company?
2.5 Oft-site location name
[ ]v [ ].
is location under control of reporting facility or parent company?
2.6 OH-sIte location name
[ ]v,,
[ ].
EPA identification Number (RCRA O. No.)
EPA identification Nivnber (RCRA . No.)
Street Address
Street Address
City
County
City
County
Slate
Zip State
Zip
location under control of reporting 1flirty or parent company?
[ ]ves
[ ]no
Is location imder control ot reporting facility or parent Bon^any?
_______________________________________________________________[ ,U
[U
[ ] Cheek If addttionei pages of Pan are attached. itow meny?
EPA Form 9350-1(1-89) Revised--Do not use previous versions.
SAL 000057c,
(Important: Type or print; read instructions before completing form.)
a CDA CrM
EPA FOHM ^ PART III. CHEMICAL-SPECIFIC INFORMATION
u
Page 3 of 5
(This space for your optional use.]
1. CHEMICAL lDENTITY(Do not complete this section If you complete Section 2.)
1.1 1.2 1.3 1.4
[Reserved] CAS Number (Enter the number exactly as it appear* n the 313 list. Enter NA It reporting a chemical category.)
1330-20-7
Chemical or Chemical Category Name (Enter the name eaactty a* it appear* on tne aia Ust.)
Xvlene
Generic Chemical Name (Complete only it Part 1, Section' 1 1 is checked 'Vet.* Generic name must be Structurally descriptive. 1
MIXTURE COMPONENT IDENTITY (Do not complete this section If vou complete Section 1.) 2. Generic Chemical Name Provided by Supplier (Limit the name to a maximum el 70 characters (e.g.. numbers, letters, spaces, punctuation). ]
3. ACTIVITIES AND USES OF THE CHEMICAL AT THE FACILITY (Check al that aocrfv.l
Manufacture the chemical:
3.1
r1
Ja. 1X Produce
tf produce or import: f v 1 For on-ette
c.L A J u*e/processlng
.\
1 For sale/ i distribution
jb. [ Import
e.[ ] As a byproduct
f.[ x 1 As an Impurity
Process the 3.2 chemical:
fY1
___k
a* * J As a reactant
d.( ] Repackaging only
J. f y 1 As a formulation
b.[ component
Jf 1 As an article
c*l component
Otherwise use
3.3 ..
.
,
the chemical:
f 1 As a chemical a.l J processing aid
.f 1
^
b.l J As a manufacturing aid
f1
_
e.l J AncNary or other use
4. MAXIMUM AMOUNT OF THE CHEMICAL ON-SITE AT ANY TIME DURING THE CALENOAR YEAR
5. RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE
A. Total Release (fes/yr)
You may report releases of less than
1.000 toe. by checking ranges under A.l. (Do not use both A.l and A.2)
A.l Reporting Ranges
0 soo-ew
A.2 Enter
Estimate
S.1 Fugitive or non-point air emissions 5.1a (][][]
51,000
S.2 Stack or point air amissions
5.2a [][][]
5.3 Discharges to receiving c
1k}
streams or water bodies 5-3-1
(Enter letter code from Pert t Section 3.10 for stream(s) in
the box provided.>
Jj
5 3 2 1__ 1
5.3.3 O
5.3.1a [][][] 5.3.2a [][][] 5.3.3a [][][]
5.4 Underground injection 5.5 Releases to land
s.s.1 On-*lte landfill
S.S.2 Land treatmenl/appilcation (arming
5.4a (][](] 5.5.1a [][][] 5.5.2a (][][]
7,700 39 NA
NA
NA 0
5.S3 Surface impoundment
5 5.3a {][][]
NA
5.5.i Other disposal
5.5.4a [][][]
NA
B. Basis of , |
Estimate
(enter code)
5.1b Q 5-2b [j^
5.3.1b [3 5.3.2b O
C. % From Stormwater 5.3.ic NA
5.3.2c NA
5.3.3b O
5.4b O,
5.5.1b
5.5.2b 01
5.5,3b 13'
5.5.4b O'
. 1 (Check. it additional information is provided on Pan IV-S\jpptem*<\t*t tnlprmatiori. )
EPA Form 9350-1(1-091 Revised--Do not use previous versions
SAL 000005755
_ mportant: Type or print; read instructions before completing form.)
oEPA
EPA FORmR
PART 111. CHEMICAL-SPECIFIC INFORMATION (continued)
^ Page 4 of S (This space for your optional use.)
6. TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
You may report transfers of less than 1,000 tos. toy checking ranges under A. 1. (Do not use
both A.1 and A.2)
A. Total Transfers ftos/yr)
A.1 Reporting Ranges
0 1-490 500-009
A.2 Enter Estimate
B. Baals of Estimate (enter code)
Dtechwe* to POTW
-------,
(enter location number 1 .11
$.1. t from Pert 1, Section i.) 1 I-I
,
1 [][][] 1
NA
6.1.1b
Other otf-eite location ---- - _ 4 (enter location number J 2 j 6.2.1 from Pert S, Section2.) ( ._](
t ir
Other otf-eite location . . . - , (enter location number j 2 i 6.2.2 from Part S, Section 2.) 1 l-l
[
i[
fOther off-site location
(enter location number
,] 1
6.2.3 rom Pert L Section 2.) |_J.|
J 1f .J |
1 1
f 1
if
if
1r Jl
] NA
]
1 J
6.2.1b 6.2.2b 6.2.3b
[ ] (Chock If Additional information la provided on Part IV-Supplementai information.)
C.Type of Treatment/ Disposal
6.2.2c |M|
6.2.3c Mi
7. WASTE TREATMENT METHODS AND EFFICIENCY
A. General Wastestream
(enter coda)
B. Treatment Method
(enter code)
C. Range of Influent
Concentration (enter code)
D. Sequential Treatment? (uivviC ii
appleable)
7.1a
0
7.1b
|B|l| H
7.1c
7.,d [ ]
7.2a
0
7.2b
|b|i|i|
7.2c 0
7.2d [ ]
7.3a
0
7.3b
ll A
7.3c 0
7.3d [ j
7.4a
7.4b
V 1*1 1
7.4c
7.d [ ]
7.Se 7.6a 7.7a 7.6a
7.9a
n
7.* 7.6b
7-7b
7.8b 79b
ITT1
||||
|||| |||
CJ 1
7.Sc 7.6c 7.7c 7.6c 7.9c
7.Sd [ ] 7.6d [ ] 7.7d [ ] 7.6d [ ]
7.9d [ ]
7.10a 7.10b |
|
7.10c
7.10d [ ]
E. Treatment Efficiency
F. Based on Operating Data? Yes
No
7.1s 7.2e 7.3a
95 % 7.If 100 % 7.2f 87'5 % 7.3f
[ ][ d l 1 [ *i [x] ( 1
7.4a
% r [ 1 [ 1
7.Ss 7.6a
% 7.Sf
% 7S'
[ 1[ ] [ 1t 1
7.7e
% 7.7f [ 1 [ 1
7.6a
7.9
% 7-
%
[ 1[ ] [ ][ 1
7.10e
% 7.10f l 1 [ ]
6,. OPTIONAL INFORMATION ON WASTe MINIMIZATION
(Indteate actions taken to reduce the amount of the chemical being released from the facflfty. Sea the Instructions for coded Items and an explanation of what Information to Include.)
A. Type of
ModMeation (enter code)
B. Quantity of the Chemical in Wastes Prior to Treatment or Disposal
C. index
D. Reason for Action (enter code)
Current reporting year (fcs/yr)
Prior year (bs/yr)
. Or percent , change
[m
EPA Form 9350-1(1-891 Revised - Do not use previous versions
SAL 0*000057RA
(Important: Type or print; read instructions before completing form.)
ApDA w l-rM
REPA FORM
PART IV. SUPPLEMENTAL INFORMATION
Use this section If you need additional space for answers to questions In Part IK. Number the fines used sequentlaty from fines ki prior sections (e.g-. 5.3.4. 6.1.2. 7.11)
rage & of 5 (This apace for your optional use.)
' 1"
ADDITIONAL INFORMATION ON RELEASES OF THE CHEMICAL TO THE ENVIRONMENT ON-SITE (Part III, Section 5.3)
You may report releases of less than 1.000 t>*. by checking ranges under A.1.'
(Do not use both A.! and A.2)
A. Total Release (tos/yr)
A.1 Reporting Ranges 0 1-499 500-999
A.2 Enter
Estimate
5.3 Discharges to receiving streams or
[][](]waterbodies
j-- ( 5.3--------l__J 5.3_____a
6. Basis of Estimate
(enter code in box1
provided)
5.3______bO
C.% From Stormwater
5.3.
c
(Cnlw Sac(ton
a.
10c(oofrlaifrraoammP(ca)rt*n1
c
3
II 1___1
tha boa providad.)
o.j.----a
_D5.3
[][-][] 5.3_____a
[][][]5.3_____a
5.3.____bl 1 S.3._____c
bC5.3._____
5-3._____c
ADDITIONAL INFORMATION ON TRANSFERS OF THE CHEMICAL IN WASTE TO OFF-SITE LOCATIONS
(Part III. Section 6)
_______
You may report transfers of less than 1.000 k>s. by checking
ranges under A.1. (Do not us# both A.t and A.2)
A.Total Transfers (bs/yr)
A.1 Reporting Ranges
o i-4#e soo-eee
A.2 Enter Estimate
B. Basis of Estimate
(enter code In box
provided)
C. Type of Treatment^ Otsposai
(enter code in box
provided)
_, 5.1.
Otaetiarga to POTW
r . f-t
(amar vacation antar | . 1 | 1
[][][]from Part . Pactton t.) I'M |
6.1._____b O
Othar off--tta location
HQ6-2---
r--t i
i
Othar oTf aha location r---i r--i
6.2.
farMar location ntnOr 1 2 I 1 1
--------from Part 1. Sadton 2.11-------ll__J
Other o*C--aha Vacation r - 6-2-______\tt&SrS32Z.%
[][][] [][][] [][][]
6.2._____b Q 6.2._____b O 6.2._____b C3
6,2._c|M| ( | 6-2. c|m| 1 1 6.2. c|m| | |
ADDITIONAL INFORMATION ON WASTE TREATMENT METHODS AND EFFICIENCY (Part III. Sutton 7)
A. General Waeteetream
(enter code
In box provided)
B. Treatment Method
(enter code in box provided)
C. Range of Influent Concentration
__(enter code)
0. Sequential Treatment?
(check If applicable)
E. Treatment Efficiency Estimate
F. Based on Operating
Data? Yes
l_Q
( 1 7. -[ 1 7.
[H 7. [ H
No
] ]
-<[ 1
7.
.<( H 1
[ ]7. 7. 7. I H 1
7. -"[ 1 7.
[ 1[ ]
7.
1 7. [ 1 7.
-'[ ][ ]
-<( n i
] 7.
(H]
HD 7.
.[ ]
7.
[ ][ ]
EPA Form 9350-1 (1-69) Revised--Do not use previous versions -
sal 000005757
1988 BARA 313 RELEASE ESTIMATION LAKE CHARLES REFINERY
CALCULATIONAL METHODS
Storage Tanks
1. Calculated total VOC loss (breathing and working) using AP-42 correlations.
2. Used Raoult's law and the liquid weight -fractions to estimate vapor weight fractions of specific chemicals.
Product Loading
1. Calculated total VOC loss using AP--42 correlations. 2. Used Raoult's law and the liquid weight fractions to estimate
vapor weight fractions of specific chemicals.
Process Equipment Fugitives
1. Estimated number of sources per unit from L.C. VOC monitoring data and/or published (Radian) study.
2. Used SOCMI emission factors to calculate total VOC emissions for each unit. Used leak/no leak factors where VOC monitoring data were available.
3. Divided the total VOC by the number of "major" streams for each unit. (Heavy streams having no 313 reportable chemicals and contributing little to total VOC were factored out)
4. Multiplied the VOC per stream by the liquid weight fraction of the chemical present in each stream.
5. All relief valves servicing streams with toxic chemical compositions above deminimus were considered to be closed; i.e. , tied into a flare system.
6. Gas valves associated with process heaters and boilers in fuel gas service were subtracted from total gas valves for these units, so that fuel gas fugitives could be calculated separately.
Process Drains
1. Estimated the number of drains from L.C. VOC monitoring data or the Radian study.
2. Assumed 75 "/. are covered based on Lake Charles VOC monitoring data. Also assumed covered drains released 90'/ less VOfc than uncovered drains.
3. Used AP-42 emission factor to calculate total VOC emission from process drains.
4. Assumed crude oil component composition. U. Used Raoult's law and the liquid weight fractions to estimate
vapor weight compositions of specific chemicals.
000005758
SAL
c-j ro
Cooling Tower
1. Used cooling tower circulation rate and AP-42 emission factors to calculate total VOC emissions.
2. Assumed crude oil composition to calculate release of each chemical.
API Separators
1. Calculated total VOC using AP--42 emission factors and refinery wastewater throughput.
. Assumed crude oil component composition for separator oils. . Used Raault's law and the liquid weight fractions to estimate
vapor weight fractions of specific chemicals.
Wastewater Releases
1. Effluent a. Used monitoring data where possible, such as for flowrate and ammonia. (Ammonia was corrected to free ammonia) b. For other compounds, used 1989 effluent analytical data. If no analytical data were available, but the chemical was suspected to be present, data for similar compounds were used.
2. Volatilization Volatilization from wastewater treatment impoundments was back-calculated from effluent release estimates anc| ERA Guidance Document values for treatment efficiency and component volatilization. Volati1ization from other impoundments was based on plant provided information.
Land Releases
1 . Land-farm a. Used landfarm disposal volumes and component analyses to estimate the amount of chemical present. b. Used ERA developed model (Chemdat 6> on land treatment to estimate waste component volatilization. c. If data were not available, analytical and published data for similar compounds were used.
2. Off-site Disposal Disposal records and analytical data were used to calculate component quantities.
3. Impoundments a. Impoundments that receive periodic cleanouts, such ins wastewater treatment lagoons, were not considered in land release totals. b. Releases to 1 and were estimated based on plant, provided* data. c. Leakage to groundwater was not considered a r ol SAL 000005759
1> l
Spills 1. Used spill volume estimate provided by plant. 2. Calculated the amount volatilized using Raoult's law and the
liquid weight -fractions to estimate vapor weight -fractions o-f peci -f ic chemi cals. ssumed all contaminated soil was excavated and stored in a manner
that prevented contact with land; i.e., no land release.
sal
OOO005 ?6q
STanks : Ca/Cc'/c^f'.on ftl&thoA *
/?,P- </2 VOC. x
La ke
frxn Cln^:cal. X
'ft)
P>j cAfiii
py ^
ur
" (O-h&W r <^*\l R&
-ira far'
3^/^p/g- CJc-at^<an *
Be^ln - 235^^0
"yft7^ Vbc /?e^ G^so/.'^e * 0,02*1 W4Fry*^
(T^n k 3^2^32.
fc>n-2
J.S~ p$'<* &n^r
!X GostfJ.'^e
70F)
4 - L37C> 7r Sen-ze^e
J ' -----------------1 1 --"
( re [ea
cv; r-')
SAL 000005761
LofibiH& Loss
L-frke. (Lh^ries*
C^\cAjlach'o*\ Fle+Aooi ;
/}P-^/2 Vbc x
P\/ C-Ay c-nfi-mi
Rv* Cl'ie*vcJ^ x p. V ^'xrtor^
" Raleas^
-ho
4;^
S<a,rKipl<_
r\C.^lcula'LtO '
Ben 7-dn
3^7*1 '/y-- VOC -FryrnX 0.01^ K/f Bhi
{yasoltne <="fy)
* AS P5'v
2 ps.'^\ ffissoi.'joe
6e> 7>~/r)
/A (release. "h> <=i-rj
SAL 00000*5^
Er<]k:C Elinor/$
Process Equipment fugitive Release :
^'a.lo-cjla'/v'otn f^&HlxocX '
&c S<^>cjrc^s_ Urxl-h
^ r\ ,
x $OC(VH -fkcd*r
x
6) " *SAM 3r$5ire^
X vXr -(Vxv-v
3/"*. cher+i`'c.f$
- Ches* ,c ( re.le.cK se
/o
^ 11 r-
S>r+fy\pE_ dcj Ecjlcuj,'at*
* 3 CTTV .g-l/kc.
vbc_ = Ijb^ &v(ooiO + 2 &v(.o<n) * ns ^.ooa)+1 ^Cn)
leak)
LUk)
0
Oetc)
+ 1%\ tfc^.ooosv) ^7^oFCoooiE) C*o le*k.)
+-tS'UPsC'26>)
K- 3 ^SA%) + n^fisC-Otf7)i-7.CSC2o)~[-^x'2.c/^r>c3SZz^
X' --^~rr
3000 /t
- Lp sm sfr~s
-
^
\
(^C-r<j^p/ Crude KJri
My>^i^yCS^\
Ke^se*^ Die^ei
T%zri-
sK
------------------------------
B S^"Z6*i.
/?, 3Z Tpy ^7-7 000 ^Y.0O23-.qo2
V S4r^ yV
^
i/
S~Cp
^.c
.o1<r -I .o/o) -- %76, tk B,,.
^^ AV,AA.
CO L.S. lfc>0 Mo rt i ~fo r-1^ date or /?/. 5oo rep SYoci y
0-) Le^ //Vtf>
Pc\/<?co.<je-
AcYorS
Ar/irs
*&<-
Used oThe^r^;^ t
^oc
(~E)
Bio^-baok- --
C
S4. 000 5763
PROCESS hR/H/VS
dv(
Pi'
(Gh^ries
x^ZW*S
fiP-^Z Fkchx- X 'tp Jr X 365
X Pv
- Cfte^r'c^f /Refe^se
ft, /H'xlure.-
X w+ -frjxry (cr*Jt
3'3
<Pfe ^ .v')
i
P>o *v^(<cl CG\l c^ularj/o
8en-E^e -
73~? o/rQ.'.5 ^ O.on ^ x O.IO + QHS' Jr~.*s ^0,07i
Capped)
(^Vppef)
^*+
*2^
?(*sih x'O.ooixb^^
.*
-- GCl (j> ^/y r
Cte'F)
SAL 000005764
Cpqung Towns'
ClUe\r(f^
Yr
X s~t ~A~x>i H'l'S oUe^ <*(
>c\yw^>/g
^A/cijf^YXoto :
A1*16I C-W,.
-*iC2J^\ Cr*) C I fiefe*i%c_ Civ <*'r^)
e--- -- SS^ ^9-ii* * 0.7 ;5^Tlv*<,'0o?it)
it _.
-
|*ZS
yr~ oe^Z-e^'g
SAL 0OOOO5765
API SEPAR4T&#.
In&rlec,
I(0^ C2uit?C~hIO K\ MetAoJl
F/oi^rofe * /4F-Yz
pVtcj-D,
x ^ F>>, 3 cAe/w/t*/
/>,,
-- <2-tl r^C-iS f Re/fc <=^1
W*
S<zr*p!e^ cjlcu(arf<\
O^i '
6 - 75D
^O^x^x3Fi/'Zfttoc
Kv-i/m
loosed Wiv
* * ao32 - -_n2^e^_
Cre(e*%* "/> <*.Y^
000576s
w/^rE^re^ treatment
ZZ* / 60 la'fiat^ Method *
L~ o J'Cc Oj-t cj (-- / e S
P-lawraE* ^
OAer*''cftf
*nce^'/ri,'f.vofcV
r^ IA/HZ
. efecf/'<a** L,'^/-/- ,'-{
- OAe^.'c^f ^e/2^5^ Efo -----------------------------------------------'
ofe/eofcct)
E-ffEe^f Re(e^s^_ rI -- fye*^ o\Ja { E~^(`'cJ.f\c
^
vvf frx,,
Vol^'zeJ
"% 13 C*n/H .' CA i
= QL ^^'Vca(
fe^sc
Sq^pig. C&lculcd1 Oio
$e>izene
Eefecfec/)
{td.L.)
- 7.7? x lo1l 7!k-r wJV
y
M x io (L Ee
10* ib viv
3*7, & yr
C*~cfe
^T^p)
^,0 ~p>
(ef/^)
I -- 0.95" <?^<^e*cy
~Y<%C>
rvi^x t'n~Pfve*3 f^e^ze^e)
1^0 "yCr7" B5ee/t^oZEeHne >< O.Jl^ wf -frw voj<*i~`ze.cl
^7 y-^t2 ifol^i'zeA
( Celpc <^c
~i-
>-l
V** /"
S4(. 6oooS76t
LtrtD Release
c (c-Lj l c\i % o
MertioA '
5L.&. k'Q, CH(^c\ rl e
L-j>
w^sfe dPuc>Ly\~('Hi
{3w*^\pec(
r
*
3/-S C. A^vt /c** (
O* nC&iiT^ -f>o *
Che^c^-l fn
/<e/gA.5e ^
rw'
d-h)
l^^d ^
X VvV',
^ _ Vo l^*/,_ C/n Ctvi .'ca / Rp((?c,$^
73e*e~w
s. K-l
O^KlT-erve
-^7/
i^,
" Z&)M1?
^
+*>*$
'"**>+<. *
"2/500 /4?
^30/6
^ jo^'/V wqsY-e
3e^>, Slu^e)
^ O, ^03 Valii~'Z.-id. i* a-K -- 2-S /^?
S;,L 6O0oi78
1788 SARA 313 REPORTING RELEASE INVENTORY
LAKE CHARLES REFINERY
ALUMINUM OXIDE
SOURCE
AMOUNT RELEASED <1b/yr)
AIR POINT RELEASE FCC Stack Release
44,000.
AIR NON-POINT RELEASE HDS Catalvst handlina
910.
TOTAL AIR RELEASE
44,910.
WATER RELEASE
N/A
LAND RELEASE On-Site Off-Site <BFI Landfill)
N/A 1,100,000.
'/. OF TOTAL RELEASE TO MEDIUM
98
2 100
SAL 000005769
198S SARA 313 REPORT WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
ALUMINUM OXIDE
GENERAL WA3TESTREAM
GASEOUS
TREATMENT METHOD
MECHANICAL SEPARATION
TREATMENT EFFICIENCY
RANGE QF INFLUENT CONCENTRATION
0.017.-1*/. (a)
GASEOUS
ELECTROSTATIC PRECIPITATOR
99.97. (b)
(a) <b>
Based on Ponca City calculation and the -fact that Lake Charles is slightly larger (per Brandt Butler). a.+taol*cl J
Based on manufacturer data (per Brandt But1er,sequenti al treatment with mechanical separation).
SAL 000005770
Made By_____________
Checked 8y___________
Date_______________
Page_______
of
Title
Conoco Inc. Calculation Sheet
Job No.
Reid State
SAL 000005771
f?ELE4SE CALCULATIONS
Al(-Jns\ iV\
Oxi^d
t.C.
m
Rw fiefgase
- ^ Tpy o^/ysP *
x 0.55- 4/J*}
CFCC Rej^ercO-or S+^dP) =
Ooo It . fij Q
Y r* '''7X5
3*5' 5
$&.(&*&.
<0^ / c o / c, */*/ a n 5
(by
<0
^^'Ty'y)
/Vo^ ~po
^cf6A.$6
/ffos C**.*/
' =xl (2>lo\sJ c\ Wa. y
r* /
y I ? HOS o^;-k, {o,S7
X O.........V.....4.. "dlzf.la<^3*>jl jo
^
lOO lb CCii lo^ ,
-- X
Qa.~h <MXp
- ............V4/ >V145*1
/yr
r^cnfU (c* \,a ry
(3) 2) f Oi)
xO,?7^Ccri uS^e
+0,<tZf'Z*\o
- ^1H K,',%- r
Xo-)
$c\$ i <5 - IZiOjl neCr'iij E-5'/'
Release
= A/ /R
(4f7o. 2^ 3
iPsoloPe
=?
flo
(5")
w<n~<ir . sR^s ^
r
wll seiile ocjf
/-/M/d ,
C s ee /fp?p X F- Sol .of UXsfe O*Release.
^ per Sm^4f cW7er
<?/)
LZ) FCC//^/)S
COwpO^W/a^ XX
^
^
by 5Xi/e_
(X L.c. cX os-^e.
peX
Fe-fy
L/oyJ LV.^e.r- X^C
^J
Cs) per~ ELP4 $Atf *$ /3 &U ReX ic A'
( Es+,'saf.'nc} fe/e*S's", pX XWc /r^XrX E'tf-'c-if
bffy & ~ CPo^ c-I / PA ys r CCl i
' e 'r C&JSAL 000005772
!
SOURCE
1988 SARA 313 REPORTING RELEASE INVENTORY
LAKE CHARLES REFINERY
AMMONIA
AMOUNT RELEASED (lb/yr >
AIR POINT RELEASES
AIR NON-POINT RELEASES Fugitive Equipment Loss CTU <#2,#3) Inhibitor Wastewater Trtmt
Total Non--p_oi nt Rel ease
TOTAL AIR RELEASE
N/A
410. 1752. 2162.
(2200)
2162.
WATER RELEASE
3117. (3100)
LAND RELEASE
N/A
7. OF TOTAL RELEASE TO MEDIUM
19 81 100 100
SAL 000005773
19S7 BARA 313 REPORT WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
AMMONIA
GENERAL WASTESTREAM
TREATMENT METHOD
TREATMENT EFFICIENCY
RANGE OF INFLUENT CONCENTRATION
WASTEWATER
BIOLOGICAL TREATMENT (AEROBIC)
367. (a)
1--100 ppm(b)
WASTEWATER
STRIPPING (STEAM)
9S7. (a)
0. 0i a-17. (b )
(a) (b>
Erased on South Plant Biopond Treatment data provided by Steve Jones (Ponca City).
Based on Ponca City data provided by Steve Jones.
SAL 000005774
AIR
Rel ease Calculations
ftfrurOn iVe=v
Release
-
AfA~
L.C,
-- po-ViT Rg/e^se_ ' Atyuc*
/S i nj-C.~f~d( !n~fo 2 <r
^3 772 ~fe ,V>l^'.b'F corros-a^
E/^.'+Ve
E^pni~t
Refuse -
0) *-
(d v) X 0,OoiZ^ lfc ^
`5_x
> *2 cto$ * 0.30 UH^
Hlo Tr-
Wi$-few-fer- Ir-t-A- _
,4
.\
Refe&se f* A.v-
iiZ52 . Csee ^ <S )
'To-fa I Non-po.'A R&l
2 i^i
6^5 *'s - E n^i/ieeT1'^ O-
WA/ eR Re l&^e- --
3,117 It C 3,joo')
(sec
UHb
Rel^s*5
NA-
O') Se ftppy g 1able
(E')
(/e
rv/^o
^ r y Eer-- cRi<? >vt f^c ^ Or" v^cW'*' ^
i)-i C SDC/AT C.ry^< $$to*y ^ 5 ctu \hc. e^F>OCce Cour: -z "frc
V) See A?Si)5 5 C* (rO /4/ox /
J.)
SAL 000005775
198S SARA 313 REPORTING RELEASE INVENTORY
LAKE CHARLES REFINERY
BENZENE
SOURCE
AMOUNT RELEASED (1b/yr)
AIR POINT RELEASES Storage Tanks
16,951. (17,000)
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss No. 3 CTU & VAC No. 2 CTU No. 4 HDS No. 3 CRU & HDS No. 1 Coker No. 2 Coker Gas Recovery Plant No. 6 HDS FCC Feed Prep FCC No. 2 CRU & HDS Thermal Cracker PBC
Mol ex SHAD/VHAD Tank Farm/Blending Process Drains Separators API DAF I AF Cooling Tower Wastewater Trt.mt Land-farm Trtmt Total Non--point Release
1,181.
876. 789. 461 . 1,738. 114.
2r>
200.
190. 118. 394. 987.
75. 1,Q06.
72. 2,541. 5,059.
276.
116.
4.
125. 187. 351 . 17,684.
(18,000)
TOTAL AIR RELEASE WATER RELEASE
34,635.
39.
LAND RELEASE On-Site (Land-farm) 0-f f -Si te
0. N/A
7. OF TOTAL RELEASE
TO MEDIUM 49
0 0 1 1 0 1
3
0 0
8 15
1 0 0 0 0 1
i
51 100
SAL 000005776
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
BENZENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment (aerobic)
Biological Treatment (aerobic)
87. 5'/. (a) 95"/. (b)
100"/. (d )
RANGE OF INFLUENT CONCENTRATION 0.01--1%(a)
lppb-lppm(c)
1-100 ppm(e)
(a) <b) (c) (d) <e)
According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
See Table A-2 (Fate of Has. &/or Toxic Pollutants...in Wastewater Treatment Plants) in Appx G.
Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
Based on ERA Chemdat 6 land treatment model in Appx F.
Solid waste composition data in Appx F.
sal
000S7??
Release c Alclulatioajs,
Benzene
L.C.
~ Ala rnj~Pciai~ts*~'eci
CX'Kck
m~f" ^cxSo|iv>^\^ clun.'n^
re-fcr*^'^ ^cnack.'/\^^ C(n4 h yc^rofrecvY^K-^ ope^+.o^i,
Preserrir in /kv,porf-ec( S<aur C-Pudes.
P^X tV>no*-v^
- S/fe CW clcjI
S*?<L Af>p * fc>
Process S+re^v*^ Co^posi-f/o^ <b*~h\
--
/f^px' f
3 V r"l C>( ~p\ TrV' 'Trtt^f- ft> rLc\*no( Pe/eAse (3 /<^s --
e
P
W^sfe.//vV- <> ^c^i~e.r- Release. C*lc<,
i'ncf.
Se.p*\nki&r<> &r ofUzs' Pr'^^ry
see. Appy< &
S~k>r<*3<E_ lZk CPoM+) Am e/e^se Ca/cs-- s^e $ppx hi
Pr'oc.esS Eyp^rt FL^i-f/Ve. 4.V- /Re feAS^r ^lcs" see 4^x -2T ^iVv^l. brA-'^vs^ G=c3|-Vv^ 7ower ^
ppbd^cf LockJ.'^oj Loss Q'r /<W<^*se C^/cs
See AppK J~
SAL 000005778
SOURCE
1988 SARA 313 REPORTING RELEASE INVENTORY
LAKE CHARLES REFINERY
1.3-BUTADIENE
AMOUNT RELEASED <1b/yr)
AIR POINT RELEASE
N/A
AIR NON-POINT RELEASE Fuel Gas Fugitives Fugitive Equipment L.oss No. 1 Coker No. 2 Coker Gas Recovery Plant FCC Cryo Cat Poly Thermal Cracker PBC Alkylation Acid Plant Tan k Farm
Total Non--pointRelease
149.
38. 7.
138. 286.
90. 123.
7. 230. 125.
2. 147. 1,342.
(1,300)
WATER RELEASE
N/A
LAND RELEASE
N/A
7. OF TOTAL RELEASE TO MEDIUM
11
3 1 10 21 7 9 1 17 9 O 1l 100
SAL 000005779
CALCULATIONS
u~/~c^d ine
L.C
Gaseous Co rv-ip o <u ^ C-I " Q>y -product <y~f Ae_ai/y & < I Cro.c/c-'n
Processed 1~
Cjas ^ecoi/ery ano(
pla/nf^,
nY--
^/Pyf^v'f/oH an <Y polyrvienf
on .
Vs e4.
as
{""foe/ <^a0.
losses ^re
Ve. ~fro ^ pr'oce.ss
(See A-ppe-^d! y
-dr- Po^.'-f.Ve Release Gxtc.uLilo*$)
C see Appendix.
{ft!- (x^-S SdT'&c, ^ Co<^p>oS <"/"'On
Append lx /> 'Ar~ ftlci-X A~/yi"f~ Ory St fa Cdc^lci'honA)
SAL 000005780
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
CHLORINE
RELEASE <1b/yr)
AIR POINT RELEASE
AIR NON-POINT RELEASE Cooling Tower, Boiler Injet
NA 2.OOP.
WATER RELEASE LAND RELEASE
NA NA
'/. OF TOTAL RELEASE
TO MEDIUM
SAL 000005781
ZS/gooooo IVs
- "5
aa5 07
^ pas^d
On3G)
J/yy
=
^^J3y
gwn
(s;y.|/ ey ^z:u<?1' C1Af-'l^loS ^l )
iM -
yaiWA
^`^Cp
jy^ &(<?' =
^-fur ^ x- -
x Jf. //Z-* 'J-fl^&loo'^^\^lo^1Ll = ^d3)^)
'fsw
S r s^/ipA
2. *>^:+s3
<r> ^
Suo/pafVj-
x -TJ ^^^Cw;/?cr^
ptjA^Jc) <2/. s^afsis'
^^:jooo a-vp
p-f^Od
' ^apjC
_)3j<pq
S( -TMyojif?
= z&Zfdy _p,;o3~->^>fl
VN - 4^! ^
m
z>-~i
^ L4 UOTO
/ijoiJL-vnnznvv 3s#3ph>/
SOURCE
1980 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
COBALT COMPOUNDS
RELEASE (lb/yr)
AIR POINT RELEASE
AIR NON-POINT RELEASE HDS Catalyst Handling
NA 15.
WATER RELEASE
LAND RELEASE On-Site Of-f-Site (BFI Land-fill)
NA
NA 2,700.
V. OF TOTAL RELEASE
TO MEDIUM
00Oos ^3
Reu=4S Calculations
Cob ck CpKHpogncj^
L\<2.
AlR
Psi'mrb Release
=
Non-paint /se/e^tse //~fDS Cert
m
loo lb caf lS5 0)
cat cbjv^p
/Z |W%<- y^MbS
! c ^
'"'^
= \jOL>~? lb cat- Cs-t
lp(o~7 ll H0$c.rfx 0.5 7
^ SS,`73 V-l Co
I'tA'i '%l CoO
ct) ($) osx0 03 2_ CoO *rt
15"
Co
--------------------
Cp^r&irelease")
SoiS'" s
i'm 0_ f~i r~iOj s ~h **i <\Ye
NAT&&
Red ease.
nA-
m)
(CoO tt^s&lulol^ iVi wc{iclt~ Soli'^5
=$>
eff/oe^-f
^>H
oJf~
LAND
See /IppK F
So/ApJ lA/^s/e /Refuse C^i.c.ul^'bo^^ j
o') >y S~/er<2_ 3o5 PiC, Cz)LiC, Cuctr uS._3e Iiair) per- J_loycf U/.Vy^er- ICOC d&fpX' P~)
rfOS cerh composiPoh
p-e-r- pP^" S/W/J- 3(3 6tJ(Vc(ciVC
Prope_r~+y
Coi.f, ,
Culru,;, ..
^ C/iei0 ( y/PAyS'Cv(
S/"- 000005784
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
CUMENE
RELEASE (lb/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss It 3 CRU & HDS HI Coker H2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker Tank Farm (P & L) Process Drains API Separators Cooling Tower Wastewater Trtmt Landfarm-Waste Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On-Site (Landfarm) Off-Site
565.
69.
1,442. 380. 73. 307. 168.
1,826. 555. 75.
6,324. 4. 2.
47. 296. 1.053. 12,621.
13,186.
39.
0. NA
% OF TOTAL RELEASE
TO MEDIUM
4
1
11 3
1
2
1
14 4
1
48
0 0 0
2 8 96
100
SAL 000005785
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
CUMENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment (aerobic)
Biological Treatment (aerobic)
87.3V. (a) 957.(b)
1 007. ( d >
RANGE OF INFLUENT CONCENTRATION 0.01-17. (a)
lppb-lppm(c>
0.01 -17. (e)
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
(b) See Table A-2 (Fate of Haz. &/or Toxic Pollutants...in Wastewater Treatment Plants) in Appx G.
(c> Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment <b). (Appx G)
(d) Based on EPA Chemdat 6 land treatment model in Appx F.
(e) Solid waste composition data in Appx F.
SAL 000005786
Release calculations
C (JrViehC
- /n* r\ U ~(~W cXU' reA Oun<^ pro^e sse_cl info gccSa r'e'ftir'^''KT^ ^cmok'^ ^ o<n4 h yctrd+rec^f--'^^
L.C,
iVnu v* //r^X Om ~ 5<'-fe CW oo ufv 0*^5
s^e Appyc t)
Process
S'fr-^o! ^
CZo^pos'^o^
~ ^c
F
I--A n c>( -fp r^v> 'Tr-f^rf- f\',r&-L^rxc{ fiele^se Gulc.s -- ^ee Appx F
VJckS fe_ ^"f-er- ft-'r b
Release. Ca/cS
S^e f\~ppyc
ir*c/*
A'RF Scpc\rui~2>r<, &~ dfUcr- Pc.vx^t\ry ~Tr~t^R)
G
Sbr-^j<c ~7a*k CR=>:r>F) /4-.V- /?e/e^se Calo^-- see ^^x A/
Pr&c-eS S E^p r*i+ /-Lq XVe_ A'r- /Refers? *lts -- see /^cpx X
6'^!. bfb,'k\s^ G=e>|-Xj^ To^ec ^
Prbduof LockJMj (~~oss
/?e/e^se Wcs. - see /i^P* X
SAL 000005787
1980 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
CYCLOHEXANE
SOURCE
RELEASE <1b/yr)
*/. OF TOTAL RELEASE
TO MEDIUM
AIR POINT RELEASES Storage Tanks (*)
8,476. (8,500)
42
AIR NON-POINT RELEASES Fugitive Equipment Loss #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant #6 HDS FCC #2 CRU & HDS Thermal Cracker PBC Mol ex, Tank Farm <P & L) Process Drains Separators API DAF IAF Cooling Tower Wastewater Trtmt Lan_cH_arm-Waste Trtmt
Total Non-point Release
1,184. 1,048.
651. 424. 380.
73. 307. 246. 358. 588.
75. 3,191.
96. 980. 516.
208.
8.
4.
219. 78.
1,259.. 11,893.
(32,000)
6
otim
2
0
r>
1
o> 0
16
0
1 0
0
1 0 6 58
TOTAL AIR RELEASE
20,369.
100
WATER RELEASE
39.
LAND RELEASE On--Site (Land-farm) Off-Site
0. NA
(*)
A LleriCdl error was made during the calculations in which eye 1 ohe:: ane storage tank release was underest i mated by 3,500 lbs.
SAL 000005788
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
CYCLOHEXANE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment (aerobic)
Biological Treatment (aerobic)
97. 57. (a) 957. (b)
1 007. < d )
RANGE OF INFLUENT CONCENTRATION 0. 01-17. <a)
1 ppb--1ppm(c)
0.01 -17. (e)
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
(b) See Table A*-2 (Fate of Haz . &/or Toxic Pollutants. . . in Wastewater Treatment Plants) in Appx G.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
(d) Erased on EPA Chemdat 6 land treatment model in Appx F.
(e) Solid waste composition data in Appx F.
SAL 000005789
Release a AL<zuurrtoa/s
Cyo(o^vex:^Ke
Present" i'r\ Oz$t
-feeoJs~fr>cX^ otor'n^
Qc*.Salt
o,iac^ ofie^
process'*
,
U.C.
Plex*'V> U yy\ (\t*& On - 5/fe (2a/ CO*| <\*oki5
S^e 7^p x &
Pf&cess S'fre^.Kv^
s i "/< o ^ i)xF
Appy E
L.A^ot'p^rrv- ~Trfwf_ /},'*- &rL*mJ, PeieAse a /os -- see /4p>/?x F*
U/^sfe^/oo fcr X
/'eo /^e/eAse C^/cS -- see Aff>X <S
tt`net*
ARE Se^\n*'fors <r atbzs' Pr'^^ry ~Tr~i^-h)
/a^P
/4-.V- /?e/eA.5^ C^los-- See
xH
Process E^P rM+ ^3;: i/e. $~*r- Pele*se CirxcJ. br^-'^S G=*3|*5 To^^r- ^
see
X
SAL 000005790
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
ETHYLBENZENE
RELEASE (lb/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES
Loading Loss
Fugitive Equipment Loss
#3 CTU
Vac
#2 CTU
#4 HDS
#3 CRU & HDS
FCC Feed Prep
FCC
#2 CRU
HDS
PBC
SHAD/VHAD
Tank Farm <P & L)
Process Drains
API Separator
Cooling Tower
Wastewater Trtmt
Landiarm-Waste Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE Gn -- Site (Land-farm) 0-f f-Si te
1,613. (1,600)
125.
165. 146.
90. 1,166.
106. 1,074.
449. 461 . 290. 4,461.
20.
8.
74. 187. 217. 9,039.
(9,000)
10,652.
39.
0.
NA
7. OF TOTAL RELEASE
TO MEDIUM
15
1
2 1 1 11 1 10 4 4 3 42 0
0
1 2 2 85
100
SAL 000005791
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
ETHYLBENZENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGi11 VRU
Biological Treatment (aerobic)
Biological Treatment (aerobic)
87.57. (a) 957. (b)
1007. (d )
RANGE OF INFLUENT CONCENTRATION 0.01 --17.<a>
Ippb-lppm(c)
1-lOOppm(e)
(a) (b) (c) (d) (e)
According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
See Table A-2 (Fate of Has. &/or Toxic Pollutants...in Wastewater Treatment Plants) in Appx G.
Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
Based on EPA Chemdat 6 land treatment model i. n Appx F.
Solid waste composition data in Appx F.
sal
OOqo5 7 92
Release c Allluletigns
EHlylbe n^ene
l.c.
o"fvre<^ X<*cA pro messed info cjccSo|i*^e. cljr.'i^
ne.-for'i^-V^ ^erwc/oWj ^
h yMroireoX1*-^ e^perorf-.'on.s,
Pf'eSe.KV'f" >r^ ^c\So|h dyC- ^^Dron'se') ^
-- See PlSfrS sc^n CApp* d)
COrtTpanen^
Ftaxt rviu v' /?*vX On ~ S.'-fe CW oo( ^X
Process
S'+re^i^
Co^,pos-7/o*,
<b^~f<L
T^eyo *r
-- S>e<i flrpfpt F
L.A^ol"pc\rvn '~Tr''trvnf- /}t'r
ftele^se &\lc.<> -- $ee A~ppx F
W<^5/^V-
^<*f~ec- Release. (2a l c$
see. $~fpx ?
i'nc/. AFT Sepcvf^i'fer^ <r oiU^T Pr< ifWKCy ~1rf^i~)
Sferc^e,
CPo^+) A.v- Rele^ se C*/c$-- 5^e
A/
Po^C,esS ET<y p r^i"f F^, +: v/e. ^.r- Fe/e-ise Calcs-" see /^y?x X
FVuJ. J>rt/K\5
G=&t**i5 Toiler' }
Pfbctt/c-f* Loc\d.'s\aj Lass (\'r /?e/e^^e Ca/cs -- See Appx X
SAL 000005793
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
ETHYLENE
RELEASE (lb/yr)
AIR POINT RELEASES
AIR NON-POINT RELEASES Fuel Gas Fugitives Fugitive Equipment Lass #1 Coker #2 Coker Gas Recovery Plant FCC Cryo Thermal Cracker Acid PI ant Tank Farm <P & LL
Total Non-point Release
WATER RELEASE
LAND RELEASE
NA
1,786.
380. 73.
154. 5,728. 2,691.
75. 202. 2.941. 14,030.
(14,000)
NA
NA
*/, OF TOTAL RELEASE
TO MEDIUM
13
3 1 1 40 19 1 1 21 100
SAL 00000579^
Release
calculations
L.Ct
G-^eooS
Compoo^c/
"" &y - product o*T Aecu/y-c5.| Cr^cio'in^
" Processed h gas recovery ano(
Cfyo^nrc pla^A;.
U*>-c(^
c^s -po-e-f 6~foe( Qj^.s ).
Ml lasses ^re
(Se^c
A~p p <g ^ o(
^e_
~Pron
pr'OC.&sS
j: -fir- E^i'-ftVe. Rele*s>e C/*l<zal*.i~tor15)
C$e-e- Append'x
S~fcec* o^ 0*>*-V\ OS t~Ho^i
(^ee fPppejnd^K
A ~f^r~ PlaX. A~sn~f~ Or-\ ~St`fc ^A.lcUyl^'ftO^S^
SAL 000005795
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
HYDROCHLORIC ACID
RELEASE <ib/yr)
AIR POINT RELEASE Storage Tanks
AIR NON-POINT RELEASE Deniineralizer Resin Regeneration
TOTAL AIR RELEASE
WATER RELEASE
-AND RELEASE
16. 614. <610) 630
O. NA
/. OF TOTAL Release
TO MEDIUM
3
97
100
0ooo5796
GENERAL WASTESTREAM
WASTEWATER
19B8 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
HYDROCHLORIC ACID
TREATMENT METHOD
TREATMENT EFFICIENCY
RANGE OF INFLUENT CONCENTRATION
NEUTRALIZATION
100'/. <a)
>17. <b>
(a) <b>
Based on wastewater discharge monitoring reports (Appx G). Based on data provided by Brandt Butler.
$At_ 00005797
f\E-t-E4SE
CALcLUL-QTlofy^
AiR
^fyoIr'Qd-i-n (or^c 4,'of
L,c
fZ,'r-rt Release -
-fain/c)
s,TM?* " m^Co.-kz
Class')
SV^e.
- uni-
Release -
bbl ibrc^Upu-f-
^ (b
0.2-t psi'tfi t~M
^5)
x 0,3fZ /k-l jir^w^
^c,ee \tfz\c,heci spoettclsh&e'fy
` /6> tb hfd
Mok- po;^t /Release
tfCt
usec( *ft>r-
reQe^e.^"f>v5i^ .
boi (er~ 'a/a'/r./~
*% Vi er-** (ier reus ^
R,<v'YVe FcyprFr Sooroe*
^'v'e 1 f^p Y Valvet, '7
r
Release = | .of/) + ^(.ota) +I^,oo/8|^ zy
V34S-^r
y
xO,3?zHCI = &M -_ H-cf X EUs.vs = E~o Oj'Heer! r\o^ G.^/ CcjUioh
t&o)
vRne^
/^e(e^5e
-o
S^St>, - p) h/ frloM i 'for'i'i
Release
- A/4-
^ppx C- ~ jcj`z>^
/(_J (? {docA-c
I^S^S 5 0.^ -- fi-ppx
CO \p p
f-jcv looc/4 o -f4pp>^ ~ /
5_/ry FR r Y*r z
<*s
d5,e> A~ppX C?-') SAL 000005798
VOC EMISSION CALCULATIONS FIXED ROOF
DATE TIME PERIOD : MONTH,YR
: MONTH,YR LOCATION POINT SOURCE I.D. # MATERIAL STORED TANK CAPACITY <bt>ls> THRUPUT (bbls/yr>
START END
20--May--89 JAN, 1988 DEC, 1988 LAKE CHARLES
HC1 TANK HC1 ACID (307.)
238 4672
BREATHING LOSS
TANK DIAMETER (-ft) TANK HEIGHT (ft) VAPOR SPACE HEIGHT (ft) DAILY TEMP CHANGE (F) MOLECULAR WEIGHT VAPOR PRESSURE (psia) PRESSURE (psia) PRODUCT FACTOR PAINT FACTOR SMALL TANK FACTOR
BREATHING LOSS (lbs)
D= H= h= dT = Mv = Pv = Pa = Kc = Fp = C=
Lb =
11
15
7.5 20 30
0.31 14. 7
1
1
0.56
WORKING LOSS
MOLECULAR WEIGHT VAPOR PRESSURE # OF TURNOVERS PER YEAR TANK CAPACITY (pal) TURNOVER FACTOR PRODUCT FACTOR
WORKING LOSS (lbs)
Mv = Pv =
N= V= Kn = Kc =
Lw --
30 0. 31 19.630252101 9996
1 1
44
TOTAL LOSS <]b/yr>
Lt = Lb + Lw
SAL OOOOO5799
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
LEAD COMPOUNDS
RELEASE (lb/yr)
AIR POINT RELEASE Storage Tanks
AIR NON-POINT RELEASE Leaded Gasoline Antiknock Addn.
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE
0. 403. <400> 403.
0. NA
7. OF TOTAL RELEASE
TO MEDIUM
0
lOO IOC
SAL 000005800
Release Calculations
Le-gyd Qo rvn pounds
L<<Z,
MR
Potrrt
Release -
t(\ ysi.tp
l ~l
Sf^,T^^k 1 Pro' \OU>Ik TEL. x /6 v /,**<
__J___j-----_---^-- 0.^9.1:_rM^>/
/
`/Z-g*! "
X jooo /m |
(.A A/
hfeAV*'er ~PPa* {MMT~ Psee i^r* c<~v
TE-L- in^A has a
~hi K\ l(
1/ja~Pa_^ ,
3^yco( Sa/ orx iLp '
relea.se Au e F>
%, fte(ea.
- O -y? Pi (
ree ^
sp"
Nor\-p+- Release
F EaDJ Source 3 Lyp
- TCt-- C. l^-ajd kAAcmCjA) `Z.Act.'/tLz
System (added % n^>'lr' ^aSaUej
Soupc^5 - e.s>~Ri^<de
to v^li/e5
3L? -p/K^es
FL5, Release - iCo^V lo(.ooo5l)+ 3&(.ooi%')f
*2^-^
ptLX^tri y Rg l,73
I It pfe
V It Tfe_
"
Cp~st
ref##se^)
d*.lcu lift'd ^
w 4-TE: &
ReJes^e. -
2 //>
(LV&ry l>Wfe perje^i^ ( f& k/AS*/^
^
Reie^s^. "
W/f --------------
<** f e.ac<ed ^ noc.f'
n> ;* nr* }
o') ^z^
6)
4ppx CL *,C
1^^? G>fmeboo^
phyS'C^l
PfopeH ,`e-5 /cTifefe
F$-pp*"
-- So(.1 of
C^Rspcis^f L/^lr^O
SAt 000005801
VOC EMISSION CALCULATIONS FIXED ROOF
DATE TIME PERIOD : MONTH,YR START
: MONTH,YR END LOCATION POINT SOURCE I.D. # MATERIAL STORED TANK CAPACITY (bbls) THRUF'UT (bbls/yr)
22-*May-B9 JAN, 1988 FEB, 1988 LAKE CHARLES
STG TANK MOTOR TEL
90 191
BREATHING LOSS
TANK DIAMETER (-ft) TANK HEIGHT (-ft) VAPOR SPACE HEIGHT <ft> DAILY TEMP CHANGE (F) MOLECULAR WEIGHT VAPOR PRESSURE (psia) PRESSURE (psia) PRODUCT FACTOR PAINT FACTOR SMALL TANK FACTOR
BREATHING LOSS (lbs)
D= Hh= dT = Mv = Pv = Pa = Kc = Fp = C=
Lb =
8
10 5
20 92 0.0009 14. 7
1 1
O. 42
0
WORKING LOSS
MOLECULAR WEIGHT VAPOR PRESSURE # OF TURNOVERS PER YEAR TANK CAPACITY (qal) TURNOVER FACTOR PRODUCT FACTOR
WORKING LD3S (lbs)
Mv = Pv =
N= V= Kn Kc =
Lw =
92 Ci. 0009
3780 1 1
0
TOTAL LOSS (lb/yr)
Lt Lb + Lw
0
S4L 000005802
SECTION III PS&S 527-82
Properties of Typical "Ethyl" Antiknock Compounds
MOTOR
TEL AVIATION
TML
Density @ 68 F, g/ml Form Freezing Point, F Flash Point. (TOC), F Viscosity < 68 F, cp Density-Temp. Correc tion Factor g/m1 (FI g Pb/lb Compound g Pb/gal. Compound (a) 68 F
1.586 Uq. -28
>245 0.86
-0.00092 178.67 2365
1.741 Liq. +16
>250 1.02
-0.00092 178.44 2593
1.582 Liq. -54 89 0.65
-0.0010 178.67 2359
~MLA" 500
1.584 Liq. -40
>180 0.74
-0.00095 178.67 2362
The following method may be used to determine the pounds of "Ethyl" Antiknock Compound required for a given lead concentration in gasoline:
42 gal/bbl Pounds Antiknock Compound req'd = bbls gasoline in blend x g Pb/gal x --... ^------------- --
9 Pb/lb Compound
Mixing Tables have been prepared for quick reference covering the blending range of 50 barrels of gasoline up to 100,000 barrels. A sample table is shown on the following page.
Maximum Lead Concentrations in Gasoline
The U.S. Public Health Service recommends that the total lead content in a motor gasoline of either TEL or TML, or mixtures of them, or related compounds and their mixtures, should not exceed 4.23 grams of lead per U.S. gallon.
Design engineer should verify maximum concentrations for area under consideration.
SAL 000058
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
MANGANESE COMPOUNDS
RELEASE (lb/yr)
AIR POINT RELEASE Storage Tanks
AIR NON-POINT RELEASE Leaded Gasoline Antiknock Addn.
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE
O. 250. (250) 250.
O. NA
/L OF TOTAL RELEASE
TO MEDIUM
O
1O0 100
SAL
00005804
Release ealculat/oa/s
/rU^g0|,>&se' Co^p^,
L.c.
AiR
R<3lea_se
=
,
S+3. Toy^k 'Throucjhpuf" ~
Lo?s =
^(0^3 lb
/ 3t IUI
,
ff.ST/l *
~ bj
Q Ib
C^&e oitbcAeJ, zpr&^JLsbeei)
Non -po ,'nf /ReI
FLS *'~-F
E^-f- Sacrce.
~-Ertyl"MAlT .AX'
Sysfe*^
AlAlT ;5 Scppl^t-vi^*-!-/-
-fe rejok r ^So/.'^e cv^ <xtrHic^ ocs/c
C-J5.sv^_ o"/"
6TE,^
Sources - eS'A'^'fe.
-I p^p to vcits/e^
Vp- >-0^~7 TM~H3C'>X 7^,0STn3 = O.Ooo<? ps<>
,_\ (IneAVy }
Refuse - ]j CoV7) 4-|o(.oog^O + 36 6oo/*)Jj^ .
-- n/^i /
V 2*-/ "^T *
- 2S__b
tk ,
'r
~yr- ^
~&\*->
Ain
Cp^reA mg/n/ C&te^c)
-- E^c,,'
G=J tu h^on
mrE% LA/VO
Re-le<\s<? - O fb
/?<s(e*<>e ^
AM
CY^ry /'rf/e po'fen^W/ ^ <^ef Vo
w5
-- sys^e^')
<T/V^> R<*el?cA. QcLSol'Ke 4a^/c o/e'Ofr'vdtJ
O') see
fi-ppx
A
-
L") PJny S'1 2< *\i
Pro per"/'
E) See Appy 6 - E
1(- ) see ^ -Appy
s*
'n
Factor's >P`
SAL 000005805
VOC EMISSION CALCULATIONS FIXED ROOF
DATE TIME PERIOD : MONTH,YR
: MONTH,YR LOCATION POINT SOURCE I.D. # MATERIAL STORED TANK CAPACITY (bbls) THRUPUT (bbls/yr >
START END
--
= ~ = = =
22--May--89 JAN, 1988 FEB, 1988 LAKE CHARLES
STG TANK ETHYL MMT
90 618
BREATHING LOSS
TANK DIAMETER <-ft) TANK HEIGHT (ft) VAPOR SPACE HEIGHT (ft) DAILY TEMP CHANGE <F> MOLECULAR WEIGHT VAPOR PRESSURE (psia) PRESSURE (psia) PRODUCT FACTOR PAINT FACTOR SMALL TANK FACTOR
BREATHING LOSS (lbs)
D= H= hdT = Mv = Pv = Pa = Kc = Fp = C=
Lb =
8 io
5 20 92 0.0009 14.7
1 1 0.42
0
WORKING LOSS
MOLECULAR WEIGHT VAPOR PRESSURE # OF TURNOVERS PER YEAR TANK CAPACITY (pal) TURNOVER FACTOR PRODUCT FACTOR
WORKING LOSS (lbs)
Mv = Pv =
N= V= Kn = Kc =
Lw =
92 0.0009 6.8666666667
3780 1 1
0
TOTAL LOSS (lb/vr)
Lt = Lb + L w
O
00000580<>
SM-
PHYSICAL PROPERTIES
"ETHYL" MMT
COMPOSITION
Methylcyciopentadienyl Manganese Tricarbonyl
[CH3C5H4Mn(CO)3l
TYPICAL PROPERTIES
Manganese, wt % (minimum) ...................................................................................24.4 Form ........................................................................................................ Orange Liquid* Density @68F(20C) ...................................................................................1.38 g/ml
11.5 lb/gal. Freeze Point (initial) ............................................................................... 30F (-- IC)t Flash Point (TCC)......................................................................................... 205F(96C) Vapor Pressure @ 68F (20C) ................................................................ 0.047 mm HgJ Viscosity @68F(20C) ......................................................................................5.2 cp Solubility: Miscible in ...................n-Hexane, n-Heptane, Iso-octane, Toluene, Ethanol
In Water @ 25C................... 102 ppm In Glycerine.................................. < 5%
Application Factors
Grams Elemental Manganese Per Pound of Compound ................... .......................Ill Per Gallon of Compound................. ........................... 1277
Density-Temperature Correction Factor..........................................--0.000663 g/ml/ F -0.00119 g/ml/ C
This material is sensitive to light and Mil decompose on exposure.
t This material forms a metastable phase, freezing at about 25.5 F which changes into the stable liquid
phase about 30 F.
t Log P(mm Hg) = 7.2283 -
1882
(*C + 200)
VI! - 1
Sal 00058o?
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
METHANOL
RELEASE (lto/yr)
AIR POINT RELEASE Storage Tanks
AIR NON-POINT RELEASE Cryo Re-frig Deicing Fuel Oil Blending (AQ23) Propane B1ending
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On-Si te ( Land-farm) O-ff-Si te
760.
72. 482. 964. 1,518.
(1,500)
2,278.
0.
0.
NA
*/. OF TOTAL RELEASE
TO MEDIUM
33
3 21 43 67
100
SAL 0000580Q
GENERAL WASTESTREAM Wastewater
Solid Waste
1968 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
METHANOL
TREATMENT METHOD
TREATMENT EFFICIENCY
Biological Treatment (aerobic)
Biological Treatment (aerobic)
lO0/i(a) 100/i(c>
RANGE OF INFLUENT CONCENTRATION lppb--lppm<b)
1 -- 100 ppm(d)
(a) See Table A--2 (Fate o-f Haz . &/or Toxic Pol 1 utants. . - i n Wastewater Treatment Plants) in Appx G.
(b) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment <b). (Appx G)
(c) Based on EPA Chemdat 6 land treatment model in Appx F.
< d) Based on solid waste composition data for similar chemicals (Appx F).
SAL 000005809
018500000 IVS
V^y 'O 'd
-----------
^0^)9
{)
3 /oj
a^;f-S5(/,;
-// -- (s-z-_52 ^>ccr
`*9
<zj j~f
w<v*V*^ 3w^vS W
3
SI3 3-SUt
<j>
^ud-vcyy
)^f P l
( /'o -
o-
jA LIL
H
^ -7__________ ---------------------------- x
(^'09WU'O0??'?3/l /h,"Z'^7
fy,
x
^10} ^%gU1?&*r>
((SSO3
(^ wo^^oXyC^^
VOQ -'^'VJ^ST ^ ^.'->'3% S3 jv;^3j
-UQ^Lj
1W
q/. pas^ap-j s/ ^^*>0 pb
.2
w*)hh(l
<?/)}
=.
foAT^Ysb :
Ao'V S O X ~J--hs)b -t^:pusjq (/-o izryji-zo]/
Ha%J 7
hVL ~-
l/,^xyi7xJ (y%, /re? =^.^,3,^
r i (On
o^r>d 'T-? f
^
Q^/Z-.T^
;: /**# -^**d
rc?p j
(^/v-jypp^ uoip^Cui . XJjd'J o/jt>
-a^kpc/o^c/ J_P<^S uo^f,,. ^
ocj ^ f) >-f > Sr?_j
~PSi?3 ly*atyi/ j+o' **gJ- ^oji
ffoWWo^L ^
^ X 4 SS-<? - (Ac?/,
c^f &ocfZ> {n^
SSp-7 %
asvaj^ y.'^cf
'D'l
\0^-^U)
SMouinrryifr^ Hsys^
yw
vfifrrEfi
file-fine*v\0 l Cco*a)
L.C.
Re.te.ase - O
(<00% de^r^ded -- p^ EPrf S/k?d-
3/3 ^ui'cfaiac^. c|oc<-"v>esrt }
B^S*
--
<V>e r.'i^
EZs^K^oY-C
<3^ - S,Ve_ Re.!e_c,se -
Q_
Ooo**/* d e^r*\c^&Y'b^( 0~ <=*,t^y
fa /qwj(A^)6)
0(F"S'*fe ftele^e " /V4~
>&*>?$ -
E^ji'neen'n^
Es-fi^A
CO s^e
Eftf <C-/ie*v% d*i- &> k^ci icre-(^eni' fKocJe! ~~
^5-fe --
<**y
i/o/^-///f'^-/,'0M
(-
SAL ooo5ail
SOURCE
19B8 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
METHYL t-BUTYL ETHER
RELEASE (lb/yr)
AIR POINT RELEASE Storage Tanks
AIR NON-POINT RELEASE Tank Farm (P & L) Wastewater Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On--Site (Land-farm) Off-Sit
8,680. (8,700)
1,128.
3-. 1,131.
(1,100)
9,811.
NA NA
7. OF TOTAL RELEASE
TO MEDIUM
89
11 0
11
100
SAL 000005812
GENERAL WASTESTREAM
Gaseous
Wastewater
J9B8 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
METHYL t"-BUTYL ETHER
TREATMENT METHOD
TREATMENT EFFICIENCY
McGi11 VRU
Biological Treatment (aerobic >
87 - 57. (a) 957. (b)
RANGE OF INFLUENT CONCENTRATION
G. 01 -17. < a)
<! 1 ppb <c )
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data. (987 was inadvertently reported as efficiency -for 1988, as it was reported -for similar compounds -for 1987. )
(b) See Table A-2 (Fate of Haz. 8</or Toxic Pol 1 utants. . . i n Wastewater Treatment Plants) in Appx G. Efficiency based on that o-f similar compounds.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b) for similar compounds. Also based on relative presence of MTBE in the refinery compared to more prevalent compounds, such as benzene.
SAC 0053I3
RELEASE CALCULATIONS
MeJAy( ~t-!3>u-fj Ether
L.C,
AiR
Pc>L-f- /?eie&.se '
Sfj (Release.
=
O)
%,6ZO lb MtbE
N^ - po'.s\f /?e/gAS e T
FLl^i'-fiVe_ Ftyprn't R&le.`K`xZ.
~ ~TLr\k.
(S^.%0 [,'ne. Slei^J
-- ^c^-'tVok
' / poi'vnf ^ /o valves^ 36?.*P/ftrt3s
/?e(ecse = I CoK*)C+/oC.o^?) + 3^6o)j4 xZ^> 3(,T
= n-z? - rMree
To+^f
^ "Tr-e^'f^e^ /Re/e\s
*=1
(Von--po^f- Release
-
3 ^ nrg
1,131 yr- ftTBEL
NFTeR
ReiAse -
jb_
_______
*2-
*Sr
vi
A1/8S
LAMP
(Re le
as<?
--
/V/l~
<C on
cle^ n.O cv ~t~ in
V!<f* (e") ^
g^soZ/^f ~hni:
nss. Akoj !/ery
0 per~
EfS -- 5-ee ^opx /"/
-0 SoC/hl e^^sl-Ch "P\C"fe>^S -- se_e /Qppy R
(_^)
wo.'fer~ /?e(eA.st Oh(cx/i<=cf<v>^*> -- see
O') Soj-'d ^-vO D'Spo^<v(
--------- See
<4ppx
P
Appy &-
sal
00058i4
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
MOLYBDENUM TRIOXIDE
RELEASE (lb/yr)
AIR POINT RELEASE
AIR NON-POINT RELEASE HDS Catalyst Handling
NA 120.
WATER RELEASE
LAND RELEASE On-Site Off-Site (BFI Landfill)
NA
NA 21,000.
V. OF TOTAL RELEASE
TO MEDIUM
SAL 000005815
Release calculatio/vs
PRolybcje-HOKi TTV^bte
L.C
Mr
Po'.n't Release
- A/A
Non -point f{e. iggyse
/ f~f&S Cccf* (4
V /^(<piA/ o way
~ IOO Its c
loss ^ ^ fVo**
X x ? tibS^-k ^ rno^i0
avg
= \ OLo'~7 lh c*f /osf-
z ,M
\o(s>i a mScA (o,sy %!,, x o,o?6
<**><*.$ z
a') CO
+ aV3 /%x' o.n
ts s^e
t
us ^03 Cl^
&G.Si'<
F*o Cj ,'nee
Exsfi'r*-i<*'f^
WATER
Release
- ///T-
{Mso no f/AS c-vf 03 '/tt.c~f~ ~/ IA/6\ s7e Aer- ^
ijIu'C
fiJcO
"fe over^Lcf^
e__*-.+-a{<.y 5-~f*- ^5
prcs-etn.ee. A
_
^p
zj
in So loLQOf) no eJcflue+\i-
(2aO
r&ie^e)
Lftttb
c
49px F
5o/,W iV-P s7^ /?e/e.ft se CZe. (cu/a i/Ufn^
Ly S'jevc 3o/ie^ PiC, Pe-fy
/LF, tffiS C/Cf"
(Up) p^*"* Ljoyc{ VJt'vna^^r' Xoc C^frx ^)
H)S c^F co^po5''4>'o
<Xi F
T) f>zr FPA S/lPM "3/5 G^;Aj>nc(> ) <3 CO
^ OAfft-'V'-'C'H
ploy ^;ct f'ropeT'fy cF"F
sal
0005Qi6
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
NAPHTHALENE
RELEASE <1b/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss #3 CTU 8< Vac #2 CTU #4 HDS #5 HDS #6 HDS #7 HDS FCC Feed Prep #1 HDS PBC Mol ex SHAD/VHAD Tank Farm (P & L) Cooling Tower Land-farm - Waste Trtmt
Total Non--point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On-Site (Land-farm) O-f-f-Site
1,238. (1,200)
987. 874. 542. 117. 142.
56. 118. 208. 384.
DO.
436. 2,941.
59. 269. 7,191.
(7,200)
8,429.
47.
0. NA
V. OF TOTAL RELEASE
TO MEDIUM
15
0
12 10
6
1
2
1 1
2 5
1
S>wJ 1
85
100
SAL 00000581
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
NAPHTHALENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment (aerobic)
Biological T reatment (aerobic)
87.57. (a) 95%(b>
iOOY.(d)
RANGE OF INFLUENT CONCENTRATION O.Ol-lX(a)
ippb-ippm<c)
0.01~17.(e>
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
<b) See Table A-2 (Fate of Has. S</or Toxic Pol 1 utants. . . i n Wastewater Treatment Plants) in Appx G.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
(d) Based on EPA Chemdat 6 land treatment model in Appx F.
(e) Solid waste composition data in Appx F.
SAL 000005818
Release a Alclulations
-- Preset -n ces < *\o> k <?a.<d ^aSo/^e a no/
crtLejr -fepJsfec4js
and
/n^enrvied' <*/e_
cfre^n^s
clur<i^<^
cr^de p^c^ss^,
~~ Used* ' ^ Nc\ Ico S'701 Process A<r+,'-fo*** liO cr"uo(e u^iVs,
See
Sc^n C4f>pK
P^ax i i^nu v' /jU'r/- CU - S//e (2W cu( fv 0^5
xr
Process S'fre^*^ Co ^ipo $ < *//V>^ <5 A/a
--
//ppx' T
L.Anct'fUri'V' Tr^f /?;r-L,^ ftele^se O /ns
-- see
F
UFsf^e./^/r ^ l^Vcnf^r- Re/e^se. Ca/cS
see. flt~fpy< C
ti'ncJ. /J-CZT Sep^rn'fars &r atL^r Pr'^^ry ~7r~t'*i~)
S-fe^. ~J^X CP^:^+) /f.v- #e/e Ase Cic5-- s^e 4pf?x H
process E^ypm~f~ FLqi-Ps/^ $~,'r- /Re/e^s^ E^ics- see Afpx I
Cinc~(. brfc.'^^ G=o|<'*^ 7o^er- )
Pc^duof Loo,c/.'n&j Eoss
/?*'r ^e/e^se Wc* -- see *^p?< J"
S*J.
00005819
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
NICKEL COMPOUNDS
RELEASE (1b/yr >
AIR POINT RELEASE
AIR NON-POINT RELEASE HDS Catalyst Handling
NA 1 1.
WATER RELEASE
LAND RELEASE n-Site 0-ff-Site (BFI Land-fill)
NA
NA 1,900.
7. OF TOTAL RELEASE
TO MEDIUM
SAL 000005820
RELB4SEL CfHXLUL&TtoMS
fVi'cke-l
dp KVgpoc;ng(.g
MR
PoiVv6 Re/ectS^
- /Wf
A/jn -po'nf /^e(e^5<- -
m^s c*t ^dc-N
^ ^ 6/ovva^ay
l&O lb Ca^ /5S ^ ^
c*f
- | o(jT1 lb c**t~ Ic^sir
Lt(Z.
X?
*
|0fo7/i*ufx0.^ *%* c*fos^
x00?0 U;o !neS<*)
* St.71 'V~i /V,'
7^71 *%o| A/;0
I I yr /Vi
Cp^re^
/
release )
^ Ew^i'wCfi-rinj s_P*'i**'/^
W/rtefi.
Rei e^se
/v/f
^ /Vi' O iVvSofoWe. vv^Gr-w) Sol^5
rvo eff/oen'P reYe^se.^
rt*fl settle ojt
uwy/) C See fippyR F ~ Sol.'J tv^s/e
CD i?y S'/ere- 3cmrs^ FCi
(X)/_X, Cct+ u$^e
per j-Joy<^ UAVvjer ITOC C&(=f>* F)
CV) [fOS CA+ Composi`rt Appx F~
P/") per
S/b?/J- 3/3
Pro p e_r^4 y ^ ^
^ Che^'c* /y/PAys*c^/
SAL Oo00058ai
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
PHOSPHORIC ACID
RELEASE (Ib/yr)
AIR POINT RELEASE AIR NON-POINT RELEASE
WATER RELEASE
LAND RELEASE On-Site Off-Site (BFI Landfill)
NA NA
0.
NA
0.
% OF TOTAL RELEASE
TO MEDIUM
GENERAL WASTESTREAM
WASTEWATER SOLID WASTE
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
PHOSPHORIC ACID
TREATMENT METHOD
TREATMENT EFFICIENCY
RANGE OF INFLUENT CONCENTRATION
NEUTRALIZATION
1007. (a)
>17.<b>
NEUTRALIZATION
1007. (b)
>17. (b)
(a) Based on wastewater discharge monitoring reports (App>i G) <b) Based on data provided by Brandt Butler.
SAL 000005823
Re<LE4SE OA-LCULATlGfVS
PPospinor/c,
L . C,
P~p <r- -pf~ deJ&Kse
(jC=CP
Poly C^'f^.fys'f'
tveV
co dv**\ pec0
'olfrie-d
Re (e<\se -- O
B \s- 5
pH- /V\Cj n,Tor.'*-^ e>P effjfoe*"f- {ke.'fa'e^ (o *" V') See 4ppx (?-- W<*$~i~iK/ci'fej~ r^^Yon,'*-*^ n?p*rh
uwo
0^ -- ST-/e Pel^se
~
04P-S<*e /?efe^e -
_0_
sPe^ c^+pjy o+/vs^
is nc/fr>Ptetf( pr.br- -ft>
B^s
n3
> y > >^vv^ yP
.C. r"0py
OpeM'tort
). faCer^ey^
SAL 000005824-
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
PROPYLENE
RELEASE (lb/yr)
AIR POINT RELEASES
AIR NON-POINT RELEASES Fuel Gas Fugitives Fugitive Equipment Loss #1 Coker #2 Coker Gas Recovery Plant FCC Cryo Cat Poly Thermal Cracker PBC A1 ky Acid Plant Tank Farm (P & L?
Total Non-point Release
WATER RELEASE
LAND RELEASE
NA
2,480.
2,663. 51 1 .
17,380. 30,430.
8,611. 27,934.
528. 28,061. 15,198.
560. 1.471. 35,827.
(140,000)
NA
NA
'/. OF TOTAL RELEASE
TO MEDIUM
2
2 0 13 23 6 21 0 21 11 0 1 lOO
00O5a
2S
Release calculations
Pro pylene
L.C.,
Gra.se^os CorMyOoo^c/
"pRcJciuc'f'
Ata.|/y cp I Cr^cic.'nj
ProoessecA
'''e^oi/e^ 0.0o(
Gryicg^ni'c plan^. Rzc*.<cf*n~h ->-i ar\o^. pcplym&f't -zjzCh'or^ ,
c\5 &->.( {"'foe/ Ojcts'}.
frll /asse5 <3/~e *Po^t-(tVe_ Tro^vx pi~oce.5$ e~cyv'
(^See i4ppe^o(Jy
^<,ee Ap/pend*' x
2
Pu^i+cVe. ^eJe^se CnlcLulcii-t'orts)
{j-^s Stfr^c,^ 0orv\poifcn ^c,"h^
fhpp>.^\d< K A -for- /n*x /b*t 0n -S;/e Cdcu/vi-.ons)
SAL 000005826
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
SODIUM HYDROXIDE (soln)
RELEASE (Ib/yr)
AIR POINT RELEASE AIR NON-POINT RELEASE WATER RELEASE LAND RELEASE
0. 0. 0.
NA
% OF TOTAL RELEASE
TO MEDIUM
SAL 000005827
GENERAL WASTESTREAM
WASTEWATER
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
SODIUM HYDROXIDE
TREATMENT METHOD
TREATMENT EFFICIENCY
RANGE OF INFLUENT CONCENTRATION
NEUTRALIZATION
1007. (a)
>17.(b)
<a) Based on wastewater discharoe monitorina reports (Appx G). (b) Based on data orovided by Brandt Butler
SAI- 000005828
RegE/XE C/k^CucATio/VS
Sod / UVY\ Hydraxri'Jz. feolh')
Ltc.
M
PL &r No* -frt Re-l&< se
~O
)C
SPr VP =
j?>o~C O
O)
' y~\ ee.r-,'1^
E-S Li
-
N/LTE-R
fte, (-eA5_
= p^
o
ITioniLari^o^ a"P
X
e^Ploe-nL (^between 6>~R)
L/WA ReJ eASe
tip
c no sp
Spewf" p/^e^a/i'c_
,5 nscyekt/^ w<\$de
n6c^>(/2.ecJl ^ s
s/ucl^e"^
Usi^ --
(0
(X)
BPft G^,;J qnce
T^bk
^?aKio ( j (Z'Uct+i1*Ca/ /Pby<,ic*( Proper^i /
Se^
fi-pf^x Gr
Wc\<=>i^n'ccbcr'
mohdor^j
report
SAL 000005829
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
STYRENE
RELEASE (lb/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Fugitive Equipment Loss SHAD/VHAD Process Drains Cooling Tower Wastewater Trtmt Land-farm-Waste Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On--Si te (Land-farm) Off-Site
27.
726. 1. 6.
90. 56. 879.
<890)
906.
39.
0. NA
OF TOTAL RELEASE TO MEDIUM
3
80 0 1
10 6
97
100
SAL 0005830
GENERAL WASTESTREAM Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
STYRENE
TREATMENT METHOD
TREATMENT EFFICIENCY
Biological Treatment (aerobic)
Biological Treatment (aerobic)
90'/. (a) 1007- (c )
RANGE OF INFLUENT CONCENTRATION lppb-lppm(b)
1-100 ppm(d>
(a) See Table A-2 (Fate of Haz . 8</or Toxic Pol 1utants...in Wastewater Treatment Plants) in Appx G.
Cb) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
(c) Based on EPA Chemdat 6 land treatment model in Appx F.
<d> Solid waste composition data in Appx F.
$Al
00q 5q3 l
Release c^l<zulft!oa/s
Sf-yre^^
2_.C.
-- tin
PeA\zy c\r`oK^<V>c ^'sW/dT^ dHA(^
Y/PcP Is ^pr^eesSe^ wdR CLCude. X
P^)ax' ^ o w> /?wrp On 'S^e. CW c,<j| <\~hKor\5
dppx l)
Process S+re_ov K>n Co '^pOSi'f'Oh c)<*-fA
S^'C Fpp?^ E
L^ndfar^ 'Tr'fvi'f- $t'r rL-oinM Release. a les -- e A-ppx F
Wt^sfe^fer /^V- A ^v'Fc- Release. C.^lcs
see /?ypx C
(i'ocI.
ARE Se-p^rtibrs &r o'fbes' fir.^py /rl^p)
S'faf'^e. ~fa.nk CPolnf) A-.V- Rele^ie Catc.$-- S^e /^px A/
prooesS E^ypr*rf /X^y-Pi/e- Av-fle/e*se
<V\eJ.
G=o{-'*^ 7ov^er }
see /?/9^x X
SAL 000005832
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
SULFURIC ACID
RELEASE (lb/yr)
AIR POINT RELEASE Acid Plant Demister
AIR NON-POINT RELEASE Fugitives (Acid Pit,Alky,Cool Twr)
TOTAL AIR RELEASE
464. (460)
<499. (<)963.
WATER RELEASE
0.
LAND RELEASE
NA
% OF TOTAL RELEASE
TO MEDIUM
48
52 100
SAL 000005833
GENERAL WASTESTREAM
WASTEWATER
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
SULFURIC ACID
TREATMENT METHOD
TREATMENT EFFICIENCY
RANGE OF INFLUENT CONCENTRATION
NEUTRALIZATION
1007. (a)
>17. (b)
<a) Based on wastewater discharge monitoring reports <Appx G> <b) Based on data provided by Brandt Butler.
SAL 000005834
RBLE/f6 CLAL.<2ULATtofl/S
L.C
m
Po.Vrf Release "
A/d S'/d/\sv*>(2_
~tr>a
heAtfy
0)
^VP = l >~7% ^ lO ^ p%}c^)
4-^J PU*r Prsoluc^^ 73ysoo yy ?z% tf*,Sy
7^5>" "
V-S'-X-"2,.f0c0 0"/4?
/hcPol
" 23,6^2 -fens
($P-h)
^
PU^ir Derht'sfer' = 0,0^2 & release x' z^&7 Z *6>^s xO.^2 ^5y
^roelvcftt
- C/G>t/ /4 /4s^y
/V^-po.VtF /?e(a\$g ~
//> // #(
^i
Ejyp*v>"f~ A'Cf'F
pf/Cy ^ CjOo/.W^j
'pi F
iKor^o*1^ ^ ocs ^(Tcsol */^cfef^
(ixPo^fP ff^so^ pf^f- ^Ff
rp>^F?cP
-(^r~ wUol e_ pi <**-{- -- E. X A7a#ncio/)
w4teR
Release
-Q
B><\S^ =
-f ePP/oeK~ppH
KHoq, kf'.Vcj o'
^)
(between G> * ^^)
U/VD
Release. - A/4-
0) P^rryi
Cke^.`C^I
inker's
boal^
Cl) Y=\%B Blotbvk --
c-
o') /^p-^z e_ ^ '5 s,l -Rcfof-
/^opK $
(cf) \fJv.Cjie i~/<=.ier Se(-T-r^o^-repo r ~lS'""
&ppy <F
SAL 000005835
SOURCE
19SS SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
TOLUENE
RELEASE <lb/yr>
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss #3 CTU $< Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant #6 HDS FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker PBC Mol e>; SHAD/VHAD Tank Farm <F $< L) Process Drains Separators API DAF IAF Coaling Tower Wastewater Trtmt Land-farm--Waste Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On--Site (Land-farm) Of -f-Si te
14,194. (14,000)
1,006.
1,233. 1,092.
678. 4,876. 1,522.
292. 1,231.
142. 384. 2,792. 2,121. 302. 4,421.
55. 1,089. 16,618.
177.
72. 7;
1. 301 .
90. 620. 41,118.
(41,000)
55,312.
39.
O.
NA
OF TOTAL RELEASE TO MEDIUM
26
o o 1 9 w* 1 2 0 1 5 4 1 8 0 2 30 0
o 0 0 o 0 1 74
100
SAL 000005836
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
TOLUENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment < aerobic)
Biological Treatment (aerobic)
87.57. (a) 907(b)
1007(d)
RANGE OF INFLUENT CONCENTRATION
0.01 17 (a >
lppb-lppm(c)
0. 01 -17 (e)
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
(b) See Table A--2 (Fate of Haz. &/or Toxic Pol 1utants...in Wastewater Treatment Plants) in Appx G.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment <b). (Appx G)
(d) Based on ERA Chemdat 6 land treatment model in Appx F.
(e) Solid waste composition data in Appx F.
^ 0005S37
Release c,alclulations
To loen^.
L.C.
n- anuRcKC.f'ureci a<nc{ processed i'i-i+o e^o
^ ^r^d. hy<Af'dfre<xi~'t~l^ ope^ohS,
Plfi^XiiOnuiV* f\rvUt Orn Sf'fe. (3=\/c,<j/cv*fi o^5
see Appx b
Process S~fre^^
^po S
<)c\~/^=\
-- -see /fppX' E
LAnolPr^v. 'H-f^rt- f\',r ZrL^*nd Pe/e^se C*/es -- se e /Jp/z* F
VJc\S "fe <v<?v T~e. r~ /^vV- ^ ^Zpi/^r- /^e/e^se Ca/cS
see. A-pp'K G
C'^ct-
frKL Se^^r*Tbr$ or- tfTkej" *i /Kh ry Trt^t)
lank CP<D`^~i~S) /f.V* $elc asc? Ca\c$-- See /^?x /"/
Pqd c_es S E^, p *vff /X^ * "fi' \/e.
iV\cJ.
Co^K*^ T&^er' )
efe-^se *'cs -- see fitfpx X
Pr^duef Loac/'/iOj Z_oss A'''
CUtcs -- See
J-
SAL 000005838
SOURCE
1988 SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
1.2.4--TRIMETHYLBENZENE
RELEASE (lb/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker Tank Farm (P & L) Process Drains API Separator Cooling Tower Wastewater Trtmt Land-farm--Waste Trtmt.
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On--Site (Land-farm) 0-f f --Si te
167. (170)
19.
360. 1,141.
219. 923.
7S. 1,110.
139. 226. 2,941.
3 i 47. 296. 847. 8,350.
(8,400)
8,517.
9.
0. NA
Y. OF TOTAL RELEASE
TO MEDIUM
2
0
4 13
3 11
1 13
2 3 35 0 o 0
10 98
1 oo
000005^39
SAL
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1988 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
1 , 2.4-TRIMETHYLBENZENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Bi ol ogi cal Treatment (aerobic)
Biological Treatment (aerobic>
87.57. (a) 957. < b)
1007. <d>
RANGE OF INFLUENT CONCENTRATION 0.01-17. (a)
lppb --1 ppm(c >
1-100 ppm(e)
(a) According to Clyde Rhodes, L. C. Transportation, based on 1988 testing data.
(b) See Table A-2 (Fate of Haz. &/or Toxic Pol 1utants...in Wastewater Treatment Plants) in Appx G.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
(d) Based on ERA Chemdat 6 land treatment model in Appx F.
<e) Solid waste composition data in Appx F.0000053
000005340
SAV-
Release calclul/tt/o/vs
RT-M-Tr tVv'e."fUyi he^nyenp
IX*a<A pro^esSe_ci to+o go.So '
Pe-ftir^-cnxck.'^^n4 hy^^dfrea.'h'^
L.C
clun.'^^
POax'^o ^ /bvrh On
Sj-fe (3^/oc(
s^e A&&y s^e Tippy:
fc>
Pf^pce S5 S+re_ov^ Compos*
s<? e
T
l_aoo('ftpirrv' 'Trti*:*f~ f*rrLaruA Pe/eAse 0^lc,<. -- $ee (\-ppx F
dt'oc/.
/> <6~ ^vUfer-
Calc$ see >4^px <3
W'^ZT 5e^^r&"br$ <&" oiU<LT Pr'.^c^ry ~7rt'v/^)
SW^e. ~7^nP CPo'<^+) /hr /?e/e^5e C^lc^-- See ^y?x
Pr&oesS Eyp^+ PLcy\f-,Ve_ &r- R,e.(e*S* (Ll\c$-- See /^X X iV\<X bn^Vs Gaslit Ih^cr- }
Prac(uof LocJ.Vu^ Loss &:<~ /?e/e*se Calc* - see 4pk 3"
SAL 000005841
SOURCE
198B SARA 313 RELEASE INVENTORY LAKE CHARLES REFINERY
XYLENE
RELEASE <1b/yr)
AIR POINT RELEASES Storage Tanks
AIR NON-POINT RELEASES Loading Loss Fugitive Equipment Loss #3 CTU & Vac #2 CTU #4 HDS #3 CRU & HDS #1 Coker #2 Coker Gas Recovery Plant FCC Feed Prep FCC #2 CRU & HDS Thermal Cracker PBC Tank Farm <P & L) Process Drains Separators API DAF IAF Cooling Tower Wastewater Trtmt Land-farm-Waste Trtmt
Total Non-point Release
TOTAL AIR RELEASE
WATER RELEASE
LAND RELEASE On--Si te (Land-farm) Of -f --Si te
7,70S. (7,700)
631.
657. 757. 362. 3,816. 2,473. 475. 2,000. 510. 7,052. 1,469. 490. 6,803. 21,667. 131.
53.
2.
1.
470. 187. 983. 50,988.
(51,000)
58,696.
39.
0. NA
7. OF TOTAL RELEASE
TO MEDIUM
13
1
1 1 1 6 4 1 3 1 12 3 1 12 37 0
0 0
0
1 0 2 87
100
000058^2
SM- 0
GENERAL WASTESTREAM
Gaseous Wastewater
Solid Waste
1980 SARA 313 REPORTING WASTE TREATMENT METHODS AND EFFICIENCY
LAKE CHARLES REFINERY
XYLENE
TREATMENT METHOD
TREATMENT EFFICIENCY
McGill VRU
Biological Treatment (aerobic)
Biological Treatment (aerobic)
87.5V. (a) 95V. < b >
100V. (d )
RANGE OF INFLUENT CONCENTRATION 0.01-1/1 (a)
lppb--ippm <c)
0.01-17. (e)
(a) According to Clyde Rhodes, L. C. Transportation, based on 198Q testing data.
<b> See Table A-2 (Fate of Haz. 5</or Toxic Pollutants. . . in Wastewater Treatment Plants) in Appx G.
(c) Based on Lake Charles 1989 effluent analysis and estimated efficiency of secondary treatment (b). (Appx G)
(d) Based on ERA Chemdat 6 land treatment model in Appx F.
<e> Solid waste composition data in Appx F.
SAL 000005843
Release c alc.ulatic>a/s
X e*ie
L.C.
(Y]<xr-\uF^<z.JT^reA CX^A processed iVvfe go^So I
clor.'nj
re-ftr^:in^ ^crwok.'^ ^ <^n4 hyc^rd'freoXr-^ opeO'f/oni,
Pr-eseni*
io ^0(1/1^ ciy^ Cbns^'Z.e.. r^d)
==> see /nsZ)5 sc, C%>* 4)
"(drrviu l*rf*l*io
^P-^
P'Vximuiv*
On " S/fe Cal ooUf>0*^5
s^e, T^cyo X &
Process S^fce<^^ Co^posi-f/o^ <)a~/a
-- 3ee. /hpp>f f
] Ok~o( -f~c\f ni~tvni~ /?V~ $rJ--c\tndi Pe/eA se a /<cs " se e Appx F
WaSfe,w'A'f'er- /f-Zr X lA^i/er- Release. Ca/c$ see. Fppx (3
Ct'ncL /bRH Se.p<\r*iz>rs &r ofU^r
~Tri^p)
S^eoL^e.
P CPalv^t) v4~V $e/e Ase C^/c5-- S^e
//
proeeSS
Flj<y~ks/^ 4.yRefe-tse ^^5" see ^9?x X
Cind. >n*`t^S^ Gr&i-'^jj IciWCr- }
Praotuof LockcIm^ Loss
Pt:<" /?e/e.se CU/cs, -- see /`ppx 3~
sal 000005844
$4 4
00
0Os 0^5
APPENDIX A REPORTABLE TOXIC CHEMICAL LIST DEVELOPMENT
SARA TITLE III, SECTION 313 1980 TOXIC CHEMICAL RELEASE INVENTORY
LAKE CHARLES REFINERY
SAL 0005846
(conoco)
Interoffice Communication
To P f am Dale Subject
P. L. Youngblood
T- G. Waltrip
February 25, 1988
SARA Tide III - "Toxic Chemicals" List for Sec. 313 Reporting
As you requested in your IOC of February 9, 1988, we have put together a survey of the "toxic chemicals" which are listed under SARA Title III for Section 313 reporting and which may be present in refineries at or above the concentration criteria and threshold quantities as defined in the final rule on reporting requirements (FR 53, February 16, 1988).
The chemicals are divided between two tables. Table 1 contains a list of chemicals which may be present above specified de minimis concentrations and threshold quantities in crudes, intermediates and products. Table II contains a list of' chemicals which may be present in additives incorporated into products, as well as chemicals which may be used as process chemicals, catalysts, etc.
This list is by no means to be considered as complete or totally comprehensive, but only represents our best effort to narrow the scope of the reporting cask and to present a guide to be used in the reporting process. Particularly, additives and process chemicals will require a thorough search of the MSDS information and any ocher descriptive material on hand relating to these. We have attempted to err on the conservative side in estimating chemicals reportable both by concentration criteria and quantity thresholds.
Pseudocumene (1,2,4 trimethylbenzene) was not Included in the Tables, in anticipation of its removal by EPA. On the other hand, however, several chemicals have been included on Che list which may not have been present in refineries in 1987, nor currently, but which may be present in alternative processes, catalysts, etc., in future years. Also as the threshold quantities decline to 25,000 pounds by 1989, ''some not reported for 1987 may then be reportable.
We hope these lists will be a reasonable and fairly comprehensive starting point for Section 313 reporting. If you have any questions, please call OLlle Engle, who has coordinated our efforts*
cc: JEC--TLT-HAC-OFE--F:011.4
SAL 00005847
(conoco)
Interoffice Communication
To Subject
P- L. Youngblood
T. G- Walcrip
March 7, 1988
SARA Tide III
Toxic Chemicals" List for Sec. 313 Reporting
REFERENCE: Subject lecter of February 26, 1988
ADDITION TO TABLE 1
Although pseudocumene was removed from the Extremely Hazardous Substances List, you have pointed out that it is still classed as a long term hazard and therefore is still included in Che Sec. 313 Release Reporting.
A corrected copy of Table I, which includes pseudocumeme and the affected streams and products, is attached. Please attach this revised copy to my February 25 letter and discard the original Table I.
T- C. Waltrip
j<*
cc: JEC-TLT-MAC-OFE-F:011-4
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2/26/88 Page 3
SARA Title III, Sec. 313 Reporting
TABLB II
Chemicals which may be used as process chemicals or as additives in finished products.
Chemical^ ^
CAS Number
De Minimis Cone. Wt.%
Process UseU'
Blending Additive Area of Use
Diethanolamine Mb (2-ethylhexyl) adipate Ethylene Dibromide Ethylene Dichloride Ethylene Glycol
Phenol Hydrazine Sodium Hydroxide Cresol
o-Cresol m-Cresol p-Cresol Asbestos (friable) Aluminum Oxide Aluminum Lead Dust Lead Compounds-Inorganic Salts Lead Compounds-Organic Manganese & Compounds Mercury & Compounds Nickel & Compounds Antimony & Compounds Barium 6 Compounds Chromium Chromium Compounds (Hexavalent) Chromium Compounds (Other) Cobalt 6 Compounds Copper '& Compounds Molybdenum Trioxide
111-42-2 103-23-1 106-93-4 107-06-2 107-21-1
108-95-2 302-01-2 1310-73-2 1319-77-3
95-4Q-7 108-39-4 106-44-5 1332-21-4 1344-28-1 7429-90-5 7439-92-1
,
1313-27-5
1 1 0.1 0.1 1
1 0.1
1 1
L 1 1 0.1 1 1 1 0.1 1 1 1 1 1 1 1 0.1 1 l 1 1
X
X
X X X X
X X X X X X X X
X X X
X X X X X X
Amine Unit X Possible Lube Oil Additive X Leaded Gasoline X Leaded Gasoline X Refrigerant Systems; Closed Loop
Cooling Systems ' FCC Caustic Wash; Sour Water Stripper. Boiler Feedwater Treatment X Caustic Wash Systems; Greasemaking' Lube Solvent Treating; FCC Caustic Wash;
Sour Water Stripper, etc. Same as above. Same as above. Same as above. X Insulation; Asbestos Filled Asphalt X Catalysts; H/T; FCC 6 Cat Poly Mechanical Greasemaking; Mechanical Bender Sweetening X Leaded Gasoline Blending (TEL) X Leaded Gasoline Blending (MMT); Mechanical Mechanical
Catalyst X Greasemaking X Lube Blending/Greasemaking x
Mechanical Cooling Water System Treating (chromate)
(?) Catalyst X Mechanical Catalyst
- Continued -
SAL 000005850
H 10/oo Page 4
SARA Title III, Sec. 313 Reporting:
TABLE II (Cont'd)
/
Chemicals which may be used as process chemicals or as additives in finished products.
Chemical^
De Minimis CAS Number Cone. Wt.%
Process Use'*'
Blending Additive Area of Use
Vanadium (fume or dust)
7AAO-62-2
1
X
Catalyst, H/T; Mechanical
Zinc & Compounds
1 X X Lube Blending/Greasemaking;
H*S Absorbent; Water Treating
Hydrochloric Acid Phosphoric Acid
7647-01-0 7664-38-2
1 1
X X
Mechanical Cat Poly Catalyst
Hydrogen Fluoride ' Ammonia
7664-39-3 7664-41-7
.1 1
X X
HF Alkylation Refrigerant; Sour Water Stripper; NASH;
Sulfuric Acid^^
7664-93-9
1
X
Overhead Corrosion Control Cooling Water System; etc.
Nitric Acid Chlorine
7697-37-2 7782-50-5
1 1
X X
Cooling Water System; Well Water System Effluent Water System
Titanium Dioxide Acetone
13463-67-7
1
X
Mechanical (Paint)
67-64-1
1
X
X Butamer Guard Reactor Spent Adsorbent;
Greasemaking; etc.
n-Butyl Alcohol
71-36-3
1
X
X Same as above.
Sec-Butyl Alcohol tert-Butyi Alcohol
78-92-2
1
X
X Same as above.
75-65-0
1
X
X Same as above.
Carbon Disulfide
75-15-0
1
X
Sulfiding HDS Catalyst
Methyl Chloride
74-87-3
1
X
Mechanical
Dichloro Methane
75-09-2
1
X
Mechanical
Formaldehyde
50-00-0
0.1
X Lube Blending (FR Hydraulic Fluid)
Hydroquinone
123-31-9
Methanol
67-56-1
Methyl Ethyl Ketone
78-93-3
1,1,1 Trichlorethane TolueneU;
71-55-6 108-88-63
(1) Listed metals in form of either fume or dust.
1X
Boiler Feedwater Treatment
1 X X MTBE Process; Mechanical
lX
Lube Solvent Dewaxing
lX
Mechanical
1X
Lube Solvent Dewaxing; Mechanical
Metals in the form of articles and which are not released to the
Environment are not reportable.
(2) Process use category includes mechanical in this list.
(3) Sulfuric Acid and Toluene also appear in Table 1, crudes, intermediates and products.
Or
Jos
*s,
P. L. Youngblood 2/25/88 Page 5
SARA Tide 111, Sec. 313 Reporting
Addendum to Tables 1 & IX
Chemicals in Tables I & II which were listed carcinogens (de minimis concentration of 0-1 percent) were determined by W. D. Broddle, per 29 CFR 1910-1200 (d)(4), through a search of
(1) (2) (3)
IARC Monographs NTP Reports OSHA 29 CFR Part 1910, Subpart Z,
as:
Asbestos Benzene 1,3 Butadiene Hexavalent Chromium Ethylene Dibromide Ethylene Dichloride Formaldehyde Hydrazine Lead Compounds (Inorganic salts only)
0OOOOS85Z SM-
POTENTIALLY REPORTABLE TOXIC CHEMICALS UNDER SARA 313
MOST LIKELY
POSSIBLY (Mosc Have Been Eliminated)
Benzene* Ethylene Naphthalene Biphenyl Xylenes 1-Methylethyl benzene (Cumene) Ethyl benzene Styrene 1,3 Butadiene* Toluene Cyclohexane Propylene MTBE Sulfuric acid Phenol Ethylene dibromide* Ethylene dichloride* Sodium hydroxide Cresol Aluminum oxide Manganese Compounds Hydrogen fluoride Ammonia Methanol MEK 2 Methoxy ethanol Molybdenum trioxide Nickel ico^pou^A.s') Chlorine Diethanolamine Hexavalent Chromium* Zinc (fume or dust) Phosphoric acid 1,2,4 Trimethylbenzene (Psuedo Cumene) 1,1,1 Trlchloro Ethane
Carbon Tetrachloride Lead (Organic)
Bis (2 ethylhexyl) adipate Hydrazine* Ashes tos* (landfilled) Cobalt (c-or*
Lead (Dust, Inorg. Salts*) Mercury
Nitric Acid Titenium dioxide- (c(clfet'Cci
Acetone Methyl chloride Dichloroethane Hydroquinone Hydrochloric acid Butyl alcohols Formaldehyde* Ammonium sulfate Ethylene glycol Antimony
)
Barium
)
Copper Dichloromethane Carbon disulfide
Freon 113 Vanadium ( cor^pou r,d S )
Isopropanol Aluminum Anthracene
t St?
Z
(_co^pooled s
* Carcinogen subject to deminiiiius concentration of 0.1 vtZ. chemicals have deminimus concentrations of 1.0 wtZ.
All other
Ouc.ie EmGtCc. L*.vr <-<1-15-88}
AP'X Mo^n Ki-Gr-
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SA<- 000005860
Research Report No. 1803-152-010-1-89 Page 48
SAL 0 0 0 0 0 5 8 6 1
Waste Stream Vent Scrubber
System Backflush API Separator Sludge
API Separator Sludge
Tank 55 Sump
Spent Phenolic Caustic
DAF Float
$LSl
Plant Seaford
APPENDIX 1 (CONTINUED) WASTE STREAM CHEMICAL CHARACTERISTICS
Typical Chemical Characteristics
Lake Charles Refinery
Billings Refinery
Billings Refinery
Billings Refinery
pH-6.7 TOC--7.9% Oil & Grease--6.1% Extractable hydrocarbon--8.2%
18% solids 64% moisture Extractable hydrocarbon--8% TOC--8%
COD--250,000 ppm Phenols--60 ppm Extractable hydrocarbon--1%-2%
5% caustic Phenols--5,000-10,000 ppm
Billings Refinery
2% solids Extractable hydrocarbon--4,600 ppm
Chemical Characteristics of Waste Sample Treated
pH-8.8 COD--3,308 ppm TOC--1,050 ppm
pH-6.7 COD--667,060 ppm TOC--215,400 ppm
pH-7.5 COD--353,542 ppm TOC--62,600 ppm
pH--10.9 COD--41,554 ppm TOC--10,900 ppm
.pH-12 COD--65,562 ppm TOC--5,900 ppm
pH-6.5 COD--61,784 ppm TOC--27,600 ppm
/Victerobi'c.
L>,'/'-fy Screen',^
JXRsnt
1^5 -/eWer5
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Research Report No. 1 $03-152-010-1-89 Page 8
TABLE 2
PONCA CITY REFINERY SPENT CAUSTIC AND SABINE AON WASTE CHARACTERISTICS
Spent Caustic
AON
COO--45,000 mg/L Phenols--8,130 mg/L pH--12.5
COD--5,595 mg/L Cyanide--816 mg/L
Nitriles--1,630 mg/L pH--9 (caustic added to prevent
cyanide volatilization)
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SAL 000005865
Interoffice Communication
TO: Dave Kersey, Lake Charles Refinery
FROM:
Paul Steele, PED, Ponca City
DATE:
March 8, 1989
SUBJECT: SARA Title III, Section 313 - 1988 Used Chemical Information
A MSDS scan has been run by Environmental and Occupational Health Services to determine materials which contain toxic chemicals listed under SARA Title III, Section 313 that were purchased and used by each refinery in 1988. Enclosed is a list of applicable materials used by the Lake Charles Refinery during 1988, giving the specific name of the material, its manufacturer, and the area in which it was used.
The amount of each chemical used in each area during 1988 and an estimate of the maximum amount stored on-site are needed to comply with SARA 313 reporting requirements. It is requested that this information be filled out on the enclosed list and returned to me by April 3. This will allow me time to determine if the amounts used during 1988 meet the reporting threshold, and if so, to estimate the amount released to air, water, or land.
This information should be available through either Plant inventory records or the Plant safety director. Please include the units of measure (gal, lb) with the estimates. An asterisk (*) has been placed by the materials for which th purpose of usage is undetermined. If possible, please provide a brief definition (i.e. paint. degreaser. weed killer, etc.) of the manner in which these chemicals were used. Certain uses of listed chemicals are specifically exempt from reporting (structural components, routine janitorial or grounds maintenance, and automobile maintenance). This description will ensure that releases from these exempted activities are not included in the 313 reports.
Please contact me if you have any questions or expect any difficulty in meeting this request.
Chemical Engineer Environmental Process Engineering Division
Approved by:
Ik att cc: DFM:LWC:KLK
Jack Cearley, Houston cc(w/o att): Brandt Butler, File EV-1040.1
Lake Charles
Refinery
C/.
SAL 000005866
Listed below are the Area Sections for the Lake Charles Refinery: 00 Refinery Wide 10 Tank Farm, Pump, Blend 12 Power Plant 14 Laboratory 20 Combination (Aik, Acd, Slf) 30 Fluid Cat Cracker 40 Reformer 50 Premium Coke 60 Sour Crude/Refined Crude 62 CDR 70 Ethylene Feed Stock 80 Docks 90 Machine Shop 99 Warehouse
SAL 000005867
LAKE CHARLES REFINERY PROCESSING SUPPLIES
Description (Manufacturer1)
Area Code
Anti-Sieze 228* (Hi-Port Industries Inc.)
V
2J Denstone 57 All Sizes* (Norton Co.)
00 00
3. Katalco 477 (Katalco Corp.)
* i- 1 40
4. PSA Adsorbent H-l (Union Carbide Corp.)
5. Shell Catalyst 324 6. Shell Catalyst 424 7. Shell Catalyst 444 8. Shell Catalyst 514 9. Shell Catalyst 544
(Shell Oil Co.)
C/i f 60
S > 1 >'" " '
f- 'x x/
r. * 'r
40 60 70 60 70
10. Union Carbide Molecular Sieve
Type 13X
cn'v
11. Union Carbide Molecular Sieve
Type 3A
12. Union Carbide Molecular Sieve
Type 13XPG
13. Union Carbide Molecular Sieve <;
Type 3AEPG
(Union Carbide Corp.)
14. Anhydrous Ammonia (Jupiter Chemicals Inc.)
/* )
15. Aqua Ammonia
t
(McKesson Chemical Co.)
30 30 30 30
50
30 70
16. Benzene (J. T. Baker Chemical Cc>-) '
40
17. Vista NPSO Solvent (Vista Chemical Co.)
* * i
40
Amount Used in 1988
144fto
~u}%00 nAoo Ajioo
5*77^
Max. Amount Stored
(OooO
\ \}ooo
~7000 Z20O
*Please describe how these items are used.
LAKE CHARLES REFINERY PROCESSING SUPPLIES (Cont.)
Description (Manufacturer}
Area Code
C/ '
18. Chlorine
00
(Thompson-Hayward Chemical Co.)
12
(Van Waters & Rogers Inc.) ,
20
r v ' 60
19. Hydrogen Treating Catalysts (American Cyanamid Co.)
20
DF A
20. Diethanolamine / r f(Union Carbide Corp.)
--v
/i /
30 50 60
21. Gasguard* (National Chemsearch Div. of NCH Corp.)
00
A 22. Oil Bronze Liquid
(DuPont)
v..,
10
23. '05/Dc.
24.
--
25.
Motor Fuel Antiknock Compound (Ethyl Corp.)
10
Ethylene Dichloride (Vista Chemical Co.)
80
Betz 409 (Betz Laboratories Inc.)
- v' 12
CMC-(
26. Cortec 347* (Sealed Air Corp.)
50
27. Gasket Eliminator 504 Sealant (Loctite Corp.)
00
_ X. 4 <>$e 2 29.
--
. r30.
No. 1000 Green Concentrate* (Meriam Instrument)j /.''jo o /F -<>e* (O' S
Ce>%-*r-0u-fy PD Activator, Developer* (Bruning)
Formalin (General Electric)
00
00
20 60
Amount Used in 1988
1
t Ifionto fy > it.
7 7oo Jb
o
o
\
Max. Amount Stored
/ lb
-Please describe how these items are used.
SAL 000005869
LAKE CHARLES REFINERY PROCESSING SUPPLIES (Cont.)
/< (
r
-./.
C- ry!
` / /*
Description (Manufacturer)
Area Code
Amount Used in 1988
31. Hydrochloric Acid
' ' 12
(Van Waters & Rogers Inc.)
- : 70
Sjt&jToe
32. Hydrofluoric Acid-Anhydrous (DuPont)
00
33. Hydroquinone* (Carus Chemical Co.)
'
80
34. Brilliance Aerosol (National Chemsearch)
00
35. Dura-Gard Aerosol
.
(National Chemsearch Div.
of NCH Corp.)
00
36. Kontol K-450* (Petrolite Corp.)
^ 30
37. Petrotec K-602* (Petrolite Corp.)
/
30
38. State Clr Aerosol
v
(State Chemical Mfg. Co.) '
00
39. Carb Care Aerosol
,v
(National Chemsearch Div.
of NCH Corp.)
00
40. Copaltite*
00
(National Engineering Products Inc. )
41. Kontol K-437* (Petrolite Corp.)
20
42. Methanol (Celanese Chemical Co. Inc.)
30 80 -
(OOO
43. Petrotec Petl330* (Petrolite Corp.)
^ 20
44. Methyl Tertiary Butyl Ether
10
(Valero Refining & Marketing Co.)
80
4qooo
Max. Amount Stored
'L'UO f
*Please describe how these items are used.
0000
LAKE CHARLES REFINER? PROCESSING SUPPLIES (Cont.)
i
Description (Manufacturer')
45. C29-2-02 (United Catalysts Inc.)
./V
46.
i/t)-
^47.
Tretolite DS-505 (Petrolite Corp.)
Heavy Aromatic Distillate (DuPont)
48. Light Fuel Oil (DuPont)
Area Code
r-- 20
' r 20
' r/V
/Cl V
10 70 80
10
Amount Used in 1988
HptoS
f4-7, ooo
U plA
49. Light Aromatic Concentrate 7 (Vista Chemical Co.)
50. Light Aromatic Distillate (Conoco Chemicals)
10 30 70 ^
10 ' 30 70^
} ooo
51. Nalco 5186 Corrosion Inhibitor t*'- 70 :
52. Nalco 5701 Process Antifoam
70 5&o
53. Nalco 87RC130
60 ^aop
(Nalco Chemical Co.)
{tope3 f^.'cC^C!
54. NR. 725 Nickel Anti-Seize Compound (Bulk)*
(A. W. Chesterton Co.)
55. Nitric Acid (J. T. Baker Chemical Co.)
\
00 00
56. Phosgene (Union Carbide Corp.)
00
57. Alphachem 3212 Acid Cleaner (Alpha Chemical Co.)
50 60
58. Betz 40P (Betz Laboratories Inc.)
12 o
59. Chemets and Vacuettes R-8510 , (Microbe Masters Inc.)
20
Max. Amount Stored
SS'o
9>0
*Please describe how these items are used.
SAL 000005871
LAKE CHARLES REFINERY PROCESSING SUPPLIES (Cont.)
Description (Manufacturer1)
60. Molybdate Reagent for P04 (Betz Laboratories Inc.)
61. Phosphate Chemets R-8510 (Chemetrics Inc.)
62. Silica 1 Reagent (Betz Laboratories Inc.)
63. Sulfuric Acid Solution, 10N (Betz Laboratories Inc.)
64. Trill* (National Chemsearch Div. of NCH Corp.)
65. Molybdate 3 Reagent for Silica (Hach Co.)
Area Code
20 20 20 20 00
20
66. Ammonium Molybdate Reagent for Silica
(Hach Co.)
67. Activator/Clear Vgy 511* (DuPont)
12
20
00
68. Carbomastic 14* (Carboline Co.)
69. T3871* (DuPont)
00 90
00 90
70. Toluol (Fisher Scientific)
71. "Ethyl" MMT Dilute (Ethyl Corp.)
20 10
72. Alphachem 2061 Degreaser 73. Alphachem 2063 Degreaser
(Alpha Chemical Co.)
00 60 70
74. C.I. Solvent Red 164 (DuPont)
10
*Please describe how these items are used
Amount Used in 1988
3 %oo
Max. Amount Stored
)A^0
00000581
SAL
LAKE CHARLES REFINERY PROCESSING SUPPLIES (Cont.)
Description ( Manufacturer-)
75. DCI-6* (DuPont)
76. Diesel Guard (National Chemsearch Div. of NCH Corp.)
77. DMD-2* (DuPont)
Area Code
10
00
70
78. DuPont Corrosion Inhibitor No. 4A " 10 (DuPont)
79. DuPont Metal Deactivator (DuPont)
Z
80. FOA-11* (DuPont)
81. Petromeen AF111 82. Petromeen EB911
(Betz Process Chemicals Inc.)
70
10
60 40
83. Zinc Re-Nu (Aerosol) 3074* (CRC Chemicals)
> 00
84. Alphachem 2056 Solvent Emulsion (Alpha Chemical Co.)
70
85. Aztron EMC 4*
-> 90
(Aztron Chemical Services Inc.)
86. Brake Job Aerosol (National Chemsearch)
87. Cable Cleaner 2069 88 . Cable Cleaner 2087
(CRC Chemicals)
90
00 00
89. Chlorothene SM Solvent (Dow Chemical USA)
20
Amount Used in 1988
soo
Max. Amount Stored ooo
5000
ID Jfi)
^Please describe how these items are used.
SAL 000005873
LAKE CHARLES REFINERY PROCESSING SUPPLIES (Cont.)
Description (Manufacturer)
Area Code
90. Electrical Quality Silicone (CRC Chemicals)
00
91. Eze-Way Aerosol (National Chemsearch Div. of NCH Corp.)
00
92. Lectra Clean (Aerosol) No. 2018 (CRC Chemicals)
00
93. PJ1 Heavy Duty Chain Lube (PJ1 Corp.)
-i
00
94. State GRS* (State Chemical Mfg. Co.)
00
95. Tri-Ethane 348 (PPG Industries Inc.)
__ r
40
96. Trichloroethane 111 600 (Thompson-Hayward Chemical Co.)
00
Amount Used in 1988
Max. Amount Stored
*Please describe how these items are used.
00000581 SM-
ACHIEVING
EXCELLENCE
TO: Dana Burke, PED
FROM:
M. Gene Hopkins, Refining
DATE:
May 2, 1988
SUBJECT: TITLE III - SECTION 313 - CHEMICALS USED
The attached list of chemicals used In the Ponca City Refinery In 1987 is a confirmation of the data supplied on April 26, 1988. A list of refinery vents and their sizes are also Included.
If there are any questions about this Information or If additional information is needed, telephone me on Extension 4346.
M. Gene Hopkins Safety and Health Supervisor Ponca City Refinery
bs Enc. cc: HRA
(conoco)
SAL 000005875
Ponca City Refinery
Sulfuric acid -- 1,693,420 lbs. used in 1987
Selecto - 233,127 lbs. added in 1987 (80Z phenol - 20Z c&cISolic acid) SSST' |S f\CCoRt>JNG ~i'0 Lu iA.
Sodium Hydroxide
50Z Solution - 1,605,680 lbs. (dry weight)
Flake
- 106,800 lbs. (Sat. Gas Propane Dryers)
1,712,480 lbs.
Aluminum Oxide
Activated Alco Aluminai 90 - 95Z - 96,770 lbs. (Chloride - Reactors) Activated Bauxite (Engelhard) - 360,071 lbs. added in 1987 to Filterhouse Clay Pall Pneumatic DE-39 100Z - 3,480 lbs. added in 1987 Air Dryers Tabular T-162 Alumina 99.5Z - 35,240 lbs. used in Reactors at Alky and
No. 2 CRU Reactors No. 4 FCC Catalyst 20 - 75Z - 1,052,659 lbs. added in 1987 No. 5 FCC catalyst 20 -- 1ST -- 1,676,720 lbs. added in 1987
Spent Caustic Returned -- 2,355,178 lbs. in 1987.
-Hydrogen Fluoride -- 566,660 lbs. added in 1987.
'Ammonia - 29,700 Lbs. added in 1987.
"Methanol -- 23,436 lbs. used in Refinery 1987 - 4,538,898 lbs. used in MTBE Unit 1987
Antioxident No- 23 (50Z Methanol) -- 22,232 lbs. added in 1987. Methanol content - 11,116 lbs.
Methyl Ethyl Ketone -- 253,057 lbs. added to MEK Unit in 1987.
2-Methoxyethanol -- 637,660 lbs. into Ponca City Refinery -- 13,952 lbs. sent to Grease Plant in 55-gal. drums 623,708 lbs. used in Refinery.
Chlorine - 456,000 lbs. used in the Refinery in 1987.
Diethanolamine (85Z) -- Started 1987 with 17,932 lbs. in inventory. Added 16,320 lbs. in 1987. Closed out all DEA 11,832 lbs. on 10-09-87.
Toluene - 503,962 lbs. added in 1987 of which 63,800 lbs. sent to R&D, leaving 440,162 lbs. used in Refinery.
1,1,1 Trichloroethane--10,656 lbs. used in Refinery in 1987.
Carbon tetrachloride -- 88,387 lbs. used in Butamer in 1987.
Xylene - 11,520 lbs. used in gasoline dyes in 1987. Fuel Oil Additive No. 208 (33Z xylene) - 39,208 lbs. used in 1987.
SAL 000005876
Listed below are the Area Sections for the Lake Charles Refinery:
00 10 12 fT#'! "20 30 40 50 60 62 70 80 90 99
Refinery Wide Tank Farm, Pump, Blend Power Plant Laboratory Combination (Aik, Acd, Slf) Fluid Cat Cracker Reformer Premium Coke Sour Crude/Refined Crude CDR Ethylene Feed Stock Docks Machine Shop Warehouse
msfts - Hiss sc^
EnV<
-Ui Er
Leu L
f\ac.c'*^e
S^r^/e* IfSy$-(~e.*vC^
voni
|4^/-fA
Se^^cts
E*~fy
00005871 SAL 0
FEB 01, 1989
iTONE
AREA/ SECT CODE
ACETONE 14 PLANT LABORATORY-QC
GTA409 (4-079) 10 RECEIPT/STORAGE/HOYEMENIS UNIT
KRYLOH INT./EXT. ENAMEL OR ENGINE COLOR 00 PLANT-HIDE/FIELD, MAINTENANCE
KRYLOH SPRAY PRIMER 00 PLANT-HIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COHPOtENTS
TASK ROLES CODE
MANUFACTURER
> 99.0 999.9
F DELTA DISTRIBUTORS INC.
10.0 10.0
CBSO D
INTERNATIONAL PAINT
36.0 37.0
CBSO D
BORDEN
33.0 33.0
CBSO
D D
BORDEN BORDEN
PAGE 1.
S4t 00000
FEB 01, 1989
ALUMINUM DRUM
AREA/ SECT CODE
100S/3080 PHOTORECEPTOR 00 PLANT-HIDE/FIELD, SRVCS-ENGft,l
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
D XEROX CORP.
> 95.0 999.9
PAGE 2
SAL 000005879
FEB 81, 1989
. _JHINUH FLAKE
AREA/ SECT CODE
ANTI-SIEZE 220 00 PLAHT-MIDE/FIELD UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE MANES OF COMPONENTS
PAGE 3
TASK ROLES CODE
manufacturer
> 3.0 999.9 0 HI-PORT INDUSTRIES INC.
>r '/
SAL 000005880
FEB 01, 1909
ALUMINUM OXIDE
AREA/ SECT CODE
DENSTONE S7 ALL SIZES 00 PLANT-WIDE/FIELD UNIT
KATALCO *>77 AO CAT REFORM, W/O HYDROGENATION AO HYDROGEN TREATING UNIT
PSA ADSORBENT H-l 60 HYDROGEN TREATING UNIT
SHELL CATALYST 32A AO CAT REFORM, W/0 HYDROGENATION AO HYDROGEN TREATING UNIT
SHELL CATALYST A2A 60 HYDROGEN TREATING UNIT 60 PLANT-WIDE/FIELD, OPERATIONS
SHELL CATALYST AAA 70 CRUOE PROCESSING UNIT
SHELL CATALYST S1A 60 HYDROGEN TREATING UNIT
SHELL CATALYST SAA 70 CRUDE PROCESSING UNIT
UNION CARBIDE MOLECULAR SIEVE TYPE 13X 30 CRVOGEMIC FUEL GAS UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
HORTON CO.
C KATALCO CORP. C KATALCO CORP.
UNION CARBIDE CORP.
.0 999.9 .0 999.9 .0 30.S
C SHELL OIL CO. C SHELL OIL CO.
C SHELL OIL CO. C SHELL OIL CO.
C SHELL OIL CO
C SHELL OIL CO
C SHELL OIL CO.
.0 999.9 999.9 999.9
.0 999.9
D UNION CARBIDE CORP.
PACE 9.
*l X\
v, %\ X 'J
S*L 00
OoSQ#-.
FEB 01, 1009
i-UMINUH OXIDE
AREA/ SECT CODE
UNION CARBIDE MOLECULAR SIEVE TYPE 3A 30 CRYOGENIC FUEL CAS UNIT
UNION CARBIDE MOLECULAR SIEVE 15XPG 30 CRYOGENIC FUEL GAS UNIT
UNION CARBIDE MOLECULAR SIEVE 3AEPC 30 CRYOGENIC FUEL GAS UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
< 0 UNION CARBIDE CORP.
< C UNION CARBIDE CORP.
< C UNION CARBIDE CORP.
.0 45.0 .0 30.0 .0 AS.0
PACE S
*/
A/
SAf- 000005882
FEB #1, 1969
AWfOHlA
AREA/ SECT CODE
ANHYDROUS AMMONIA 56 COKING UNIT
AQUA AMMONIA 30 CRUDE PROCESSING UNIT 70 CRUDE PROCESSING UNIT
SOUR HATER STRIPPER ACID GAS 20 SULFUR RECOVERY, CLAUS 20 CAT CRACK, FLUID-BED W/O H2S R
STATE CLR AEROSOL 00 PLANT-HIDE/FIELD, MAINTENANCE
STATE HGP HIGH GLOSS PROTECTANT 00 PLANT-HIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PAGE
TASK ROLES CODE
MANUFACTURER
99.6 99.8
D JUPITER CICMICALS INC.
28.0 30.0 D MCKESSON CHEMICAL CO. D MCKESSON CHEMICAL CO.
.0 999.9
C CONOCO INC. C CONOCO INC.
< .0 1.0
DXXX D
STATE CHEMICAL MFG. CO.
< .0 1.0
DXXX 0
STATE CHEMICAL MFC. CO.
/
-JL ^
/ V
SAL 00005883
FEB 01, 1989
..sEHIC
AREA/ SECT CODE
100S/3060 PHOTORECEPTOR 00 PLANT-WXDE/FIELD, SRVCS-ENGR,!
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE HANES OF COMKMEMTS
TASK ROLES CODE
HANUFACTURER
D XEROX CORP.
30.0 35.0
PAGE 7
SAL 000005884
FEB 01, 19*9
ASBESTOS
AREA/ SECT CODE
CHRYSOTILE ASBESTOS 00 NO PROCESS CODE
PYROCRETE 102 70 PLANT-WIDE/FIELD, MAINTENANCE
LUCE OURLES REFINERY REPORT LIST
FOR TRADE NAMES OF CWONEHTS
TASK ROLES CODE
MANUFACTURER
0 GENERAL ELECTRIC
<
CBSO D
CAR&OL1NE CO.
.0 999.9 .0 1.0
PACE a.
SAL 000005885
FEB 01, 1989
. _NZEHE
AREA/ SECT CODE
BENZENE
1* PLANT LABORATORY-OC 40 CAT REFORM, W/0 HYDROGENATION
CASINGHEAD GASOLINE
20 THERMAL CRACKING UNIT
COKER NAPHTHA
10 RECEIPT/STORAGE/HOVEMENTS UNIT SO COKING UNIT 60 COKE, DELAYED-FUEL GRADE W/ H2
CRUDE OIL (SOUR)
0 RECEIPT/STORAGE/HOVEMENTS UNIT 70 CRUDE PROCESSING UNIT 80 DOCK OPERATIONS UNIT
CRUDE OIL (SWEET)
10 RECEIPT/STORAGE/MOVEMENTS UNIT 30 CRUDE PROCESSING UNIT 70 CRUDE PROCESSING UNIT 60 DOCK OPERATIONS UNIT
CTU OVERHEAD/DEBUTANIZER GAS
30 CRUDE PROCESSING UNIT 40 CAT REFORM, W/O HYDROGENATION 70 CRUDE PROCESSING UNIT
HEAVY AROMATIC DISTILLATE
10 RECEIPT/STORAGE/MOVEMENTS UNIT 70 CRUDE PROCESSING UNIT 80 DOCK OPERATIONS UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PACE 9.
TASK ROLES CODE
MANUFACTURER
90.0 100.0 EF J. T. BAKER CtEHICAL CO. EF J. T. BAKER CHEMICAL CO.
.0 999.9
C CONOCO INC.
AC CONOCO INC. AC CONOCO INC. AC CONOCO INC.
C CONOCO INC.
c CONOCO INC. c CONOCO INC.
c CONOCO INC.
C CONOCO INC.
c CONOCO INC.
c CONOCO INC.
c CONOCO INC. c CONOCO INC. c CONOCO INC.
c DU PONT c DU PONT c DU PONT
.0 999.9 .0 999.9
.0 999.9
ZS.O 3S.0
x;
SAL 000005886
FEB 81, 1989
BENZENE
AREA/ SECT CODE
ICAVY BLEND FEEDSTOCK
SO CRUDE PROCESSING UNIT 70 CRUDE PROCESSING UNIT
HEAVY CATALYTIC CRACKED NAPHTHA
10 RECEIPT/STORAGE/MOVEHENTS UNIT SO CAT CRACK, FLUID*-BED W/0 H2S R
HEAVY CATALYTIC REFORMED NAPHTHA
90 CAT REFORM, W/O HYDROGENATION 70 CAT REFORM, W/ HYDRO W/ K2S RE
HEAVY STRAIGHT RUN NAPHTHA
10 RECEIPT/STORAGE/MOVEMENTS UNIT ZO THERMAL CRACKING UNIT 30 CRUDE PROCESSING UNIT 90 CAT REFORM, W/O HYDROGENATION 90 HYDROGEN TREATING UNIT 60 HYDROGEN TREATING UNIT 60 PLANT-WIDE/FIELD, OPERATIONS 70 CAT REFORM, W/ HYDRO W/ KZS RE 70 CRUDE PROCESSING UNIT
HEAVY THERMAL CRACKED NAPHTHA
ZO THERMAL CRACKING UNIT 90 CAT REFORN, W/O HYDROGENATION 50 COKING UNIT 60 CRUDE PROCESS, VIRGIN LT ENDS 60 HYDROGEN TREATING UNIT 60 PLANT-HIDE/FIELD, OPERATIONS
HYDRODESULFURIZED HEAVY NAPHTHA
90 CAT REFORM, W/O HYDROGENATION 90 HYDROGEN TREATING UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAICS OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
C CONOCO INC. C CONOCO INC.
C CONOCO INC. C CONOCO INC.
C CONOCO INC. C CONOCO INC.
C CONOCO IHC. C CONOCO INC. C CONOCO INC. C CONOCO INC. C CONOCO INC. C CONOCO INC. C CONOCO INC. C CONOCO INC. C CONOCO INC.
C CONOCO INC. C CONOCO INC. C CONOCO IHC. C CONOCO INC. C CONOCO INC. C CONOCO IHC.
C CONOCO INC. C CONOCO INC.
.0 999.9 .0 999.9 .0 999.9 .0 999.9
.0 999.9
.0 999.9
sal oooo
FEB 01, 1989
rtZEME
AREA/ SECT CODE
HYDRODESULFURIZES LIGHT NAPHTHA
AO CAT REFORM, M/O HYDROGENATION AO HYDROGEN TREATING UNIT
LEADED REGULAR GASOLINE
10 RECEIPT/STORAGE/MOVEMENTS UNIT
LIGHT AROMATIC CONCENTRATE
10 RECEIPT/STORAGE/NOVEMENTS UNIT 30 PLANT-WIDE/FIELD, OPERATIONS 70 CRUDE PROCESSING UNIT
LIGHT AROMATIC DISTILLATE
0 RECEIPT/STORAGE/MOVEMENTS UNIT 30 PLANT-HIDE/FIELD, OPERATIONS 70 CRUDE PROCESSING UNIT
LIGHT CATALYTIC CRACKED NAPHTHA
10 RECEIPT/STQRAGE/MOVEHEHTS UNIT 30 CAT CRACK, FLUID-BED W/O H2S R
LIGHT CATALYTIC REFORMED NAPHTHA
AO CAT REFORM, M/0 HYDROGENATION 70 CAT REFORM, W/ HYDRO / H2S RE
LIGHT FEEDSTOCK - SM
10 RECEIPT/STORAGE/MOVEMENTS UNIT 30 CRUDE PROCESSING UNIT 60 HYDROGEN TREATING UNIT 60 PLANT-HIDE/FIELD, OPERATIONS 70 CRUDE PROCESSING UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMKMEMTS
PAGE II
TASK ROLES CODE
MANUFACTURER
CONOCO INC. CONOCO INC.
CONOCO INC.
.0 999.9 .0 999.9
VISTA CHEMICAL CO. VISTA OCHICAL CO. VISTA CHEMICAL CO.
CONOCO CHEMICALS CONOCO CHEMICALS CONOCO CHEMICALS
AO.O 50.0
7
f/
CONOCO INC. CONOCO INC.
CONOCO INC. CONOCO INC.
.0 999.9
CONOCO INC. CONOCO INC. CONOCO INC. CONOCO IHC. CONOCO INC.
S4L 0005888
FEB 01, 1959 BENZENE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
LIGHT STRAIGHT RUN CASOLXIC
10 RECEIPT/STORAGE/HOVEHEHTS UNIT so CRUDE PROCESSING UNIT AO HO PROCESS CODE 70 CRUDE PROCESSING UNIT
LIGHT STRAIGHT RUN GASOLINE INTERMEDIATE STREAM
10 RECEIPT/STORACE/HOVEMEHTS UNIT 20 NO PROCESS CODE 30 CRUDE PROCESSING UNIT AO CAT REFORM, W/0 HYDROGENATION AO NO PROCESS CODE 70 CRUDE PROCESSING UNIT
LIGHT THERMAL CRACKED NAPHTHA
20 THERMAL CRACKING UNIT AO CAT REFORM, W/O HYDROGENATION SO COKING UNIT 60 CRUDE PROCESS, VIRGIN LT ENDS 60 PLANT-HIDE/FIELD, OPERATIONS
NAPHTHA
10 RECEIPT/STORAGE/HOVEHENTS UNIT 50 DOCK OPERATIONS UNIT
STABILIZER OVERHEAD LIQUID
AO CAT REFORM, W/O HYDROGENATION 70 CAT REFORM, U/ HYDRO U/ HZS RE
SUPER UNLEADED CASOLINE
10 RECEIPT/STORAGE/KOVEHENTS UNIT
A CONOCO INC. A CONOCO INC. A CONOCO INC. A CONOCO INC.
C CONOCO INC. C CONOCO INC.
c CONOCO INC. c CONOCO IHC. c CONOCO IHC. c CONOCO INC.
C CONOCO INC.
c CONOCO INC.
C CONOCO INC.
c CONOCO INC. c CONOCO INC.
AC CONOCO INC. AC CONOCO INC.
C CONOCO INC.
c CONOCO INC.
A CONOCO INC.
. 999.9 . 999.9
.0 999.9 .0 999.9 .0 999.9 .0 999.9
PACE 12
SAL 000005889
FES 01, 1909
_HZENE
AREA/ SECT CODE
SWEETENED NAPHTHA
40 CAT REFORM, W/0 HYDROGENATION TAIL GAS STREAMS
00 PLANT-HIDE/FIELD UNIT 40 CAT REFORM, M/0 HYDROGENATION SO COKING UNIT 60 CRUDE PROCESS, VIRGIN LT ENDS 60 PLAHT-HIDE/FIEL-O, OPERATIONS UNLEADED GASOLINE 10 RECEIPT/STORACE/MOVEHENTS UNIT VISTA HPSO SOLVENT 40 HYDROGEN TREATING UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE HARES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
C CONOCO INC.
c CONOCO INC. c CONOCO INC. c CONOCO INC. c CONOCO INC. c CONOCO INC.
A CONOCO INC.
SC VISTA CHEMICAL CO.
.0 999.9 .0 999.9
.0 999.9 .2 1.0
PACE 13
SAL 000005890
FEB 01, 1909
BUTYL ALCOHOL
AREA/ SECT CODE
KRYLON INT./EXT. ENAMEL OR ENGINE COLOR 90 PLANT-WIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMNMCNTS
TASK ROLES CODE
MANUFACTURER
CB59 D
BORDEN
< .0 3.0
PAGE 10
$4*.
0005892
FEB 91, 1989
i3BOH TETRACHLORIDE
AREA/ SECT CODE
CARBON TETRACHLORIDE 14 PLANT IABORATORY-OC
LAKE CHARLES REFINERY REPORT LIST
FOR TRACE MAKES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
90.0 100.0 F J. T. BAKER OCHICAL CO.
PAGE 13
$Al 0oOosq 9a
FEB 01, 1909
CHLORINE
AREA/ SECT CODE
CHLORINE
00 PLAMT-WIDE/FIELQ UNIT 12 UTILITY UNIT 20 SULFURIC ACID MFG, CONTACT 60 UTILITY, PUMP HOUSE (COOLING T
99 .5 99.5
00 PLANT-HIDE/FIELD UNIT 12 UTILITY UNIT 20 SULFURIC ACID MFC, CONTACT 60 UTILITY, PUMP HOUSE (COOLING T
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
100.0 100.0
D THOK>SOH-HAWARD CHEMICAL CO. 0 THOMPSON-HAYWARD CHEMICAL CO. D THOMPSON-HAYWARD OCHICAL CO. D THOMPSON-HAYWARD OCHICAL CO.
*
D VAN WATERS A ROGERS INC. D VAN WATERS * ROGERS INC. D VAN WATERS A ROGERS INC. D VAN WATERS A ROGERS INC.
*
PACE 1
V
SAL 000005893
FEB 01, 1969
.OBALT
AREA/ SECT CODE
HYDROGEN TREATING CATALYSTS 20 SULFUR RECOVERY, CLAUS
LAKE CHARLES REFIICRY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
O AMERICAN CYAMAMID CO.
999.9
PAGE 17 l/
SAL 000005894
FEB 01, 1989
CUMENE HYDROPEROXIDE
AREA/ SECT CODE
ADHES1VE/SEALAHT 2*2 00 PLANT-WIDE/FIELD, MAINTENANCE
ADHESIVE/SEALANT 271 00 PLANT-WIDE/FIELO, MAINTENANCE
CASKET ELIMINATOR 50* SEALANT 00 PLAMT-UIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE MAHES OF COMNMEMTS
TASK ROLES CODE
MANUFACTURER
D LOCTITE CORP. D LOCTITE CORP. D LOCTITE CORP.
< .0 2.0
2.0
5.0
Z.O
2.0
PAGE 18
SAL 000005Q95
FEB PI, 1949
.THANOLAHINE
AREA/ SECT CODE
DIETHANOLAMINE 30 CAT CRACK, FLUID-BED H/O H2S R SO COXING UNIT 60 CRUDE PROCESS/ VIRGIN LT ENDS 60 PLAHT-WIDE/FIELDz OPERATIONS
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COHPOICHTS
PAGE 19
TASK ROLES CODE
NANUFACTURER
> 9B.0 999.9
D UNION CARBIDE CORP. 0 UNION CARBIDE CORP. D UNION CARBIDE CORP. D UNION CARBIDE CORP.
* \J
SAL 000005896
FEB SI, 1989
ETHYL BEKZEtC
AREA/ SECT CODE
GASGUARD 00 PLANT-HIDE/FIELD, MAINTENANCE
HEAVY AROMATIC DISTILLATE 10 RECEIPT/STOfiAGE/MOVEMENTS UNIT 70 CRUDE PROCESSING UNIT 80 DOCK OPERATIONS UNIT
OIL BRONZE LIQUID 10 REC/STOR/HOVE, BLENDING-PRODUC
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PAGE 20
TASK ROLES CODE
MANUFACTURER
OXXX D
NATIONAL CHEMSEARCH DIV. OF NCH CORP.
Z.O A.O
C DU PONT C DU PONT C DU PONT
C DUPONT
-X
^
>
J
/ '/
SAL 000005897
FEB 01, 1989
.TYLENE DIBROMIDE
AREA/ SECT CODE
MOTOR FUEL ANTIKNOCK COMPOUND 18 REC/STOR/MOVE, BLENDING-PRODUC
LAKE CHARLES REFINERY REPORT LIST
FDR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
C ETHYL CORP.
5.0 56.0
^
PAGE 21
SAL 000005893
FEB 01, 1969
ETHYLENE DICHLORIDE
AREA/ SECT CODE
ETHYLENE DICHLORIDE 80 DOCK OPERATIONS UNIT
MOTOR FUEL ANTIKNOCK COMPOUND 10 REC/STOR/HOVE, BLENDXMG-PRODUC
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COWNJNEHTS
TASX ROLES CODE
MANUFACTURER
> 99.0 999.9 I VISTA CHEMICAL CO.
5-9 19.0 C ETHYL CORP.
"X
A
PACE ?Z
SAL 000005399
FEB 01, 1989
HYLEME GLYCOL
AREA/ SECT CODE
BETZ 989 1Z UTILITY UNIT
CORTEC 597 SO COKING UNIT
ETHYLENE GLYCOL - ANTIFREEZE GRADE 00 PLANT-HIDE/FIELD UNIT 30 PLANT-WIOE/FIELD, OPERATIONS
GASKET ELIMINATOR 504 SEALANT 00 PLANT-HIDE/FIELD, MAINTENANCE 1000 GREEN CONCENTRATE 00 PLANT-WIDE/FIELD UNIT
PD ACTIVATOR, DEVELOPER 00 OFFICE/NON-FIELD UNIT
STATE HGP HIGH GLOSS PROTECTANT 00 PLANT-MIDE/FIELO, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE MAKES OF COMPONENTS
PAGE 23
TASK ROLES CODE
MANUFACTURER
.0 999.9
D BETZ LABORATORIES INC. 1-0 5.0
0 SEALED AIR CORP.
9S.0 9S.0
D CONOCO INC. D CONOCO INC.
i.o
3.o
D LOCTITE CORP.
9.0
9.0
D MERIAM INSTRUMENT
25.0 35.0
D BRUHIKG
< .0 1.0
DXXX D
STATE CHEMICAL MFC. CO.
^ v/
* </ ^
z? J
SAL 000005900
FEB *1, 1989
FORMALDEHYDE
AREA/ SECT CODE
FORHALIN 28 SULFUR RECOVERY* CLAUS NO PROCESS CODE
LAKE CHARLES REFIICRV REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
D GENERAL ELECTRIC D 6EIERAL ELECTRIC
37.0 SS.O
PACE 29 ^
SAL 000005901
FEB 01, 1909
HYDROCHLORIC ACID
AREA/ SECT CODE
CHEMETS R-751Z Z SULFURIC ACID MFC, CONTACT
DISSOLVED OXYGEN CHEMETS R-751Z 20 SULFURIC ACID NFC, CONTACT
HYDROCHLORIC ACID 12 UTILITY, BOILER HOUSE (ELEC/ST 70 CRUDE PROCESSING UNIT 70 CRUDE PROCESSING UNIT
LAKE CHARLES REFIltfRY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
< .0 .1
F HICROBE MASTERS INC.
< .0 .1
F O0CTRICS INC.
27.9 35.2
D VAN WATERS A ROGERS INC. 0 VAN WATERS A ROGERS IHC. D VAN WATERS A ROGERS INC.
PACE IS
^ 00005902
FEB 01, 19*9
HYDROGEN FLUORIDE
AREA/ SECT CODE
HYDROFLUORIC ACID-ANHYDROUS 00 HQ PROCESS CODE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMNDCMTS
PACE gjt,
TASK ROLES CODE
MANUFACTURER
0 DU PONT
10*.0 100.0
*^
000005903 SM-
FEB !, 1969
JROQUINOHE
AREA/ SECT CODE
HY9R0QU1H0NE 60 DOCK OPERATIONS UNIT
LAKE CHARLES REFDERY REPORT CIST
FOR TRADE NAMES OF CQWNHEMTS
PACE ff
TASK ROLES CODE
MANUFACTURER
D CARUS CHEMICAL CO.
160.0 100.0
ay
sal
000590^
FEB (1, 1989
ISOPROPANOL
AREA/ SECT CODE
BRILLIANCE AEROSOL 0 PLANT-HIDE/FIELD UNIT
DURA-CARD AEROSOL M PLANT-HIDE/FIELD, MAINTENANCE
CASCUABP 00 PLANT-WIDE/FIELD, MAINTENANCE
KONTOl K-450 30 PLANT-WIDE/FIELD, OPERATIONS
PETROTEC K-60Z 30 CRUDE PROCESSING UNIT
STATE CLR AEROSOL 00 PLANT-HIDE/FIELD, MAINTENANCE
UKE CHARLES REFIICRY REPORT LIST
FOR TRADE HANES OF COMPONENTS
PAGE
TASK ROLES CODE
MANUFACTURER
.0 999.9
B NATIONAL CHEMSEARCH
.0 999.9
DXXX D
NATIONAL CHEHSEAROI DIV. OF NCH CORP.
.0 999.9
DXXX D
NATIONAL CHEMSEARCH DIV. OF NCH CORP.
.0 999.9
0 PETROLITE CORP.
.0 999.9
0 PETROLITE CORP.
< .0 10.0
DXXX D
STATE CHEMICAL MFC. CO.
i/ 'f i/ % c/'
-A. ^
SAL 000005905
FEB 01, 1989
j<n
AREA/ SECT CODE
WHITE URETHANE ENAMEL S26V 00 PLAMT-UIDE/FIELD UNIT 10 PLANT-HIDE/FIELD UNIT
LAKE CHARLES REFUCRY REPORT LIST
FOR TRADE NAfES OF COWOCKTS
TASK ROLES CODE
MANUFACTURER
0 DU PONT D DU PONT
< .0 1.0
PAGE Xf
SAL 000005906
FEB *1, 19*9
H-CSBESOL
AREA/ SECT CODE
NR. 573 CARBON AND VARNISH REMOVER *0 PLAMT-HIDE/FIELD, MAINTENANCE
LAKE CHARLES RtfINLET REPORT LIST
FOR TRADE NAMES OF COWNMENTS
TASK ROLES CODE
HANUFACTVtER
0 A. V. CHESTERTON CO.
1.*
5.*
PAGC jx
SAL 000005907
FEB *1, 19
THAMOL
AREA/ SECT COSE
CARS CARE AEROSOL H PLAHT-WIDE/FIELD, MAINTENANCE
COPALTITE 80 PLANT-HIDE/FTELD, MAINTENANCE
FORMALIN 20 SULFUR RECOVERY, CLAUS 60 NO PROCESS CODE
KONTOl K-6S7 20 SULFUR RECOVERY, CLAUS "HANOI. 30 PLANT-WIDE/FIELD, OPERATIONS 80 DOCK OPERATIONS UNIT
NR. 573 CARBON AND VARNISH REMOVER 60 PLAHT-WIDE/FIELD, MAINTENANCE
PETROTEC PET1330 20 SULFUR RECOVERY, CLAUS
1-854 00 PLANT-WIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF CGMKMCNTS
RAGE J*
TASK CODE
ROLES
MANUFACTURER
.0 999.9
DXXX D
NATIONAL CHEHSEARCH DIV. OF MCH CORP. 15.0 15-0
D NATIONAL ENGINEERING PRODUCTS INC.
15.8 15.0
D GENERAL ELECTRIC 0 GENERAL ELECTRIC
.0 999.9
D PETROLITE CORP.
> 99.0 999.9
ID CELAKESE CHEMICAL CO. INC. ID CELAHESE OCMICAL CO. INC.
0 A. N. CHESTERTON CO.
1.0
5.0
D PETROLITE CORP.
.0 999.9
< .0 1.8
D hATCOTE CO. INC.
y ^
y ^^
^J
AV
SAL 000005908
FEB *1.
METHYL ISOBUTYL KETONE
AREA/ SECT CODE
KRYLOH INT./EXT. ENAMEL OR ENGINE COLOR 0 PLANT-HIDE/FIELD, MAINTENANCE
METHYL ISO-BUTYL KETONE 14 PLANT LABORATORY-OC
THA505/THA506 (1-8505 A * 8) 10 RECEIPT/STORAGE/MOVEMENTS UNIT
THA525/TKAS26 (1-85Z5 A 8 8) 10 RECEIPT/STORAGE/MOVEMEHTS UNIT
THA8S2/THA724 (1-652 Alt) 10 RECEIPT/STORAGE/MOVEMEHTS UNIT
THA8S5/TKA724 (1-850 A 8 B1 10 RECEIPT/STORAGE/MOVEMEHTS UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE MAICS OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
CBSO D
BORDEN
2.8
4.0
100.0 100.0
F FISHER SCIENTIFIC
< .0 1Z.0
CB50 0
INTERNATIONAL PAINT CO.
< .0 12.0
CBSO 0
INTERNATIONAL PAINT CO.
> 17.0 499.9
CBSO D
INTERNATIONAL PAINT
> 4.0 999.9
CBSO D
INTERNATIONAL PAINT
PACE 3j|
SAL 000005909
FES SI, 1989
^THYL TERTIARY SUTYL ETHER
AREA/ SECT CODE
METHYL TERTIARY SUTYL ETHER 10 RECE1PT/ST0RA6E/H0VEHEHTS UNIT 80 DOCK OPERATIONS UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE MANES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
> 80.0 999.9
C VALERO REFINING A MARKETING CO. C VALERO REFINING 0 MARKETING CO.
^
PACE ftk
SAL 000005910
FEB 01, 1969
MOLYBDENUM TRIOXIDE
AREA/ SECT CODE
CZ9-Z-0Z 29 SULFUR RECOVERY, CLAUS
KATALCO <*77 AO CAT REFORM, W/0 HYDROGENATION AO HYDROGEN TREATING UNIT
LAKE CHARLES (STOCKY (SPORT LIST
FOR TRADE NAfCS OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
in.* is.o
C UNITED CATALYSTS INC* 12.0 16.0
C KATALCO CORP. C KATALCO CORP.
PACE \/
000Q5911
SAL
FEB 01, 1989
jlPHTHALENE
AREA/ SECT CODE
HEAVY AROMATIC DISTILLATE
10 RECEIPT/STORAGE/MOVEMEHTS UNIT
70 CRUDE PROCESSING UNIT M DOCK OPERATIONS UNIT LIGHT FUEL OIL 10 RECEIPT/STORAGE/HOVEHENTS UNIT HALCO 5186 CORROSION INHIBITOR 70 CRUDE PROCESSING UNIT HALCO 5701 PROCESS ANTIFOAM 70 CRUDE PROCESSING UNIT HALCO 87RC130 60 COKE, DELAYED-FUEL GRADE W/ HZ
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE HANES OF COMPONENTS
PAGE J7
TASK ROLES CODE
MANUFACTURER
C DU PONT c DU PONT c DU PONT
C DU PONT
0 HALCO CrfHICAL CO.
D HALCO CHEMICAL CO
C HALCO CHEMICAL CO.
6.9 6.0
^y
7.0 53.a
1.0 10.0 1.0 10.0
v/
/
1.0 10.0
*
0000
c aL
FEB 01, 1909 NICKEL
LAKE CHARLES REFUCRY REPORT LIST
FOR TRADE KAICS OF CONPO^fTS
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
HYDROGEN TREATING CATALYSTS CO SULFUR RECOVERY, CLAUS
NR. 725 NICKEL ANTI-SEIZE COMPOUND (BULK) 00 PLANT-WIDE/FIELD UNIT
.0 999.9 AMERICAN CYAHAMID CO.
25.0 50.0 A. N. CHESTERTON CO.
*
PAGE &
/ 1/7
SAL 000005913
FEB 01, 1909
-BUTYL ALCOHOL
AREA/ SECT CODE
7RET0LITE DS-SOS 29 SULFURIC ACID ALKYLATION UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
D PETROLITE CORP.
PACE 6
*/
SAi~ OOOOO591
FEB 01, 1989
NORMAL BUTYL ALCWSL
AREA/ SECT CODE
PLASTIC LEAD SEAL NO. Z 08 PLANT-WIDE/FIELD, MAINTENANCE
LAKE CHAM.ES REFINERY REPORT LIST
FOR TRADE NAMES OF COW*OHENTS
TASK ROLES COSE
MANUFACTURER
D FEDERAL PROCESS CO.
2.8 2.8
PACE**
000005915 S/0-
FEE 01, 1969
RIC ACID
AREA/ SECT CODE
NITRIC ACID 00 PLANT-WIDE/FIELD UKTT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAICS OF COtPOHEHTC
PAGE 39
TASK ROLES CODE
MANUFACTURER
6S.8 75-0 06 J- T. BAKER CHEMICAL CO.
'-fc
SAL 000005916
FEB *1, 1989
O-CRESOL
AREA/ SECT CODE
HR. 573 CARBON AND VARNISH REHOVER 60 PLAHT'WXDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRACE NAMES OF COWOfCKTS
TASK ROLES CODE
MANUFACTURER
D A. N. CHESTERTON CO.
1.0
5.0
PAGE
ooooos''17 s M-
FEB 01, 1989
CRESOL
AREA/ SECT CODE
HR. 575 CARBON AMD VARNISH REMOVER 60 PLANT-VIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAIES OF CQWONEMTS
TASK ROLES CODE
MANUFACTURER
D A. H. CHESTERTON CO.
1.0
5.0
pace *2
FEB 01, 1989
PHENOL
AREA/ SECT CODE
SPENT CAUSTIC 20 SULFURIC ACID ALKYLATION UNIT 30 CRUDE PROCESS, ATMOS DISTILL AO WASTE TREAT, AOUEOUS 60 CRUDE PROCESS, VIRGIN LT ENDS
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
C CONOCO INC. c CONOCO INC. c CONOCO INC. c CONOCO INC.
( 999.9
PAGE 43 *
SAL 000005919
FEB !, 19G9
. _HOL (HYDROXY BENZENE)
AREA/ SECT CODE
SOUR WATER WASTE STREAMS
20 SULFURIC ACID NFS, CONTACT 2 THERMAL CRACKING UNIT 30 CRUDE PROCESSING UNIT 40 CAT REFORM, M/0 HYDROGENATION 40 HYDROGEN TREATING UNIT SO COKING UNIT 60 CRUDE PROCESS, VIRGIN LT ENDS 60 PLANT-WIDE/FIELD, OPERATIONS 70 CRUDE PROCESSING UNIT
LAKE CHARLES REF1HERV REPORT LIST
FOR TRIBE HMB OF COMPONEHTS
TASK ROLES CODE
MANUFACTURER
E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC. E CONOCO INC.
.0 999.9
PAGE ^
SAL 000005920
FEB II, 1989
PH0S6QC
AREA/ SECT CODE
PH0S6EIC 0 HO PROCESS CODE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PACE *8
TASl CODE
ROLES
MANUFACTURER
> 99.8 999.9 0 UNION CARBIDE CSRP.
^
SAL 0000592
FEB Bl, 1989
. .iOSPHORXC ACID
AREA/ SECT CODE
ALPKACMEN 3Z12 ACID CLEANER SO C0KXM6 UNIT 60 PtAMT-tflDE/FlELD, OPERATIONS
BETZ 40P 1Z UTILITY UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COHPOtCHIS
PARE
TASK ROLES CODE
MANUFACTURER
. 999.9
D ALPHA CHEMICAL CO. D ALPHA CHEMICAL CO.
.0 999.9 D BETZ LABORATORIES 1HC.
^
/ J
SAL 000005922
FEB II, 1989 STYRENE
UKE CHARLES REFItCRV REPORT LIST
FOR TRADE HANES OF COMMENTS
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
HEAVY AROMATIC DISTILLATE
10 RECEIPT/STORA6E/HOVEHEKTS UNIT 70 CRUDE PROCESSING UNIT 80 DOCK OPERATIONS UNIT
PLASITE 5602 FINAL COAT
20 SULFURIC ACID NFC, CONTACT
PLASITE 5602 VINYL ESTER TOPPING TILE RED
20 SULFURIC ACID NFC, CONTACT
6.0 10.8
C DU PONT C DU PONT C DU PONT
30.0 70.0
CBSO B
WISCONSIN PROTECTIVE COATINGS
< .0 30.0
CB50 D
WISCONSIN PROTECTIVE COATINGS
PASE^r
J
S41 000005 923
FEB #1, 19S9 .lFIRIC acid
LAKE CHARLES REF1ICRV REPORT LIST
FOR TRADE NAMES OF COMPONENTS
AREA/ SECT CODE
CHEHETS AND VACUETTES R-BSM
20 SULFURIC ACID MFC, CONTACT
MOLYBDATE REAGENT FOR P94
20 SULFURIC ACID MFC, CONTACT
PHOSPHATE CHEHETS R-S510
20 SULFURIC ACID MFC, CONTACT SILICA 1 REAGENT
20 SULFURIC ACID MFC, CONTACT
<1ILFURIC ACID
12 UTILITY UNIT
20 - SULFURIC ACID ALKYLATION UNIT .
20 SULFURIC ACID MFC, CONTACT
40 CAT REFORM, H/O HYDROGENATION
40 WASTE TREAT, AQUEOUS
60 UTILITY,
HOUSE (COOLING T
SULFURIC ACID (SPENT)
20 SULFURIC ACID ALKYLATION UNIT 20 SULFURIC ACID MFC, CONTACT
SULFURIC ACID ALKYLATION MET BLOWDOWN GAS
20 SULFURIC ACID ALKYLATION UNIT
SULFURIC ACID SOLUTION,10H
20 SULFURIC ACID WG, CONTACT
TASK ROLES CODE
MANUFACTURER
MICROBE MASTERS INC.
5.0
>
S.I
.0 999.9 F BETZ LABORATORIES INC.
F CHEtCTRICS INC.
s.o
s.o
.0 999.9
F BETZ LABORATORIES INC.
.0 999.9
AC CONOCO INC. AC CONOCO INC. AC CONOCO INC. AC CONOCO INC. AC CONOCO INC. AC CONOCO INC.
.-
.0 999.9
AC CONOCO INC. AC CONOCO INC.
C CONOCO INC.
.0 999.9
.0 999.9 F BETZ LABORATORIES INC.
PACE
A/
A n. y
TT
v/
t7
l/
it v/
SAL 000005924-
FO II. 1969
SULFURIC ACID
AREA/ SECT CODE
TRILL O PLANT-WIDE/FIELD UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
0 NATIONAL CHEMSEARCH DIV. OF NCH CHRP.
PACE
y
SAL 000005925
FEB n, 19*9
*ULFUR1C ACID ACS 6RA0E
AREA/ SECT CODE
HOLYBOATE 3 REA6EKT FOR SILICA 20 SULFURIC ACID (TO, CONTACT
UKE OUkRLES WEFIMsRV REPORT LOT
FOR TRADE NAMES OF COMPONENTS
PACE *
TASK ROLES COOE
MANUFACTURER
F HACH CO.
< .1 n.i
-A
\J
r
v-
SAL 000005926
FEB 01, 1989
SULFURIC ACID 952
AREA/ SECT CODE
AMMONIUM MOLYBDATE REAGENT FOR SILICA 12 UTILITY UNIT 20 SULFURIC ACID WC* CONTACT
LAKE CHARLES RU-1MSY REPORT LIST
FOR TRADE NAtCS OF CCBftBCKTS
PAGE
TASK ROLES CODE
MANUFACTURER
F HACH CO. F HACH CO.
.< 10.0
Jt<3
SA(- 000005927
FEB lr 1989
.tETIARY BUTYL ALCOHOL
AREA/ SECT CODE
TR1QO.OROETHANE 111 600 00 PLANT-WIDE/FIELD UNIT
LAKE CHARLES REFIHEKY REPORT LIST
FOR TRADE NAMES OF CMMVEKTS
PACE
TASK ROLES CODE
MANUFACTURES
.* 999.9 0 THONPSON-HAYNARD CHEMICAL CO.
-k y
y V..
}
000005928 SM-
FEB !, 19B9
TITANIUM DIOXIDE
AREA/ SECT CODE
AEROSOLS, PAINT - LEAD FREE 0 PLANT-WIDC/FIELD UNIT
EPAA57/EPAAS8 (1-857 ABB) 10 RECdPT/STORADE/NOVEMEMTS UNIT
EPI-SEAL TUBE-IN-TUBE REPAIR KIT-PART A 00 PLANT-WIDE/FIELD, MAINTENANCE
MATSTICK 1-10 A 00 PLANT-WIDE/FIELD, MAINTENANCE
PLASITE 7155 LIGHT GRAY 00 PLANT-WIDE/FIELD UNIT
THA007/THAOOB (1-07 ABB) 10 RECE1PT/STORAGE/MOVEHENTS UNIT
THA5Q5/THA506 (1-BS05 ABB) 10 RECEIPT/STORAGE/MOVEMEHTS UNIT
THAS25/THAS26 (1-8S25 ABB) 10 RECEIPT/STORAGE/NOVEMENTS UNIT
THAA52/THA724 (1-652 ABB) 10 RECEIPT/STORAGE/HOVEKENTS UNIT
THABSS/THA7Z4 (1-650 ABB) 10 RECEIPT/STORAGE/MOVENEMTS UNIT
LAKE CHARLES REFIhERY REPORT LIST
FOR TRADE NAJCS OF COWOMEKTS
TASK ROLES CODE
MANUFACTURER
D RAABE PAINT CO. INC.
. 9*9.9
< .0 10.0
CBSO D
INTERNATIONAL PAINT
.0 999.9
0 BONDED PRODUCTS INC.
> 1.0 999.9
D MATCOTE CO. INC.
< .0 30.0
CBSO D
WISCONSIN PROTECTIVE COATINGS
> 4.0 999.9
C85Q D INTERNATIONAL PAINT
< .0 7.0
CBSO 0 INTERNATIONAL PAINT CO.
< .0 13.0
CB50 0 INTERNATIONAL PAINT CO.
> 11.0 999.9
CBSO D INTERNATIONAL PAINT
6.0
6.0
CBSO D INTERNATIONAL PAINT
PACE ^
000005929
SAL
FES !, 1989
_ fAMIUH DIOXIDE
AREA/ SECT CODE
1 -854 00 PLANT-HIDE/FIELD# MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OP COMPONENTS
TASK ROLES CODE
HAMFACTURER
i > lt.1 999.9
0 MATCOTE CO. INC.
PACE *
****'***''?'
SAL 00005930
FEB 01, 1969 TOLUENE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
AREA/ SECT CODE
TASK ROLES OWE
MANUFACTURER
ACTIVATOR/CLEAR VGY SI1
6.0
6.0
00 PLANT-HIDE/FIELD, MAINTENANCE
CBSO D
DU PONT
AEROSOLS, PAINT - LEAD FREE 00 PLANT-HIDE/FIELD UNIT
CARBOHASTIC 19
D RAABE PAINT CO. INC. <
.0 999.9 .0 5.0
00 PLANT-HIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
CBSO
D D
CARBOLINE CO. CARBOLINE CO.
EPA857/EPA8S8 (1-857 A A B) 10 RECEIPT/STORAGE/MOVEMENTS UNIT
<
CBSO D
INTERNATIONAL PAINT
.0 20.0
GTA906 (9-076)
< .0 95.0
10 RECEIPT/STORAGE/HOVEHEMTS UNIT GTA909 (9-079)
CBSO D
INTERNATIONAL PAINT
10.0 10.0
10 RECEIPT/'STORACE/MOVEHENTS UNIT HEAVY AROMATIC DISTILLATE
CBSO 0
INTERNATIONAL PAINT
10.0 1S.0
10 RECEIPT/STORAGE/NOVEHENTS UNIT 70 CRUDE PROCESSING UNIT 80 DOCK OPERATIONS UNIT
C DU PONT C DU PONT C DU PONT
INTERGARD CURING AGENT (EC57Z5) 00 PLANT-HIDE/FIELD, MAINTENANCE
CB50 D
INTERNATIONAL PAINT
90.0 95.0
ISOOCTANE (RESEARCH, PURE AND SPECTRO GRADES)
.0 999.9
19 PLANT LABORATORY-QC
F PHILLIPS CHEMICAL CO.
^
"7?
V
PAGE S5
/ 1/
SAL 000005931
FEB 01, 1909 jLUEHE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
KRYLON INT./EXT. ENAMEL OR ENGINE COLOR
2.0 3.0
00 PLANT-WIDE/FIELD, MAINTENANCE KRYLON SPRAY PRIMER
CBSO 0
BORDEN
23.0 Z7.0
00 PLANT-WIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
CB50
D D
BORDEN BORDEN
KARSH SPRAY STENCIL INK BLACK, RES, WHITE, BLUE A SILVER
.0 999.9
00 PLANT-WIDE/FIELD UNIT
D HARSH STENCIL HACH1KE CO.
KARSH SPRAY STENCIL INK YEUOR, GREEN t ORANGE
.0 999.9
00 PLANT-HIDE/FIELD UNIT TOR FUEL ANTIKNOCK COKPOUHD
0 KARSH STENCIL HACHItC CO. 1.0 13.0
Tf
10 REC/STOR/HOVE, BLENDING-PRODUC
C ETHYL CORP.
HR. S73 CARBON AND VARNISH REHOVER
1.0 5.0
60 PLANT-HIDE/FIELD, MAINTENANCE
D A. W. CHESTERTON CO.
OCE'REVERSAL TONER 2610000 OR 2610001
12.0 12.0
00 PLANT-WIDE/FIELD, SSVCS-EMCR.I
B OCE*-INDUSTRIES INC.
PLASITE 7155 LIGHT GRAY
< .0 30.0
00 PLANT-WIDE/FIELD UNIT
CB50 D
WISCONSIN PROTECTIVE COATINGS
PYROCOTE 767 70 PLANT-WIDE/FIELD, MAINTENANCE
T 3671
CB50 D
CARBOLIHE CO.
> 1.0 999.9 1.0 1.0
00 PLANT-WIDE/FIELD, MAINTENANCE
C850 D
DU PONT
PACE SO
1 ,
^
SAL 000005932
FEB Bl, 1949
IOLUENE
AREA/ SECT CODE
TOLUENE STANDARDIZATION FUEL 1061 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 1080 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 1099 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 1116 14 PLANT LABORATORY-QC
TOLUENE STANDARDIZATION FUEL 948 14 PLANT LABORATORY-QC
TOLUENE STANDARDIZATION FUEL 960 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 967 14 PLANT LABORATORY-QC
TOLUENE STANDARDIZATION FUEL 97Z 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 985 14 PLANT LABORATORY-OC
TOLUENE STANDARDIZATION FUEL 996 14 PLANT LABORATORY-OC
LAKE CHARLES REFINERY REPORT LIST
FOR TRUE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER ,,--
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
74.0 74.0 F PHILLIPS CHEHICAL CO.
PACE SB
0005933
FEB 01, 1989
TOLUENE
AREA/ SECT CODE
T 3871 90 NO PROCESS CODE
THA5O5/THAS06 (1-8S05 A * B) 10 RECEIPT/STORAGE/HOVEMENTS UNIT
TKAS25/THAS26 (1-0525 A 8 B) 10 RECEIPT/STORAGE/HOVEMENTS UNIT
THA85Z/THA724 (1-852 A 8 B) 10 RECEIPT/STORAGE/HOVEHENTS UNIT
THA855/TKA7Z4 (1-850 A 8 B)
10 RECEIPT/STORAGE/HOVEMEHTS UNIT TOLUENE
14 PLANT LABORATORY-OC 14 PLANT LABORATORY-OC TOLUENE STANDARDIZATION FUEL 1010 14 PLANT LABORATORY-QC TOLUENE STANDARDIZATION FUEL 1025 14 PLANT LABORATORY-OC TOLUENE STANDARDIZATION FUEL 1033 14 PLANT LABORATORY-OC TOLUENE STANDARDIZATION FUEL 1042 14 PLANT LABORATORY-OC
LAKE CHARLES REFXtCRY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PAG 57
TASK ROLES CODE
MANUFACTURER
1.0 1-0
0 DU PONT
< .0 2.0
CBSO D
INTERNATIONAL PAINT CO.
< .0 2.0
CB50 D
INTERNATIONAL PAINT CO.
> 1.0 999.9
CBSO D
INTERNATIONAL PAINT
> 12.0 999.9
CBSO D
INTERNATIONAL PAINT
> 99.0 999.9
0 VAN HATERS A ROGERS INC. F VAN HATERS 0 ROGERS INC.
74.0 74.0
F PHILLIPS CHEMICAL CO.
74.0 74.0
F PHILLIPS CHEMICAL CO.
74.0 74.0
F PHILLIPS CHEMICAL CO.
74.0 74.0
F PHILLIPS CHEMICAL CO.
^7
y
SAL 000005934
FEB OX, 1949 TOLUENE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAtCS OF COMPONENTS
AREA/ SECT COSE
TASK ROLES CODE
MANUFACTURER
TOLUOL
> 99.0 999.9
20 SULFURIC ACID MFC, CONTACT
F FISHER SCIENTIFIC
TPAS30/FHA72S <1-430 A A B)
> 6.0 999.9
10 RECEIPT/STORAGE/MOVEtCNTS UNIT
CBS 0
INTERNATIONAL PAINT
WHITE URETHANE ENAMEL 326Y
2.0
2.0
00 PLANT-WIDE/FIELD UNIT ID PIANT-WIDE/FIELD UNIT
D DU PONT D DU PONT
ZINC RE-HU (AEROSOL) 3074
00 PLANT-WIDE/FIELD, MAINTENANCE
D CRC CHEMICALS
1-4S6
.0
00 PLAHT-WIPE/FIELD, KAINTENAHCE
D HATCOTE CO. INC.
3M SUPER WEATHERSTRIP ADHESIVE PN. 4001 - 4003 - 4004
6.0 999.9
00 PLANT-WIDE/FIELD, HAINT-ROUTIN
D 3H
PAGE S9
FEB 01, 1989
,,TLEME
AREA/ SECT CODE
"ETHYL" HMT DILUTE 10 REC/STOR/MOVE, BLENDING-PROOUC
ACRILAST S70 70 PLANT-WIDE/FIELD, MAINTENANCE
ACTIVATOR/CLEAR VGY 511 00 PLANT-NIDE/FIEID. MAINTENANCE
AEROSOLS, PAINT - LEAD FREE 00 PLAMT-WIDE/FIELD UNIT
"PHACHEH 2061 DEGREASER 00 PLANT-HIDE/FIELD UNIT
ALPHACHEH 2063 DEGREASER 60 MO PROCESS CODE 70 NO PROCESS CODE
C. I. SOLVENT RED 164 10 REC/STOR/KOVE, BLENDIHG-PRODUC
CARBOHASTIC 14 00 PLANT-WIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
CORTEC 347 50 COKING UNIT
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COtOMMEKTS
TASK ROLES CODE
MANUFACTURER
ETHYL CORP.
.0 999.9 1S.0 15.0
CBSO 0
CARBOLIME CO.
CBSO D
DU PONT
S.O
5.0
RAABE PAINT CO. INC.
.8 999.9
ALPHA CHEMICAL CO.
ALPHA CHEMICAL CO. ALPHA CHEMICAL CO.
.0 999.9 .0 999.9
DU PONT
30.0 30.0
CB50
D D
CARBOLIME CO. CARBOLIME CO.
10.0 10.0
SEALED AIR CORP.
1.0 S.O
PAGE 0
J
*y
j
J
*y
9: w/
SAL 000005936
FEB 01, 1989
XYLENE
AREA/ SECT CODE
DCl-6 10 RECEIPT/STORAGE/MOVEHENTS UNIT
DIESEL GUARD 00 PLAMT-WIOE/FIELD, HAIHTEKANCE
DHD-2 70 HZ TREAT, DESULF/DENITRIF
DUPONT CORROSION INHIBITOR NO. 4A 10 RECEIPT/STORAGE/MOVEHENTS UNIT
DUPONT METAL DEACTIVATOR 70 H2 TREAT, DESULF/DENITRIF
EPA857/EPA856 (1-657 A S B) 10 RECEIPT/STORAGE/MOVEIENTS UNIT
FOA-11 10 REC/STOR/MOVE, BLENDING-PRODUC
6ASCUARD 00 PLANT-HIDE/FIELD, MAINTENANCE
GTA409 (4-079) 10 RECEIPT/STORAGE/MOVEHENTS UNIT
KRYLON INT./EXT. ENAMEL OR ENGINE COLOR 00 PLANT-WIDE/FIELD, MAINTENANCE
LAKE OURLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
C DU PONT
21.0 21.0
.0 999.9
DXXX D
NATIONAL OBtSEARCH DIV.. OF NCH CORP.
46.0 46.0
D DU PONT
C DU PONT
25.0 25.0
D DU PONT
20.0 20.0
<
CB50 D
INTERNATIONAL PAINT
.0 5.0
C DU PONT
1.0 1.0
.0 999.9
DXXX D
NATIONAL CHEMSEARCK DIV . OF NCH CORP.
CBSO 0
INTERNATIONAL PAINT
50.0 30.0
6.0 14.0
CBSO 0
BOROEN
PACE 61
~K / v/
*/ A v/ X V/
y
L/
SAL 00005937 '
FEB 01, 19*9 /LENE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE KANES OF COMMENTS
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
MOTOR FUEL ANTIKNOCK COMPOUND 10 REC/STOR/MOVE, BLEHDXHG-PROOUC
P-10 BLACK MARKER INK 14 PLANT LABORATORY~OC
PETRQNEEN AF111 60 HYDROGEN TREATING UNIT
PETROMEEN EB911 40 HASTE TREAT, AQUEOUS
PLASITE 7155 LIGHT GRAY 00 PLANT-WIDE/FIELD UNIT
PYROCOTE 787 70 PLANT-WIDE/FIELD, MAINTENANCE
RED URETHANE SEAL COAT (AEROSOL) NO. 2044 00 PLAHT-WIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
T 5*71 00 PL ANT-HIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
THA852/THA7Z4 (1-8S2 A * B) 1* RECEIPT/STORAGE/MOVENENTS UNIT
49.0 50.0 C ETHYL CORP.
62.0 62.0 D PACIFIC POLY CRAFTS
.0 999.9 D BETZ PROCESS CHEMICALS INC.
.0 999.9
D BETZ PROCESS CHEMICALS INC.
< .0 30.0
CB50 0
WISCONSIN PROTECTIVE COATINGS
> 1.0 999.9
CBSO D
CARBOLINE CO.
> 13.0 999.9
CBSO
D D
CRC CHEMICALS CRC CHEMICALS
84.0 84.0
CBSO
D D
DU PONT DU PONT
<
CB50 D
INTERNATIONAL PAINT
.0 1.0
PAGE *2
y ' ^
y'
SAL 000005938
FEB 01, 1909
XYLENE
AREA/ SECT CODE
THA8SS/THA724 (1-4S0 A 0 B) 10 RECEIPT/STORAGE/MOVEMENTS UNIT
TPA830/FMA7Z5 <1-630 All) 10 RECEIPT/STORAGE/MOVEMENTS UNIT
ZINC RE-NU tAEROSOL) 3076 00 PLAHT-HIDE/FIELD, MAINTENANCE
1-856 00 PLANT-HIDE/FIELD, MAINTENANCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
<
050 D
INTERNATIONAL PAINT
.0 1.0
> 12.0 999.9
CBSO D
INTERNATIONAL PAINT
D CRC OEHICALS
> 7.0 999.9
> D MATCOTE CO. INC.
6.0 999.9
PACE 63
l/
SAL 000005939
FES 01, 19S9
fLENES
AREA/ SECT CODE
OIL BRONZE LIQUID 10 REC/STOR/HOVE, BLENDING-PRODUC
XYLENES 14 PLANT LABORATORY-QC
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE HANES OF COHPOICNTS
TASK ROLES COOE
MANUFACTURER
4a.o 4o.a C DUPONT
90.0 100.0 F J. T. BAKER CHEMICAL CO.
PACE M 7% y
SAL 000005940
FEB 01, 1989 ZIKC DUST
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PAGE AS
AKA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
------------------------------------------- ------------------------------------------------------------------------
5074 ZINC RE-MU (AEROSOL)
> 27.0 999.9
K
00 PLAMT-WIDE/FIELD, MAINTENANCE
D CRC CHEMICALS
FES 01, 1969
,,1-TRXCMLOROETHAME
AREA/ SECT CODE
ALPHAOCH 2056 SOLVENT EMULSION 70 CRUDE PROCESSING UNIT
AZTROM EMC 6 90 PLANT-MIDE/FIELD UNIT
BRAKE JOB AEROSOL 90 MAINTENANCE SHOP UNIT
CABLE CLEANER 2069 00 PLANT-VIDE/FIELD UNIT
CABLE CLEANER 2067 00 PLANT-WIDE/FIELD UNIT
CARS CARE AEROSOL 00 PLANT-HIDE/FIELD, MAINTENANCE
CHLOROTHENE SH SOLVENT 20 SULFUR RECOVERY, CLAUS
ELECTRICAL QUALITY SILICONE 00 PLANT-WIDE/FIELD UNIT
EZE-UAY AEROSOL 00 PLANT-WIDE/FIELD UNIT
LECTRA CLEAN (AEROSOL) NO. 2016 00 PLANT-HIDE/FIELD, MAINTENANCE
LAKE CHARLES REFItCRY REPORT LIST
FOR TRADE NAMES OF COWHNBfTS
PAGE 66
TASK ROLES CODE
MANUFACTURER
D ALPHA CHEMICAL CO.
.0 999.9
.0 999.9
CC10 D
AZTRON CHEMICAL SERVICES INC.
.0 999.9
D NATIONAL CHEMSEARCH
72.0 72.0
D CRC CHEMICALS
92.0 92.0
D CRC CHEMICALS
.0 999.9
DXXX D
NATIONAL CHEMSEARCH DIV . OF NCH CORP.
D DOW CHEMICAL USA
96.5 96.5
51.0 51.0
D CRC CHEMICALS
.0 999.9
D NATIONAL CHEMSEARCH DIV . OF NCH CORP.
72.0 72.0
D CRC CHEMICALS
i/
& i/
j
-y
ir
y
*
*y
L/ >
y
7
SAL 000005942
FEB 01, 1969 1,1,1-TRICHLOROETHAME
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
PAGE 67
AREA/ SECT CODE
TASK ROLES CODE
MANUFACTURER
PJ1 HEAVY DUTY CHAIN LUBE 00 PLANT-HIDE/FIELD, MAINTENANCE
RED URETHANE SEAL COAT (AEROSOL) NO. 2044 00 PLANT-WIDE/FIELD, MAINTENANCE 90 NO PROCESS CODE
STATE 6RS 00 PLANT-HIDE/FIELD, MAINTENANCE
TRI-ETHANE 3*6 40 CAT REFORM, H/O HYDROGENATION
TRICHLQROETHANE 111 600 00 PLANT-WIDE/FIELD UNIT
42.0 42.0
'"V"
D PJ1 CORP.
17.0 17.0
CBSO
0 D
CRC CHEMICALS CRC CHEMICALS
< .o io.o
DXXX D
STATE CHEMICAL HFG. CO.
100.0 100.0
D PPG INDUSTRIES INC.
> 9S.0 999.9
D THOMPSON-HAYWARD CHEMICAL CO.
366
n \y
-jr 1
SAL 00005943
FEB 81, 1989
I TRICHLOROETHANE
AREA/ SECT CODE
JIHCO 00 PLANTWIDE/FIELD, KAINTENAMCE
LAKE CHARLES REFINERY REPORT LIST
FOR TRADE NAMES OF COMPONENTS
TASK ROLES CODE
MANUFACTURER
0 STEWART SALES CO.
95. 95.8
PAGE 28
0059AA
SAC 00
APPENDIX B EMISSION FACTORS SARA TITLE III, SECTION 313 198B TOXIC CHEMICAL RELEASE INVENTORY LAKE CHARLES REFINERY
SAL 000005945
TABLE 0-1, AVERAGE FUGITIVE EMISSION FACTORS FOR THE , SYNTHETIC ORGANIC CHEMICALS MANUFACTURING INOUSTRY (SOCHI)3
Fugitive-emission source
Emission factor (Ib/h)
Pump seals
Light liquids Heavy liquids
0.11 0.047
Valves (in-line)
Gas Light liquid Heavy liquid
0.012 0.016 0.00051
Gas safety-relief valves
0.23
Open-ended lines
0.0037
Flanges
0.0018
Sampling connections
0.033
Compressor seals
0.50
3 Emission Factors for Equipment Leaks of VOC and HAP,
EPA-450/3-86-002, January 1986, Table 3-4. These factors take into account a leak frequency determined from field studies in the synthetic organic chemicals manufacturing industry. Light liquids have a vapor pressure greater than 0.1 psia at 100F.
_ KMfc>
FBuewoes Fb4_-mGr vo^A/ p>A/ /2L-87
\*^TMexfr
D-2
SAL 000005946
TABLE D-2. LEAKING AND NONLEAKING AVERAGE FUGITIVE EMISSION FACTORS FOR THE ^ SYNTHETIC ORGANIC CHEMICALS MANUFACTURING INDUSTRY (SOCMI)a
Fugitiveemission source
Leaking (>10,000 ppm) emission factor (Ib/h)
Nonleaking (<10,000 ppm) emission factor (Ib/h)
Pump seals
Light liquids Heavy liquids
0.96 0.85
0.026 0.030
Valves (in-line)
-
Gas Light liquid Heavy liquid
0.099 0.19 0.00051
0.0011 0.0038 0.00051
Gas safety-relief valves
3.72
0.098
Open-ended lines
0.0263
0.0033
Flanges
Sampling connections
0.083 _
0.00013
Compressor seals
3.54
0.20
Emission Factors for Equipment Leaks of VOC and HAP, EPA-450/3-86-002, January 1986, Table 3-3. These factors take into account a leak frequency determined from field studies in the synthetic organic chemicals manufac
turing industry. Light liquids have a vapor pressure greater than 0.1 psia at 100F.
j>, >-3
0 "fiV\ Append. iX
0-3
SAL 000005947
TABLE 5.17-3. EMISSION COMPARISON AND COLLECTION EFFICIENCY OF TYPICAL ELECTROSTATIC PRECIPITATOR AND FIBER MIST ELIMINATORS*
Control device
Particle size collection
efficiency, I
>3 |io
^3jim
Acid mist emissions 981 acid plants1* Oleum plants
kg/Mg
lb/ton
kg/Mg lb/ton
Electrostatic
precipitator
99
100 0.05
0.10
0.06
0.12
Fiber mist
eliminator
Tabular
100
95-99 0.01
0.02
0.01
0.02
Panel
100
90-98 0.05
0.10
0.05
0.10
Dual pad
100
93-99 0.055
0.11
0.055
0.11
^Reference 2.
Based on manufacturers1 generally expected results. SO^ concentration in gas converter.
Calculated for 62
References for Section 5.17
1. Atmospheric Emissions from Sulfuric Acid Manufacturing Processes, 999--AP--13, U.S. Department of Health, Education and Welfare, Washington, DC, 1966.
2. Unpublished report on control of air pollution from sulfuric acid plants, U.S. Environmental Protection Agency, Research Triangle Parle, NC, August 1971.
3. Standards of Performance for New Stationary Sources, 36 FR 24875* December 23, 1971.
4. K. Drabkin and Kathryn J. Brooks, A Review of Standards of Performance for New Stationary Sources - Sulfuric Acid Plants, EPA Contract No. 68-02-2526, Mitre Corporation, McLean, VA, June 1978.
5. Final Guideline Document: Control of Sulfuric Acid Mist Emissions from Existing Sulfuric Acid Production Units. EPA 450/2-77-019, U.S.Environmental Protection Agency, Research Triangle Park, NC, September 1977.
frP-Cf 2_ -
Refers
4/81
Chemical Process Industry
5.17-9 SAL 00000594.*
Table 9.1-2. FUGITIVE EMISSION FACTORS FOR PETROLEUM REFINERIES*
Ulaalai |M
Maaltaa aalaa4
pTMa Strwp
ii
m
IT
Opaaa dial nlan4'* I
rialiaa4 P^ amaU4
1 III
IT
J fWC<M 4C4lM^
ir V i.
fmnai viiwl nllal aalaaa. . Ua aaffUa) *
<*11*4 t*Mf
it
talaala. facta
Bale* ll/b a .area t(/b| aaw
"
"
-
.
.
"
*
**
-
Oacaatrallal talalMM
i ract*r
0.019 0.44
(o.eio - 0.1102 (4.31 - 1-1*1
0.01* .H
<0.011 > 0.034) <0.10 - 0.3*)
0.0001 (9.0001- 0.0013) .m <0.002 * 0.014)
0.010 0.20
<0.002 - 0.0*1) <0.0* - 0.4*)
CMftalla* BU HA HA HA
UpiXdU Caattal UebaUn Nm(UcU| *4 doU<OdMC yrdetMt
UiaIii rc*c UMw A
A
A
A
0.0*1 0.01
<0.0014- 0.014) (0.011 - .)*)
HA
laacilUtba at cap at (lab m >( n rnmt
A
at dlaa/llaa
0.0001C <0.0001- 0.0021) HA UalMUi aad aalaiaaaata pidraa 0.0041 <0.002 - 0.022)
A
0.2} 2.1
(0.14 - 0.32) <1.1 - 4.0)
0.0*4 0.30
<0.011 - 0.11) <0.21 - 1.2)
KA Ulblllil aaala, laal
pai|d
A
aaali, Itafbi amt alaiaata
|H|rni aaatrilUl ttfuiat data
HA A
1.4 11
O.M " 1.2
.1.44 - 2.*) <2.1 - 32)
<0.01 - <J <0.1 - Ul
HA Wa(Malta! Mala. Aaal aaala. par|M
A
mil, adliwla) amt ailataaaaaa pTilfiia. Iiaidll a 4a|aaala( mta
NA A
0.010 0.14
<0.021 - 4.20) <0. - 2.2)
U Trap a m4 maara
A
0.34 3.0
<0.10 - U3> <1.1 - l*>
PadUlUa
aalaaa M/at *aMta (a 4 Clara
A
lu/io* ti diim mwt
ki/|* libn wallx
1W10* bl jdbafy **/!* Uun
atl.aif taad
4
0.2
_10
0.03
0.70
0.043 L.2 0.00*
UalaliaiUa at Iplracadia Uala la(a aMlIaa* aatat aftam. UaaHaa lat at irillat dtat tat Uftiatialaaa
0
((/It1 Unr wmm
un> Ml rrf
I4/W* llttn wtuiiy
Cm I^|M M
0.4 MO
0.4
0.024 M
0.01
ffat-a
*k>< (0- <.
2. 4. 13 aaO Ua
w MMl.
o'IM nlMlUtr
I
lUa nno ilmtll.
<mm at da (min (<
- - *1 Um (4a XX ty MUM a< da Meal TOC atoilao *n oidux.
1 laa a ad ((<! attaat aa da alala Ma alTikM seal
lKta MhIm
d--aral
|W Craal > itrlKla
ll<iimTn qh/ii'mk at |(m intlda* (cautalut Um dn MX
W
Ufta UdU amt gam/UtaU M 40 -ir -
thim
U(Mi at
HIM OUT Mfw (rHf |dMM do Uut .(
fcieil-- <* 0.1 fob P IOOT M M N T M*CJ. MM m da MM MbUU (Um
qhiim at id
mUm
UmU wna dd m ir iTiia.n 1(1(1 u at Um dw (Um at Mraaa.i (a 0.1 pmta ld*T at 4*t Pa * 11*0, (ml am da mm aaUclla Um (m*m( >1 > Ml Ur
Cm mm-- MUbld lid daa MX ||UbU Up dUn
amt b(M lidb at (M *11 mlUaaM bund tat da i ill Hi lanw.
-----------II.
, (lit at dm (!( U (( W d* .............
blirtm an d--* d did mm at d 1-- did.
{nw (w nlU< dim U *m nfdit U <M IiUiqi. mat tat aUtii
1 tp didl (loibM rdU(.
SdbMT nu U MM m da enK all (ad nu (a da mnplurtc IbdllMUa Umu
9.1-10
xi
EMISSION FACTORS
^eFefi-eMCir - p-4z. ~7H!Rb
10/80
j- i J -/o\.
SAL 000005949
REVISED VOC EMISSION FACTORS FOR REFINERY WASTE WATER SYSTEMS
Based on more recent information, we suggest the following emission
factor.
Source;
"VOC Emissions From Petroleum Refinery Wastewater
Systems - Background Information For Proposed Standards" Preliminary
Draft July 1984.
I. API Separator
AP-42 emission factors: Uncontrolled Controlled
5.0 0.2
lb/103 Gal. lb/103 Gal.
Revised Factors: Uncontrolled Covered
Covered w/Vent to Vapor Collection System
(420kg/M Gals.) (8SZ Control)
0.93 0.14
lb/103 Gal. lb/103 Gal.
(97Z Control)
0.03
lb/103 Cal.
II. Air Flotation Systems
AP--42 Emission Factor Dissolved Air Flotation (DAF)
0.01 lb/103 Cal.
Revised Factors:
Dissolved Air Flotation (DAF)
Uncontrolled
(15.2 kg/M Gal.)
Cover w/Atmospheric Vent
(77X Control)
Cover w/Vent to Vapor Collection System
(97Z Control)
0.033 0.008
lb/103 Gal. lb/103 Gal.
0.001 lb/103 Gal.
Induced Air Flotation (IAF)
Completely Uncontrolled
(15.2 kg/M Gal.)
Covered w/Doors Open
( 8.7 kg/M Gal.)
* Covered w/Doors Closed Covered (Tight Seals)
( 3.0 kg/M Gal.) ( 2.3 kg/H Gal.)
Covered w/Vent To Vapor Collection System
( 0.45kg/M Gal.)
0.033 lb/103 Gal. 0.02 lb/103 Gal. 0.0066 lb/103 Gal. 0.005 lb/103 Gal.
0.001 lb/103 Gal.
* Typical IAF Operation
SAL 000005950
The data for Table A-2 were extracted from "Report to Congress on the
Discharge of Hazardous Waste to Publicly Owned Treatment Works", U.S. Envi
ronmental Protection Agency, EPA/530-SW-86-004, 1986. The following notes
apply to this table:
The data from this table apply only to secondary biological wastewater treatment plants receiving low concentrations (s 500 ppb) of the compounds listed. A number of design and operational factors will affect the fate of these compounds in any given treatment plant. These numbers are useful only as rough approximations of pollutant fate.
All percentages are based on influent loading. The original ref erence provided removals for volatilization and sludge partitioning as a percentage of overall removal. This data was translated to removals based on influent loading by assuming that all material not volatilized, transferred to sludge, or passed through untreated was biodegraded.
(Percent volatilized to air) + (percent partitioned to sludge) + (percent biodegraded) + (100 - overall percent removal) 100.
Percent biodegraded was determined by difference in the preceding equation.
The percentage which is discharged to receiving waters equals 100 minus the "overall percent removal" (percent discharged to receiving wastes = 100 - overall percent removal).
(Percent volatilized to air) + (percent partitioned to sludge) +
.(percent biodegrded) + (percent discharged to receiving waters) =
100
"Acclimated" represents those processes which receive a relatively steady amount of the pollutant in question, such that biodegradtion rates stabilize. "Unacclimated, Median and Low" refer to processes which receive unsteady or "slug" loadings of the pollutant in question.
A-12
SAL 000005951
TABLE A-2.
FATE OF HAZARDOUS AND/OR TOXIC POLLUTANTS AT LOW CONCENTRATIONS SECONDARY, BIOLOGICAL WASTEWATER TREATMENT PLANTS
DVERAL 'ERCEN 1EMOVA
Ipercen r VOLATILE D
TO AIR
PERCENT PARTITIONED TO SLUDGE
IN
PERCENT BIC DEGRADED
POLLUTANT
ACCLIMATED JNACCL IMATEC ACCLIMATED UNACCL MATED ACCLIMATED UNACCLIMATED ACCLIMATED JNACCLIMATED
MEDIAN LOW
MEDIAN LOW
MEDIAN LOW
MEDIAN LOW
% %%
% %%
% %%
% %%
2.4-D ACENAPHTHYLENE
ACETALDEHYDE ACETONE ACROLEIN
ACRYLAMIDE ACRYLIC ACID ACRYLONITRILE
ALDRIN ANILINE ANTHRACENE ANTIMONY ARSENIC BARIUM BENZAL CHLORIDE BENZENE BENZOTR CHLORIDE BENZYL CHLORIDE BIS-2-CHLOROETHYL ETHER BIS-2 ETHYLHEXYL PHTHALATE BROMOMETHANE BUTYL BENZYL PHTHALATE CADMIUM CAPTAN CARBON DISULFIDE CARBON TETRACHLORIDE CHLORDANE CHLOROBENZENE CHLOROBENZILATE CHLOROETHANE CHLOROFORM CHLOROMETHANE
(continued)
90 95 95 95 95 90 90 90 90 95 95 60
SO
90 90 95 90 90 90 90 95 95 27 90 95 90 90 90 90 95 90 95
60 SO 90 90 95 95 50 30 95 95 62 50 65 60 76 70 90 90 65 60
80 90 60 60 60 60 90 90
55 60 90 90 45 40 90 90 SO 30 90 90 95 95 90 90
27 27 50 30 85 80 65 80 90 90 90 90 60 50 90 90 80 80 90 90
0 00 19 54 54 0 5S 0 32 0 55 0 00 0 00 0 44 0 00
0 00
0 00
0 00 0 00 0 00
0 17 15 24 72 72 18 14 12 23 45 45 0 32 0 00 06 90 90
0 00
0 00
0 00
76 77 72 72 77 72 9 99 27 45 45
9 65
76 81 81 63 72 72 66 86 86
7 54 9 86 10 10 10
10 5 3 10 10 10 9 65 9 98 9 87 33 33 33 10 9 8
52 . 50 50 60 60 60 SO 50 SO 90 90 90 7 44
2 22 7 43 7 77 9 53 66 66 66
0 00
43 41 41
27 27 27 7 42 1 11
12 9 8 33 33 33 14 14 14 7 54
1 11 2 22 1 11
83 SS 46 67 28 28 85 61 81 85 43 26 85 61 81 81 56 45 81 77 72 81 64 60 57 57 57
86 77 72 43 41 41 0 00 0 00 0 00 83 34 31 69 16 16 65 28 25 60 38 38 81 43 26 24 24 24 10 5 5 52 50 50 0 00 83 46 28 18 a 7 6 00 48 48 46 50 32 32 74 49 41 18 8 6 25 6 6 9 44
SAL 000005952
TABLE A-2 (continued)
DVERAL . ^ERCEH
1EMOVA
PERCEN r VOLATILI2 1
TO AIR
PERCENT PARTITIONED TO SLUDGE
|
PERCENT QK^DEGRADED
POLLUTANT
ACCLIMATED JNACCL IMATED ACCLIMATED UNACCL MATED ACCLIMATED UNACCl IMATED ACCLIMATED JNACCLIMATED
MEDIAN LOW
MEDIAN LOW
MEDIAN LOW
ME01AN LOW
% %%
% %%
% %%
% %%
2-CHLOROPHENOL
95 65 60 0 0 0
8 55
87 60 55
CHROMIUM
70 70 70 0 0 0
70 70 70
0, 0 0
CRESOLS .
95 SO 40 0 0 0
8 4 3 . 87 46 37
CUMENE
95 95 95 38 57 57 4 4 4 S3 34 34
CYANIDE
60 60 60
0
33
57 57 57
3
00
CYCLOHEXANE
95 95 65
10 86 86
4
44
82 6 6
DI-N-BUTYL PHTHALATE
90 90 90
0
00
20 20 20
70 70 70
DI-N-OCTYL PHTHALATE 90 90 90 0 0 0 7 7 7 63 83 83
DIBROMOMETHANE
65 60 80 43 64 64
13 12 12
30 4 4
1,2-DICHLOROBENZENE
90 87 85 45 78 77 32 9 9
14 0 0
1.3-DICHLOROBENZENE
90 87 85 45 78 77 3 3 3
42 6 6
1.4-DICHLOROBENZENE
90 87 85 45 78 77 23 9 9
23 0 0
1.2-DICHLOROETHANE
90 50 30
46 45 27
5
32
41 3 2
1.1 -DICHLOROETHYLENE
95 90 90 76 81 81
0 00
19 9 9
2.4-DICHLOROPHENOL
95 55 50 0 0 0
8 4 4 07 51 46
1.2-DICHLOROPROPANE 90 70 70 45 63 63 0 0 0 45 7 7
DtCHLORVOS
90 50 30 0 0 0 9 5 3 61 45 27
DICOFCL
90 90 90 45 45 45 8 8 8 37 37 37
DIETHYL PHTHALATE
90 75 70 0 0 0 1 1 1 89 74 69
3,3-DIMETHOXY BENZIDINE 60 30 20 0 0 0
8 32
72 27 16
2.4-OIM ETHYL PHENOL 95 85 80 0 0 0 8 7 6 87 78 74
DIMETHYL PHTHALATE
95 65 60 0 0 0
0 0 0 95 65 60
2.4-DINrTROPHENOL
90 75 70 0 0 0
9 87
81 68 63
1.4-DIOXANE
90 50 40 0 0 0 9 5 4 81 45 36
EPCHLOROHYDRIN
87 59 25 0 0 0 9 6 3 78 53 23
ETHYLBENZENE
95 90 90 24 72 72 6 5 5 66 13 13
ETHYLENE OXIDE
90 50 40 0 3 2 9 5 4 81 43 34
ETHYLENE THIOUREA
65 67 60 0 0 0 9 7 6 77 60 54
FORMALDEHYDE
65 85 80 0 4 4 9 9 6 76 72 68
HEXACHLORO-1.3-BUTAOIENE
95
90 90
0
55
9 88
86 77 77
HEXACHLOROETHANE
95 90 90 0 5 5 9 8 8 66 77 77
HYDRAZINE
95 85 80 0 4 4
10 9 8
65 72 68
(continued)
SAL 000005953
TABLE A-2 (continued)
DVERAU 'ERCEtf
1EMOVA
Ipercen r VOLATILIZl D
TO AIR
PERCENT PARTITIONED TO SLUDGE
1-------fERCENT Bid[(DEGRADED
POLLUTANT
ACCLIMATED JNACCl IMATEC ACCLIMATED UNACCL MATED ACCLIMATED UNACCLIMATED ACCLIMATED JNACCL IMATED
MEDIA!- LOW
MEDIAN LOW
MEDIAN LOW
MEDIA!' LCW
% %%
% %%
% %%
% %%
A-15
LEAD MALEIC HYDRAZIDE
MERCURY METHANOL METHOXYCHLOR METHYL ETHYL KETONE METHYL ISOBUTYL KETONE METHYLENE CHLORIDE N-BUTYL ALCOHOL NNITROSODIMETHYL AMINE NAPHTHALENE
NICKEL NITROBENZENE 2-NITROPROPANE P-BENZOOUINONE PARATHION
PCB PENTACHLOROPHENOL
PHENOL PHENYLENE DIAMINE
PHOSGENE PHTHALIC ANHYDRIDE
PYRIDINE SELENIUM SILVER STYRENE t. 1.2.2.TETRACHLOROETHANE TETRACHLOROETHYLENE
THIOUREA TOLUENE TOLUENE DIAMINE TOXAPHENE
(continued)
70 90 SO 100 90 95 90 95 95 90 95 as 90 95 95 0 92 95 95 90
too 90 15 50 90 90 90 90 90 90 90 9S
70 70 75 70 so so 95 95 90 90 50 30 50 30 07 85 90 90 75 70 75 70 35 35 25 20 95 95
50 40 55 40 92 92
25 20 85 80 75 70 too 100 90 90 15 10 so 50
90 90 90 90 25 20 85 80 75 70 90 90 75 70 90 90
0 00
0 00
0 33
1 55
54 54 64
0 32
0- 0
0
38 52 51
0 00
0 00
0 44
0 00
0 00
66 90 90
0 00
0 00
9 99
0 00
0 00
0 00
1 55
0 00
0 11
0 00
0 00
23 72 72
36 15 12
45 68 64
0 00
23 72 72
0 00
57 72 72
70 70 70 9 67 48 48 48 10 10 10 8 66 10 S 3 9 53 13 12 12 10 9 9 9 87 27 21 20 35 35 35 9 32 11 8 43 0 43 22 22 22 17 5 4
14 13 12 9' 8 7 10 10 10
9 99
2 21 so so 50
90 90 90 14 14 14 4 11 3 32 9 87 25 18 18 9 87
4 44
0 00
81 68 63 2 00 90 81 81 28 28 26 85 43 26 61 45 27 44 23 22 86 81 61 61 68 63 6B 50 47
0 00
81 23 16 9 44
87 46 37 0 51 37 61 61 61
78 21 16
61 72 66 81 68 63
90 85 65 81 81 81
13 13 9
0 00
0 00
54 5 5
50 9 7
42 14 14 81 68 63 42 0 0
81 68 63 34 14 14
TABLE A-2 (continued) POLLUTANT
DVERAL L 5ERCEN` 1EMOVA
PERCEN r VOLATILEp
TO AIR
ACCLIMATED LlNACCL IMATED ACCLIMATED UNACCL IMATED
MEOIAN LOW
MEDIAN LOW
% %%
% %%
PERCENT PARTITIONED TO SLUDGE
1
ACCLIMATED UNACCLIMATEO MEDIAN LOW
% %%
--------1-------PERCENT BK DEGRADED
ACCLIMATED JNACCLIMATEC MEDIAN LCW
% %%
TRANS-1,2-DICHLOROETHYLENE
90
60 80
63
72 72
27
88
TRIBROMOM ETHANE
65 35 30 36 21 18 5 3 2
1.2.4-TRICHLOROBENZENE
85 85 85
43 51 51
8
88
VI .1 -TRICHLOROETHANE
95 90 85
78 81 77
1
11
t.1,2-TRICHLOROETHANE
80 25 20
40 20 16
0
00
TRICHLOROETHYLENE
95 87 85
67 70 68
6
65
2.4.6-TRICHLOROPHENOL 95 55 50 0 0 0 6 4 4
1,1.2-TC 1.2.2-TF ETHANE
90
85 80
63 68 64
4
33
TR1FLURAUN
90 90 90 0 0 0 33 33 33
VINYL CHLORIDE
95 95 95
86 90 90
2
22
XYLENES
95 87 85
24 70 68
14 13 13
0 00
24 11 10
35 26 26 18 8 8 40 S 4 23 12 12 87 51 46 23 14 13 57 57 67
6 33 57 4 4
I* x i"ar*M'tR^)
LAND TREATMENT MODEL DATA
(land treatment *
L,Loading (g oii/cc soil;
Enter Ci
10^6 VO ppnw
1,Depth (cm)
Total porosity
Air Porosity (default=0)
MW ail
VG di55. in water enter 1
Time o-f calc, (days)
Biodegradation, enter 1
Temperature (Deg. C)
Wind Speed (m/s)
Area (m2)
0.036 2000 20 0. 61 0-5 282
365-25 1
25 '1-47 25000
COMPOUND NAME
LAN DTRE AT MENT
FRACTION LOST
AIR
BIOL
INTERMEDIATE TIME
365.25 days
AIR
BICL.
METHYL ETHYL KETQNF BENZENE TOLUENE CRES0LS NAPHTHALENE PHENOL CARBON TETRACHLORIDE TRICHLGRQETHANF{i,1,>
METHANOL ETHYLBENZENE CUMENE ( i sopropy 3 H'jni er: XYLENE<-o>
\
0.7 i 4 0.903 0. 4 9 /]
0.056 0.04 7 0.076 0.996 0.996
0.966 ) -3o3 O.998 0. 320
O. 286 0. 097 0.506 0. 944 O. 953 0- 924 O. 002 0. 002
O. 034 O. 667 0.002 O. 660
0.714 0. 903 0.492 0.056 0.047 0.076 O. 993 0.996
0.966 0. 362 0.968 0.320
0.286 0.097 0.508 0-944 0-953 0.924 0.000 0.000 0.034 0.638 0.000 0-680
SAL 000005956
C^b&rni c.o.1
Beo^ne. c T^fueKie tf>
Ben^ne.^ Yulene^' CyC-^ohex-a ne(C
Nlop h+tin {ene.
Cu.mcncu' P&ewdo- Cxunersfi^ B'lphenyP1
.Gasoline0^ Cr L0 K&rosene.01 T)itiSeJ01
Ma-ph-H^CL,^
;
Vd-p^ Pressure. ^ffeCA-)
L5: a.i
0. 12 o-iff
l 3 lo\
Q.op^fc
o.pq^
0.0, 0/9 : 0.02,93; 0.01*13
t:
. L.x sA .
.0.0/ /
0.009
L L> .
(0 Cp ep/s
VeRSfOAl 3 T*SLe
It
Ovulo latioa] (S*-> i^a^Ce,
Conoco Inc. Calculation Sheet
Job Nc F ie'0
SAL 000005957
APPENDIX C 1988 OPERATING EXPENSE AND YIELD DATA
<BLUE BOOK) SARA TITLE III, SECTION 313 1988 TOXIC CHEMICAL RELEASE INVENTORY
LAKE CHARLES REFINERY
000005953 SAU
SAL
REPORT NO. 08-0512 JOB NO 6656 PROGRAM _NO- A7632
LAKE CHARLES REFINERY
PROCESSING SUPPLIES ---OTHER DETAIL - SCHEDULE C (IN THOUSANDS)
ITM-FTR---------- DESCRIPTION---------
___nfrFMRFR 14AA___ QUANTITY DOLLARS
PROFTT Oft.l 14AA QUANTITY DOLLARS
CUMULATIVE TO DATE ACTlIAt 1488
ACTUAI 14A7
QUANTITY DOLLARS QUANTITY DOLLARS
PROC SUPP-NONCLASSIFIED -- 01)6 Altai Arm SOI FURTC
1 ftS
006 0531 ACIDIC ACID LBS
006 0103 ACTIVATED ALUMINA DE-'4 LBS
006 0)04 ACTIVATED ALUMINA-H-151LBS __________________ 00A 0X7A ArTTUtTD CflRftON
ms
006 0116 ALUM
LBS 62.0
006 0394 ALUMINA BALL T-162 1/2 LBS
006 046? AHBERLITE 200
LBS
_______________ t= flflA-PQlg-AMMQMTA_______________ __--LBS,
3. A
006 0699 AN - 676 CHEVRON OLOA GALS
006 0502 ANION RESIN
CUFT
006 0406 B - SQUARE 10025
GAL
__________________ fl04_flSflA-BPT7 ADJUNCT ?l/_______ - LBS.
2.6 1.6
006 0557 BETZ AF11
006 0169 BETZ C-30 SLIM1CIDE LBS
1.3
006 0176 BETZ DEI 166 L6S
__________________ 004.040* rstt
___________ ftil ______ g-A _
006 0177 BETZ DM1112
GALS
006 0061 BETZ DM1331 PROCHEM
006 0526 BETZ EB 911 ftftA 1)412 RFT7 flR-16
LBS GA1S
006 0209 BETZ OS-6 OS-22 006 0460 BETZ SULFITE 3
GALS LBS
006 0074 BETZ 2W10 PROCHEM aoa nnAn ppt? 7Wi ? ppocmph
006 0163 BETZ 2*2
006 0164 BETZ 2W30
.2
006 0332 BETZ 2W33
LBS
A R6A APT? 7ftn?6
1 RS 14. A
006 0437 BETZ 2020
GAL
006 0439 BETZ 2040
006 0424 BETZ 22K 006 0426 BET7 742
LBS.
. LBS
13.7 .9
006 0179 BETZ 30K
006 0442 BETZ 35A
006 0423 BETZ 407 nflfc 0*70 RPT7 AS
LBS 1 RS
3.1 LBS LBS 2.1
006 0061 BICARBONATE SODA
LBS
006 0017 CALCIUM HYPOCHLORITE
006 073S CALGON KID LBS AAA 0370 TAI Itmi PCI -F-7 2466 1 RS
36.1
006 0251 CALGON WT 2460
GAL 23.6
1 006 0363 CALGON MT 2511 L8S 006 0094 CATALYST FCC EPZ -55 LBS
A4
)R & 4.8 1 .0 3.2
13.7 5.9
94 0
1.8 73.5
15.2 4.1 1.4 2.0
9.0
8.3
7.4AA.1 10.7
141.2 3.8
22.1 16.4
527.2
17.9 46.4
41.1
7.0 54.7
39.3 19.8 19.0
13.5 17.3
50.0 64.9 141.2
8.8 7.1 31.3
46.5 .. 574.0
.3 7.1
.6
11
1.2 5.9
.9 944.7
5.8 11 A
12.8 63.3
8.5 77A.4
140.9 12.2 38.2
27.8
.6 .3
525.7 8.4
402.1
148.2 52.8 16.9
25.7
.2 .4 135.4 14.3 140.9
11 . A 52.4
2.3 37 n 562.8
.7 .7 S2.2 42.8
23.2 .4
2.0 20.7 76 A
1 .3 2.3
647.1 10.7 .2 3.2 31 3 74.1 .9 13.813.0 54.2
202.1 .7
6.3 24.5 774 7
.6
1.61 .1 3.7
.6
5.0 8.2
262.2 .5
1.3 47.1
4.9 29.4
.6
22.8 6.4
53.0 86.1
286.4 .7
1.5 48.0 20.5 29.2
.7 20.5
4.7
.3
318.4
.3
60.0
355.3 116.4
268. B
43.6
1260.5 1,012.4
PACE 10 RUN DATE 01/24/69
-1988 CUMULATIVEACT OVER(UNDER)_P
QUANTITY DOLLARS
2.488.1 10.7
22.1 16 4 527.2
7.0 54.7 39.3 19.6 19.0
7.1
46 4
.3
141.7 3.6
17.9 66.4 41.1
13.5 17.3 50.0 64.9 141.2
8.6 31.3
474 n
7.1
.6
11
1.2 5.9
.9 745.2
5.6 lift
12.6 63.3
8.5 77A.4
140.9 12.2 36.2
27.6
.6 .3
525.7 8.4
402.1
146.2 52.8 16.9
25.7
.2 .4 135.4 14.3 140.9
I
REPORT NO. 08-0512
LAKE CHARLES REFINERY
PACE 11
JOB NO 5658
RUN DATE 01/24/89
PROGRAM. NO. A7632________________________________PROCFSSTNG SDPPLTFS OTHER DETAIL - SCHEDULE C__________________________________________________
UN THOUSANDS)
ITM-FTR............ DESCRIPTION..............
-- MONTH .........
DECEMBER IflBB. QUANTITY DOLLARS
-PROFIT OBJ 1988 QUANTITY DOLLARS
CUMULATIVE TO DATE
.ACTUAL., 13fl&. QUANTITY DOLLARS
ACTUAL 14A7 QUANTITY DOLLARS
-1988 CUMULATIVEQUANTITY DOLLARS
PROC SUPP-NONCLASSXF1ED
_______ 006 1116 CATALVST_FCg SP_________ LBS
-S.4-_
7 5-
9% A-
006 0128 CATALYST HYDRO-REGENERATXO
006 0109 CATALYST-DESULF
LBS
006 1113 CATALYST-FCC SPENT
LBS
_______ UAL. ft181 TATAI VgT-MFPf>y__________ LBS.
15.03
90.8
19.47.6
26.0 12.6
S4.6 2.1
16.919
006 001S CATALYST-POLY
LBS
006 0US CATALYST-PLATINUM
LBS
006 111S CATALYST-PLATIUK SPENT LBS
_______ IAL. 0133 CATALYST-RHFNTFQRMTNft LBS.
006 0028 CATALYST-SULPHUR
LBS
006 0217 CATALYST-VANADIUM
LBS
006 9999 CATALYST,PREC METAL TR-oz
_______ ELM. OOQ4 CilKTTC AflDA.~MPRC_ CELL LBS
36.8
61.5 15.1
-------- 3.0 __-
124.4
18-4
463.2 .5
-________________________ 2-3 _ 133.7
1 .AA6.0
775.4 194.3
118.4 109.6
247.7
660.0 2.0
17.4 9.9
1.778.4
1,102.9 233.7 95.1 145.8
63.8 16.1
18.9 144.A
006 0010 CAUSTIC SODA LIQ 006 0021 CAUSTIC SODA FLAKE
006 1010 CAUSTIC SODA-SPENT _______ ELBA. ftftftd rAUCTTP MAI PflTiCM
LBS 602.5 LBS LBS 181.1 1 RA
57.2 10.2
7,399.2 1,630.5
620.6 48.4
8,620.9
128.1
1,654.5 138.4
399.9
28.0
266.9 64.3
006 0389 CERAMIC BALLS
LBS
144.9
91.5
225.9 160.1
006 0393 CERAMIC PELLETS AGGREGATE
006 0190 CHEMLINK, IPC 5120
LBS
--0Q6
PRIME_________________
2.3
6.7 - 8,0
1.0 9.2 1?
89.7
65.5 117.5*
41.4 109.2
96. n
141.4 54.7 40.6
65.2
69.3 14.A
006 0007 CLAY-ATTAPULGUS 16/30 LBS
1,271.2
95.3
006 0365 COP 850 PROMOTER LBS
.4 7.9
2.7 55.2
006 0117 DAVISON COMBUSTION PRO LBS
_______ UAL QQ3A ntPTHviPMP fti vent
LBS
.5 10.5
2.9 67.1
106.0
7A.6
006 0289 DIMETHYL SULFIDE
LBS .1
.3
26.0
25.6
71.9
61.3
006 0067 DUNNAGE MATERIAL
299.8 509.5
599.7 1,019.0
006 0294 DUPONT AO 23
LBS 14.1
flnA 047A OI1PPNT nr.i-4____________ 1 as -......5 .
27.9 4
153.7 5A.4
299.5 41 .3
168.1 69 6
321.9 33.6
006 0093 DUPONT DMD-2
LBS .5 1.7
.5 1.7
006 0149 DUPONT FOA 11
LBS 9.4 11.9
141.2 238.9
114.3 169.1
006 0325 DUPONT FOA 939 LBS
1.3 1.9
- 006 0058 -DYE BRONZE REG GAS .LBS.
7.7 35.3
4.3 19.2
Ln
006 0059 DYE RED PREM GAS
LBS
> 006 0559 ELCO 231
LBS 2.2
3.0
3.8 30.2
16.4 42.3
5.3 116.8
21.7 156.5
006 0401 ENJAY PARADYNE 25
LBS 15.5
14.0
69.2
58.1
22.2
17.6
_______ LL6l_ 0037_ETHYL_MERCAPTAN_________ LBS_
13.4
U.2
O -- 006 0087 FCC CATALYST HEZ 55 LBS 153.6 121.0
1,966.6 1,566.9
542.0 411.4
Q 006 0139 FILTER MATERIALS (HISC) O 006 0397 FILTREN SUPPORT MEDIA LBS
15.6
.9 167.1 2.0
9.2 .5
_______ OCA- 0003 FIRE FIGHTING CHEMICAL
1.3
< 006 0070 HALD0R TK10
LBS
31.3 125.5
o> -- 006 0212 HYDRO TREATING CATALYST LB
144.2-
968.2 2,402.4
932.4 2,465.1
_,006 0211 HYDROCHLORIC ACID
LBS 370.2
8.5
5,896.7 150.6 5,224.3 139.3
78
90.6 1
463.2 .5
7.3 133.7
19.4 76
775.4 194.3
118.4 104.6
1.9A6.0 7,399.2
767 7 620.6
1,830.5
48.4
144.9
89.7
65.5 117.7
91.5 41.4
109.2 74 A
2.7 55.2 .5 10.5
28.0 599.7 153.7
8A.4
.5 141.2
1.3 7.7 3.8 30.2 69.2
25.8 1,019.0
299.5 41 3
1.7 236.9
1.9 35.3
16.4 42.3 58.1
1,966.5 1,566.9
15.6
.9
31.3 125.5 968.2 2,402.4 5,896.7 150.6
REPORT NO. 08*0512 JOB NO 6658 PROGRAM-NO. A7A3?
LAKE CHARLES REPINERY
PROCESSING SUPPLIES.? OTHER DETAIL - SCHEDULE C (IN THOUSANDS)
PAGE 12 RUN DATE 01/24/89
ITH-FTR............DESCRIPTION --
- MONTH.......................................................... CUMULATIVE TO DATE..................................................1988 CUMULATIVE-
DECEHftER 1988
PPftFTT OS.l 1 988________ ACTUAL 1988___________ ACTUAL 14ft?_________ ACT-OVERlUHDERi. P
QUANTITY DOLLARS QUANTITY DOLLARS QUANTITY DOLLARS QUANTITY DOLLARS
QUANTITY DOLLARS
PROC SUPP-NONCLASSIFIED
_______ 006-0138--HYDROGEN^ELECTRO CU-FT
119.7 4.7 AA.4 3.4
119.7
4.7
006 0300 K602
LBS
006 0136 METHANOL
GALS
006 0387 MOLECULAR SEIVES
LBS
_______ tLQA--04S4- MORPMniIMF___________ - 1 BS
006 0520 NALCO D5163
LBS
006 0337 NALCO 1214
LBS
006 0524 NALCO 1701
GALS
AAA -0223- NALCO 19_____________
1 BS
006 0669 HALCO 19
LBS
006 0193 NALCO 2RB431
LBS
006 0244 NALCO 356
_____ 105.-0280- NALCO SI&3_.... GALS.
LBS
006 0231 NALCO 5166
LBS
006 0597 NALCO 5180 LBS
006 0493 NALCO 5196
AAA 200 Nil rn 37AS
1 BS
.8 .1
4
1.1
3.6 1 .4 1.5
.1
1.2
1 . ft
1.5
7.1 1 .7 4.0
.1
8.8 1.0 21.8 2ft. 7
6.5 10.0 73.6
4.1 4.5 47.5 IAS 17.0 1.7 7.0
14.9 .8
24.4 77.ft
11.4 16.6 19.8
3.2 7.0 89.4 70. A
43.8 4.0
10.8
16.6 6.6
22.3 6.3 9.6
.5
40.4 36.6 46.6
3.7 16.4
4.7 6.6
25.6 1.6
19.1 1A. A 10.7
.6
28.1 54.5 79.7
A.ft 40.4 11.2 10.2
1A
6.6 1.0 21.6 7fl 7
6.5 10.0 73.6
4.1 4.5 47.5 1A. 3
17.0 1.7 7.0
14.9 .8
24.4 7? A
11.4 16.6 14.8
3.2 7.0 89.4 7ft.A
43.6 4.0
10.6
006 0347 NALCO 5375
LBS
006 0353 NALCO 5553 LBS
006 0322 NALCO 5701
LBS
----------- 004 -0502- MALCQ_72flfl___________ - 1 BS
21.7 2-2
18.2 2.9
21.7
5.8 47.1
18.2
7.5 60.7
26.8 34.4
29.2 66.0
21.7
5.6 47.1
16.2
7.5 Aft. 7
6 490 NALCO 8252
LBS
006 0265 NALCO 8263
006 0354 NALCO 85RB253 AAA AA1A MAI CO A3PP174
LBS 22.4 1 RS
15.2
466.6 .7
321.0
1.5 a-
213.3
5.4 A.A
137.5
12.8 3.7
466.6 .7
321.0
1.5 4
006 0339 NALCO 87RC130 LBS.
006 0351 NALCO 87RE010 LBS
006 0137 NITROGEN
CU FT
AAA 0377 NTTPOCFN CYLINDERS
1.6 49.3
4.1 65.4
3.0
609.2 1
7.6
2.7 644.2
.9
4.5
592.6 .1
4.7
532.5 .3
3.0
609.2 1
7. 6
2.7 644.2
.7
006 0685 OXYGEN
LBS .7 29.4
10.8 452.1
13.9 530.2
10.6 452.1
006 0705 OXYGEN P/L FEE
LBS
4.3
47.1
51.3
47.1
006 0013 PLATINUM
TR OZ
_____ 006 0303 POTASSIUM-PERMANGANATE LBS
2.9 1.0 1.0
38.4 7.9 13.1
2.9 1.0 1.0
006 0703 SHELL CATALYST HPS 544LBS
006 0503 SHELL 514 1/3" SPHERE LBS
006 0392 SILICA GEL
IBS
_____ (ULL 0024 SnnA ASH
_____LBS-
.7
.1
>
006 0053 SODIUM CHLORIDE (SALT) LBS 150.1
1.8
r- 006 0459 SODIUM HYPOCHLORITE LBS
4.8 17.4
1.8 6.4
858.0
2.0
10.3 35.8
2.5 .7
10.3 .2
4.5 14.1
1.6 4.1
748.6 6.5
9.1
29.9 3.4 .6
13.4 1.0
4.6 17.4
1.8 6.4 656.0 2.0
10.3 35.6
2.5 .7
10.3 .2
006 0050 SODIUM SULFITE - HYDRO LBS
.3
006. 0018 SODIUM*MOHQSOOIUM PHOS_LBS_ 47.1_____28.5_______________________________472.6
.2 28S.6
.5 S37.8
.4 .3 .2 352.3________ 472.6_ _ 285.6
006 0020 SULPHUR
LBS
.1
006 0022 SULPHUR DIOXIDE
LBS
12.5 4.3 19.4 3.6
12.5
4.3
006 0321 TRET-O-LITE PET 4400 LBS
2.4 5.1
2.4 S.l
000059
REPP NO. 08-0512
JOS 6656 PB06RAH. Mft. A7649
LAKE CHARLES ','CINERY
PROCESSING S1IPPI TPS - OTHPk .IgTAIL - SCHEDULE C (IN THOUSANDS)
PAGE 13 RUN DATE 01/24/89
ITM-FTR-
----- MONTH ..........
CUMULATIVE TO DATE -
___ DECFHftgR_A4HA____ _pgnfTT nn- 14aa _____APTH1I 14HA_______ ACTUAL.1987.
QUANTITY DOLLARS QUANTITY DOLLARS QUANTITY DOLLARS QUANTITY DOLLARS
-1986 CUMULATIVEAPT fll/PR t MNflFft 1 P
QUANTITY DOLLARS
PROC SUPP-NONCLASSIFIED
on6 QAH9 TPFT-n-l TTP K447
Gtl *
006 0612 TRET-O-LITE DS 415
GAL
006 0613 TRET-O-LITE K450
GAL
006 1186 TRET-O-LITE AF-61 006 fillA TPCTfll TTP PET 79ftn 1LBS_____
006 0617 TRETOLITE K-4S6 LBS
6 702 TRETOLITE DS 4056
GAL
006 0712 TRETOLITE PET40000
_______________ 0Q6 0718.jTBETnLiT_amn
QAI
006 0046 TRIETHYLENEGLYCOL
006 0052 TRISODIUH PHOSPHATE
LBS
006 0468 TYSOL HW50
LBS
006..0469.-LICARS01_-.UnEA_________ i ft*
006 0471 UCARSON HS - 101
LBS
006 0106 VAN DRI-O-LITE
LBS
006 0123 ZEOLITE AMBERL1TE 120 LBS Qfl6_nfl2L tHI.PBftfHtM__________
006 0073 5K10 PH1LHPULUS
TOTAL PROC SUPP-NONCLASSIFIED
___________________ppnr. supp.rnpp thh rppnn
006 0485 BETZ 562
LBS
006 0601 TRET-O-LITE K-430-H GALS
TOTAL PROC SUPP-CORR INH (PROC)
An 2.8 4.2
.8 1.9 2.8
9.3
1 to &
1.2 2.1 6.0
6.9
196.7
i 11 .1 .7
1,277.5
2.1 2.8 2.6
54 4
5X.1
39.2
57.0
9.n
19.1 34.4 34.4
%
164.4 3.0
V4
26.5 35.2 68.8
5
96.3 1.0
1 .79(1.7 1.504.4
.6 .4
1.7 16.7 .8 6.2 14,606.1
.5 24.3
.9 32.8 33.7
44.1 1.4
44.2 37.9
13.3 30.0 38.3 40.9 36.2
15.0 690.9
44.0 .1
11.2
44.9 1.6
58.0 56.5
17.4 25.9 66.2 70 .7
9.8
8.0 784. (1
51.0
16.3
14,024.0
27.3
33.7 33.7
54.4
54.1
39.2
57.0
9A
19.1 34.4 34.4
4
164.4 3.0
44
26.5 35.2 68.6
5
96.3 1.0
1 .94(1 7 1 .504 4
.6 .4
1 7 16 9 .6 6.2 14 ,606.1
.5 24.3
.9 32.6
33.7
TOTAL CLASSIFIED
2.6
33.7
33.7
33.7
TOTAL PROCESSING SUPPLIES ___________________ PFR RRI f.RUflP..CHARGE______
1,280.4 96ft?
14,639.8 -2715
14,057.7 __ .2821____
14 ,639.6 -2715_______________________
V> >
O
o
o-
o o
VJ1 *0 O' i\>
in >
r* o
o
--o
OIk)'
<
REPORT NO. 08-0514 JOB NO 6658 PROGRAM N0.-A7632--
LAKE CHARLES REFINERY
OTHER PURCHASES DETAIL SCHEDULE D (IN THOUSANDS)
PAGE 14 RUN DATE 91/24/89
FTR
DESCRIPTION
MONTH ...........
rtrrPMnpB iaaa
QUANTITY DOLLARS
profit na.i iom QUANTITY DOLLARS
CUMULATIVE TO DATE ACTUAL I4AA
ACTUAL _
QUANTITY DOLLARS QUANTITY DOLLARS
-1988 CUMULATIVE-
act m/FBMJHnrm po
QUANTITY DOLLARS
7413-REF OTHER PURCH INTERDEPT 111? A?43 ftllTANF <NflRHit RIITANF> 012 8216 CASINGHEAD <LT. GASO> 012 8539 CAS OIL 010 8982 GREEN ANODE COKE (119 A?5? TSORIITANF 012 0191 ISOPENTANE 013 0180 NAPHTHA CUTTERSTOCK 013 8285 SLOP
TOTAL REF OTHER PURCH INTERDEPT
7414-REF OTHER PURCH INTERDEPT nxn A7A5 rr xro saetuav 030 8096 CITCON WAX 074 0000 EXCHANGE BALANCE INC/OEC 001 8982 GREEN ANODE COKE rtAft OOOA OTHER fHTRC ITEMS * FVP1 009 7100 VACUUM BOTTOMS <VAC RESID> 00300000741400000000
A? 24
AX 8
179
7A9 360
4
1 .17? 123 3
2,452
351 261
10
836 93
1,208 5
2,783
4.819 4,295
119
13.106 1,422
16,363 24
42,166
266 291
10 20 648 101 2,062
3,449
4.5S0 5,104
68 243 13.754 1,762 36,140
61,646
351 281
10
A36 93
1,208 5
2,763
4.814 4,295
119
It.llU 1,422
16,38.24
42,168
1 33
11
303
39
?16
?.A?S
1 . A7?
4.360
112
1
?1A
33____________ 11 303
3 r8?3 112
?1 7
X.?AX
1 .872
4.344
?17 3. ?a:.:
7415-REF OTHER PURCH OUTSIDE 082 8932 ANODE COKE LC
081 8934 CAL HIGH SULFUR 082 8986 CAL LS RECARBURIZER 082 8981 CAL RECARBURIZER LC
081 8988 CALCINED ANODE COKE 081 6981 CALCINED RECARB COKE 025 6579 DUST ABATEMENT OIL oas A979 Flirt cpinp coke 025 6539 GAS OIL 082 6940 GREEN ANODE COKE LC 062 6972 GREEN ANODE COKE HAP AAA? GBFEN ANODE COKE 063 6950 GREEN HI SULFUR FUEL 021 0235 HEAVY AROMATIC - VISTA
2S 6280 HYDROGEN OA? A9?1 INTER GRAPHITE 021 0043 KEROSENE 021 8932 LCH ANODE COKE 081 8911 LOW SULFUR RECARB COKE
i 4
31 1 6
194 9 127 95 1,634
?1 13- 301-
24
2
147 83
1,006
117 44
386 3
14 3-
64 102
3 131
3
2,626 1,098 16,422
67 12
280
117 1 34___________
366
20 3
9 31 14
686
3-
37
2 64
3.602
102
1 24
3
131
3
s
221
147
2,625
61 1,368
83 1,096
956 19,125 1,006 18,422
31 67
60 1,333
12
5 280
REP. NO. 06-051*4 JOB NO 6656 PROGRAM NO. A7632
l LAKE CHARLES
INERY
DTHFR PURCHASES DETAIL - SCHEDULE D (IN THOUSANDS)
t
PAGE IS RUN DATE 01/24/69
FTR ................... DESCRIPTION ................
........... MONTH ........... nrrFHRPP irp.a
QUANTITY DOLLARS
-- CUMULATIVE TO DATE
PPOFTT OBJ 1988
AOTUAl 1986
APTIIAI 1987
QUANTITY DOLLARS QUANTITY DOLLARS QUANTITY DOLLARS
-1968 CUMULATIVEACT rWFRMINnFftl PO
QUANTITY DOLLARS
741S-REF OTHER PURCH OUTSIDE mn flflOfl NAPKFT PI tRCHA3F8-0HTRTnF
021 0300 MOLEX GASOLINE 21 66 MOLEX RAFFINATE
026 0115 MTBE _______________022 A182 NAPHTHA__________________________
061 6987 NO. 1 CALCINED COKE 082 6922 NORMAL PREMIUM GRAPHITE 062 8930 NORMAL RECARBURIZED COKE
24 8442 OLD PI ANT TAR 022 0915 PYROLYSIS GAS 021 8286 SABINE HAD 021 8285 SLOP n?? 7?on soHTn siurry on
21 280 STRIPPER OVERHEAD 025 0001 SULFURIC ACID 082 6920 SUPER REGULAR COKE fl24 716 0 UAPrilM BOTTOMS
082 6910 X COKE 081 6931 IV. SULFUR RECARB COKE
TflTAI PFF OTHFP PURPH nilTSTOF
54 923 263 5,844
23 3
A 3 786 9 47
IPS 1 .8A8 35 664
643 217-
668 12.547
546 2,652
40 - 130
495 147 1 .048 398
743
7.636
10,127 55,218
1,236 2.166
14 73 130 7.158
1 740
8 14 .404
6,765
6 10.156
94147
1 31 .636
13 423 2,560
216
413 129
17 4
565 327
5
1 .720
7.443
76 6,069 55,205
4.337 270 12 31
6.649 2,544
78 42 9.381 6,465 45
6 29.377
144.307
546 2,852
40 13ft
495 147 1 .048 398
743
7,638
10,127 55,216
1,236 2.164
14 73 130 7.158
1 740
8 14.404
6,765
6 10.156
94147
131.638
TOTAL OTHER PURCHASES PER BEL CRUDE CHARGE
848 14,996 3.1473
10,638
177,089 3.2636
22,614
220,351 4.4223
10,638
177,089 3.2636
in
>
o o
o
o
o Ul o CN
Vt
> r* o o o o
O
Ln
O O' u.
REPORT NO. 08-0532
JOB NO. 6658 PPnnRIM NO. A763A
LAKE CHARLES --CA3DL TNF Rl FMncg
REFINERY
0029 - CODE
DECEMBER 1988 ____________ QUANTITY_________ nm i 6R3
CURRENT YEAR
OUANTTTY
nni 1 AB3
PAYROLL 002 0002 OPERATORS _____ C02 0403 TRUCK--DBIUFRS_____________________
013 0000 MAINTENANCE LABOR TOTAL PAYROLL
_________contract. costs___________________________ 022 0001 GENERAL LABOR 023 0000 MAINTENANCE LABOR 024 0000 MAINTENANCE MATERIAL fl?ft anni-CONTRACTORS foliip-BENTals
TOTAL CONTRACT COSTS
MATERIAL-OPERATING on* nnpq mi * *n notifies. ________________
003 0013 GENERAL LAB SUPPLIES 003 0015 SAFETY SUPPLIES 003 0017 STATIONERY OFFICE SUPPLIES ftn* nfl*n_MTSr.FH ANrnus______________________
TOTAL MATERIAL-OPERATING
MATERIALS-HAINTENACE ni6 ftflftrt MATFRTII4 MATMTFNACF
TOTAL MATERIALS-MAINTENACE
PROC SUPP-NONCLASSIFIEO ftftA nflgft nvF. - .Rgnyjyp oer. ta*
i ftg
006 0059 DYE - RED PREH GAS
LBS
006 0160 LEAD ALKYL (REG) H GRAMS
006 0294 DUPONT AO 23 ftfiA ft*** ntlPONT FflA 434
1 RR
LBS
006 0327 NITROGEN CYLINDERS 006 0499 ETHYL MHT COMPOUND GRAMS
TOTAL PROC SUPP-N0NCLASSIF1ED
6,872,802 14,070
3,284,490
5,404 5,404
6,785 757 *47
7,838
46 1 .264 1,317
7.mn 2,700
106,735 27,859
187,873 322,466
261 4Aft
85,361 66,110
1,697 24,663
3,601 S .464
36,830
26 365 107
7.720 6,240
32.144 32,195
7 . Aftfl 3,840 37,755,736 135,404
1 .914
32,642,125
34.744 16,445 579,160 263,548
1 .40?
1,672,669 2,769,223
CLEARANCE FROM OTHER DEPTS 018 0036 ELECTRICITY-KWH CLEARANCE
TOTAL CLEARANCE FROM OTHER DEPTS
MISCELLANEOUS EXPENSE 020 0021 DEMURRAGE 020 0026 OTHER TRAINING EXPENSE
651,645 651,645
29,111 29,111
300
7,202,292 7,202,292
308.359 306.359
420
102
r
PAGE 69 RUN OATE 01/24/89
PREVIOUS YEAR
MUMTTTV
nm i AP4
131 303
66,573 69,007
1,251 24,609
3,066 3.320
32,246
1,462
588 3
327
2,360
3A.32? 56,322
4.320 5,260 25,016,213 160,916
1
15,653,575
14 174 21,724 258,145 307,464
2
894,093 1,500,603
4,909,130 4,909,130
178.179 176.179
REPORT NO. 08-0532
JOB NO. 6658 ______________________PROCffAH_NA A7t>tft_________
LAKE CHARLES fiASfti TNF Bl FHflFB_________
REFINERY
0029 - CODE
DECEMBER 1988
CURRENT YEAR
_______________Qiiamtttv___________ nnn a a ft_____________ QUANTITY
nm i ap9
OTHER STATISTICAL DATA
UNLEADED GASOLINE 8LENDED-BBLS ___________________ fXPENBF-TNinBTTQBS___________________________
528,008
-iaf943________
EXPENSE-OTHER
12,479
TOTAL UNLEADED GASOLINE EXPENSE
31,422
COST PER GALLON _______________________TNHlBTTQB^-PnilimS___________
.0014 ______________________a^S6Z_____________
INHIBITORS-POUNDS PER h EEL
18.1190
SUPER UNLEADED GASOLINE BLENDED-BBL
221,979
EXPENSE-MMT COMP. ______________________ FXPFNSF-BFn nvF____________
EXPENSE-INHIBITORS
3,901
EXPENSE-OTHER
5,246
TOTAL SUPER UNLEADED GASOLINE EXP.
9,147
______________________T PCB-ftAi i mj____________________________________ ______________________QP1P______________
RED DYE-POUNDS
RED DYE-POUNDS PER h GALS
INHIBITORS'POUNDS
1,970
______________________iNHtftiTnRS-pmiNna pfb h rri_____________________________________ R.A7U7______________
8,061,295
.0011 9** A74 11.4217 4,440,357
. nnr>A 3,840 .0206 18,957 A.9AO*
179 . P11 177,914 357,125
Pft.470 37,898 96,170 150,512
PAGE 71 RUN DATE 01/24/89
PREVIOUS YEAR
OUAMTTTV
DAI 1 A
9,709,651
.0009 1 f>9 .676 11.2696 5,199,312
nni7 5,280 .0242 22,529
?fl9.A76 157,462 366,536
218,681 19.771 43,046 88,346
371,797
CO
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o o o o
o
VJI
"O
O'
RE, i NO. 08-0532 JOB NO. 8658 __________________ PROERAH h'Q. A7LZR-----------------------------------------
LAKE CHARLES
REFINERY
PAGE 58 RUN DATE 01/28/89
0008 - CODE
DECEMBER 1988 ______________ QUANTITY__________nm 1 ARS
0030008090ST02018982
REGULAR GASOLINE
UNLEADED GASOLINE SUPFR UNI FAflFn
LVT OIL NAPHTHA COKER
201 8992 SULFUR AS H2S NflPMAI P4PAFFTN FFFnsTOrif
KEROSENE (JET-50) NO 2 DIESEL FUEL
NO 2 H.O./NO 2 FUEL OIL POP AS47 Sill FIIB - TONS
TOTAL STOCKS LOADED REGULAR GASOLINE 8BLS
UNLEADED GASOLINE BBLS SIIPFP MMI FAflFn RASOITMF
JET so 9 GRADE NO 2 HEATING OIL TOTAL STOCKS LOADED-LC PIPE LINE run - rn utsta
HYDROGEN - TO VISTA
FUEL GAS - TO VISTA
TOPPED CRUDE TO CIT-CON MvnpnftFN to rtTRn
820 0055 MOLEK RAFF-CONOCO SPEC TOTAL NISC STOCKS LOADEO
SLOP Hm FV PAFFTNATF
CHEMICAL PLANT RETURNS AROMATIC DISTILLATE
CIT-CON BY-PRODUCTS TOTii srnrvs uni OAnFn
HYDROGEN NP GASOLINE TOTAL MISC STOCKS UNLOADED ________________ HLA CARS UNLOADED___________________________
KMT CARS UNLOADED
CURRENT YEAR -------- QUANTITY_____ DOLLARS____
PREVIOUS YEAR
QUANTITY
dollars
1,190
802,396
620,786
368.870
15,917 103,209
11,635 976.182
36,511 538,326
6,128 39.813
2,997,079 1,805,503 3,815,582 9.976.881
2,197,358 6,151,808
16,586,292 9A.766
1
501,322
1,971,317 303.601
38,866
2,913,873 7,720
1.084.66A
.
159,025 38,128
1,830,318 7.728.897
672,938 180,912 653,886
________________ 2_
_
_
REPORT NO. 08-0532
LAKE CHARLES
JOB NO. 6658
PROGRAH HO. A7658__________________________________LIGHT PIL LOADING
REFINERY
RAGE 60 RUN DATE 01/24/89
0012 - CODE
........................ MONTH
DECEHBER 1988 QUANTITY_________ DOI 1 ARS
CUMULATIVE TO DATE...............
CURRENT YEAR
PREVIOUS YEAR
QUANTITY
DOLLARS
QUANTITY
DOLLARS
PAYROLL 002 0005 TRUCK DRIVERS 00? 0008 LANDSCAPING AND GARDENING_________ 002 0019 DISMANTLING 013 0000 MAINTENANCE LABOR
TOTAL PAYROLL
1,854 1,854
CONTRACT COSTS 022 0001 GENERAL LABOR
023 0000 MAINTENANCE LABOR QgA 0000 MAINTENANCE MATERIAL_________________
028 0001 CONTRACTORS EQUIP RENTALS TOTAL CONTRACT COSTS
_________ MATERIAL`OPERATING____________________________ 003 0008 HOUSE SANITATION SUPPLIES 003 0030 MISCELLANEOUS TOTAL MATERIAL-OPERATING
150 636 786
MATERIALS-MAINTENACE 014 0000 MATERIALS MAINTENACE
TOTAL MATERIALS-MAINTENACE
2,778 2,778
PROC SUPP-NONCLASSFIED
006 0149 DUPONT FOA 11
LBS
9,400
006 0347 NALCO 5375
LBS
21,668
006 0401 PH-IAV PARAnYNF 75________ LBS________ ____________ 15,544________
006 0478 DUPONT DCI-6
LBS
501
TOTAL PROC SUPP-NONCLASSIFIED
11,936 18,201 IS.956
472 44,566
_________ riEARAMCE FROM OTHPR nFPTS________________ 018 0036 ELECTRICITY-KWH CLEARANCE TOTAL CLEARANCE FROM OTHER DEPTS
</> _________MISCELLANEOUS. EXPENSE________________________ 020 0013 RENT (EX CONTRACTOR 28-00) 020 0021 DEMURRAGE
O TOTAL MISCELLANEOUS EXPENSE o
TOTAL DEPARTMENTAL EXPENSE o PER BBL THROUGHPUT
HO O'
6,000 6,000
268 268
28 28 50,282
141,239 21,666 64.162 58,910
72,000 72,000
165 75
709 24,797 25,766
32 76,343
5.903 5,950 86,227
696 719 1,617
27,427 27,427
236,894 18,201 56.11D 41,275
356,479
3,074 3,074
285 28
313
502,904
243
19,922 20,165
114,340 22.734 42,395
60,944 60,944
15,301 7.095 4,197
26,S94
155 1,401 1,557
5,452 5,452
189,065
17.669 55,594 240,224
2,259 2,259
4,642,491
240 240
296,450 .0612
MMX.
REPORT NO. 08-0532 JOB NO. 6656 PRORBAH NO A7A3A
0012 - CODE
NET DEPARTMENTAL EXPENSE PER BBL THROUGHPUT
OTHER STATISTICAL DATA
LVT OIL NO ? nTf;FI FJJFI NORMAL BUTANE PROPANE TOTAL STOCKS LOADED WITAHF T/T PROPANE T/T TOTAL STOCKS LOAOED FOR NGP-BBLS NORMAL BUTANE T<5nR[ITtHF TOTAL STOCKS UNLOADED TOTAL LOADED AND UNLOADED
A
LAKE CHARLES 1TfiHT OTI 1ninTMR
REFINERY
PAGE 6.1 RUN DATE 01/24/69
DECEMBER 1988
OIIAMTTTV
nm 1 APR
50/282
CURRENT YEAR
nnawTTTV
nm i a pc
502/909
PREVIOUS YEAR qUAMTTTY-------- nm iars_________________________________
4/842/491
296,450 .0612
10,947 1A3.K94
4,048 575,967 732,556
4.AAA
575,967 578,015 142,732 344.049
487,831 1,220,387
-------- (A
>
O
--o
o
o o
Ul
-- so
sj o
10:25 01/09/89
CONOCO INC.-LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 36
**x* UNIT 03 - HO. 3 CTU & VAC HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 352.06 DAYS TO DATE THIS YEAR *xx*
STREAM **** CHARGES **KX
VOLUME. .._________ ..WEIGHT___
BBLS
PCT
MLBS
PCT
CONOCO PIPELINE
TEXACO PIPELINE CONDENSATE
CABINDA-SWEET DOMESTIC BARGE ALASKAN N/SLPE E-A
KUWAIT LAGUNA
E. TEXAS SOUR IRAQ LR
R BUDRAN EGYPT BACH AfUIERD 17 BACHAOUERO 13
HEREY ORIENTE EQUADOR
MENFMOTA VENEZ LAGO TRECO
ARAB MEDIUM PILON MAYA
NAPHTHA C/STOCK DIST. C/STOCK
SLOP SI OP FROM STRGE
SABINE HAD RECYCLE NAPHTHA SEAL OIL FLUSH BA HOS STR GAS B4/B5 HDS GASO
ELB
0.
0522 . 0.
0.
14877. 752933.
0. 0. 0.
0. 0.
166032. 0. 0.
4595. 344867.
0. 0.
3499 . -10.
2041755. 200. 0.
25199 . 4 (1984
14919. 0.
84943. 31971
25473.
0.0 0.2
0.0 0.0
0.4 21 .1
0.0 0.0 0.0
0.0
0.0 4.7
0.0 0.0 0.1 9.7 0.0 0.0
0.1 0.0 57.3
0.0 0.0
0.7 1 .2
0.4 0.0 2.4
0.9
0.7
0. 2455 .
0.
0.
4287. 234990.
0.
0. 0.
0.
0. 52160.
0. 0. 1536. 105960. 0. 0.
1066. -3 .
655473.
52. 0.
7220. 12961.
4688. 0.
26933. 9224. 6052 .
0.0 0.2
0.0 0.0 0.4
20.9 0.0
0.0 0.0
0.0
0.0 4.6
0.0 0.0 0.1 9.4 0.0
0.0
0.1 0.0
58.3
0.0 0.0
0.6 1.2
0.4 0.0 2.4 0.8 0.5
TOTAL 3560764. 100.0 1125050. 100.0
YIELDS itxxx
> TAB OH GAS TAB OH LIQ
--..TAB LSR O IAPHTHA
O RECYCLE NAPHTHA
O ' FROSENE
gDIESEL SC'AS .OIL
SEAL OIL FLUSH M 1 VGO
hvUE VACUUM RES ID
SLOP
ELB
21868. 45537.
179105. 281015.
0.
578590. 305194.
242786. 192698. 315651. 384866. 992650.
0.
0.6 1.3 5.0
7.9 0.0
16.2 8.6
6 .6 5.4
fl.9
10.0
27.9 0.0
4427 . 10202. 44829. 74092.
0.
164560. 91538. 75364. 61120.
100082.
126242. 365744.
0.
0.4 0.9 4.0 6.6 0.0 14.6 8.1 6.7 5.4
TTl
32.5 0.0
____ VOLUME MBBLS PCT
4.3 129.3
0.0 1277.6
97.5 4581.5
717.2 498.6
90.4
1167.9 0.2
858.4 1333.9
307.0 6391.4
344.9 6.3
140.4 562.7 4261.4 14377.2 979.8 228.0 452.3 294.7
185.2 50.3
432.1 89.2
437.8
40298.1
0.0 0.3 0.0 3.2
0.?
11.4 1.8 1.2 0.2
2.9 0.0 2.1 3.3 0.8 15.9 0.9 0.0 0.3 1.4 10.6 35.7 2.4 0.6 1.1 0.7
0.5 0.1 1.1 0.2 1.1
100.0
245.6 512.3 2101.4 3046.9
50.3 5221.8 3635.4
1814.1 1353.6
3747.4 53 <5571 13030.2
80.5
0.6 1.3 5.4 7.6
0.1 13.0
9.0
4.5 3.4
,9.3 13.3 32.4
0.2
WFTGHT
MMLBS
PCT
1 .4 37.5
0.0 386.8
28.3 1429.4
233.3 152.1
31 .3
361.2 0.1
270.2 444.1 105.8 2142.8 106.0
2.1 43.8 171.3 1459.6 4625.5 257.2 67.0 125.6 92.6
58.2 13.4 137.9 26.7 103.0
12914.0
0.0 0.3 0.0 3.0 0.2
11.1 1.8 1.2 0.?
2.8 0.0 2.1 3.4 0.0 16.6 0.8 0.0 0.3 1.3 11.3 35.8 2.0 0.5 1.0 0.7
0.5 0.1
1.1 0.2 0.8
100.0
49.7 104.4
538.1 811.7
13.4
1498.7 1099.2
567.0
432.9 1198.7 1760.i
4784.6 22.3
0.4 0.8 4.2 6.3 0.1 11.6
8.5 4.4 3.4 9.3
13.6 37.0
0.2
m m m pi
K> e> eo
o
C-J o to sy to --*
O' (M
-t o o oo
f-. F-*
m co
fSI O'
C*J
o 'T
*o o o
<V O r- m r- o s in
<\l
so O O CCS3
stsyl ovr- i". e> o
Csl so
m
to
lA --l CO < O *--
_J o
000005972 SAL
6 10:25 01/09/69
CONOCO INC.-LAKE CHARLES REFINERY
I
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 37
UNIT 10 - NO. A HDS
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 347.28 DAYS TO DATE THIS YEAR xxxx
STREAM *#** CHARGES ***#
DECEMBER
_________VOLUME.
WFTfiHT
BflLS
PCT
MLBS
PCT
______ VOLUME_____ MBBLS PCT
WEIGHT_________________ '
MMLBS
PCT
HPU HYDROGEN
^^mjr^TTrroH
tt5 HDS SEP M2 H2 ttl 2 S HPU l H3 CTU KEROSENE
'l *3 CtU DIESEL
'I,: CYC OIL FM STGE ^ CRACKED NAPHTHA ^ MU. 6 HDS GAS0LI
^ MOLEX^GAsOtlNE
FOE
FOE FOE
1666?.
24735. 45382.
19094.
114614. 258661.
309208. 181295. 102793.
0.
1.6 2.3 4.2 1.8
10.7 24,1 28 . B
16.9 9.6
0.0
2976. 6317. 8811.
2974.
32726. 77566.
98726. 49294. 29900.
0.
1.0 2.0 2.8
1.0 10.6 25.1
31.9 15.9
9.7 0.0
190.1 329.2 580.3 147.6
1071.4 3534.0 2279.1 2207.5
866.4 23.2
.. 1.7 2.9 5.2 1.3 9.5
31.5 20.3
19.7 7.7 0.2
31.6 82.1 113.3
23.0 307.4
1068.8 730.9 599.4
251.4 6.2
1.0 2.6 3.5 0.7 9.6
33.3 22.7 18.6
7.8 0.2
**** YIELDS XrfXX
TOTAL 1072444.
100.0
309290. 100,0
11228.8 100.0
3214.2 100.0
STR REFLUX #5HDS
CRACKED GASOLINE____________
H2S RECbVEREDFOE
H2 TO S5 HDS
FOE
' STRP OH GAS
ELE
SWT ST0H TO FUEL FOE
DES DISTILLATE
DES KEROSENE
DES NAPHTHA
SLOP
0. 47490.
2212. 64999. 15154.
0. 799699.
0.
129137. 0.
0.0 4.4
0.2 6.1 1.4
0.0 74.6
0.0
12.0 0.0
0. 11455.
1958.
12749. 4901 . 0.
243406. 0.
33972. 0.
0.0 3.7
0.6 4.1 1.6 0.0 78.7 0.0
11.0 0.0
41.4 453.3
23.3 746.8 172.6
4.9
7417.0 78.2
2017.1 99.3
0.4 4.0
0.2 6.7 1.5 0.0 66.1
0.7 18.0
0.9
9.4 106.0
20.6 138.6
54.0 1.3
2257.6 24.0
533.8
28.4
0.3 3.3 0.6 4.3 1.7
0.0 70.2
0.7
16.6 0.9
LOSS 13753.
1.3
849.
0.3
174.9
1.6
40.5
1.3
TOTAl 1072444. i no. n 309290. i no. n 11228.8 -1PQ.Q._____3214.2_ 100.0
CO
>
o ----o
o
o o vn
----- >0
OJ
0516 10:
01/09/89
CONOCO INC.-LAKE CHARLES . -FINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 38
**** UNIT 14 * NO. 5 HDS
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 334.54 DAYS TO DATE THIS YEAR xx*x
sTReam
xxxx CHARGES xxx*
DECEMBER VOLUME BBLS PCT MLBS
PCT
YEAR TO DATE ......................
VOLUME. MBBLS PCT
weight
MMIBS
PCT
#3 CTU DIESEL
CRACKED UISTILLA
1 3 CTU GAS OIL
2. LT VAC GAS OIL
HV VAC GAS OIL
H2 Hi it"HDS
FOE
STR REFLUX FM 04
46533.
254452. 71414.
124705. 0.
64999. 0.
8.3
45.3 12.7 22.2
0,0 11 .6
0.0
13973. 78997. 22142.
39542. 0.
12749. 0.
8.3 47.2 13.2 23.6
0.0 7.6 0.0
46.5
254.5 1472.4
3247.3 218.7 746.8 41.4
0.8 4.2 24.4
53.9 3.6
12.4 0.7
14.0 79.0 460.6
1039.7 71.7
138.6 9.4
0.8 4.4
25.4 57.3
4.0 7.6 0.5
TOTAL
x x * x YIELDS x * :< x
h STP OVIID TO #4
HYDR SULFIDE SWEET SEP HYD DCS GAS OIL DFS DIST
FOE FOE
562103.
24735. 1679 .
45382. 193122. 293594.
100.0
4,4 0.3 8.1 34.4 52.2
167403. 100.0
6317. 1486.
eon.
59668. 90208.
3.8 0.9 5.3
35.6 53.9
6027.6 100.0
306.7 25.9
580.3
4808.7 293.6
5.1 0.4 9.6
79.8 4.9
1812.9 100.0
77.2 22.9 113.3
1505.2 90.3
4.3 1.3 6.2 83.0 5.0
LOSS
3591 .
0.6
833.
0.5
12.4
0.2
4.0 0.2
______________________ _____ TOTAL . . 562103. . 100,0 -- 167403. 100.0 _6.L22^6- 100,0
1812.9 JMJ____________________________________________
in >
o o o o
o -c
16 10:25 01/09/69
CONOCO INC.-LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 39
xnx* UNIT 82 - NO. 3 CRU 8 HDS HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 354.23 DAYS TO DATE THIS YEAR xxxx
STREAM xxxx CHARGES xxxx
_______VOLUME_______ ____ WEIGHT_________ ______ VOLUME__
BBLS
PCT
MLBS
PCT
MBBLS PCT
______ WEIGHT___________ _ _
MMLBS
PCT
, NAPHTHA
f tf 2 Ml IDS NAPHTHA
403909. 100.0 0. 0.0
105718. 100.0 0 . 0.0
4039.8 173.6
95.9 4.1
1060.6 45.1
95.9 4.1
TOTAL xxxx YIELDS xxxx
403909.
100.0
105718. 100.0
4213.3 100.0
1105.7 100.0
ABSORBER H2
FOE
STAB GAS TO FUEL FOE
~ SWEfcf NAPH/StOR
, STRIP OH LIO
,J STRIP/STAB OFF G ELB
S3 DEPROP OH LIO
~r rePurmate
LOSS
50259. 0.
14269. 31246.
4266. 0.
306434.
-2565.
12.4 0.0 3.5 7.7 1.1 0.0
75.9
-0.6
10111. 0.
3727 . 1551.
937 . 0.
86725.
2668.
9.6 0.0 3.5 1.5 0.9 0.0 82.0
2.5
484.1 2.7
14.3 198.9
69.9 26.6 3274.9
141.9
11.5 0.1 0.3 4.7 1 .7 0.6
77.7
3.4
90.0 O.B 3.7
34,2 15.3
4.7 929.8
27.3
8.1 0.1 0.3 3.1 1.4 0.4 84.1
2.5
TOTAL 403909. 100.0 105718. 100.0
4213.3 100.0
1105.7 100.0
DECEMBER ENDING VALUES RF_ORMATE_RQNC_____________ 100.02______________________________
xxxx UNIT 30 - REGULAR COKER
HAS BEEN ON STREAM 0.0 DAYS IN DECEMBER AND 42.54 DAYS TO DATE THIS YEAR xxxx
STREAM xxxx CHARGES Xxxx
-rDECEMBER ................... ............................................. YEAR TO_DATE_-....................
VOLUME
WEIGHT
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
CC BRIGHT STOCK
CC RESIDUMM
THERMAL TAR SI HCGO
ANOb'E" VAC RES HOT RESID COKER NAPHTHA PYRO TAR
TOTAL
0 . 0.0 0 . 0.0 0. 0.0 n. 0.0 0. 0.0 0. 0.0 o. 0.0 0. 0.0
o. 100 . 0
0. 0.0 0. 0.0 0 . 0.0 0. 0.0 0. 0.0 0. 0.0 0. 0.0 0. 0.0
0. 100.0
175.4 324.4
0.0 1.3 67.1 4.5 1.0 0.0
573.8
30.6 56.5
0.0 0.2
11.7
o.e 0.2 0.0
100.0
62.1 110.1
0.0 0.5 24.2 1.7 0.3 0.0
198.9
31.2 55.4
0.0 0.2 12.2 0.8 0.2 0.0
100.0
xxxx YIELDS xxxx
COKER GAS-FUEL COKER GAS REG COKER GASO
Lit'cui; Gas oil
HVV CClK GAS OIL
CRN LCH ANODE
FOE ELB
TONS
o. 0.0 o. 0.0 0 . 0.0 0 . 0.0
0 . 0.0 0 . 0.0
0. 0.0 0 . 0.0 0 . 0.0
0 . 0.0 0 . 0.0 0. 0.0
6.5 82.6 77.0 249.6
111.1 18.3
1.1 14.4 13.4
43.5 19.4
3.2
1.9
20.5 20.1
7775"
38.7 36.6
0.9 10.3
10.1 3972
19.5 16.4
000005975
O'OOI 9' X
6 ` 861 2*
0*001 O'S
0 * S 9'82
0*001 TO
*0 0
0*001 0*0
*0 0
1V10I sscn
SAL 000005976
516 10:25 01/09/89
i
CONOCO INC."LAKE CHARLES REFINERY
1
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE AO
**** UNIT 39 - PREMIUM COKER
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 309.89 DAYS TO DATE THIS YEAR x**x
STREAM **** CHARGES xxxx
_ VOLUME
BBLS
PCT
WEIGHT_________ ______ VOLUME.
MLBS
PCT
MBBLS PCT
ANODE VAC RESID
CC RESIDUUM CC BRIGHT STOCK HOT RESID THERMAL TAR PVKU 1AR ANODE VAC RESID
.. FCC LCO DIST. RECYCLE
0.
0. 0. 0.
14389G. 88789. 0.
17538. 0.
n. o 0. _____0.0-
0.0 0. 0.0
0 . 0 0. 0.0
0.0 0. 0.0
57.5
54875.
58.2
35.5
33866. 35.9
0 . 0 0. 0.0
7.0
5600 .
5.9
0 . 0 __________ JU.
0.0
... 18.3 91.5 72.6 0.1
2190.3
336.0 96.2
205.8 9.4
0.6 3.0
2.4 0.0
72,5 11.1
3.2 6.8 0.3
TOTAL 250225. 100.0
94342. 100.0
3020.3 100.0
**x* YIELDS *xxx
COKER GAS
ELB
COKER GAS-FUEL FOE
GASQLE.HE____________
LCgo
HCGO
GRN NORM PREMIUM TONS
GRN INTR PREMIUM TONS
GRN LS RECARB
TONS
GRN IX S RECARB TONS
GRN X COKE
TONS
GRN NORM RECARR TONS .
33749. 336 .
10131.
95221. 76004.
0. 0.
4691 .
0.
8235. 1884.
13.5
8254.
0.1 95.
4.0 ....... -2823lfc.
38.1
32537.
30.4
28890.
0.0 0.
0.0 0.
1.9 9382.
0.0 0.
3.3 16471.
0.8 3767.
8.7 0.1 3.0 34.5 30.6 0.0 0.0
9.9 0.0
17.5
4.0
378.7 12.8 95.5
1005.6 945.8
17.1
23.5 24.6
3.5 73.6 12.6
12.5 0.4 3.2
33.3 31.3
0.6 0.8
0.8 0.1
2.4 0.4
LOSS 19974 . 8.0 -7877. -8.3
426.8 14.1
TOTAL -250225. A 00.0 _ _ 9-4342-., 100.0 --3020.3 -100.0 Co
WFTGHT
MMLBS
PCT
6.9
33.5' 27.9
0.0
832.5 127.9
32.7
66.0 3.3
_0^_______________________________________________ 3.0
2.5 0.0
73.6 11.3
2.9 5.8 0.3 .
1130.7 100.0
91.0 3.5
?$ 342.8 360.9
34.3 47.0 49.3
6.9 147.2
25.3
-2.B
1130.7
8.0 0.3 2.3 30.3 31.9 3.0 4.2 4.4 0.6 13.0 2.2
-0.2
100,0___________________________________________________
o
o
o
o OLrp >0
0516 10:
01/09/89
CONOCO INC.-LAKE CHARLES -FINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 41
* xx** UNIT 56 - TiO.'T'CALCINER HAS BEEN ON STREAM 27 79 DAYS ilT DECEMBERAND 210.30 DAYS TO DATE THIS YEAR #***
---------------------- SIRESM------------**** CHARGES ****
BBLS
DECEMBER PCT MLBS
PCT
YEAR TO DATE .....................
VOLUME
MBBLS PCT
WglgHT MMLBS
PCT
GRN NORM PREMIUM TONS
----------- l5Hn"nURM "EECARiT" TuTTS
GRN HI S FUEL
TONS
GRN X CO:(E
TONS
0.
0.
8791. 0.
0.0
0.0
100.0 0.0
0. d.
17582. 0.
0.0
6.6 100.0
0.0
0.9
2.7 56.6
2.3
1.4
4.4 90.6
3.7
1.7
5.4 113.2
4.6
1.4 4.3
90.6 3.7
TOTAL
8791 . 100.0
17582. 100.0
42. 100.0
124.9 100.0
xxxx YIELDS K**x
XCOKt NORMAL PREMIUM NORMAL S RECARB HIGH SULFUR
coke burned
TONS TONS TONS TONS TONS
0. o.
0. 6593.
2198.
0.0 0.0 0.0 75.0
25.0
6. 0.
0. 13185.
4397 .
0.0 0.0 0.0 75.0
25.0
1.6 0.7
2.2 42.5
15.3
2.9 1.1 3.5 68.1
24.5
3.7
1.3 4.3 85.0
30.6
2.9
1.1 3.5 68.1 24.5
LOSS TOTAL
0. 8791.
0.0 100.0
0. 17532.
0.0 100.0
0.0 0.0
TT7S 100.0
0.0 0.0 124.9100.0
**** UNIT 96 - NO. 2 CALCINER HAS BEEN ON STREAM 28.5 DAYS IN DECEMBER AND 309.67 DAYS TO DATE THIS YEAR MMM*
STREAM
..............DECEMBER........................................................
YEAR TO DATE...........
VOLUME
WEIGHT
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
GRN X COKE
TONS
GRN NORM PREMIUM TONS
GRN LS RECARB
TONS
Gf?N NORM RECARB" TONS
GRN IK S RECARB TONS
GRN INTR PREMIUM TONS
GRN LCM ANODE
TONS
----------- CC"35iT SOFT WAX'"
3557 . 0.
5697.
55.
0.
5442. 2409 .
0.
38.6
0.0 25.7
0,2 0.0 24.6 10.9 0.6
TOTAL
iA --------------- --------------------
***#"Yields ****
22160. 100.0
X COKE
TONS
6888
LS RECARB
TONS
4586
normal s recarb "ToNs
------------
NORMAL PREMIUM TONS
o.
' IK S RECARB
TONS
0.
IfJTR PREMIUM
TONS
4381 .
---------- LTR" A?!uL)E---------------"TORS------- ------- 1956.
COKE BURNED
TONS
4304.
COKE FINES
TONS
0.
`
31.1 20.7
6.2 0.0 0.0 19.8
6.6 19.4
0.0
17114.
0.
11394. 110.
0.
10884. 4818.
0.
44320.
38.6 0.0
25.7 0.2 0.0
24.6 10.9
0.6
100.0
72.6 18.0 25.9
8.7 15.8 25.3 41.7
1.6
210.5
34.5 9.0
12.3 4.1 7.5
12.0 19.8
6.7
100.0
13777. 31.1
57.5
9172. 20.7
20.9
--------- M~------ 575------ -------- 775
o. 0.0
16.2
0. 0.0
11.7
8762. 19.8
20.2
3912.
6.6
3379
8609. 19.4
38.6
0. 0.0
2.5
27.3 9.9 373 7.7 5.5 9.6
16.1 18.3
1.2
145.1 37.7 51.9 17.4 31.6 50.7 83.5 6.4
418.3
34.7 9.0
12.4 4.2 7.5
12.1 20.0
6.1
1Q0.0
115.0
41.8
15.0 32.4
23.3 40.4 6 7.8 77.4
5.1
27.5 10.0
3.6
7.7 5.6 9.7
16.2 16.5
1.2
000005978
sal 000005979
LOSS TOTAL
1. 22160.
0.0 100.0
0. 0.0 44320. 100.0
1.5 0.7 210.5 100.0
0.2 0.0 410.3 100.0
0516 10.
01/09/89
CONOCO INC.-LAKE CHARLES ..iFINERY
HE05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 42
*X*X UNIT 27 - PT ARTHUR CALCIN HAS BEEN ON STREAM 14.5 DAYS IN DECEMBER At'ID 88.49 DAYS TO DATE THIS YEAR ***#
STREAM XXXX CHARGES *XXX
DECEMBER
VOLU ME
WF1'GUT
BBLS
PCT
MLBS
PCT
TO
VOLUME.
. WEIGHT
MBBLS PCT
MMLBS
PCT
GRN LCH ANODE URN HI S FUEL
TONS TUNS
TOTAL
**** YIELDS XXXX
6034 .
10128.
16162.
37.3 62.7
100 . 0
12068. 20256.
32324.
37.3 62.7
100.0
8.0 145,4
153.3
5.2 94.8
100.0
15.9 290.3
306.7
5.2 94.8
100.0
LCH ANODE HIGH SULFUR
CUKE BURNED
TONS TONS TONS
LOSS
4167 . 7685. 4312.
0.
25.8 47.5 26.7
0.0
8333. 15365.
8623.
2.
25. B 47.5 26.7
0.0
5.6 106.5
41.2
0.0
3.6 69.5 26.9
0.0
11.1 213.1
82.4
0.0
3.6 69.5 26.9
0.0
TOTAL 16162. 100.0
32324. 100.0
153.3 100.0
**** UNIT 79 - HO. 2 COKER
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER
306.7 100.0 AND 352.33 DAYS TO DATE THIS YEAR *XXX
STREAM **** CHARGES XXX#
DECEMBER
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
VOLUME MBBLS PCT
WEIGHT
MMLBS
PCT
#6 CRACKED GASO
0.
B/D SLOP OIL
6822.
. . _8ICH-.SPONGE..Oil______________ -52577.
, SEAL OIL FLUSH
74867.
1 CHG FM STGE
1229640.
0.0
0.5 3.8
5.5 90.2
0. 2499. 16116.
23747. 449763.
0.0
0.5 3.3
4.8 91 .4
34.8
43.4 527.0
661.1 13826.9
0.2
0.3 3.5
4.4 91.6
10.6 15.9 162.7
211.6 5077.6
0.2 0.3 s.n
3.9 92.7
_________TOTAL 1363706. **** YIELDS XXXX
IQJL..CL ,, 492126. --18 0-^0--,15023.. 2..-100.0
5478.3 -100.0-
COKER GAS "Coker-gasolinE
LT COKER GAS OIL
HV COKER GAS OIL LEAH SPG OIL GR LCH ANODE
GRN W. S RECARB
GRN HI S FUEL
ELB
TONS TONS TONS
227409.
197263. 419046, 211934.
44778.
2908 . 0.
74642.
16.7
14.5 30.7
15.5 3.3
0.2 0.0 5.5
53757. 51170.
128945.
72004. 13802.
5816.
0. 149285.
10.9
10.4 26.2 14.6
2.8 1.2 0.0 30.3
2741,3 2409.6 4358.3
2439.3 391.3 31.6
6.2 782.1
18.2
16.0 28.9 16.2
2.6 0.2 0.0 5.2
657.5
631.7 1346.1
830.0 120.8
63.3 12.3 1564.1
12.0
11.5 24.6 15.2
2.2 1.2 0.2 28.6
0 0 0 0 5 9 80
LOSS 185726.
13.6
17348.
3.5
1933.6 12.8
252.5
4.6
TOTAL 1363706. 100.0 492126. 100.0 15093.2 100.0
5478.3 100.0
0516
' 1
l, /
10:25 Qi/09/89
CONOCO INC,-LAKE CHARLES REFINERY
HE05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE A3
**** UNIT 75 - GAS_REC PLANT
HAS BEEN ONSTREAM 31.0 d'AYSTn DECEMBER AND 352.A6 DAYS TO DATE THIS YEAR X***
STREAM xx*x CHARGES ****
DECEMBER .............................................YEAR TO DATE..............
VOLUME_______________ WEIGHT_______________ VOLUME_______________ WEIGHT.
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
MISC LT ENDS
FI B
COKER-TCU GASES ELB
CRYO P/B TO GRP
#3 DEPROP OH LIQ
#6 HDS GASOLINE
THERMAL GASOLINE
COKER GASOLINE
M2 CK LN SPG OIL
39299. 29A7A8.
A9036. 0.
0. 62651. 20739A . AA77B.
5.6 A2.2
7.0 0.0
0,0. . 9.0 29.7 6.A
8870. 69569.
9515. 0.
0. 157A2.
53992. 13802.
5.2 AO.6
5.5 0.0
-0.0 -- 9.2 31.5 8.0
690.8. 3A76.7
A78.B 5.0
10.5 A7A.A 2579.7
391.3
8.6
A2.8
5.9 0.1 0.1 5.8 31.8 A.8
171.0 831.7
9A.2 0.9 3.2
122.3 676.6 120.8
-8.5______________________________________________ A1.2
A.7 0.0 07
6.1 33.5
6.0
TOTAL 697906. 100.0 171511. 100.0
8115.1 100.0
2020.7 100.0
x**x YIELDS ****
ABS.TAIL GAS
FOE
PROPANE PROPYLEN
BUTANE BUTYLENE
GRP GASOLINE
PP TO FUEL
FOE
SPONGE OIL
H2S
FOE
15A883. 98298. 99A39.
35AA7A.
383. 52377.
1A986.
22.2 1A.1 1A.2 50.8
0.1 7.5 2.1
A2A3A. 17638. 20262. 90175 -
11A.
16116. 13265.
2A.7 10.3 11.8 5?.6
0.1
9.A 7.7
1751.7 10A9.1
818.1 ._Aooa^?_
l.A 527.0
150.2
21.6
A80.0
12.9
187.A
10.1
167.0
A9.A _-- 1034.0
0.0 0. A
6.5 162.7
1.9 133.0
23.8 9.3 8.3
51.2_______________________________________________
0.0
8.1
6.6
LOSS -7693A. -11.0 -28A9A. -16.6
-191.1 -2.A
-1A3.9 -7.1
TOTAL 697906. 100.0 171511. 100.0
8115.1 100.0
2020.7 100.0
co
r_
o
o
o o a cr >o
03
0516
10: 0j./09/89
CONOCO INCLAKE CHARLES .FINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 44
**** UNIT 7A - NO. 6 HDS
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 3A7.89 DAYS TO DATE THIS YEAR xxxx
STREAM xxxx CHARGES xxxx
____ VOLUME
BBLS
PCT
WEIGHT_________
VOLUME_
MLBS
PCT
MBBLS PCT
WEIGHT_____________________________________________
MMLBS
PCT
1 #7 & #8 STROVHD
RECYCLE H2
FOE
. CRACKED DISTILIA
49684. 75751 . 618798.
6.7 10.2 83.1
16008. 12777. 19A07A.
7.2 5.7 87.1
473.3 753.6
6962.5
5.8 9.2 85.0
TOTAL _2.44 23.3-. --1QO.O . _222fl&,- 1PQ.0,_____ 8189.3 _UQ l.Q.
**** YIELDS X#*X
152.1 118.5 219A.5
6.2 A.8 89.0
2A6S.1 iQiLH_______________________________________________
SEP H2 TO HPU
FOE
HYDROGEN" SULFIDE FOE
STRIPPER OH GAS ELB
STRIPPER REFLUX
t- #6 HDS GASOLINF
DES DISTILLATE
66669.
2903. 23033.
78AA . 80776, 57A1G8.
9,0 0.A
3.1
1. 1 10.9
77.2
11833.
2569. 6368. 2379. 2AA97.
176203.
5.3
1.2 2.9 1.1
11.0 79.1
673.8
21.7 160.A
93.1
916.0 668A.0
B. 2
0.3 2.2 1.1 11.2 81.6
111.2 19.2 52.8
27 .A 268.3 2067.7
A. 5 0.6
2.1
1.1 10.9 83.9
LOSS TOTAL
-11180. 7AA233.
-1.5 100.0
-989. 222859.
-0, A 100.0
-379.7 8189.3
-A.6 100.0
-81.5 2A65.1
-3.3 100.0
*#** UNIT 8A - NO. B HDS
STREAM **** CHARGES XXXX
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 350.00 DAYS TO DATE THIS YEAR XXXX
DECEMBER --
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
........ - YEAR TO DATE ---
VOLUME
WEIGHT
MBBLS PCT
MMLBS
PCT
PURCHASED SLURRY KOCH SLURRY L CH St URRY
SOHIO SLURRY CHAMPLIN SLURRY PYRO. TAR
GAS OIL FR T-398 LT CYC 01L-T023
RECYCLE H2 REG COK GAS OIL PREM COK GAS OIL
FOE
A2AA9.
3121. 1985A8. 107225.
0. 0. 0. 0. 9566A.
0. 0.
9.5 0.7 AA.A
2A.0 0.0
0.0 0.0 0.0
21.A 0.0 0.0
152A7. 1131.
72658. 39579.
0.
0. 0. 0.
1603A. 0. 0.
10.5 0.8
50.2 27. A
0.0
0.0 0.0 0.0
11.1 0.0 0.0
129.0 138.0
1502.2 961.9
231.2 276.9
27.3 71.1
1063.9 75.6 17.2
2.9 3.1 33.A 21 .A
5.1 6.2 0.6
1.6 23.7
1.7
0 .A
A7 . 0
51.3 557.A
358.1 86.1
105.2 9.1
2TT9
166.A 25.8 6.5
3.3 3.6 ^8.8________________________________________________ 2A.9 6.0 7.3 0.6 1.6
11.6 1 .6 0.5
xxxx YIELDS
xxxx
TOTAL
AA7007.
100.0
1AA6A8. 100.0
AA9A.3 100.0
1A35.8 100.0
NO. 8 SEP GAS .NO. 8 STRIP GVHD
NO.8 DES, SLURRY NO.8 DES. GAS 01 HYDROGEN SULFIDE
FOE FOE
toss
8986A. 13068. 3A388A.
0. 833.
-642 ,
20.1
2.9 76.9
0.0 0.2
15520. A222.
121986. 0.
737 .
-0.1 ........ 2m,.
10.7 2.9
8A.3
0.0
0.5
968.5 127.6 3396.5 126! 6
7.0
1.5 _ _!!_1 3 1 _._9_
21.5 2.8
75.6 2.8 0.2
-2,9.
158.1 Ai.O
1213.9 A 2.7 6.2
-26.2
11.0 2.9
8A.5
3.6
0 .A
"1,8________________________________________________
SAt- 000005982
li (I If
H
I
f
I I
l f
I
i
I
r
i
I
SAL 000005983
*001 0*St>t 0*001 '* 6 * b 0*001 - 8 m b T 0*001 'lO O lM 1V101
0516 10 j 2L Jl/09/89
CONOCO INC.-LAKE CHARLES Ri_ iNERV
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 45
**** UNIT 90 - NO. 7 HDS
HAS BEEN CN STREAM 26.6 DAYS IN DECEMBER AND 326.42 DAYS TO DATE THIS YEAR **XX
STREAM XXXX CHARGES XXXX
DECEMBER
. VOLUME
HF1:ght
OBIS
PCT
MLBS
PCT
_ VOLUME....... MBBLS PCT
. WEIGHT_____________________________________________________
1TMLBS
PCT
SEAL OIL FLUSH FTTTTJ H2 SYS 1 Ed FOE It 6 HDS STP REFLX . - LL'GO HVGO "Reg HCbO
3 CTU GAS OIL i CHG FM STORAGE
32883. 190197 .
7899 . 135C10. 250577. 191116. 118998.
313322.
2.9 12.9
0.7 11.8 21.8 12.3
10.3 27.3
10990. 25286.
2379. 93071. 82199. 97897. 36787 .
103712.
3.0 7.2 0.7 12.2 23.9 13.6
10.5 29.5
269.5 1713.5
93.1 135.8 9399.7
1151.9 126.9
2617.0
2.5
16.3 0.9 1.3
41 . 9
11.0 1.2
24.9
84.7
269.9 27.4 43.1
1449.1
391.9 39.2
869.3
2.7
8.5 0.9 1.4 45.6
12.3 1.2
27.4
xxxx YIELDS xxxx
TOTAL 1197997.
100.0
551670. 100.0
10500.9 100.0
3174.7 100.0
SEP GAS TO HPU FOE STRIP OVHD GAS
DES GAS OIL . HYDROGEN.SULPHID FOE
192967. 36616.
923618. 2219.
12.9 3.2
80.5 0.2
25509. 11706.
299096. 1969.
7.3 3.9
83.9 0.6
1207.5 395.7
8699.9 .34.3
11.5 3.3
J 82.4 0.3
203.5 111.1 2793.2
30.3
6.4 3.5 68.0 1.0
LOSS 93077.
3.8
17521.
5.0
263.6
2.5
36.5
1.2
TOTAL 1197997. 1QQ.Q
35147Qt. 1QQ.0 ..... 1Q5QQ.9 _1Q(L_Q
3174.7 1QQ.0________________________________________________
to
>
o o
o
o
o u 'O
CO
KE05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 46
**** UNIT 89 - HYDROGEN SYSTEM HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 366.00 DAYS TO DATE THIS YEAR x*xx
STREAM **** CHARGES ****
vm IIMF
BBLS
PCT
TOTAL VISTA IMPO
1OTAL JUP IMPORT
HDS SEP H2 NO. 3 CRU HYDROG H2 FRM 1 8 #2 H
FOE FOE
FOE FOE FOE
56532. 38817 . 298999. 50259 . 31800.
11.9 8.1
62.8 10.5
6.7
xkx* yTFI HS xxxx
TOTAL
47 6 4 0 7 .
100.0
RECYCLE H2 LP H2 TO EFS HDS HP H2 TO JJ4 HDS HP H2 TO #2&ttl H REC PURGE TO FUE H2 TO CITIES H2 TO VISTA JUPITER H2-FUEL VISTA H2-FUEL
PSA TG TO FUEL
FOE FOE FOE FOE FOE FOE FOE FOE FOE
FOE
319612, 19094 . 16662. 7928 . 572.
38209.
1. 0.
11106.
13704.
67 .1
4.0 3.5
1 .7
0 .1
8.0 0.0
0.0
2.3
2.9
LOSS 49519.
10.4
TOTAL 476407 . 100.0
WFTGHT
NLBS
PCT
9219. 4109 . 52857. 10111. 5061.
81357.
11.3 5.1
65.0 12.4
6.2
100.0
54096. 2974. 2976. 1010. 96. 6 356. O.
0.
1825. 4182.
7843.
81357.
66.5 3.7 3.7 1.2 0.1 7.8 0.0 0.0 2.2 5.1
9.6
100.0
vm IJMF MBBLS PCT
606.5 . 399.6
2849.B 484.1 485.9
12.6 8.3
59.1
10.0 10.1
4825.9 100.0
3530.9 147.6 190.1 105.6 15.6 576.0 6.6 11.9 164.4 195.2
-117.9
4825.9
73.2 3.1 3.9 2.2 0.3
11.9 0.1 0.2 3.4 4.0
-2.4
100.0
WFTftHT
MMLBS
PCT
105.7 42.2
472.8 90.0 84.4
795.1
13.3 5.3
59.5 11.3 10.6
100.0
554.6 23.0 31.6 12.4 2.5
104.0 0.8 1.3
29.1 43.2
-7.5
795.1
69.8 2.9 4.0 1.6 0.3
13.1 0.1 0.2 3.7 5.4
-0.9
100.0
(/> >
--o oo oo
-- ut o
00 <J\
0516 10:-' 01/09/89
CONOCO INC.-LAKE CHARLES 'FINERY
MEQ5 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PASE 47
**** UNIT 85 - FCC FEED f3REP
HAS BEEN ON STREAM 26.6 DAYS IN DECEMBER ALID 335.47 DAYS TO DATE THIS YEAR *xxx
STREAM X*XX CHARGES *x*X DESUL. GAS OIL
xxxx YIFLDS xxxx
TOTAL
DECEMBER
VOLU ME .___________ ___HJ:ght
BBLS
PCT
MLBS
PCT
951522. 951522.
mo.o 100.0
303500. 303500.
100.0 100.0
TO VOLUME . MBBLS PCT
WEIGHT
MMLBS
PCT
12735.3 12735.3
100.0 100.0
4070.4 4070.4
lon.o
100.0
DIESEL DES GAS OIL SLOP
109902.
847035. 1 490 .
11.6
89.0 0.2
33725. 271517.
422.
11.1
89.5 0.1
1553.0 10636.1
56.0
12.2 83.5
0.4
479.8
3421.1 15.9
11.8 64.0
0.4
LOSS
-6955.
-0.7
-2164.
-0.7
490.1
3.8
153.7
3.8
TOTAL 951522. -10 0.0
303500. . 100.0
12735.3 100,0.
4070.4 100.0
V *x*x UNIT 86 - CDR UNIT
STREAM *xxx CHARGES **XX
HAS BEEN OH STREAM 6.0 DAYS IN DECEMBER AMD 65.001 DAYS TO DATE THIS YEAR #*x*
DECEMBER
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
- YEAR TO DATE------
VOLUME
WEIGHT
MBBLS PCT
MMLBS
PCT
CbR RAFFINATE DECENE DIBAC ETHFR
TITANIUM CL3 VAN LUBE SL
GALS GALS GALS RAIS
LBS GALS
TOTAL
x*xx YIELDS ****
221789. 19860 . 221 . 28. 293 . 49 .
242240.
91.6 8.2 0.1 0.0 0.1 0.0
100.0
1515. 123. 2. 0. 0. 0.
1641.
92.3 7.5 0.1 0.0 0.0 0.0
100.0
4958.2 425.3 10.5 0.6 6.8 1.1
5402.5
TTT 7.9 0.2 0.0 0.1 0.0
100.0
33.9 2.6 0.1 0.0 0.0 0.0
36.6
92.5 7.2 0.2 0.0 0.0 0.0
100.0
DRAG REDUCR 102M GALS
241288.
99.6
DRAG REDUCfTib2S GALS
l/> >
DRAG REDUCER T/R GALS
0 , 0.0
0 . 0.0
r~
LOSS
952.
0.4
o
o o
TOTAL 242240. 100.0
o
o
\Jt
NO
09
o
1641 . 0. 0.
0.
1641.
100.0 0.0 0.0
0.0
100.0
5189.3 22.3
162.4
96.1 0.4 3.0
28.4
0.5
5402.5 100.0
35.3 0.2
1.1
0.1
36.6
96.4 0.4 3.0
0.2
100.0
515 10:25 Cl/09/69
CONOCO INC.`LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 48
~ **** Ulilt 67 - CDR UNIT CROSBY HAS BEEN ON SI REAM 2.0 DAYS IN DECEMBER AND 9.00 DAYS TO DATE THIS YEAR ****
STREAM #** CHARGES X***
DECEMBER
VOLUME
_________ WEIGHT________________ VOLUME_____ ___________ WEIGHT________________________________________________________
BBLS
PCT
MLBS
PCT
MfiBLS PCT
MMLBS
PCT
CDR RAFFINATE
DtCENL DIBAC
ETHER TITANIUM CL3 VaN LUftk'"5C
GALS GAL? GALS
GALS LBS GAL?
55186.
46847 54 . 7. 77 . IT!
91.6
377.
6.1 0.1 0.0
30 .
0. 0.
0.1 ___________ !L_
076
iT.
92.4 7.4 0.1 0.0
O.Q--... 070
244 0_ 20.8 0.2
0.0
0.3 071
91.9 __________L4___ -92-4___________________________________________________
7.8
0.1 7.2
0.1
0.0
0.1
0.0
0.0
0.0
0.1
0.0
0.0
OTO
070
070
TOTAL 60220. 100.0
408. 100.0
265.4 100.0
1.8 100.0
"innnrYTrnj? ***#
DRAG REDUCR 102M GALS LOSS"
60053. 167.
99.7 0.3
408. 0.
100.0 0.0
264.7
6.7
99.8 6.2
TOTAL 60220. 100.0
408. 100.0
265.4 100.0
*** Unit 02 - no. 2 crude unit has BEEN ON STREAM 31.0 DAYS IN DECEMBER
1.8 100.0 6.6 0.6 1.8 100.0
AND 364758, DAYS TO DATE THIS YEAR ****
------------- STUE'SH xxkx CHARGES xxxx
DECEMBER
VOLUME
_________ WEIGHT_________ _____ VOLUME____
BBLS
PCT
MLBS
PCT
MBBLS PCT
WEIGHT
MMLBS
PCT
CONOCO PTPFlTNF TEXACO PIPELINE
DOMESTIC BARGE ALASKAN N/SLPE CABINDA-SWEET CONDENSATE SLOP
696106. 283886. 448375.
0. 0. 0. 62646.
TOTAL 1491013.
46.7 19.0 30.1
0.0 0.0 0.0 4.2
100.0
196004. 79574.
126826. 0. 0. 0.
20393.
430798.
45.5 18.5 29.4
0.0 0.0 0.0 6.6
100.0
6624.7 4251.6 5234.8
26.5 109.8 535.1 555.8
17338.3
38.2 24.5 30.2
0.2 0.6 3.1 3.2
100.0
1874.4
1205.5 1464.1
8.1 32.6 143.7 269.1
_3Zj_4___________________________________________________ 24.0 29.6 0.2
. 0,7____________________________________________________ 2.9 5.4
5017.4 100.0
xxxx YIELDS XXKX
CRUDE/DEFUT GAS
LSR (i'A5DUIt;E
> NAPHTHA
f" KEROSENE
--
o
HEAVY HOD DiESEL"
GAS OIL
o TOPPED CRUDE o SLOP
wi o
CD
-4
ELB
55644. " 134824.
163412. 226239.
72041.
310966.
148149. 348244.
0.
LOSS 31494.
TOTAL 1491013.
3.7
9 . (J
11.0 15.2
4.8 20.9
9.9 23.4
0.0
2.1
100.0
11647. 33961. 43761. 63529. 20693. 91416. 44916. 111272.
0.
9602.
430798.
2.7
7.9
10.2 14.7
4.8 21.2 10.4 25.8
0.0
2.2
100.0
721.0 1106.7 2320.5 2518.9
848.8 372674* 1953.2 3811.1
4.0
4.2
6.4 13.4
14.5 4.9
21.5
11.3 22.0
0.0
333.7
1.9
17338.3 100.0
150.8 277.3 619.3 706.9 243.8 i693.6 593.3 1223.3
1.1
107.9
5017.4
3.0
5.5
12.3 14.1
4.9 2l.B 11.8 24.4
0.0
2.2
100.0
J516 10:2 01/09/89
CONOCO INC.-LAKE CHARLES k 1NERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE A9
**** UNIT 35 - FCC UNIT
H AS DEEM ON STREAM 31.0 DAYS IN DECEMBER " AND 169767, DAYS TO DATE THIS YEAR **x*
STREAM #X*X CHARGES XX*#
DECEMBER
VOLUME
VIE]iGHT
BBLS
PCT
MLBS
PCT
1 U DM 1 C
-
_______ VOLUME.. .
_ WEIGHT
MBBLS PCT
MMLBS
PCT
. _ . ..
CHARGE FROM STGE h. uv'CLT'Dll LT SLOP FM STGE
THERMAL GASOLINE COK'ER GASOLINE wi'U UVLKHEAD LTQ 2 CTU GAS OIL CES GAS OIL MISC. LT. ENDS
1 C lI Wb 1 GAS P2C LIQUIDS
ELB
-on
m
526692. 0.
9611 , 0. 0. u.
197961. 735090.
9190 . 0. 0.
37.1 0.0
0.3 0.0 0.0 0.0
10.9 51.8
0.3
0.0 0.0
166963.
0.
1203. 0. 0. 0.
99859. 235915.
905.
0. 0.
37.2 0.0 0.3 0.0
0.0 0.0 10.0 52.9
0.2
b.o
0.0
5517.9
2.2 70.8
9.7 0.9 2.5 1932.4 7818.6 310.5 1.7 39.6
35.1 o.a
0.5 0.1 0.0 0.0 12.3 99.8 2.0 0.0
0.2
1757.9
0.7 19.7
2.9 0.2 0.6 587.0 2519.3 65.9 6 .5 6.9
35.4
a. o 0.4 o.o 0.0
0.0 11.8 50.8
1.3
0.6 0.1
TOTAL 1918999. 100.0 999925. 100.0 15701.9 100.0
9960.2 100.0
xxx# YIELDS kxxx
H2S
FOE
il- ABS VAIL GAS
FOE
PR0PANE-PR0PLENE
P-P TO FUEL
FOE
'j> BUTANE-BUTYLENE
7 FCC GASOLINE V LT CYCLE OIL ' H CYCLE OIL RECY
7 S! L'RRY SLOP
CC.<E BURNED
TONS
979.
70637. 67291.
0. 198509,
725822. 397832.
0. 126133.
0. 9980 .
0.0 5.0 9.7 0.0 19.n
51.2 28.0
0.0 ft.9
0.0 0.7
929. 22997. 12200.
0. 90383. 187923.
127000. 0.
95969. 0.
18960.
0.1 5.0 2.7 0.0 9.0 9178 28.3 0.0 10.1 0.0 9.2
.... 5.2 759.8
1021.9 1.3
1819.8 8097.6 9385.0
2.2 1341.9
17.1 101.1
0.0 9.8 6.5 0.0 11.6 51.6 27.9 0.0 8.5 0.1 0.6
9.6 239.0
186.7 0.4
369.7 2094!3
1407.3 0.7
488.3 4.4
202.2
0.1 4.8 3.8 0.0 7.5 42.2 28.4 0.0 9.8
0.1 4.1
LOSS -177689, ---12.5
-5376.
-1.2 -1891.1 -11.7
-37.5 -0.0
TOTAL 1918999. 100.0
999925. 100.0
15701.9 100.0
4960.2 100.0
oo >
o oo o
o on
'O ' co
co
UX/ u *
uuhucu lf<U.-lAlSt LHAKLtS KtHNERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 50
**** UNIT 83 - CRYO GAS PLANT HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 322.46 DAYS TO DATE THIS YEAR ***X
STREAM **x* CHARGES #xxx
TO
VOlUME
___________WEIGHT________________ VOLUME_____
DBLS
PCT
MLBS
PCT
MBBLS PCT
WEIGHT
MMLBS
PCT
CRYO FEED GAS
223666 . 100.0
63127. -10 Q-. 0 ---2136.8 100.0
604.0 100.0
TOTAL 223666, 100.0
63127. 100.0
2138.8 100.0
604.0 100.0
YIELDS *xx*
CRYO GAS TO FUEL FOE CRYO GAS TO FLAR FOE CRYO P/B
170487. 0.
49036,
76.2 0.0
21,9
47685.
75.5
1698.6
0 . 0.0
0.7
- 9515. -- 15.1 _ 511.9
79.4 0.0
23.9
474.6 0.2
99.9
78.6 0.0
16.5
LOSS
4143.
1.9
5926.
9.4
-72.3 -3.4
29.3
4.8
.... . _
TOTAL 223666 .___ 100.0
63127. 100.0
-2138.8 100.0
-604.0 100.0
#**# UNIT 41 - CAT POLY UNIT
HAS BEEN ON STREAM 30.4 DAYS IN DECEMBER AND 364.92: DAYS TO DATE THIS YEAR ***#
STREAM **** CHARGES ****
DECEMBER
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
- YEAR TO DATE ---
VOLUME
WEIGHT
MBBLS PCT
MMLBS
PCT
PROP-PROPYLENE
110259. 100.0
19807. 100.0
1663.4 100.0
300.3 100.0
TOTAL 110259 . 100.0
19807. 100.0
1663.4 100.0
300.3 100.0
**** YIELDS *xxk
FROPANE PP TO FUEL BUTANE POLY GASO
FOE
76311. 0.
8480 . 16108.
69.7 n. 0
7.7 14.6
13632. 0.
1533. 4146.
68.8
857.1
_ 0.0____ _____ 0^3_
7.7
203.8
20.9
457.3
51.5
0-0 12.3 27.5
151.9 0.1
36.8 117.6
50.6
-0-0 12.2
39.2
to r-
oo
o
o o
'O CO 'O
LOSS TOTAL
8860 . 110259.
8.0 100.0
496. 19807.
2.5 100.0
144.9 1663.4
8.7 100,0
-6.1 300.3
-2,0. 100.0
I I K 1 IUIBIII
0516 10i25 01/09/89
CONOCO INC.-LAKE CHARLES RtrINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 51
**** UNIT 68 - NP SPLITTER
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 363.12 DAYS TO DATE THIS YEAR xxxx
.....................
DECEMBER ................................................YEAR TO DATE..........................
_______________________________________________ VOLUME________________ WEIGHT________________ VOLUME________________ WEIGHT_______________________________________
STREAM
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
xxxx CHARGES xxxx
N0RM.U__PARAFF1NS______________ 11686 6., 1 QQ . 0_______ ____________ UULJ1______ 1275., 8 1DQ-.Q_______ 356.5 10Q.Q__________________________________
xxxx YIELDS
TOTAL 118866. 100.0
31346. 100.0
1275.8 100.0
336.5 100.0
xxxx_____________________________________________________________________________________________________________________________________ _________p
LT PARAFFINS HVY PARAFFINS
83674, 3A301.
70.A 28.9
21995. 9171.
70.2 29.3
874.8 A09.0
68.6 32.1
230.1 109.2
68.A 32.A
LOSS
891.
0.7
180.
0.6
-7.9 -0.6
-2.8
-0.8
TOTAL 118866. 100.0
313A6. 100.0
1275.0 100.0
336.5 100.0
**** UNIT 50 - LIGHT GASO SPLIT HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER. AND 366.00 DAYS TO DATE THIS YEAR XXXX
STREAM xxxx CHARGES xxxx
....................
DECEMBER ................................................ YEAR TO DATE...........................
VOLUMEWEIGHTVOLUMEWEIGHT_________________________________________________________________________________
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
J_GRP_GASOLIijE^_________ __________ ___________________________ 2JULZJL_____ 5AJ______ AQ08.7____ 56^5______ 1Q3A.0____
n6 HDS GASOLINE
0. 0.0
0. 0.0
19.9
0.3
6.0
0.3
TCU GASOLINE
0. 0.0
0. 0.0
12.2
0.2
3.1
0.2
COKER GASOLINE
0. 0.0
0. 0.0
1.6
0.0
O.A
0.0
tt2/#3..C.TU.LSR___________________ 3Q5A52_____ 46.3_____ 76610. AS.9
3055.3 43.0
758.5 42.1___________________________________
xxxx YIELDS
TOTAL 659926. 100.0 166705. 100.0
7097.7 100.0
1802.1 100.0
xxxx__________________________________________________________________________________________________________________________________________________
PRIMARY TWR GAS ELB PRI TWR GAS FUEL FOE LSR GASOLINE LIGHT CRACKED GA
~ NAPHTHA CRACKED NAPHTHA SLOP fJvHlTTS
LOSS
* TOTAL
601. 1457 . 73294. 166199. 219691. 162943.
0. 0.
30741.
659926.
0.1 0.2 11.9 25.2 33.3 24.7
0.0
0.0
4.7
100.0
164. 408. 18366. 45073. 55737. 44300.
0. 0.
2738.
166785.
0.1 0.2 11,0 27.0 33.4 26.6 0.0 0.0
1.6
100.0
29.9 5.4
,855.5 1511.2 2112.7 2356.4
0.3 1.5
224.8
7097.7
0.4 0.1 12.1 2l .3 29.8 33.2 0.0 0.0
3.2
100.0
6.4 1.5 201.4 409.6 536.8 639.7 0.1 0.3
6.4
1802.1
0.4 0.1 11.2________________________________________________ 52.7 29.8 35.5 0.0 0.0
0.4
100.0
SAL 000005990
CONOCO INC.-LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 52
**** UNIT 57 - NO. 1 HDS
HAS BEEN ON STREAM 28.5 DAYS IN DECEMBER AND 304.06 DAYS TO DATE THIS YEAR ****
STREAM xxx* CHARGES xxxx
DECEMBER ................................................YEAR TO DATE................
VOLUME________________ WEIGHT________________ VOLUME________________ WEIGHT
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
H2 FRM HPU SEP H2 F-M 82CRU CRACKED NAPHTHA It3 CTU KEROSENE
FOE FOE
715a ,______ -Ll9_________ 909.
0 0.0
0.
0 0.0
0.
174188
96.1
49494.
_____1.8 0.0 0.0
98.2
82.7 5.9 2.0
1849.7
-4.-3. 0.3 0.1
95.3
9.7 1.2 0.5 531.6
1.8__________________________________________________ 0.2 0.1
97.9
xxxx YIELDS xxxx
TOTAL
161346 .
100.0
50403. 100.0
1940.3 100.0
543.0 100.0
-----------H2 H4 6 HPO
SOH LIQ TO #4HD$ SOH GAS DES. KEROSENE SLOP
FOE ELB
8267 0
517 168128
0
4.1 0.0 0.3 92.7 0.0
906. 0.
162. 48239.
0.
1.8 0.0 0.3 95.7 0.0
86.6 52.1
6.2 1773.6
6.0
4.5 2.7 0.3 91.4 0.3
4.5
11.4 1.9
508.9
1.7
1.} 2.1 0.4 93.7 0.3
LOSS TOTAL
4434 181346 .
2.4 100.0
1096 . 50403.
2.2 100.0
15.8 1940.3
0.8 100.0
9.6 543.0
1.8 100.0
xxxx UNIT 62 NO. 2 CRU & HDS HAS BEEN ON STREAM 22.3 DAYS IN DECEMBER AND 322. 30 DAYS TO DATE THIS YEAR ****
.....................
DECEMBER ................................................ YEAR TO DATE..........................
VOLUME
WEIGHT
VOLUME
WEIGHT
STREAM
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
CHARGES xxxx________________________________________________________________________________________________________________
NAPHTHA
MOLEX GASOLINE BUTANE-BUTYLENE HPU HYDROGEN #1 HDS SOH LIQ
FOE
TOTAL
xxxx YIELDS xxxx
325783, 27473.
0.
770.
0.
354026,
92.0 7.8 0.0 0.2 0.0
100.0
85494. 7366.
0.
101.
0.
92960.
92.0 7.9 0.0
0.1
0.0
100.0
4526.9 451.2 4.3 22.9 29.6
5034.9
89.9
9ft..01
0.5 0.6
100.0
1206.8 121.0 0.9 2.7 6.5
1337.9
90.2 9.0 0.1 0.2 0.5
100.0
SP H2 ttl #4 HPU LESUl . NSPfHNA EXPT FUEL LASHOR HYDROGEN TO FUEL STAB GAS
5TOTTU REFORMATE
FOE
FOE FOE ELB
LOSS
23533. 5384 . 2049 . 1361. 3953.
42080. 279193.
-4327.
6.6 1.5 0.8 0.4 1.1
l i. 9
78.9
-1 .2
4155. 1469.
625. 241. 779, 6092. 75896.
3702.
4,5 1.6 0.7 0.3 0.8 6.6 81.6
4.0
405.2 246.1
2.8 99.5 76.1 511.0 3853.9
-159.8
8.0 4.9 0.1 2.0 1.5 16.1 76.5
-3.2
76.1 53TT"
0.6 18.6 16.2 92.2 1057.1
12.8
5.7 4.8 0.0 1.4 1.2 6.9 79.0
1.0
TOTAL DECEMBER
354026. 100.0 ENDING VALUES
92960. 100.0
5034.9 100.0
1337.9 100.0
SAL
wmw
m
. <\J O' O' in o o
o
o
< </)
88 ' 6
OMOa 51 JOd3d
0515 10:25 Oi/O9/09
CONOCO INC."LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 53
**** UNIT 15 - THERMAL CRACKER HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 336.55 DAYS TO DATE THIS YEAR XXXX
STREAM xxxx CHARGES xxx*
TO
_______ V-QUIME
___________ WEIGHT_________ ______ VOLUME _
BBLS
PCT
MLBS
PCT
MDBLS PCT
WEIGHT
MMLBS
PCT
i GAS OIL FM STG ! FCC CYCLE OIL KM
354?43. 100.0 -125703. 100.0- _ 3255.0-. .99.0
15? .
0.0
51 . 0.0
31.7
1.0
1164.8 9.1
99.2 0.8
xxxx YIELDS
XxiTx
TOTAL
354400.
100.0
125753. 100.0
3286.7 100.0
1173.9 100.0
'L FRACT GAS-GRP
ELB
FRACT GAS-FUEL FOE VtNV GAS TO FLAfTFOE
W-10 PBC CAS ^ THERMAL GASOLINE J, CYCLE OIL 4 THERMAL 'TAR
SLOP
ELD
33590. 0.
635 . 0.
62651. 15102.
250613. 0.
9.5 o. n
0.2 0.0 17.7
4.3 70.7
0.0
7578. 0.
179. 0.
15742. 4417.
95462. 0.
6.0 0.0 0.1 0.0
12.5 3.5
75.9 0.0
274.0
- 41,2 8.3 7.2
496.3
180.3 2360.3
3.2
8.3 1.3 0.3 0.2 15.1 5.7 71.8 0.1
62.6 11.3
2.3 1.6
127.8 58.9
902.6 1.0
5.3 1.0 0.2 0.1
10.9 5.0
76.9 0.1
_______________________________________ LOSS- -B271.
-2.3 ______ 2375^
1.9_____ -92.2 -2.fi
5.8
0.5
TOTAL 354400. 100.0 125753. 100.0
3286.7 100.0
1173.9 100.0
XXXX UNIT 42 - CASINGHFAD UNIT HAS BEEN ON STREAM 31.0 DAYS _IN____ DECEMBER.__ AND 364.91 DAYS TO DATE THIS YEAR XXXX
SAL 000005993
4 ,
1 l >
'
STREAM XXXX CHARGES XXXX
FIELD PBC REF PBC HO , MISC LT ENDS CAT POLY/ALKY C3 POLY a ALKY C4 #3 REF PP
ELB
TOTAL
**** YIELDS xxxx
PBC VAPORS
DEETH TAIL GAS PROPANE
TGUHANE TO FUEL BUTANE IS33UTANE CH GASOLINE
ELB FOE
FOE
LOSS
TOTAL
VOLUME 5BLS _ --PCT.
29418. 1Q3555-.
44806. 90590.
79767. fl .
.
8.5 29.7
12.9
26.0
22.9 0.0
348136. 100.0
3S1. 9448 . 138019. 1098 . 78033. 3CQ96. 74102.
.8159.
348136.
0.1 2.7 39.6 0.3 22.4 11.2 ?1.3
2.3
100.0
WEIGHT MIBS... PCT
VOLUME --MBBLS _.... PCX _
4973. 15590*..
6922. 28259. 12213.
0,
7.3 22.9
10.2
41.6 18.0
0.0
67956. 100.0
374.0 1160.7
394.5 851.9 770.4
20.8
3572.3
10.5 32.5 11.0 23.8 21.6
0.6
100.0
110. 2733. 24297.
323. 15922.
7650. 19023.
-2110.
_ 67956.
0.2 4.0 35.8 0.5 23.4 11.3 28.0
-3.1
100.0 .
3.0 128.6 1156,1
10.6 677.8 546.6 937.5
112.0
3572.3
0.1 3.6 32.4 0.3 19.0 15.3 26.2
3.1
inn.n
WEIGHT
-MMLBS,.-- PCT
66.5 181 a2.
64.0 265.8 124.4
2,9
705.3
9.4 ?5. B
9.1 37.7 17.6
0.4
100.0
0.9 37.2 20LI
138.7 107.4 238.5
-24.1
705.3
0.1 5.3 20.9 0.4 19.7 15.2 33.8
-3.4
100.0
SAL 000005994
t
0516
25 01/09/89
CONOCO INC."LAKE CHARLES REFINERY
1
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 54
**XX UNIT 43 - ALKYLATION UNIT HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 342.37 DAYS TO DATE THIS YEAR ****
STREAM xxxx CHARGES ****
________ VOLUME- ___________ WEIGHT. .______
VOLUME_____
BBLS
PCT
MLBS
PCT
MBBLS PCT
WEIGHT____ _________ -_______ _
MMLBS
PCT
: B-B FM STORAGE 1C4 F?T"STORAGE FCC P-P PDC VAPORS
ELB
TOTAL
xxxx YIELDS xxxx
289272. 194345.
231 . 3C1 .
484229.
59.7 40.1
0.0 0.1
100.0
58789. 38267.
42.
no.
97207.
60.5 39.4
0.0 0.1
100.0
2584.9 1975.6
162.3 3.0
4725.7
54.7 41.6
3.4 0.1
loo.a
527.0 387.4
29.6 0.9
944.9
55.8 41.0
3.1 0.1
ioo. o
TPROPANE < BUTANE
ISOBUTANE , AtKYLATF.
WET BL DUN-FUEL WET BL DWN-FLARE
FOE FOE
. LOSS
13779. 79590. 66503. 257188.
0. 0.
67169.
2.8 16.4 13.7 S3 . 1
0.0 0.0
13.9
2442. 16182. 13153. 62895.
0. 0.
2.5 16.6 13.5
.. 64.7 0.0 0.0
2535.
2.6
93.6 618.2 648.5 2630.9
10.8 0.3
723.4
2.0 13.1 13.7 55.7
0.2 0.0
15.3
16.6 126.1 127.8 642.6
3.1 0.1
28.6
1.8 13.3 13.5 68.0
0.3 0.0
3.0
TOTAL 484229. 100.0
97207. 100.0
4725.7 100.0
944.9 100.0
.****. UNIT 23_-,&ClIL.ELftHTHAS-BEEN -ON STREAM _3J3._8_DAYS IN---------------------- DECEMBER--ANH 362.52 DAYS TO DATE THIS YEAR *
________________ STREAM xxxx CHARGES xxxx
DECEMBER
VOLUME
WEIGHT
BBLS
PCT
MISS
PCT
- YEAR TO DATE *-
VOLUME
WEIGHT
MRRI S PCT
MMl BS
PCT
AMINE ACID SWS GAS SPENT ACID CALC. 02 8
GAS H20
FOE FOE 100* TONS
TOTAL
xxxx YIELDS xxxx
28 . 0.4
851 . . _ 11 .-5_
5019.
78.4
728.
9.8
7426 . 100.0
1250. 753.
11638. 1457.
15098.
6.3 5.0 77.1 9.6
100.0
1.7 9.6 59.2 8.8
79.4
2.2 12.1 74.6 11.1
100.0
4.0 6.5 118.6 17.6
... 149.0
2.7 5.7 79.8 11.8
100.0
982 SUL ACID
100*
7549. 101,7
15098. 100.0
73.5 92.6
147.0 98.7
LOSS TOTAL
-123. 7426 .
-1.7 100.0
0. 0.0 15098. _IM,0
5.8 79.4
7.4 100.0
1.9 149.0
1.3 100.0
'
i
316 10:25 Cl/09/69
CONOCO INC.-LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 55
xxx* UNIT 91 - SULFUR PLANT
HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 366.00 DAYS TO DATE THIS YEAR xxxx
STREAM xxx* CHARGES xxxx
DECEMBER
-vnLUME:
-WEIGHT
BfiLS
PCT
MLBS
PCT
YEAR TO DATE............ .
VOLUME_____________ WEIGHT
MBBLS PCT
MMLBS
PCT
AMINE ACID GAS FOE TOTAL
xxxx YIELDS xxxx
18433. 18433.
100.0 100.0
16600. 16600.
10Q.Q_____ -133.8
100.0
163.8
100.0 100.0
162.2 162.2
100.0 100.0
FUEL MAKE
SULFUR-TONS CALC. PROC LOSS
FOE
TONS TONS
360. 7790.
____ ?-3,
2.0
42.3 2.6
75. 0.4
15580.
93.9
946. _____U_____
4.7
2.5
75.9 41.3
4.7 ____ ^1-
1.0 151.9
9.4
0.6 93.6
5.8
LOSS
9810.
53.2
0. 0.0
98.5 53.6
0.0
0.0
___________________________________ total ^ xxxx UNIT 22 - NASH PLANT
18433. 100.0
16600. 100.0
183.8 100.0 ______ 162.2 100,0 ______
_
______
HAS; BEEN ON STREAM 28.2 DAYS IN DECEMBER AND 318.25 DAYS TO DATE THIS YEAR xxxx
STREAM xxxx CHARGES xxxx
DECEMBER
VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
- YEAR TO DATE --
VOLUME
WEIGHT
MBBLS PCT
MMLBS
PCT
AMINE ACID GAS FOE
5885. 100.0
4910. 100.0
71.6 100.0
66.4 "16670
TOTAL
5885. 100.0
4910. 100.0
71.6 100.0
60.4 100.0
xxxx YIELDS xxxx
SULFUR AS H2S wPROCESSING LOSS
r
TONS TONS
LOSS
2300. 155.
3430.
39.1 2.6
58.3
4599. 311.
0.
93.7 6.3
0.0
28.1 2.0
41.4
39.3 2.8
57.8
56.3 4.1
0.0
93.3 6.7
0.0
g
TOTAL
5005 , 100.0
4910. 100.0
71.6 100.0
60.4 100.0
0516 10
01/09/89
CONOCO INC.-LAKE CHARLES. .-FINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 56
**** UNIT 05 - REG BLEIIUIN(3
HAS "BEEN" ON STREAM 25.0DAYS IN DECEMBER AND 227.00 DAYS TO DATE THIS YEAR **X*
STREAM **xx CHARGES xx*x
DECEMBER ................................................YEAR TO DATE................
VOLUME________________ WEIGHT________________ VOLUME________________ WEIGHT
BfiLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
1 BUTANE
91666 .
1 ibOBUlAUfc
------------------------------ 0.
; ALKYLATE
131507.
| LSR GASOLINE
25256.
, LIGHT CRACKED GA
103219.
;CASINGHEAD gaso
9044 .
POLY GASOLINE
12362.
: FCC GASOLINE
526308.
MO. 2 REFORMATE
144603.
-------------NO. 3 REFORMATE-------
i657ii;
7.5 A.0 10.7
2.1 8,4
0.7 1.0 42.8 11.8 15.1
18701. 0.
32130. 6767.
28078.
2450.
3069. 135725.
40387. 52314.
5-9 0.0 10.1 2.1 8.8
0.8
1.0 42.5 12.6 16.4
4B0.6 4.0
399.8 90.2
930.0
220.7
230.6 4317.9 ,698.9
1775.7
5.3 0.0 4.4 1.0 10.2 2.4
2.5 47.2
7.6 ITT?
98.3
0.8 97.7 23.9 253.0 59.4"
58.0
1126.2 192.0 496.0
4.1 0.0 4.1 1. 0 10.5
2.5
2.4 46.8 jrg8--.0g
TOTAL 1229676. 100.0 319621. 100.0
9148.5 100.0
2405.4 100.0
*** "YIELDS kkxk
REGULAR GASOLINE
1229670. 100.0 319621. 100.0
9148.5 100.0
2405.4 100.0
LOSS
-2. 0.0
0. 0.0
0.0
0.6
0.0
6.6
TOTAL 1229676. 100,0 319621. 100.0
9148.5 100.0
2405.4 100.0
**** UNit 06 ""Unleaded blend
has been onstream"i^TcfDA^ffl
December AWtT2"24.~&o days to date this year ****
STREAM
**** CHARGES ****
DECEMBER
_ VOLUME
WEIGHT
BBLS
PCT
MLBS
PCT
- YEAR TO DATE
VOLUME
_____ WEIGHT
MBBLS PCT
MMLBS
PCT
BUTANE
1SOBUTAm : ALKYLATE \ LSR GASOLINE
LIGHT CRACKED GA
------- ^TASINGHCTITff/CT-----' POLY GASOLINE
, FCC GASOLINE 1 NO. 2 REFORMATE
----------NO. 3 REFORMATE------
38756. 0.
53248.
1168. 33051.
1106
5664 . 261248. 120201.
20543.
7.2 0.0 10.0
0.2 6.2
0.2 1.1 48.8 22.5 3.0
7907. 0.
13009. 308.
8975.
296.
1397 .
66714. 33928.
57247"
5.7 0.0 9.4
0.2 6.5
0.2
1.0 48.3 24.5
4.1
373.3 2.4
1114.9
36.1 568.9
202.6" 228.8 3855.4 1764.7 133.5
4.5 0.0
13.5 0.4 6.9
2.4 2.8 46.6 21.3 1.6
76.3 0.5
272.3
9.5 154.9
54.6
57.2 1000.3
484.3 36.0
3.6
0.0 12.7
0.4 7.2 2.5 2.7 46.6 22.6 1.7
SAL 0 0 0 0 0 5 9 9 6
TOTAL 534985. 100.0 138258. 100.0
8280.8 100.0
2145.9 100.0
xxx* Yields **x*
- UNLEADED
534985. 100.0 138258. 100.0
8280.9 100.0
2145.9 100.0
LOSS
0 . 0.0
0. 0.0
0.0
0.0
0. 0
0.0
TOTAL 534985. 100.0
138258. 100.0
8280.8 100.0
2145.9 100.0
iu
AU i
111 / u
9
CONOCO INC.-LAKE CHARLES REFINERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 57
**** UNlY 0 7" "SUPER UNL BLEND HAS BEEN ON STREAM 8.0 DAYS IN DECEMBER AND 143.00 DAYS TO DATE THIS YEAR X***
------------------- STREAM **** CHARGES ***X
BBLS
DECEMBER
PCT
MLBS
PCT
MBBLS
YEAR TO DATE
JLLl-------------
PCT
MMLBS
PCT
-
- --------
----- -
BUTANE --------- rSOBUTARE-------------
l ALKYLATE
MTBE , L SR GASOLINE
i Um\ CRACKfcb'GA
CASINGHEAD GASO
POLY GASOLINE
: FCC GASOLINE N(J". ` 2 "REFORMATE NO. 3 REFORMATE
TOTAL
17285. 0.
75459. 0.
90 . 1929 .
37. 233. 9790 .
28911.
09970.
222715.
7.8 0.0 33.9 0.0 0.0 0.6 0.0 0.1
4.4 ITTe 90.9
i no. o
3528.
0. 18969.
0. 10. . 387 .
10. 58. 2952. 7 925.
25919.
6.1
0.0 31.7
0.0
0.0 0.7 0.0 0.1 9.2
ITT5
93.6
58253. 100.0
299.0 2.5
1109.8 25.5 0.9 9.7 2.0 21.0
.292.9 1?35.6 1379.3
--4572.7
6.5 0.1 24.3 0.6 0.0 0.2 0.0 0.5 6.4 51.4 30.1
100.0
61.2 0.5
270.9 6.6 0.2 2.6 0.5 5.2
75,1
396.9 385.8
5.1 0.0 22.4 0.5 0.0
0.2 0.0 0.4
, 6.2 33.0 31.9
-1207.6_ 100.0
xxxx YIELDS ****
SUPER UNLEADED
222715. 100.0
58253. 100.0 ____4572.7_ 100.0
1207.6 100.0
o o
LOSS
0. 0.0
0. 0.0
0.0
0.0
0.0
T0TA1 222715. 100.0
100.0
-4S73.7. - 1QQ 0 ..
-1.00 J_____________________________________________________________________
i/i > o . o o
o
Lft oo
* M J*. W_ . -
m w m
0516
10:;
01/09/89
CONOCO INC.-LAKE CHARLES
IMERY
ME05 - MONTH END AND YEAR TO DATE FINAL UNIT YIELD REPORT
PAGE 58
**** UNIT 97 - AREA 1 FUEL HP HAS BEEN ON STREAM 31.0 DAYS IN DECEMBER AND 366.00 DAYS TO DATE THIS YEAR *XX*
STREAM *#** CHARGES x*x#
VOlUMF
___________ WEIGHT_________ ______ VOLUME_____ ___________WEIGHT______________________________
BBLS
PCT
MLBS
PCT
MBBLS PCT
MMLBS
PCT
CRYO GAS TO FUEL
FCC TAIL GAS GRP TAIL GAS PROPANE VISTA H? TO FIJFI
JUPITER HYDROGEN H2 RICH FUEL MISC FUEL GASES PURCHASED FUFl
FOE
FOE FOE FOE FOE
FOE FOE FOE FOE
170487.
70637. 154883.
1098. 11106.
0.
1933. 11904. 18785.
38.7 16.0 35.1
0.2 2.5 0.0
0.4 2.7 4.3
47685.
22447. 42434.
323 . 1825.
0. 337. 3425. 5128.
38.6 18.2 34.3
0.3 1 .5 0.0
0.3 2.8 4.1
1698.6 754.8
1751.7 10.6
164.4
11.9 115.1 219.0 266.1
34.0 15.1 35.1
0.2 3.3
0.2 2.3 4.4 5.3
474.6 239.0 480.0
3.1 29.1
1.3 21.1 61.9 72,6
34.3 17.3 34.7
0.2 2.1 0.1
1.5 4.5 5.2
XX*X YIFlDS
**X
TOTAL
440913.
100.0
123606. 100.0
4992.2 100.0
1382.8 100.0
CRYO FEED GAS CRYO GAS TO LGS
EXP.FUEL TO VIST FUEL CONSUMED AREA II MAKE-UP
FLARE
FOE FOE FOE FOE FOE
223666. 0.
56677. 109726.
64642. 428.
50.7 0.0
12.9 24.9
14.7
0.1
63127. 0.
15854. 30507.
18005. 120.
51.1 0.0
12.8
24.7 14.6
0.1
2138.8 0.0
772.4
1186.3 814.9
27.8
42.8 0.0
15.5
23.8 16.3
0.6
604.0 0.0
216.3
322.1 220.6
7.7
43.7 0.0
15.6
23.3 16.0
0.6
LOSS -14226.
-3.2
-4008.
-3.2
52.1
1.0
12.0
0.9
TOTAL 440913. 100.0
123606. 100.0
4992.2 100.0
1382.8 100.0
SAL 000005998
_i n
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in O' c mo csi NT to x to oeo ctcoe O' r. CM CM
X co cc CM nJ *m e in r-. pH fs.
X COCOS min mi O' rO O' CM O'
* o -- rn. Nc in cm nc O to PH nT to x into eg to (M pH pH NT pH CD NT
X <T
eg \rin c in to o
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CO c pH CM eg 'T
CM
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=
1-- (-- LU in in X
_j wU
o
PH PH Q Q Oh UJ
UJ JZ<
UJ
PHQ
O' at t-- Z. X Q. xt-xx i- in
X JJXZ>
OS t-- LU
UJ LU PH x X
= <r cni--<
U. X
a UJ X Z
X o CO < 69 -- >ZID
LUUJ0
<
oo Daruj -J Q- m <
>a
-- z o ph o
a to
oa <OUJ XO-X
-to
QZ o x x m m O z <UX J
UJCS t--
>- UJ PH lu x a: ir ZlLliJ < UI jJ C h-- O X <1- --i t- <
ax uKt Jit- uoa< LU UJ r-
~oox *" _J--1PH cunmu:
x 2<X CD CD < X UJ c CD o: u. o
X
< 0. X X PH
a *r X-iph xr ja M Ct to O X
t-- lu n eg ro nt n x x CC PH o PH .
a X 7* PH >- o
C Of Lu O
UJ z
CCQ Jj X
a: O CD Uj 1-- CO lU in > X_l>
CE X -
X tu a
Q_ O O UJ CC <K _l UJ D<OX > X O'
_J o o o xxoa JCZOO '
Lu m x a a hi (x zoxa x in o
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< :k
ir n r* --mitnr^ " ^ ON t ^ --
t-- *
- ~ ** *
**
SAL 000005999
0517 10.
01/09/89
CONOCO INC . -LAKE CHARLES ..EFINERY MEOB * MONTHLY FUEL BALANCE REPORT
62 NO. 2 CRU 8 HDS 74 NO , 6 uns
79 NO. 2 COKER 82 NO . 3 CRU 8 HDS 84 NO . 8 HDS 90 NO . 7 HDS 91" SULFUR PLANT 96 NO . 2 CALCIN5R
MSCF 92388.
5658. 179159 . 226134.
6517 . 11 4fl7 .
19074. 115916.
FUEL GAS FOE
15218. 912.
24463. 30942.
1040.
1059. 3198. 19275.
DECEMBER ..----.................... -----------
XXXXX XX FUEL OIL XX TOTAL
HHV
BBLS
FOE
FOE'S
1049. 0. 0. 15216.
1026. 0 . 0. 912.
870 . 0 . 0. 24463.
871 . 0. 0. 30942.
1024 . 0 . 0. 1048.
1031 . 0 . 0. 1859.
1025. 0 . 0. 3198.
1 0S9 . . 0. 19275.
TOTAL
-1514892. 235360.
909 .
n.
n. 235360.
**** NET FUEL BALANCE XX**
(PROD - CONS)
-101753. -15708.
0. 0. -15708.
PAGE 62
-------............ ---YEAR-_TO _-DATE
XXX
FUEL GAS
XXXXX
XX FUEL
MMSCF
MFOE
HHV
MBBLS
1297.
190.
935.
0.
91 . 14. 972.
n.
2186 .
277 .
807 .
0.
2367.
302.
B13.
o.
73. 11. 979.
0.
125.
19. 984 .
0.
201.
31. 969.
0.
1272.
212.
1061.
0.
OIL *x MFOE 0. 0.
0. 0.
0. 0.
0. 0.
TOTA MFOE'
19 1
27 30
1 17
21
18586. _____ 2713._____ 924 . __________ CL___ ________(L--____ 211
95. 20
0. 0. *
' o o o o
to
Os
o o
SAL 000006001
cEPrsT -NUMBER: A7641-01 JCB NUMBER: JNXXXX TPCO/iCCT CODES
7401 0010 C010 0010 0010 0010 001S 001S 001S 0015 0015 0017 0017 0017 0017 C017 00c 5 0025
0150 OISO 0150 0150 0150 0162 0162 0162 0162
0060 0060 0060 0060 0060 00A.2 3 04 2 0 042
0066
MARKETING TRANSFERS GASOLINE, REGULAR-SALES
-PURCHASED -NET SALES -DELTA TOTAL REGULAR-PPOOUCEO UUIEADEO-SALES -FUPCHASEO -NET SALES -OELTA TOTAL UNLEADED-PROOUCED SUFER UNLEADED-SALES -PURCHASED -NET SALES -DELTA TOTAL SUPER UNLEAOED-FROCUCED GASOLINE COMPONENTS GASOLINE COMPONENTS PRICE AOJ. TOTAL MOTOR FUEL JET 50 FUEL-SALES
-PURCHASED -NET SALES -DELTA TOTAL JET 50 FUEL-PROOUCEO CONOCO LVT OIL-SALES DELTA FROIB MONTH SALES-ADJ TOTAL CONOCO LVT OIL-FFCOUCED TOTAL NO. 1 FUEL OIL DIESEL GRADE 2-SALES -PURCHASED -NET SALES -DELTA TOTAL DIESEL GRADE 2-PRODUCEO NO. 2 FUEL OIL-SALES
-OELTA
TOTAL NO. FUEL OIL-PPOOUCED TOTAL NO. 2 FUEL OIL OISTILLATE COMPONENTS TOTAL DISTILLATE
TOTAL TPANSFEPS TO MAPKETING TOTAL PURCHASES FOR RESALE
BARRELS
1,144,724
1,144,724 79,691
1,224,615 471,914
471,914 56,095
526,007 215,465
215,465 6,515
221,960 77,659
2,052,261 542,399 66,002 474,397 -21,055 453,342 10,276 1,352
11,630 464,972 120,590
120,590 -65,415
35,175 2,192,032
-6,509 2,183,523 2,218,698
160,706 2,644.376 4,696,627
-66,002
LAKE CHARLES. REFINERY
ACCOUNT 7401 - ANALYSIS OF TRANSFERS TO MARKETING
MONTH OF DEC 1988
GALLONS
UNIT PR
AMOUNT
BARRELS
PAGE Y1
RUN DATE: 01/19/69
CUMULATIVE THROUGH DEC 1988
GALLONS
UNIT PR
AMOUNT
48,078,400
48,078,400 3.355,422
51,433,622 19,620,381
19,620,381 2,355,906
22,176,267 9,049.529
9,049,529 273.630
9,323,159 3,261,678
86.194,946 22,760,776 -2,656.084 19,924,692
-884,310 19,040,362
431,667 56,764
486,471 19,526,653
5,064,797
5.064,797 -3,587,430
1,477,367 92,065,341
-357,3/6 91,707,963 93.165,330
6,749,652 119,463,635 205,6S3,761
-2,656,064
44.53
44.53 44.53 44.53 42.95
42.95 42.95 42.95 53.31
53.31 53.31 53.31 42.95
45.01 51.96 51.96 51.96 51.98 51.98 54.33 54.33
54.33 52.04 47.09
47.09 47.09 47.09 47.09 47.09 47.09 47.09 47.09 47.90 46.69 51.96
21,409,311.52
21,409,311.52 1,494,169.42
22,903,480.94 8,512,653.64
6,512,653.64 1,011,861.63 9,524,715.27 4,624,303.91
4,624,303.91 145,672.15
4,970,176.06 1,400,690.70
38,799,262.97 11,641,447.36 -1,464,592.46 10,356,854.90
-459,664.34 9,897,190.56
234,535.55 30,650.75
265,336.30 10,162,576.66
2,365,012.91
2,365,012.91 -1,689,320.79
695,692.12 43,3S3,569.06
-166,269.30 43,165,279.76 43,680,971.90
3,178,411.13 57,221,959.69 96,021,222.66 -1,464,592.46
9,049,633
9,049,633 137,356
9,167,169 8,042,357
8,042,357 16,940
6,061,297 4,495,099
4,495,099 -54,744
4,440,355 315,143
22,003,984 5,531,460 -776,126 4,755,332 -16,866 4,736,444 102,300 -873
101,427 4,639,671 1,360,308
1,360,308 21,662
1,402,190 20,642,059
-2,391 20,639,666 22,241,655
141,919 27,223,648 49,227,632
-776,126
380,092,966
360,092,966 5,766,952
365,661,920 337,778,996
337,776,996 795,460
336,574,476 168,794,157
168,794,157 -2,299,246
166,494,909 13,236,006
924,167,311 232,321,313 -32,597,376 199,723,937
-709,296 199,014,641
4,296,596 -36,666
4,259,930 203,274,571
57,972,943
57,972,943 919,044
56,691,967 675.366,493
-100,422 675,266,071 934,156,056
5,960,598 1,143,393.227 2,067,560,536
-32,597,376
46.41
46.41 50.10 48.44 46.91
46.91 17.24 46.04 54.53
54.53 46.58 54.62 43.55
49.03 45.97 46.15 45.94 70.30 45.65 46.35 39.64
46.42 45.91 42.50
42.50 67.97 42.90 42.62 45.35 42.62 42.63 49.13 43.25 45.63 46.15
164,014,473.49
184,014,473.49 2,690,506.4$
186,904,979.94 158,460,313.77
158,460,313.77 137,105.13
156,597,416.90 102,942,930.51
102,942,930.51 1,070,956.54
101,871,971.97 5,763,914.77
453,136.265.56 106,796.566.49 -15,043.502.73
91,755,063.76 -496,617.00
91,256,446.76 2,077,334.26 -14,534.39
2,062,799.69 93,319,246.65 24,639,739.36
24,639,739.36 624,642.00
25,264,361.38 373,044,460.66
-45,545.74 372,996,915.12 393,263,296.50
2,926,206.30 494.510,749.45 947,649,035.03 -15,043,502.73
REPORT -NUMBER: 47641*01 JOB IfJt^ER: JNXXXX PPDD/ACCT COOES
74 02 0056 CC62 0100 0109 0160 0102 6542 054 J 0544 0545 0546 0548 3549 0550 6551 6552 3565 esr>o 9920 6910 0911 6-321 3922 39 JO 3 9 J1 6932 736 6940 9950 0951 3971
6997 3992 e99J 3996 3996
006S 0116
0065 6539
'
PEFIN1NS TRANSFERS CIT-CCN FEEOSTOCK LT. CYCLE GAS OIL NCOMAL PARAFFIN FEEDSTOCK NAPHTHA REFORMING NAPHTHA REFC=MATE INTP CCKER GAS OIL LSP COKER GAS OIL HEAVY PREMIUM COKE GAS OIL NO. 1 HEAVY COKER GAS OIL RESIDUUM HYDROGEN TO CITGO nOLEX RAFFINATE TO CDR REFINERY P-P`S 1 PROPANE ) REFINERY P-P'S (PROPRTLENE) PrPOLYSIS TAR SLURRY OIL VACUUM RESIDUAL BASE PREMIUM COKE* X COKE* LOW SULFUR PECAPBCRIZEP* INTERMEDIATE PREMIUM* NO=MAL PREMIUM GRAPHITE* NORMAL RECAREORIZED COKE* \V. SULFUR RECAP0ORIZER* ANODE COKE LC* HIGH SULFUR FUEL* GREEN ANCOE COKE* GREEN HIGH SULFUR FUEL* C0VE FINESGREEN X CCV CCKE PRICE ADJUSTMENT SULFUR* SULFUR AS H2S* SULFURIC ACI0-93X* SULFURIC ACID*96/i* SULFUPIC ACIO-96X* TOTAL MISCELLANEOUS TRANSFERS DIESEL LT. S. P. GASOLINE TOTAL LIGHT BLENO FEEDSTOCK OIESEl GAS OIL TOTAL HEAVY BLEND FEEOSTOCK TRANSFERS TO CHOCOLATE BAYOU TOTAL PEFINING TRANSFERS GALLONS COLUMN IS TONS t UNIT
COLUMN IS CENTS PER TON. GALLONS COLUMN IS POUNDS.
BARRELS
265,103 366
214,007
15,993 56,211
225 36,209
6,906 1,539 40,344
650
24,204 755
25,669 7.107 676
13,931 52 ,436
457 2,726
21,525 6.645
3.516 800,626
143.472 143.472
143,472 944,096
LAKE CHARLES REFINERY
ACCOUNT 7402 - ANALYSIS OF TRANSFERS TO MARKETING
MONTH OF DEC 1988
GALLONS
UNIT PR
AMOUNT
BAPRELS
PAGE Y2
RUN OATE: 01/19/89
CUMULATIVE THROUGH DEC 1988
GALLONS
UNIT PR
AMOUNT
11,134,326 15,467
9,021,894
40.70 53.21 54.11
671.706 2,360,656
9,449 1,604,778
290,123 64,650
1,6 94,44 7 27,300
36.29 36.16
33.68 42.87 53.39 16.76 52.55 14.29
5,030 157
5,330 1,477
162
36,499.28 34,501.54 24,701.14 16,230.32 14,030.76
2,895 10,697
6,012.25 7,994.77
95 2,986.63 567 4,999.11
7,233 2,300
7,558.74 3,899.99
4,531,670.66 8,229.99
4,681,746.84
243.762.11 853,685.53
3,162.42 687,968.33 154,896.67
10,646.27 690,431.90
3,901.17
1,936,513.78 54,167.42
1,328,921.33 239,721.63 25,535.98
231,954.64 871,190.09
2,639.20 28,344.95
546,723.66 89,699.77
1,311,932 6,726
2,326,556
116,351
194,690 76,646
642,676
565 576,028 127,510
56,315 220,4S4
756 10,389 263,852
9,913 252,736
79,629 92,650 101,264 139.379 60,168 182.173 671,909
3,150,307 13,392 2,204
225,605 63,775
55,101,144 282,512
97,715,352
4,886,721
44.38 43.33 46.30
36.61
6,176,970 3,219,150 26,992,406
32.99 34.26 32.60
23,749 24,193,176
5,355,434
2,365,241 9,259,052
31,743 436,344 11,061,799
2,060 52,522 16,546 19,254 21,044 26.965 12,508 37,656 139,632
33.66 41.52 45.63 16.65 51.51 13.95 21.41
26.22 19,721.65 37,987.51 30,643.56 24,551.62 26,111.33 13,326.74 10,443.25
9,743.60 6,374.11
654,676 2,763 456
2,245.28 5,393.92 30,029.47
75,606 26,150
7,565.93 4,253.31
24,454,129.53 122,423.76
45,244,172.68
1,866,762.46
2,697,853.68 1,102.764.09 6,654,633.20
7,996.66 10,044,664.16
2,443,836.10 393,740.73
4,769,366.15 4,429.44
93,421.25 2,905,513.34
406,270.14 19,951,797.74
5,103,992.66 4,727,168.32 5,915,746.66 3,660,668.96 1,306,241.15 3,688,731.05 11,62,932.72
14,699.347.93 150,112.65 137,534.97
5,735,576.70 1,197,304.35
1,133 26,932,342
6,025.838 6,025,833
1,350.00 65.50
34.62 34.82
6,025,638 32,958,160
34.82 59.69
15,295.50 17,641,232.06
2,098,196.79 2,090,196.79
2,098,196.79 19,739,428.65
33,503 11,030,073
91,555 1,516.212 1,607,767
49,946 49,946 1,657,713 12,687,766
10,797 250,223,858
3,845,293 63,680.900 67,526,193
2,097,721 2,097,721 69,623,914 319,847,772
1,350.00 73.43 41.24 36.76 37.01
19.53 39.53 37.09 65.52
145,759.50 163,745,141.52
1,565,798.63 23,406,151.15 24,991,949.98
829,229.11 629,229.11 25,821,179.09 209,566,320.61
SAL 0 0 0 0 0 6 0 0 2
FOOTNOTES FOR DEC 1968 * *
7402 7404 7402
TRANSFERS REFINING TRANSFERS TO SATELLITE INTRANSIT SALES, INC/DEC MISC LOSS (OTHER) TOTAL REFINING TRANSFERS
943,760
650 -312 944,098
19,624,642.86
9,916.79 104,869.20 19,739,428.85
1/1
*
Oo
o
oo
cr o o o*
Lie
PEPOP7-KUM9EP: A7641-C1 JOB MUMCEP: JMXXXX f'POO/ACCT COOES
7hOJ
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T^OS 6CA3 652 5274 7^0 7 0111 7<0 9
PEF INERT CONSUMPTION
FUEL GAS CONSUMED FUEL OIL CONSUMEO
PROPANE CONSUMEO 90/ SULFURIC ACIO* TOTAL PEFINERT CONSUMPTION
INTEPPEFINERT TRANSFERS CIT-CCN ACJUSTMENT TOTAL INTEPPEFINERT TRANSFERS TRANSFERS TO NGP BUTANE LPS PROPANE ISCQUTANE CRTO GAS TO NGP TOTAL TRANSFEPS TO NGP TRANSFERS TO OTHER DEPARTMENTS NAPHTHA CUTTER STOCK-COT TOTAL TRANSFEPS TO OTHER DEPTS. MISCELLANEOUS REVENUE MISCELLANEOUS REVENUE MISCELLANEOUS PEVEfflJE-VISTA \ LC TOTAL MISCELLANEOUS REVENUE
BAPRELS
153,963 1.098 96
155,157
108,368 2,899
111.217 10.356 10,356
56,676 56,676
LAKE CHARLES REFINERT
NISC. TRANSFERS AND CONSUMPTION BASEO ON PRODUCTION
MONTH OF DEC 1968
GALLONS
UNIT PR
AMOUNT
BARRELS
PAGE Y3
RUN DATE: 01/19/69
CUMULATIVE THROUGH DEC 1988
GALLONS
UNIT PR
AMOUNT
6,966,996
96,116 31
6.512,593
36.69
36.69 3,885.55
36.71
9,551,956
119,658 9,671,119
939,998 939,998
2,380,392 2,380,392
20.97
28.86 21.17
32.15 32.15
90.01 99.90
2,372,539.09
16,919.96 1,209.52
2,390,663.52
-361,977.78 -361,977.78
959,990.32
34,533.30 988,973.62
139,835.78 139,835.78
235,363.90 952,394.84 1,187,758.74
1,971,691
10,636 1,136
1.983,463
3,693 1,236,399
2,849 1,242,941
171,566 1,160,807 1,160,807
777,827 777,627
82,811,022
446,712 366
83,258.100
30.30
32.79 3,885.55
30.33
155,106 51,928.758
119,658 52,203.522
7,205,754 48.753.910 48.753.910
32.668.734 32.668.734
30.33 22.09
28.86 22.13 33.15 35.26 35.26
30.78 36.67
25,091,157.08
146,489.28 14,221.12
25,251,667.48
-3,886,671.19 -3,866.671.19
97,042.71 11,473,376.04
34,533.30 11,554,9S2.05
2,388,707.45 17,192,193.65 17,192,193.65
1,924,965.58 10,054,639.43 11,979,625.01
GPAMO TOTAL TRANSFERS
6,179,191
252.616,008
97.55
120,106,405.59
67.080,456 2,604,292,576
46.82 1,219,307,122.64
SAL 00000600^
APPENDIX D MAXIMUM AMOUNT ON-SITE CALCULATIONS
SARA TITLE III, SECTION 313 1988 TOXIC CHEMICAL RELEASE INVENTORY
LAKE CHARLES REFINERY
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00000601^ sM-
Profile
1. SULFUR PROCESSING DIVISION The Profile provides a general look at the Sulfur Processing
Division. The process information given here will be expanded in depth in the individual manual sections. PURPOSE The Sulfur Processing Division is responsible for: 1. The unloading and/or loading of sulfur, fresh or spent acids and caustics, via the loading rack; spent acid, fresh acid and spent .caustic storage and transfers within the tank farm area; and the storage, mixing, and transfers throughout the refinery of various strength caustics. 2. The regeneration of spent acid from the Alkylation Unit to an acceptable grade of sulfuric acid for reuse In the alkylation process, and the processing of waste gas streams with high concentrations of anvnonla (NH^), and hydrogen sulfide (H^S), into a marketable grade of sulfuric acid. 3. The removal of H2$ and NH^ entrained In the sour water received from the various refinery divisions, so the water may be reused within the refinery or leave the refinery as an environmentally safe effluent, via the Reformer Division. 4. The removal of H^, entrained In the propane butanes (PB's) from the No. 3 CTU Division, as well as the removal of H2S entrained In the tailgas from the various refinery divisions prior to Its use as Cryogenic Unit feed and refinery fuel gas. 5. The regeneration of H^S laden rich amine received from contactors throughout the refinery and Vista Chemicals, into a relatively H2S free lean amine, for reuse in the refinery and Vista Chemical
SAL 000006018
Prof)le
2. GENERAL DESCRIPTION LOADING AND TRANSFER (SECTION 1) (See Figure 1)
The loading and transfer section 1$ divided Into three parts: Loading Rack, Tank Farm, and Caustic Mixing and Transfer. Loading Rack 1. Rail Car Loading Rack
The loading rack Is made up of ten rail car loading spots (or stations) and three truck loading spots. The following products may be loaded or unloaded at each spot:
Spot 1 - Unload 50% caustic rail cars and trucks. Load spent caustic (acid oil or sulfides) rail cars and trucks. Spot 2 - Unload 50% caustic rail cars. Load spent caustic (acid oil or sulfides) rail cars. Spot 3 - Load or unload 93%, 96X, 98% sulfuric acid rail cars. Load or unload spent acid rail cars. Spot 4 - Load or unload 93%, 96%, 98% sulfuric acid rail cars. Load or unload spent acid rail cars. Spot 5 - Load 93%, 96X, 98X sulfuric acid rail cars. Spot 6 - Load 93X, 96X, 98% sulfuric acid rail cars. Spot 7 - Load 93%, 96%, 98% sulfuric acid rail cars. Spot 8 - Load 93%, 96%, 98% sulfuric acid rail cars. Located at Spot 8 is a truck loading station at which 93%, 96%, 98% sulfuric acid can be loaded. Spot 9 - Load product sulfur trucks or rail cars. Spot 10 - Load product sulfur trucks or rail cars.
4
SAL 000006019
Profile
to transfer sulfides or acid oils to the loading facilities. The SC/RC Division sends sulfides from the caustic wash tower to T-204
and is gravitated with T-203 and T-205 to provide additional storage. Sulfides from this unit are sent in batch amounts.
Sulfides in T-203, T-204, T-205 can be pumped directly to the loading rack at spots 1 and 2 or to T-1802 with P-231 or P-82. If there would be any hydrocarbons in these tanks they could be pumped to the heavy slop line going to the Pumping and Transfer Oivision. Provisions for truck loading Is also present at these tanks.
The 982 sulfuric acid, also referred to as fresh acid. Is sent to the Alky Unit, No. 2 Reformer and Power House Division, by either pressuring with nitrogen at about 35 pslg or by pumping (P-1805). Fresh acid is stored In two horizontal drums, called bullet tank, D-80 and 0-81. Fresh acid can also be stored. In some Instances In D-78 and D-79, but these bullets are usually used as spent acid storage.
When empty, these bullets are filled from T-1803 with P-1807. P-1807 can also pump fresh acid directly to the Alky Unit.
The fresh acid sent to the Alky Unit in the Thermal Cracking Division Is vital to their operation, and It Is important that the acid flow not be interrupted.
The "used" or spent acid Is pumped back to the storage area from the alky unit to bullet tanks D-79, D-78, D-77, D-76, D-75 and D-74. The spent acid Is sent back at about 89-922 strength.
As spent acid Is pumped back to the storage area, liquid hydrocarbons are sometimes entrained with the spent acid. Since hydrocarbons are lighter than spent acid, they will separate and "float" on top of the spent acid and can be removed. D-74 Is reserved for storage of hydrocarbons.
SAL 000006020
6
Loading and Transfer
SECTION PROCESS EQUIPMENT
Drums
Description
D-74
Alky Spent Acid
D-75
Alky Spent Acid
D-76
Alky Spent Acid
D-77
Alky Spent Acid
D-78
Alky Spent Acid
D-79
Alky Spent Acid
D-80
981 Acid to Alky
D-81 Pumps
Oriver/Innerdriver
981 Acid to Alky Description
R-4
Recipr. steam driven
Caustic Transfer
R-I02
Recipr. steam driven
Caustic Transfer
R-113
Recipr. steam driven
Caustic Transfer
P-1804 M-1804
Alky Spent Acid to Blend Tank
P-1805 M-1805
981 Acid to Alky
P-1806 M-1806
Alky Spent Acid to Blend Tank
P-1807 M-1807
981 Acid Product Loading
P-1808 M-1808
Spare Acid Product Loading
P-1809 M-1809
931 Acid Product Loading
P-1810 M-1810
Hydrocarbon Skim Pump on T-1806
P-1811 P-1801A
M-1811 M-1801A
Spent Acid to Blend Tank ^Acld Oil Loading-Pump --------------- -
P-1801B M-1801B
(^Acid Oil or Sulfide Spare Loading Pump ^
P-1801C M-1801C
Sulfide Loading Pump
P-221
M-267
41 Caustic Transfer to No. 3 CTU Division
P-82
M-265
Sulfide Loading Pump
SAL 0006021
Profi1e
Cracking and Sulfur Processing. Caustic at 252 can also be routed to the SC/RC Division.
T-50A and T-508 can also be used as 252 caustic storage. These drums are used as backup storage after dilution and mixing in T-54, T-55 or T-56' in the event of low 501 caustic inventory.
Caustic at 122 is stored In T-45 to be used by the Alky Unit for their process. T-45 is filled from one of the mix tanks (T-54, T-55 or T-56) where 122 caustic has been prepared.
T-l is used as 42 caustic storage for the No. 3 CTU Division. This 42 caustic Is transferred with pump P-221 to that unit.
252 caustic from the mix tanks and well water, at specific amounts are used to mix 42 caustic. A recirculation line from the discharge of P-221 back to T-l continuously mixes the caustic.
SAL 000006022
8
LouisianaEmergencyResponse Commission
P.O. Box 66614 Baton Rouge, I x>nitana 70S96
(504)926-6113
The enclosed l/wima TierTwo inventory form is the official inventory form for compliance with Louisiana's Right-to-Know law. This Tier Two form is also toe form required by toe i Emergency Response Commission for compliance with Title m of toe Superfund Amendments and Reauthorization Act (SARA). The form has been slightly modified for use in Louisiana in thata line for Parish has been added along with blocks for a Louisiana code number used to aid data management The Louisiana Tier Two inventory form is the only Tier Two form which will satisfy bothcommunity right-to-knowlaws.
It is imperative that, priorto completing toe Tier Twoform. the Rules for Louisiana's Right-toKnow law be read. We have made every effort to ensure that when the form is completed according to the state Rules, it will also satisfy the federal reporting criteria. Because of the volume of Tier Two forms submitted statewide, any TierTwo form notcompleted according to the Rules and the instructions accompanying the Tier Two form will be returned. Compliance with both laws will not be attained until corrections have been made. Please read the Rules and the instructions before attempting to complete the Tier Two form.
Your attention is also directed to Attachment C of the Rules. In this attachment we have addressed some of the most commonly asked questions about compliance with these laws. If, after reading this attachment, toe Rules, and all applicable instructions, you have any questions, you may call (504) 925-6113. Due to the large number of calls we have experienced in the past, and because of the limited personnel available to answer these calls, we ask thatevery attempt be made to thoroughly read the Rules and instructions prior to calling.
SAL 000006023
INSTRUCTIONS
Before attemptingto complete yourTierTwo form, please read the Louisiana Hazardous Materials Information Development, Preparedness and Response Act rulebook. TTien, read these instructions carefully. Print or type all responses.
Failure to comply with the state rules and/or submission of an incomplete or incorrectly completed Tier Two form will result in Its rejection.
WHEN AND WHERE TO SUBMIT THIS FORM
Owners or operators must submit the Tier Two form to the T/amdana Emergency Response Commission, the local emergency planning mmnuttm* of the parish in which the facility is located, and die local fire department haring jursidiction over the facility on March 1 ofevery year.
PENALTIES
Any owner or operatorwho violates any federal reporting requirement or a Louisiana reporting requirement regarding submission of the Tier Two form shall be liable to the United States andfer the State ofInuiniana for civil penalties ofup to $25,000 under both federal and state law for each violation. Each day a violation continues shall coostititute a separate violation.
NOTE
If your responses require more than one page, fill in the page number at the top of the form.
FACILITY IDENTIFICATION
Eater the fuU name ofyour facility and company identifier where appropriate. Do not use working names. The name ofyour facility should match your letterhead.
Cuter`the MI shear
This is the physical location ofyour facility. Davataafrpestofficfr
boass.*ifa street or road address is doc available, enter other appropriate identifiers that describe the physical location
ofyour facility (e^. latitude and longitude, or 'five miles from the intersection of Hwy 94 and La 135 on
unmarked gravel road*)- Indude dty, state, and rip code.
Enter the primary Standard Industrial Classification (SIC) code for your facility. The SIC code may be obtained by calling the OSQA section of the Louisiana Department of Labor at (504) 342-9601.
OWNER/OPERATOR
Enter the owner's or operator's full name, mailing address, and phone number. This is the address to which all correspondence regarding your annual submission will be sent.
1
SAL 0006024
EMERGENCY CONTACT
Enter the name, title, and work phone number ofat least one local person or office who can act as a referal if m w^pnnrBng trt a ehwrrifal /'riAnt at yftr fr^lity. Ifthere it DO Specific
person accountable (e^. facilities winch operate 24 houmadayX fat the title ofthe responsible petty (e^. shift supervisor).
Provide an emergency phone number when such emergency chemical information will be available 24 bouts a day, everyday.
REPORTING PERIOD
Enter the appropriate caiendar year, beginning January land ending December 31. Please remember that you are reporting for the previous calendar year.
CHEMICAL INFORMATION: Description, Hazards, Amounts, and Locations
The mainsectionofthe TiorTwoform requires specific information on amounts and locations of hazardous chemicals, as definedin the OSHA HazardConmmnimtioTW Standard.
* WHAT UNITS SHOULD I USE ? Calculate all amounts as weight in pounds. To convert gas or liquid volume to weight in pounds, multiply by an appropriate density factor. Many material safety data sheets (MSDS) indude this density factor.
CHEMICAL DESCRIPTION
NOTE: ENTER ALL CHEMICALS IN ALPHABETICAL ORDER.
1. Enter the Chemical Abstract Service number (CAS #). CAS numbers for many of the regulated substances
may be found in the state rule booh. MSDS may also provide CAS#. For mixtures, enter the CAS# of the mixture
as s whole if it has been
a mmher distinct from its components. If the mixture has no CAS#, leave this
item blank. Do not enter the CAS# of its component parts.
2. Enter the rh^miral naiw, nnnmnnniiM, or trade name nfeach hziriM mhatanr* Please refer to the State niiebook for a description of how to list trade names ancVbr mixtures. (The question and answer section of the rulebook should provide additional information). Finally, enter the Louisiana code number. Many of the Louisiana code numbers may be found in the state rule book. Ifno code is found, you need do nothing more.
3. Circle ALL applicable descriptors: pure or mixture, and solid, liquid, or gas.
EXAMPLE You have pure chlorine on hand as a liquid anc as a gas. You enter the CAS# for chlorine, write 'chlorine', then circle 'pure* as well as 'liquid' and 'gas'.
2
SAL 000006025
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apjj. -)3loos apuj, pa^ma zoq acp :p3tp pm (arem&oci onrcfiio ct aprasXoocnp aawjoi jsy ^*a) snp itoarap ausoaff cup jojod *37p nooaag apt] m ponrods tojuo tym aompioan pi
parawp *jo wmn aqj SurpyxyiM anr noXjj :SAHX3HS aCIVHX NO HXON V
AVERAGE DAILY AMOUNT
L For each hsTartVws chemical, estimate the avenge weight in pounds that was present at jour facility during the year. To do this, total all daily weights and dvide by the/mimber ofdays the chemical was present on the site. 2. Rod the appropriate range value in TaUeL X Eater this range value as the Avenge Daily Amount
EXAMPLE
The 5,000 gallon shipment ofthe substance you received last year was gradually need up and completely gone in 313 days. The sum of the daily volume levds in the tank, is 929,250 gallons, tty dividing 929,250 by 315 days on-site, you calculate an avenge daily amount of 2,950 gallons. You already know that the density ofthe substance is 7.29 pounds so you multiply 2,950 by 7.29 to get a weight of 21.505.5 pounds. You look at Table land find that the range value 03 corresponds to 21,505.5. You enter 03 as the Average Daily Amount
NUMBER OF DAYS ON - SITE
Enter the number ofdays that the hazardous substance was present on-eitc.
STORAGE CODES AND STORAGE LOCATIONS
List ail non-confidcntial rhermr*} locations in tins column along with storage typesfanditions aw4arrf with cadi location. Enter the appropriate code in the three blocks provided as follows: 1. Look at Table JJL. For each location, find the appropriate storage type(s). Enter the corresponding code in the
first block.
2. Look at Table in. For each storage type find the pressure and temperature conditions. Enter the applicable
pressure code in the second block and the applicable temperature code in the third and final block.
EXAMPLE
The benzene in the main building is kept in a tank inside the building, at ambient pressure and leas than ambient temperature. Table II shows you that the code for a tank inside a building is G Table III shows you that the code for ambient pressure is 1, and the oode for less than ambient temperature is 6.
You enter. C]T[6 TABLES MAY BE POUND ON FOLLOWING PAGE.
4
00000602^
SAL
TABLE n - STORAGE TYPES
CODES
A B C D E F G H I J K L M N 0 P
Q R
Types ofstorage
Above ground tank Below ground tank Tank inside building Steel drum Plastic or non-metaUic drum Can Carboy Silo Fiber drum Bag Box Cylinder Glass bottles or jugs Plastic books or jugs Tote bin Tankwagon Rati car Other
TABLE m - TEMPERATURE AND PRESSURE CONDITIONS
CODES
Stomecoafitkaw
(Frame)
1 Ambient pressure 2 Greaterthanambientpressure 3 Less than ambient pressure
(Tsapsntsre) 4
5 Greaterthanambienttemperature 6 Less than ambient temperature but not
cryogenic
7 Cryogenic conditions
STORAGE LOCATIONS
Provide a brieftfcscriptton ofthe precise location ofthe chemical, ao that emergency responders can locate the area easily (e.g. near west will of warehouse). The street address is not mm acceptable location. Y<xi may Sod it advantageous to provide an optional site plan or site coordinates as explained below.
For each substance, indicate at a minimum the building or lot Atkfitionally, where practical, the room or area may be indicate^. You may respond in narrative form with appropriate site coordinates or abbreviations.
If a chemical is present in more than one building, lot, of area location, continue your responses down the page as needed. If the chemical exists everywhere at the plant ate wirmiltanroiwly, you may report that fee chemical is ubiquitous at the site.
Optional
if you cboose to attach one of the following, check the appropriate Attachments box at
the bottom of the Tier Two form.
a. A site plan with site coordinates indicated for buildings, lots, areas, etc. throughout your facility.
b. A list of site coordinate abbreviations that correspond to buildings, lots, areas, etc. throughout your facility.
5
SAL 00G06028
CONFIDENTIAL LOCATION SHEET
Under Tide Kit Section 324, you may elect to witl^ location Information a spedfte chemical ftom&adosme to the public. If you cfaooae to do sot
a. Enter the word ^confidential in the Non-Owfiritemial Location aectioncf the Tier Two fbim. bw On a separate Tier Two ConfktennalLocatian Information Sheet, enter the name sad CAS# ofeach
chemical for wbidi yon arc beeping the location confidential. c. Enter the appropriate location and storage information, a* described above for nan-confidential locations. d. Attach the Tier Two Confidential Location Information Sheet to the Tier Two form. This separates
confidential location* from other information that will be disclosed to the public.
CERTIFICATION
TittsnMrtbcccmptetedby the owtectot operate or the officially designated wpwwnistiveoftbe owner oroperator. Enter your fUU same and official title. Sign ycatr name and eater the current date.
FEES
Please refer to the section on fees in the state ratebook. Attach the check for the appropriate amount to the Tier Two form and mail tin* form to the Louisiana Emergency Response Commiasion, Office of State Police, Transportation and Environmental Safety Section, P.O. Bor 66614, Baton Rouge, La. 708%.
REMINDER
You are required under federal law to seed copies ofyour submission to the local emergency pluming committee and die local fire department as well aa to the Louisiana Emergency Response Commiwwioa. A listing of all local emergency planning frtmmittws in operation in the state ofI rmfcriana is provided as an attarhmwtt to the state ratebook. No information is available on local fire departments.
6
SAL 000006029
+-----TIER TWO
Emergency k Hazardous Chemical Inventory Specific Infortation By Cheiicai
For Official Use Only
ID : Date Received:
Reporting Period Frot January 1, to Decetber 31, 1988
Facility Identification:
Etergency Contacts:
Nate: CONOCO INC. Address: P.0. BOX-37
OLD SPANISH TRAIL City: WESTLAKE, LA 70669-0000
Nate: Steve Brouillard Title: SAFETY DIRECTOR Phone: (318)491-5224 24 Hr Phone: (318)491-5301
SIC Code: 2911 Dun l Bradstreet #: 80-842-7692
Owner/Operator Intonation:
Nate: Don R. Unruh Address: P.O. Box 37
OLD SPANISH TRAIL City: WESTLAKE, LA 70669-0000 Phone: (318)491-5222
Nate: Doug Frey Title: SAFETY AND HEALTH SUPERVISOR Phone: (318)491-5023 24 Hr Phone: (318)491-5301
+ CONOCO REFINERY, WESTLAKE,LA.
fio
Ho
o
flc
Cheiicai Description
CAS #: N/A
Trade Secret [ I
Chet Nate: 1100-S
LA Code: 8433 [ 3 Pure 1X3 Mixture I 1 Solid [XI Liquid I 3 Eas
CAS *: 64197 Trade Secret I 3
Chet Nate: ACETIC ACID, 6LACIAL
LA Code: 0617 EX] Pure [ 3 Mixture [ 3 Solid m Liquid [ 3 Gas
CAS l: 67641 Trade Secret [ 3
Chet Nate: ACETONE
LA Code: 0629 m Pure [ 3 Mixture t 3 Solid m Liquid C 1 Gas
CAS 1: 74862 Trade Secret E 3
Chet Nate: ACETYLENE
LA Code: 0655 (XT Pure l 3 Mixture [ 3 Solid [ 3 Liquid EXJ Gas
CAS f: N/A
Trade Secret l 3
Chet Nane: ACID GAS/SOUR GAS
LA Code: IXJ Pure l J Mixture ( ] Solid L 1 Liquid EH Gas
Phys, 4
Avq. No. of
Health Max. Daily Days
Hazards Atount Aiount On-Site Code
Storage Codes l Locations *** Non-Confidential ***
Storage Locations
X Fire SROP
X React
X Acute Chron
03
A14 CRYG 00 366
X Fire SROP React
X Acute Chron
03
A14 THERMAL UNIT A14 FCC
01 366 /
X Fire SROP React
X Acute X Chron
01
D14 LAB 01 366
X Fire X SROP
React l Acute
Chron
03
L24 REFINERY WIDE 03 366
X Fire X SROP
React X Acute X Chron
04
R25 ACID PLANT R25 SULPHUR PLANT
84 366
SAL 000006030
'Hr
*
& {Jo
to bio do
A/<9
CONOCO REFINERY, NESTLAKE,LA.
Cheaical Description
CAS t: N/A
Trade Secret t 3
Che* Naie: AERO N-39 CATALYST
LA Code: 8563 [ 3 Pure m Mixture m Solid C 3 Liquid 3 Gas
Phys. &
Avo. No. of
Health Max. Daily Days
Hazards Aaount Aiount On-Site Code
Storage Codes & Locations ** Non-Confidential *** Storage Locations
Fire X SROP
React X Acute X Chron
03
R25 SULPHUR PLANT 03 366
CAS #: 1333842 Trade Secret [ 3
Chea Naae: ALCOA ACTIVATED ALUMINAS
LA Code: 6963 [ 3 Pure 1X3 Mixture [I] Solid [ 3 Liquid [ 3 Gas
CAS 8: 68527275 Trade Secret [ 3
Chea Naae: ALKYLATE
LA Code: m Pure 3 Mixture [ 3 Solid LZ3 Liquid ] Sas
Fire X SROP X React X Acute
Chron
04
I Fire SROP React
X Acute X Chron
06
R25 POWER PLANT R25 LAB R25 SULPHUR PLANT 04 366 R25 82 CRUDE R25 FCC R25 CRYO R25 #3 REFORMER
AM EAST TANK FARM R24 ALKY UNIT
05 366
CAS I: N/A
Trade Secret I 3
Chea Naae: ALPHACHEK 11S1-C
LA Code: 8446 3 Pure X3 Mixture 3 Solid CXI Liquid 1 Gas
Fire SROP React X Acute Chron
04
AM REFINERY HIDE 02 366
CAS #: N/A
Trade Secret 3
Chea Naae: ALPHACHEK 2042 DEGftEASER
LA Code: 7018
3 Pure X3 Mixture 3 Solid m Liquid l 3 Sas
Fire SROP React X Acute Chron
03
DM REFINERY HIDE 00 366
CAS 8: N/A
Trade Secret 3
Chea Naae: ALPHACHEK 2063 DEGREASER
LA Code: 8447
[ 3 Pure 13 Mixture [ 3 Solid LXI Liquid [ 3 Gas
CAS 1: N/A
Trade Secret 3
Chea Naae: ALPHACHEM 2072 DEGREASER
LA Code: { 1 Pure 1X3 Mixture
[ 3 Solid HI Liquid C 3 Gas
Fire SROP React X Acute X Chron
01
X Fire SROP React
X Acute X Chron
01
DM REFINERY HIDE 00 366
DM 43 CRUDE, VACUUM 01 366
CAS #: N/A
Trade Secret 3
Chea Naae: ALPHACHEK 2076 DEGREfiSER
LA Code: 0445 [ 3 Pure Cxi Mixture 3 Solid N Liquid ] Gas
Fire SROP React X Acute X Chron
03
A14 REFINERY WIDE 01 366
SAL 000006031
lio
do
0
CONOCO REFINERY, WESTLAKE,LA.
Cheiiical Description
Phys. L
Avq. No. o4
Health Max. Daily Days
Hazards Arount Aeount On-Site Code
Storage Codes L Locations * Non-Confidential * Storage Locations
CAS l: 10043613 Trade Secret [ ]
Che* Nate: ALUMINUM SULFA"
LA Code: 0770 1X3 Pure [ 3 Mixture I 1 Solid m Liquid l 1 Gas
Fire SROP React X Acute X Chron
03
A14 REFORMER
02 366
CAS 1: N/A
Trade Secret t 1
Che* Naae: AMBERLITE 200, 200C 16/40 RESINS LA Code: 8437
m Pure C 3 Mixture
[X] Solid [ 1 Liquid [ 1 Gas
Fire
SRQP
React X Acute
Chron
02
A25 POWER PLANT 01 366
CAS t: N/A
Trade Secret [ ]
Che* Natoe: AMBERLITE 1R-120 PLUS (HI RESIN LA Cade:
m Pure [ ] Mixture m Solid [ 1 Liquid [ ] 6as
X Fire SROP React
X Acute X Chron
01
A25 POWER PLANT 00 366
CAS #: 7664417 Trade Secret I 1
Chei Nase: AMMONIA
LA Code: 070?
inCXI Pure l 3 Mixture
[ 3 Solid
Liquid t 3 Gas
Fire X SROP
React X Acute
Chron
03
A24 42 CRUDE A24 43 CRUDE, VACUUM
02 366
CAS s: 1336216 Trade Secret I 3
Chea Naae: AMMONIUM HYDROXIDE
LA Code: Itl Pure [ ] Mixture t 3 Solid CX3 Liquid C 3 Gas
Fire SROP
X React X Acute
Chron
02
A14 43 CRUDE, VACUUM 01 366
CAS i: N/A
Trade Secret [ 3
Che* Naae: ANTIOXIDANT NO. 23
LA Code! 0441 I 3 Pure [X] Mixture [ 3 Solid 1X1 Liquid [ 3 Gas
X Fire SROP
React X Acute X Chron
03
A14 PUMPHOUSE 01 366
CAS 1: 7440371 Trade Secret [ 3
Chea Nase: ARGON
LA Code: 0740 1X3 Pure [ 3 Mixture [ } Solid [ 3 Liquid U3 Gas
Fire X SROP
React Acute Chron
03
L24 REFINERY WIDE 03 366
CAS #: N/A
Trade Secret [ 3
Chea Naae: AR1-100L
LA Code: 3502 tX3 Pure [ 3 Mixture [ ] Solid 1X3 Liquid I 3 Gas
Fire X SROP
React X Acute
Chron
02
R25 REFORMER R25 GRP
02 366
SAL 000006032
CONOCO REFINERY, WESTLAKE,LA.
Chetical Description
ft*
< *
Phys. i
No. Of
Health Max.
Days
Hazards Aaount Aaouftt On-Site Code
Storage Codes & Locations *** Nan-Confidential Storage Locations
CAS t: M74M53 Trade Secret [ 1
Che* Naae: ATMOSPHERIC TONER RESID
LA Code: 7151 1X3 Pure C 3 Mixture [ ] Solid I'll Liquid l I Gas
CAS #: 71432 Trade Secret I I
Chea Nate: BENZENE
LA Code: 1030 CI3 Pure [ 1 Mixture [ 3 Solid [X] Liquid [ 3 Sas
I Fi-e X SROP
React X Acute X Chron
05
X Fire SROP React
I Acute X Chron
04
R25 12 CRUDE R25 PREMIUM COKER R25 13 CRUDE, VACUUM 04 366
R25 REFINERY HIDE
04 366
CAS *: N/A
Trade Secret [ 3
Chea Nate: BETZ 204*
LA Code: 8432 E 1 Pure EX3 Mixture E ] Solid CXI Liquid C 1 Gas
X Fire SROP React
I Acute X Chron
03
A14 UTILITIES, DEMINERALIZER, COOLING T 00 366
CAS #: N/A
Trade Secret [ ]
Chea Nate: BETZ 20K-20223
LA Code: 8459 C 1 Pure CX3 Mixture [ 3 Solid CX3 Liquid l 1 Gas
Fire SROP React X Acute X Chron
03
A14 ACID PLANT 01 366
CAS f: N/A
Trade Secret C 3
Chet Naee: BETZ 20K-2022?
LA Cade: I 3 Pure CX3 Mixture C ] Solid CXI Liquid I 3 Gas
CAS i: 1310533 Trade Secret [ 3
Chee Nate: BETZ 20K SERJES
LA Code: C 3 Pure CX3 Mixture [ 3 Solid CX3 Liquid [ 3 Sas
X Fire SROP React
X Acute X Chron
02
X Fire SROP React
X Acute X Chron
03
A14 ACID PLANT 01 366
A14 POWER PLANT 02 366
CAS 8: N/A
Trade Secret t 3
Chea Raise: BETZ 22K-220B0
LA Code: 843E U3 Pure [ } Mixture
[ 3 Solid m Lieuid [ 3 Sas
X Fire SROP React
X Acute Chron
02
AM ACID PLANT 0! 366
CAS 4: N/A
Trade Secret C 3
Chet Nate: BETZ 22K SERIES
LA Code: 3434 l 3 Pure XJ Mixture [ 3 Solid [X] Liquid t 1 Gas
Fire SROP React X Acute Chron
03
AM UTILITIES, DEMINERALIZER, COOLING T 0! 366
Q00006033 SM-
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
fhys. t
Avg. No. of
Health Max. Daily Days
Hazards Aiount Aaount On-Site Code
Storage Codes & Locations Non-Contidential *o Storage Locations
hi?
CAS t: N'A
Trade Secret t 3
Chee Naae: BETZ 3PK-38296
LA Code:
( 1 Pure CX3 Mixture 1 Solid [I] Liquid ] Gas
Fire SROP React X Acute X Chron
02
AI4 COOLING TOWER-SOUR CRUDE 00 366
CAS t: N/A
Trade Secret I 3
fjo
Chee Naae: BETZ 30K-30327
LA Code: ( ) Pure 13 Mixture 3 Solid [13 Liquid 3 Gas
CAS *: N/A
Trade Secret 3
bto
Chee Naae: BETZ 30K SERIES
LA Code: 7055 [ 1 Pure EXT Mixture [ 3 Solid [13 Liquid 3 Gas
X Fire
SROP React X Acute X Chron
02
Fire SROP React X Acute X Chron
03
A14 ACID PLANT 00 366
A14 UTILITIES, DEHINERALIZER, COOLING T 00 366
CAS t: N/A
Trade Secret 3
Chee Naae: BETZ 407C
LA Code: 7661 3 Pure CX3 Mixture 3 Solid 13 Liquid 3 Gas
X Fire SROP React
X Acute X Chron
03
A!4 UTILITIES, DEMINERALIZER, COOLING T 00 366
('Jo
CAS i: N/A
Trade Secret 3
Chee Naae: BETZ 40K-4B143
LA Code: 8435 3 Pure N Mixture 3 Solid m Liquid 3 6as
Fire SROP React X Acute Chron
03
A14 UTILITIES, DEMINERALIZER, CODLING T 00 366
7 CAS l:
N/A
Trade Secret I
Chee Naae: BETZ 40P
LA Code: 6439 [ 3 Pure X3 Mixture 3 Solid EXT Liquid 3 Gas
X Fire SROP
X React X Acute X Chron
01
D14 POWER PLANT 00 366
f\] 0
CAS : N/A
Trade Secret 3
Chea Naae: BETZ Dfl-132?
LA Code: l 3 Pure 113 Mixture [ 3 Solid m Liquid 3 Gas
X Fire SROP React
X Acute X Cnron
03
A14 #3 CRUDE, VACUUM 02 366
CAS t: 106978 Trade Secret [ 3
Chea Naae: N-BUTANE/'D' GRADE BUTANE /ISOBUTANE LA Code: 1215
( 3 Pure 13 Mixture [ 3 Solid 13 Liquid E 3 6as
i, Fire X SROP
React Acute X Chron
05
A24 RUN-DOWN AREA R25 THERMAL UNIT R25 ALKY UNIT 05 366 R25 FCC R25 CAT POLY R25 GRP
SAL 00000603A
CONOCO REFINERY, WESTLAKE,Lfl
Cheaical Description
CAS t: m
Trade Secret [ 3
Chen Nine: C125-1-01
LA Code: 8489 [ 3 Pure C33 fixture HI Solid C 3 Liquid [ 3 Gas
Phys. i
Avq. No. o{
Health Max. Daily Days
Hazards Aaount Aaount On-Site Code
Storage Codes k Locations * Non-ConTidential Storage Locations
Fire X SKQP
React X Acute X Chron
03
R25 13 REFORMER 03 366
CAS t: 64743051 Trade Secret f 3
X Fi'e
Chea Naae: CALCINED PETROLEUM COKE
SROP
0 React 05
LA Code:
X Acute
l 3 Pure CXJ Mixture
X Chron
CX3 Solid 1 3 Liquid I 1 Gas
CAS t: 77785^3 Trade Secret I 3
Che* Nane: CALCIUM HYPOCHLORI'E
LA Code: 1345 m Pure C 3 Mixture CXJ Solid [ 3 Liquid I 3 Gas
X Fire SROP
React X Acute
Chron
01
CAS t: 1305788 Trade Secret [ 3
Chea Naae: CALCIUM OXIDE
LA Code: 1347 m Pure C 3 Mixture m Solid [ 3 Liquid I 3 Gas
Fire SROP X React X Acute Chron
02
Hid PREMIUM COKER S14 PREMIUM COKER R14 PREMIUM COKER 05 366
114 UTILITIES, DEHINERALI2ER, C00LIN6 T 00 366
D14 REFINERY HIDE 00 366
CAS : 7448444 Trade Secret t 3
Chea Naae: CARBON, ACTIVATED
LA Code: 1387 m Pure [ 3 Mixture CXI Solid t 3 Liquid I 3 Gas
X Fire SROP React Acute Chron
04
R25 46,7,8 HDS 04 366
CAS I: 124389 Trade Secret C 3
Chen Naae: CARBON DIOXIDE
LA Code: 1391 tX] Pure 1 3 Mixture C 1 Solid [ 3 liquid 1X3 Gas
Fire X SROP
React X Acute
Chron
81
L24 REFINERY HIDE 00 366
CAS l: N/A
Trade Secret I 3
Chea Naae: CASINGHEAD GASOLINE
LA Cade: 2464 CX3 Pure f 3 Mixture [ 3 Solid CX3 Liquid I 3 Gas
X Fire X SROP
React Acute X Chron
04
R24 THERMAL UNIT 04 366
CAS 1: K/fi
Trade Secret t 3
Fire
Chen Naae: CAT FLOC K-10
SROP
X React 03
0
LA Code:
1 Acute
[ 3 Pure CXI Mixture
Chron
[ 3 Solid [X3 Liquid [ ] 6as
A14 TRAPS 02 366
sal
00006035
i
A //
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
Phvs. k
Avq. No. of
Health Max. Daily Days
Hazards Arount Aaount On-Site Code
Storaoe Codes & Locations ** Ron-Confidential * Storage Locations
CAS #: K/A
Trade Secret ]
Chei Naae: CHEVRON RHENIFORNER TYPE F CATALYST LA Code: 8504
3 Pure (X3 Mixture CX] Solid [ ] Liquid [ 1 Gas
Fire
X SROP React
X Acute X Chron
84
R25 REFORMER 83 366
CAS i: 7782585 Trade Secret [ 1
Chea Naae: CHLORINE
LA Code: 1465 X3 Pure 1 Mixture [ 1 Solid m Liquid 1 Gas
X Fire
X SR3P X React X Acute
Chron
83
L24 UTILITIES. DEMINERALIZER, COOLING T L24 ACID PLANT L24 COOLING TONER-SOUR CRUDE 01 366
CAS t: 353593 Trade Secret ]
Chea Naae: CHLGRODIFLUOROBRQMQNETHAN E LA Code: E460
X3 Pure [ 1 Mixture I 1 Solid ] Liquid m Gas
Fire X SROP
React X Acute
Chron
01
L24 REFINERY WIDE 01 366
CAS t: N/A
Trade Secret 1
Chea Naae: CHL0ROTHENE SM SOLVENT
LA Code: 8585
C 3 Pure fX3 Mixture 3 Solid U) Liquid 3 Gas
X Fire SROP React
X Acute X Chron
81
D14 REFINERY HIDE 01 366
CAS 1: N/A
Trade Secret 3
Chea Naae: CIT-CON FEEDSTOCK
LA Code: [ 3 Pure X3 Mixture 3 Solid XJ Liquid [ 3 Gas
X Fire X SROP
React Acute X Chron
86
A15 PUMPHOUSE A25 12 CRUDE
05 366
CAS l: N/A
Trade Secret 3
Chea Naae: COKER BLOWDOWN
LA Code: [ 1 Pure CX3 Mixture
3 Solid m Liquid 3 Gas
X Fire X SRDP
React X Acute X Chron
84
A14 PUMPHOUSE A25 PREMIUM COKER
A25 SOUR CRUDE COKER 83 366
CAS i: 64741828 Trade Secret 3
Chea Naae: COKER NAPHTHA
LA Code: [ 3 Pure CXI Mixture C 3 Solid [X3 Liguid C 3 Sas
CAS i: N/A
Trade Secret [ 3
Chea Naae: CQHAC 618
LA Code: l J Pure LX3 Mixture 3 Solid it) Liquid [ 3 Sas
X Fire X SROP
React X Acute
Chron
07
X Fire SROP React
X Acute Cnron
02
A14 PUMPHOUSE A25 PREMIUM COKER A25 SOUR CRUDE CDKEfi 86 366
A14 SOUR CRUDE COKER
80 366
00006036 SAL 0
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
PtW5. 1
Avq. No. of
Health Max. Daily Days
Hazards Aaount Aaount On-Site Code
Storage Codes 6 Locations ** Nan-Confidential ** Storage Locations
CfiS t: 1318747 Trade Secret t 1
Chen Nate: CO COMBUSTION PROMOTERS, COCAT AND PROCAT LA Code: 8436
IX] Pure t 3 Mixture m Solid [ 3 Liquid l ) Gas
Fire SROP React X Acute Chron
81
D14 FCC 88 366
CAS t: 38669339 Trade Secret [ 1
Chea Nate: CONOCO CDR FLOW IMPROVER
LA Code: 8488 IX] Pure l ] Mixture I ] Solid CX3 Liquid C 1 6as
X Fire SROP
React X Acute X Chron
84
A14 CDR 83 366
CAS t: 64741851 Trade Secret [ 3
Che* Naae: CONOCO LVT OIL
LA Code: 8485 [X3 Pure [ 3 Mixture [ 3 Solid [U Liquid [ ] 6as
X Fire SROP React
X Acute X Chron
85
A14 RUN-DONN AREA 85 366
CAS : 7732185 Trade Secret t 3
Che* Naae: COOLING TONER SLOWDOWN
LA Code: l 3 Pure [X3 Mixture [ 3 Solid CX3 Liquid [ 3 Gas
CfiS *: 64742478 Trade Secret [ 1
Che* Naae: CRACKED DISTILLATE
LA Code: t 1 Pure 1X3 Mixture [ I Solid [Kl Liquid [ ] Gas
Fire X SROP
React Acute Chron
85
R26 PCWER PLANT R26 ACID PLANT
02 366
-- ------
X Fire SROP React
Acute I Chron
87
A14 R24 R24 86 366
EAST TANK FARM THERMAL UNIT FCC
CAS i: 8082058 Trade Secret t I
Che* Naie: CRUDE OIL SOUR
LA Code: 1669 I 3 Pure CX3 Mixture t 3 Solid IXJ Liquid I 3 Gas
CAS *: 0002057 Trade Secret l 3
Che* Naae: CRUDE OIL SWEET
LA Code: 1669 IX] Pure [ 3 Mixture I 3 Solid 1X3 Liquid I 1 Bas
X Fire SROP React
X Acute X Chron
88
X Fire SROP React Acute
X Chron
88
A15 PUMPHOUSE R25 16,7,0 HDS R25 43 CRUDE, VACUUM 08 366
A14 SOUTH TANK FARM R25 12 CRUDE R25 S3 CRUDE, VACUUM 07 366
CAS i: N/A
Trade Secret l I
Chea Raise: CTU OVERHEAD DEBUTANIZER GAS LA Code: 8475
I 3 Pure 1X3 Mixture t 3 Sol i d l 3 Li quid CXI Gas
X Fire X SROP
React X Acute X Chron
82
R25 *2 CRUDE
R25 REFORMER
R25 43 CRUDE, VACUUM 02 366
/
000006037
SAt
a!
Ho
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
Phys. t
Avii. No. o{
Health Max. Daily Says
Hazards Aaount Aaount On-Site Code
Storage Codes & Locations * Non-Confidential ** Storage Locations
CAS : 800B206 Trade Secret [ ]
Chea Naae: KC CUTTER STOCK
LA Code: 8487 (XT Pure C ] Mixture [ ] Solid Q'3 Liquid [ 1 6as
I Fire
SROP React Acute X Chron
06
A14 SOUTH TANK FARM 05 366
CAS : 1330207 Trade Secret I ]
Chea Naae: DCI-6
LA Code: I 3 Pure EXT Mixture ( 3 Solid m Liquid 1 I Gas
X Fire
SROP React X Acute X Chron
02
A14 PUMPHOUSE 02 366
CAS 1: 64741624 Trade Secret [ 3
Chea Naae: DECANT OIL
LA Code: [ 3 Pure U3 Mixture t 3 Solid m Liquid I 3 Gas
X Fire X SROP
React Acute Chron
06
A14 PUMPHOUSE A25 FCC
05 366
CAS i: N/A
Trade Secret E 3
Chea Naae: DECTOL
LA Code: 1X3 Pure t 3 Mixture [ 3 Solid m Liquid t 3 Gas
X Fire SROP
React Acute X Chron
02
D14 REFINERY HIDE 01 366
CAS i: N/A
Trade Secret [ 3
Chea Naae: DENSTONE 57 ALL SIZES
LA Code: [ 3 Pure CX3 Mixture [X3 Solid [ 3 Liquid C 3 6as
Fire X SROP
React Acute Chron
03
R25 1 1 t 2 HDS R25 16,7,8 HDS R25 44,5 HDS 03 366 K14 WAREHOUSE
CAS t: 342961 Trade Secret I 3
Chea Name: DIBUTYL ETHER
LA Code: 1835 1X3 Pure C 3 Mixture [ 3 Solid 1X3 Liquid [ 3 Gas
X Fire SROP
X React X Acute
Chron
02
D14 CDfl 00 366
CAS 4: N/A
Trade Secret [ 3
Chet Naae: NO.2 DIESEL FUEL
LA Code: 19P8 t 3 Pure CX3 Mixture [ 3 Solid [X] Liquid [ 3 Sas
X Fire SROP React Acute
X Cnron
03
A14 RUN-DOWN AREA A14 EAST TANK FARM A14 SOUTH TANK FARM
06 566 R24 12 CRUDE R24 PREMIUM COKER R24 SOUR CRUDE CQKER R24 43 CRUDE, VACUUM
CAS l: 111422 Trade 5ecret C 3
Chea Naae: DIETHANOLAMINE
LA Code: 1X3 Pure t 3 Mixture C 3 Solid m Liquid I 3 Eas
Fire SROP React X Acute Chron
04
A25 FCC 04 366
000006038 SAL
CONOCO REFINERY, NESTLAKE.tA
Chemical Description
Phys. 1
Avq. No. o{
Health Max. Daily Days
Hazards Aiount Aaount On-Site Code
Storage Codes & Locations * Non-Contidential t Storage Locations
CflS t: 1779255 Trade Secret I 3
Chei Naie: DIISOBUTYLALUKINUK CHLORI DE Lfl Code: 8429
CX3 Pure { I Mixture [ 1 Solid m Liquid [ ] Gas
X Fire SRQP
X React X Acute
Chron
02
A14 CDR 02 366
CAS : 624928 Trade Secret I ]
Che* Naie: DIMETHYL DISULFIDE
LA Code: [13 Pure t 3 Mixture [ I Solid m Liquid [ 3 6as
X Fire SROP React
X Acute Chron
02
R24 1 & 2 HDS
R24 16,7,8 HDS R24 14,5 HDS 02 366
CAS 1: 75183 Trade Secret t 3
Chea Nane: DIMETHYL SULFIDE
O LA Code: til Pure f 3 Mixture [ 3 Solid. EXT Liquid [ 3 Gas
X Fire SROP React
X Acute Chron
02
R24 REFORMER 02 366
CAS *: 68177391 Trade Secret [ ]
Chet Naie: DQKEX (R) SBR-F-CL ANION EXCHANGE RESIN LA Code: 6259
C 3 Pure CX3 Mixture [X3 Solid L 3 Liquid [ 3 Gas
Fire X SROP X React X Acute
Chron
03
R24 PCKER PLANT 03 366
CAS *: N/A
Trade Secret I 3
Chef Nane: DRY-O-LITE DESSICANT
LA Code: [X3 Pure I 3 Mixture [X3 Solid [ 3 Liquid I 3 Gas
Fire X SRQP
React X Acute
Chron
01
A25 REFINERY HIDE 00 366
CAS I: N/fi
Trade Secret I 3
Chea Nace: DUPONT OIL BRONZE LIQUID DYE LA Code:
[ 3 Pure [XI Mixture C 3 Solid EX] Liquid [ 3 Gas
X Fire SROP React
X Acute X Chron
03
A14 PUMPHOUSE 00 366
CAS f: N/A
Trade Secret [ 3
Chea Nane; DUPONT GIL RED 6 LIQUID
LA Code: l 3 Pure EX3 Mixture [ 3 Solid EXT Liquid C 3 Gas
X Fire SROP React
X Acute X Chron
03
A14 PUMPHOUSE 00 366
CAS 1: N/A
Trade Secret [ 3
X Fire
Chea Name: DUPONT SOLVENT 32035 0
SRQP React
01
LA Code:
X Acute
l J Pure LX3 Mixture
X Chron
[ 3 Solid EX3 Liquid t 3 Gas
D14 REFINERY HIDE 0! 366
SAL 000006039
*
>
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
Phys. 1
Avq. No. of
Health Max. Daily Days
Hazards Aiount Aiount On-Site Code
Storage Codes 6 Locations * Non-Ccnfidential *#* Storage Locations
CAS i: N/A
Trade Secret C ]
Chei Naie: EUMINOX OXYGEN SCAVENGER
LA Code: 8428 [ 3 Pure EX] Mixture [ 3 Solid [XI Liquid ( I Gas
Fire SROP React X Acute Chron
01
D14 POWER PLANT 01 366
CAS #: N/A
Trade Secret [ 3
Che* Naie: ENGELHARD FCC CATALYST
LA Code: [ 3 Pure UJ Mixture [X] Solid T 3 Liquid I 3 6as
Fire X SROP
React I Acute X Chron
04
R25 FCC 04 366
CAS #: 187211 Trade Secret [ 3
Chea Naie: ETHYLENE GLYCOL
LA Code: 2273 [X] Pure [ 3 Mixture [ 3 Solid m Liquid [ 3 Gas
Fire X SROP
React X Acute X Chron
02
R24 REFINERY WIDE 01 366
CAS V. 12108133 Trade Secret I 3
Che# Naie: ETHYL MHT DILUTE
LA Code: 2967 [ 3 Pure CXI Mixture [ 3 Solid 1X3 liquid I 3 Gas
X Fire SROP React
X Acute X Chron
04
A14 PUMPHOUSE 03 666
CAS : N/A
Trade Secret C 1
Chei Naie: FCC LIGHT CYCLE OIL
LA Code: I 3 Pure [X] Mixture ( 3 Solid [X] Liquid [ 3 Gas
X Fire X SROP
React Acute X Chron
85
A14 PUMPHOUSE A14 RUN-DOWN AREA
R25 THERMAL UNIT 05 366 R25 FCC
R25 PREMIUM COKER R25 13 CRUDE, VACUUM
CAS i: N/A
Trade Secret [ I
Chei Naie: FDA-11
LA Code: 8442
[ 3 Pure [X] Mixture l ] Solid m Liquid [ I Bas
X Fire SROP React
X Acute X Chron
0!
A14 PUMPHOUSE 01 366
CAS t: 68308270 Trade Secret I 3
Chei Naie: FUEL GAS
LA Code: [ 3 Pure 1X3 Mixture l 3 Solid [ 3 Liquid U3 Gas
X Fire X SROP
React X Acute
Chron
85
A24 REFINERY WIDE 34 366
CAS f: 64741646 Trade Secret I 3
Chea Naie: FULL RANGE ALKYLATION NAP HTHA LA Code: 8313
in Pure I 3 Mixture [ 3 Solid [13 Liquid I ] Gas
X Fire X SROP
React Acute X Chron
85
R25 ALKY UNIT 05 366
;
000604-0
SAL 0
d
hi.
0
CONOCO REFINERY, WESTLAKE,LA
Chetical Description
Phys. i
Health Hazards
Avq. No. of Max, Daily Days fifount Aaount On-Site
Code
Storage Codes i Locations * Non-Confideatial *** Storage Locations
CAS *: m
Trade Secret [ ]
Chei Naie: GAS OIL. NO,2, N0.3-SH
LA Cede; 2462 [ 1 Pure HI Mixture
I I Solid [XJ Liquid C 1 Gas
X Fi'e SROP React
X Acute X Chran
08
A15 EAST TANK FARM A15 SOUTH TANK FARM R24 42 CRUOE 06 366 R24 43 CRUDE, VACUUM
CAS 4: 56S15 Trade Secret C 3 Chei Naie: 6LYCERIKE,USP,96I
LA Code: 2473
( ] Pure CXI Mixture ( 1 Solid 1X3 Liquid C 1 Gas
X Fire SROP
X React X Acute X Chron
n
A14 PUMPHOUSE 00 366
CAS i: 64741793 Trade Secret I 3
Chet Naie; GREEN PETROLEUM COKE
LA Code: 3787 I 1 Pure (XI Mixture
CX3 Solid [ 3 Liquid [ 3 6as
CAS 4: N/A
Trade Secret [ I
Che* Naae; HDS RECYCLE HYDROGEN
LA Code: 2640 IX] Pure t 3 Mixture t 3 Solid t 3 Liquid CXI Gas
X Fire SROP React
X Acute X Chron
07
X Fire X SROP
React X Acute X Chron
66
H14 PREMIUM COKER 014 PREMIUM COKER R14 PREMIUM COKER 06 j66 H14 SOUR CRUDE COKER 814 SOUR CRUDE COKER R14 SOUR CRUOE COKER
R24 4 1 t 2 HDS R24 46,7,8 HDS R24 44,5 HDS 06 366
CAS 4: N/fi
Trade Secret C 3
Che* Naae: HDS SEPARATOR GAS
LA Code: 1X3 Pure [ 1 Mixture t 3 Solid l 3 Liquid CXI Gas
X Fire X SRDP
React X Acute X Chron
06
R25 1 i t 2 HDS R25 46,7,8 HDS R25 44,5 HDS
06 366
CAS 4: N/fi
Trade Secret t 3
Che* Naae: HDS STRIPPER OVERHEAD GAS
LA Code: [X3 Pure t 3 Mixture t 3 Solid l 3 Liquid CX] 6as
X Fire I SROP
React
I Acute X Chron
04
R25 46,7,8 HDS R25 44,5 HDS
04 366
CAS 4: N/fi
Trade Secret E 3
Chea Mane: HDS STRIPPER OVERHEAD LIB UID
LA Code; 8474 [ 3 Pure U3 Mixture [ 1 Solid CX3 Liquid [ ] Gas
X Fire X SROP
React
Acute X Chron
04
R25 #6.7,8 HDS R25 44,5 HDS
04 366
CAS #: N/fi
Trade Secret C 3
ChE* Race: HEAVY AROMATIC DISTILLATE
LA Code: I 3 Pure C'X] Mixture C 3 Solid CU Liquid [ 1 Gas
X Fire SROP React
X Acute X Chron
05
AIA PUMPHOUSE R24 #3 CRUDE, VACUUM
05 364
SAL 000006041
f'Jo
0
CONOCO REFIN-RY, WESTLAKE,LA.
Cheiical Description
Phys. &
Avo. No. of
Storage Codes 4 Locations
Health flax. Daily Days
*** Non-Confidential *+
Hazards Aiount Aiount On-Site Code
Storage Locations
CAS l: 68512616 Trade Secret ( 1
Che* Naie: HEAVY COKER GAS Oil
-
LA Code: in Pure [ ] Mixture [ ] Solid 1X1 Liquid [ 3 Gas
X Fi'e SROP React
X Acute
X Chron
04
A25 FCC Xli 43 CRUDE, VACUUM
04 366
CAS t: 64741511 Trade Secret [ 3
Che* Naee: HEAVY PARAFFINIC DISTILLA TE LA Code: 7993
EX3 Pure E 3 Mixture [ 3 Solid CXI Liquid t 3 Gas
X Fire
SROP React X Acute X Chron
05
A14 PUMPHOUSE R25 46,7,8 HSS R2? 43 CRUDE, VACUUM 04 366
CAS f: 68512618 Trade Secret E 3
Che* Nans: HEAVY PREMIUM COKER GAS 0 IL LA Code: 8464
EX3 Pure [ 3 Mixture [ 3 Solid EX] liquid I 3 Gas
X Fire
SROP React
Acute X Chron
06
A1S RUN-DOWN AREA A15 EAST TANK FARM ftl5 PREMIUM COKER
06 366 A15 16,7,8 HDS
CAS 4: 64741419 Trade Secret E 3
Chei Naie: HEAVY STRAIGHT RUN NAPHTH A LA Code: 8083
[13 Pure E 3 Mixture [ ] Solid CXI Liquid 1 3 Gas
X Fire
X SROP React
X Acute X Chron
06
A14 PUMPHOUSE A14 SOUTH TANK FARM
R25 42 CRUDE 05 366 R25 REFORMER
R25 46,7,8 HDS
R25 43 CRUDE, VACUUM R25 43 REFORMER
CAS 1: 64741817 Trade Secret I 3
Che* Naie: HEAVY THERMAL CRACKED DIS T3LLATE LA Code: 8006
E 3 Pure IX] Mixture [ 3 Solid EX3 Liquid E 3 Gas
X Fire
I SROP React Acute
Chron
05
R25 THERMAL UNIT R25 PREMIUM COKER
04 366
CAS 4: 64741577 Trade Secret [ 3
Chei Naie: HEAVY VACUUM GAS OIL
LA Code: 8466 EX] Pure E 3 Mixture E 3 Solid EX3 liquid E 1 Gas
X Fire SROP
React Acute X Chron
06
R35 43 CRUDE, VACUUM 86 366
CfiS 4: 7440597 Trade Secret I 3
CtiEH Naae: HELIUM
LA Code: 2512 EX! Pure E 3 Mixture [ 3 Solid E 3 Liquid EX3 Gas
Fire
X SROP React
X Acute
Chron
03
L24 REFINERY WIDE
03 366
CAS 4: 111273 Trade Secret E 3
Che* Nase: 1-HEXANE3L
LA Code: 2579 [XI Pure E 3 Mixture
[ 3 Solid m Liquid [ 3 6as
X Fire SROP
React X Acute X Chron
0!
A14 CDR
02 366
SAL 000006042
CONOCO REFINERY, WESTLAKE,LA
Chetical Description
Phys. i
Avq. No. of
Storage Codes & Locations
Health Max. Daily Days
** Non-Confidential ***
Hazards Aaount Aaount On-Site Code
Storage Locations
CAS i: 592416 Trade Secret I ]
Chei Nate: 1-HEXENE
LA Code: CX3 Pure C 3 Mixture ( 1 Solid m Liquid [ ] Gas
X Fire SHOP React
X Acute Chron
05
A24 CDR 05 366
CAS : 7647010 Trade Secret [ 1
Chet Nate: HYDROCHLORIC ACID
LA Code: 2613 ( ] Pure IX] Mixture 1 ] Solid [XI Liquid [ 3 Gas
Fire SROP
React
X Acute Chron
03
A14 UTILITIES, DEMINERALIZER, COOLING T 03 566
CAS 0: 64742796 Trade Secret C 3
Chet Naae: HYDRQDESULFURIZED GAS OIL
LA Code: 0472 [XI Pure [ 3 Mixture [ 3 Solid CXI Liquid C 3 Gas
X Fire I SROP
React
Acute X Chron
07
A15 RUN-DOWN AREA
R25 16,7,6 HDS R25 04,5 HDS
06 366
CAS f: 64742818 Trade Secret C 3
Chet Nate: HYDRQDESULFURIZED KERQSEN E LA Code: 8473
[X3 Pure [ 3 Mixture [ 3 Solid in Liquid C 3 Gas
X Fire X SROP
React
Acute X Chron
05
R25 * 1 t 2 HDS 05 366
CAS 4: 64742730 Trade Secret I 1
Chet Nate: HYDRQDESULFURIZED LIGHT k HEAVY NAPHTHA LA Code: 8471
1X3 Pure f 3 Mixture I 3 Solid 1X1 Liquid I 3 Gas
X Fire X SROP
React X Acute
X Chron
05
R25 REFORMER 05 366
CAS 0: 64742809 Trade Secret I 3
Chet Nate: HYDRQDESULFURIZED MIDDLE DISTILLATE LA Code:
[X3 Pure [ 3 Mixture I 3 Solid 1X1 Liquid 1 3 Gas
X Fire X SROP
React
Acute X Chron
06
R25 06,7,8 HDS R25 04,5 HDS
06 366
CAS l: 1333740 Trade Secret 1 3
Chea Nate: HYDROGEN
LA Code: 2640 1X3 Pure 1 3 Mixture 1 3 Solid 1 3 Liquid 1X1 Gas
X Fire
X SROP React Acute
Chron
01
124 REFINERY WIDE 00 366
CAS i: 7722841 Trade Secret 1 3
Chen Nate: HYDROGEN PEROXIDE 0
LA Code: 2641 1 3 Pure 1X3 Mixture C 3 Solid 1X1 Liquid 1 3 Gas
l Fire SROP React
X Acute
Chron
01
314 ACID PLANT 01 366
00060^ SAL 00
CONOCO REFINERY, WESTLAKE,LA.
Chetical Description
Phvs. i
Avq. No. ol
Storage Codes k Locations
Health Max. Daily Days
Non-Confidential *
Hazards Airount Aaount On-Site Code
Storage Locations
bio
CAS U 7783064 Trade Secret C 1
Chet Nate: HYDROGEN SULFIDE
LA Code: 2646 [X] Pure t 3 Mixture [ 1 Solid [ 3 Liquid 1X3 Gas
X Fire X SROP
React X Acute
Chron
04
R25 REFINERY HIDE 04 366
*
CAS : N7A
Trade Secret I 3
Chet Nate: HYDROPROCES5IN6 CATALYST
TK--551 LA Code: 08493
I 3 Pure EXT Mixture
m Solid [ 1 Liquid [ 1 Gas
Fire X SROP
React X Acute X Chron
03
R25 * 1 i 2 HDS 03 366
CAS 1: N/A
Trade Secret t 3
A
Chet Nane: HYDROPROCESSING CATALYST TK-7U
LA Code: 8301
I 3 Pure 1X3 Mixture
m Solid [ 3 Liquid C 3 Gas
a CAS *: 64742467 Trade Secret E 3
Chet Nate: HYDROTREATED KIDDLE D1ST1
LLATE
f^Jo
LA Code: 3235
EXT Pure C 3 Mixture
[ 3 Solid EX3 Liquid 1 1 Gas
Fire X SROP
React X Acute X Chron
X Fire X SROP
React X Acute X Chron
03 06
R25 #6,7,B HDS 02 366
R25 #6,7,8 HDS R25 #4,5 HDS 06 366
A/o
CAS : 64742592 Trade Secret E 3
Chet Nate: HYDROTREATED VACUUM GAS 0 IL LA Code: 8478
1X3 Pure C 3 Mixture [ 3 Solid m Liquid [ 1 Gas
X Fire X SROP
React Acute
X Chron
08
A15 EAST TANK FARM A15 SOUTH TANK FARM
R25 #6,7,8 HDS 07 366 R25 #4,5 HDS
CAS *: 1302676 Trade Secret I 3
Chet Nate: TK-10 R7H INERT TOPPING M ATERIAL LA Code:
EX3 Pure [ 3 Mixture in Solid E 1 Liquid C 1 Gas
Fire
X SROP React
X Acute Chron
02
R?5 1 & 2 HDS R25 #6,7,8 HDS
02 366
CAS #: N/A
Trade Secret t 3
Chet Nate: IPC 5120 ADDITIVE
LA Code: 3451
t 3 Pure [X] Mixture E 1 Solid [XI Liquid [ 3 Gas
X Fire SROP React
l Acute Chron
02
A14 REFINERY WIDE 01 366
CAS : 67630 Trade Secret [ 3
X Fire
d Chet Nate: ISOPROPYL ALCOHOL
SROP React 02
LA Code: 2767 X Acute
EX3 Pure [ 3 Mixture
Chron
E 3 Solid m Liquid E 3 Gas
D14 CDft 00 366
SAL OOOOO6O44
(4? tJo
J
o 10
CONOCO REFINERY, WESTLAKE,LA
Cheiical Description
Phys. i
Avq. No. of
Storage Codes l Locations
Health Max. Daily Days
*** Non-Confidential *
Hazards Aiount Aiount On-Site Code
Storage Locations
CAS i: N/A
Trade Secret [ 3
Ctiei Naie: JET-A
LA Code:
I 3 Pure Cl] Mixture [ 3 Solid m Liquid t 1 Gas
J Fire SROP React Acute
X Chron
07
A14 RUN-DOWN AREA A14 EAST TANK FARM
R24 12 CRUDE 06 366 R24 4 1 * 2 HDS
CAS t: 8808206 Trade Secret [ 1
Che* Nate: KEROSENE
LA Code: 2815 CI3 Pure [ 3 Mixture [ 3 Solid [X] Liquid t 3 Gas
X Fire SROP React
l Acute
Chron
05
A14 PUMPHOUSE A14 RUN-DOWN AREA R24 *2 CRUDE 05 366 R251 42 CRUDE R24 43 CRUDE, VACUUM
R25 43 CRUDE, VACUUM
CAS i: N/A
Trade Secret I 1
Che* Nate: KONTQL K-430-N
LA Code: [ 1 Pure [XI Mixture
C 3 Solid EI3 Liquid C I Gas
Fire
SROP React X Acute Chron
02
A14 42 CRUDE A14 FCC
00 366
CAS : N/A
Trade Secret [ 1
Chet Naie: KONTOL K-437
LA Code: { 3 Pure rn Mixture [ ] Solid CXI Liquid C 3 Gas
i Fire SROP
X React X Acute
t Chron
02
AM SULPHJR PLANT 01 366
CAS t: N/A
Trade Secret I 1
Ches Nane; KONTOL K-450
LA Code: { 3 Pure tX3 Mixture
[ 1 Solid EX] Liquid [ 3 6as
X Fire SROP React
I Acute Chron
02
AM 42 CRUDE AM FCC
00 366
CAS i: N/A
Trade Secret [ 3
Che* Naae; KR0MTR01 X-5
LA Code: 8458 in Pure [ 3 Mixture t 3 Solid m Liquid t 3 Gas
Fire
SROP React X Acute Chron
02
D14 PCWER PLANT DM ALKY UNIT
D14 REFORMER
01 366
CAS 8: N/A
Trade Secret E 3
Chen Naie: LEADED REGULAR GASOLINE
LA Code: 2444 t 3 Pure 1X3 Mixture
E 3 Solid CI3 Liquid [ 3 Gas
X Fire SROP
React Acute
X Chron
07
A14 RUN-DOWN AREA A14 EAST TANK FARM
07 366
CAS 8: E4742S22 Trade Secret [ 3
Chen Nane: LIGHT AROMATIC CONCENTRAT E LA Code: 8434
[ 3 Pure tX] Mixture [ 1 Solid m Liquid 1 3 Gas
X Fire
X SROP React
I Acute X Chron
03
A14 PUMPHOUSE R24 FCC
R24 #3 CRUDE, VACUUM 03 366
$A L 000^604S
CONOCO REFINERY, NESTLAKE,LA.
Chemical Description
Phys. 4
Avq. No. of
Storage Codes It Locations
Health Max. Daily Days
* Non-Confidential *
Hazards Arount Atount On-Site Code
Storage Locations
CAS t: 64741420 Trade Secret [ 1
Che* Naie: LIGHT FEEDSTOCK SM
LA Code: 8483 m Pure [ 3 Mixture
[ 3 Solid [I] Liquid C 1 Gas
CAS 1: N/A
Trade Secret [ I
Che* Nase: LIGHT FUEL OIL
LA Code: 9443 I 3 Pure [X3 Mixture I 3 Solid 1X3 Liquid I I Gas
X Fi'e
X SROP
React Acute X Chron
07
X Fire
SROP React X Acute
X Chron
07
A14 EAST TANK FARM A14 SOUTH TANK FARM R25 12 CRUDE 06 366 R25 13 CRUDE, VACUUM
A14 PUMPHOUSE
05 366
CAS #: 64741555 Trade Secret [ 3
Chet Naae: LIGHT & HEAVY CATALYTIC C RACKED NAPHTHA LA Code: 8012
1X3 Pure C 3 Mixture { 3 Solid [XI Liquid I 1 Gas
X Fire
X SROP React
X Acute X Chron
06
A14 PUMPHOUSE
A14 EAST TANK FARM
R25 FCC 05 366
CfiS l: 64741635 Trade Secret [ 3
Che* Nae: LIGHT & HEAVY CATALYTIC R EFORMED NAPHTHA LA Code: 60:6
1X3 Pure E 3 Mixture [ 3 Solid [X3 Liquid I 3 6as
X Fire I SROP
React Acute
X Chron
07
A14 EAST TANK FARM R25 REFORMER R25 13 REFORMER
05 366
CAS l: 6474174B Trade Secret E 3
Chei Nace: LIGHT & HEAVY THERMAL CRA CKED NAPHTHA LA Code: 8004
EX3 Pure I 3 Mixture ( 3 Solid CXI Liquid C 1 Gas
X Fire X SROP
React X Acute X Chron
04
R25 THERMAL UNIT
R25 REFORMER R25 PREMIUM COKER 04 366 R25 GRP
CAS I: 64741500 Trade Secret C 3
Che* Nase: LIGHT PARAFFINIC SISTILLA TE LA Code: 847fl
1X3 Pure C 3 Mixture I 3 Solid CXI Liquid I 3 Gas
X Fire SROP
React X Acute X Chron
05
A14 EAST TANK FARM R25 13 CRUDE, VACUUM
04 366
CAS l: 64741464 Trade Secret t 3
Che* Nase: LIGHT STRAIGHT RUN GASOLI NE LA Code: 0002
CXI Pure t J Mixture [ 3 Solid CXI Liquid I 3 Ess
X Fire
X SROP React
X Acute X Chron
05
AM PUMPHOUSE A24 RUN-DOWN AREA
R25 2 CRUDE 05 366 R25 GRP
R25 43 CRUDE, VACUUM
CfiS l: 64741464 Trade Secret t ]
Che* Nase: LIGHT STRAIGHT RUN GASOLI NE INTERMEDIATE STREAM LA Code:
[ 3 Pure CXI Mixture ( 3 Solid in Liquid C 1 6**
X Fire X SROP
React I Acute
X Chron
05
A24 EAST TANK FARM
R24 2 CRUDE R24 43 CRUDE, VACUUM
04 366
SAL 0000060^6
CONOCO REFINERY, WESTLAKE,LA.
Cheiical Description
Phys. L
five. No. ot
Storage Codes & Locations
Health Max. Daily Days
*** Non-Confidential
Hazards Aeount Aiount On-Site Code
Storage Locations
CAS : 64741028 Trade Secret [ ]
Che* Naie: LIGHT THERMAL CRACKED DIS TILLATE LA Code: 8005
m Pure t ] Mixture ( 3 Solid m Liquid I 3 Gas
CAS #: 64741588 Trade Secret [ 1
Che* Naie: LIGHT VACUUM GAS OIL
LA Code: E465 m Pure 1 1 Mixture [ 3 Solid CXI Liquid t ] Gas
I Fire
X SROP React Acute
X Chron
04
X Fire
SROP React Acute
X Chron
05
R25 THERMAL UNIT 825 PREMIUM COKER R25 SOUR CRUDE COKER 04 366
R35 SOUR CRUDE COKER R35 16.7,8 HDS R35 13 CRUDE, VACUUM 05 366
CAS i: 111773 Trade Secret [ 3
Che* Kane: METHYL CARBITDL
LA Code: E ] Pure EX1 Mixture [ 1 Solid HI Liquid t 1 Gas
X Fire SROP
React I Acute
Chron
03
A14 PUMPHOUSE 02 366
CAS : 78933 Trade Secret C I
Che* Naie: METHYL ETHYL KETONE
LA Code: 3113 [13 Pure [ 3 Mixture C ] Solid U1 Liquid [ ] Gas
X Fire
SROP
React X Acute X Chron
02
D14 REFINERY WIDE 02 366
CAS i: N/A
Trade Secret t 3
Che* Nate: MICRO PRO *D' (ORY CULTU
RE) LA Code: 8506
I 3 Pure (X3 Mixture m Solid I 3 Liquid l 3 Gas
Fire SROP
React X Acute X Chron
01
F14 TRAPS 00 366
CAS l: N/A
Trade Secret 1 3
Che* Naae: MOLECULAR SIEVE 3A
LA Code: 6307 C 3 Pure m Mixture CX3 Solid I 1 Liquid t 3 Sas
Fire
X SROP X React X Acute
Chron
03
R25 CRYO 03 366
CAS 4: 64741851 Trade Secret [ 3
Che* Nae: HOLE! RAFFINATE
LA Cede: 8455 m Pure I 3 Mixture C 3 Solid CXI Liquid l 3 Gas
X Fire SROP
React
X Acute X Chron
05
AH RUN-DOWN AREA R24 CDR
05 366
CAS l: !1091B Trade Secret [ 3
Chen Mane: MORPHOLINE
LA Code: 3279 CX3 Pure C 3 Mixture I 3 Solid m Liquid I 3 Gas
X Fire SROP
X React
X Acute X Chron
01
D14 REFORMER 00 566
SAL 000006047
{\]o
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
Rhys. &
Avg. No. of
Storage Codes & Locations
Health flax. Daily Days
*** Non-Confidential ***
Hazards Aaount ftaount On-Site Code
Storage Locations
CAS l: 64742525 Trade Secret t 1
Che* Naae: N-750-HT
LA Code: [ 3 Pure m Mixture ( ] Solid UJ Liquid C 1 6as
X Fi-c SROP React
X Acute X Chron
13
A15 PREMIUM COKER Aid SOUR CRUDE COKER
02 366
CAS t: N/A
Trade Secret t 1
Che* Ka*e: NALCO 1?
LA Code: 6473 t 3 Pure CXI Mixture
m Solid C 1 Liquid C 1 6as
CA5 : N/A
Trade Secret t 3
Che* Nate: NALCO 356 CORROSION INHIB I TOR
LA Code: 6464 t ] Pure CX3 Mixture l 1 Solid [X] Liquid [ 3 6as
Fire SROP React X Acute Chron
X Fire SROP React
I Acute Chron
02 03
114 POKER PLANT
01 366
`
A14 PCWER PLANT 01 366
CAS t: N/A
Trade Secret [ 1
Che* Nate: NALCO 5151 CORROSION 1NHI BITOR LA Code: 6547
[ 3 Pure [X3 Mixture [ 1 Solid [XI Liquid [ 3 Gas
Fire SROP React I Acute
Chron
02
A14 03 CRUDE, VACUUM 00 366
CAS 4: N/fi
Trade Secret [ 3
Che* Nate: NALCO 5165 CORROSION INHI BITOR LA Code: 8453
I 3 Pure CXI Mixture t 3 Solid m liquid ( 3 Gas
X Fire SROP React
X Acute Chron
03
A14 THERMAL UNIT A14 3 CRIDE, VACUUM
02 366
CAS 0: N/A
Trade Secret C 1
Che* Naae: NALCO 5166 CORROSION INHI BITOR LA Code: 8452
[ 3 Pure 1X3 Mixture 1 3 Solid CX3 Liquid l 1 Gas
X Fire SROP React
X Acute
Chron
03
A14 43 CRUDE, VACUUM 00 366
CAS I: N/A
Trade Secret [ 3
Chen Naae: NALCO 5180 CORROSION INHI BITOR LA Code:
[ J Pure It) Mixture
C 3 Solid CX3 Liquid E 3 Bas
X Fire
SROP React X Acute X Chron
02
A14 03 CRUDE, VACUUM 00 366
CAS i: N/A
Trade Secret [ 1
Che Naae: NALCO 5196 CORROSION INHI
BITOR LA Code:
UJ Pure t 3 Mixture { 3 Solid CXI Liquid C 1 Sas
X Fire
SROP React X Acute
Chron
03
A14 THERMAL UNIT A14 13 CRUDE, VACUUM
00 366
SAL 000006048
fJ O
o
A/o
CONOCO REFINERY, WESTLAKE,LA
Chemical Description
Phys. 6
Avq. No. ot
Storage Codes l Locations
Health Max. Daily Days
** Non-ConTidential <tt
Hazards Aaount Aaount On-Site Code
Storage Locations
CAS I: N/A
Trade Secret [ ]
Chea Race: NALCO 5701 PROCESS ANTIFO
AN LA Code:
[ 3 Pure EX3 Mixture [ 3 Solid lU Liquid [ 3 Gas
X Fire SROP
React X Acute
Chron
03
A14 13 CRUDE, VACUUM 01 366
CAS l: N/A
Trade Secret 3
Chea Nate: NALCO 8263 FUEL TREATMENT
LA Code: 9454 13 Pure 3 Mixture
[ 3 Solid [H Liquid [ 3 Gas
Fire SRQP
React X Acute
Chron
03
A14 PREMIUM COKER A14 CALCINES 02 366 A14 SOUR CRUDE COKER
CAS t: 64742945 Trade Secret 1 1
Chea Naae: NALCO B7RC130
LA Code: [ 3 Pure EX3 Mixture l 3 Solid m Liquid l 1 Gas
X Fire SROP React
X Acute Chron
02
A14 PREMIUM COKER 01 366
CAS I: 64741420 Trade Secret E 3
Chea Naae: NAPHTHA
LA Code: 3394 ( 3 Pure X3 Mixture E 3 Solid EX3 Liquid E 1 Gas
X Fire X SROP
React X Acute X Chron
07
A!4 PUMPHOUSE A25 12 CRUDE A25 REFORMER 05 366 A25 13 CRUDE, VACUUM A25 13 REFORMER
CAS #: 64743128 Trade Secret C 3
Chea Na*e: NEOCENE 10 ALPHA OLEFIN
LA Code: 8431 113 Pure E 2 Mixture t 3 Solid EX] Liquid t 3 Gas
X Fire SROP
React X Acute
Chron
05
A24 CDR 04 366
CAS l: 7697372 Trade Secret E 3
Chea Naae: NITRIC ACID
LA Code: 3463 IX] Pure E 3 Mixture E 3 Solid El] Liquid [ I Gas
X Fire SRQP
X React I Acute
Chron
01
E14 ACID PLANT 00 366
CAS #: 7727379 Trade Secret t 3
Chea Hate: NITROGEN
LA Cede: 3502 [i3 Pure [ 3 Mixture E 3 Solid I ] Liquid EX3 Gas
Fire X SROP
React l Acute
Chron
03
R24 REFINERY WIDE 02 366
CAS i: 111659 Trade Secret E ]
Chea Nace: N-OCTANE
LA Code: 3631 EH Pure E ] Mixture E I Solid El] Liquid C 3 Gas
X Fire SROP React Acute Chron
01
D14 LAB 01 366
SAL 000006049
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Cheiical Description
CAS t: 7782447 Trade Secret [ ]
Che* Nate: OXYGEN
LA Code: 3663 EX] Pure E ] Mixture E ] Solid m Liquid EX] 6as
Phys. &
Avq. No. of
Storage Codes fc Locations
Health Max. Dami Days
*** Son-Confidential ***
Hazards Arount Atount On-Site Code
Storage Locations
X Fire
X SRDP React Acute Chron
02
L24 REFINERY WIDE R26 SULPHUR PLANT
02 366
CAS 1: N/A
Trade Secret E I
Che* Naae: PARADYNE 25
LA Code: E ] Pure EX] Mixture ( ] Solid EX] Liquid E ] Gas
X Fire SROP React
I Acute
Chron
03
A14 SOUTH TANK FARM 01 366
CAS l: N/fi
Trade Secret E 1
Che* Nate: PBC DEETHANIZER TAIL GAS
LA Code:
E 1 Pure EX] Mixture E 7 Solid E 1 Liquid EX] Gas
X Fire X SROP
React
X Acute X Chron
03
R15 THERMAL UNIT 03 366
CAS 4: 107153 Trade Secret E 3
Chei Naie: PET 1100
LA Code: 2303 I 3 Pure 1X3 Mixture E 3 Solid EX3 Liquid E 1 Gas
Fire SROP
React X Acute X Chron
02
A14 FCC 00 366
CAS 4: N/A
Trade Secret [ 3
Che* Nate: PET 1300
LA Code:
E 3 Pure EX] Mixture { 3 Solid EX] Liquid E ] Gas
X Fire SROP React
l Acute X Chron
02
A14 FCC 01 366
CAS I: N/A
Trade Secret I 3
Che* Naie: PETROTEC K 0456
LA Code: C 3 Pure EX3 Mixture
E 3 Sol id EX3 Liquid I 3 Gas
X Fire
SROP React
X Acute X Chron
02
A14 12 CRUDE 00 366
CAS 4*. N/fi
Trade Secret E 1
Che* Na*e: PETROTEC K-602
LA Code: [ ] Pure [XT Mixture [ ] Solid EX] Liquid E ] Gas
X Fire
SROP React X Acute X Chron
02
A14 42 CRUDE 00 366
CftS 4: N/A
Trade Secret E 3
Che* Naie: PETROTEC PET 1202
LA Code:
C ] Pure [XT Mixture [ I Solid m Liquid C 3 Gas
X Fire SROP React
I Acute
X Chron
02
A14 FCC 00 366
SAL 000006050
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CONOCO REFINERY, HESTLAKE.LA.
Chetical Description
Phys. 1
Avq. No. at
Storage Codes 6 Locations
Health Max. Daily Days
*** Nor-Confidential ***
Hazards Aaount Aaount On-Site Code
Storage Locations
CAS : N/A
Trade Secret [ ]
Che* Naie: PETROTEC PET 1328
' LA Code: I ] Pure [X] Mixture
C 1 Solid m Liquid [ 1 Gas
X Fire SROP React
X Acute Chron
02
A14 FCC 00 366
CAS t: N/A
Trade Secret 1
Chei Naae: PETROTEC PET133#
LA Code: 7949 C 3 Pure [X] Mixture
C J Solid CX] Liquid C 1 Gas
X Fire SROP
React
X Acute X Chron
02
A14 SUIPHJR PLANT
02 366
1
CAS t: N/A
Trade Secret [ 1
Che* Naie: PETROTEC PET 4000
LA Code:
1X3 Pure C 3 Mixture [ 1 Solid [X3 Liquid [ 3 6as
X Fire
SROP React X Acute I Chron
02
AH CAT POLY 01 366
CAS : N/A
Trade Secret [ I
Che* Naee: PETROTEC PET 7130
LA Code: l 3 Pure EX1 Mixture
t 3 Solid tX3 Liquid [ 3 Gas
X Fire
SROP React
X Acute X Chron
02
A14 FCC 00 366
CAS : N/A
Trade Secret [ 3
Chet Naee: POL-E-Z 7736
LA Code: 8455 1X3 Pure [ 1 Mixture
l I Solid [XI Liquid C 3 Gas
Fire SROP
React X Acute
Chron
02
A14 REFORMER 01 366
CAS t: 1336363 Trade Secret 3
Chea Naae: POLYCHLORINATED BIPHENYLS
LA Code: 3952 1X3 Pure [ 3 Mixture l 1 Solid [XI Liquid 1 Gas
Fire SROP
React
X Acute X Chron
01
R15 13 CRUDE, VACUUM 01 366
CAS 1*. 64741726 Trade Secret t 1
Chea Nate: POLYMERIZATION NAPHTHA
LA Code: 1X3 Pure [ 1 Mixture 1 3 Solid CX3 Liquid t ] Gas
X Fire X SROP
React
Acute X Chron
04
R25 CAT POLY 04 366
CAS t: 1310583 Trade Secret [ 3
Chea Naae: POTASSIUM HYDROXIDE
LA Code: 4010 [XJ Pure t 3 Mixture [I] Solid [ 1 Liquid [ ] Gas
Fire SROP React X Acute
X Chron
04
A24 PUMPHOUSE 01 366
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Chetical Description
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Storage Codes & Locations
Health Ha*. Daily Days
*** Non-Confidential *
Hazards Aeount Atount On-Site Code
Storage Locations
CAS t: 7722647 Trade Secret [ 3
Chei Nate: POTASSIUM PERMANGANATE
LA Code: 4024 CXJ Pure I 3 Mixture [XI Solid [ 1 Liquid [ 1 6as
X Fire SROP
X React X Acute X Chron
01
014 REFORMER 10 366
CAS l: 64741828 Trade Secret C 1
Chet Naae: PREMIUM COKER LIBHT CYCLE 8AS OIL LA Code:
C 3 Pure CXI Mixture I 3 Solid [13 Liquid I I Gas
X Fi-e
X SROP React
X Acute X Chron
06
A14 PUMPHOUSE A25 PREMIUM COKER
A25 <6,7,8 HDS 05 366
CAS #: N/A
Trade Secret t 3
Chet Naee: PROCHEM 2N2
LA Code: I 3 Pure 1X3 Mixture [ 3 Solid 1X3 Liquid [ 3 Gas
X Fire SROP React
X Acute
X Chron
03
AI4 REFORMER 00 366
CAS I: N/A
Trade Secret [ 3
Chei Naee: PROCHEM 2K30
LA Code: EI3 Pure I 3 Mixture [ 3 Solid CXI Liquid [ } Gas
X Fire SROP
React X Acute
Chron
02
A14 <3 CRUDE, VACUUM 00 366
CAS t: N/A
Trade Secret L 3
Chea Naae: PROCHEM 4H3
LA Code:
[ 3 Pure 1X3 Mixture I 3 Solid m Liquid I 3 Gas
X Fire
SROP React X Acute
X Chron
01
A14 43 CRUDE, VACUUM 00 366
CAS t: 74786 Trade Secret I 3
Chet Kate: PROPANE
LA Code: 4052 [X] Pure t 3 Mixture I 3 Solid CXI Liquid l 3 Sas
X Fire X SROP
React Acute Chron
05
A24 PUMPHOUSE A25 PRODUCT FRAC
05 366
CAS C 68512914 Trade Secret C 3
Chet Naee: PROPANE-BUTANE INTERMEDIA TE STREAM LA Code: 7163
I 3 Pure CX3 Mixture [ 3 Solid CX3 Liquid [ ] Gas
X Fire X SROP
React Acute X Chron
06
R25 SULPHUR PLANT R25 CRYO R25 GRP
06 366 R25 13 CRUDE. VACUUM
CAS '. 68512914 Trade Secret l 3
Chet Nate: PROPANE-BUTANE MIXTURE
LA Code: 7163 C 3 Pure CX3 Mixture [ 3 Solid 1X3 Liquid t 3 Gas
X Fire X SROP
React X Acute
Chron
07
A24 REFINERY WIDE 06 366
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Phys. tt
Avq. No. o<
Storage Codes 4 Locations
Health Max. Daily Days
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Hazards Aiount Aaount On-Site Code
Storage Locations
CAS I: 749B6 Trade Secret [ I
Chei Kate: PROPANE INTERMEDIATE STRE AH LA Code: 4052
t I Pure [XI Mixture ( 3 Solid m Liquid C 3 Gas
X Fire
X SROP React
Acute X Chron
05
R25 THERMAL UNIT R25 ALKY UNIT
R25 FCC 05 266 R25 CAT POLY
R25 GRP
jc
CAS 4: N/A
Trade Secret [ 1
Chet Naie: PSA ADSORBENT H-l
LA Code: 7048 [ 3 Pure U3 Mixture
CXI Solid I 1 Liquid t 3 Gas
Fire X SROP X React X Acute X Chron
03
R25 *6,7,8 HOS 03 366
CAS 4: N/A
Trade Secret [ 1
X Fire
fjo Chen Naie: RICH SPONGE OIL
X SROP React
LA Code:
X Acute
CX3 Pure C 1 Mixture
X Chron
[ I Solid CXI Liquid [ 1 Gas
R25 GRP 366
CAS 4: N/A
Trade Secret C 1
Chen Naie: SAFETY-KLEEN 165 SOLVENTMS
LA Code: C I Fure CXI Mixture C 3 Solid CXI Liquid [ 3 Gas
X Fire SROP React
X Acute X Chron
02
014 REFINERY HIDE 02 366
CAS 4: 69013214 Trade Secret C 3
(Jo X Fire Chei Naie: SHELL BLENDED PYROLYSIS P SROP ITCH React 06
LA Code: 8462 X Acute
CX3 Pure f 3 Mixture
X Chron
C 3 Solid CX3 Liquid C 1 Gas
A15 PREMIUM COKER A15 46,7,8 HDS
05 266
CAS 4*. N/A
Trade Secret [ 1
Chei Naie: SHELL CATALYST 424
LA Code: 8500 l 3 Pure 1X3 Mixture
[XT Solid [ 3 Liquid C 3 Gas
Fire X SROP
React X Acute X Chron
04
R25 * 1 lc 2 HDS R25 46,7,8 HDS R25 14,5 HDS 04 366
CAS fl: N/A
Trade Secret C 3
Chei Naie: SHELL CATALYST 444
LA Code: 8496 [ 3 Pure [XI Mixture
1X1 Solid C 1 Liquid l 1 Gas
X Fire X SROP
React
X Acute X Chron
R25 46,7,0 HDS R25 14,5 HOS
04 366
CAS t: N/fi
Trade Secret [ ]
Che* Naie: SHELL CATALYST 514
LA Code: 8497 [ 3 Pure [X] Mixture IX] Solid C 3 Liquid [ 3 Gas
X Fire SROP React
X Acute X Chron
03
R25 f 1 t 2 HDS R25 46,7,8 HDS
R25 #4,5' HDS
03 366
SAL 000006053
CONOCO REFINERY, NESTLAKE.LA.
Cheaical Description
Phys. A
Awj. No. of
Storage Codes 6 Locations
Health Max. Daily Days
** Son-Confidential m
Hazards Aaount Aaount On-Site Code
Storage Locations
CAS l: N/A
Trade Secret t ]
Chea Nae: SHELL CATALYST 544
LA Code: 9498 t 3 Pure X3 Mixture
.1X1 Solid C 1 Liquid l I Gas
X Fire
SROP React X Acute Chron
#2
R25 14.5 HDS 82 366
CAS 1: 63231674 Trade Secret C 3
Che* Nate: SILICA 6EL-N40f
LA Code: 4241 I 1 Pure UJ Mixture m Solid [ 1 Liquid t 1 Sas
Fire C SROP X React
l Acute Chron
#2
R25 CRYO
82 366
1
CAS t: N7A
Trade Secret I 1
Chea Naie: SL1HICIDE C-31
LA Code:
( 1 Pure CX3 Mixture l ] Solid m Liquid { 1 Sas
X Fire
SROP React X Acute X Chron
13
A14 UTILITIES, BENINERAtIZER, COOLING T 00 366
CAS i: N/A
Trade Secret [ 1
Chea Naae: SLIMICIDE C-41
to LA Code:
I 3 Pure m Mixture I 3 Solid m Liquid I 3 Bas
X Fire SROP
React X Acute
Chron
93
A14 UTILITIES, BEHINERAUZER, COOLING T 00 366
CAS #: N/fi
Trade Secret C 3
Chea Mane: SLOP OIL
LA Code: [ 3 Pure 1X3 Mixture t 1 Solid m Liquid t 3 Bas
X Fire SROP
React X Acute X Chron
05
AI4 RUN-DQHN AREA A14 12 CRUDE AM TRAPS
04 366
CAS 4; 4741624 Trade Secret l 3
X Fire
Chea Naae: SLURRY Oil
X SROP
to
LA Code: 8468
React 98 Acute
in Pure 1 3 Mixture
X Chron
l 3 Solid m Liquid l 1 Bas
A14 RUN-DQNN AREA
A15 SOUTH TANK FARM R25 FCC
07 366 R25 *6,7,8 HDS
CAS t: 497198 Trade Secret t 1
No Chea Naae: SODIUM CARBONATE LA Code: 7222 CU Pure C 3 Mixture m Solid t 1 Liquid I 1 Sas
Fire SROP
React X Acute
Chron
82
DM REFINERY HIDE 00 366
CAS 4; 7775146 Trade Secret l 3
Che* Nate: SODIUM HYDROSULFITE
LA Code: 4357 HI Pure t 3 Mixture EX3 Solid l ) liquid [ 1 Gas
X Fire
SROP X React I Acute
Chron
03
A14 REFINERY HIDE D14 REFINERY HIDE
81 366
SAL 000006054
CONOCO REFINERY, NESTLAKE,LA.
ChMical Description
Phys. k
Avo. No. of
Storaae Codes 6 Locations
Health Max. Daily Days
Ron-Confidential *
Hazards Aaount Aiount On-Site Code
Storage Locations
CAS l: 1310732 Trade Secret E 3
Che* Na*e: SODIUM HYDROXIDE
LA Code: 4359 EX] Pure E 1 Mixture CX3 Solid EX1 Liquid E 3 Gas
Fi-e
SROP React I Acute X Chran
05
A24 REFINERY HIDE 624 PUHPw0U5t 03 366
CAS t: 7558B07 Trade Secret l 1
Che* Naee: SODIUM PHOSPHATE. NON08AS
IC LA Code: 4396
EX3 Pure l 3 Mixture E 1 Solid EX3 Liquid E 3 6as
CAS : N/A
Trade Secret l I
Chei Naee: SOUR HATER STRIPPER ACID
SAS LA Code: 8476
C 3 Pure CXI Mixture C 3 Solid E ) Liquid IU Sas
Fire SROP React X Acute Chron
X Fire X SROP
React X Acute X Chron
03 #4
A14 PRODUCT FRAC A14 GRP 02 366
R25 SULPHJR PLANT R25 FCC 04 366
CAS : N/A
Trade Secret E 3
Che* Nate: SOUR HATER HASTE STREAMS
LA Code:
E 3 Pure EX3 Mixture E 3 Solid EX] Liquid ! ] Sas
Fire X SROP
React I Acute X Chron
06
A14 PUMPHOUSE A25 ACID PLANT A2S 42 CRUDE #4 366 A25 REFORMER A25 PREMIUM COKER
A25 SOUR CRUDE COKER A25 43 CRUDE, VACUUM
CAS 4: N/fi
Trade Secret [ 3
Chet Naae: P6 SOUTHWEST SILICONE B10
025 - COKER ANTIFOAM LA Code: 8444
i 3 Pure EX3 Mixture E 3 Solid EXI Liquid E ] Gas
X Fire SROP
React X Acute X Chron
02
014 SOUR CRUDE COKER 01 366
CAS t: N/fi
Trade Secret E 1
Chea Naee: SPECIAL FUEL OIL
LA Code:
l 3 Pure 1X3 Mixture E 3 Solid EX3 Liquid E 3 Gas
X Fire SROP React
Acute X Chron
05
A14 PUMPHOUSE 04 366
CAS S: N/fi
Trade Secret E I
Chea Nate: SPENT CAUSTIC
LA Code: L ) Pure L X J Mixture E 3 Solid EX] Liquid E 3 Gas
X Fire
X SROP X React X Acute
Chron
04
A25 ALKY UNIT A14 SULPHUR PLANT
A25 PRODUCT FRAC 02 366 A25 TRAPS
A25 GRP
CAS 4; N/fi
Trade Secret E 3
Chea Nate: SPENT FLUID CATALYTIC CRA CKIN8 CATALYST LA Code: 3494
E 3 Pure EX3 Mixture 1X3 Solid E 3 Liquid E 3 Gas
Fire SROP
React X Acute X Chron
04
H14 FCC 04 366
faO^ 00
CONOCO REFINERY, WESTLAKE,LA.
Cheaical Description
Phvs. 1
Avq. No. of
Storage Codes 6 Locations
Health Max. Daily Days
*** Non-Confidential *
Hazards Atount Atount On-Site Code
Storage Locations
CAS #: N/A
Trade Secret E 3
Chet Mace: SPENT HYDROTREATING CATAL YST LA Code: 6495
C ] Pure EX] Mixture EX3 Solid E I Liquid C 3 Gas
X Fi-e SROP
X React X Acute X Chron
04
D14 1 1 i 2 HDS 3J14 #6,7,8 HDS 014 44,5 HDS 04 366
CAS I: 7664939 Trade Secret E ]
Cfcec Nate: SPENT SULFURIC ACID
LA Code: 4519 [XI Pure C 3 Mixture [ ] Solid m Liquid I 1 Gas
X Fire SR3P
X React X Acute
Chron
05
A24 ALKY UNIT A24 ACID PLANT 05 366
CAS : N/A
Trade Secret E 1
Chea Nate: STABILIZER OVERHEAD USUI C LA Code: 8481
[ 3 Pure [XJ Mixture I 3 Solid Eli Liquid ( 1 Gas
X Fire
X SROP React
X Acute X Chron
04
R24 REFORMER R24 43 REFORMER
04 366
CAS t: 64741431 Trade Secret t 3
Ches Nate: STRAIGHT RUN 6AS OIL/ VIR GIN GAS OIL LA Code: 8479
U3 Pure C 3 Mixture [ 3 Solid 1X3 Liquid I 3 Gas
X Fire X SROP
React
Acute X Chron
05
R25 42 CRUDE R25 13 CRUDE, VACUUM
05 366
CAS : 64741442 Trade Secret E 3
Chet Nate: STRAIGHT RUN MIDDLE DISTI LLATE LA Code: 7717
U3 Pure l 3 Mixture f 3 Solid EX] Liquid E 1 Gas
X Fire X SROP
React X Acute X Chron
06
A14 SOUTH TANK FARM R25 42 CRUDE
R25 REFORMER 06 366 R25 43 CRUDE, VACUUM
CAS 1: 7704349 Trade Secret C 3
Ches Nate: SULFUR
LA Code: 4496 CX3 Pure [ 1 Mixture [ 3 Solid CX3 Liquid C 3 Gas
X Fire SROP React
X Acute Chron
05
B15 SULPHUR PLANT 04 366
CAS 1: 7446095 Trade Secret E 3
Chet Mate: SULFUR DIOXIDE
LA Code: 450! [X3 Pure t 3 Mixture [ 3 Solid E 3 Liquid EXJ Gas
Fire X SROP
X React X Acute X Cnron
03
R25 PCWER PLANT R25 ACID PLANT
R25 SULPHJft PLANT
03 366
CAS t: 7664939 Trade Secret E 3
Chet Nate: SULFURIC ACID
LA Cade: 4509 EX3 Pure E 3 Mixture [ 3 Solid m Li Quid E 3 Gas
X Fire SROP
X React X Acute
Chron
05
A24 POWER PLANT
A24 ALKY UNIT
A24 ACID PLANT 05 366 A14 TRAPS
A14 C00LI4G TONER-SOUR CRUDE
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CONOCO REFINERY, NESTLAKE.LA.
Cheaical Description
Phys. 4
Avq. No. of
Storaoe Codes 4 Locations
Health Max. Daily Day*
** Non-Confidential **
Hazard? Acount Aaount On-Site Code
Storaoe Locations
CAS f: K/A
Trade Secret [ 3
Che* Nate: SULFURIC ACID ALKYLATION NET BLONDQHN SAS LA Code!
U3 Pure [ 1 Mixture
t 3 Solid t 3 Liquid 1X3 Sas
CAS t: N/A
Trade Secret I 3
Che* Naae: SULFURIC ACID CATALYST
LA Code: 71388 [ 3 Pure [X] Mixture IXI Solid I 3 Liquid I 3 Gas
X Fire
X SROP X React X Acute X Chron
82
Fire
X SROP React
X Acute X Chron
83
R25 ALKY UNIT 02 366
R25 ACID PLANT 03 366
CAS *: 744611? Trade Secret I I
Che* Naie: SULFUR TRIGXIDE
LA Code! 4587 tX3 Pure I 3 Mixture I 3 Solid I 3 Liquid m 6as
Fire SROP X React
X Acute Chron
83
R25 ACID PLANT R25 SULPHUR PLANT
03 366
CAS t: N/A
Trade Secret I 1
Che* Naie; SUPER UNLEADED GASOLINE
LA Code: 2464 I 3 Pure 1X3 Mixture
t 3 Solid 1X3 Liquid t 1 Gas
CAS *: 64741873 Trade Secret I 3
Che* Naee: SWEETENED NAPHTHA
LA Code*. 1X3 Pure C 3 Mixture [ 3 Solid 1X3 Liquid I I Gas
X Fire
SROP React Acute X Chron
87
X Fire SROP
React X Acute X Chron
85
A14 RUK-DQMN AREA A14 EAST TANK FARM 06 366
A14 RUN-DOWN AREA R24 REFORMER 05 366
CAS t: N/A
Trade Secret I 3
Che* Naee*. TAIL GAS STREAMS
LA Code: 8488 { 3 Pure 1X3 Mixture l 3 Solid C 3 Liquid m 6as
X Fire
I SROP React
I Acute X Chron
86
R15 REFINERY WIDE 06 366
CAS V. 78882 Trade Secret t 3
Che* Naae: TETRAETHYL LEAD
LA Code: 4686
1X3 Pure [ 3 Mixture
C 3 Solid IX) Liquid C 3 Gas
CAS t: 64741886 Trade Secret I 3
Che* Naae: THERMAL CRACKED RESID
LA Code: 8469 [X3 Pure [ 3 Mixture [ 3 Solid m Liquid [ 3 Gas
X Fire
SROP React X Acute X Chran
84
X Fire SROP
React X Acute
X Chron
07
A34 PUMPHOUSE 02 366
AI4 THERMAL UNIT A14 PREMIUM COKER 06 366
SAL 000006057
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Cheaical Description
Phys. &
Avq. No. of
Storage Codes k Locations
Health Max. Daily Days
Ron-Confidential *t#
Hazards Arount Aaount On-site Code
Storage Locations
CAS l: 7550458 Trade Secret [ I
Chea Naae: TITANIUM TETRACHLORIDE
LA Code: 4723 [II Pure [ I Mixture m Solid t ] Liquid C J Gas
Fire
SROP I React I Acute
Chron
01
A14 CDR 01 366
CAS 4: 12003133 Trade Secret [ 1
Chea Naae: TITANIUM TRICHLORIDE AA
LA Code: [ 3 Pure [XI Mixture [ I Solid m Liquid [ 3 Gas
Fire I SROP I React
1 Acute Chron
02
A24 CDR
00 366
1
CAS *: 108B83 Trade Secret [ 3
X Fire
Chea Naae: TOLUENE 0
SROP React 01
LA Code: 4733 I Acute
m Pure C 3 Mixture
X Chron
[ 3 Solid CI3 Liquid t 3 Gas
D14 LAB 01 366
CAS #: N/A
Trade Secret I 1
I Fire
Chea Naae: TOLUENE STANDARDIZATION F SROP
0 UELS
LA Code:
React 01 I Acute
[ ] Pure [I] Mixture
Chron
[ 3 Solid m Liquid [ 3 Gas
D14 LAB 00 366
CAS l: N/A
Trade Secret [ 3
Chea Naae: TRANSPORT-PLUS 7200
LA Code: 7052 L 1 Pure UI Mixture [ 3 Solid [I] Liquid t 3 Gas
Fire SROP React I Acute Chron
03
A14 POWER PLANT 00 366
CAS S: N/A
Trade Secret E I
Chea Naae: TRANSPORT PLUS 7201
LA Code: t 3 Pure [13 Mixture I I Solid ill Liquid E 3 Gas
Fire
SROP React
I Acute Chron
03
A14 POWER PLANT 01 366
CAS : N/fi
Trade Secret t 3
Chea Naae: TRETOLITE D5-505
LA Code: \X) Pure l 3 Mixture E 3 Solid [13 Liquid C ] Gas
X Fire
SROP
React X Acute t Chron
01
214 ALKY UNIT 00 366
CAS 4: 12103133 Trade Secret t ]
Chea Naae: TRICAR60NYL HETHYLCYCLOPE NTfiDlENYL MANGANESE LA Code: 2?67
1X3 Pure E 3 Mixture C ] Solid CX3 Liquid I 3 Gas
X Fire SROP
React X Acute
Chron
03
A14 PUMPHOUSE 02 366
SAL 000006058
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CONOCO REFINERY, NESTLAKE.LA.
Chetical Description
PhV5. i
Avq. No. of
Storage Codes & Locations
Health Max. Daily Days
* Non-Confidential ***
Hazards Arount Atount On-Site Code
Storage Locations
CAS l: 74131 Trade Secret t 3
Chet Nate: 1,1,2-TRICHLOROTRIFLUOROE THANE LA Code: 0018
U3 Pure [ 3 Mixture [ 3 Solid HI Liquid 1 3 Gas
Fire
SROP React X Acute
Chron
01
D14 LAB 81 344
CAS i: 112274 Trade Secret I I
Chet Nate: TRIETHYLENE GLYCOL
LA Code: 4798 1X3 Pure t 3 Mixture [ 3 Solid [13 Liquid [ 3 Gas
Fire SROP
React X Acute
Chron
03
A14 PRODUCT FRAC 01 344
CAS #: 7563B Trade Secret t 1
Chet Nate: TRIFLUORQBROflQMETHANE
LA Code: 4494 IX] Pure t 3 Mixture { 1 Solid [ ] Liquid HJ Gas
Fire X SROP
React Acute Chron
02
A24 PUMPHOUSE A24 LAB A24 CALCINER
82 344 A24 SC/RC CONTROL
A24 43 CTU CONTROL
CAS *: N/A
Trade Secret t 3
dies Nate: TRILOBE HDN-3# CATALYST
LA Code: 8492
( ] Pure 1X3 Mixture [XI Solid C 1 Liquid i 3 Gas
Fire
X SROP React
X Acute X Chron
04
R25 t 1 l 2 HDS 03 346
CAS *: N/A
Trade Secret t 1
Chet Naae: TURBINE OIL
LA Code:__
1X3 Pure [ 3 Mixture
~~
[ 1 Solid CX} Liquid C 3 Gas
X Fire SROP React
Acute X Chron
02
014 REFINERY NIDE 01 346
CAS *: N/A
Trade Secret C 3
Che* Nate: UCARSQL SOLVENT HS-101
LA Code: 8427 L 3 Pure tX3 Mixture [ 3 Solid CXI Liquid [ 3 Gas
X Fire
SROP React X Acute Chron
03
A14 SULPHUR PLANT 02 344
CAS *: N/A
Trade Secret [ 3
Chea Nate: UNION CARBIDE MOLECULAR S IEVE TYPE 3AEPG
LA Code: [ ] Pure [XI Mixture
U3 Solid [ ) Liquid [ 1 Gas
Fire
SROP React l Acute X Chron
01
A25 CRYO 08 344
CAS #: N/A
Trade Secret I 1
A25 CRYC
Chet Nate: UNION CARBIDE MOLECULAR S IEVE TYPE 13XPG LA Code:
t 1 Pure [X3 Mixture [X3 Solid [ 1 Liquid t 3 Sas
SROP React X Acute
Chron
01
00 344
SAL 000006059
CONOCO REFINERY, NESTLAKE,LA.
Che*ical Description
Phvs. &
Avq. No. o<
Storage Codes & Locations
Health Max. Daily Days
*** Non-ConFidential +
Hazards Aount Aeount On-Site Code
Storage Locations
CAS t: N/A
Trade Secret C I
Che# Rate: UNLEADED GASOLINE
LA Code: 2464
[ 1 Pure CXI Mixture [ 1 Solid CXI Liquid l I Gas
X Fire SRQP
React Acute X Chron
07
A14 RUN-DOWN AREA A14 EAST TANK FARM
06 366
CAS : N/A
Trade Secret t 3
Ctiea Naae; UOP TYPE R-32 CATALYST
LA Code: 8490
C 1 Pure CX3 Mixture m Solid [ I Liquid C 1 6as
Fire
X SROP React
I Acute Chron
03
R25 3 REFORMER D14 WAREHOUSE
03 366
CAS i: N/A
Trade Secret [ 1
Che# Nate; UOP TYPE SPA-t AND SPA-2
LA Code: 8491 [13 Pure [ 3 Mixture
[X3 Solid [ 3 Liquid C 3 Gas
Fire I SRQP X React X Acute
Chron
03
R25 CAT PDLY D14 WAREHOUSE 03 366
CAS i: 64741566 Trade Secret C 3
Che# Naae: VACUUM RESIDUUM
LA Code: 8467 [X] Pure E 3 Mixture [ 3 Solid m Liquid [ 1 Gas
X Fire SROP
React X Acute X Chron
07
A15 RUN-DOWN AREA A15 TANK FARM-SOUR CRUDE R35 13 CRUDE, VACUUM 07 366
CAS l: 64741497 Trade Secret 3
Chea Naae: VACUUM TOO CONDENSATE
LA Code: [ 3 Pure 1X3 Mixture [ 3 Solid [11 Liquid l 3 Gas
X Fire X SROP
React Acute X Chron
06
A25 43 CRUDE, VACUUM 04 366
CAS 4: N/A
Trade Secret [ 3
Che# Naae: VANLUBE SL
LA Code: 5872 1X3 Pure 1 Mixture [ 3 Solid X1 Liquid [ 1 Gas
X Fire SRQP React
X Acute Chmn
02
014 CDR 00 366
CAS 4: 64741598 Trade Secret t 1
Che# Naae: VIRGIN GAS OIL
LA Code: 8465 [XI Pure [ 3 Mixture [ ] Solid [XI Liquid [ 3 Gas
X Fire X SROP
React Acute
X Chron
07
A15 PUMPHOUSE
A25 #2 CRUDE A25 FCC 06 366 A25 13 CRUDE, VACUUM
CAS t: N/A
Trade Secret l 3
Chea Naae: VISTA NORMAL PARAFFIN
LA Code: 8507
[ I Pure [XI Mixture [ I Solid [XI Liquid [ I Gas
X Fire SROP React
X Acute
Chron
06
A14 PUMPHOUSE A14 EAST TANK FARM
05 366
SAL 000006060
CONOCO REFINERY, NESTLAKE,IA.
Cheiical Description
Phys. &
Avq. No. of
Storaae Codes & locations
Health Ha*. Daily Days
* Non-Confidential
Hazards Amount Amount On-Site Code
Storage locations
CAS : N/A
Trade Secret I 1
Chet Kane: HT-2&44
IA Code: 8457 II] Pure I I Mixture I ] Solid m Liquid I I Gas
Fire
SRQP React
X Acute Chron
03
A14 TRAPS #2 366
CAS l: 133927 Trade Secret [ 3
Chet Nate: XYLENE, NIXES ISOMERS
LA Code: 4985 IX] Pure C 3 Mixture I 1 Solid m Liquid I 1 Gas
X Fire SROP
React X Acute X Chron
01
014 LAS 01 366
Certification (Read and Sign After Completing All Sections)
I certify under penalty of law that I have personally examined ana aa familiar with the information submitted in this and attached documents, and that based on my inquiry of those individuals responsible for obtaining the infor mation, I believe that the submitted information is true, accurate and complete.
+ ----------------------------------------------------------------------- +
!! Optional Attachments (Check One)
I
I J +--+
i ! Ill have attached a site plan
5
I
II III have attached a list ofsite
I
I I +--+ coordinate abbreviations 11 tI
I
Ii
! 4-------------------------------------------------------------------------------------------------------+
Name and Official Title of Owner/Qperator OR Owner/Operator's authorized Representative
Signature
Date Signed
SAL 0006 061
/\fc
Afc
o Kf^>
4 -+
Emergency & Hazardous Chemical Inventory !
TIER TWO
!
,
Specific Information By Chemical
!
+--------------------------------------------------------------------------- +
For Official ID t: ..................... Use Only Date Received:
Reporting Period From January 1, to December 31, 1968
Facility Identification:
Emergency Contacts:
Name: CONOCO INC. - DOCKS Address: HIKE HOOK ROAD
City: WESTLAKE, LA 7*669-0000
Name: STEVE BROUILLARO Title: SAFETY DIRECTOR Phone: (318)491-5224
24 Hr Phone: (318)491-5301
SIC Code: 2911 Dun l Bradstreet #: 00-842-7692
Owner/Operator Information:
Name: DON R. UNRIIH Address: F.Q. BOX 37
Name: DOUG FREY
Title: SAFETY fc HEALTH SUPERVISOR
Phone: (318)491-5023 24 Hr Phone: (318)491-5301
City: WESTLAKE. LA 70669-0000 Phone: (318)491-5222
CONOCO DOCKS, WESTLAKE, LA.
Chemical Description
Phys. It
Avg. Mo. of
Storage Codes & Locations
Health Max. Daily Days
* Nan-Confidential **
Hazards Amount Amount On-Site Code
Storage Locations
CAS t: N/A
Trade Secret I ]
Chem Name: ALFOL 410<ADE,AFC,DBC,BDE ) ALCOHOL
LA Code: 8510 I ] Pure (XI Mixture [ 1 Solid II] Liquid 1 ] Gas
X Fire SROP React
X Acute X Chron
06
A14 DOCKS 06 366
CAS *: N/A
Trade Secret C ]
Chea Name: ALFOL 810, ALFOL 810-FD A LCOHOL
LA Code: 850B I I Pure IX] Mixture
I 3 Solid [X] Liquid I ] 6as
X Fire SROP React
I Acute X Chron
06
A14 DOCKS 05 366
CAS I: 107062 Trade Secret [ 3
Chem Name: 1,2-DICHLGROETHANE
LA Code: 2271 CX3 Pure ( 3 Mixture I 3 Solid CXI Liquid { 3 Gas
X Fire
SROP React X Acute X Chron
04
A14 DOCKS 03 366
CAS : 68512618 Trade Secret I 3
Chem Name: HEAVY PREMIUM COKER GAS 0 IL LA Code: 8464
1X3 Pure I 3 Mixture [ 3 Solid m Liquid C 3 Gas
X Fire SROP
React Acute X Chron
06
A14 DOCKS 05 366
CAS t: 123319 Trade Secret [ 3
Chen Name: HYBRQGUINONE
LA Code: 2658 [ XJ Pure [ ) Mixture I 3 Solid [X] Liquid t I Gas
Fire
SROP React
X Acute Chron
01
R14 DOCKS 00 366
feO&Z 00
(Md
/Vs
:ONOCQ DOCKS, WESTLAKE, LA.
Cheaical Description
Phys. 1
Avq. No. of
Storage Codes 6 Locations
Health Max. Daily Days
** Ron-Confidential **
Hazards Affount Aaount On-Site Code
Storage Locations
CAS t: 67561 Trade Secret t 3
Chea Naae: METHANOL
- LA Code: 3075 [X3 Pure [ 3 Mixture ( ] Solid [X3 Liquid t 1 Gas
1 Fire SROP React
1 Acute X Chron
05
A14 DOCKS 05 366
CAS 1: 64741420 Trade Secret [ 3
Che* Hate: NAPHTHA
LA Code: 3394 [ 1 Pure [13 Mixture [ 3 Solid [13 Liquid [ 3 Gas
1 Fire 1 SROP
React I Acute 1 Chron
07
A14 DOCKS
85 366
4
CAS #: 1336363 Trade Secret [ 3
Chea Naie: POLYCHLORINATED BIPHENYLS
LA Code: 3952 m Pure [ 3 Mixture [ 3 Solid [13 Liquid [ 3 Gas
Fire
SROP React 1 Acute
X Chron
01
R15 DOCKS 01 366
CAS *: 64741566 Trade Secret [ 1
Chet Nate: VACUUM RESIDUUM
LA Code: 8467 [13 Pure [ 3 Mixture [ 1 Solid U1 Liquid [ 1 Gas
X Fire SROP React
I Acute X Chron
06
A15 DOCKS 85 366
CAS 1: 75014 Trade Secret [ 3
Chea Nate: VINYL CHLORIDE
LA Code: 4943 (13 Pure [ 3 Mixture C 3 Solid [13 Liquid [ 3 Gas
1 Fire 1 SROP
React 1 Acute
X Chron
06
R24 DOCKS 04 366
CAS t: 6774747 Trade Secret [ 3
Che* Nate: VTSTA NALKYLENE 550L DETE RBENT ALKYLATE LA Code: 8589
[ 3 Pure [13 Hixture t 3 Solid [13 Liquid [ 3 Gas
X Fire SROP React
X Acute Chron
06
A14 DOCKS 05 366
CAS t: 68648873 Trade Secret I 3
Chea Naae: VISTA NALKYLENE 680L DETE RGENT ALKYLATE LA Code: B511
[ 3 Pure 1X3 Mixture C 3 Solid m Liquid [ 3 Gas
Fire SROP React
1 Acute
Chron
05
A14 DOCKS 85 366
CAS t; N/fi
Trade Secret t 1
Chea Haael VISTA NORMAL PARAFFIN
LA Code: 8587 l 3 Pure 1X3 Mixture [ 3 Solid CXI Liquid [ 3 Safi
1 Fire SROP React
I Acute
Chron
06
A14 COCKS 06 366
SAL 000006063
CONOCO DOCKS, WESTLAKE, LA.
Chemical Description
Phys. It
Avq. No. of
Storage Codes fc Locations
Health Max. Daily Days
** Non-Confidential *o
Hazards Arount Amount On-Site Code
Storage Locations
CAS t: 8410968 Trade Secret t 1
Chet Name: VISTA NFSO SOLVENT
LA Code: [ ] Pure [X] Mixture [ ] Solid CXI Liquid [ 1 Gas
X Fire
SROP React
X Acute X Chron
*3
A14 DOCKS 02 366
t----------------------------------------------------------------+
! Certification (Read and Sign After Coipleting All !
! Sections)
II
I
11
! I certify under penalty of law that I have
!
I personally exaiined and ai failliar with the
!
! information subaitted in this andattached
!
! documents, and that based on my inquiry of those !
! individuals responsible for obtaining the infor- !
! mation, I believe thatthe subaittedinformation ! +
! is true, accurateand cosplete.
!
Optional Attachments (Check One)
+--+
!! (I I !: +--+
I have attached a site plan
I have attached a list of site coordinate abbreviations
Name and Official Title of Owner/Operator OR Owner/Operator's authorized Representative
1 Signature
Date Signed !
t-------------------------------------------------------------------------- +
|
i ll ! !
a 1
SAL 000006064
APPENDIX E PROCESS. STREAM COMPOSITION DATA
SARA TITLE III, SECTION 313 1988 TOXIC CHEMICAL RELEASE INVENTORY
LAKE CHARLES REFINERY
sal
ooo 606S
STREAM
FCC Tail Gas . P-B P-P B-B Cryo Tail Gas Cat Poly Charge Alky/Cryo Feed A1ky Tail Gas Coker Wet Gas Cryo Liquid B-B to MTBE MTBE DH Poly OH SWS OH Fuel Gas
GAS PROCESS STREAM COMPOSITION Lake Charles
(1)
Ethvlene 16 BD BD BD 15 BD BD BD 1 BD BD BD BD 9 3.6
COMPOSITION <wt 7.)
Proovlene
1.3-Butad
N
o
12
33 0- 2
68 0.3
5 0.3
7 BD
50 0. 1
8 0.3
30 BD
7 0. 1
5 BD
5 0.4
5 0. 3
20 0. 1
25 0. 1
5 0. 3
( 1) Based on Ponca City TSL Report "Annual Summary o-f GC Data,1987"
(2) Carcinogen ( de minimus = 0.1 wt '/.)
(3)
by 6:11 Pete
PED fences
cm 000006066
CALC-oc^TiOiV F vvTV*
.
CoNo&NTRA-rioW FcR Ms streams
) Fc-^- ~r&tc_ g-4s
^e,
= '7.5* ih
}Ofrcl % c~
* . zs
,I 7--,^,--TT/> ^ -R^r. .G,
- \(o vvt% C.
SV*l%<r5 X _^L_ =
/ 7.?
C5
O' I r*ol /o 31i ^ S*~(
Tir
i) Rlc
ft - &
^
0.7. ~i% = VV.
Cl / wio/ A Oj,
X ~ZJS ?V.3.
~ ^ I wf-^ O.
% Cj
x -
yy.3
l^wtX c
O. 2, rv^>( % BO y
5) Foe p-p
W.3 A1
% ^/)O.Z- vv"/
= Vo
6^ v^rA 0/ X -^|-
6s
c
O.^-oct/% w V 51L ^ Ho
O.^ wf% 6/> -----------------------------------
6) Po^ccv O+y olccb
***>!%.
~fo c/c'f^.Ve rf- --fa resold w<*. rv^f" ^
~jo ^vi~ 4 R&yo'>*<i
^
SAL 000006067
4) Fee, B-&
7 wo/ %> <c3~ X-
= S3,
= 5~^tya c3~
BD x Si. - o.i wf 4. Bh
S(p
______________________
*)CRVo~\/Ru T4IL &AS
mvJ i ,<*
10 *>/ % Ca * ici . /s-wf-% Ct~
3 -=/ % cf x ^ ^ y vdy. cy
(*) 3/f7~ PolY CHARg-E.
0]W^v
^-2.
5& *^>o/ /a
X"
-- $23 wi 4
O.I -1^ BO x SO - 0,1 vvf% SB
7z-
-7) fl-LKj/CKyo FEEb
h^Av= 5-i
Io ^o( 4 c - x iL ^ % wO 4 c,~
57
-------------------------
o.z not % BO X Si tr (7.3
B
OV
----------------------------- ---------
*) i i 3i
o.H^ri C~X f~ = <) wf%C7
3Z mo(%
X ^ x 3o
~
P. c.
000006068 SAL
i) CqkeR vver <s-A-s
~2-- /y\o} / -X. zs
V3
I wt-% C-
7 IX C- x ^ -- 7
C
O./ % BO x _5l - 0,1 *f% SO vs ----------------
to) CR^o liqoiO
= HS
5~ >~l % C% x i?: - S wt/o O ~
Vs
;0 fnr&E e-e>
C~ = S rh%
;) RWBB__OR
c~ - SwiV*
V>D = O,
i) Cft-r Poly oH
= ^3
20 o^j I fa
X" ^ - -zo wi'% C
0.1 ~v/% > X Jl. - >,/ wf% )
n) Sot;^ ^AteR stripped OH
*-j s*\oi
(2Z
7J5 7a
OJ /vwf % &>
SAL 000006069
LIQUID PROCESS STREAM COMPOSITIONS Lake Charles
STREAM
Regular Gasoline Unleaded Gasoline Super UL Gasoline Sweet Crude Sour Crude Base Gasoline FCC Gasoline Casinghead Gasoline LSR Gasoline Reformate Coker Gasoline Crude Wet Gas Naphtha Jet-A 4*2 Distillate Kerosene Sabine HAD Conoco LVT Oil Thermal Gasoline PBC (Field)
* BNZ
T0L
COMPOSITION (wt X> ETB XYL CYHX CUM PCUM
NAPH
* STY
2.4 9.8
2.9 9.8
4. 1 9. 8
0. 32 BD
0. 23 BD
3. 0 9.8
1. 1 7.8
2. 1 5. 1
3. 9 3.0
7.2 18.5
0.3 4.0
0. 2
BD
1.0 4.5
BD BD
BD BD
BD BD
35. 0 15. 0
BD BD
1.0 4.0
1.3 3.2
2.7 2.7 2.7
BD BD 2.7 3. 0 1.2 BD 4.5 BD BD 1.0 BD BD BD 4.0 BD BD BD
13.0 13. 0 13.0
1.2 BD
13.0 19. 7
7. 9 BD
14.0 6. 5 BD 4.0 BD BD BD BD BD 6. 5 4. 9
BD BD BD BD BD BD 1.0 3. 7 5.2 BD 1.0 BD 2.0 BD BD BD BD BD 1.0 2.3
4.3 4.3 4.3
BD BD 4.3 5. 1 BD BD 6.8 1.0 BD BD BD BD BD BD BD 1.0 BD
2. 0 2. 0 2. 0
BD BD 2.0 3. 1 BD BD 1.7 3. 0 BD BD BD BD BD BD BD 3. 0 BD
BD BD BD BD BD BD BD 1.0 BD BD BD BD BD 3.0 3.0 3.0 6.0 3.0 BD BD
BD BD BD BD BD BD BD BD BD BD BD BD BD BD BD BD 10. 0 BD BD BD
* Carcinogen ( de minimus = 0.1 wt 7.)
SAL 000006070
LiGUtb P/tocESS Stream Compositions
Uo.(ce k<*r/e<> R^~fy
Benzene
<0) tis^ (SUs^^ <- - 3. CD ivf" /a
>a.se4
/<?^'c? L.C~.
/^ses )
t) Ae*)
-- 2-.^/ w"f% "2, ^fA-f/oecJ
~EEE fieparl'
c') U/_ Gt^Salr'l^^ -
2.,^ kvf% ( n-3,'2--g'S <r/yl W CUy-fr- Joe (t-n)
V, / wt^/a J bexsed OO
proolo<jf/o^ >~
f C.ul aASoi* '
3.o w^-%
/^fS0?
J.
^ (2-^ %)(o.'5<>) +
C. j^5a/'Vie
(n 8fc)
),<r wf 7 = L\A(>C_0^s) + (in/XAo) +
/f**7q /yj^S ")
o.zs)
o.zs
v+.b
/17
=?
t<m
^7
*a~-(iTCia)
z.1 = OnXl'~>)
l'^(nr>)
Y. / - CiAYCz-H)
sT^ 3^v/e^"f (En-'rfd
f) & ^
_/
0.^2 "2-3
/o w 7 /c.
loosed, o^ 1*1%*} <j- E&o c~ Cr~t-j A f
L.C. S^eeT /? O** fy c,P S /
^ FjC (5dS</tVc_ " /. f w'f_ ^ p Lsp GUso|/^e. - "3-3 ^% ^) Coke.r fi^Sdl^e - 3.3= ^Y
j ^ C <xS rv ^ In e <^cX (Rye* So, - 2.1 wf a/o
F) Pc"f~>(~rvio'Ac. ~ 3,2. vv^ /
(^ pe.r TJ^ ^7ye_rs -ZTOCL^ l/7/^#)
C <keSr<z r/in.' ^e d jby /^1-=iss ixWoinc^
o"f (Jc< <; o I >'m e /? n&lyse^>^ o. *cl
c*. sEjdy "P re-Fr'^^rva re<*c-/;oF
PESt
S4t ooo6o7i
LlQOiO Process STtfErf/V ComPosiTio/Vs Lake- CP a rje.% $e.4y
BenzePE C<->vdr'd ^
(Z^.t
'0,2
*o (pz-c /77/ fatncc* C>-iy
S^rve^ - *3>d>5~'0-2-?'/}
Ahph~ti\e\
"
r,)Zkf A kerlse^e
w't ft>
Cper iff*1 A^7yj-~5 XOC.J
o.'l
`/7/?s)
__ iOJ ,,tz ^ er T5<L to/.* B^Uc/B.H
'*
Use^
8Pr0
) S^b-Vie fj/fi)
-
^ 7rcO)a| ^S0l'`ner
3^.^ w+/4 {per PlsZJS-y/JSS 5ccin
>`
fippx $-)
(fpej- T'rv, ^yers
IOC;
"0 P/Sc CFte(d')
1/7/s*)
= 1.3 *1-% ( fx=j~ TS.C Ref>ci~ *^-Z?--2s)
\OL-UBNE
a~) ULJ SULJ &<se 6Wso/;^ - P.? wtVc (l!tl E.c. <SUs /*<= #r1e, /y se5 )
b) S^vee"f~ So^r Cr^et e - ^ 1
cT) FCC 6^so(/i^ -- V.? tvf%
d ") e "f~o r~/v^ cK~i~ EL --
is.S'^fVo
{o/cf^r^rcl
/n^ss k^/a*ic^
11^*7
Co^p^r^
*j/ Pel
sar/i s/3
*vi'e.\ (
Co^v,po<=,,'/"*'<3 ^ L,'-( &-r+i~vC. Se<* rc/^
SAL 000006072
TOLUENE-
LTQ,
STtfE-rifii Compositions
La\lce
CAa^/^5
Red
Y
Cca~id)
<^S) dc\.S
&c*& o/<V\< ' d,i
^nsff/oeJ
e.e, S'wee/ COcud^
e ~7'7__Tq / ferine ^ x
0,32- feu C<^r<scte)
OI '
4sv3.!y<,es ^
z 6s%~)^el') ~
(frie^E. COnc<?^yr*af,on5}
/ 7?/ (Tcs^M)
f) LSft (>^so / tV\^ --
5)Cker (?iSof.'hc: ~
k) A/p/r/A
-
3,0 tsvi 'Y*
H ,0 wl Yt
</,S~ *v1%
{per /?-?/ P.C. Sfr-e'. #**
Sur./ ey j 2,13 OS' - O- 2 - 7 ^
c') Cr<-*c(e. |a/^+
'3e'H-$
2 btsi~d(^fe^ KenoSene^ <LV'7"0,`[
<i
f Pei"
SNe^ Sursexf
OH, e Er\^{e! S',II lycoiselfe
CrsC) es-himaits )
j) S^L>.'ne hlfid ~ /5~,<3
^-er TiSfos -- filSS sCa^;
/?7^xr A ")
lc) ~J~h^i~r^a, ( 6^So|. ,,e - ^f,0 <*/f /
creu")
fiSiume S^./c^r "/ dk<J~ S^,%al,'nd)
0 P6C 6f,`e(j) -- 3*21, vV^ /l
^ ro.^> 0 o/T Rot *> j ^ o/
Ac\beK *^cl PBC /Cs^4
cXcT^
EfrHYeSe\/zEA/
"\ C2B ><JZ
; Jj
"
6R soh'ne - 3? .2 \o/f /a ^
Z < C . 0*^ 50 /* K (p /hn-fyiei')
b\ SivA , Sour druJr
Z) Foe (3^s^l,ne-
3,0 vvt %
Ow ^'c` ^ nq
iy g<*so/,vi^
lo&xUr\cZj ir cov^p^rr^ `V P_Z L.*'-/^"ic?r e S<2.<*rck)
SAL 000006073
LiQ, STHeAPI ComPcsfTtoNS
L.C,
/?e^i
ethl/l Benzene
d)
- ^.S~ wf /&
/ /*??/ P<C, S'fr'e***' Surrey \
\ <r rvj^^s h}*(#.nc^
J
&) iie^^
/j*2. w
^naf.voe^ off Z..C. S~f Coo^e. analysts &- t>e*iE. CancelW*,)
rrrr v2-,<5* &*>* l'18^
~p) LSPk C?t*$aI> *%Cj Eu>l<^ (Jra^ol^e^
/
P,CZ, Sdre#** -Survey
Cru^e IVef 6WSy 3e> * -*2 d&ifUtyy. ^( wf% ICeojse^e ^ LVT^: I }T^er^i trod) 1 (jU.se* I -v *^e
Ts(_
/
OzukeUe) es-A^/e^
^ tj^pk-tk^ * 1-0 <vf%
CB.&^eik es-fc^fe)
K) S^Lve hlAb^ y.O wf% (f /VS5- ///SS
4-^4),
t) PfeS ->'<?(ct
^ I % Xr^'f.oeci
0=is/'n^Ae^ .t
-ve>( P&C-^CTs^ Aie>( Pen^-, c/q"/^
XVLEA/f
a)
^ OLj SiULj B^e. 6kso/-'^e "
/3<0 vf X> (^ If^l
^ * (S** s^J*
<* ho/ySi' S ^)
b) Suyee'f Cruclf r
P2
X ^ (l*j%Gj ^ Clrod e
Sour <Z.rude
'
<-j ui~ V*
s*l 0006074
U.Q. STREfrfll Compositions
L.C. kefy
Xylene_ cConij')
C) f~CC.
c) Re-fW-^c*'/C.
-
*sf~/o
CHeA~ersHt'neel by gcL$o(tj\e /h^ts5
&r Cjor*\(pc*. Ti^_ck
P-SX
L.'ier-tfar^ Se^rcA)
i*~i,0 \*/i %
Cde'fern*;^^ by j<=tso/*Xe_
h^la^ce
ei^t{
B>. (ye^loeff^
) Ca$i A^he^d (jiiso/A'ie - 7,*7
^nerAopd
L.C,. SweeH cru^G
cmct bo-n'zBne CP^cerrfr<(f)\^
ii?__xy/-^^ ^1 ^>2 0n2 CcroJe)
^
p) C-o\czr ($Wso/.V\e_ = 6. ^ /o
~TL . r*v^( (l~COS) (r*.5ai`he (*SSuy*e 5'^,V`V' 1(3 CskpjJ
$H {cs^hdC) z ~7.^ Xy/
by ^5h'he
b)^/^MCe ^ *"''(
5. <?e
e^-b^vvpffe-)
3^ Z_5^? G-Cxso L'hej CruJ. e VVe^
^2. >tG5tl kknsseKe, Ll/rcst / sJ
= < / *vf%
P<< 5P"e*,^ Survey B.GeubeKe esWej
h) N^pln^h*
-= i-o ^tYo
B*(( (9cvieffc e.sL^Ye V-/?-2te)
<) S<\h
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0000060&0 SA'-
IUWJ
Interoffice Communication
TO:
Dave Kersey, Lake Charles Refinery
FROH:
Paul Steele, PED, Ponca City
DATE:
January 26, 1989
SUBJECT: SARA Title III, Section 313 - Solid Waste, Crude, and Gasoline Analyses
Attached are lists of 1) solid vaste and process stream samples that are needed for analysis and 2) the chemicals for which Che samples are to be analyzed. As previously discussed, the purpose of the analyses is to accurately report 1988 and future chemical release values as required by SARA Title III, Section 313.
The solid vaste samples should be sent to the Technical Services Lab in Ponca City. The samples should be labelled "SARA 313 Analysis" in the sample description to prevent confusion with other analyses performed by TSL. These samples are needed by February 28 to provide ample time for the analyses and evaluation of the data.
The crude oil and gasoline samples will be obtained by TSL through their normal procedures.
Research Services Division will provide support on Che volatile and semi-volatile organic analyses. A conservative preliminary estimate of $800-$1000-totaL cost, .per sample has been determined. A proposal is being prepared and will be forwarded to you prior to the analyses. A charge number will be needed from the refinery for RSD's participation.
Please contact me if you have any questions or expect any difficulty in meeting these requests.
Paul E. Steele Chemical Engineer Environmental Process Engineering Division
lk att cc:
DFM LWC KLK DDO OFE MMM DEL Jack Cearley, Houston Brandt Butler, Lake Charles Refinery
File EV-1040.1
Approved
Solid Waste: Crude Oil: Gasoline:
SARA 313 RAOTTJtt!
1. Biological Solids 2. API Separator Bottoms
A composite sample will be crude unit (No. 2 and No. sample will be performed.
requested by TSL for 3). An analysis of
each each
Samples of regular, unleaded, and super unleaded gasoline will be requested by TSL. These three samples will be blended proportionally, by the total volume of each produced in 1988, into one sample for analysis (35 vol% Reg, 40% UL, 25% SUL).
000 feO & 0 spS~
SARA 313 ANALYSES
Volatile Organj.??
Benzene S tyrene Ethyl Benzene Toluene Xylene 1-Hethylethyl Benzene 1,2,4-Trimethylbenzene Cyclohexane Biphenyl 1,2-Dibromoethane 1,2-Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Methyl Chloride Dichloromethane Methyl Ethyl Ketone Methyl t-Butyl Ether
Semi-Vol atile Orranlcs facid>
Cresol Phenol 2,4-Dimethylphenol
Semi-Volatile Oreanics ('base/neutral}
Anthracene Naphthalene Pyridine Quinoline o-Toluidine 2,6-Xylidine Aniline
X X X X X X X X X X X X X X X X X
X X X
X X X X X X X
Crude
X X X X X X X X X
Casolinft
X X X X X X X X X X X
X
X X X
XX XX XX XX XX XX XX
SAL 000006083
Metals
Aluminum Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Mercury Nickel Selenium Vanadium Zinc
Oreanic Metals
Org. Lead (TEL, TML) Org. Manganese (MMT)
SAIUL_313 ANALYSES
Solid Waste
X X X X X X
x x
X X X
x x x
X
Crude
on
X X
x
X X X
x
X X X X
x x x
X
XX
000608A SAL 00
1 J, ,1 INTEERRNNAATTIOIONNAAL I U y TECHNOLOGY f T 1 CORPORATION
ANALYTICAL SERVICES
CERTTHCATE OF ANALYSIS
CONOCO-LACE CHARLES REFINERY CONOCO, INC. P 0 ORAUER 1267 RE 346 PONCA CITY OK 74604 DON LINDER
Date: 04/18/69
Job Nuober: 449900
Uork Order: A9-03-095
This ie the Certificate of Analysis for the following saoples:
Client Work ID: SARA 313 ANALYSIS Date Received: 03/24/89 Nuober of Saoples: 2 Ssople Type: GASOLINE, CRUDE
TABLE OF CONTENTS FOR ANALYTICAL RESULTS
PAGES 3 5
LABORATORY SAWPLE IDENTIFICATION A9-03-095-01 PC 1498 SoOr A9-03-095-02 PC 1635 Gasoline.
t_>C. s--
33S5
I %% Re^}
Ho/0UL}
2.5% SOL)
Donnie L. Reinrich Laboratory Manager
American Council ol Independent Laboratories International Association of Environmental Testing Laboratones
American Association tor Laboratory Accreditation
IT Analytical Services. 5307 Industrial Oaks Boulevard, Austin, TX 78735
mi ie?
I
Company: CONOCO-LAKE CHARLES REFINERY ate: 04/16/69 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-095
Job Muaber: 449900
TEST NAME: HAZARDOUS SUBSTANCE VOLS SAMPLE 10: PC 1498 (S'ooC C-rude)
Results in
ag/kfi:
DATE COLLECTED: 02/10/69 OATE ANALYZEO: 03/30/89
COMPOUND
COMPOUND
acetone benzene 2-butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2-dichloroethane 1,1,1-trichloroethane 1,1*dfchloroethane 1,1,2-trichloroethane 1,1,2,2*tetrachloroethane chloroethane 2-chloroethylvinyl ether chlorofora 1,1-dichloroethylene trans*1,2*dichloroethylene 1,2-dfehloropropene cts-1,3-dichloropropene
<6600 2300
<6600 <330 <330 <330 <330 <330 <330 <330 <330 <660 <660 <330 <330 <330 <330 <330
trsns'1,3-dichloropropene ethylbenzene 2~hexanone aethylene chloride aethyl chloride aethyl broaide
broaofora broaodichloroaethane dibroaochloroaethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cuaene isoaers cyclohexane
<330 1900 <3300 <330 <660 <330 <3300 <330 <330 <330 <330 <330 5300 <330 <3300 <660 6200
650 <0.66
Coanents: A less than <<) indicates the coapound is not detected at the level indicated.
Page Z
SAL 000006086 >82-1-89
CMpany: CONOCO-LAKE CHARLES REFINERY Date: 04/18/09 Client Work 10: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN. TX
Uerk Order: A9-03-095
Job Nuaber: 449900
TEST NAME: ABN NSL CC/HS EXTRACTABLES
SAMPLE 10: PC 1498
Results i
*9/kg:
OATE COLLECTED: 02/10/89 DATE EXTRACTED: 04/03/89
DATE ANALYZED: 04/04/89
COMPOUND
Phenol
<8500
bis(2-Chloroethyl)ether
<8S0O
2-Chlorophenol
<8500
t ,3-01chlorobenzene
<8500
1,4-Dichlorobenzene
<8500
Benzyl alcohol
<17000
1,2-Dichlorobenzene
<8500
2-Methylphenol
<8500
bi s<2-Chlorof sopropyl)ether
<8500
4-Hethylphenol
<8500
N-Nttroso-di-n-propylamine
<8500
Hexachloroethane
<8500
Nitrobenzene
<8500
lsophorone
<8500
2-Mitrophenol
<8500
2,4-D!aethyIphenol
<8500
Benzoic Acid
<42000
bi s<2-Chloroethoxy)*ethane
<8500
2,4-0ichlorophenol
<8500
1,2,4-Trlchlorobenzene
<8500
Naphthalene
<8500
4-Chloroaniline
<17000
Hexachlorobutadiene
<8S00
4-Chloro-3-methylphenol
<17000
2-Methyl naphthalene
<8500
Hexachlorocyclopentadiene
<8500
2,4,6-Trichlorophenol
<8500
2,4,5-Trichlorophenol
<8500
2-Chloronaphthalene
<8500
2 -M11roan{line
<42000
Oiaethylphthalate
<8500
Acenaphthylene
<8500
2,6-0initrotoluene
<8S00
Comments: A less than (<) Indicates the compound i
COMPOUND 3-Nttroaniline Acenephtbene 2.4-0fnitrophenol 4-Nitrophenol Dibenzofuran 2.4-Dinitrotoluene 0(ethylphthalate 4-Chlorophenyl-phenyl ether Fluorene 4-Nltroaniline 4,6-0 initro-2-eethyIphenol N-Nitrosodiphenylanine 4-8romophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene 0i-n-butylphthalate Flueranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine 8enzo<a)anthrecene Chrysene bis(2-Ethylhexyl)phthalate 01-n-octylphthalate 8enzo(b)fluoranthene Benzo<k)fluoranthene Benzo< a)pyrene lndeno(1,2,3-cd)pyrene 0ibenzo(,h)enthracene Benzo<g,h,i)perytene
^
not detected at the level indicated.
<42000 <8500
<42000 <42000
<8500 <8500 <8500 <8500 <8500 <42000 <42000 <8500 <8500 <8500 <42000 <8500 <8500 <8S0O <8500 <8500 <8500 <17000 <8500 <8500 <8500 <8S00 <8500 <8500 <8500 <8500 <8500 <8500
Page 3
S*L 000006087
662 '69
Company: CONOCO-LAtE CHARLES REFINERY Date: 04/18/89 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work order: A9-03-095
Job Umber: 449900
TEST KANE: HAZARDOUS SUBSTANCE VOLS
SAMPLE ID: PC 1635
Results in
COMPOUND
acetone benzene 2-butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2-dichloroethane 1,1,1-trfchloroethane 1,1-dlchloroethane 1,1,2-trfchloroethane 1,1,2,2-tetrachloroethane chloroethane 2-chloroethylvinyl ether chloroforn 1,1 *dlchloroethylene trens-1,2-dichloroethylene 1,2-dichloropropene cis-1,3-dtchloropropene
<81000 30000
<61000 <3100 <3100 <3100 <3100 <3100 <3100 <3100 <3100 <6100 <6100 <3100 <3100 <3100 <3100 <3100
0/kg:
DATE COLLECTED: 03/06/89 DATE ANALYZED: 04/30/89
COMPOUNO
trans-1,3-dlchloropropene ethylbenzene 2-hexanone ethylene chloride ethyl chloride ethyl broalde 4-Methyl-2-pentanone broaofora bronodlchioroaethane dibroaochloronethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cunene isoners cyelohexane ethyl t-butyl ether ethylene dibronide
<3100 27000 <31000 <3100 <6100 <3100 <31000 <3100 <3100 <3100 <3100 <3100 98000 <3100 <31000 <6100 130000 43000
<6.1 <6.1 <6.1
Consents: A less than (<) Indicates the coepound Is not detected t the level Indicated.
Page 4
$al 0000*Oaa 6S2 -9
Company: COHOCO-LAKE CHARLES REFINERY Oatc: 04/18/89
"Ilent Work ID: SARA 313 ANALYSIS
ITANALTHCAL SERVICES AUSTIN, TX
Work Order: A9-03-095 Job (Umber: 449900
TEST NAME: ASH NSL CC/MS EXTRACTASLES
SAMPLE 10: PC 1635
\
Results In
mg/kg:
DATE COLLECTED: 03/06/89
DATE EXTRACTED; 04/03/89 DATE ANALYZE0: 04/04/89
COMPOUND
Phenol
<1800
bistZ-ChloroethyOether
<1800
2-Chlorophenol
<1800
1,3-0{chlorobenzene
<1800
1,4*0{chlorobenzene
<1600
Benzyl alcohol
<3600
1,2-Dichlorobenzene
<1800
2-Hethylphenol
<1800
bis!2-Chloroisopropyl>ether
<1800
4*Methylphenol
<1800
N-Nitroso-df-n-propylamine
<1800
Kexachloroethane
<1800
Nitrobenzene
<1800
Isophorone
<1800
2-Nitrophenol
<1800
2,4-Dimethylphenol
<1800
Benzoic Acid -
<8900
biat2-Chloroethoxy)methane
<1800
2,4*0ichlorophenol
<1800
1,2,4-TrI chlorobenzene
<1800
Naphthalene
<1600
4-Chloroanfline
<3600
Hexachlorobutadiene
<1800
4-Chi oro-3-nethylphenol
<3600
2-Methylnaphthalene
<1800
Hexachlorocyclopentadiene
<1800
2,4,6-Trichlorophenol
<1800
2,4,5-Tr{chlorophenol
<1800
2 -Chloronaphthalene
<1600
2-Nitroaniline
<6900
Dimethylphthalate
<1800
Acenaphthylene
<1800
2,6-0 initrotoluene
<1800
Comments: A leas than t<) indicates the compound
C0MPOUH0 3- Nitroaniline Acenaphthene 2,4~Dinltrophenol 4- Nitrophenol Dibenzofuran 2,4-Dlnftrotoluene Diethylphthelete 4-Chlorophenyl-phenylether Fluorene 4-N Itroani1fne 4,6-Oinftro-2-methylphenol N-Nitrosodiphenylanine 4-Sroarophenyl-phenylether Hexachlorobenzene Pentechlorophenol Phenanthrene Anthracene Oi-n-butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Ofchloroben:idine Benzo(a)anthracene Chrysene bist2-Ethylhexyl)phthalate Oi-n-octylphthalate Benzo(b)fluoranthene 8enzo(k)fluoranthene Benzole)pyrene 1ndcno<1,2,3-cd)pyrene O(benzole,h^anthracene 8enzo(g,h,f)perylene
not detected at the level indicated.
<8900 <1800 <8900 <8900 <1800 <1800 <1800 <1800 <1800 <8900 <8900 <1800 <1800 <1800 <8900 <1800 <1800 <1800 <1800 <1800 <1800 <3600 <1800 <1800 <1800 <1800 <1800 <1800 <1800 <1800 <1800 <1800
Page 5
SAL 000006089
< 99
Coapany: COHOCO-LAKE CHARLES REFIMERT Data: 04/18/89 Client Work 10: SARA 313 AVALTSIS
COHOCO-LAgg CHARLES REFIHERT
A903095/01B Sot/r" Crvde.
1,1 `-biphenyl
pyridine aniline quinoline 0-toluidine 2r4*xylidine
A903095/00.B
I '*.
1,1 'biphenyl
0-toluidlne 2,6-xylf dIne pyridine quinoline aniline
Fage 6
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-09S Job Muober: 449900
<42000 <42000 <42000 <42000 <42000 <42000
<8900 <8900 <8900 <8900 <8900 <8900
SM 000006090
Coapany: CONOCO-LAZE CHARLES REFINERY Date: 04/18/89 Client Work IDs SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Orders A9-03-095 Job Muaber: 449900
TEST C00E 8240
TEST NAME HAZARDOUS SUBSTANCE VOLS
Hazardous Substance list Volatiles
EFA 8240-Test Methods for Evaluating Solid Wastes, 3rd Edition, Noveaber 1986. GC/MS Purge and Trap analysis
TEST COOE 8270
TEST NAME ABN NSL GC/HS EXTRACTARLES
Hazardous Substance list Extractebles
EPA 8270-Test Methods for Evaluating Solid Waste,3rd Edition, Noveaber 1986. Acid/Base-Heutral Extraction followed by GC/KS analysis.
Page 7
SAL 00000609X
iconocoj
Facility______ l-GIte h*rks feCiner-Y Address
Telephone (____)
Transporter Name _ Ye./U/ Fte&hf
Address Telephone ()
Process Producing Sample _ Method of Shipping_______ Special Shipping Instructions Remarks_________________
Chain of Custody Record
Sample 10 No. Sample Location /cm T Sour Crudt
Date
Time
Sample Type
on
Total 1Container* | VoL Type No.
Empty** Refinqutshed by: (denature) Relinquished by: (Signature) Relinquished by: (Signature) Relinquished by: (Signature) Relinquished by: (Signature)
Received by^Stgnature) Received by: (Signature) Received by: (Signature Received by^Signature) Received by: (Signature) Received by: (Signature)
Date/Time Date/Time Oate/Time Data/Time Date/Time Date/Time
Condition of Samples Upon Arrival at Final Destination
Signature
Date
Temp, of Samples Upon Arrival at Final Destination (for Temp. Sensitive Analysis Only).
Signature
7-236 X3, 12-65
____
SAL
Date________ _____________________________________
Distribution: White & Canary--Analyzing Laboratory Copies. (White will be returned lo Originator
with analysis results.) 00006092*--^Originator Copy
(conoco) 00,1
Facility---------- C^wco $e/Aer/es_________
Address_______________________________ ___ Telephone ()___ -______
Transporter Name___ Address_______ Telephone (____)
Process Producing Sample___ Method of Shipping_____ Special Shipping Instructions _ Remarks_______ ____________
Chain of Custody Record
Sample
- ffl NO.' -- Sample Location
FC MSS ) ~K~rc* 5
Marita
FCIL2 FT. mzl
Date
/
Time
Sample Type
I 1
Total Containers Vol. Type No.
Employee Sampiiro:j(Sianature} Relinquished by; (Signature) Relinquished by: (Signature) Relinquished by: (Signature) Relinquished by: (Signature) Relinquished by: (Signature)
Received by(SJgnature) Received by: (Signature) Received by. (Signature Received by:(Signature) Received by (Signature) Received by (Signature)
Dale/Ttme
i
Dale/Ttme
1
Date/Time
1
Date/Time
Date/Time
Date/Time
Condition of Samples Upon Arrival at Final Destination
Signature______________________________________________ Date__________________________ __________
SAL 000006093
Temp, of Samples Upon Arrival at Final Destination (for Temp. Sensitive Analysis Only).__________________ ____
Signature . Date.--
7-236 X3. 12-65
Dletrtbutlon: White 4 Canary--Analyzing Laboratory Copies. ' (White win be returned to Originator
with analysts results.)
Pink--Originator Copy
I J, "I INTERNATIONAL I TECHNOLOGY r T m CORPORATION
ANALYTICAL SERVICES
CERTTHCATE OF ANALYSIS
CONOCO-LAKE CHARLES REFINERY CONOCO, INC. P O DRAWER 1267 RE 346 PONCA CITT OR 74604 DON LINDER
Oatc: 04/19/89
Job Number: 449900
Work Order: A9-03-075
Thfe Is the Certificate of Analysis for the folloning saaptes:
Client Work ID: SARA 313 ANALYSIS Date Received: 03/16/89 Nuaber of Saaples: 3 Saaple Type: SOLID / CRUOE
TABLE OF CONTENTS FOR ANALYTICAL RESULTS
PACES 3 S 7
LABORATORY S A9-03-075-01 A9-03-075-02 A9-03-075-03
SAMPLE IDENTIFICATION PC1497 SWEET CRUOE PC1504 0 IOLQC1 CAL SOL-IOSPC150S API SCP OOTTOH3
Oonnic L. Heinrich Laboratory Manager
SAL OOOOO6O94
American Council ol Independent Laboratories International Association ol Environmental Testing Laboratories
Amencan Association lor Laboratory Accreditation
r
IT Analytical Services 5307 Industrial Oaks Boulevard. Suite 160, Austin, TX 78735 (5L2) 892-6684
mm-ot
Company: CONOCO-LAKE CHARLES REFIHERT Date: 04/19/89 Client Work 10: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03'075 Job Nuaber: 449900
TEST NAME: HAZARDOUS SUBSTANCE VOLS
SAMPLE ID: PC1497 SWEET CRUOE
Results in
COMPOUND
acetone benzene 2-butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2-dichloroethane 1.1.1-trichloroethane 1.1- dichloroethane 1.1.2-trich loroethane 1.1.2.2-tetrachloroethane chloroethane 2-chloroethylvinyl ether chlorofora 1.1-dichloroethylene trans-1,2-diehloroethylene 1.2-dieh loropropane ci s- 1,3dichloropropene
<5800 3700
<5800 <290 <290 <290 <290 <290 <290 <290 <290 <580 <580 <290 <290 <290 <290 <290
mg/kg:
DATE COLLECTED: 02/10/89 DATE AMALYZE0: 03/29/89
COMPOUND
tran*-1,3-dichloropropene ethylbenzene 2*hexanone methylene chloride aethyl chloride aethyl bromide 4*methyl-2-pentanone broaofora broaodichloromethane dibromochtoronethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cumene isoaers cyclohexane ethylene dibromide methyl t-butyl ether
<290 1900 <2900 <290 .. <580 <290 <2900 <290 <290 <290 <290 <290 7700 <290 <2900 <580 12000 1200 5800 <580 <580
Comments A less then (<) indicates the compound is not detected at the level indicated.
Page 2
o000069^ SM-
66? '-89
Company: CONOCO-LAKE CHARLES REFINERY Oate: 04/19/89 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-07S Job Member: 449900
TEST NAME: ABM MSI CC/NS EXTRACTABLES
SAMPLE ID: PC1497 SWEET CRUDE
Results in
mg/kg:
DATE COLLECTED: 02/10/89 OATE EXTRACTED: 04/03/89
DATE ANALY2E0: 04/04/69
COMPOUND
COMPOUND
Phenol
<850
3 -Nitroanil i ne
bis(2-Chloroethyl)ether
<650
Acenaphthene
2-Chlorophenol
<650
2.4-Dinitrophenol
1.3-D{chlorobenzene
<850
4-Nitrophenol
1.4-D(chlorobenzene
<650
Dlbenzofuran
Benzyl alcohol
<1700
2.4-Dinitrotoluene
1,2-Dichlorobenzene
<650
Diethylphthalate
2`Hethylphenol
<650
4-Chlorophenyl-phenylether
bis<2*Chloroisopropyl)ether
<650
Fluorene
4*MethyIphenol
<850
4-Nitroaniline
N-Nitrcao-di-n-propyl amine Hexachloroethane
<850 <650
4,6-0 ini tro-2*aiethylphenol N-Nitrosodiphenylaaine
Nitrobenzene
<650
4-Bromophenyl-phenyl ether
Isophorone
<650
Hexachlorobenzene
2-Hit rophenol
<850
Pentechlorophenol
2.4-Dimethyl phenol
<850
Phenanthrene
Benzoic Acid
<4300
Anthracene
bis(2-Chloroethoxy)methane
<650
Di-n-butylphthalate
2.4-Oichlorophenol
<650
Fluoranthene
1.2.4-Trichlorobenzene
<850
Pyrene
Naphthalene
1500
Butylbenzylphthalate
4-Chloroaniline
<1700
3,3'-01chlorobenzidine
Hexachlorobutadiene
<850
Benzol a>anthracene
4Chloro-3-nethylphenol
<1700
Chrysene
2*Hethylnaphthalene
2300
bis(2-Ethylhexyl)phthalate
Hexachlorocyclopentadiene
<850
Di-n-octyIphthalate
2,4, 6-Trichlorophenol
<850
Benzo(b)fluoranthene
2.4.5-Trichlorophenol
<850
Benzo<k)fluoranthene
2-Chloronaphthelene
<850
Benzo<a)pyrene
2-Nitroaniline
<4300
Indenol1,Z,3-cd)pyrene
0 i(nethylphtha late
<850
Dibenzol a,h)anthracene
Acenaphthylene
<850
Benzolg(h,i)perylene
2, 6-0initrotoluene
<850
Coaments: A less than (<) indicates the compound is not detected at the level indicated.
<4300 <850
<4300 <4300
<850 <850 <650 <650 <850 <4300 <4300 <850 <850 <850 <4300 <850 <850 <850 <650 <850 <850 <1700 <850 <850 <850 <650 <650 <650 <850 <850 <650 <650
Page 3
sAi
Oo Oq
60*6
602-1-89
Company: CONOCO-LAKE CHARLES REFINERY Data: 04/19/89 Client Work ID: SARA 313 ANALYSIS
CONOCO-LACE CHARLES REFINERY
A90307S/01S
Pc 1^7
A903075/028
pc i <5oH
1,1*-biphenyl niline quinoline pyridine O-toluidine 2,6-xylidine
1,1'-biphenyl aniline pyridine quinoline O-toluidine 2,6-xylidlne
A903075/038
1,1*-biphenyl quinoline pyridine niline 0-toluidine 2,6-xylidine
Page 8
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-Q75 Job Number: 449900
<4200 ag/kg <4200 ag/kg <4200 ag/kg <4200 ag/kg <4200 ag/kg <4200 ag/kg
<2400 ag/kg <2400 ag/kg <2400 ag/kg <2400 ag/kg <2400 ag/kg <2400 ag/kg
<13000 ag/kg <13000 ag/kg <13000 ag/kg <13000 ag/kg <13000 ag/kg <13000 ag/kg
091
Oooob
602 1 09
Company: CONOCO-LAKE CHARLES REFINERY Date: 04/19/809 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN. TX
Work Order: A9-03-075 Job Munber: 449900
TEST CODE 8240
TEST NAME HAZARDOUS SUBSTANCE VOLS
Hazardous Substance List Volatiles
EPA 8240-Teat Methods for Evaluating Solid wastes. 3rd Edition, November 1986. GC/MS Purge and Trap analysis
TEST CODE 8270
TEST NAME ABN NSL GC/MS EXYRACTABLES
Hazardous Substance List Extractables
EPA 8270-Test Methods for Evaluating Solid Waste,3rd Edition, November 1986. Acid/Base-Neutral Extraction followed by GC/MS analysis.
Page 9
SAL 000006098 682t-e9
Facility
(conOCQ) uonoco me.
Zqfe- QJ\*rh &Ciery
Address____________________________________ Telephone ()____-______
Transporter Name_____--^Xf^^L-------------------
Address___________________________________ Telephone ()___________
Process Producing Sample-----------------------------------
Method of Shipping_______ !f/f~-------------------------
Special Shipping instructions______________________ Remarks____________________________ .__________
environmental uuamy oampie Chain of Custody Record
Sample
10 No.
Sample Location
Pc. /*r ^7 Suteh Crude. PC !S( > V 8iobCic*A St/tcU frTTs 0~ QPT Szptwhr Gaf'Hfss
Date
Time
W>TFT
VvW
Sample Type
Oufe 0ft Srftd Ufid?
si/
Total Containers Vol. Type
Employee
ignature)
Reinquished by; (Signature)
Relinquished by: (Signature)
Relinquished by: (Signature)
Relinquished by: (Signature)
Relinquished by: (Signature)
Reoeived by:(Signat Received by: (Signature) Received by: (Signature Received by:(Signature) Received by: (Signature) Received by: (Signature)
Date/Time 7/-'AT\
Date/Time
Oate/Time
Oate/Time
Oate/Time
Oate/Time
Condition of Samples Upon Arrival at Final Destination
Signature
Date 3/nAi
Temp, of Samples Upon Arrival at Final Destination (for Temp. Sensitive Analysis Only).
Signature
7-236 X3. 12-8S
_ Date . s/r/M
OUtrtbutlon: White & Canary--Analyzing Laboratory Copies, (White wil be returned to Originator with analysis results.)
Pink -- Originator Copy
SAL 000006099
ANALYTICAL SPECTROSCOPY REPORT
istomers Cindy Quy
ReferencesESICP #1 p. 189
te Analyzed: 04/E8/89
Analytical Code: ESICP
finery Crude Oils/Communtiy Right--To--Know
lits: ug/g
imple #
JV901444 PC W901445 PC.- 14^3
W901446 PC - \10to 701448 Pt-l44l
MV901449 MV901453 PC - IS*?/
W901454 PC -- ICo36-
A1
<1000 <1000
<1000 <1000
<1000 <1000
<1000
aml_e_#
W901444Dup. MV901445 Dup.
MV901446 NV9O1440
MV901449 NV901453
MV901454
Cr
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Sb
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Cu
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Ba
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Ni
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Be
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Cd
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Co
<1000 ~i Lake <1000 _J CJbajJja)
<1000 'Jlduud*- toojuA*
< 1OOO vulLljuu^
<1000*5
< 1000_r Uiawua,
<1000 Pcvi&Ldttf
V
<1000 <1000
<1000 <1000
<1000 <1000
<1000
Zn
<1000 <1000
<1000 <1000
<1000 <1000
<1000
ample preparation: Muffle ash at 450 degrees Centigrade ; Aqua-regia digest.
eported ate_________________________
Reviewed
Date
OOOOOt-T-00 sM-
ANALYTICAL SPECTROSCOPY REPORT
stomers Cindy Quy
ReferencesESICP #1 p. 189
te Analyzed! 04/HB/S9
Analytical Code ESI CP
finery Crude OiIs/Communtiy Ri gh t--To--Know
its: ug/g
mole #
V901444 Dup. IV901445 Dup.
ank 1 ik
ank 3 ank 4
r. Std. ue Value
A1
<1000 <1000
<0. 16 <0-16 <0. 16 <0.16
0.96 0.97
Sb
<1000 <1000
<0.26 <0.26 <0.26 <0.26
0.90 0.99
Ba
<1000 <1000
<0.006 <0.006 <0.006 <0.006
1.1 0.97
Be Cd
<1000 <1000
<1000 <1000
<0.006 <0-006 <0.006 <0.006
<0.016 <0.016 <0.016 <0.016
0.97 0.96
1. 1 0-94
Co
<1000 <1000
<0.11 <0.11 <0.11 <0.11
0.92 1 .00
imp 1 e #
lV901444Dup. JV901445 Dup.
ank .ank .ank .ank
1 3 4
?r. Std. -ue Value
Cr
<1000 <1000
<0.031 <0.031 <0.031 <0.031
1 .2 1 .03
Cu
<1000 <1000
<0.016 <0.016 <0.016 <0.016
0.99 1 .03
Ni
<1000 <1000
<0.076 <0.076 <0.076 <0.076
1.1 1.02
V
<1000 <1000
<0.026 <0.026 <0.026 <0.026
0.99 1 .Ol
Zn
<1000 <1000
<0.026 <0.026 <0.026 <0.026
0.99 1 .Ol
imple preparation: Muffle A*Y\ at 450 degrees iCentigrade ; Aqua-regia di
?pot ted By________Q- -
11 e J_[ 3 I S __________
Reviewed Date__S-j3il
SAL 0006101
(conoco)
Conoco Inc. Analytical Research Section Research & Development Dept.
Analysis Report Environmental Samples Chemical Analysis Group
To K, GU-n/
---------------------- ZT-------------------XT -
Project Number
^1 SS
/w
Sample Description
O
Comments
Date 5 III I 84
Date Analyzed 5 / ? /
Location Reference CTWW ^ ^
^ *?
Analysis Codes Hy_
EPA or Std. Method* Number
5m 320 A
Concentration Units
0 -O
Analytical Number Env Number
17381-
I'+'+L
'Utt-'J
1443
l73*?8
1444
Samole Number Data
0
%
pc 150+
ISoS
3.S
14<?7
Q, Oi
1445 144^
1418
1706
0. 35 o, 06
1447
13of
0.18
1 4M8 1441
14^1 1 S<5
0.03
0.33
|45o
1
0. 07
1 45 1 I4SL 1 453
1 S&7
1 15*3
vt / 511
0
0. 04 5,02-
01
\ti
QA/QC Data
(Mi
<3.1C 1.---O---4---z------A-----V------- 0. is
Analyst 7 , IAJ
c. .A Y? 1 1GGR
ST Approved
sal 000006102 o)
(conoco)
Conoco inc. Analytical Research Section Research & Development Dept.
Analysis Report Environmental Samples Chemical Analysis Group
to
Project Number
Q y O/
2* / .} X ' ` / 4
Sample Description
Comments
Date S/tl 1 $
^ ^ ^Date Analyzed
^
Location
CS"Reference
t/OL-J
^ 7-33
S
Analysis Codes
EPA or Std.**Methods Number
Sm 320 A
Concentration Units
Analytical Number Env Number
I4-SM1M 55 IM-56
IH-S7 IHSS
Sample Number
Data
Pc [611 0.1#
l<>37 O- f3 III?
/<Wo
z.<+
o.of
\
QA/QC Data
193^ (73+*/
A/^hc/ *F ^ Po o 0
Fee (3^%so(^
turw
<5%,,
a;2.o|, (x>
R C-forvv^af^
//m, O
fllky[ai.
<s,Ho,i
L 'Q ki Cr,, eked &*S 0 ^'^e. C&ker) ^ 4 lo. s
Bo~hr\_ / s*i>ui**c Cfid- Poly (y*iSa(
2?7%
) zo.H
&-$'> r^h&*.c{ ($Ws2lV*2_ ^
rs^
^
//y. s" 3-5,0
i^TSE. ^
6 * 6?
sy 757 . 7
l^&lce. CP^rl-e<
W/ % erf Fi A1
3z,a 3^.6
II, 1
7, /
4. 1
2`l
7.0
0,(o o, 1 iOo.Q
lo-fc^f 1^2/3 (JA.sal*Vy Pao 1 Was bl&tncfed ~h> cre-\~f~<z
35% Re0oUr)
'ZS % ScJoer Urt ie<A.dle<Ji.
3 Samples of "ffese ^Sof.'^es *^re Uz^deA by Y^ese.
prQ porf ,b^-s '/2S
c^eA*/^. a.
11 *
s^^/e rep^eseo/^f-Vc '
^e*5o/<Vi<^ Savip/e "f>/" Ot. *7 c\ / y S J
-fo/foi^ys
us?o( "i"2 Uelp o-/ef? r
l^e
Sffif 3*3 c^ie^-'cAf& ^ ~fAe bte^J srfocJcs
coto re^fro'f-o n of
O') Ses
/f/^e^7o/,'x
O--
@Lebc**h
f^ --^5^"S7)
(3) Coni'^'^-S SfiR$ 3/3
(?) f^lTS^ in
b/encf
cJ^Ci^y /o^/. *
J- I iV/' % (below o{^
SAL 000006104
Sf\RA 3/3
/^ss &a(cir\ce- a-P L<<2, 6W^o/' `'l d
C $*r*ple.
Fc f&Z5~S)
6e.oze ne_
3.0 */f X
/ "N V Ana/ysts /
0.3^2 (u^i%) + 0.Z^L C?^~\y.) t 0,00&(l.<=TA)
f=OZ &*iSo/('n^
LSR
- 0. 070 Cz,|/0 + 0.O7l(o,zX) - 3,Cust7&*
To/cje^e
<?.? wf%
/(Sct<k5/<'^ ^ ^ flna/ySG-S /
a3?z^v.?^) + o^CoClZ.S'Z) + o.oo&Cs.oY.)
F<Cc1
/? e -P
LS ^
+- o.ozi (^.r/) + o.cniCH.oy) = 9,% w-rz izi
CL^S
o(
1o2J*'
Z,"?w+7o --
&^soi:<z\ Ane* ( yse 5 /
0,^2 (Vo/0 + o.^&(^/sy)
Foe
= -2.7 ^7 E
0.02. 6.1*/") CsgH^(
o.^*i(i1,7 */.) 4 o.z<j&( iq,0/) + d.oi /7,=f %)
Fee.
e*p Cs^Fc^
+ 0,071 (a,s 7) - ;3 ,o
7 xy
dokej-
SAL 000006Z05
S/3'/?/? 3/3
^t51 So/Vi<2- /%5S
Cyc/oiieXAh. ^ I \s-sf % (qol$oI'*q. C\r\c{ (ys<rs^) ^
(con~f~*)
^vv^S5>
pZ-cfor^edl,
g_-
^,Z wt%
/\ v /^-tn.a(yse.S /
c.vizCs'.r/J) + o.n(,( 0,.$%)+ 0.071(1.0%')
pCC
eo^er-
-
<L/. 3> vf~ /o
^Tc/w
Psec/g/o
g
- r-4)
xo wt%
r
(&S < KV\oiie)
o.yt>2j(?,r/.') 1-P.3V&0.7/0 + o.ouCz.ot:)
Fee
Re-f
Cd ^co~
- Q.O
Pcu^
SAL 000006106
CONOCO INC.
PONCA CITY, OKLAHOMA
Pit.: LC
TECHNICAL SERVICES LABORATORY
Flic; 662.1 924
Date: 9-11-85
LABORATORY NO.: 1-32-85
CHARGE: SUBJECT:
TSL
Summary of Benzene. Content of Finished Gasoline and In--Plant Streams - 1977 to 1985 - Lake Charles Refinery
CONCLUSION:
None of the Lake Charles Refinery finished gasolines or In--plant streams analyzed by fh-fa laboratory contain as much as 10.0 wt. Z benzene* Therefore* the control provisions of EPA regulation 40 CFR 61* Subpart J, do not apply.
DISCUSSION:
A June 6* 1984* promulgated regulation from EPA mandates controls on benzene fugitive
emissions at petroleum refineries. A key definition In the regulation Is: "In
benzene service
that a piece of equipment either contains or contacts'a fluid
that is at least 10 percent benzene by weight as determined according to the
provisions of 561.245(d)Unless fluids produced or used in the refinery contain at
least 10 wt.Z benzene* the controls In the regulation do not apply.
At P. L. Youngblood's request of 9-6-85, the results of previous laboratory studies of benzene in Lake Charles Refinery streams are summarized In this report. Five major studies on this topic were made from 1977 through 1985. Benzene content of all the streams measured in them was lower chan 10 wt.Z. Additional analyses have been done by- the Lake Charles Refinery Laboratory.
Attachment II is a laboratory crosscheck comparing benzene concentrations determined using gas chromatography and Infra-red analytical methods. The benzene results Included In this report were obtained using both methods, at different times. The method described in the regulation at 561.245(d) is gas chromatography.
ANALYTICAL DATA:
Attachment I.
REFERENCE:1 2
1. Verbal request from P. L. Youngblood to R. S. Jones* dated 9-6-85. 2. Several laboratory reports dated in 1977* 1983, and 1985.
Approved:
/
cc: PWL-RMc-EW-PLY-RSJ-TGW-GM-F Att: 2
SAL 000006107
MORATORY NO.: 1-32-85 September 11, 1985 Page 2
ATTACHMENT I BENZENE CONTENT OF LAKE CHARLES;* REFINERY
FINISHED GASOLINES AND IN-PLANT STREAMS
Finished Gasolines
Regular Gasoline Unleaded Gasoline Super Unleaded Gasoline Regular Gasoline Premium Gasoline Unleaded Gasoline Unleaded Gasoline Regular Gasoline Premium Gasoline
In--Plant Streams
Naphtha Cutterstock
Naphtha Cutterstock
Naphtha Cutterstock
Naphtha Cutterstock
Field PBC
--
Denuded Casinghead --
No .1 2 CTO LSR
No. 3 CTU LSR
W-10 OH
W-10 Btms
FCC Gasoline
No. 2 Lt. St.~ Run Gasoline
No.- 3 Lt. St. Run Gasoline
Denuded Casinghead
Cat Poiy Gasoline
Alkylate
Coker Gasoline
No. 2 Reformer Charge
No. 2 Reformate (95 RON)
No. 3 Reformate (101 RON)
No. 2 CTU Lt. Straight Run
No. 2 CTU Naphtha
Thermal Gasoline
Coker Gasoline
Coker Gasoline
Thermal Gasoline
TCC Gasoline
No. 1 Lt. Straight Run
No. 2 Lt. Straight Run
Denuded Casinghead
No. 1 Reformate
No. 2 Reformate
Primary Tower OH
Sample Date
8/83 8/83 8/83 5/77 5/77 5/77 3/77 3/77 3/77
5/85 4/85 4/85 4/85 1/85 1/85 1/85 1/85 1/85 1/85 8/83 8/83 8/83 8/83 8/83 8/83 8/83 8/83 8/83 8/83 11/77 11/77 11/77 11/77 5/77 5/77 5/77 5/77 5/77 5/77 5/77 5/77 5/77
Benzene Wt.Z
2i*.67/
2.8 V, 1.3 (
1.2 1.3 1.8 i.2 1.3 /
V
ZPoc
tb/n/'zc,')
000006108
SAL
(conoco)
Tr
Interoffice Communication
To Mike' Johnston
' ' ' *
From
M. W. Clayton
Oate
June 19, 1986
Subject
Benzene Analysis of Gasoline Tanks -- Lake Charles Refinery
0'*'
The benzene content of Refinery base gasoline tanks and finish product
gasoline tanks was determined. All of the tanks were below the five percent
maximum allowable concentration*. The tanks showing the highest levels of
benzene were the reformate tanks and the super unleaded tanks which contain a
high percentage of reformate.
Tank
Sample Date
Gasoline Type
L.V7' Benzene
y.? /
***/*
-------
38 77 85 98 99 33 78 64
65 80 25 32 92 93 31
6-11-86 6-13-86 6-13-86 6-13-86 6-12-86 . 6-11-86 6-13-86 5-27-86 6-09-86 6-13-86 6-01-86 5-29-86 6-08-86 6-13-86 6-05-86
,
Light St. Run No. 2 Reformate FCC Gasoline Alkylate Alkylate No. 3 Reformate Super Unleaded Super Unleaded Super Unleaded Regular Leaded Regular Leaded Regular Leaded Unleaded Unleaded Unleaded
0.93 .. 3.47
0.94
0.10 0.10 4.14 1.79 3.18 1.49 1.86 1.65 2.36 1.87 0.29 2.12
* Maximum allowable concentration for gasolines sales
7?/. M. W. Clayton0 Analytical Chemist
_________
mr cc:
PFM/DLW RJH/PAN/RLK RHC KWC/JJM/JI/FILE T. ^ Waltrip - Ponca City
SAL 000006109
CONOCO
ACHIEVING
*
***
** -
*
** SAFETY **
**
** **
EXCELLENC
INTEROFFICE
COMMUNICATION
To:,
All Supervisors
From:
Tim Myers
Date:
January 07, 1938
Subject:
Lab Results Of The Refinery's Streams That Have Been Tested For Benzene Content
Attached you will find a list Of the refinery's streams that have been tested for Benzene'content. The samples dated 1214-87, wsre taken after the HAD frarti T^n>: 27 had b/?n injected into the # 3 CTU'S crude charge for over a week. Th total Benzene content of # " CTU* s crude charge wan &.ZV. .
We are iiionitoring a represented number of the job tals wher
an employee is apposed to a stream with a Benzene
c oncer.tr At i cn of 0.17. * A list should be develop by the
Operating Department of all equipment that is in
of
these treams, or Any l.ie streams that would enntain
0.1
Sen;ene.
Please contact the Safety Department, in advance, as equipment m service of these streams is brought down repair. This will help us in setting up the personnel monitoring required by the new Benzene Standard.
for
Many of the employees have already rectri /ed the reunite of the monitoring that they took part in. Additional results will be made available as we receive it.
Please contact your area Safetv Super/iior or the Safety Department with any questions concerning Benzene Exposure.
T l m fl\ Safelv Superv*scr
SAL 000006110
BENZENE RESULTS OF REFINERY* S STREAMS
UNIT
SAMPLE
FIRST RESULT
SECOND RESULT
I HDS UNIT * 2 CUKfcFC
n l HDS EFFI. WENT * 2 COKER GASOLOINE
0. IB% (01-3'1-Qo) 0. 437. (i? 1 -23--36)
0 . 1 97. (12-14 G"
# 2 CRU
HDS
# 2 CRUDE UNIT
ff 2 HDS CHARGE # 2 REF. REFORMATE
# 2 L5R GASOLINE 2 NAPHTHA
1 . 16% (01-31-66) 2.717. !!? 1 -31 --36)
1. 95% (01-31-86) 0, 18% (01--31- 361
0.907. (12-14-3" 3. 76% <12-14- 87
5 . 49% <12-14-3? 0.21 % (12-11-3?
n 3 CRU HDS
# 3 HDS CHARGE 3 REF STB OH l IQ # 3 REFORMER CHARGE tt 3 REFORMER REFORMAT
1. 16% <0. 1% 1. 17% 2.71%
<01-31-06 > (12-14-87) (12-14-07) (01-31-86)
1.01 % <12-14 35. 207. ( 1 2-- 1 4 --8-1
* 3 CTU
# 3 HUD CHARGE (W/ 300 BPD HAD) Desalted Water
<0.01% (02-04-66) 0.3% (12-14-07) <0.01% (12-14-87)
0. 03% < J 2 -14-37
3 CTU & VAC
# 3 LSR GASOLINE If 3 NAPHTHA
2. 79% (02-04-86) 0. 41% (01-31-86)
5. 28% <12-14-87 '0.41% <12-14-97
# HDS
ft 4 HDS Strip. OH LG
0. 19% (12-14-87)
$ 4 Mod
#4 #4 44
ft 4
Frac. Frac. Frac. Frac.
Btms. HOD Naphtha uh Liquid
<0.01% <12-14-67) <0.01% (12-14 -07) 0. 07% (12-14-07) 2. 76% (12-14-07)
1 A HCS
4 6 HDS Strip. OH LQ
0. 12% (12-14-07)
ALKYLATION UNIT
TOTAL ALK.VALTE
< 0.01 % (02-02-Q6-'
IASINGHEAD
PBC DENUDED CASINGHEAD 1.29% (02-03-86)
2.33% <12-14-67
;at pcly unit
CAT POLY GASOLINE
< 0.01 % (01-28-86)
rCC PRODUCT FRACT
FCC GASOLINE LV*/. FCC GASOLINE
1.21% (01-28-86) 1.21% (01-28-86 >
0. 93% <12-14 3 7
iRF
- GRP GASOLINE
-IT GASO. SPLITTEft FRIM TWR B^MS FRIM1 TWR CH GASOLINE
0.39% <01-20-86.*
0.43% (12-14- 7
* 0.01% <01 - 3 l -86) 0. 32% (01-31-06)
1.41% '.12-14 - r^
4K FARM
TL. 33 LSR T . 85 FCC. CP
1.30% '12-14 87 0. 87% (12-14-97?
HCFMAL crack cp.
THERMAL. GASOLINE W-1* gasoline W I 0 NAPHTHA
0 - 23% 3. :s% 2. 29%
(02-i34- Si) (02-04-86) (H2-04-86
l . 66V. I-. 787. 4 . 6 27.
(12-14-2: ( 1 2 - ! 4 - = '
<4 3- 1 -s:
SAL 000006111
*-- fot\0
PEI ASSOCIATES, INC.
1 1409 CHESTER ROAD CINCINNATI. OHIO 4S246
(51 3i 752-4700
TEt-ECOPIER iSISi 702-4007
REVIEW OF HYDROCARBON EMISSION
FACTORS FOR THE PETROLEUM INDUSTRY APPLICABLE TO
SARA TITLE III SECTION 313
Prepared by
PEI Associates, Inc. 114,9?> Chester Road
Cincinnati, Ohio 45246-0100
PN 6421
Prepared for
AMERICAN PETROLEUM INSTITUTE 1220 L STREET, N.W.
WASHINGTON, O.C. 20005
CHESTER TOWERS
July
RANCH Of^FICCS
TEXAS
COUUMOO*. OHIO
OENVER, CCCORAOO
DORMAH. NORTH CAROUNA
Kansas cmr. kansa*
SAL 000006112
TABLE 2-3. SARA 313 CHEMICAL COMPOSITIONS CATALYTIC REFORMER (Wetherold, 80b)a
(ppm)
Chemical
De minimis concentration
Naphtha feed
Product naphtha
Overall process
Anthracene
10,000
-
4-
Benzene
1,000
1,040
84-826
3,000
Cyclohexane
10,000
-
2,000
Ethylbenzene
10,000
550-2,500
142-15,000
-
Naphthalene
10,000
-
9-2,800
-
Toluene
10,000
1,800-2,400 396-85,000 8.000
1,2,4-Trimethylbenzene f m,p-Xy1ene
10,000 10,000
2,200-2.600 4,500-6,600
184-1,400 632-75,000
8,Q00b
o-Xylene
10,000
1,700-3,000
.1
86-30,000
-
a When more than one value was found. the range of concentrations is presented.
b Total xylene.
2-7 Oooobl1'
S M-
TABLE 2-2. SARA'313 CHEMICAL COMPOSITION - FCC UNIT (Wetbero)d, G0b)a ,7(ppm)
Chemical
De minimis concentration
Low pressure separator liquid
Light cycle gas
oil
Heavy cycle gas
oil
CO boiler flue gasD
Benzene
1,000
4,300-6,600
2
5
-
Cresol
10,000
- - - 0.0003
Oibenzofuran
10,000
- - - 0.000008-0.0003
irnio Ethylbenzene Naphthalene
10,000 10,000
7,300-39,000 15,000-15,600
9 97-52,000
419 0.00002-0.001
Phenol
10,000
- - - 0.000003-0.0004
-- tb
Toluene 1,2,4-Trlmethylbenzene
10,000 10,000
5,000-160,000 20,000-46,000
14-40 30
15 38
-
-
m.p-Xylene
10,000
55,000-260,000
20-360
27
-
o-Xylene
10,000
21,300-76,000
9-270
13
-
a Where more than one value Mas found, the range of concentrations Is presented. b Because this is a waste rather than a process stream, de minimis Is not applicable; however, composi
tions are presented for information purposes.
SAL 00000611A
w
LABORATORY NO.: CHARGE: SUBJECT:
CONOCO INC. PONCA CITY. OKLAHOMA TFCHNICAL SERVICES LABORATORY
Pit.: PC File: 610
Date: 4/19/89
D-65-89
TSL - PC
Styrene and Cumene Content of Cracked Stock - Ponca City Refinery
DISCUSSION: Samples of cracked refinery streams were analyzed for cumene and styrene by R&E in connection with sample analysis for SARA Title III data reporting.
ANALYTICAL DATA: Sample:
Sample Date: Cumene, mg/Kg Styrene, mg/Kg
PC 1732 No. 5 FCC
Light Cycle Oil
3/16/89
<2 <1
PC 1733 No. 5 FCC
Heavy Gasoline
3/16/89
85000 <1.3
PC 1734 No. 5 FCC
Light Gasoline
3/16/89
33000 <1.7
TK 160 No. 2 No. 2
Diesel Fuel 3/16/89
<1.5 <0.75
Kequest for Analysis: Request from W. D. Broddle to 0. F. Engle on 3/7/89.
Approved:
Senior Technologist bl cc: DRP-WDB-TGW-F
Associate Technologist
sal
0ooo6115
CONTINENTAL OIL COMPANY RESEARCH AND DEVELOPMENT DEPARTMENT
PETROLEUM PRODUCTS DIVISION PROCESS LABORATORY
SURVEY OF PONCA CITY REFINERY STREAMS
By W. H. Kegler
Research Report No. 305-0-2-71 May, 1971
Distribution: WWW-Library(2)-DAS-JHS-CVF-CDS-HTC-IFW-CAN WRB-FK-JRU-OCK-AJL-JLS-RLP-DJR-FME-HTF-MCH DRU--EEF--HAS--RJF-RSB-JBL-WBW-WWWi-HRJ--LDW 'RLG--AJM-JHD--JfK-SYW--JRF-GAS--PCP-ALA-WHK-RWY MWH-CDK-File-AJN-GWW-WRS-KMB-JBS-BEC-CLS
CONFIDENTIAL
THIS DOCUMENT IS CONFIDENTIAL AND THt PROPERTY OF CONTINENTAL OIL COMPANY.
SAL 000006116
SAL 0000061X 7
Hr.--
Itren He. Sexyle He. Civ*tRon*ftt *hna Ethana hreyene
Ne?AliA4
aH^t 1,2-Dlaethyl butene
2,3<Pl*athrl but ana 1-Methyl yentene ] -Methyl yentene a -h UM
Methyl cycleyentene ) 1,4`Olaethyl yentene
I.l.l-Trleethyl butane
Cy 1-Methyl hexene l.S-HMthyl yentene 1 1.1-01**thy| cycleyentene)
L-Irtni -)-0l<tet hyl cycleyentene) l,ele-3-0l**thy) eyeLoyentene 1-lthyl yentene l .ttafit*2*Dta4hy{ cyl?a*t4na
A *h*taiW
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)
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l.t-Olaathyl hexane!
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l rtene -1. ft -A-tel Methyl r-tr 1 nnenien
), t KmA]
lelvene
)
7,7,4 -Tt leet hyl yentene
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1-Methyl-3-tthyl yentene
)
1 , l, lf 1 tatfthy | eye lapant lu)
1 -Methyl heytana
l ,cl*2 ,<l* * *Tflvvthyl ylapanta* 1-Methyl hyytene ),4*0iM(hyl 1 -Ethyl hexene
1 , 1 e -1, cleO-Trlsethyl cycloyentene 1,1,tle-1, trene-4-Tette.ethyl cyeley ntanr 1.7,1-TrtHethyl hexene <le,<|e,trtne-l.l,l.TMCl
1 , trail * *Dt*ehyt eye lehamana)
1,1-Oloethyl eyetehexenx
1,2,1,1-Tetmethyl butene
1-Methyl-trim-1-ethyl tycleyenltnt
1 -Methyl-ttxnx-3-ethyl CYtloyenteot _
cycleyentene
l.l.tli-3,le^'Tetmethyl cyeloyentxne
Cytleheytene
>
1-Methyl,l-etnyl cytloyentene)
1 , (ran* -2 0i**thy l <y< teh#a4*t i, i rana *1,*(],Irana -* -Tat f a*rt fiy J rye 1 **+M a^i 1,4 -AIMethyl heytene 1,1,4,4 -fatranehyl yentene
\, c ta -4 hyj <f< Uhauna J
CCKMmm ARALYIII IT CA1-1
osiyaiffigHau
OUtOttTMUm 1R WttCHT HMZKT(t)
Ho. 1 CTV Vt Cj*
(More. Oy. ) 1
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(Mot. Oy.) )
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ho. i cm Heavy
Njpfctr*
(Hot*. Oy.> 4
4414'U
1.41 11.4] 44.15 1.51 23.2( 3.34 1.14
1.11
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t .> 15.41 0.14 1.(2 .(! Ml 5.11 15.(0
1.(1 0.11 1.17
0.07 4.07 1.57 1.5T
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1.50 1.31
1.12
i.)
0.04 0.01 A 14
0.04 0 01 0.10
0.01 0,01 0.01 0.14 0.11 0.05 l.ol 0.14
0.21
0,71 0.54 0.03 0.10 0,01 i.H 1.41 0.11 i.n 1.30 1.53 2.43 (.75 0.43 0.(0 .n 0.30 1.10
1.21 3.04 1.32 0.01 0.40 0,22 0.32 5.34 Qi.2.**
1.13
He. 1 CTV Troyan*-
Butane (Hot. Oy.)
11 5573 *
0.11 11.01 15.11 71,55 4.1! 0.73 0.14
Re. 2 CTV Light Strxl|ht
Jbia Caeellne
He. 1 CTV (ylltter lattaaa
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Olf At***,
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lun Heyhthe
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Da. b CTO Unatehlllied
CeaellA*
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Cut
Mo. 3 CTV Tell Cat
(Men. Oy.) 12
(Hen. Oy.) II
(Hen. Oy.) If
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not'd
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T 0.31 0.02
r 0.14
0.01 0.02 0.27 0.41 0.12 0, OR 0.01 I.ol 4.04 2.30 3.41 1.10 3.40 3.21 li.U 1.01
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t 0.34 0.31 3.14 0.11 0.31 2,14
(Hon. Oy.) 10
3S71-W
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(131-0
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(Hen. Oy.} 13
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1.22 1.41 10.33 13.41
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T 0.01 1.30 0.32 ------------or-----------r.r4.04 1.13 1.70 0. li J.R4 10.41 2.44
------------rrr~-----------nr-- 0.23 0.10
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2.00 1.00
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r 0.34 0.00
1.41 1.44 0.54 1.03
o.ot 0.11 0.33 s.ll A. 02 0.21
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0.13 1.04
1 ; i 1 3
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--------t.lt--
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COMPONENT ANALYSIS BY GAS-LIQUID CHROMATOGRAPHY 1H WEIGHT PERCENTfa)
Unit
Stream
Stream No.
Sample No.
Component Grouping
Compounda before n-Butane n-Butane n-Butane to Isopentane Excl. Isopentane Taooentane to n-Pentane Excl. n-Pentane o-Pentane to 2-Methylpentane Excl. 2-Methylpentane to 3-Methylpentane Incl. 3-Methylpentaae to a-Hexane Excl. n-Hexane n-Hexane to Benzene Excl. Benzene Benzene to 2-Methylhexane Excl. 2-Mathylhexane to 3-Methylhexane Incl. 3-Methvlhexane to n-Heotane Excl. n-Heptane n-Heptane to Toluene Excl. Toluene Toluene to 2^4ethylheptane Excl. 2-Methvlbeotane to 3-Methvlheptane Incl. 3-Methylbeptane to n-Octane Excl. n-Octane n-Octane to Ethylbenzene Excl. Ethylbenzene Ethylbenzene to p-Xylene Excl. p- & m-Xylene a-Xylene to o-Xylene Excl. o-Xylene o-Xyleoe to n-Nonane Incl. n-Nonane to n-Decane Excl. n-Decane and Beyond
roc
Stabilized Gaaollne
(Norm. Op.)
121
7409-0
0.19 0.24 0.92 8.90 1.83 2.76 6.49 10.41 3.36 1.36 4.63 0.97 1.43 6.97 4.57 0.84 4.32 4.39 0.63 3.56 2.4S 0.34 2.45 1.20 0.25 5.97 2.17 1.92 1.35 9.41 3.74
CATALYTIC CRACKING DIVISION
FEED PREPARATION
Fractionator Bottoms
TCC Gasoline
(Norm. Op.)
(Norm. Op.)
134 7378-U
135 7382-U
CROUP WEIGHT PERCENT
0.78 0.54 1.39 3.75 1.61 2.32 5.21
4.90 3.58 1.51 1.05 1.97 3.02 3.74 4.47 1.36
4.57 4.16 1.09 2.37 4.03 0.98
2.97 1.30 0.55 6.01 3.00 2.17 2.59 11.55 11.46
1.32 0.60 1.33 3.89 1.62 2.72
5.37 5.47 3.84 1.51 4.30 1.20 0.71 4.00 4.57 1.54
4.27 4.05 0.73 2.34 3.15 0.90 1.48 0.64 2.33 5.80 1.68 0.70 4.51 12.55 10.84
(a) Because of the large mounts of unidentifiable olefins, the components in these samples were grouped as outlined in reference 6 for ease in calculating their various properties.
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APPENDIX F SOLID WASTE RELEASE DATA AND CALCULATIONS
SARA TITLE III, SECTION 313 1988 TOXIC CHEMICAL RELEASE INVENTORY
LAKE CHARLES REFINERY
$41 0O6i 27
LRNb Release calculations
Lake Charles
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'2icl - TF.wH y f betnzP ng z cjcf fc^s ^ 20 o& fi?
\y.t^oo Ihlrtg ~ /oj ibi m
ioto lb
----------------------------
irv/pcJ Yoy
SAL 000006131
LfiNb RBLEAS C//-LC5
L.C,
1--c\n cl pa r no Disposal
- S'~f C ^
PPj /C-PL S^p&r'cdaf' Sluof^c. z
30,^/3 *fbnS
(Use.
APJT Se_p Bof/ono s bd~*< "" Pc /S'oS')
Benzene = 30.H3 tor,s w*.ste-x "2ooo x ^30^ &!> _ ^ ^ ^
i "fz o
(O^lk w^s'/e
-----
ET-Bi-ylbenz-enf - 3X>, ^3 Yns x 'z~e>^----- x '^'Z-O !L E-b _
I "h*
lo< IL
"
`S+yrene ~ 30,^3 ~foos >< Z--o--o-o---f-tX 1 ~fo.O
(X b.u) ^<3 lL> 5ty
IO* lb
"To/ue^c = 30.Yl
x
"5looo ft? Hro
v
770 /> ~Tol lofc \L
Xv lee. - 30. c/3 '/an; X 2poo /t 1 f~on
\ooo li> Xv lo^iy
^
^ ^y
-----------------------
I IL ^i.
X S(p lb T2j
7 3 IL X Y-
30,^3 Vz>"S V
-T--o--c-o---/->- >< I *f*
l~Z,C>o /> Co^i 10 fc ^
lb Cu^
Cyefo^ex^ne - KcMl -hns x ^ ,u ^ ^U C^x ~ H lb Cybx
f 'to'-'i
(O^ />
fVcPHUUe - 3G> <JS ^,5 x 2000 (L v st{oolk /^= 3"? 3
-f-? r'l
lo^/t
I 2 cf-T?,',,e+Lvl&ehzee - ?673 7o*s v 2oooX ^-1300ILC^ . -7-7 H '<>
^------------------------ -1-----------------
"T^r
iow/i.
----
SAL 000006132
land Release c/kcs
L.C,
Lcxnci
biSpos^ I (On - St Ve )
lv^S`fe.^/o'_/^-r XVv^yOotJ^C'/KVi^n"/ S(<-^OjC
CBtologi'ce*! So( u^s
ASU CJPi'er Su*^^
^iofa t&r\S (dry)
(Ose
>&rrze,yng
(W B^Jo-\ rv CJfl. f So 1.W5
- pc iToy)
ck o.O
-- *~{OLd {z>n? w<*sic
'2x>oo (b >y _2------- R'*f -- ^
=
^3 /B
/ ft*-
10^ U> wcfsle
Ef-By/benzene - [oG /*rs x ^Q ^ >c t
/
~~
/O^/A
^3 lb Bb
S+yre^e
~ ^06
x ^_^ * j I -fa*
SVy
to* tk
T5/Ue = Xvke ---------------- --I -.:--
= tov.xSi* / /w-*^ i/^ ///
2000 14
du^et^e. - Hot# ~/z)^5 ^
x
fei
/^O / Cu^
loto
2, !L Siy
= Cdl
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//V A a.
cj.l,..e = </o( *>* X
- ICiiS? - S- It cvk
-1-----------------
]^
w* ib
.
/i / i
-^ooolL
1,2 c~l - Tr.VvWky floe^ze*e ~ ^OG in*s X - --
-U---- '------ ----------- ------------- t-------------------------
/ fo>^
~k x IRo IbC,^ v- ;
IO /<a
I/ t ^
7000 /2
Abpkdkfi, <*.i^e -- ^OG TZ>*$ x -S~fj^T >f
4x
y^o 11= n*,fl
IO0' fa
-_
I^S/i/va A
5AL 000006133
L Release calc, s
D/SpoSaJ Co*-Slb^C)
L.c,
I {c\*-)lx SoH-pr^ Slud^Q -- /S75~ fenS iVe.&*/-.
^ L)$-Z-
PonCcA 0-Ay Ror\~ (-JSJ^ckoA i^r\i{ Ea'tfb***C, - Pc ILio )
c-feo.c.)
0e_n^e_>^>6L ~ IS"75" "/ons >Vftsfe X SLPOO lP ^ ^ X
lUB-z
e^-y ^ g
I i~*r\
lo** IL u/asfe
Eftyf bentene = /5T7S 7^s x 7^03 lb
4o^\
lc>^ lb
3i(e th EP
/ *n
/O6 /
r 7 /& Sfy
~ToLe^e - ISISx ^
/ -fao
x /ZO/A 72/
loto lb
379 /fe 72/
Xyle^ =
IS7f? -fe.s v ^ _'fc X 5"5o lb Xy
I +2"'
lo& lb
C^ene -- /S'?? i^s k
'2gooJk fo.
/23 IP Cu^
to* lb
. \L 7o IP xy 37S /2
CyaUex^e ISIS-fo^ v 2A x
/
Pl^pLiUJe^e. x 157S
x ^- x H
3 SO IP CyA*
(o ^ IL
^6? *1b fJ^P^ lo^ lb
//OZ IL
Zog /b
(-proi~i S"-f Srode a''^/yss ! --- /T^0
v S"5.0 ppTM Xy - (obpp*.
I'LOOO pp'xX'y f5*^< CrJe^)
Cs/wcJge')
/Vi*p^
i ITV^e+tylLe^^e^
(^SS jrv^c ^2. Co^r,"^
37% It T~t^S
6\^ 0000 sM-
(conoco)
Interoffice Communication
To Paul Steele
From
David Kersey
Date
February 27, 1989
Subject
1988 SARA Data, Hazardous and Solid Wastes
The attached table summarizes Hazardous and Solid waste quantities and dispositions of the Lake Charles Refinery, by waste stream.
If you have any questions about this data, please call me at ETN 640-5591.
David Kersey Associate Engineer Lake Charles Refinery
cc/no att. cc w/ att. PBB AJN RDT/AEK file:
SAL 000006135
# / ) / / tv a s lf*', c> >hpe+ / /?re h t - u t r d w *
>\ 1 i
3^
5:
<-
J
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vj
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ts
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3 -
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ii
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5
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fl.
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s 3*
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k 1
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U
SAt~ 000006137
y * ./'/
/~7>?Z -4 & /9 Q V * a * d
- A / A t^ A P ^ & S f y y T Z P / } f 0 > A t - / ? % %
tA
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34
*
*
-wtl> Jo!
000006138 SAL
Dwt- U (.DERtWLT-
LAND TREATMENT MODEL DATA
i1 and treatment)
L,Loading <g oii/cc s-oil)
Enter Ci :< 10^6
VQ ppraw
1,Depth (cm)
Total porosity
Air Porosity (default=0)
MW oil
VO diss. in water, enter 1
Time of calc, (days)
Biodegradation, enter 1
Temperature (Deg. C)
Wind Speed (m/s)
Area (m2)
0.036 2000 20 0. 61 0-5 282 0
365.25 1
25 .47 25000
COMPOUND NAME
!_ njr.Tp;P ;:it m p y
srp^yCTIOW LOST
AIR
BIOL
INTERMEDIATE TIME
365.25 days
AIR
BIOL.
METHYL ETHYL KETONE BENZENE TOLUENE CRES0LS NAPHTHALENE PHENOL CARBON TETRACHLORIDE TRICHL0R0ETHANE(1,1,1) METHANOL ETHYLBENZENE CUMENE (isopropylbenrere.) XYLENE(-o)
O. 71* 0.903 0. 494 0.056 0.04 7
o76 O. 998
<500 O. 966
0. 99B ,*t y rvTi
O. 286 0. 097 0.506 0. 944 9 - 953 0. 924 O. 002 0.0/02 0. 034 0. 667 0.002
Aon
0.714 0.903 0. 492 0.056 0.047 0.076 0.993 0.998 0.966 0.362 0.968 Q. 320
0.286 0.097 0.508 0. 944 0.953 0.924 0 . OOO 0.000 0.034 0.638 0.000 0.680
SAL 000006139
pAWy D/hr
TABLE 5-A SUMARY Of HIGH OIL CONTENT WASTE CHARACTERISTICS
.WN -
`xttsr
Nuaber
Rang*
rarKter
Saaplea Neon
Lower Opp**
S.D.
C.V.
OH and Grease, g/fcg Chloride, *g/fcg Hetale, ag/kg
Arsenic fiariua Barylliua ^ Cobalt - Chroaiua - Lead ^ Nickel SelOrtiua - Venodiua - Nereury Volatile Organics, ag/kg 3* Beniene ^ Toluene ^ Ethylbentene "A- Styrene Total Xylenes - Methyl ethyl ketone Sai-volatile Organics, ag/kg .^-Phenol 1,2-biehlorobentene jfr- Naphthalene Phenenthrcne -- Anthracene 0i<n)butyl phthelete* fluorantnana Pyrene B1C2-ethylhexyl >phtha late benzole)anthracene Chrysene Benzo(b)fluoranthene** ftenzoCk)fluoranthene Benzola)pyrene bitoanzo(a,h)anthracene 2-Methyl naphthalene
6 143950 5 3120
2700 310000 105859
1200
9000 3743
2 0.42 <0.23 <4.3 0.07
7 83.3 34.0 14S.0 40.1
4 0.14 <0.10 0.18 0.03
7 2.1
0.8
4.7
1.7
7 7.7 4.6 13.0 2.7
6 10.8
2.3 20.0 7.2
4
8.3
<2.1
12.0
3.7
4 4.5 0.4 <13 4.1
7 6.8 1.0 20.0 6.7
3 0.43 <0.074 0.30 0.13
7 43 10
7 128
38
7 43 17
4 12.2
4.5
7 196
17
1 2.10 2.10
100 310
86 33 520 <24
32 99 24 13.9 171
***
1
3.8
3.8
<67
***
1
3.4
<3.3
<120
***
7 791
140 1600 477
6 1930
<33 7900 2953
6 131
28 2S0 73
1
310 <3.3
310
**
6 109
27 220 71
6 51? <33 1200 415
1
5.8
<3.3
<120
Mr*
6 TO 15 140 43
6 143
2$ 280 92
6 3? 13 90 27
6 3? 13 90 27
3 33 <3.3 72 25
2 3.2 1.4 <120 2.S
7 2384
300 4800 1914
0.74 1.20
0.17 0.48 0.23 0.81 0.36 0.66 0.45 0.90 0.98 0.30
0.75 0.77 0.56 1.15 r 17
0.60 1 .S3 0.56
0.65 0.80
0.61 0.64 0.69 0.69 0.75 0.80 0.80
B.C. * Detection H*it * - compound detected in blank
** ecluting
** * Standard deviation not possible for one apl.
49 SAL 000006140
SftM 3 IS /Wyses
SOUP PASTE SAMPLES ^
Ponca Citv:
Take Charles: Denver:
Billing: Santa Maria:
1) Slop Oil Emulsion Solids 2) API Separator Bottoms (2 samples)
a) East Plant Separator b) lube Oil Trap 3) Mon-leaded Tank Bottoms
1) Biological Solids 2) API Separator Bottoms
1) API Separator Bottoms 2) Biological Solids (Clarifier Bottoms) 3) Slop Oil Emulsion Solids 4) Non-leaded Tank Bottoms
(2) 1) Leaded Tank Bottoms 2) Emergency Pond Solids (if available)
1) API Separator Bottoms (if available)
(1) Addicions/deletions are possible. As discussed, metals analyses will be performed by TSL and volatile and semi-volatile organic analyses will be performed by RSD.
(2) Organic lead and organic manganese concentrations need to be
determined for leaded tank bottoms.
L J, ,1 INTERNATIONAL I U U TECHNOLOGY f " 1 CORPORATION
ANALYTICAL SERVICES
CERTIFICATE OF ANALYSIS
CONOCO-LAKE CHARLES REFINERY CONOCO, INC. P O DRAWER 1267 RE 346 PONCA CITY OK 74604 DON LINDER
Date: 04/19/89
4ob Nuaber: 449900
Work Order: A9-03-075
This is the Certificate of Analysis for the following saaples:
Client Work ID: SARA 313 ANALYSIS Date Received: 03/16/89 Nuaber of Saaples: 3 Saaple Type: SOLID / CRUDE
TABLE OF CONTENTS FOR ANALYTICAL RESULTS
PACES
3 5 7
LABORATORY > SAMPLE IDENTIFICATION A9-03-0 75 *01 PC1497 GWCCT CftUOC A9-03-075-02 PC1S04 BIOLOGICAL SOLIDS A9-03-075-03 PC1505 API SEP BOTTOMS
Donnie L. Heinrich Laboratory Manager
00000^^ stf-
American Council ol Independent Laboratories International Association ot Environmental Testing Laboratories
American Association lor Laboratory Accreditation
IT Analytical Services 5307 Industrial Oats Boulevard, Suite 160. Austin. TX 78735 (S12) 892-6684
Company: COMOCO-LAKE CHARLES REFIHERT Date: 04/19/89 Client Work 10: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Uerk Order: A9-03-075
Job Nuaber: 419900
TEST MAKE: HAZARDOUS SUBSTANCE VOLS
SAMPLE ID: PC1504 BIOLOGICAL SOLIDS
Results in
COMPOUND
acetone benzene 2-butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2-dichloroethane 1,1,1-triehloroethane 1,1-dfchloroethane 1,1,2-trichloroethane 1,1,2,2-tetrachloroethane chloroethane 2-chloroethylvinyl ether chloroform 1,1*dichloroethylene trana-1,2-dichloroethy l ene 1,2-dichloropropene cis-1,3-dichloropropene
*A
VI
<130 <6.5 ` <130 <6.5
<6.5 <6.5 <6.S <6.5 <6.5 <6.5
<13 <13 <6.5 <6.5 <6.5 <6.5 <6.5
mg/kg:
DATE COLLECTED: 0Z/08/89 OATE ANALYZED: 03/Z9/89
COMPOUND
trans'1,3*dichloropropene ethylbenzene 2-hexanone aethylene chloride nethyl chloride nethyl broaide 4-methyl-2-pentanone broaofora broaodichloronethane dibroaochloroaethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cuaene isomers cyclohexane ethylene dibroaide methyl t-butyl ether
<6.5 <6.5
<65 <6.5
<13 <6.5
<65 <6.5 <6.5 <6.5
<6.5-- <6.5 <6.5 <6.5
<65 <13 <6.5 -- 140" <13 <13 <13
Comments: A less than (<) indicates the compound is not detected at the level indicated.
Page 4
ooooofa1''3 t,8? > *
Company: CONOCO-LAKE CHARLES REFINERY Date: 04/19/89 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-075
Job Humber: 449900
TEST NAME: ABN NSL SC/NS EXTIACTABLES
SAMPLE ID: PC1504 BIOLOGICAL SOLIDS
Results in
mg/kg:
DATE COLLECTED: 02/08/89 DATE EXTRACTED: 04/03/89
0ATE ANALYZED: 04/04/89
COMPOUNO
COMPOUND
Phenol
<480
3-Nitroaniline
bis(2-Chloroethyl>ether
<480
Acenaphthene
2-Chlorophenol
<480
2,4-0 initrophenol
1,3 -Dichlorobenzene
<480
4 -Nitrophenol
1,4-Dichlorobenzene
<480
Oibenzofuran
Benzyl alcohol
<950
2,4-0 initrotoluene
1,2-Dichlorobenzene
<480
Diethylphthalate
2-MethyIphenol
<480
4-ChIorophenyl-phenylether
bis(2-Chloroisopropyl)ether
<480
Fluorene
4*Methylphenol
<480
4-Nitroaniline
N-Nftroso-di-n-propyl amine
<480
4,6-Dinitro-2-methylphenol
Hexachloroethane
<480
N-Nitrosodiphenylamine
Nit robenzene
<480
4-Bromophenyl-phenylether
Isophorone
<480
Hexachlorobenzene
2 * N11 rophenol
<480
Pentachlorophenol
2,4-0imethylphenol
<480
Phenanthrene
Benzoic Acid
<2400
Anthracene
bis<2-Chloroethoxy)methane
<480
Di-n-butylphthalate
2,4*0 ichlorophenol
<480
Fluoranthene
1,2,4-Trf chiorobenzene
<480
Pyrene
Naphthalene
<480
Butyl benzylphthalate
4-Chloroanitine
<950
3 ,3 ' -0 ichlorobenzidine
Hexachlorobutediene
<460
Senzo(a)anthracene
4-Chloro-3-methyl phenol 2-Methylnaphthalene
<950 <480
Chrysene bis(2-Ethylhexyl)phthalate
Hexachlorocyclopentadiene
<480
Di-n-oetylphthe late
2,4,6-Trichlorophenol
<480
Benzo(b)fluoranthene
2,4,5 - Trichlorophenol
<480
Benzo(k)fluoranthene
2 -Chloronaph thelene
<480
8 enzo(a)pyrene
2-N i t roaniline
<2400
Indeno(1,2,3-cd)pyrene
Oimethylphthalate
<480
Dibenzol a,h)anthracene
Acenaphthylene
<480
Benzo(g,h,i)perylene
2,6-Dinitrotoluene
<480
Comments: A less than (<) indicates the compound is not detected at the level indicated.
<2400 <480
<2400 <2400
<480 <480 <480 <480
700 <2400 <2400
<480 <480 <480 <2400 1700
500 <480 <480 1000 <480 <950 <480 <480 <480 <480 <480 <480 <480 <480 <480 <480
Page 5
SAL 000006144
LH'S 1 89
Company: COMOCO-IACE CHARLES REFIHERT Date: 04/19/89 Client Work ID: SARA 313 AHALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Uork Order: A9-03-075 Job Number: 449900
TEST NAME: HAZARDOUS SUBSTANCE VOLS
SAMPLE ID: PC150S API SEP BOTTOMS
Results in
COMPOUND
acetone benzene 2*butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2-dichloroethane 1f1,1 -triehloroethane 1,1-dichloroethane 1,1,2-trichloroethane 1,1,2,2* tetrachloroethane chloroethane 2-chloroethylvinyl ether ch lorofora 1,1*dichloroethylene trans-1,2-dichloroethylene 1,2*dichloropropene cis-1,3*dichloropropene
<800 430
<800 <40 <40 <40 <40 <40 <40 <40 <40 <80 <80 <40 <40 <40 <40 <40
mg/kg:
DATE COLLECTED: 02/08/89 OATE ANALYZED: 03/29/89
COMPOUND
trans1,3-dichloropropene ethylbenzene 2*hexanone methylene chloride methyl chloride aethyl bromide 4-aethyl- 2 *pentenone broaofora bromodichioromethane dibromochloromet hane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cumene isomers cyclohexane ethylene dibromide methyl t-butyl ether
<40 220 -- <400 <40 <80 <40 <400 <40 <40 <40 <40 "" <40 770 -- <40 <400 <80 1000 ' 1300 240 <80 <80
nts: A less than (<) indl cates the coapound is not detected at the level indicated.
Page 6
SAL 00006145
CSV < K9
Company; CONOCO-LAKE CHARLES REFINERY Date: 04/19/89 Client Uerk ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN. TX
Work Order: A9-03-075
Job Number: 449900
TEST NAME: ABN NSL GC/NS EXTRACTA8LES
SAMPLE ID: PC1S0S API SEP BOTTOMS
Results in
mg/kg:
OATE COLLECTED: 02/0B/89 DATE EXTRACTED: 04/04/89
DATE ANALYZED: 04/04/89
COMPOUND Phenol
<2600
COMPOUND 3-Nitroaniline
bfs(2-Chloroethyl)ether 2 *Chlorophenol
<2600 <2600
Acenaph thene 2,4*0 initrophenol
1.3-Dichlorobenzene
<2600
4 -N i trophenol
1.4-Dichlorobenzene
<2600
0ibenzofuran
Benzyl alcohol
<5200
2,4-Dinitrotoluene
1,2-Dichlorobenzene 2-MethyIphenol
<2600 <2600
Diethylphthalate 4-Chlorophenyl- phenyl ether
bis(2-Chloroisopropyl)ether
<2600
Fluorene
4-MethyIphenol N-Nitroso-di-n-propyl amine
<2600 <2600
4 -N i troaniline 4,6-Dinit ro-2-aethylphenol
Kexachloroethane
<2600
N -Nitrosodiphenyl amine
Nitrobenzene
<2600
4 -B ronophenyl- phenylether
Isophorone
<2600
Hexachlorobenzene
2-Nitrophenol
<2600
Pentachlorophenol
2.4-0iaethylphenol
<2600
Phenanthrene
Benzoic Acid
<13000
Anthracene
bis(2-Chloroethoxy)methane
<2600
Di-n-butylphthalate
2.4-0ichlorophenol
<2600
Fluoranthene
1.2.4-Trichlorobenzene
<2600
Pyrene
Naphthalene
5400.
Butyl benzylphthalate
4-Chloroaniline
<5200
3,3 *-0ichlorobenzidine
Hexachlorobutadiene
<2600
Benzol a)anthracene
4-Chloro-3-aethylphenol
<5200
Chrysene
2-Hethylnaphthalene
10000
bis(2-Ethylhexyl}phthalate
Hexachlorocyclopentadiene
<2600
Di-n-octylphthalate
2,4,6-Trichlorophenol
<2600
8enzo(b)fluoranthene
2.4.5-Trichlorophenol 2-Chloronaphthalene
<2600 <2600
6enzo(k)fluoranthene B enzo(a)pyrene
2-Mitroaniline
<13000
Indeno(1,2,3-cd)pyrene
Dimethylphtha late
<2600
Dibemo(a,h)anthracene
Acenaphthylene
<2600
8enzo(g,h,i}perylene
2,6 - 0initrotoluene
<2600
Comments: A less than (<) indicates the compound is not detected at the level indicated.
<13000 <2600
<13000 <13000
<2600 <2600 <2600 <2600 <2600 <13000 <13000 <2600 <2600 <2600 <13000 <2600 <2600 <2600 <2600 <2600 <2600 <5200 <2600 <2600 <2600 <2600 <2600 <2600 <2600 <2600 <2600 <2600
Page 7
SAl 00006I46
11
Company: CONOCO-LAKE CHARLES REF INERT Oate: 04/19/89 ' Cl'feht Work 10: SARA 313 AMALTStS
CONOCO-LAKE CHARLES REFIMERT
A903075/01B
1,1*`biphenyl aniline quinoline pyridine O`toluidine 2,6`xylidine
A903075/02B
1,1*-biphenyl aniline pyridine qufnoline O-toluidine 2,6-xylidine
A903075/03B
1,1`-biphenyl quinoline pyridine aniline O-toluidine 2,6-xylidine
Page 8
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-075 Job Nuaber: 449130
<4200 ng/kg <4200 ng/kg <4200 ng/kg <4200 ng/kg <4200 ng/kg <4200 ng/kg
<2400 ng/kg <2400 ng/kg <2400 ng/kg <2400 ng/kg <2400 ng/kg <2400 ng/kg
<13000 ng/kg <13000 ng/kg <13000 ng/kg <13000 ng/kg <13000 ng/kg <13000 ng/kg
SAL 0006I47
<,H? 1 H`l
Company: CONOCO-LACE CHARLES REFINERY Date: 04/19/89 Client Work 40: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Uork Order: A9-03-07S
Job Kuaber: 449900
TEST CODE 8240
TEST NAME HAZARDOUS SUBSTANCE VOLS
Hazardous Substance List Volatiles
ERA 6240-Test Methods for Evaluating Solid Wastes, 3rd Edition, Noveaber 1986. GC/MS Purge and Trap analysis
TEST CODE 8270
TEST NAME ABN NSL CC/MS EXTRACTABLES
Hazardous Substance List Extractables
EPA 8270-Test Methods for Evaluating Solid Waste,3rd Edition, Noveaber 1986. Aeid/Base-Neutral
Extraction followed by GC/MS analysis.
Page 9
SAL 000006148
Grt? I -4)9
(conoco) Conoco,nc
Facility
Qhftrlcs
e/y
Address____________________________________ Telephone ()____-
Transporter Name_____ __________________________ Address____________________________________ Telephone ()____-
Process Producing Sample_______________________ Method of Shipping_______ _______________________ Special Shipping Instructions______________________ Remarks________________________________________
Environmental Quality Sample Chain of Custody Record
Condition of Samples Upon Arrival at Final Destination
Signature
^
~=rr>n
Date
Temp, of Samples Upon Arrival at Final Destination (for Temp. Sensitive Analysis Only).
Signature
7-236 X3, 12-85
Date x/rz/rt
Distribution: White & Canary--Analyzing Laboratory Copies. (White will be returned to Originator with analysis results.)
Pink --Originate* Copy SA(_ Q00006149
INTERNATIONAL TECHNOLOGY CORPORATION
ANALYTICAL SERVICES
CERTIFICATE OF ANALYSIS
CONOCO, INC. P O DRAWER 1267 PONCA CITY OK 74604DON LINDER
Oate: 04/19/89
Job Nuaber: 449900
Work Orders A9-03-074
This ii the Certificate of Analysis for the following saaples:
Client Work IDs SARA 313 ANALYSIS Date Received: 03/16/89 Member of Saaples: 5 Saaple Type: CRUOE AND SOLID* 11
TABLE OF CONTENTS FOR ANALYTICAL RESULTS
PACES 3 5 7 9 11
LABORATORY < A9-03-074-01 A9-03-074-02 A9-03-074-03 A9-03-074-04 A9-03-074-05
SAMPLE IDENTIFICATION PC1636 CRUOE PC1637 SOP OIL EMULSION PC1638 API SEP SOT E.PLANT PC1639 API SEP/LU8E OIL PC1640 NOW-LEADED TANK 80T
Laboratory Manager
American Council ol Independent Laboratories International Association ol Environmental Testing Laboratories
American Association lor Laboratory Accreditation
S*L ooo0o &150
IT Analytical Services 5307 Industrial Oats Boulevard, Suite 160, Austin, TX 78735 (512) 892-6684
tJji i fly
Company: CONOCO, INC. Date: 04/19/89 Client Uorfc ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN. TX
Work Order: A9-03-074 Job Number: 449900
TEST HAKE: HAZARDOUS SUBSTANCE VOLS
SAMPLE ID: PC1637 SOP OIL EMULSION
Results in
COMPOUND
acetone benzene 2-butanone carbon disulfide carbon tetrachloride chlorobenzene 1,2*d(chloroethane 1,1,1 -trichloroethane 1,1-dichloroethane 1,1,2-trichloroethane t,1,2,2-tetrachloroethane chloroethane 2-chloroethylvinyl ether chlorofora 1,1-dichloroethylene trans'1,2-dichloroethylene 1,2'dichloropropane cis-1,3*dichloropropene
<1000 <50
<1000 <50 <50 <50 <50 <50 <50 <50 <50
<100 <100
<50 <50 <50 <50 <50
mg/kg:
DATE COLLECTED: 03/01/89 DATE ANALYZED: 03/29/89
COMPOUND
trans-1,3-dichloropropene ethylbenzene 2-hexanone ethylene chloride Methyl chloride Methyl broMide 4"Methyl- 2 -pentanone broMofotm broModichioronethane dibroMOchloronethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cuaene isomers cyclohexane ethylene dibromide nethyl t-butyl ether
<50 250 <500 <50 <100 <50 <500 <50 <50 <50 <50 <50 310 <50 <500 <100 1300 2300 <100 <100 <100
Comments: A less than (<) Indicates the compound is not detected at the level indicated.
Page 4
SAL 000006151
f>A? 1-H9
Company: CONOCO, INC. Date: 04/19/89 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN. TX
Work Order: A9-03-074
Job Number: 449900
TEST NAME: A8N MSI CC/NS EXTRACTABLES
SAMPLE 10: PC1637 SOP OIL EMULSION
Results in
mg/kg:
DATE COLLECTED: 03/01/89 0ATE EXTRACTED: 04/03/69
DATE ANALYZED: 04/03/69
CONFOUND Phenol bist2-Chloroethyl>ether 2-Chlorophenol 1,3-Dichlorobenzene
<920 <920 <920 <920
COMPOUND
3- Nitroaniline Acenaphthene 2.4- 0 initrophenol 4- Hitrophenol
1,4-Dichlorobenzene Benzyl alcohol 1,2-Dlchlorobenzene 2-Hethylphenot bisl2-Chlorolsopropyl)ether 4-Methylphenol
<920 <1800
<920 <920 <920 <920
Dibenzofuran 2.4- Dinitretoluene Diethylphthalate 4-Chlerophenyl-phenylether Fluorcne 4-N1troaniline
N-Nltro*o-di-n-propyl anine
<920
4,6-D1nitro-2-methylphenol
Hexachloroethane Mitrobenzene Isophorone 2-Nitrophenol 2,4-0imethylphenol
<920 <920 <920 <920 <920
N-Nitrosodtphenylaaine 4-Bromophenyl-phenylether Hexachlorobenzene Pentachlorophenol Phenanthrene
Benzoic Acid
<4600
Anthracene
bis(2-Chloroethoxy)nethane
<920
Oi-n-butylphthalate
2,4-0ichlorophenol
<920
Fluoranthene
1,2,4-Trichlorobenzene
<920
Pyrene
Naphthalene
<920
Butylbenzylphthalate
4-Chloroaniline Hexachlorobutadiene
<1800 <920
3,31-Oichlorebenzfdine 8enzo<a)anthracene
4-Chloro-3-methyl phenol 2-Methyl naphthalene Kexachlorocyclopentadiene
<1800 2100 <920
Chrysene bisl2-thylhexyl)phthalate 0i-n-octylphthalate
2,4,6-Trichlorophenol
<920
Benzo<b)fluoranthene
2,4,5-Trichlorophenol
<920
Benzolk)fluoranthene
2-Chloronaphthalene
<920
Benzols)pyrene
2-Nitroaniline 0imethylphthalate
<4600 <920
Indenol1,2,3-cd)pyrene 0ibenzo1a,h)anthracene
Acenaph thylene
<920
Benzotg.h,i)perylene
2,6-0initrotoluene
<920
Comments: A less than (<) indicates the compound is not detected at the level indicated.
<4600 <920
<4600 <4600
<920 <920 <920 <920 <920 <4600 <4600 <920 <920 <920 <4600 <920 <920 <920 <920 <920 <920 <1800 <920 <920 <920 <920 <920 <920 <920 <920 <920 <920
Page 5
00oo615
2
6? 1-ft9
Coapany: CONOCO, INC. Date: 04/19/89 :llent Work IS: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-074 Job Rusher: 449900
TEST HAKE: HAZARDOUS SURSTANCE VOLS
SAMPLE 10: PC1640 NON-LEADED TANK SOT
Results in
og/kg:
OATE COLLECTED: 03/01/89 OATE ANALYZED: 03/29/89
COMPOUND
C0MP0UN0
acetone benzene 2*butanone carbon disulfide carbon tetrachloride chlorobenzene 1.2-dichloroethane 1,1,1-trichloroethane 1.1-d(chloroethane 1.1.2-trichloroethane 1,1,2,2* tetrachloroethane chloroethane 2-chloroethylvinyl ether chloroforai 1.1-dlchloroethylene trans-1,2-dichloroethylene 1,2*dichloropropene cis-1,3-dlchloropropene
<1100 <55
<1100 <55 <55 <55 <55 <55 <55 <55 <55
<110 <110
<55 <55 <55 <55 <55
trans-1,3-dichloropropene ethylbenzene 2-hexanone aethylene chloride nethyl chloride aethyl broaide 4-methyl-2-pentanone broaofora broaodichloroaethane dibroaochloroaethane styrene tetrachloroethylene toluene trichloroethylene vinyl acetate vinyl chloride xylenes, total cuaene tsoaers cyclohexane ethylene dfbroaide aethyl t-butyl ether
<55 110 ~ <550 <55 <110 <55 <550 <55 <55 <SS <55 ^ <55 120 <55 <550 <110 530 ~ 120 350 <110 <110
Coaaents
A less than (<) indicates the compound is not detected at the level indicated.
Page 10
SAL 000006153
G&M-89
Company: CONOCO, INC. Date: 04/19/59 Client Uork 10: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-074
Job Number: 449900
TEST NAME: ABN NSL CC/NS EXTRACTABLES
SAMPLE ID: PC1640 NON-LEADED TANK BOT
Results i n
mg/kg:
DATE COLLECTED: DATE EXTRACTED:
0ATE ANALYZED:
03/01/89 04/03/89 04/04/69
COMPOUND
COMPOUND
Phenol
<4200
3-H1troaniline
bis(2-Chloroethyl)ether
<4200
Acenaphthene
2-Chlorophenol
<4200
2,4-Dinitrophenol
1, 3-DIchlorobenzene
<4200
4-Nitrophenol
1,4-Dichlorobenzene
<4200
D Ibenzofuran
8enzyl alcohol
<8400
2,4-01nftrotoluene
1,2-Dichlorobenzene
<4200
Oiethylphthelate
2-Methylphenol
<4200
4-Chlorophenyl-phenyl ether
bis(2-Chloroisopropyl)ether
<4200
Fluorene
4-Methylphenol
<4200
4-Hitroaniline
N-N itroso-dl-n-propyl amine
<4200
4,6-Dinltro-2-methylphenol
Hexachloroethane
<4200
N-M11rosodiphenyl amine
Nitrobenzene
<4200
4-Bromophenyl-phenylether
1sophorone
<4200
Hexachlorobenzene
2-N1trophenol
<4200
Pentachlorophenol
2,4-01methylphenol
<4200
Phenanthrene
Benzoic Acid
<21000
Anthracene
bisl2-Chloroethoxy)methane
<4200
Di-n-butylphthalate
2,4-0ichlorophenol
<4200
Fluoranthene
1,2,4-Trichlorobenzene
<4200
Pyrene
Naphthalene
<4200 -
Butyl benzylphthalate
4-Chloroanil1ne
<6400
3,3*-Dichlorobenzidine
Mexachlorobutadiene
<4200
Benzo(a)anthracene
4-Chloro*3-methyl phenol
<8400
Chrysene
2-Methylnaphthalene
<4200
bisCZ-Ethylhexyl)phthalate
Hexachlorocyclopentediene
<4200
Di-n-octylphthalate
2,4,6-Trlchlorophenol
<4200
8enzo(b)fluoranthene
2,4,S-Trichlorophenol
<4200
Benzo(k)fluoranthene
2-Chloronaphthalene
<4200
Benzol a)pyrene
2 - N 11 roan(line
<21000
lndenol1,2,3-cd)pyrene
Oimethylphthalate
<4200
Dibenzola,h)anthracene
Acenaphthylene
<4200
8enzolg,h,i)perylene
2,6-Dinit rotoluene
<4200
lommentc: A less than (<> indicates the compound i s not detected at the level indicated.
<21000 <4200
<21000 <21000
<4200 <4200 <4200 <4200 <4200 <21000 <21000 <4200 <4200 <4200 <21000 <4200 <4200 <4200 <4200 <4200 <4200 <8400 <4200 <4200 <4200 <4200 <4200 <4200 <4200 <4200 <4200 <4200
Page 11
ooooo^s*
Coapany: CONOCO, INC. Date: 04/19/89 Client Work ID: SANA 313 ANALYSIS
CONOCO. INC.
A903074/018 A903074/026 A903074/036 A903074/04B A903074/05B
1,1*'biphenyl aniline pyridine quinoline 0-toluidine 2,6-xylidine
1,1'-biphenyl aniline pyridine quinoline O'toluidine 2,6-xylidine
1,1*-biphenyl aniline pyridine quiniline 0-toluidine 2,6-xylidine
1,1*-biphenyl aniline pyridine quiniline O'toluidine 2,6-xylidine
1,1*-biphenyl aniline pyridine quinoline 0-toluidine 2,6-xylidine
Page 12
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03'Q74 Job Nuaber: 449900
<4900 g/kg <4900 g/kg <4900 g/kg <4900 g/kg <4900 g/kg <4900 g/kg
<4600 g/kg <4600 g/kg <4600 g/kg <4600 g/kg <4600 g/kg <4600 g/kg
<230001 g/kg <23000 g/kg <23000 g/kg <23000 g/kg <230001 ag/fcg <230001 ag/kg
<2500 g/kg <2500 g/kg <2500 g/kg <2500 g/kg <2500 g/kg <2500 g/kg
<21000 g/kg <21000 g/kg <21000 g/kg <21000 g/kg <21000 g/kg <21000 g/kg
SAL 000006155
Company: CONOCO, INC. Date: 04/19/69 Client Work ID: SARA 313 ANALYSIS
IT ANALYTICAL SERVICES AUSTIN, TX
Work Order: A9-03-074 Job Huaber: 449900
TEST CODE 8240
TEST NAME HAZARDOUS SUBSTANCE VOLS
Hazardous Substance List Volatiles
EPA 8240-Test Methods for Evaluating Solid Wastes, 3rd Edition, Noveaber 1966. GC/MS Purge and Trap
analysis
TEST CODE 8270
TEST HAKE ABN NSL CC/NS EXTRACTASLES
Hazardous Substance List Extractables
EPA 8270-Test Methods for Evaluating Solid Waste,3rd Edition, Noveaber 1986. Acid/8ase-Neutral Extraction followed by GC/MS analysis.
Page 13
SA<- 000006156
Ji? 1
(conoco) Conocolnc
Facility_______ PtX\Cfr CjfY
Address_____________ ______________________ Telephone ()____-______
Transporter Name
^--
Address____________________________________ Telephone ()____-______
Process Producing Sample_______________________
Method of Shipping_____ 0 VjtHltfht.___________
Special Shipping Instructions______________________ Remarks________________________________________
Environmental Quality Sample Chain of Custody Record
Sample
to No.
Sample Location
Oate Time
Ctitdt.
3/r/rt
PC/&3? ShpOi'l &'**Istsn Sahd-s
3/i/tf
PC/03t ttH Sf*riar-
- //W
m - Luk. Off 77 A
PdlLHa
7Aa<
*s
V
A?
Sample Type
L&htvsrk* (iru/r 0t! StUJS UtsfcS \
A
Ni/
Total Vol
Containers Type No.
Employee
lure)
Relinquished by: (Signature)
wished by (Signature)
ReHnquished by (Signature)
Relinquished by: (Signature)
Relinquished by (Signature)
Received by(Sig Received by. (Signature) Received by: (Signature Received by(Signaiure) Received by: (Signature) Received by: (Signature)
te/Time
/
'f?M I <*j* Date/Time
Date/Time
Date/Time
Date/Time
Date/Time
Condition of Samples Upon Arrival at Final Destination________________
Signature
'ttf-s
riato Z/zy/V
mp. of Samples Upon Arrival at Final Destination (for Temp. Sensitive Analysis Only).
Signature
Date 3/-7A7
Distribution: White & Canary--Analyzing Laboratory Copies. (While will be returned to Originator
with an^tvsis results.)
Pir-L . - O'l'-'ir.TlO' r'/llv SAL 000006157
ANALYTICAL SPECTROSCOPY REPORT
istomer: Cindy Quy
ReferencesESICP #1 p. 189
tte Analyzed: 05/01/89
Analytical Code: ESICP
finery Solid Waste/Communtiy Right--To--Know
tits: ug/g
imo 1 e #
JV901442 PC- - 1 S'Ot/ W901443 PC--150^
A1
1700 3800
4V901447 PC -- iio<g 901450 PC- --
630 7300
'JV901451 PC - \SIp1
MV90145S PC - IS(08
18,000 6.4
W901455 fC - JL.37 MV901456 PC - 1033
W901457 PC -16*37 NV90145Q PC -logo
250 1200
590 1000
Cr
Ba
160 8.8
14 19
110 <1 .0
96 130
34 200
Cu
Be
<1.0 <1.0
<1.0 <1 -O
1.4 1.7
<1.0 <1.0
<1.0 <1.0
Ni
A
b*
4
O
Cd
<1.0 2.5
13 <1.0
1.3
<1.0 1.2
<1.0 <1.0
V
Co
<2.5 X ff&Lfa CJxoaJjuJ 9.4 ^
46
<2.5 V ;? Qcav'kxo'
6.8 / <2.5 /
<2.5 v 2.6 \ ^
?\ UAV^IA.
<2.5/^
* Ujw
Zn
IMV901442 NV901443
17 34 11 39 1 lO 53
28 110 55 540
NV901447 NV901450
160 26
450 7.8
170 28
150 17
1600 15
NV901451 IMV901452
O
H V
27 1 1 <1.0
16 35 59 50 200 1.8
NV901455 NV901456
160 470
54 140
8.6 26
5.1 12
130 370
NV901457 "*9901458
36 100
180 72
3.2 15
2.7 13
190 140
Sample preparation: Muffle ash at 450 degrees Centigrade; Aqua--regia digest.
eported
O*
ate_^/S^______________
jLxA_
Reviewed Date__/_a_j_a.3
ooooo^59 SM-
ANALYTICAL SPECTROSCOPY REPORT
istomer: Cindy Quy
Reference: ESICP #1 p. 189
tte Analyzed: 05/01/B9
Analytical Code ESICP
?finery Solid Waste/Communtiy Right--To--Know
lits: ug/g
W901A51 Dup . \iV901AA7 Dup.
1 ^nk nk
lank lank
1 2 3 A
er. Stdrue Value
A1
17,000 790
<0.16 <0. 16 <0.16 <0. 16
0.96 0.97
Qa
HO 17
<0.006 <0.006 <0.006 <0.006
1.1 0.97
Be Cd
1.3 <1.0
1.3 13
<0.006 <0.006 <0.006 <0.006
<0.016 <0.016 <0.016 <0.016
0.97 0.96
1. 1 0.9A
Co
6.1 A8
<0.11 <0.11 <0.11 <0.11
0.92 1 .00
amgle_#
NV901A51 Dup. NV901AA7 Dup.
lank lank lank lank
1 2 3 A
er. Std. rue Value
Cr
28 1Q0
<0.031 <0.031 <0.031 <0.031
1 .2 1.03
Cu
11 A90
<0.016 <0.016 <0.016 <0.016
0.99 1 .03
Ni
15 190
<0.076 <0.076 <0.076 <0.076
1.1 1.02
V
30 170
<0.026 <0.026 <0.026 <0.026
0.99 1 .Ol
2n
61 1600
<0.026 <0.026 <0.026 <0.026
0.99 1.01
ample preparation: Muffle ash at A50 degrees ICentigrade ; Aqua--reg
!ep_.'ted >ate__
Reviewed ByjZfc SAL 000006159
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SAL 00006I62
ENGELHARD CORPORATION SPECIALTY CHEMICALS OlVISlON MENLO PARK, ON 28 EDISON, NEW JERSEY 08818
1CCHNICAL SERVICE REP : 8. A. GILLJ.S
TELEPHONE:
: 713-627-0619
DOTE : 12-21-88
LTFINFKY : CONOCO CONOCO, INC. P.O. BOX 37 WESTLAKE , LA 70669
ICC UNIT NO : 1018-03-1
FCC l UILIBRIUM CATALYST ANALYTICAL DATA REPORT
COPIES TO s
D. R. UNRUH B. CASON T. WALTRIP P. F. MORSTEAD ERIC VETTERS
L.T. WINGER
P.i
S.H. DEPRIEST P,C,
B. CHAHAR
).,
D.L. WOHLGENANT P. E
K. A. SECK
REFINERY UNIT NO
UNIT DESCRIPTION
: KELLOGG ORTHOFLO
CATALYST INVENTORY
i 90 TONS
NOMINAL UNIT CAPACITY : 35000 BPD
T. WALTRIP CONOCO. INC. P.O. B&X 1267
EAST PLANT T.S.LAB
PONCA CITY , OK 76603
. SAMPLE
, M.A.T.
RECV DATE
ID
DATED ACT
C.F.
ii PHYSICAL PROPERTIES
PAR. SIZE MICRi INS
T-2tr 6-40 0-00 WT.% WT.% WT.%
APS
S.A. M2/G
ABD G/CC
CU PPM
CHEMICAL PROPERTIES
MISC TESTS
Nl v FE NA c AL203 TI PPM PPM WT.% WT.% WT.% UT V. im
REO WT 7.
CATALYST
REMJ*
RPC \
RATIO l
0801 194 0728 i':` 7 0 .70 0 12 67 65 170 .90 20 429 1596 .40 .22 .08 53.51 1.30 3.26 HEZ-E5
0S08 195 0803 ^,70 .84 ^ 0 12 65 67 169 .88 34 395 1451 .39 .21 .05 53.56 1.31
OS-12 196 0810 t74 .88
o 10 65 68 164 .90 48 421 1439 .40 .22 .09 53.80 1.32
0818 197 0817 **6? .87 0 10 64 69 164 .89 20 420 1456 .40 .22 .07 53.93 1.31
0923 202 0821 .75 .78
D 13 67 67 176 .86 20 41C 1264 .39 .24 .06 54.21 1.31
09D1 198 0824 $73 .80
2 12 67 64 167 .86 20 419 1433 .40 .21 .07 53.95 1.32 3.19
0908 199 0831 $72 .86
1 12 68 66 169 .87 20 434 1451 .39 .23 .06 53.73 1.30
0914 0916
200 0907 201 0914
$7723
.79 .76
1 `2
9 11
65 68
69 175 .90 68 172 .85
20 435 1417 .40 .22 .07 54.18 1.31 20 444 1427 .40 .23 .07 54.22 1.31
0930 203 0928 *72 .75
0 14 63 68 176 .86 20 393 1193 .40 .22 .06 54.32 1.29 3.16
1006 204 100S 74 .77
1 11 66 68 180 .84 20 405 1172 .40 .24 .09 54.51 1.30 3.10
1013 2 OS 1012 ?71 .81
0 14 67 64 179 .86 20 393 1112 .40 .23 .10 54.57 1.29
1020 206 1019 *72 .77 . .1 11 64 69 183 .87 20 436 1160 .45 .24 07 54.60 1.2-9
1027 207 1026 Y73 .81 1103 208 1102 72 .80
0 10 69 67 180 .85 20 455 1135 .45 .25 .07 54.53 1.28 2 12 66 68 186 .84 20 441 1077 .45 .25 .06 54.65 1.28 2.91
1110 209 1109 76 .76
1 11 63 70 173 .86 20 445 1062 .45 .26 .09 54.96 1.29
1117 210 1116 ~ 71 .81
0 12 69 63 176 .86 20 444 1122 .44 .25 .16' 54.86 1.29
v>
>
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1202 213 1116 74 1.202 214 1118 72 1128 211 1123 -N72
.77 .84 .85
0 13 63 67 174 .86 20 467 1249 .42 .24 .06 53.74 1.25 1 14 65 65 176 .85 20 453 1204 .43 .24 .06 S3.97 1.26 0 10 65 69 178 .86 20 450 1193 .43 .24 .06 54.91 1.30
O o Q O
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SEND SAMPLES TO: ENGELHARD CORP., CATALYST SERVICE DEPT.. MENLO PARK. CN 28. EDISON. NJ 08818; (201)-321-5370
^ c (conoco)
Interoffice Communication
To Mike Pannell - Ponca City
From
Lloyd T. Winger - Houston
Date
October 21, 1987
Subject
ESTIMATED CATALYST LIVES FOR NAR KYDROPROCESSING UNITS
T^-
As we discussed recently, you are attempting to establish standard amortization procedures for North American Refining hydroprocessing catalyst. Since these amortization procedures depend on the catalyst life, the attached Tables I and II give the estimated catalyst life for precious metal and non-preclous metals hydroprocessing catalysts, respectively.
Please call if you need more information, or if you have questions.
Lloyjf TL Winger Operations Analysis MT&E
LTW:ci MT20/ltw3
cc: KVM, RJH, EMR, JTM, File .7 - Houston RGM, PCP, SHD - Ponca City MSJ - Billings FDB - Denver GWP - Lake Charles
SAL 000006164
NAS. PRECIOUS METALS CATALYST CATALYTIC REFORMERS
UNIT
Billings No. I No. 2
Denver existing new
Ponca City No. 2 No. 3
Lake Charles No. 2 No. 3
CATALYST
Chevron D/E Chevron F
Chevron F Chevron F
Chevron F Chevron F
Chevron F U0P R-62
ESTIMATED LIFE YRS
5-15 5-15
5-15 5-15
5-15 5-15
5-15 3-5
AMOUNT MLBS
15 70
30 (70)
150 120
72 62
ISOMERIZATION UNITS
Billings Butamer
Ponca City Butamer Penex (future)
UOP 1-8
UOP 1-8 UOP 1-7
3-7
3-7 5
9
22 (100)
DESCRIPTION
Pt/Re on Alumina
Pt/Re
M
Pt/Re Pt/Re
11 11
Pt/Re Pt/Re
Pt/Re Pt/Sn
If 11
11
,, (1)
Pt on alumina
Pt Pt and zeolites on alumina
Pt = Platinum Re = Rhenium Sn = Tin
(1) Continuous make up of fines due to attrition losses for cat circulation (approximately 500 lb/month).
SAL 000006165
TABLE II CONOCO NAR HYDROTREATING CATALYSTS
UNIT
Billing No. 1 No, 2 LCO
Denver NDS DHDS
Ponca City No. 2 No. 3 Cycle Cdl FCC GCHDT
Lake Charles No. 1 No. 2 No. 3 No. 4 No. 5 No. 6 No. 7 *fo. 8
FEED ^
N, K, D N, K, D D
N K, D, G.O.
N N D G.O.
N, K N N H.K.D G.O. K. D G.O. Hvy Oil
CURRENT CAEALZST
S-344/444 S-344/444 S-344/444
S-344 S-444
KF-840 HM-30 S-324 S-424/HDR-30
S-424/HCN-30 S-424/BCN-30 S-424 S-444 S-444 S-444 S-42A/HM-30 S-444
ESTIMATED LIFE YRS
<1 2
2-5
5+ 1-2
2 5+ 5+ <1
<1 2
1-2 1-2 <1 1-2 <1 <1
AFDUNT MLBS
40 127
15
73 60
117 72 48 165
27 72 30 87 98 130 200 125
DESCRIPTION ^
Regenerated Co/Mo Regenerated Co/Mo Regenerated Co/bfo
Regenerated Co/to New Co/to
New Ni/fo Regenerated Ni/Mo New Ni/Mo Regenerated Ni/Mo
Regenerated Ni/Mo Regenerated Ni/Mo New Ni/Mo New Co/Mo New Co/Mi Nor Co/Mo Regenerated Ni/Mo New Goto
(a) N = naphtha, K kerosoie, D *= diesel. G.O. * gas oil (b) Current load, note that mast unites ran use riagmararad catalyst.
sal
0oO06166
Don R. Goff
(conoco)
to fade jr&fcje:
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OOOOO6I67 $M-
CATALYSTS
PRODUCT BULLETIN:
CRITERION* 444 Cobalt/Molybdenum Hydrotreating Catalyst
CRITERION 444 catalyst is a cobatt/molybdenum catalyst on an extruded alumina base. It was devel oped for applications requiring greater desulfuriza tion activity than available from the best secondgeneration catalysts. CRITERION 444 uses new technology to increase the efficiency of the active metals providing a 10-20F (6-11C) improvement in activity relative to CRITERION 344 at no increase in catalyst density. Moreover, CRITERION 444 pos sesses the same high stability and strength charac teristic of all CRITERION catalysts.
Applications
CRITERION 444 is recommended where the utmost in desulfurization activity is desired. It was principally
developed for cycle oil and vacuum gas oil opera tions where refiners are, ever more frequently, being faced with feedstock sulfur levels increasing to well above design. In these services, the high activity of 444 enhances both product quality and run length relative to second-generation catalysts. CRITERION 444 may also be used profitably with lighter feed stocks, particularly if the unit is underdesigned or if significant debottlenecking is desired.
Packaging and availability
CRITERION 444 is available as 1/16-, 1/10- and 1/8inch (1.5,2.5, and 3.0 mm) TRILOBE* or cylindrical extrudates, packed in steel drums or in flexible bulk containers.
Typical Properties
Shape Nominal size, in (mm) Loss on ignition at 900F (482C), wt % Chemical composition, wt % dry basis
Cobalt A* c*>
Molybdenum oi m o Physical properties
Surface area, m2/g Pore volume, cc/g Side plate crush strength,lb (kg) Bulk crushing strength,1 kg/cm2 Attrition index1 Reactor loading density, lb/ft3 (kg/I) Compacted bulk density, lb/ft3 (kg/I)
Cylinder441 1/16 (1.5)
1.1
3.2 9.6
230 0.57 18(8.2)
15 99+ 42-44 (0.67-0.71) 48 (0.77)
3/16-mch-tong particles 01 Pressure applied to produce 0.5% w fines <40 mesh TM wt % retained on 20 mesh screen after tumbling 1 hour at 40 rpm w Also available as TRILOBE extrudates
Cylinder441 1/10(2.5)
1.1
Cylinder441 1/8 (3.0)
1.1
3.2 3.2 9.6 9.6
230 0.57 20 (9.1)
15 98+ 42-44 (0.67-0.71) 48 (0.77)
230 0.57
23(10.5) 15 96+
42-44 (0.67-0.71) 48 (0.77)
CRfTERiON CATALYST COMPANY L.P. TWO GREENSPOINT PLAZA. SUtTE 1000. 1682S NORTHCHASE DR. HOUSTON. TEXAS 77060. 713/874-2600
`Trademark
' CCC-121
2K S/B8
SAL 000006168
CATALYSTS
PRODUCT BULLETIN:
CRITERION* 424 Nickel/Molybdenum Hydrotreating Catalyst
Introduction
CRITERION 424 catalyst is a third-generation nickel/ molybdenum catalyst on an extruded alumina base. It was developed for use in severe, heavy oil services in which diffusional limitations may be a problem. This applies to all heavier-than-distillate feedstocks. CRITERION 424 provides much better activity and stability than traditional Ni/Mo catalysts. This catalyst differs from CRITERION 324 in several ways: The most significant change is a totally new
technology for distributing the metals on the catalyst. The technique provides a much more even dispersion of metals throughout the catalyst The base has been modified to make the catalyst more tolerant to metals and contaminants. CRITERION 424 is 3-lobed in shape to reduce
diffusional limitations.This catalyst has the same high strength characteristics that all CRITERION catalysts share, and the product has been dense loaded in nearly every application to date. The 3lobed shape also provides reduced pressure drop compared with the same sized cylinder. The metal content was optimized for heavier feedstocks.
Commercial experience
VGO hydrotreating and hydrocracker pretreating CRITERION 424 found rapid acceptance throughout the industry, in less than one year it was purchased by a dozen companies in over 20 locations through out North America. It has been extremely successful in both first-stage hydrocrackers and VGO hydro-
Typical properties
Shape
Nominal size, in (mm)
Loss of ignition at 900F (482C), wt %(1>
Chemical composition, wt % dry basis
Nickel * s
o
Molybdenum as
03
Physical properties
Surface area, m2/g
Pore volume, cc/g
Side plate crush strength, lb (kg)
Bulk crushing strength, kg/cm2
Attrition index141
Reactor loading density, lb/ft3 (kg/1)
Sock loaded
Dense loaded
Compacted bulk density, lb/ft3 (kg/I)
TRILOBE* 1/16(1.5)
0.7
3.0 13.0
162 0.47 24(10.9)
16 99+
47-48 (0.75-0.77) 52-53 (0.83-0.85)
52 (0.83)
TRILOBE 1/10 (2.5)
0.7
3.0 13.0
160 0.47 37(16.8)
17 98+
47-48 (0.75-0.77) 52-53 (0.83-0.85)
52 (0.83)
TRILOBE 1/8 (3.0)
0.7
3.0 13.0
156 0.47 47 (20.9)
18 98
47-48 (0.75-0.77) 52-53 (0.83-0.85)
52 (0.83)
'" As manufactured
3/16-inch-long panicles 01 Pressure applied to produce 0.5% w fines<40 mesh 1,1 wl % retained on 20 mesh screen after tumbling 1 hour at 40 rpm
SAL 000006169
CRITERION CATALYST COMPANY LP. TWO GREENSPOINT PLAZA. SUITE 1000. 16025 NORTHCHASE DR. HOUSTON. TEXAS 77060. 713/674-2600
Trademark
CCC-120
k s.-sa