Document n9BE5w3mznKeMnyDo71dNyLjX
RECYCLED C'yi
AR226-2661
RESEARCH
AR226-2661
Analytical Report
Air Sampling Fluorochemical Report
DuPont Washington Works-Air Sampling Program Round 5
Exygen Research Report No. L0001400
Testing Laboratory
Exygen Research . 3058 Research Drive State College, PA 16801
Requester
Michael D Aucoin URS Corporation Barley Mill Plaza Building 27 Room 1260 Lancaster Pike and Rt 141
Wilmington, DE, 19805
ALL DATA-CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 1 of 7
3058 Research Drive State College, PA 16801, USA
T: 800.281.3219 F: 814.272.1019 exvaen.com
Summary
,".''' /^'':' : ; .
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Seven solid media samples were received by Centre Analytical Laboratories, Inc. (dba Exygen Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes
collected. Sample WWK-A-AMS4-E5 had sampler problems during collection. No results are
reported for this sample.
The samples were analyzed for Perfluorooctanoic Acid (C8 Acid) using liquid chromatography /mass spectrometry (LCMS). The method employed is entitled "Method of Analysis for the Determination of Perfluorooctanoic Acid (PFOA) in OVS Airtubes by LCMS" (James Miller,
Exygen Research, February 17, 2003).
The OVS tubes were separated into three fractions for specific fluorochemicai analysis.
Fraction A consisted of the filter, backing material and plastic ring. Fraction B contained the
. . - . ' , -'',, first bed of XAD resin and the PUF backing. Fraction C contained the second bed of XAD
^Nlli?
'
.
.
.
'
.. , .
resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C
was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (C10 Acid)
" was added as a surrogate spike to each fraction prior to extraction.
Instrument operating conditions can be found at the beginning of each analytical run. Raw
instrument data is given in Appendix A. Chain-of-custody information can be found in
AppendixB.
;
9* 3 ' 1
.
'
'
'
'
. ^
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Pae 2 of 7
Results Summary
Request #
WWK-A-AMS1-E5 A WWK-A-AMS1-E5 B WWK-A-AMS1-E5 C WWK-A-AMS1-E5 (Total)
; Air Volume Sampled (L)
1480 1480
.
1480
C8Acid (mg/m3)
'
< 0.00007 < 0.00007
NA < 0.00014
WWK-A-AMS2-E5 A WWK-A-AMS2-E5 B WWK-A-AMS2-E5 C : WWK-A-AMS2-E5 (Total)
WWK-A-AMS3-E5 A WWK-A-AMS3-E5 B WWK-A-EMS3-E5 C WWK-A-EMS3-E5 (Total)
WWK-A-AMS5-E5 A WWK-A-AMS5-E5 B WWK-A-AMS5-E5 C WWK-A-AMS5-E5 (Total)
1459 1459 , 1459
1460.
1460
1460
'
: 1462 . .
-1462
.
1462
0.0007 < 0.00007
MA 0.0007
0.0007 < 0.00007
NA . 0.0007
< 0.00007 .: < 0.00007
NA < 0.00014
WWK-A-AMS6-E5 A WWK-A-AMS6-E5 B WWK-A-AMS6-E5 C WWK-A AMS6-E5 (Total)
1479 1479 1479
< 0.00007 < 0.00007
NA
< 0.00014
NA - Not Analyzed. B fraction was below the quantitation limit, therefore the backup fraction does not require analysis. 1. "<" is defined as not detected at or above the reported level.
2. Sample results have not been corrected for blank results or control spike recoveries.
3. Please note the following descriptions of the OVS sample tube fractions:
Fraction
Fraction Description
Frit Extract 1st set beads extract 2nd set beads extract
(not analyzed)
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 3 of 7
Please note: One control sample was spiked with each perfluorooctanoic acid to give a final concentration of 500 pp through the tube at a rate of 1-liter per minute for one hour (60 liters of air). The fractions were separated and analy
'
acceptable range for control recovery is 75-125%.
Request# Control 1
CSAcid (amount spiked - ppb)
500
CSAcid (amount recovered -
508
ppb)
CSAcid
(percent recovery 102
Blanks
Request # WWK-A-AMSFBLK-E5 A WWK-A-AMSFBLK-E5 B
Vol. Of Air (L)
0
. .
0
C8Acid
(ug/fraction)
<0.10
<0.10
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 4 of 7
B Surrogates I A surrogate spike (C10 Acid) was added to allOVS tubes to give a final concentration of 500 ppb in the extract.
Surrogate spike recoveries are given in the following table. There are no set criteria for surrogate spike recoveries. Advisory ranges-are 75-125%.: : ;
.
Sample #
.
,
Amount Spiked
'
(ppbF
Amount Recovered
(ppb)
Percent Recovery (%]
I WWK-A-AMSFBLK-E5 A ~ WWK-A-AMSFBLK-E5 B WWK-A-AMS1-E5A ,
.
500
500. ,
'
500 ' :
558 295 500
112 59* 100
. WWK-A-AMS1-E5B
-
^ ; ,
.550000 WWK-A-AMS2-E5 A :
:
;
WWK-A-AMS2-E5 B ' .
'.: ' : 500
.WWK-A-AMS3-E5A . .
500
:'? :
.'. -
319 . 490
334 482
64* 98 67* 96
WWK-A-AMS3-E5 B
: \500 '-
.../- : 289
:
58*
,
WWK-A-AMS5-E5A WWK-A-AMS5-E5 B
, -: .500 -.:' . \ . ~
.
496 315
.
'/;-^-'':550000'- : WWK-A-AMS6-E5 A
':
." . .
488
WWK-A-AMS6-E5 B ^ ^ - '^oo^ ; :^ .'-:" : 317":'-"
Control Spike A
'
500
"/ 552
.' Control Spike B
500
\
331
99 63* 98 63* . 110 66*
* Surrogate recovery outside of advisory range.."
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 5 of 7
Calculations
Request#
WWK-A-AMSFBLK-E5 A WWK-A-AMSFBLK-E5 B
WWK-A-AMS1-E5A ,WWK-A-AMS1-E5B
'
WWK-A-AMS2-E5 A WWK-A-AMS2-E5 B WWK-A-AMS3-E5 A WWK-A-AMS3-E5 B WWK-A-AMS5-E5 A WWK-A-AMS5-E5 B WWK-A-AMS6-E5 A WWK-A-AMS6-E5 B
Control Spike A Control Spike B
Vol. Of Air
(L)
0
0
1480 1480 1459 1459 1460 1460 .. 1462 1462 1479 1479
0
0
C8 Acid
(raw-ppb)
<10 <10 <10 <10
1020
<10
1074
<10 <10 <10 <10 <10
508
<10
08 Acid
(ug/fraction)
<0.10 <0.10 <0.10 <0.10
1.0
<0.10
, 1.0
<0.10 <0.10 <0.10 <0.10 <0.10
0.51
<0.10
08 Acid (mg/m3) .
< 0.00007 < 0.00007
0.0007 < 0.00007
0.0007 < 0.00007 < 0.00007 < 0.00007 < 0.00007 < 0.00007
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 6 of 7
. \ ^".^h:' S^^amEle^alculation'
:;"
Por sample WWK-A-AMS2-E5 A C8 'Acid, ^^; '
:
=
[1020 ng/ml of C8 Acid x (1ml) x (1 ug / 1000 ng) x (1 mg / 1000 ug) ] / [(1459 L) x (1 m3 /
'
......-^^l.OOOL)],:.'.',;'':'^^-."^'-'"^":.-'. . .',,., ...
.
,. . \
.0.0007 mg/m3
Signatures
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-
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? ;l^;IIV(i. ^\ ^' \-~-~Jvs
'",. .
Paul Conn1o1 ily, LC;MSTeam LBader^ ^ :,', V^,
a/W fU^^^Wf. ^./i^.^-'-:':; \: ^.'';
<John M. Flaherty, VifcePresident ; -;;^^,-^ ..,
Other Lab Members Contributing to Data;? ^.
James Miller
M^/^^
Date
^ M i Date
ALL DATA CONTAINED INTfflS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 7 of 7
Table 1. Login Information / Field Data
Sample ID
Exygen Lab ID
'
Date Received Description
Air Volume Sampled (L)
WWK-A-AMSFBLK-E5 A
L0001400-1
12/2/03
Frit extract
:
:
0
WWK-A-AMSFBLK-E5 B WWK-A-AMSFBLK-E5 C
WWK-A-AMS1-E5A
L0001400-2 L0001400-3 L0001400-4
.12/2/03
12/2/03
12/2/03
1st set beads extract 2nd set beads extract Frit extract
.00 1480
WWK-A-AMS1-E5B
L0001400-5
12/2/03
1st set beads extract
1480
WWK-A-AMS1-E5C
L0001400-6
12/2/03
2nd set beads extract
1480
:
WWK-A-AMS2-E5 A
L0001400-7
12/2/03
Frit extract
:
1459
WWK-A-AMS2-E5 B
L0001400-8
12/2/03
1st set beads extract
1459
.
WWK-A-AMS2-E5 C
L0001400-9
12/2/03
2nd set beads extract
1459 '
.
-
,
.
.' ;
WWK-A-AMS3-E5 A
L0001400-10 . 12/2/03
Frit extract
1460
,
WWK-A-AMS3-E5 B
L0001400-11
12/2/03
1st set beadsextract
1460
WWK-A-AMS3-E5 C
L0001400-12
12/2/03
2nd set beads extract
1460
WWK-A-AMS5-E5 A
L0001400-16
12/2/03
Frit extract
1462
o
WWK-A AMS5-E5 B
L0001400-17
12/2/03
1st set beads extract
.
1462
0
WWK-A-AMS5-E5 C
L0001400-18
12/2/03
2nd set beads extract
1462
c':;
WWK-A-AMS6-E5 A
L0001400-19
12/2/03
Frit extract
1479
'
ex.
WWK-A-AMS6-E5 B
L0001400-20
12/2/03
1st set beads extract
1479
WWK-A AMS6-E5C
Control Spike A Control Spike B
L0001400-21 L0001400-22 L0001400-23
12/2/03 12/2/03 12/2/03
2nd set beads extract Frit extract 1 st set beads extract
1479
,.'' '0 '
'/1/- :'.'
'
!
- 0-
.
.
Control Spike C
L0001400-24
12/2/03
2nd set beads extract
: !
!
"
0 '
'
'.'
..
Table 2. Chain of Custody
Sample ID
WWKrA-AMSFBLK-ES A WWK-A-AMSFBLK-E5 B WWK-A-AMSFBLK-E5 C
WWK-A-AMS1-E5A WWK-A-AMS1-E5B WWK-A-AMS1-E5C WWK-A-AMS2-E5 A WWK-A-AMS2-E5 B WWK-A-AMS2-E5 C WWK-A-AMS3-E5 A WWK-A-AMS3-E5 B ' WWK-A-AMS3-E5 C WWK-A-AMS5-E5 A WWK-A AMS5-E5 B WWK-A-AMS5-E5 C WWK-A-AMS6-E5 A WWK-A-AMS6-E5 B WWK-A AMS6-E5C
Control Spike A Control Spike B Control Spike C
Date Collected
Date Received at Exygen
11/30/03 11/30/03 11/30/03 11/30/03
.
11/30/03' 11/30/03 11/30/03 11/30/03 11/30/03 11/30/03 11/30/03 11/30/03 11/30/03 11/30/03 : 11/30/03 11/30/03 11/30/03 11/30/03
NA
NA
NA
12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03
12/2/03..
12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 12/2/03 : 12/2/03
Date Extracted by Exygen ,
Date Analyzed by Exygen
12/11/03
12/11/03
NA
12/11/03. 12/11/03
. NA
12/11/03
12/11/03
;
. NA
12/11/03
12/11/03
NA 12/11/03
12/11/03 NA
12/11/03
12/11/03
NA 12/11/03 '
.
12/11/03
NA
12/11 -12/12/03
12/11 -12/12/03
NA
12/11 -12/12/03
12/11-12/12/03
NA
12/11 -12/12/03
.12/11 -12/12/03
NA
.'.
.
12/11-12/12/03 12/11 -12/12/03
NA
12/11 -12/12/03
12/11 -12/12/03
NA
12/11 -12/12/03
12/11-12/12/03 NA'
12/11 -12/12/03
12/11-12/12/03 NA
Login #:
1510
Project:
P0000419
Project Storage: Company Name: Submitted By:
Status:
DuPont de Nemours & Co, Inc. Michael D. Aucoin
Unreceived
Login Type: Started: . Date Start: Due Date: Received Date:
Immediate Receipt of Samples
T :
'.
^
.... .
.
12/02/2003
.
.
.
12/16/2003
12/02/2003
Received By:
AMMERMAN, MARK
Spread Sample:
Label:
Project Title/Type: Analysis of PFOA in OVS Tubes / ROUTINE
Exygen SD/PI: MILLER, JAMES .
Login Notes:
Conform Notes:
Conform COC: Conform Sample: Conform Request:
;K0001982 Carton
Packages/Containers
Mail Date / Condition
Shipper /_ID
12/2/2003 10:30:09PM Package & Contents Uncompromised
FEDEX 8363913019710200
Temp. Control/Temp.
None 23.3
Container # C0020357 C0020358 C0020359 C0020360 C0020361 C0020362 C0020363 C0020364 C0020365 C0020366 C0020368 C0020369 C0020370 C0020371 C0020372
, C0020373 C0020374 C0020375 C0020376 C0020377 C0020378 .C0020379 C0020380 C0020381
Gross Weight
7.2 g 7.2 g 7.2 g
7.1 g 7.1 g 7:1 g 7.1 g 7.1 g 7.1 g 7.3 g 7.3 g 7.3 g 7.2 g 7.2 g 7.2 g 7.1 g 7.1 g 7.1 g 7.1 .g 7.1 g 7.1 g 7.1 9 7.1 g 7.1 g
Container Type Other
Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other Other
Preservative NONE NONE NONE NONE NONE NONE NONE
. NONE NONE NONE NONE. NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfg.J-ot
True True True
Direction / Handled By RECEIVED
AMMERMAN. MARK Mfg. ID
12/12/2003 Login.rpt
u056
Report Version: Dec 12 2003 11-.28AM Page 1 of 5
Instance:
R0076077
R0076077
ogin
Login #:
1510
Project:
P0000419 .
Project Storage:
"ompany Name: jubmitted By: Status:
DuPont de Nemours & Co, Inc. Michael D. Aucoin Unreceived
Login Type: Started: Date Start: Due Date:
Immediate Receipt of Samples
T
"
.
...
12/02/2003
'.:
"
12/16/2003 ;
Received Date: 12/02/2003
Received By:
AMMERMAN, MARK
;
Spread Sample:
Label:
Project Title/Type:. Analysis of PFOA in OVS Tubes / ROUTINE
ExygenSD/PI: MILLER. JAMES
Login Notes:
Conform Notes:
Conform COC Sample: Conform COC: . Conform Sample: Conform Request:
True True True True
Package
Carton
Miscellaneous Item Key
None
Packages / Containers
Mail Date / Condition
' "
: . , .:.
,
Description
Shipper /_ID "
icoc :V:
Temp. Control/Temp.
.:.
.
Direction / Handled By
.,SSS!^ Sample ID .j001400-0001 L0001400-0002 L0001400-0003 L0001400-0004 L0001400-0005 L0001400-0006 L0001400-0007 L0001400-0008 L0001400-0009 L0001400-0010 L0001400-0011 L0001400-0012 L0001400-0013 L0001400-0014 L0001400-0015 L0001400-.0016 L0001400-0017 L0001400-0018 L0001400-0019 L0001400-0020 L0001400-0021 L0001400-0022 L0001400-0023 L0001400-0024
Matrix GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS
Fraction OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes
OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes
Samples
Sample WWK-A-AMSFLBK-E5 A WWK-A-AMSFLBK-E5 B WWK-A-AMSFLBK-E5 C WWK-A-AMS1-E5 A WWK-A-AMS1-E5 B WWK-A-AMS1-E5 C WWK-A-AMS2-E5 A WWK-A-AMS2-E5 B WWK-A-AMS2-E5 C WWK-A-AMS3-E5 A WWK-A-AMS3-E5 B WWK-A-AMS3-E5 C WWK-A-AMS4-E5 A WWK-A-AMS4-E5B WWK-A-AMS4-E5 C WWK-A-AMS5-E5 A WWK-A-AMS5-E5 B WWK-A-AMS5-E5 C WWK-A-AMS6-E5 A WWK-A-AMS6-E5 B WWK-A-AMS6-E5 C Control 1 A Control 1 B Control 1 C
Date Sampled Date Received 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 11/30/2003 12/02/2003 12/02/2003 12/02/2003 12/02/2003
Date Due 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003 12/16/2003
12/12/2003 Login, rpt
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Report Version: Dec 12 2003 11.-28AM Page 2 of 5
Instance:
R0076077
^ ^ 62910925
001400-0001
Container .,0020357 /Other / NONE
L0001400-0002
Container C0020358 / Other / NONE
L0001400-0003
Container C0020359 / Other / NONE
L0001400-0004
Container C0020360/Other / NONE
L0001400-0005
Container . C0020361/ Other /NONE
L0001400-0006
||(|y ^g^
Container
0020362 / Other / NONE
LU001400-0007
Container C0020363 / Other/ NONE
L0001400-0008
Container C0020364 / Other/NONE
L0001400-0009
Container C0020365/Other/NONE
L0001400-0010
Container
C0020366 / Other / NONE
L0001400-0011
Container C0020368 / Other / NONE
101400-0012
Container
12/12/2003 Login.rpt
ogm
Bottles
Method
; Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
,
u U 0 <3
Method
------
Report Version: Dec 12 2003 11:28AM Page 3 of 5
Instance:
R0076077
R0076077
C0020369 / .Other / NONE
L0001400-0013
!||?
Container
.
,
C0020370 / Other / NONE
I L0001400-0014
( Container C0020371 /Other/NONE
L0001400-0015
| Container .
C0020372 / Other / NONE
JL0001400-0016
Container
.
j"
.. C0020373 / Other / NONE
L0001400-0017
1 . Container C0020374 / Other / NONE
|L0001400-0018
Container ,^i|||(, C0020375 / Other / NONE
T!Lj001400-0019
(. ..
Container
C0020376. / Other / NONE
L0001400-0020
| ! Container .. C0020377 / Other / NONE
IL0001400-0021
Container
( : C0020378 / Other / NONE
L0001400-0022
[Container C0020379 / Other / NONE
I L0001400-0023
Container
C0020380 / Other / NONE
MD001400-0024
I
Container
C0020381 /Other/NONE
12/12/2003 Login.rpt
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
Method
u059 Method
Report Version: Dec 12 2003 11:28AM Page 4 of 5
Instance:
R0076077
R0076077
12/12/2003 Login.rpt
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Report Version: Dec 12 2003 11:28AM Page 5 of 5
Instance:
R0076077
R0076077
CHAIN OF CUSTODY/ANALYSIS RE
RESEARCH
Exygen Research Sample Receiving 3117 Research Drive State College, PA 16801, U T: 814.231.8032 F.-814.231.1580 exygenresearch.com
j ;<ll^jjl^^^S^j^^BI^
Client (name & address):
(VO^m ,
n, T^.' ^<\-k ^^^^'^on \^Q<\^
'':
'
'
.
/ \
Phone:
i7^) ^-W^ Fax: 1 .
' . . > Sampler:
'
R.Ko.Mo:U|
'.'
.1 . .
..K^.rOojJ.
Project Manager (Name & E-mail Address):
f^V^ft-u.te-^
<r\ reject Name: (--^
0
Pr^r ^o^^p\'^^\ V^O-^Ca^vu
R0.#:
.i
^
Quotati on i^:
'
!
.
".
.
'
Pie ase flII out this form completely to ensure correct anal^/sis cind proper handling of your samples.
b A M j ^ f c ' a N . A D ' S i S ' ^ . /"'"' ^ f1 ^ .^"^ ^ K''"" ^ ^ I? !^ ^ ^ ^".if^ ^ ^saf '
ExyLIMS# Client Sample Identification
Collection Collection i
Date
Time
u
\^voy^- rWvsfW,- ^
-^ f^ lyo^K-ft'Prrws^ - 6^
'nM1 o7 Qfn\&rb\Qa
n
^E^ !
VI
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<u.S
Q- JS nl
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Specify Matrix
\ r^C
\
^vo^^A^A--^sa-e^ -^ %C ft-ovS ^ - e^
e^o v^^^-ft-p^^ 4-&l:s
^ ^f \O\A)^-^-(VWS 5-66'
o^V \A)v3\<-rY-Tfn\^ \o-;5
/
^>,^/ LAB USE ONLY
o^-lb J^ o'A\5 JL
^
0^.00 -2^ >.
^
-\ V Pv\C
\
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p^r
^
Comments
^-^e\(^
/-^,
sino^/v^
rtMil^ ^ "'wi f^"'^"l
i
t ^ .'
Relinquished by
2A ^^{alQ
Date
Time
i^s^.^'Tr^o
Cooler ID # //"^4^- Cooler Temp. (C) /^
OTHKR INFORMATION
M
r--<^^^^- C< .
LAB USE ONLY
r^ ^^^ ^^.5 ^ ^-C^b^^ %V^
^-y._____^.:;.____ij_ "p- \(^b <
Sampler(s): LK, REK
DuPont Washington Works Air Sampling Program
FedEx Airbill #:
Event Number
669842
669908
669878'
669901
669769
669848
Hours 0 '/
1
:
2
/.
3
.4
AMS-1
AMS-2 AMS-3
AMS-4
AMS-5
AMS-6
Minutes
0
'
60
120
180
240
WWK-A-AMS1-E5
WWK-A-AMS2-E5
WWK-A-AMS3-E5
WWK-A-AMS4-E5
WWK-A-AMS5-E5
WWK-A-AMS6-E5
Hours
;
5 ?
6
7
.
8
9
1.019 1.011 1.013 1.013 ; 1,018 1.017 Minutes 300 360 420 480 540
29-Nov
29-Nov
29-Nov
29-Nov
29-Nov
29-Nov
: Hours 10 /
11 ..:
:
12
; 13
r
14
0547 0550 0550 0558 0540 0605 Minutes 600 660 720 780
840
30-Nov 0630
30-Nov 0615
30-Nov 0615
30-Nov 0640
30-Nov 0600
30-Nov 0649
Hours Minutes
'900 15
'.' 16
960
17
1020
18
1080
19
1140
Field Blank:
yes
WWK-K-AMSFBLK-E5
-
:
yes or no
Weather: 11/29=
T'e.mpe.r.a'ture
. '
'
.
about 30 degrees,
' .
with
' '
.
.
light snow.
'''. i' '
11/30=
Temperature about 32 degrees, and clear.
0.9162
1.013
1.077
1.19
1.015
1.022
Hours
20
.
21
22
23
24
SAFER operational:!
yes yes or no
Comments:
Total minutes column is the reading from the monitor counter.
* Pump AMS-4 had an intake fault iconon the display and had stopped running at 957 minutes. When brough post calibration pump would run for 10 to 15 seconds with a flow of 1.190 and then stop again with the fault ic
showing.
12/1/03
'wy
Page 1of2
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