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METHODS SUMMARY DrG270329
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PEE
ARJLeYaTInCAL rPeRTEaPoARnATION
:
Le/us/ns, pron
Dex -1c-0012
References:
omy OSepveerrantinTgrenPtrocLeadbuorrea.tores, Denver, Facility Standard
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DEP2-SDWB-000002
METHOD / ANALYST SUMMARY DrG270329
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mmTLHrOTDICN,
mer
nave
oan -1c-0012
Jaqueline Bonnett
003601
References:
ax OSepveerrantinTgrenPtrocLeadbuorrea.tores, Denver, Facility Standard
|
DEP2-SDWB-000003
SAMPLE SUMMARY 76270329
| MnOa#msapororEs cmLaiEnverseumiesn 333300603 000032 sRovUaNmEDMAELDEE Fpo0z8
ooe ArmkE(d esr).ntse0mgeos rioerpsr mf12lr
| TPeo r are tt begppee,s esi por i ty eepeercl, or ne.dn,ktpl,ho,
hr.eype, vty, lspe ec t,t i,i,ml,ee, ty, we.
soawtpsiE snueee
ssn ove
0077//2265//0077 3113::2000
DEP2-SDWB-000004
Aoerican Water Company
Client Sample ID: MURRAY AVE POR
mc
DLaotte-SSaemmpplleed#.....:: D0I7G/22750/30279-0090:125 WDoartke ORredceeri4v.e.d...:: J0I7C/R2X7/L0A7A
PPrreepp DBaattec.h..#......:: 0772/13211/9017 onoaallyyssiies DTaitmee....:: 0048:/2033/07
Dilution Factor: 1
Method.........: DEY -1C-0012
Matrix.........: WATER
rPohsm.ETER ro
R0e.s0v0u8r9 5 oon a
oREaPOrRTING ware wo 0o.i01s0 wuag//un 00..00002260
su13r0R4ooPAFTOEA 130s pros
RsEECROCVEENRTY. 3Go.
Rpecroevery ((5500 -- 220000)0
B+oSruE(rSa)eryce ct
DEP2-SDWB-000005
Aserican Water Company
Client Sample I: RUMNOGDE POE
me
DToatt-eSSaammpplleed......:: D0176/22750/30279-1010:220 WDoartke ORredceeri#v.e.d...:: J0I7Q/K27I/I0A7A
pPrreepp DBaattec.h........:: 0772/13211/9017 Dilution Factor: 1
AAnoaallyyssiise DTaitmee::.. 0048:/3053/07
Method.........: DEN -LC-0012
Matrix......... WATER
EPraoasveTER. Pron
smsour
RievporRTING mars wo
wWw
0o.m01s0 uugg//LL 00..00002206
`1s3u0m4oa2aRTOER 1304 PROS
ReEeCROcVEENRTY. 0a
`oRaECrOVsERY ((5500 -- 220000)
DEP2-SDWB-000006
American water Company
Client Sample ID: SWERDALE 7OE
mc
DZoatt-eSsamapmlpele#d.....:.: D0I70/22760/30279-1030:300WDoartkeORredecreiv.e.d...:: J0I7Q/H27I/I0A7R
PPreeepp DBaattec.h...,....:: 7072/13211/9017 Ahanaallyyssiins DTaitmee..:: 0048:/5063/07
Dilution Factor: 1
Method... DEN -Lc-0012
Matrix... WATER
roonserER ron,
ResuLr
mREaROrRTING gms woo
ww
o0.i01s0 uugg//Lh 00..00002266
`Ts3ucmemooparTos. 130s peo
RPEECROCVEENTRY 47s.
Rpercoevyery
((5500
-
2007 200)
Sorien(asn) : reynme
DEP2-SDWB-000007
QC DATA ASSOCIATION SUMMARY DrG270329
Sample Preparation and Analysis Control Numbers
:
swmiss mix RpoermToIoCN,
BAAcTCkHS eBATdCH Mms ow
001 WATER DEN 10-0012
7212191
002 WER DEN -1c-0012
mas
ous WATER DEN -1c-0012
212101
DEP2-SDWB-000008
METHOD BLANK REPORT
mic MCBlieLnott-SLaotmpl#.e..#:: RDI106237100302090-151 ForkOrder ...: JIWKQLAA Aaalysis Date..: 08/03/07 PPrreeppDBaattec.h........:: 0772/13212/5017 Dilution Factor: 1
atrix.........: WATER Analysis Time..: 03:35
e=aRnTER srs
wREsoLT ww
`1s3u0R8RoPGRAOT"E 1304 pros
`PREERcCoEvNETRY a7re
CaoTtE(oS)epee es dn 7 0re i pp------------
RwEaPOrRTING wars o0.o01l5 uwa//tL RLencaovsERY ((5500 -- 220000))
|
ymwee-16-0013 DEW -1c-0012
DEP2-SDWB-000009
LABORKTORY CONTROL SAMPLE EVALUKTION REPORT
mic
CIlCiSenLtot-lSoatmp4l.e.t.: DR7IG6321700030209-151 Work Order #...: J3KQIAC PPrreepp DBaattec.h..#......:: 0772/13211/9017 hRaoaallyyssiiss DTaitee...:: 0038:/5013/07 Dilution Pactor: 1
Matrdx.........c WATER
rPhoannaTER ros
PREERCCOEVNETRY m120
RELCmOmVTsERY ((309 -- 113200))
mwewTHo1D0-0812 DEW -1c-0012
s13o0m4RoPcOTAs 130s pros
RsEERccoavNRTy G52e
RELCpOaVsERY ((5500 -- 220000))
olrsi(sn)veered lorerie retfs a
tt ie
es
DEP2-SDWB-000010
`LABORATORY CONTROL SAMPLE DATA RRFORT
mic
Cl10i5enLtotl-oStam#p.l.e.d::DRI7GG231100302090-151WorkOrder ...:JIKQIAC || pPrreepp Dmaatree.k..#.1...: 7072/23110/007 hAoaaallyyssidss TDiamtee....:. 0038:/5013/07
Dilution Factor: 1
Matrix.........c WATER
PPrroanmTER eros
sneorwer MEmAoSoURrED. wuts
00..22003 00.222270
waa/nu
mPeEcRoCvEmNRTy memo 11120 `DbeRat 1-16c--00001122
STu3RcRaoaparTosx 1304 PROS uotTRe(sS)oepeor or erinottrhe
pe seco rs
sssEcRoCEvNeTRy 52
`RLemcwozvsery ((5500 -- 220000))
DEP2-SDWB-000011
LABORXTORY CONTROL SAMPLE EVALUATION REPORT
mic
1Cl0i5enLtot-ZSoatmp4l.e.d.:: RD716G237100302050-151WorkOrder f...: JIWKQIAD PPrreepp DBaattec.h..4......: 70271/23119/107 AAnnaallyyssiiss TDiamtee....:: 0048:/0073/07 Dilution Factor: 1
Wateix.........: WATER
P=hmETER Pros.
PBBECROCVEENRTY 11280
RELCIOITVSERY ((309--331200))
MDEETNHO1D6-0012 mw -xc-o012
`1s3u0m4oapnrTos 1304 pros
EPEECRoCvENETR.Y n7
RLeuctovsery ((5500 -- 220000))
loruesn): ord ior remieg r of rs 4pr dsco ros
DEP2-SDWB-000012
`LABORATORY CONTROL, SAMPLE DATA REPORT
me
1Cl0i5enLtot-LSoatmp4l.e.k.:: RDI1GG237100302050-151 Work Order ...: J3KQLAD PPrreepp DBaattec.h..4......: 70231/23119/107 Bhaaallyyssiise TDaitme.e.:.: 0048:/0073/07 Dilution Factor: 1
Matrix.........: WATER
PehaRmnMETER Pros.
smeroew ool.o0220011
EARvSoTwRrED mums 0o.l0oa2s3z vvoa//nu
RRcRNT 1R1e8covery Dmeem1o6-6013 . 120 Dax -10-0012
s1u3R08RoBarToEa 1301 pros CHolroE(nS)vs+pee to nig i it opm
oof re
`pBesRcocvEeNRTy E7X en
RLEmCeOzVsERY ((5500 -- 220000))
DEP2-SDWB-000013
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LFi
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Table Of Contents
Standard Deliverables
Report Contents
Th`SetCoavnerdLaartderDaendlihve eRrepaobrtlCeasve pagear considered niegrel
partsofthisStandard Deliverpaacbkalgee.Thisreips inocomrplette
Tableof Contents + CaseNarrative Executive Summ--Daeterctiyon Highlights
+ Methods Summary + Method/Analyst Summary
+ Lot Sample Summary
* Analytical Results + QC Data Association Summary
+ Chain-of-Castody
Total Number of Pages
DEP2.SDWB-000015
CasDeG2N7a0rr3a2t9ive `MTahneuraelsu.ltAslilncrleusudletdsihnatveisbreeepnorftouhnadvteobemeenetraelvireewqeudifroermecnotmsplofiaNnEcLewAiCthanthdeaLnayboerxacteoptriyoQnusalairteynoted below. "sTphoinssorerp.oDritlsuhtaillonnofatcbteorrseapnrdofdouoctendoetxecsehpatvienbuelel,npwriotvhoiudtedthonwreiatcthednaatpapsrhoeveatlotftahseslaiibntosrhatetory or interpretationofthe results. `TShaemptlhreeAerwraitvearlsaanmdplReescepirepstented inthisreport was received at the TestAmerica Denver Isboratory ata temperatureof5.1C on July 27, 2007. S`Atnaanlydtaircadlsstandazds werepreparedusing the acid formofthe compoundperfluorooetanoic acid (PFOA). PFOS is a commercial prepared and certified solution. sPtearnfdlaurodrof-onr-q{u1a,n2t,i3t4a-t"iCo.nJoofctPaFnoOiAc.acPiedrwflausorion-tr1o-d(u1c,e2d34a-t"tCh,eJoecxttraancattieosnuslftopnaatnedwwaassiunsterdodausceadnaitnttehrenal extraction step and was used as n intemal standard for quantitation ofPFOS. `ETShaemxpslaemtplers parescentaetnddiiAnutahoilsyrsenpiosrtwere analyzedfo th targetanalytesby TestAmericaDenver'sSOP DENLC0012. Fexotrrawcatteedrussaimnpglseosliad2p5h0asmeLexatrlacitiqoonfueteoacchthnisqaureopwlietih maectihdaifnioeldcwointdhit1imonLedofC618NcHaCrtIrisdgoelsu.tioEnaacnhdsiatmsple thiesapniakleydtweistahrctheeluitnetderwniatlhst4amndLardo,fmperitohratnooelx.tTrahcteiofni.nalAvfotlerumteheisabmrpolueghisttpoassmeid.tuhsrionugghmethtehacanrotlraidngde, the extract is analyzed by LOMSIMS. M`TehtehMoedthOoCd BSlaamnpkliessprocessed reagent water spiked with surogate and prepared with each batchof20 amplesofthe same matrix. Themethod blank was non-detect atth reporting limit or the target analytes. Each batchi prepared with Laboratory Control Samples (LCS). TheLCS recoveries forboth levels were within established control mits. `ATnhaelyitnitceamlalCsotmamndeanrdtsrecovery for 13C4 PFOS was below the lower control limit in samples MURRAY AVE POE and SOMERDALE POE. Because the control limits for the 13C4 PFOS have not yet been determined, no cormestve action was taken. "Th internal standard recovery for 13C4 BFOS for the method blank associated with QC batch 7212191 was below the lower control limit. The controllimitfor the internal standard has not been established. `There was insufficient sample volume 10 provide MS/MSD analysis in the analytical batch 7212191. However, two laboratory control samplesmetall method citer, indicating the analytical system was in control.
DEP2.SDWB-000016.
Nochesna were ne, || b|
i DEP2-SOWB-000017
EXECUTIVE SUMMARY -Detection Highlights Dreamz
repoRTING
RUALYTICAL
EAMMETERmeswr Lmar mats MEmED
MURRAY AVE POS 07/25/07 09:25 001
Perroosn
o0.0b00s93 o0.0s20 uuge//nm BRNW -11-c-0010122
DEP2.SDWB-000018