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R226 -- 3260 442 --~ <9 DuPon`tanHdaEsnkveilrloLnambeonrtaatlorSycefnorceHesalth ARA2E_ 3260 Novembe4r, 2002 co `w Quallty T Assurance TO: MR FILE{@RBPOCKET 15425 FROM: 1.C.Maslanka Ft `TESTSUBSTANCE STABILITY OFH.25425 9 MHaesdkieclallSRuemspelaercNhuPmrboejre:ct Number: m75i42l5 Haskell Reference Standard Number: 25425 `AAnnaallyyttiiccaall RTeesptorCtodNeu:mber: wHAe-2002-094 Notebook References: (--] pAtetrafcohremdedisttohseatainsaflyytpircoatlorceoplorretqfuoirretmheensttsufdoy itdeesnttisfuibesdtaabnocveset,abTilhiitsyabnuatlymsiasywaalso be used for other purposes. 4 M`HeadsikcelallSRaemspelaercNhuPmrboejre:ct Number: Analytical Report Number: [254--25 HA2002-094 pA samtple oef H-2o5f4s25iweasgsruebimint1eodn1Ocwtiosbemres14s,e2d00t2aR end anaR lyzed oM n October 15,is2002. `when the sanmoploenwea!sfsourbrmeiptltiecda.te analyses (n = 3). The sponsor reported a purity ACKOWLEGEMENTS 5 SStaomsptleekp(rSeepnairoartiRoensbeyarSchheiClhaeAmi.sRti)l.ey(ChemistryAssociate). SampleanalysisbyBogdan SIGNATURE Report: -- L. _Gonct Cptunte, shtsnons AnaJlaynteitcaCl.StMaafsflCahnekmaist. Date . = Moree 08) _ @ pe ` d ) ww HA-2002-09 page20r2 METHODS acAcnhcarolorymdsaiitnsoggfr0oratpthhhey fp(eoHrlPclLeonwCti)nogwimfteiht.haionGde.lsSPaoemnrpimlceeaaottifioonBn-wC2aos5l4uu2smenwda((sGoPcbCoym)hpialgnehdt-erpleeyfrrdfaiocsrtsimovalenvcieentdlheienqutdieesdtsector substance and the analytical standard stock solution. SAMPLE PREPARATION & ANALYSIS (Al1i0qmuoLt)s t(o0.g0i4v1e3n,o0m.i0n4a0l7caonndce0n.t0ra4t1i2ognsroafms4)o13f0,H-4205704,25anwder4e12d0ispsoyl.vedreisnpetcettirvaeblyyc.rofuran CHROMATOGRAPHIC CONDITIONS CIonlsutmrunmse:nt: Mobile Phase SH1e0tw0ly%ertttae-tgPrHaaeRchlky4ad;rrod7f.Mu8oradmnueml(Tx1H31F00)00HmPmLC(GPC column) IFnljoewctRiaotneV:olume: s1o0umlLimin DeCtoelcutminonT:emperature: ~~ R3e5frCactive Index CALIBRATION & QUANTITATION {sAmtaaskneedpaacrradalti(eb9rs3aat.im1op7nl%espooulfruetH)i-.o2ns5As4tt2ha5otctbkersatscoskluuebttsietodnatnohcfeeHtw-sa2ts5s4doe2ls5uitgiionnnatst.eetdrPaaehsaytkdhrheoefaiungrahaltnystwifcarasolmurserefepedlriteocnactee dcHeuPtrLevCerm/biGynPelCde/absRytI-asapqnpualalyryiessnigsroerfgeresepasesccihtoincv.aelpiMbeeraaakstuihoreneigdshoctlosunttcioeonntthwereacrtaieloiunbssrfeaodtirtooneacccouhnrsvetesr.tucstoalactailoinuawteirone,. RESULTS 8H.2556422%50e.l0u1temdinfutreosm.thTehHePsLpConscoorlurmepnorstedaraespoulrviteydf peakwE ith ahreen ttheestanmmptloeifwaaosbosnuutbmi `TaIb. `lThee percent ofa.. nthe H-2p5o4m215s.2a5425 iyzed = Oct1o5b,2e00r2. ted. quo Fominal _Mesired~_Nominal 21 3 a1n30 a0 mmoo o0l3a ET [[SAtvaenrdaagred%DeNvoiamtiinoanl |CoeetentofVariation 0182s 1%