Document mqQXDkGqVME9Z06ejrNg430eg
i. ,01 CODE YE >72,1 ~D
Q>
i-U^/M~ ( DATE >
< LOT ) '
4448* LBS. { EST WT >
PROCESSES ( ) YE-721-D (M)
APPROVED BY: FWP 11/08/82
COMTYP JOB NAME: 01YE721DMH
BLENDED BACK: CG 01, F`Q 98, ____ _________ (CODE)
(LOT)
(POUNDS)
EQUIP
USE |
1 ACCT
MENT I |
NAME: MOLYBDATE RED
PREP I i x Sb t a in FOR S-12
LBS | N-CODE | LBS
-T- ,, | 68 ! 108--A
i |
68
1 I 2 /Ob t a in f o r s-34
600 1 4--A 1 600
1 3 1X5BTAIN FOR S-38
! 4 V^OBTAIN FOR S-40 I 5 1 J0BTAIN FOR S-44
/} SA'\'T>-
fVU< &
'
120 1 3--A | 120
195 &STO 350
| |
32--D 3--A
| |
195
6 >T OBIAIN FOR S-47
Sc^
61 J 711--BD | 61
WEIGH IN: OPTR OPTR __
MK___ , T-V- / MK T- .
WEIGH IN: OPTR___ MK S7_, l-JbD, 33j 0&
j p j m j
%
.mi
-~--i ID--D |
1 ------ 1
423--D |
150? 24?
OPTR____ ,, MK __ T-________ ,______ %
iUN 10* (500 G) WATER INTO V-358
-RUN V-359 INTO V-351 6 PUMP IN V-351
SDJ TO 55* (2600 G)
^ J-'SIFT IN N-108-A FROM S 1
UC^KSTIR 5 MIN l> RECORD: PH_Z2'JZ(9,0-1 0.0)
VK4 1 ADJ TO PH 9.8-9.9 & RECORD: PH,,:M-
II
ASSUME 50%
is* ASSUME 66%
RUN INTO V-351 FROM BADGER METER. JT OPTR, MK_3., 3D&&-.X
\M J^PUMP FROM V-351 TO V-358
071 FLUSH V-351 *. PUMPING LINES WITH 1000G
| i'-UATER INTO V-358
i>? | ADJ TO 74* (3530 G) AT 67-69*F
RECORD: VOL^ill-* 6 __4Z_*F
STIR 5 MIN 6 RECORD: PH52t/_(7.2-7.4) &
! G/ML
1.055-1.058)
I NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
I LIST & ATTACH, TAKE 1 QT SAMPLE.
::z::
JZL^o l - I
I i
7-D 33-D
28-D
l_Z_. I |
RUN 20" (996 G) WATER INTO V-________ ?Ji&8RD-Mt*44^D STORAGE TANK TO PUMP FROM.,
CIRCLE QN>>402 410 411 420 424 425 cflgtnr~cf.t i-f t c u s u p v :
*STORAGE TANK MUST CONTAIN AT LEAST 1900
GAL: 402=392. 410=20*, 411=38*, 420=20*,
424=20*,{425=25 *_ ^STORAGE TSNriTOff HAVE STIRRED AT LEAST
20 MIN SINCE LAST ADDITION OR ADJUSTMENT *STORAGE TANK MUST BE ISOLATED UNTIL ALL ^ . JMPING FOR THIS BATCH IS COMPLETE/ SET METER FOR 300 G 6 PUMP TO SV Jg/SlZ
NOV 151982
ft
LOT: ____ EQUIP KENT I
CDMTYP JOB NAME: 01YE721DMM PAGE 02
AT APPROX 100 G WHILE CONTINUING TO PUMP,
DATE PRINI D:11/08/82 I USE | N- ACCT I LBS | CQDE LBS
,,,lL
CHECK PH 6 DENSITY. RECORD BELOW. IF NOT
IN RANGE, STOP PUMPING & SEE SUPV.
* (2.2-3.7)
ENSITY:
G/ML (1.270-1.328)
IP S-23 OK 6 WHEN S-22 COMPLETE, RECORD
DENSITY A3J1 G/ML ON TRAPPED SAMPLE
L^FROM END OP S-22 PUMPING.
25T USING DENSITY PROM S-24, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE
ACCOUNTS FOR 300 G ALREADY PUMPED IN S-22.
CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
***# TABLE **#
G/ML 1.270 1.271 1.272
1.273
SETTING 1 G/ML 1259 1 1.291 1253 1 1.292 1248 1 1.293
1242 1 1.294
SETTING 1 G/ML 1146 | 1.312 1141 | 1.313 1136 | 1.314
1131 1 1.315
SETTING 1 1049 | 1045 1 1040 |
1036 |
1 1 1 1
f
1.274 1 .275 1.276 1.277 1.278 1.279 1.280 1.281
1.282
1.283 1.284 1.285
1.286 1 .287
1.288 1.289 1 .290
"-30***
1236 1231 1225 1219 1214 1208
1203 1198 1193
1187 1182 1177
1171 1166
1161 1155 1151
\ 1.295 1126 r 1.316 1032 |
1 1.296 1121 | 1.317 1027 |
l 1.297 1116 1 1,318 1023 |
1 1.298 1112 1 1.319 1019 |
1 1.299 1107 | 1.320 1015 1
1 1.300 1103 | 1.321 1010 1
I 1 .301 1098 | 1.322 1006 |
1 1.302 1094 I 1 .323 1003, |
1 1.303 1089 | 1 .324
999 |
I 1 .304 1084 | 1 .325
995 |
I 1 .305 1080 i 1.326. ..... 99J_ 1
1 1.306 1076 | ^7327
987J I
1 1 .307 1070 | 1.328
983 J
1 1.308 1066 1 1.329
979 |
1 1.309 1061 | 1.330
975 |
1 1 .310 1057 1 1.331
971 |
1 1.311 1053 1 1.332
967 |
-- _---- ------------
-------- --------1
1 1 1
1 I 1 1 i
1 1 1
1
1 1
1 1 1 |
^SET METER 6 PUMP
; (RECORD FROM TABLE)
|
' FLUSH-i-INE WITH WATER INTO SV FOR APPROXIMATELY |
1 1
SECONDS
{
ADJ LEAD NITRATE TO 3244 G <68"-242/245 6 66.5" |
I
*1 AT 67-69#F
I
CORD:_________ *F & ICE CONSUMED (330S/BL0CK) I330X.
ST>R 5 MIN 6 RECORD PH:
(2.2-3.7)
***** USE TI TRIMETER TO ADJUST N-41-D PH ****
I |
' IF NECESSARY ADJ TO PH-3.0-3.1 >RECORD PH:
ASSUME 66%| ASSUME 50%f
_I
I L^NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING|
S&w RECORD: /s /3&L G/ML (1.128-1.129) IF OUT OF SPEC I
1 L^PILL OUT CHECK LIST 6 ATTACH.
|
MT STIR AT 67-69*F FOR S-33. TAKE 1 QT SAMPLE.
|
41-D 57-A
337-
4094
DUP050059756
LOT*5_______ __ COMTYP JOB NAME: 01YE721DMM PAGE 03 EQUIP I
DATE PRINTED:11/08/82
USE N- USE LBS CODE LBS
I OBTAIN 1 QT SAMPLES OF S-19 6 S-31 SOLUTIONS
| & TITRATE TWICE
1 NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
i 9.5-9*9 OR IF THE TWO TITRATIONS DIFFER BY
I MORE THAN 0.10 ML N-10-D <IF YES, FLUSH ALL
I EQUIPMENT 6 REPEAT TITRATIONS). DO NOT
I PROCEED IF N-10-D TITRATION IS OUT OF RANGE
I ADJUST V-358 FOR A TITRATION PH OF 1^3^333=^90
I FROM FINAL IN-LINE TITRATION, RECORD LOWEST
\ PH ^--------- & ML N-10-D ____________
/,90~<?.0d
33*-D 7-D
WHEN S-32 TITRATION OK, STRIKE*V-358 THRU BOTH
UNDERSURFACE DISTRIBUTORS INTO SV IN/44-46 MIN
RECORD: START
TOTAL MIN
___
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
BUBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER
JJB-15 MINUTES
RING S 34, WASH IN V-358
MIN & RECORD PH_jt/jfiL-.< 1 .7-1.8)
BXS, _JjpL__< MUST BE + >
IR TOTAL OF 15 MIN FROM S-34 6
RECORD: TEMP_!7f___#F <67-73*F)
P N-3-A FROM S-3
TlR 3 MIN
_ R IN N-32-D FROM S-4
iMTflR 2 MIN
IN LIQUID ALUM USING BADGER METER
IR^S MIN & FLUSH ALUM LINE WITH WATER
P IN N-3 FROM S-5
STIR 4 MIN FOR S-49
RUN IN HYDROCHLORIC ACID USING WEIGHT 6 FLOW
CONTROL PANEL
MK &&@f_V.
MK ____ _____________%
DURING S-45 SIFT N-711-B FROM S-6 INTO V-390
H AGITATOR ON IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION
WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B
SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
TIL FOAM SUBSIDES.
IN BLANC FIXE N WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1
.-'" RECORD : CODE________ * LOT____________________ S=
IR 20 NINx/J 5SH RECORD: PHSii_7____ (5.8-6.0)
54^<lF NECESSARY, ADJ TO PH 5.8-6.0
ASSUME 50%
6 RECORD: PH-___ *_______
ASSUME 66%
LOOD TO 153* <7298 G) 6 STOP AGITATOR
START
I ..
IrM-
FINIS
OPTR
I 604 115-DI 302
--------- ! --------I
28-D | >0-" 28-D I______
I
I--------
l I
275 28-A I 275
7-D1______ 33-DI______
I I
DUP050059757