Document mp9rqvxkMz2zBBpRaQ1Gn8Nk4

J hbUssnto |Mftf (MMt IMtMSNI D. K. Mitchell September 28. 1970 PCB Analysis TO B. T. Dean C>p iidj V/. K. Ciatuwsui. J. E. Li ` K. M. Warner s The following compilation liete ell analyses on PCB presently In our flies. The data on pages 1 through 6 are listed in chrono logical order. The remaining pages are analyses by the Bureau of Commercial Fisheries and are so presented as received. y,: ?//<#*< - D. K- Mitchell bab i. MON-MT-008748 TOWOLDMON0003925 WATEFLPCB-00000947 Date 6/5/69 6/5/69 6/5/69 6/5/69 6/5/69 . 6/5/69 7/1/69 7/t/69 7/1/69 7/6/69 6/11/69 6/11/69 6/11/69 8/11/69 8/13/69 8/14/69 Sample Fish Location Flounder Liver Muletto Bayou Flail Flounder Muscle Mulatto Bayou Flah Flounder Cills Mulatto Bayou Fish Croaker Mulatto Bayou Fish Menhaden Mulatto Bayou Fish Pinfiah Mulatto Bayou Fish Menhaden Mulatto Bayou Shrimp Mulatto Bayou Sediment Mulatto Bayou Sediment Highway 90 Veter Pensacola Plant Saat Ditch Veter Monaanto Plant Outfall Ditch Veter Veter Eacambia River at Station "DM below plant Eacambia River at Station "W" above plant Blue Crab Northern Escam bia Bay Fish Speckled Trout Cilia Pensacola Bay Result 76.ppm 4.5 ppm 19. ppm 12.ppm 11.ppm 10.ppm 12. ppra 1.5 ppm ND. 1.7 ppm 74.8 ppB 12.5 ppB 4.7 ppB 0 ppB 7.0 ppm 7.5 ppm 1*13 c Duke Dke Duke Duke Duke Duke Duke Duke Duke Duke E.S. Tucker E.S. Tucker E.S. Tucker E.S. Tucker Duke Duke Reference Federal Report Federal Report Federal Report Federal Report Federal Report Federal Report Federal Report Federal Report Federal Report Federal Report Samplea sent to St. Louie Semples sent to St. Louis Samples aent to St. Louta Samples aeut to St. Louis Federal Report Federal Report MON-MT-008749 TOWOLDMON0003926 WATER_PCB-00000948 -2- Date 8/14/69 8/15/69 8/15/69 8/15/69 8/15/69 8/15/69 8/18/69 8/20/69 8/20/69 8/22/69 8/26/69 8/26/69 8/26/69 8/26/69 Sample Location Result Analyst PI ah Speckled Trout Liver Pensacola Bay 21 .ppm Duke Sediment Garcon Point N.D. Duke Sediment Mulatto Bayou N.D. Duke Sediment Horthem Escambia Bay .14 ppm Duke Sediment Highway 90 1.4 ppm Duke Sediment Outfall 6 Miles North of 486.ppm Duke Water Monsanto Plant Outfall Ditch 1.0 ppB E.S. Tucker Water Escambia River @ 270.ppB Monsanto Co. Out fall E.S. Tucker Fish Escambia River 13312 ppm E.S. Tucker Water Monsanto Plant Outfall Ditch 1.4 ppB E.S. Tucker Water Escambia River <3 White River Above Monsanto Co. Top Sample 3.ppB Symea(Wlntechsven) Water Escambia River @ White River above Monaanto Co. 3/4 Depth Sample 2'PPB Symes(Winterhsven) Water Escambia River @ Monsanto Co. Outfall * Top Sample 6.5 ppB Symea(Winttrhaven Water Escambia River <? Monsanto Co. 3/4 Depth 3.ppB Symea(Winterhaven) -... Reference Federal Report Federal Raport Federal Report Federal Report Federal Report Federal Report Samples sent to St. Louis Reference sample Bureau of Fisheries Campbell to Tucker Fish caught by W.A. Calloway Samplea sent to St. Louis Sampled by G. Richmond #1 Sampled by G. Richmond #2 Sampled by G. Richmond #3 Sampled by C. Richmond #4 MON-MT-008750 TOWOLDMON0003927 WATER_PCB-00000949 3- Dale 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 8/26/69 Sample Water Water Water Water Water Water Bottom Sludge Bottom Sludge Bottom Sludge Bottom Sludge Localiuu Eacambia River United Gaa Line Top Sample Reauli. 6.ppB Aualyat Symea(Winterhaven) Eacambia River United Gaa Line 3/4 Depth Sample 5.5 ppB Symea(Winterhaven) Eacambia River 9 Gulf Power Out" fall Top Sample 3.3 ppB Svmee(Wlnterhavan) Eacambia River @ 7.5 ppB Gulf Power Outfall 3/4 Depth Sample Symei* (Winterhavan) Eacambia River <? 3.7 ppB Highway 90 Bridge Top Sample Symea(Wlnter* haven) Eacambia River @ 5+`PPB Highway 90 Bridge 3/4 Depth Sample Symes(Winter haven) Eacambia River @ 0 ppm White River Above Moneanto Company Symea(Winterhaven) Eacambia River 9 0.33 ppm United Gaa Line Symea- (Wintarhaven) Eacambia River @ 1.5 ppm Highway 90 Bridge Symea(Winterhaven) Eacambia River @ Monaanto Co. Out" fall Detritus only Sand only 385tppm iOOOtppm 2.5 ppm Symea(Winterhaven) Syroee(Winterhaven) Reference Sampled by G. Richmond #5 Sampled by G. Richmond #6 Sampled by G. Richmond #7 Sampled by G. Richmond #8 Sampled by G. Richmond #9 Sampled by G. Richmond #10 Sampled by G. Richmond #1A Sampled by G. Richmond #3A Sampled by G. Richmond #4A Sampled by . G- Richmond #2A MON-MT-008751 TOWOLDMON0003928 WATER_PCB-00000950 -4- -.Bate,.. 8/31/69 8/31/69 8/31/69 8/31/69 9/9/69 9/15/69 10/3/69 10/3/69 10/3/69 10/3/69 10/8/69 10/8/69 10/8/69 10/10/69 Sarnui* Flah FI ah Shrimp Blue Crab Blue Crab Water Watar Watar Water Water Water Water Watar Watar Location Result Speckled Trout Northern Eacambla Bay 20. ppm Flounder Liver Northern Eacam~ bia Bay 184.ppm Northern Eacambia 2.5 ppm Bay Northern Eacambia 6.3 ppm Bay Mulatto Bayou 1.0 ppm ' Analyst Duke Duke Duka Duka Duke ___ Refarfnca Federal Report Fadaral Report Federal Report Fadaral Report Federal Report Monaanto Outfall 3.8 ppB Skimmer ' Eacambia River @ Station **W" Above Plant 0 ppB Eacambia River (3 Station "D" Belov Monaanto 0.2 ppB Monaanto Plant Outfall Ditch 17.3 ppB Monaanto Outfall 20.3 ppB Skinner Monaanto Plant Outfall Ditch 1.6 ppB Panaacola Plant East Ditch 45.0 ppB Panaacola Plant Power Kouae .Out fall 0.2 ppB Panaacola Plant Eaat Ditch Above Bldg 408 0.1 ppB Lubkovitz Analyzed at Mon santo-Pensacola Lubkovlt* Analyzed at Monsanto-Pcnaacola Lubkovitz Analyzed at Monsanto-Fenaacola Lubkovitz Analysad at Mon santo-Panaacola Lubkovitz Analytad at Monaanto-Paniaeola Lubkovitz Analyzed at Monaanto-Penaacola Lubkovltz Analyzed at Monaanto-Penaacola Lubkovitz Analyzed at Monaanto-Pamacola Lubkovitz Analyzed at Monaanto-Pensaeola MON-MT-008752 TOWOLDMON0003929 WATER_PCB-00000951 -5- p*ir* 10/10/69 10/10/69 10/10/69 10/17/69 10/23/69 10/30/69 11/28/69 11/28/69 H/28/69 6/30/60 6/30/70 BWUPU location Oiiumyewn t4fV*> Anclvot Reference Water Water Flab Penaacola Plant Bast Ditch Below Bldg 408 Penaacola Plant Eaat Ditch 11.7 ppB 11.9 ppB Menhaden Mulatto Bayou 5.7 ppm Lubkowl tz Analysad at Mon* santo-Penaacola Lubkowltz Duke Analysed at Honanto-Penaacola Federal Repott Water Water Bldg 408 Decanter Eff. Penaacola Plant Baft Ditch 6,300 ppB 1.3 ppB Lubkowlts Analysed at Mon aanto- Penaacola Lubkovltt Analysed et Monanto-Penaacola Bottom Sludge Monsanto Outfall 112 ppm Skimmer Lubkowlts Analyzed et Mooeento-Peneecols Sediment Escambia River West Side 150 ft Above Monsanto Outfall Detrltua . Pine* Coarse 3.4 ppm 4.6 ppm Cutehens Monsanto-Penaacola Sediment Escambia River Weet Side 100 ft Below Monsanto Outfall Detritus Fines Coarse 1.4 ppm 2.3 ppm Cutchena Monaanto-Pensacola Sediment Escambia River East' Side Across Prom Mon santo Outfall Detritus Pines Coarse 70.ppm 62.ppm Cutcbena Monaanto-Pensacola Water Escambia River $ C0.4 ppB Station "WM Above Monaanto Cutchena Monaanto-Pensacola Water Monsanto Plant North Outfall <0.4 ppB Cutchena Monsanto-Fentacola MON-MT-008753 TOWOLDMON0003930 WATER_PCB-00000952 -6- Date 6/30/70 3/17/70 3/18/70 3/19/70 Sample Water Water Water Water Location Result Monsanto Plant < 0.4 ppB Outfall Ditch River Water From Moneaato River Water Pumping Station 0.6 ppB River Water From Monsanto River Water Pumping Station <0.4 ppB River Water From Monsanto River Water Pumping Station 1.9 ppS Analyst Cutchens Reference Monsanto*Pensacola Cutchens Monsanto- Ponsit-oU Cutchens Monsanto-Pensacola Cutchens Monaanto-Fensacola MON-MT-008754 TOWOLDMON0003931 WATER_PCB-00000953 TOWOLDMON0003932 WATER_PCB-00000954 TOWOLDMON0003933 WATER_PCB-00000955 TOWOLDMON0003934 WATER_PCB-00000956 1 IRATORY: _ yp8T2CU>E ANALYSIS REPORT Chemicri. analyses supervised BUREAU OF~COlOiERCIAL FISHERIES Alfred J. Wilson, Jr. tiwtiivwii m/nj.i`v:vxm? rtvwruu't Culf Pre^ze, Florida ' Third collection of camples on. Escambia Rlvor by BCF f^ ga < d-m-y 17-7-69 tl It % . II II M tl 1 tl ' - ft \ j- < i1 ......... >t j- --. j STATION LOCATION # | S DOE g "i.--................. --:.... ... M2O " Bwy. 90 126 i6. " :'i S.R. 184 127 rr : ft *; Just below Skimmer . 128 4. : By Horse Shoe Lake 129 V rx ; #1 r `Just above White River 130 / i 4. 11 Above Skimmer m 1 / 5. Above Skimmer ~T. ; 132 Above Skimmer 133 8. Williams Ditch 134 9. M Canal . 1 135 . .......... - - ......... .......... ................ - -.................. * ------...------ -- PART0PER KILLIOtt or $/ DDD DDT OTHER PCB #1254 0,43 ppb m> 1 5*8 ppb { ND ' [ 0.6 ppb a ND : 1* nd t ND '' Jl ^ ND ND ~------------ j (0 . i ( MON-MT-008758 TOWOLDMON0003935 WATEFLPCB-00000957 I TOWOLDMON0003936 WATER_PCB-00000958 TOWOLDMON0003937 WATER_PCB-00000959 TOWOLDMON0003938 WATEFLPCB-00000960 PESTICIDE ANALYSIS REPORT BUREAU OF COMMERCIAL FISHERIES PESTICIDE MONITORING PROGRAM ` Chemical analyses supervised ty* Alfred J. Wileon, Jr. DC* Biological Field Statio* Cult ureeze, riorina JZbui JOEY; Seventh collection of samples at Escambia River by BCF . nrhS*d . Date 0 STATION LOCATION II 1 b DDE n\ g I \ 'dia-y kt 25-8-69 2C \ pH Sal. Temp. -Skimmer 772'T572Xr7S?C 254 ;.'j 1LI1' ." H Sediment Skimmer . 253 # ' Vk - , . ../"N - ^ -' .,J 1 y. ...... 1 V* PARTS PER MILLION or us/ DDfir DDT OTHER 1PCS 01254 * 1.7 ppb 44. ; ' 4' fi "* j." :ni - -. !` i. 4 1 .1 i-- ; 1 -- (' 1 l- * > ' MON-MT-008762 L_J___ ! TOWOLDMON0003939 WATER_PCB-00000961  AUAOC. nmUtiOAO Wii'Vl'.A BUREAU OF COMMERCIAL FISUERIES PESTICIDE MOHirCRINO PROGRAM unamiCAi analysis sujerviaaat by: Alfred J. Wilson, Jr. BCF Biological Field Station Gulf Breast, Florida 32361 r. /th collection of samples on Escambia River lyrTH'j* tyi K k JbifavJL BCF / . PARTS PER JIILIIOll or pj/f TOWOLDMON0003940 WATER_PCB-00000962 BUREAU OF COMMERCIAL FISHERIES by: Alfred J. Wilson, Jr. PESTICIDE MOHITORINC PROGRAM BCF 8ioIogitI Field Stscion . * ' Culf Breeze, Florid* 52S61 TOWOLDMON0003941 WATER_PCB-00000963 . BUREAU OF COMMERCIAL FISHERIES . by: Alfred J. Wilton, Jr. ' . . . ' BCF Biological Field Scation Gulf Breeze, Florida 32561 TOWOLDMON0003942 WATEFLPCB-00000964 I { TOWOLDMON0003943 WATEFLPCB-00000965  PESTICIDE ANALYSIS REPORT Chemical *r.l7il* tu?**vi Ift . /' BUREAU OF COMMERCIAL FISHERIES ^0C2/ik . CULP BREEZE, FLORIDA 3?SA1 by: Alfred J . ,f ; 4yM * Sample* / October Oy*tr Monitor :v ., I"- y/iyM^//U JO . SCTrac--r-777 />. IS d-m-y ,l,,.. -i *, i 30-y-6v / >r O '| ' 8 3 H Oyster II II ' STATION location 0 * . . : E. I . u !; * i g Tt............. ........ East Bay ........... -- 16' $ '' iA Trout Bayou ' ^2 -- -- 17 Escambia Bay 18' DDE tr DOD DDT <m ' OTHER a 1254 .44 1254 i "O" .yjfee $ 1. V*d V - ._ %* t: V1 "1 s A i . . . ' * . ' .. * - ' * * r f *. * .. ' '* _- \ * --- |. -------- ------ -- i * 't : v ,N MUN-M. 1 -UUo /O ( TOWOLDMON0003944 WATER_PCB-00000966