Document mp3BVLXga2LqN94kEm7bLw3y4
* CG 32
CODE RT-870-D
QCT>i 5/1982
K2K;7
PKG
< DATE '
( LQT'>
< EST WGT-)
^ , Appr*)
>#&? PREPARATION NOTES: ^
v________-_________
PROCESSES
APPROVi
< >RT-87-D <H> EWK 1-11-83
CGMTYP JOB NAME: 32RT870DKH
TYPED BY: JMH
STANDARD HRS.
TIME
NON-BLEEDINp
EQUIP MENT
I I I I I I
NAME: WATCHUNG RED B
USE LBS
| NOTE: DO'NOT START IF PRESS WILL'NOT BE
|
I AVAILABLE WITHIN 3 HRS AFTER MAKING * SUPV. )
I TO REVIEW WITH P.R. SUPV 6. RECORD:
|
1 PRESS WILL BE READY.:__ ____M______ /______ PR SUPV.I
I START MAKING________M______ __________ MAKING SUPV,]
t NOTE:j. NOTIFY PRESS ROOM BEFORE ROPING OFF i
' AREA UNDER V-922
1
: RUN 15* WATER INTO V-904, PUMP WATER 1
FROM V-904 THRU DISTRIBUTOR, IF WATER DOES !
1 NOT COME OUt OF ALL DISTRIBUTOR HOLES WITH |
i FULL FORCE, NOTIFY SUPERVISOR.
j
N-CODE | ACCT ] LBS
PREP 1
RECORD :
___ "BATCHES SINCE SPARKLER LAST
CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
SFARKLER & PRE-COAT WITH 15# DICALITE,
TER AID.
:N FOR S11 2-CHLQR0~4-AMINOTGLUENE-5-
13NTC ACID,
N FOR S27 3-HYDR0XY-2-NAPHTH0IC ACID
TALL DV & DV RECORDER b CONTROLLER CHART
.1 777--A |_.
i ' : ]. I 740--C 1 i 82-C |
11 * (10GG 5 WATER'INTO V-, L$c ADJ TO ' i
100 DEG F
I
Aj^ADD IN 2-3 MIN DRESINATE X
] 1@8 | 53--A |
>TJarlR 3 MIN & RECORD PH_JljL <9.5-10,5) 1
I
I
I B8 ^TSTIR 20 MIN OR LONGER TO DISSOLVE FOR S49 1
1
922 3
I9 \**r
c MA.U/4^
RUN 35* (722G) WATER INTO V-922 WEI*t+~ SODIUM HYDROXIDE IN V-926 b RUN IN
TURN ON AGITATOR b STEAM b DUMP IN FROM. S.2
2-CHL0R0-
LOJ
#100^
4-a m.t n o t o l u e n e
5-s u l f o n ic
fraS- -
ac id
P IN a c t iv a t e d c a r b o n
d u mp in f il t e r a id
HEAT TO 212-214 DEG F WATCH FOAM!!
RECORD; BY____< + > IF NECESSARY ADJ TO +BY
SODIUM HYDROXIDE
ASSUME 50%
STIR' 30 MIN AT 212-214 DEG F, THEN SHUT OFF
STEAM WATCH FOAM! NOTE: RECORD SPARKLER
PRESSURE i3L_.,,PSI, IF NOT ZERO NOTIFY SUPERVISOR.
7^> 7-D 740-C 7oc-
1 13-B 777-A
7-D
OCT U91982
1^8 \ ,
LOT= ...
EQUIP MENT
CQMTYP JOB NAME 32RTi370DMH PAGE 02
BA 1 L PKIN itu : . ,'/
PAGE 2 OF 4
i USE | N-CGDE \ ACCT '
CG 32 CODE R7-870-D - <H> 1 LBS (
| LBS
i CIRCULATE 15 MIN OR LONGER THRU SPARKLER 1 '
I
UNTIL SOL1N IS CLEAR* MAINTAIN AT J90-195 I.
I
i DEG F FOR S22* RECORD: START3L#
.XT.. "X 1
{ TOTAL MIN__L5____ CcLlAaRr I:TY__4/F.____ A./1/VW 'VI
______ F & REC m-
| '1
|J I 1 1 ` *
1
EASURE______` UNITS IN V-928 FOR- S39
HYDROCHLORIC ACID
M___ _____ ,
| JJEIGH SODIUM NITRITE IN PT^OR S^^^
i WEIGH SODIUM NITRITE IN DRjLiM~FOR S50 ~~ M
Ll 725-A } 39t Jj 3-\ 725-A. I -43
S^/CVii2Vi RUN 2" C5SG) WATER INTO VHMM/CV.: 5 L3S i WHEN SI7 IS COMPLETE,' PUMP IN V-922 THRU ^ ! SPARKLER, MAINTAIN*V-922 AT 190-195 DEG F*
RECORD: START-ft/ftfh . TOTAL MIN
\ J
l
1
WHEN S22 COMPLETE, SHUT OFF PUMP-AND INSERT|
V-922 FOOT PLUG
' i
RUN IN 10" (209G) WATER & HEAT TO' 190-195 FI
CIRCULATE 15 MIN THRU SPARKLER *
l
i .
7CV>0fBi AND PUMP V-922 THRU SPARKLER INTO
902 8
Xj A
RUN 65>"< 1696G) WATER INTO V-902
SODIUM HYDROXIDE IN V-926 J, RUN IN
M_Z.lr____ ,J5&~%
I DUMP IN FROM S3
34,EOT
I 3-HYDROXY-
-JkiJOEU-._____ L.
}1 2-NAPHTH0O1IC ACID -
______ ,
12m\ AD J to 70-90 DEG Jr STIR TO DISSOLVE
Z'ZUiA i1
] ,2 J - | i IBl Ei
I
922 4 9i
RUN IN 5* <104G> WATER J, HEAT TO 190-195 F J
| CIRCULATE 15 MIN THRU SPARKLER
,"
I
1 i 7-D 1 82-C I
399 994
4m/CVjt&fyi PUMP V-922 THRU SPARKLER INTO V^SWr/CV
!
10 WHEN MTY BLOW OUT SPARKLER INTO V-904/CV |
: ,.
DISSOLVE ALKANOL XC IN 20G WATER AT 150-160!
! AfF FROM HOT WATER MIXER IN DRUM & POURIN*
f HEAT TO 165-170 F FOR S38
!
RUN 3^ C32SG) WATER INTO V-932 J. ADj TO'
1 >| 80-100 DEG F*
ADD IN 6-7 MIN DRESINATE X '
135^1 STIR 5 MIN & RECORD
9*5-10*5)
I STIR' 20 MIN OR LONGER TO DISSOLVE FOR S59
| I
DUP050102108
LEVr= ________ COMTYP JOB NAME 32RT870DHH PAGE 03
DATE PRINTED: 7/19/82
USE N-CODE | ACCT
I I PAGE 3 OF 4 CG 32 CODE RT-870-D CH)
LBS
1 LBS
i ] NOTE; IF N-740-C SOL- WAS PUMPED DIRECTLY
i | FROM SPARKLER TO CV S2i,24B,29 OMIT S37 6381
CV Jt&f i RUN t* < 95 G) WATER INTO
|
12 JmC\ PUMP V-904 AT 165-170 DEG F THRU UNDERSUR- |
FACE DISTRIBUTOR INTO CV AFAP (12-15 MIN) |
RUN IN N-28-B HYDROCHLORIC ACID FROM SI 8 INI
12-15 MIN, MAINTAIN 165-170*F IN CV-
|
STIR 15 MIN AT 165-170 DEG F
I ADJ TO 46' C4347G) AT 32-38 DEG F RECORD; TEMP_3l 2~DEG F, V0LUME__fci2."
|& 1 X330I i
57-A
OP
RUN IN N-725-A SODIUM NITRITE FROM SI 9 AFAP|
(5-10 MIN) 6 RINSE IN PT
|
NOTE: PROCESS HAS A VERY LOW N-28-D EXCESS I
I S1
CHECK CR VERY CAREFULLY
43 | STIR 20 MIN AT 32-38 DEG F MAINTAININ k.ttfi
, I +CR, ,+KI FOR S44j,, RECORD: TIME START|____ ____.1 57-A
I CR_rfl-.NOTE:
II
I | f>' IF CR-, KI- ADD 20=2= "AS IS" INCREMENTS |
|
I | RECORD CR_______< + > KI______ < + ) '
,1
|
I | HYDROCHLORIC ACID
,
ASSUME 32% I____ j
;s -d i_____ _
I | 2) IF CR+, KI- ADD 20$ "AS IS' INCREMENTS [
[
I I RECORD CR_______( + ) KI______ <+)
Ij
SODIUM NITRITE DUMP IN CALCIUM CHLORIDE
ASSUME 33% \__ _ | 725-A I___ _ I 1026 | 20-A | 126
I ADD FOR MAINTAINING 32-38 DEG F THRU S55 132X3301 57-A ibi.Sis.0
PT 13
902 14
jjri ]
FILL PT APPROXIMATELY 1/2 FULL WITH 90-110* F WATER FROM HOT WATER MIXER DUMP IN STRONTIUM NITRATE
STIR 30'MIN OR LONGER WITH LIGHTNIN MIXER TO SOLUTION FOR S58
IjJ^I WHEN S28A COMPLETE, STEAM EJECT(^-92
i FROM SO.INTO V-902
IN;sM-7'2p7^ SODIUM NITRITE FROM S20
a d d a mmo n iu m Ch l o r id e
I
I
i .i ii 68 |.246-B,E|
213 j 165-A I
68 >13
IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE
H_i5*P_r_/_4 /_______ _% XJ_L MAXI MUM VOLUME < +/.-Toi&) ^Fo F.SS*
WHEN S52 COMPLETE, STIR 3D MIN 6 RECORD: \
DI AZO,,iHb.__( + )
BASE_^TT_____ ( + )
|
-` rr_ikS,,(5*0-6-0>
TEMP_.^fe^,,(32-38 F) I
RUN SODIUM HYDROXIDE IN PT FROM S54 THRU !
DERSURFACE LINE, RINSE IN FT 6 STIR 15 MNI
DIA20 _--(-) BASE_rfc < + >
I
PR__ij__ (9.0-9.8)
|
STRONTIUM NITRATE N-246-B,E SOL1 N |
6 RINSE IN PT
1
TEAM EJECT IN V-932 FROM, S36
|
TIR 5 MIN , RECORD: PWUx^i 9 -0-9 8)
|
7-D I 140
DUP050102109
________ COMTYP JOB WANE = 32RT870DMH PAGE 04
DATE PRINTED:
EQUIP MENT
PAGE 4 OF 4 CG 32 CODE RT-S70-D <H>
II IF PH BELOW 9.0 ADJ TO PH 9.0-9.8 WITH
f
-"ONLY. RECORD PR__i
TDIUM HYDROXIDE
ASSUME 50% I
162T |
IN I QCTANOL
I
163--THEAT TO 193-195 DEG F IN 70-75 MIN 6. RECORD}
} 1___ DEG F AND REC_iW,_DEG F 16^1 STIR 60 MIN-AT 193-195- DEGrF.
! {
l l ^e c o RD: s t a r t _^l _J3!T^ !6rT AFTER 28 MIN S64 STIR
RECORD.: '
! }
II
PH_o!^y__(8.8-9.3) I
I I IE-TN4 BELOW 8.8, ADJ TO BH 8.8-9.3 WITH
1
} ^.f'N-T-D ONLY - RECORD PH___ TjP
ASSUME 50% l
I Po J AFTER S64 STIR, FLOOD TO 180-1.90*
I i (+/-18,00OG) AND STOP AGITATOR
I
~ "'"n ~c o d e"'T _ACCT 1 LBS
7-D 583-A
7-D /w
WHEN INSTRUCTED BY PROCESSING AREA. HALFWAY THRU PRESSING, DUMP IN, STIR 5 MIN 6 STOP AGITATOR. RESUME PRESSING.
10 j 588-A
10
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