Document meV5Mde2rq77r7p42bXrjE2d

Section Number: Issue Number: Original Date: Revision Date: Title: References: Ethanolamines/Glycol Ethers Tier 3 Procedure 605 1.5 12-13-91 Author: P. L. Bourgeois 01-15-98 Preparing Diethanolamines And Triethanolamines (T-260/271 Overheads) Samples For Gas Chromatograph #'s 7 And 9 Glossary Of Equipment Identification (Text #114) 605. Preparing Diethanolamines And Triethanolamines (T-260/271 Overheads) Samples For Gas Chromatograph #'s 7 And 9 1.0 Objective: 1.1 To ensure consistency in preparing a sample for analysis among all operators. 2.0 Responsibility: 2.1 It is the responsibility of the lab operators running sample analysis to execute this procedure in a safe and efficient manner. 3.0 Procedure: 3.1 Inject 10 milliliters of isopropyl alcohol (ipa) into a vial using the pipette designated lor this purpose. 3.2 Draw up 0.4cc's of sample using a 1 .Occ plastic disposable syringe. 3.3 Inject the sample into the vial with the ipa. 3.4 Cap the vial with an aluminum seal cap and hp crimper. 3.5 Shake the vial well to get a complete mixture. 3.6 Set up the hp 5890 GC following the instructions on the multichrome system. Date Printed: April 18, 1998 Paper Copies Of This Document Are Uncontrolled & Not Subject To Update. The Controlled Document Resides In File: Lab/Deateagc.doc Page 1 Of 2 D0 A 059831 CONFIDENTTA' 4.0 Revision: Revision No. 1 Revision No. 2 Revision No. 3 Revision No. 4 Revision No. 5 02-19-93 12-21-94 02-24-95 12-29-95 01-15-98 Yearly Review Yearly Review January/Yearly review Yearly Review Revised Section 3.6 Date Printed: April 18, 1998 Paper Copies Of This Document Are Uncontrolled & Not Subject To Update. The Controlled Document Resides In File: Lab/Deateagc.doc Page 2 Of 2 _. D0 A 05983? CONFIDENTIAL