Document mbDdMJR69VJ3Bkewpnkq70yXJ
CG 32
CODE RT-698-D PKG
frNOV 5 ,1982 ,
: /__/__
L2J32
'( DATE /
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PROCESSES
APPROv 3'b ?T
< > RT-69B-D <0> EUK 3/22/82
COMTYP JOB NAME: 32RT698DM0
A
STANDARD HRS. ___ _______ TIME
,
PREPARATION NOTES'. _J
___
___ ________ ______ __________ ., ;
NON-BLEEDING
EQUIP I MENT
N-CODE
ACCT LBS
;s?~
2
I RECORD; _____ _ BATCHES SINCE SPARKLER LAST
I CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
_______ I 777--A 1.
| SPARKLER & PRECOAT WITH 15$ DICALITE
I1
FILTER AID OBTAIN FOR SH 2-CHL0R0*:4-AMIN0T0LUENE-5-r
I' I I 740-C I
SULFONIC ACID
i .I
I 3 OBTAIN FOR S40 3-HYDROXY--2-NAPHTHOlC ACID
I 82-C 1
I 4 INSTALL DV 4, CV RECORDER & CONTROLLER CHART
NOTE: NOTIFY PRESS ROOM BEFORE ROPING OFF '
AREA UNDER V-922
NOTE: RUN 15* WATER INTO V-904. PUMP WATER
.1
FROM V-904 THRU DISTRIBUTOR. IF WATER DOES NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH
NOV 5 (382
r FULL FORCE, NOTIFY SUPERVISOR
RUN34* <494G> WATER INTO V-93I & HEAT TO I
I
'80-100 DEG F t^<>'ADD IN 8-9 MIN DRESI NATE X
I 4GO J 'i >
5 MIN 4, RECORD: PH_Jit'X__<9.5-1 .5) I
i STIR 2 MIN OR LONGER TO DISSOLVE FOR S50 ' I
I > </00 530-rA 1 '
35* (721G) WATER INTO V-922
WEIGH SODIUM HYDROXIDE IN V-926 4. RUN IN
I
TURN ON AGITATOR 4, STEAM 4. DUMP IN FROM S2
I
i 2-CHL0R0
LOT 4100%
4-AMI NOTOLUENE _3&J0U-- -/&&!&--
Jl&gL!
5-SULFONIC ACID___ ______________ _________________
i
MP IN ACTIVATED CARBON
25 1
DUMP IN FILTER AID -
10 i
,T0 212-214 DEG F WATCH FOAM!!!!
RECORD: BY_j"X_ <+> IF NECESSARY ADJ TO
4-BY
ASSUME 50%
___ _l
STIR 30 MIN AT 212-214 .DEG F, THEN SHUT OFF
STEAM. J4ATCH FOAM. RECORD: SPARKLER PRES
SURE
___ PSI IF NOT ZERO NOTIFY SUPVR.
i
CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOL`N IS CLEAR. MAINTAIN, AT . 190-1 95 F
FOR SI9. RECORD: SIART_AXCd?frOTAL MIN_/_
CLARITY^^-._ HT_/Z&_,_ F 4. REC_ZfZ._ F
7-D 2/i 2 740-C 1D86
113-B 777-A
251
7-D I____
i
LUJ =
uun I I r vJWP rti-iriu
W y w.i t w
EQUIP ! MEN? J.
I PAGE 2 OF 3
USE CG 32 CODE RT-69S-D (0) } LBS
N-CODE
ACCT LBS
994 A 4
RUN 2* <380 WATER INTO V-904/CV
J WHEN SI? COMPLETE, PUMP IN V-922 THRU
I
I SPARKLER. MAINTAIN V-922 AT 190-195 BEG F 1
I RECORD: STARTJg/^r^LTOTAL MlN_.jLsl-- t
902 UN 65* <1696G) WATER INTO V-902
I
3
I DUMP IN CALCIUM HYDROXIDE & STIR TO SMOOTH I 255
542-D I ^55
I SLURRY FOR S43
' . *. I.
MISC 4
922 ?
MEASURE
UNITS IN V-928 FOR S35 .
f Jx+ffDR0CHL0RIC7ACID
M JL
UK
IJKM WEIGH SODIUM NITRITE IN FT FOR S38 . .
I ^ ,J
m__j l Q___,MaLjK \i*L\
"I WEIGH SODIUM NITRITE IN DRUM FOR S43
m___IQ_______ i--SS-
I
i
-f5 r WHEN SI9 COMPLETE, STOP PUMP & INSERT V-922M
FOOT PLUG
-I
| RUN IN`"10" (200G) WATER & HEAT. TO 190-195 FI
I CIRCULATE 15 MIN- THRU- SPARKLER
I
I28-0 f 394
I7,25-A I -,f388
r 725--A I 32
I
I PUMP V-922' THRU SPARKLER INTO V-904/WBP
WEIGH SODIUM HYDROXIDE IN PT
_
M___ ______ _ *LfeSs3L.%
23 | DILUTE TO MAXIMUM VOLUME +/-100G FOR S47
324_i
7-D I 194 I
922 10,
r u n in 5* (80G> `Wa t e r & h e a t t o 190-195 r I tt CIRCULATE 15 MIN THRU SPARKLER
904/CV it ,
P V-922 THRU SPARKLER INTO V-904/WT
EN MTY BLOW OUT SPARKLER INTO V-904/4E R IN IGEPAL CO-630
HEAT TO 165-170 DEG F FOR S34
I
| 68 | 979--D | 68 I' . I
NOTE: IF N-740-C SOL'N WAS PUMPED DIRECTLY
ROM SPARKLER TO CV OMIT STEPS-37.* 38
CV N IN i ' <95G) WATER INTO
12 WHEN S32 COMPLETE, PUMP V-904 'AT -165-1 70 F | THRU UNDERSURFACE DISTRIBUTOR IN(TO CvV9 AnFApP
I | U 2-15 MIN), M^NTAIJy 165-170 DE:G F ItoCV
l Vr ECORD: STARR5Ztfag</ifci.T0TAL MIN.
___
I^^I^RUN IN N-28-D FROM S22 IN 12-15 MIN / -
j^^UsTIR 15 MIN AT 165-170 DEG F.
i srT /ADJ TO 46* <4&47GJ AT 32-38 DEG FiL.
CORD: TEMP'&M.-DEG F, VOLUME.ZT^L.
RUN IN N-TaS^A FROM S23 AFAP <5-1MIN)
& RINSE IN PT' |. STIR 30 MIN AT 32-38 DEG F MAINTAINING.
I +CR, +KI FOR S40. RECORD TIME START.
] CR^Jb._.._._< + >, Ki,_2fe_,,_< + )
l NOTe T N-28-D HYDROCHLORIC ACID X'S IS LOW
i f) FOR THIS PROCESS. BE VERY CAREFUL WHEN
I CHECKING CR-K IF YOU LOSE +CR, YIELD WILL
BE LOW.
' *,
_I I
3301 57-A
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_ COMTYP JOB NAME - 32RT698DM0 PAGE 03
* %^
_ . '__ __
EQUIP J I
..
WENT. I f ^'AtE 3 vjjOF-3 CG 32 CODERT-698-D
<0>
DATE PRINTED: S/10/82
USE N-CQDE ACCT LBS LBS
NOf E 1 ) - IF CR-JH^ ADD 20* * ASIS * * INCRMTS |
HYDROCHLORIC^tCID
/
J-
CONT
RCRD: CR__^( + ) KI__-/__< + > ASSUME 32% . JJL___
I 2) IF CR+,KI- ADD 20* *AS IS* INCREMENTS. \>v
SOMdM NITRITE
f \ ;/|
r D: CR_ ^Tl< + ) KI_>^( + > ASSUME 33% /I ______
^YotiDUMHPYDIRN0XFYR-O3M-NASP3HT&HSOTICIR.A1CIDMIN
^JJU/T. X'ZSJ'jl-
J I
^
I
28-D |^____
" I :8 '
'I "
725-A |___
82-C I 994
/.
UMP IN CALCIUM CHLORIDE I ADD FOR MAINTAINING 32-38 DEG F THRU S46
448 X33
20-A | 48. 57-A
902 . _UR N725A SODIUM NITRITE FR S24 INTO V-902I
13 DUMP IN AMMONIUM CHLORIDE
I 245 | 165-A I 245
CV IMMEDIATELY AFTER S44 COMPLETE, WITH V-902
14 AGITATOR ON PUMP V-902 THRU UNDERSURFACE
DISTRIBUTOR INTO CV IN 18-22 MINftAH0TAIN
32-38 DEG F WTCV. RECORD: START.
TAL MIN_J2rS__l_
,//
STIR 30 MJN 6,RECORD: PHJfJl.___ (5.0-6.0)
MP F <32-38 EEG F)
RUN IN. FT SODIUM HYDROXIDE FR 28 THRU UN-
RSURFACE* NE, RINSE IN PT"{. STIR 15 MIN.
ORD PH. L<9.0-9.8)f IF PH IS BELOW 9.0
AfJ TO PH-9, 0-9.8 SODIUM HYDROXIDE
~^
ASSUME 50%
RECORD: p h _J_ DiAZQ__rmr_^->
SE_j^rr,,_< + >HYDROCHLORIC ACID ASSUME 32*
St e a m e j e c t v-93* f r o m s s in t o c v
POUR IN I OCTANOL
HEAT TO 1737i75^E& F IN 55-65 MIN AND
I
57-A |_____
I 1
7-d Lsrrz:
j
28-D l._____
I
588-A 1 32
URG 52 HEATG, RUN 10*<268G> WTR INTO V902I ^
TURN ON AGITATOR 6 STEAM 6 DUMP IN BARIUM
10
RIDE
I
TO 155-160 DEG F 6 STIR TO DISSOLVE !
CV S52 COMPLETE, STRIKE V-902 AT 155-160F|
16 UNDERSURFACE DISTRIBUTOR. INTO CV IN,
MIN. RECORD: START/2j /.Z10TAL MIN_^f__
I.
HEAT CV TO 193-195 DEG F IN 10 15 MIN //}
IR/60 MIN AT 193-195 F. REC
TART/ZiZ
20 MIN S59 STIR RECORD PH
8.8-9.3)
NECESSARY, ADJ TO PP>H 8.8-9.3 ASSUME 50% .2.4..
,7-0 \^A_
AND RECORD: pH
ASSUME 32%
28-D |______
AFTR S59 STIR FL'ODD TO 180-190* (+/-18000G)
I
AND STOP AGITATOR
I
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY
I s"
THRU PRESSING, DUMP IN I OCTANOL, STIR 5
10 588-A i 10
MIN 6 STOP AGITATOR. RESUME' PRESSING.
I.
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