Document mBDngd0xyXOYXKkgerkDQMbYO

n NaTLSCD National Loss Control Service Corporation Long Grove, Illinois 60049 (312)540-2488 ENVIRONMENTAL SCIENCES LABORATORY, K-2 TO: CAROLINE TUTTLE SOUTHWESTERN REFINING CO. P.0. BOX 9217 CORPUS ORISTI TX 78469 LABORATORY ANALYSIS REPORT REPORT DATE APR. 30. 1986 SAMPLES REC'D APR. 22, 1986 REQUEST NUMBER 44336_______ PAGE NUMBER 1 OF REQUEST. SAMPLE NUMBER ANALYSIS REQUESTED 86-14 15 16 18 .19 20 21 22 BLANK BLANK BLANK BLAW BLANK BENZENE XYLENE TOLUENE BENZENE XYLENE TOLUENE ASBESTOS ASBESTOS ASBESTOS ASBESTOS ASBESTOS ASBESTOS . BLANK___ BLANK.... BLANK.... BLANK.... BLANK___ ASBESTOS ASBESTOS ASBESTOS ASBESTOS BLANK RESULTS PPM Front Back 0.44 <1.0 <1.0 <0.01 <1.0 <1.0 0.47 2.7 <1.0 <0.01 <1.0 <1.0 Fibers/ 72 Fids Fibers/cc 100.5 0.30 Fibers/100 Fids Fibers/cc 33 0.23 56 0.38 0.5 <0.01 15.5 0.04 0 <0.01 SUBTRACTED SUBTRACTED SUBTRACTED SUBTRACTED NONE DETECTED C0(l ENTS: SIGNIFICANT "AS HEXANE" RESULT NOTED ON SAMPLE# 86-13. < NEANS LESS THAN METHOOS: GAS CHROMATOGRAPHY (ROUTINE) PHASE CONTRAST MICROSCOPY TIE RESULTS WERE CORRECTED FOR TVE FOLLOWING DESORPTION EFFICIENCY: 991 - BENZEhE, 98X - XYLENE, 97Z - TOLUETE. Respectfully submitted, Joan A. Wronski, CIH, Manager Environmental Sciences Laboratory ACCREDITED BY THE AMERICAN INDUSTRIAL HYGIENE ASSOCIATION NC44S 10M 1-86 1380 SWR^sbesWS IB 000514 PRINTED IN U.S.A. INDUSTRIAL. HYGIENE SURVEY DATA WORKPLACE AIR MONITORING FACILITY OPERaTiON/jOB TITLE n ^fittest/ J EMPLOYEE &OU oJtcY __ lOolfoffc) SURVEYOR gtua-t/c. SAMPLE NUMBER 20- IL FILTER PE SAMPLE TYPE w Breathing Sj Zone r _ General D Air milh pofC- IMPINGER 1 0 ? AX LJ Resp. SOLUTION 0 Total 1 I Midget CONTAMINANT D Bubbler TIME ON t.lti Aj-- TIME OFF / ' /5 DEPARTMENT (T\Ct | rL-t-- SPECIAL TUBE 0 Detector Cj Silgel PUMP NUMBER Mu *3 FLOWRATE /V FLOWRATE QjC^ \ Minut Flowrate rr Sample Volume 509,3 X SAMPLING CONDITIONS TEMPERATURE ^HUMIDITY i ___________________________________________________________________ I_________________________ CONTROL MEASURES UJCX , 0 ^Oz&hlsL AIR VELOCITY cocrt/aJLPji- fCtyUfoOtOO , jcyjp (-3 C___________ DATE 3 ~ \(a "J(js NUMBER OF SHIFTS / EMPLOYEE NUMBER 0 Charcoal CALIBRATION DATE Hi*IK* BAROMETRIC PRESSURE \JA/ ..iiri mn foor- inSualoX u>s Q>\finCj > r\ goncraXeY /C6>~frrSsaf ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION XoJ? TuA - ~ ,30 f |cO .nr/cc SWRf/Asbestos 1373 IB 000507 INDUSTRIAL HYGIENE SURVEY DATA WORKPLACE AIR MONITORING kM-93 FACILITY DEPARTMENT T)nu&~uoc\tc/r' 6e-F/vicjrq operation/job title ' j rtlaiAt Tniml^or u EMPLOYEE La/ck- TcIqc SURVEYOR w/ C Tu.T?fc. SAMPLE NUMBER 0^1 filter type 1 j SAMPLE TYPE !,_/ Breathing :3Zone :* _ General Air SPECIAL TUBE 'nll/l0D(<- IMPINGER 1 O.Kj, V. Midget CONTAMINANT \H Bubbler As bat & TIME ON I'.Hl TIME OFF cw ! Resp. | SOLUTION 1 Total Detector PUMP NUMBER 6zmSix FLOWRATE /A FLOWRATE O Silgel DATE '5~lb'%L NUMBER OF SHIFTS / EMPLOYEE NUMBER Q Charcoal CALIBRATION DATE M inute TEMPERATURE Flowrate = Sample Volume HUMIDITY SAMPLING CONDITIONS AIR VELOCITY CONTROL MEASURES fcWwOQiS) lo&C , CftUu'aiJU aS-ify jrtb 7s i/vyiC~__________________________________ BAROMETRIC PRESSURE agbotca i Tr<j^ Piping liSl ^G^crtCtor [ Ccr^ffc^So/' r QDr-___________________________________________________________________________________ ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION CTViuaJb-Q. ' caisZCCL farC^o-uxUj -CffCf" ^cyfas-ytuQ SWRf/Asbestos 1374 1B 000508 INDUSTRIAL HYGIENE SURVEY DATA WORKPLACE AIR MONITORING 3o lq;Ato fj/~ Cfn operration/job title (~cf(tncSU t DEPARTMENT flla/rCX EMPLOYEE surveyor 'TcIq j m/y-'Cf' SAMPLE NUMBER sy V-./( 10 FILTER TY=E IMPtNGER * I i Midget Bubbler CONTAMINANT roboK} TIME ON H'.iH Or* TIME OFF r.rto- (SAMPLE TYPE v--XBreathing Zone r--i General CH Air Resp. SOLUTION Total SPECIAL TUBE tZl Detector [D Siigel PUMP NUMBER 6^s>a*3 FLOWRATE i\ FLOWRATE 1 Minuter "WX |t^{ Flowrate -- Sample VoiuL* SAMPLING CONDITIONS temperature ink. CONTROL MEASURES bU-&-Q lpcC 3l3i AIR VELOCITY A) E ft f dbfcZdLMk cfjyo*5 *'Goue/gjJj, rcjf/raLors, aftef joJr h cp NUMBER OF SHIFTS EMPLOYEE NUMBER [H Charcoal CALIBRATION DATE ' 1" BAROMETRIC PRESSURE 30. o -- Ta>^oqo CLSbcvtcfl -4/Or- H 1 j /A, Ccur-a fCoLtpCS ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION Lab ^ ^^/cc i <-^/T . 6^/cC SWRf/Asbestos 1375 IB 000509 INDUSTRIAL HYGIENE SURVEY DATA - WORKPLACE AIR MONITORING FACILITY ^ .SoujJ-uj zji cSr^ OPERATION/JOB TITLE jHcf{ nts<s J ^JPnytj.ioJLo^' EMPLOYEE SURVEYOR /rf. "2-1 rh ^ SAMPLE NUMBER <j / -- \Cf // FILTER TYE mnUtpOf*- O.f-U, IMPINGER 1_! Midget C] Bubbler CONTAMINANT AsJx^iol TIME ON ff'.'SN o~ TIME OFF {SAMPLE TYPE L__ breathing JS^Zone | OResp. i SOLUTION 1 | _ General Air Total DEPARTMENT SPECIAL TUBE d Detector ED Silgel PUMP NUMBER FLOWRATE I. ? J-iu* FLOWRATE Minutes^S^ ^ Flowrate -- Sample Volume l(p(t ^ J. SAMPLING CONDITIONS TEMPERATURE .HUMIDITY CONTROL MEASURES LOCX^ , d) ( AIR VELOCITY AJE. 3X'tO cooer&jjs, rcsf/fVXor's a.fto' Jnb )* <a DATE NUMBER OF SHIFTS / EMPLOYEE NUMBER Q Charcoal CALIBRATION DATE m ' BAROMETRIC PRESSURE 3b,o- JOB DESCRIPTION sjr~v^- -fironr- ~L*'flftnj jr~ s4rx_ toic CGo-ctOCS ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION /vO^ fezuJiS Office fuJA .ol^jcL SWRf/Asbestos 1376 IB 000510 INDUSTRIAL HYGIENE SURVEY DATA - WORKPLACE AIR MONITORING FACILITY operation/job title EMPLOYEE bU UODl'foY'S SURVEYOR j C "Tuit/c SAMPLE NUMBER FILTER TYPE 6 .* IMPINGER 1 1 Midget CD Bubbler CONTAMINANT fV\b*ih35 TIME ON i<b\ TIME OFF ii: i5 SAMPLE TYPE .\_J3reathing Zone __. General Air Resp. SOLUTION Total DEPARTMENT rUatrv'l'c^a^-t DATE NUMBER OF SHIFTS I EMPLOYEE NUMBER SPECIAL TUBE CH Detector CD Silgel Q Charcoal PUMP NUMBER box FLOWRATE FLOWRATE 1 CALIBRATION DATE ____________________________________ Minute^P^ X Flowrate =_ Sample Volume SAMPLING CONDITIONS TEMPERATURE HUMIDITY AIR VELOCITY _ _ _ _ _ _ QSl_ _ _ _ _ _ _ _ _ _ _ _ _ CONTROL MEASURES 'Di^csoLbU cjlr^oc-S , c^oc/nUs , hoJ-^v^uA fCQfiraXor t BAROMETRIC PRESSURE oC)Jo. 7L> uJA~ JOB DESCRIPTION ((A^ 7 i rbQulaXZcih-' ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION ^ foafe-- 'Ll) A- .q t> ^ -f?TS ^ a.oj- SWHf/Asbestos 1377 IB 000511 INDUSTRIAL HYGIENE SURVEY DATA - WORKPLACE AIR MONITORING kM-S3 FACILITY DEPARTMENT 5ou^A 6_>ej4 exr- jcf< ncsu\ OPERATlON/JOB TITLE ^ ^fn^AoJrof EMPLOYEE ha Ifad SURVEYOR CL Taff/c SAMPLE NUMBER tt(e ' >< FILTER TYPE SAMPLE TYPE ^ Breathing IS Zone r __ General LJ Air SPECIAL TUBE IMPINGER CD Resp. SOLUTION CD Total CH Detector CH Midget CH Bubbler CONTAMINANT A^bcj-io} TIME ON T-hl TIME OFF ir.No PUMP NUMBER 6PX*3 FLOWRATE FLOWRATE CD Silgel 3H3x 1%Minute lowrate = Sample Volume *~( u>[' SAMPLING CONDITIONS TEMPERATURE (oi CONTROL MEASURES HUMIDITY n% T- <lQ0~T(3XPjj AIR VELOCITY /(o rHf1-' ASlq^XuHjiiX. iUx ^fdZj yCoJicj_________________________ DATE NUMBER OF SHIFTS / EMPLOYEE NUMBER O Charcoal CALIBRATION DATE BAROMETRIC PRESSURE I uJ^L . kkxrtSt JOB DESCRIPTION -- g/f&urQ- ({ ucdub on ioujpf ^ _____ uaUt ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION .OMf [cc .o SWRfIAsbestos 1378 IB 000512 INDUSTRIAL HYGIENE SURVEY DATA - WORKPLACE AIR MONITORING FACILITY ^ouX^-ujesfzsr- dcfm^rCf_ _ _ _ _ _ _ _ _ _ OPeEaTION/JOB TITLE ~ / DEPARTMENT ftamT EMPLOYEE \iojfOr Tel4c, SURVEYOR / <TTidf/c. SAMPLE NUMBER ~ T "X' FILTER TYPE O.fr-CA IMPINGER 1 1 Midget CONTAMINANT HU Bubbler A^bc^to') TIME ON TIME OFF ' 3^0 fir- SAMPLE TYPE \/ Breathing r\A\ Zone CD Resp. SOLUTION General LJ Air (H Total SPECIAL TUBE EH Detector Cl Silgel PUMP NUMBER FLOWRATE .................. .......... P-DM' FLOWRATE _____________________________________________________ 1 DATE - H'S^O NUMBER OF SHIFTS / EMPLOYEE NUMBER Cl Charcoal CALIBRATION DATE Minutes*"X^?> Q^owrate co Sample Volume TEMPERATURE HUMIDITY SAMPLING CONDITIONS AIR VELOCITY BAROMETRIC PRESSURE CONTROL MEASURES X)i^oxe<-^24j (^/Qsog 3 c<u>oZ/aJL$ 5r yLtefouxXjx. , h^MjLDo^r JOB DESCRIPTION *^r) 005^/IP- Alt*JA UunJ" ANALYTICAL TECHNIQUE EXPOSURE CONCENTRATION CALCULATION [jbz^SXS ^.&(-(cc_ SVJRfIAsbestos 1379 IB 000513