Document km8a2mrpde8q54v0ka3Ne12k0
Vv,M *
PROCESSES: . - -APPROVED-?*
I, KYr-?^8-|D <G) ' 7/FWP 66/3<&&^
tr^r: / . ^ :.^ ?:r:::i.:? ma k in g n o t e s :
' *' ; : .
WT 4226* LBS*-.v.>v
fV ?'.60B~NAME7;^^3KT95iDPG^rr~-~^'TM#"'~ :
INSTRUCT^] bH'- %^`'VsS'''&?^,RPSStNG ;=
' RECORD
T 1 ''-' I--:' i
I,' | PRESSLOAD
\ J 1 ST I 2ND 1
I I ` .7 J . | :' ,i ,; , J STARTED
SiiELEASED-BY!
I
I23 Y 24 }
1 CAKES USED i WATER ON | HRS. WASHED'
I
i
'%?0,.OF CAKES! 46 | 46 46/! 52 J
I M HHOS
IPfe'S WITH - ; :#-
TON ` ! HRS. WASHED
M fH 500 M MHOS - r13!5-145 F WATER! M MHOS
4SEST AFTER 2 HOURS
' | HRS. WASHED
,*^LOAD ON 7 CARS " '"V-'
1 M MHOS
f
____ ! CAKE CONDITION!
I
I
_____ _| NO,CARS .LOADED!
1
l
___ 1 EXPLAIN LOSSES,._________ ___
. 3RD|
.V>;~ 4TH1; 5TH
I I 1 1`- ;i" - !. !
-&flftfLIVER TO
:.
-J "s a mp l e d "? "
J: RELEASED BY
------
- DRYING .
X 24 HOURS AT i 80 T
i LUMP:
-I^NOTE: DRY ON FIRST STAGE ONLY. .
4# RE-SET ON FIRST STAGE TIL DRY. !______
- OK - WET - SALTS - CONTAMINATD ___ ____
SAMPLES ' DELIVER TO
ADDITIONAL DRYING HOURS REQUIRED
.!,
NO DRUMS
I NO CARS PULLED
LUMP WGT
! SAMPLED BY
1 RELEASED BY
GRINDING -
MILL 93? HSP 3/32*RP SCREEN 3500 RPM | SCREEN
MAX. TEMP.
170 F
! MAX.- TEMP.
RPM F
______________ __________ 1____________________ * ! EXPLAIN LOSSES
- SAMPLE W/0 MIXING 1 ENV 6 2 FT CANS !_;____ ________,___ _
IF PACKED IN BAGS SAMPLE AS FOLLOWS:I
FIRST BAG: 1 ENV.
I DATE MIXED
40TH BAG- 1 ENV. & 2 PINT CANS
I____________________
LAST BAG: i ENV..
i SAMPLED BY
DELIVER TO CtL '
I RELEASED BY
LOT*________ COMTYP JOB NAME: 03KY908DMG PAGE 03
DATE PRINTED:10/D5/82
EQUIP HENTT
I PAGE 3 i
CG 03 KY-908-D '"
"
USE n - mccr LBS CODE | LBS
~S9*k I43" I~WHiN"s28--C0MpGETE--HEAT~SV^O~798-2O0~DEG~"F~~IN
I 5 TO 10 MIN
.
'^SS?]44 I CLOSE WATER LINE 6 DISCHARGE.VALVES AT STEARATE
1 PUMP `
. 43 I OPEN V-388DISCHARGE VALVES TO STEARATE PUMP
I INLET '
1 OPEN WATER VALVE AT STEARATE PUMP & RUN WATER
I THRU HOMOG AT 2900-3100 PSI, TO SEWER
I WHILE HOMOG WATER AT 2900-3100 PSI, OPEN HOMOG
I DISCHARGE VALVE TO SV AND CLOSE VALVE TO I SEWER
I IMMEDIATELY OPEN STEARATE PUMP DISCHARGE VALVE,
j TURN ON PUMP & HOMOG V-3S8 TO SV AT 2900-310
| PSI. MAINTAIN SV AT 198-20#F.
V-SBBJ3W9 I WHILE HOMOG V-3B8 TO SV, SHUT OFF WATER VALVE
. I . . 1 AT STEARATE PUMP ASAP
V ;|5 1 WHEN HOMOG COMPLETE, RINSE IN V-388 WITH HOT
-- I | WATER FROM HOT WATER MIXER
' !51 I WHEN S50 COMPLETE TURN OFF HOMOG 6 STEARATE
. I 1 PUMP' 152 } STIR 5 MIN AT 198-20*F
153 1 SHUT OFF STEAM
154 1 WHEN S53 COMPLETE, OPERATOR PB
... 155 ! SP STEP 23/53 RECORD PH____ ____ <3.3-3*7) 156 | IF NECESSARY, ADJ PH TO 3.3-3*7 (DOWNWARD ONLY)
1 & RECORD: PH_____.
I NOTE: USE LIQUID ALUM, N-115-D. ADD TO SV VIA
| BADGER METER. STIR 5 MIN AFTER EACH
I ADDITION.
ASSUME 50%
157 i RUN IN N-7-D FROM S-3 IN 10-12 MIN 6 STIR 5MJ.N
158 | RECORD: PH_____. (4.2-4.4) & IF NECESSARY, ADJ
| TO PH 4.2-4.4 6 RECORD: PH,,,___ ASSUME 50%
| (DILUTE 1 PARTS TO 1 WITH WATER) ASSUME 78%
I 1 SIPHON N-7-D INTO SV 159 | OPERATOR STEP PB
160 1 OPERATOR STEP PB
161 I.SP STEP 6 - BATCH COMPLETE
I
I START
FINISH
OPERATOR
TIME SP STEP TIME SP STEP
115-D 1___
I I 7-D 1_____ 27-D 1___ _
DUP050060034
' >* 'tr*... $03
( "5)ATE'5
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.1 I _--
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. ~ 11 _ 1
* ''
---------- ----- ---
CODEKY-908-D PKG
L2J2n 4226*
( LOT > - ( EST WGT
aft
PROCESSES < ) KY-908-D (G)
>yt/ COMTYF* JOB NAME: ) fj
STANDARD HRS-
APPR01 FWP 10/05/82
03KY908DMG
TIME ____ M
* BEFORE USING SV MAKE SURE N-28-D LINE ( HYDRO- |
----- i i|
CHLORIC ACIffTYlF ANY .IS BLANKED OFF.*
||
|
RUN 60*(99h.G) WTER IN V-203. SET AGITATOR ON | |
|
I |\HIGH SPEED
1
- Ij
|
,205 I 2. I WEIGH IN DRUM IT POUR IN ( SODIUM SILICATE )
| 420 I 32-D | 42
| 3 I DUMP IN AND Sl\ip 5 ~pN ( CHROME YELLOW) ' i I | RECORD : START..___ LOT______________________
I 63X5IYC-3-BI 3150
I______ |
|
ii
f in .------------ yc
------------- LL
I______ I
4 | ADJUST TO 75 (1275 G) *NOTrr^OLUMES~HIGHER
Y-t h a n ^^mAy , c a u s e d u s t i><g in e x h a u ^h o o d .
I 5J WITH. A TATOR- ON LOW SPIED PUMP V-203 T^RU
I 1 i HOMOG'
2400-260 PS1 iNTO V-205
.'Hr
- ! 6 1 WHEN V-2 MT, WASH 0L0w\THRU HOMOG WITH MIN
, | | OF HOT
AT 2400-260 PSI INTO V-205
| 7 | RECORD: V-205LVOI______6 AD.
| 8 } INSPECf HOMOG STAINER & CLEAN IT
-205"~9T^RUN~;?0T_75T4~G7~WAtE|_INTO V-___ - ST>^T AGTTATOR
SV |10 | PUMP V-205 THRU HOMOGNAT 4800-520 PSIn 5N0 SV. | | RECORD: TIME START ___ _V TOTAL MINUTES ___ __
2 i I NOTE: IF HOMOG PRESSURE FALLS BELOW 4800 PSI, V I | | 3-WAY VALVE WILL RECIRCULATEXSLURRY TO V-205 |li | WHEN V-205 MT, RUN IN 5' (240 ^3 WATER 6 PUMP | i THRU HOMOG AT 4800-5200 PS I INTCKSV
SP I 12 6I CP I 13
"I 3 I 14
I ns
. SP STEF' 01 - SET FORMULA SELECTOR T(
2 (V-243) OR POSITION 7 (V-244)
PRESS SV CAM RESET PB - SET 22 TC IN
REMOTE (TEMP IS SET AT i90-194*F)
RECORD- LEVELS & SET R/M COUNTER *1 AS FOLL0 JS:
A. 11 LG_____7. PRESET
95 GaI
(LIQUID ALUM)
SET STRIKE FLOW CONTROLLERS AS FOLLOWS;
3FC10 (N-27-D CONTROLLER - SULFURIC ACID ,
1 IN MANUAL
0.65
3FC20 (N-27-D WATER) IN MANUAL LOCAL 5.2 GPM
3FR1 (N-27-D/WATER) RATIO
0.8
8FC10 (N-32-D CONTROLLER) IN MANUAL 0.87
8FC20 (N-32-D WATER) IN MANUAL LOCAL 4.8'
8FC20 (N-32-D WATER) IN REMOTE <1 8FR10 (N-32-D/UATER) RATIO
1 .1
1115-D | 504
II 1I I 27-D I 218
II II
!I I 32-D | 1476
DUP050060035
N41015.01
LOT*____ _ _ COMTYP JOB NAME: 3KY908DMG PAGE 02
BATE PRINTED:10/05/82
EQUIP MENTI
| PAGE 2 |
CG 03 KY-908-D
USE | N- |ACCT LBS | CODE | LBS
|16 OPERATOR STEP PB
320 |17 RECORD LEVEL 2LG___ Z3F (35% FOLLOW SOLUTION
SV i
MAKE-UP PROCEDURE F0RN-27-D~\
SP IIS I ADJUST SV TO 47' <2400 0 7`
"
CP |19 RECORD PH ___ . ADJ TO 11*0-11.2 WITH N-7-D
(CAUSTIC SODA SOLN) AT 5% <10 PARTS WATER TO 1
PART N-7-D)
A, I I SIPHON INTO SV* RECORD:"PH l SL*ASSUME 50%
120 | OPERATOR STEP PB
_______l I
I
7-D |.___ I
T5T~T 7jp~STEP~667397~AFTER~HEAT-0p~RECQRD~""pH~ZZZ7
SV 122 | SWITCH 3FC20, 8FC10, 6 8FC2 TO AUTO
SP 123 | OPERATOR STEP PB
124 | SP STEP 10/43. WHEN 3FC20, 8FC10 6 8FC20 FLOWS
ARE IN LIMITS, SWITCH 3FC10 TO AUTO* 6 PB
125 I SP STEP 11/44* WHEN 3FC10 6 3FC20 FLOWS ARE IN
I I LIMITS, SWITCH 3FC20 TO REMOTE
126 I OPERATOR STEP PB
127 | DURING STRIKE RECORD;v
SP STEP
V-243/V-244
' '".IP " PH RANGE / TIME
13/46 <30 MIN)
_____ 9*3-10.0
_____,
14/47 <60 MIN)
' ___ . 9.3-10.0
_____
15/48 C2 HRS)
%}/i_____ 9.3-10*0 ________
16/49 <2 HRS, 25 MIN)____ 9*3-10.0 ___ _____
17/50 (FINAL 3 HRS)>%ste__ .7 .5-8*5 L____ ___
I ` I NOTE: IF PH NOT IN RANGEZ NOTIFY SUPV & NOTE
I l ; IN LOG* IF FINAL PH >8*5, ADJ TO "7r5-8.5*
I I 6 RECORD: PH___ *
* ASSUME 77%
27-D
128 | SIFT IN (BLANC FIXE N) '
/.'/t:.//-5
I 55 | f28-#
' tfr&fSS8jkyfr-' ~55r':~
-385 129 | ADD 42' (320 G) WATER TO V-385 -6 130 | ADD & STIR FOR 2 MIN FOR-S 57
I ASSUME 50% i 260 I 7-D | 130
|31
387 |32 7 |33 I 134 I
| DURING STRIKE CHECK LEVEL IN V-387.
| IF LOW LEVEL LIGHT IS NOT LIT, GO TO S-35 | IF LOW LEVEL LIGHT IS LIT, VERIFY BY CHECKING | THAT LOW LEVEL PEG IN VAT IS- ABOVE SURFACE | IF VISUAL CHECK CONFIRMS LOW LEVEL, FOLLOW | STEARATE MAKE-UP PROCEDURE.
135 | RUN IN 2S' <244 GAL). DO NOT MAKE UP THIS
I | SOLUTION MORE THAN 30 MINUTES IN ADVANCE.
I | DELAY BETWEEN END OF STEP 41 HEAT-UP AND
I
I I START OF STEP 48 HOMOGENIZATION SHOULD BE
I-
I I LESS THAN 30 MINUTES. 388 136 | TURN ON STEAM it, AGITATOR -
l-yI
8 137 I ADJUST TO 32' (317 GAL) AT 478-182*F
I.
138 | SET BADGER METER FOR- 466*
^-
I
139 | PUMP IN FROM V-387 THRU UNDERSRFCE DISTRIBUTORS| 378
I I AS FAST AS POSSIBLE <ISOBUTYL. STEARATE, BUTYL I 44
STEARATE, EMCOL P-10-59)
^. . I 44
|40; |. SHUT OFF PUMP
- v ^-V
I
141 L STIR 30 MIN AT 178-182*F FOR S48'
l
|42 | . DO NOT SHUT OFF AGITATOR
.
I
DUP050060036