Document kDGRjgRDoDRJOvEJ2ekr2aoeD
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'
DATE PRINTED:
GG S*1 N CODE YE-698-D ^ ,,
iM$m' -Loam 5527* LBS.
C . DATE ) .
( LOT > ./ ( EST WGT >
f
PROCESSES
APPROVED'SY
( ) YE-698-D <S) FWP 6/22/82
A yj CGMTYP JOB NAME: 1YE698DMS
TYPED BY: JMW
EQUIP MENT
NAME: MOLYBDATE ORANGE
1 1
USE LBS
*1 J
N-COPE
1!
ACCT LBS
PREP A
i- 1>S*^T5DbETTYAIN. FOR S-2 I JT I CDAALLCCULATE & SET ON BADGER METER FOR S-23
V . -jfa&d&u*
4 ^4 i .108-A
195J 33-D
! 3 L/OBTAIN FOR S-2S
I 734 i - 4-A
I-'4 1/CBTAIN FGR S-32
1 146 1 3-A
j 5t/OBTAIN FOR S-34
i 237 1 32-D
1 6 OBTAIN FOR S-38
i 35 I 3-A
! 7/ OBTAIN FOR S-41
1 7 | 711 --B
---------- j------ ------------------------------------------------------------------------------------------------
351 \ sr\ WEIGH INTO V-351 CHECKED BY:*___ M&1&M3U;
n tr i
ji\-$-3-9-2-S--2-I-Z2--.-..-.1|!----------11-u--..-~_~--DD-.. ii i i
i 84
1 ! 6 l 734 i 146 i 23? i 35 | 11 7
I 1885
1
359
wWEIGH IN. OPTR_____, MK $7_, l-Zlnf)
x i &52L2L i 425--D- i / vTHJW* /* -6 , j A*ru
sv 4
358 5
IjXRliH 20" (996 G) WATER INTO
~
ilj^TRUN IN FROM V-354. OPTR ?,/)/ , MK 34, .%?.*Fj
RECORD: G/MLASZfcjCi .270-1.328)
[ 41 --D | 511
j i ^-RECORD: PH,,iL2._<2.2-3.?}
II
V
11 AD J TO 76" (3625G) AT 67-69*F `
I'
RECORD: TEMP_jfe$L__*F
'
Vmssdv 57-
I
i Ada:
U-3--I .STIR 5 MIN & RECORD:.- PH^fi.C2.2-3.7)
r IF NECESSARY,ADJ TO PH 3.0-3.1
RECORD:
___
ASSUME 6` S
! I NOTE: DILUTE N-7-D 16:1*WITH WATER BEFORE 1
33-
I i .-ADDING
ASSUME 5G5S!
7-1
i jX' RECORD: Ji/4Q_G/ttL (1 .142-1.144)
i
I i NOTE: IF G/ML OUT OF LIMITS FILL OUT
I
i 1, CHECK LIST &.ATTACH
'
!
14'" i STIR AT 67~69*F FOR S26. TAKE 1 QT SAMPLE. _________________ L_X
-------------------------
117- I RUN 10" (50 G> WATER INTO V-358
!}3^r RUN V-359 INTO V-351 PUM IN V-35
H> 1 ADO TO 55* (260 G)
`1
r&r" I- SIFT IN N-1G8-A FROM 121 i .STIR 5 MIN & RECORD:
9.--1 .)
1
f
122 T ADJ'TO PH 9.8-9.9 6 RE
ii
' ASSUME 5% I_______i
ii
ASSUMS<5% if
123 ! ADD f-i-33-D FROM S 2 U:
DGER METER
1
124 1 ADJ TO 66" (3121 G) AT.67~69*F
I.'*
7 -D 33 D
I RECORD: VOLa/-_* & 125-1 STIR 5 HIN*& RECORD: PR'Zdi(7.4-16) &
.I
I ! G/ML
.089-1 .83)
I 1 NOTE IF G/ML .OUT OF LIMITS FILL OUT CHECK
x^S <*. /*> JUljl 1
! > t LIST & ATTACH'. TAKE 1 QT SAMPLE
N32801
LOT= . EQUIP WENT L
COMTYP -JOB NAME = 01YE693DMS PAGE 02
DA III PKiNIt-i,: ii/ .c'.^/ a, i USE ! N~ iACCT 1 LBS I CODE i LBS
iXi I
OBTAIN 1 QT SAMPLES OF S-16 & S-25 SOLUTIONS & TITRATE TWICE
RECORD: LOWEST PH ______ & ML N-10-D LOWEST PHit ML H-10-D_____i_
NOTIFY SUPV IF ML N-10-D 'IS NOT IN RANGE 7*1-7.4 OR IF T-HE TWO TITRATIONS DIFFER BY MORE THAN 0.10 ML N-iO-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS)
DO NOT PROCEED IF N-iO-D TITRATION IS OUT OF RANGE
ADJ0ST V-353 TO OBTAIN A TITRATION PH = 2.05 (2.00-2*10)
.! 7-D
WHEN $-26 TITRATION OK , STRIKE V-358 THRU
SV BOTH,.UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN
.
RECORD: STAF,`T
__. TOTAL MIN_7V_______
hTOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
BUBBLES APPEAR IN SIGHT GLASSES
IMMMEEDIATELY DUUMMFP IN N-4-A FROM S 3 & SET TIMER 1
! ..FOR 15 MINUTES
L29^X~DURING S 28, WASH IN V-358.
VS5 \ STIR 2 MIN & RECORD
< i .8-2,.5)
__(MUST BE + )
STIR TOTAL OF 15 MIN FROM S-2S &
RECORD: TEMP__jt;rl*F (67-?3*F>
UMP N-3--A FROM S-4
...STIR 3 MIN '
2HrX.P0UR IN N-32-D FROM S-5 ' 3ff'"LsTITt 2 MIN
L-.RUN IN USING BADGER METER.
t
iII i 734 I 115-Di 367
Ub ^LdSuTmIRp
3 MIN & FLUSH ALUM IN N-3 FROM S-6.
LINE
WITH' WATER,
I i .1
STIR 4 MIN FOR S-43
> |4<i RUN IN USING WEIGHT & FLOW CONTROL PANEL-
(
390 f ' 1 .
MK _V___, JSSJS&JL
!I i 28-D i 105
7 I '\
MK______ ,_________ % f_______ i 28-D 1.
\AJ^T DURING S-39 SIFT N-711-B FROM S-7 INTO V-390
I. i
WITH AGITATOR ON IN 1-2 MIN
Ii
?TIR 1-2 MIN.TO MILKY SOLUTION
WHEN S-3.9 COMPLETE, IMMEDIATELY RUN IN N-711-B
SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
WATCH FOAMS!I IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES,*
7"DUMP * IN
'
raff"I .STIR 10 MIN ,
[^1. RECORD : PH vfoQy' (5.8-6.0)
!47 i IF NECESSARY, ADJ TO PH3.S-6.0
ASSUME SOX
& RECORD: PH-._vJlV.____
ASSUME 66%
RECORD: TIME
rLOOD TO 153' (7619 G>
STOP AGITATOR
START, FINISH* OPTR HELPER
.JZIPSA -JB
ii *
330 -Ti 28-A! 330
. 7-D | 33-DI
I
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