Document k6oeQdo2XXVEdD8z2ydQrXwYO
E. I. DU PONT DE NEMOURS & COMPANY
KREBS PIGMENTS DEPARTMENT 256 VANDERPOOL STREET NEWARK. NEW JERSEY
Serial No. KN-50-4 Copy No. #1 Numerical
NEWARK PLANT PIGMENT COLOR RESEARCH REPORT
Final Report "MDNASTRAL" GREEN TONER, GT-674-D Period Covered; March 1, 1949 - May 1, 1950 (11-18 Charge; 1101(12-18
FILE: 223.42 DATE: 6-30-50
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1, 1949 Hay X# 1950
Jmm 30, 1950
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faefcoiy product jpRor^culjurl^ for lals and p&astiee end-use.
This
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v ,__ ..... w /a| ^ef-Flei^^-^ee^ysLy^^saiF^h. sae^ad"aadpeii*ed^ewp--^S a saadee--sf * cdT ^w^ew^eMeA^pFe^aa--e ,^*sr^pa^MaF4^^^w|*wpre.^wem*aw| Fe4ie*^te^^weeaaieiei ateMeia*ae^njFa^nspadeseF'art*f
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N674r0%^ 'QtaastaoO* Orem Toner, for n * plootlco, hat now bom recoded 0?-7fcM},
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. poraticn, and 0 compUto aepwration of flgueb from .
01^%!^ f0 O^U^y fpfiftti*** |y bftiiiJlf#| 4# jfrpMpflfty %f0tt6<l mftgyyflt-
prlilollt
adbogg bo tiff ffyffb pell ao tfhff fnV yff00ff|> &fQ& tbo
. 0# wuJ --4*-- dill iMwrfdw IM'*II ma Kl4 ft* mm0tt --
t-tt*i;0f 'blub ffy# Timtllj Kfrfjm doNH '00 ttUXing* Qq tiff
seal, o grit-
froo Ink voold rooeivo a rating of 8,
ffal y^ftbiVff ffbyffBft'bt by fObSKb Of thftftO
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OT*67W>, lot 430 va lot 451 S fttreag, o. yt&Xmt
oM9v lot 451 vo lot m*m*t lot 234 1 aB^Iggp ffgPPftr^g--g^p^f V^fglliglglplSggair* I'IRfPlVt^A^^poMopp
OWit#* Lot 160 v lot 234 2-3* tro*
P my typo fflitfHffl jjppc0sjjBbag tlOl OtlPffn^th of wt 451* 2$ owatalao no HUM luv*
^01 yntflititifli
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fepgpk o {ggy *ko 4ffV* ft
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in tbo
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in poop tcactuno^
yit, poo* ^4fffBPii1.<ffff in jp** o h I jflLftatlcg* if tfoo*
jo f0^ iit^o m ink oobiolo --4 ptnood oym* 0 j'-noll init
jdv01ffHCfc
jttJ *wiimi<iw a*?jt^ltm mu ih m4 W ftm fftHflTHI mm-- ' An Mm
o psoporfly tyofttodflofb'powdftj*null gjjvon pwpfftOfcly uulfoonis
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sfcft&i* Hay ****** tttt
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_ for the preparation of BT-284*D tea Bimft;&nn
LB
) involves
^WWOHEtv w* * 4&Q* feS'ItMteWMMnOrt#il pwpg jAHrW Mv) -wmwimm*'gifePfljRlilfiifil^fre .
the Abbe Lena
u (Set BT-28L4) fosttla s bNi *) tuts tfslpeu#
used tea Kcvenb 194a, to June, !%$ to prepie- oMM ftete
paste (H**b24)* ` `
a p&flte of excellent -tastes is ob-
sietw *pse*ew ea.<sepw*w>p gwoaff-ew fWapMMannawwe wvn^gbf j-wMwfa*ei*maw ime the C"wrafo ae*'"t twhmme^ *--w--pmpme>
IBfift'ftttd
intensity* It :h m thought that this Ooo to the
S| ww
innr-r-riwmr ottii diffwest types of aglbatloiig
Ab# Lensrt Biscay, Vat ^| nd a
tehij,
th#
In the
+ o.pv^p*SmSf UAb^.f eg^snfiofeop gnaemF*Fwfedese^P;ri.:.
Hjf flftplstaluCLttM^
SSIr1
jaiupio aoill with
all yfjpypti **ifxdLcl0SjOn yielded pewdsrs %dth
texture and
be*
fettvl^lo>ry*. tthhe_ir H_Tset on the- co_lor was
eerie ***w
of the Itof o^f,
( (A) OT-674-D) process* tdum TEA-CTo ester 'en'u"ls*ion* with c^at i Imw. _b
{vorast with regard to Both texture and strength '**m
la
foot, all agents bat the COa-TBA-CTM eater eaalaicn were eventually discarded,
bWewWcaWuMsVePF e**Ppi*tPfhP^e^fOrp t^hMPeF iWnwMkP mMIOTWiMlHli `t^Br^BoF'.PnBreF^r'Pf^cPJlPeF^FaBP oIf wf the BtPrp*eiPF^a^F-^tF'ie^F'^^dF -
a not
or the agents affected the strength or intensity
2n Table if are listed the various agents thaiy affect on the ink mill properties and oOlor of 1 idtb good texture and ink ndll behavior wave alee However, none of then could natch the CSU treated or strength in vinyl, or in ease of oamfacture.
with
couleian of^^iJI
powdersimilar to i
.o^Rjsa^aaaF*atFo^epd^^a 0pf aI4mw iBnsearete*F^xe^^te*uFeer^Be e^woeal^p TMr sphs^^r us^srtvprispl^pf behaviorj*w w^"Vint^Fh^Be ewnap^Speabjgr a F^aa<w^p^sves*s.r plops^s^feSp^*^b sipbf^f ?# in inteiud.tr or strength* cotanared to an untreated control* Labor works atudiss indicate that this treatment retpiru ffioi.eBfe high suoh as that provided by a BLigbtnin aiasr* an Ahbs'lsnart adaear* or * w*. unit* Vat 240 and the draft tube unit (Vat 190) in 6 Building arc need for GT-674-D* because they provide good agitation, end Will handle 1200 lbs* on the :
revived *AB forsnla* The Abho Lenart alxer umot hold we#* than AGO lbs. of a lOf slurry of M24*
The elnriy concentratico 'is -so inpsrtsht factor in -the (jiditar of the
Increasing *hf J@(
concentration in the *&* or ''(F fonu^Uui tw**.
0 Bn^ dullness, w^ ^wiyows tide
.hahavior slightly*
The C fomila is ths nB process, with the addition of to 0 hlsne Ox** to adjust the strength of current that of tho GfdVH) standard. Loot 451.
DUP050068146
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Wfwtiiw tho VWt dunv |s ihg #ABPbBBVbP^^BBB^BB t BIB lPBB^B "BPPBj^W
.BBB*^^ *PV
ismyaa strength *p4 Istfloaitr. tefe
.^B P
^B ^P^P
BBB ^p ^BPB^P
seriously afreets texture end ink adll behavior.
fto si* nrofiftsB nailfas no htstlm* tut e iittiif&etfiFs ira^iMt
be obtained fro the .c^wamdaico treatment without heating the slurry. the ih *4i ha.<wo neriodfor e Ai# lb. %%# to ground 90 ntautes. Ice 1200 llii.
*^bsp>BQ^eeiumwumi lweb^pusb a^^elenseeuae^t^epepsep.w t.^hbwe^b tsmoaratur*e^p can bbw^eb varied ppebbob^mn'msf ^l^d^peb r^Ba^ptid^ngsrMASr!^r^e*me 4e1e,r9ae0**mF^ef^^eeew
abort periods without affecting the promt, -
' *" :
l' wjp f*fhWBfTpl WsT#JH emr*wnosorAeBSepMep isesw e"ptbsmiaBmweseiuiaipvy Msue*boppsppspvmpbpi
t^MeOWTinff, i^^taP c^Pa^WnBB b^Be^P bgpP^h^Bb^Bb^PS^B ^Pr^fP.W t^oP^P >.^hPPw r^t^pB^wj, ^iPpws^B*.M T^wPw tBk^^iPsB^P M^BPia*^BnBVtP ^ ^P*B^*B cBPBbSiBt^i^PMMlM aHaese
set nay be sllminated. the {ft of the slurry is
from S-IO to H mean
to facilitate the crossing operation. Washing ot the ifp .ft%%fi ^^PxtAydj %Q
sub Is of ^||j| %pa&&iBg
A* treesina *ten4y of t?hPBBe^B aBiPa a^MPsrtSaPMBBSCpui&PBePe**
ends.
(B-&3) in vXI&O gave l
of the
t Bine W
results as
sd what wij^*t 'be eeefffdfyed sar>*
prising is tha.-t a__d_d_i_ti_o_n_o__f_iq......C...&. a.., to...a....1.Q.. dmf in fab 340, as in the M*2&b&
material .ae good as tie CC3j.-aalaioo poem end $& '......... " ''
in the AbW&mart sixer, phis stronger material is
ABT-322-C*)
fh quality of both GT-674f D end 0r*2SIHD hade in fat 240 and the
draft tabs aeptare to Ins due to the excellent saltation availahle. If th* treat**VMBBW BB*PPB
W PB B^ " "" P*r ^BPp ^BWb ^*p **P*B^BiCB e^Q|^ if^BB|^B^B BPB^BPBepWBPPSBW^P B
*(* SPBPPP RpCb Wb ^B*^
log agsnb, shleh aagr be water iadscihle, ie dispersal thoroti^r end tadfenedy, :
it should not affect the odor* Hosovw, if dispersion is non-endJam and anas -V
of the particles ore in contact with eaceePsUeiWve wmwowunwts oV*f tWhe agenta. WdiUll4nUeVsSeO
utiakntoM Mar dui ttfchwp to(1) oriratol (toi9 of the *%i -- mmddip^^b^b fBBwpwMBB
s p d mt'^Cp*'"* b *^p^
*'B
PPf
BMBB*m>W ^P^P WBP BWB B*Be*BBB PPBPPBBP.pPBP'
by the plvmt or (2) to the mem
fhe cpali^r of the podaet, thmefors. s^^P^s^J^Bi^f^BaPB^^BSPiPi^^BwBB used iBnBP the tSrPI^eP waPBBtPPmBBSe^B^n^PPt^.b VoPP*tP escesmPPl^eP^*B epbv^bepw mhig the treatment gives a product ns softer in
upn the type of vet or peddle mtatioB
fet if m use hi# speed agitation with a tusbine blade lightnian
bladed vab agitator, we obtain a prodnet Uhleb is finely teextured end above little
or no separation, slight tailings, and good strength dwelopoant on ink tests, end
mod disoemlon in ni,*4 or rubber* {enhfr is ie >*b p b Cb Mm> of tha
ibpnb tbtbobb ^SMr h^Ijspr MBBPpagglBtp eSrgtFaVBfi'wt't*l ^^gg*pesBB^(B,^w*B th b^b ab^yfag fvr.%*^t#nWirin j*^Btwttoieei*ieit"f*t*.egBh' me^ppiimhealiPlBfs*peBgmijfgB %em&r 4'Khimm
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DUP050068152
aSaMSwsessessttti 1* t. G,
Psp&eoaa for soft W|tp^r4g
2. f
fel*r*
Soft Powde;p ftnoceaa for CPC
Ha* 77, Serial 8*. 19909
3, Uotobookas 1^36, 1367.
DUP050068153
DUP050068154
Codot <?N674-2> F
AbbO*
Mlstr
:^ULllSlo>
U ftaml or poor Into AIM or vat la dru*a with ntfa flwyimqfc <jf
wator no axpoodlng 4 gallons poo <tras
3.
4* SfifcVi dLwalatlffla potp*
0 Stir 10 aitwtoo or longw to eaaooth aLuriy.
6, md paw M
?. stir 35*35 l*ite to a oaoolh slurry, g^tot if wwaosaiy, fm*ii incrawA of wa&sraheold bo edftMt ia m4m Hn4' afro tCbwxy vili loot Oa$$^ <
vslv nD3nPw8UMvvwyQ^o CXSBSpjt
40
f pm out diroeWy to feyor *
.^r,'r--' A^.
DUP050068155
ProcMa*
Pressing Instructionsj Veil AbW Lensrt Mixer #2, r 240 Press without agitation* lioeg ee 5 owe.
Special instructional Ron-BlOoding. Hast not conteainste with im blue,
wP-- *Hoars Temp.
L.V, 40 140*
H.V. Hurricane 30 40 140*F 140*0
Mt
DUP050068156
Cod** G?-67W> Ssti 400# Vat* 2#
X# (B)
Vat 240 1. !*m* o* jwnfr into Vat 240 I 10
2. DM in dams with dU#t oV vstip q o ^ yftflyfjtii'tag gallons
424 m
3. Site to 12 (530 pl,>, 4* Start agitator, 5* Start centrifugal droulation 6. Vast and'record* cB nomal 7*5*40*0
o* H122 :
*
% .'/' " /
s* Weigh mid eiurry in clean drum with 14) gallons water at 100-040*7,
4
9* Weigh end add to alnrrlod 8-666 in 1*2 ahmtw wlth agitatien - 20
10, m* mm 8-650 is dispersed ^ and eeulelflodln solution* -
m
m m
x'-Wj P'-:',
'/ "Ml.
;V:m'^ *
' -. .i 4s--?vv?:
& ' ': .''v-;;,..:;-::i? ;: . 20
'* v>,,
240 11* host to MI7. 1
12* Stir up drua of prepared etmloloo ' and poor into Vat 240,
13* Sold at l^SCte*f with agitation sad drculation for 70 MLnataa.
.* .* 3*C--$j--5ttrj3i rTffVi#S B*m*, IBmmfmi*
14, mfd SHj bih thru Ttf.Oft p3&t& hft||fl|
* - ' i.
13* Chat off drcaladoa puap.
1A.
.*Snt*
tmA mrii Haw* l*b> Via Ofcft.
***^w *v 'apnai^rw
e *pw
"
17* rraos idth agitatioo.
DUP050068157
Code* GT-67V let* WOorW Process* (8) or (c)
Presdog Instructions! . Tat* 249 Press 8c. 92 So* of eakca 50 Press *&th agitation. *'. Do Sot Wash Load on 2 ears.
Special Instructions* Nen-Slee<Sliig
PoSr wist resaatn at vtt daring cashing In to avoid excessive use of wash eater*
Paying laafcractioast
tm X..V. S.V.
Scare
4a
n
Ump* 140*F
Hurricane 48
T#trngtioo8* Grinder Mo. f US
i . *
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DUP050068158
:fhs )SV< proopes replsejea vie precious eApocei^es'feal 11A foro.aXeu
:ifXis: l::nt*a,'L;;. fcs lit neaii'iHotor-O of Oft? grccois stiMs
\.'.,, '. -'. i* : *> , cu v..-., '- >':*-
l 1 *.e p.
.>
It Imrslmm imorfjfstim of Xfto fy mizMo of of.ifni tate&oliloyidfe
,,-
,, . <
'
,,' . '
.1
! > r: *Mifj ,rt
tteecsgla a oen.vSf.:?uyxX- oefip in tit Xawiyj fb'bi fEjagaf;; mix***
She pnofuot of ttolsr
Iv t% Y&vy tfm soft pig"*
iMmtf with good i^rirpao cad bxoaiXEtfl fc3 .f,XX baluxvios:** 15w> diii*"
a#?srfaga Xe v.h.c> l-lf norB;Hit loos sad ca;a feu inoirf* so abispsrs-i.
i tlx aafaeafad awyarnrl*
ifhe ??B3' pcscsiS x s x b coaoloaaf la. cr*&
with a .utilisestony ncx!; ca siwd
eilXl bof aaXffl
strcrgfx ioto,, ffla .pa.scas3 oonsi.oto of a ire
agitate a S;1 pigosaf iXffff wifi mi oaalsiaxi of
asifi '!.>
.sstsa fen osier of ta:lsth.g,nol .a:
fatty mi<l) if Xfo-aSOB'M for IOO ?<dt.va.to;s,
to at tain a pigmmfb
iof. with. a mijnimizxx
acerb of a pioXoxrtly % nmfhQT* tst2;saoklofii4
no -Mith a
SM. process >a.s boon, adapted to fat Sidy Alicia la ^mipped with .ecu 100 f?Il lafbiao Orso a^iefor $ las toad cf tih dot# calxor for tfo foj.laoftxy roasenoj
1# Xfes AIM. Is aot oquXype;r! olff .a sloom lire*
2,, It ia arff.cl pried ifei; bat la cdpoo too Harpy ferr ilia fitll will be bandies. Mi oat 310>
3* Sefeetdli&g difdlmffifsi: riff. It r.sjxf eodcs msisg tf AIM*
S! featoa-XaX uic.ce l-.y tleo uif peeooee fa. the &JM,Ii@.$ not
pyesssd* bui policed dl/ostly lab tho de-yca? pea,a lb ^Bss y&m*Wt
usiyg a tbiricaaa l-.,TS?yit :ri?quloaa pf'ccaaliag la either* a af^las4
eeatob'-foosS freaf c Feoa-ifo^, Ifxo pxcscaoaf.o is act wa*aoo3 irn Ofdea
to asiam th.o fe-oafiag aryat o:: ta. pi|oa@a.t* Xf-yiags gyintllssg ass<l
testing otepa ^caouia fixe @arre Yi. testiais Eettioclo j&ow !a as fos*
both gf*g4- ax:fl (al0f-S14-Ef liooeos5 KtiXor X'vtsonfe
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gjqiiacie with toxfaa tshould suTfioo i'oe? ^outisf |a?odi*ot:i<^i*
gllfgit Bi:odifXoati.oiCi'i aas aseossajry la tlxo pyoomae* dp@diag oa ^hotjaow tits soa^oa of oolo:a 1 H-lli g;vai- rest; as shipped Hpca?% or G~M3\M"I ms-fstoBko ffova hfpaoh.Xoyltfis reoof'osad sbataboard
gs?o3a>
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fa:>om 7 to 'XOf Siti.i mat;rial tXil .rwi: p.-o'.",
&mm stftsr
ooft powdop troatso , mlosb it is oong'f clod by aoidifyig to
pH S-%, Adjustic'sg tf s pH is wtif nsoosray 'Hon X-fSO-P i@ fixed*
DUP050068159
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DUP050068160
05?-67^0 (C)
Til C" prpeooo noplaces the previous dxpsrimertal !iB" formula., It differs |m th@ :,sBft process primarily ia wiser forsmia ehEage, necessitated by operating and costing rsouireissnis.*
The change are a .follows:
1) Decrease in the initial volume in the vat from 575 gal* to 530 gal, of slurry to provide .for the inorsass in ycltms produced by condensed stosm and foam,
2) Th@ heating period has been cut back 10 minutes to 00 minutes. Otherwise the process through drying, grinding* and testing remains tbs same..
Strength of this color is currently standardised vhoro necessary by the dry addition of blaac ix however* the proposed standard Gf*.674*"Bji lot 451 contains
no added extender
CALCULATED CdiPGSXTIOIl
CPC T*?
W
"Saar
COM, YIELD
400 lbs. ss is" 400 lbs* anhydrous Moistures nil
Hefemxcei i-U8, 1336
Bxpis* 4S .10* 13* 15g 16*
SPECIAL MOTES
The above "C" process submitted by the Chemical Division has been modified by Operating* to include the addition of blonc - fisse to the. slurry rather than by
dry mfctilng, This modification .is bsing mad in order to obtain a .more realistic and lower cost as well as increase "OK Straight" performance^
ftubout result indicate the proposed standard, lot 451 is opproximtely 5#8# soak and slighUy bluer than the gcal standard, lot 430* Based on this strength difference, th amount of blaac fix ussd in step 18 has been sot .at 20#* if necessary, the quantity wi3.1 b# varied depending upon the (polity of the CPG Orson Paste, Beoent manufacture made without blanc f b-e averaged 3/5 strong versa lot 451e
CALCULATED COMPOS ITIQi'I
CPG
Blanc Fiscs
*SrSwM'
400
20 "sar
/r>f
ims.ee
GOAL IXdLD
420tf "as is"
420# anhydrous i;istu5 Mil ksfersnes: UT-674-D (C) notes
Signed K. B, VM KOOX 12/5/49 ... Approved d. H. COOPER ^ 12/S/49
a, WOUL 12/27/49*
DUP050068161