Document jyKoaEEodODDpRwyDKrZwjZMO

, -s * V V." * i V .. . .1 I; . ': ' ' `* . . " : '. ' * . -v-- y . !} ^ y <'V i :-\ i ' ; '!< f ' I . 'i '*'*..* * , t- * V* V- ' ' > . .. : / .***,. **' ' r' V *' X f. *. Y f ;v 7 %* %'V jVj. ' `A / *, . , 1 } *'*'**<* V/.:* *.y.V ` . *'* * t. i _* 1: /."-*-*"" ' ' '-RRAAWW-MMAATTEERRIIAAL CHARACTERISTICS #AN40D TTEESSTTININGG>./M** ' . 'jj 7iY.dc_fName:-..3feLfi..Slligatg..P...LgA4,,_ j^.X___Dat0. .^_ /.l/5. ._1.,,'- ::.. N 1 *o**.- -**.t^ * .^^4- 'f. r *..,..f . **,f . <-i `* 3 * < . Chemical Nam-.Si.lAP."g_9.f._Lsd______ ._______ Card No--X.-- Previous No_?-jLJL. ; i _________ _____ _______________ ^______________Composition Sub-CIass^9PQr.68fl2__- - ;:*: /' . I Usage (Name & _________ Most Similar Classified No.-------------` Gals./100lbs. Ibs./Gal.................... .........Related Nos--l8..ta. > '!V> . V'V -',.; OV#! hr;Ci:<:>v;;'-''4v-H' *:i *" . * 4 * ! Expan. Cosff. 0.000--I.,,perF Flash Pt. :fTOC) Storage Loss...... .--.Tanks..............Drums ROUTINE TESTS (Run on Eeeh Shipment) SECONQARY1ESTS (Ren Dirrerant One Each Shipment) TEST MIN. STO. MAX. MCTHOO TEST MIN. STD. MAX. METHOD irj 'M-/'; Color .* ` Texture Equal`to Std. Lead Oxide Si02 325M Res. Oil Abs. S0o k7-9% . *U7.955 01 ti5 j U-2jf lao U19.3 r*i-' .. :*. . V V . \.y. "s* > > v*v 1 y*. \' : 5% * . . ' fT-}\ ; V * ' ." i * \ . * N15815 t ** . ' . . 0 7-SWP-0048428 . , .' t' . .. i ... < ! ( v ** * ' ; ..*. * *.?*** s TV* ./ A '.* I `-X }.*. <i*, *.- . | * \ ...> .. .*:v .a "y ; & X1*.a --N^/vy ?,- ' . y..:'Vt*f.V/vy.H^:>AVY^ ' " ' .yyyA-yy- ,CF<TOC) STORAGELCKS'^^LTANKS-I-'iiri-.DRUMS ' SECONDARY TESTS (RUN DIFFERENT 0H EACH SmPKgfi? '?i. ~. MIN. STD. MAX. METHOD .TEST ttw. STD. MAX. METHOO Equal to S' d. % , 1|21^ Fbo,2 \y;V' U7.0 1*7.9 1*9.0 ; ^ . So 2,?'^M V v i . d a it .yyj '.'ly''.- 325M, Res.*' % yboi * j. . V.;-' * : * .V ' .5 - ; -: l ' rd- ' <' .*3`. ... _ "* ..'j- is- ^rd * '* "**( .. v.. ~iiV: -i- -- J . > * r" . .I<TJfc * oil yAbs/S 16;; 17.5 . Iul" lw2f. .* . . . s^. ? . W .. . . -r .. .. * 1'T '*1 ?: V ... v,,.'-: i> 5 'y'. U.3 r`= " *1 '--wff-':'?'.*-' ; - s- . *** &; . .?<: **i^. ;r . urf!'-'- loo'.%' .id 'i* ` f ' -VSii V. - * v r- , - - ".' r ' '.' .. v-.'*! .V*v:!Ci** . . ;: kX\-:A ' :< v-K.. , \'- t ';. ' v.. ' ' \ <: V;'i *, .:.> v;t,yv i ^:'kJ ' \x- v V-- :\. ` '* ' J. ; N15815.02 "; ;V V , ,, ; v * . ,* . .* r' ^/. . ; . ;* v'i...*.; J................ *../j *. I-V ; ;* *.//; *- * *,. * ' '*_ ':/ . - i v i , j 0007-SWP-0048432 * . * f ' VC..**. < - ^ ` * :' 4V-!s: v .. V v--y.` . . : / , ; -Vif *:- . :. v. / ^ NAME'OF SUPPUEf^":;--^;..: SUPPLIERS CODE NO. OR NAME , :; SAMPLE REPORT - >;4V. l***,:'vjJ ** - '-V' '* 'V-- * . ''":'X'-'' ;'' '- ,- "v;^ :/ ' "*". ". `-'r` J^V-'. ' `` * . ..r .' x*': r. .* "4 * * 'S*.# . \Vt'yV.*' National Lead Co* ; Basic Lead. Silicate, U5X - Sv 1 - * *. \ * **.**" "4 *' .}' . ' . - _< " .:r v i^ .*.it ..** _t J, .. , . ; */r . x ` -.* . ?. /*V ,, - i- ' v^:-i - : '- ;= r.\ . JT- - v, ;. '?if* ,. . V-.V' :- . *. .r*;vV;.r. *,*:.*7t*.*--fVA* ' '.iy.vV.Yy, *\-f.-i , GENERALDESCRIPTION: (SHOW CHEMICAL ANALYSIS IF AVAILABLE! *' * ~X- *- . * < ' ^ . ' ^ ' -... .* ;. /V t'v'p' . ' . -i -..I.- b>. \ y r` , * .y ; USAGE(NAME & NO.)SULK--3___GALS./100 LBS. LOSyGAL9________________ .MOST SIMILAR CLASSIFIED NO. .RELATED NOS________________,, EXPAN. COEFF.O.OOOPER F FLASH PT.____ . OFfTOCi STORAGE LOSS____:_____TANKS d r u ms ROUTINE TESTS (RUN ON EACH SHIPMENT) TEST MIN. STD. MAX. METHOD SECONDARY TESTS (RUN DIFFERENT ONE EACH SHIPMENT) TEST " MIN. STD. j u x ; METHOD Color Texture Equal. to.Std. n it PbO,* U6oO U75 sio2,* lt6o0 32$M, Bes.,* Od Oil Aba. lUoO 16 so3,% ltd lto2 It9o0 k9c0 D185 18.0 0281 lt.3 Moisture Loss . 0.20 D280 b^D:-v- . i ft.. fc&VJ:ary. j S:' - V ^ -** * \ i* V >. ' * 7* .* ' / - -* -* * f . V /; ! *t'J' ' * >. *' * . fV; ; ' .*'> V **...*:* .*4 .%**.* *'**.. * *{. ** * .>?*. * . \v\:r\' V;` r .. V ; ';* ** ,, *.*'*. *- * . I * -...i. . . * . mssis.o3 : --b*" -vS0007-swp^48434 I , / .V C \ - %*'* < .'v/. t. ./V, . * /, *.f. . \. ..t NAME OF SUPPLIER National Lead Co, SUPPLIERS CODE NO. Oft NAME SAMPLE REPO Basic Lead Silicate, U$H . f'V'.AA^v GENERAL DESCRIPTION: (SHOW CHEMICAL ANALYSIS IF AVAILABLE) card revised to show suppliers new Spec. 68 01 00 s t d . s a mpl e is s u e d a t e-^22s L--d is t r ib u t e d w .Cleveland Tech Service iv iiIM WL/ I . SPECIFICATION FOR PURCHASED MATERIAL w.,tor;ai Basic Silicate White Lead_________________ naft> 3/12/7068 01 00 General Description: Supersedes Specification Date 9/21/6kCode 68 01 00 A Mhite pigmeht designed for use in exterior paints. CHARACTERISTICS 1. Specific Gravity .2 Oil Absorption G/lOOg 3. Color h. Residue 325 Mesh % 5. Lead Monoxide (P6o) % .6 Silicon Dioxide (Si02) % 7 Sulfur Trioxide (S0^)/S .8 Moisture (Loss at 105C) % 9. Dispersability ' MIN. 3.90 Hr STD. it.00 16 MAX. ii.io 18 Equal i o Standarc U6 U7.5 0.1 U9 k6 U7.5 . h9 h is. 2 k.h Equal to Standai d 2 TEST METHOO ASTM D 153 ASTM D 281 ` ASTM D 332 ASTM D 185 Supplier's Method * Supplier's Method * or ASTM 718 Siplier's Method * ASTM D 280 ITM U21.1* * Test methods can be obJ ained fror National Lead Comps ny SPECIAL TESTS ANO/OR CHARACTERISTICS! .4 N15815.04 0007-SVff-048436 68 01 00 PRACTICAL REflUIREMENTS: The material shall remain constant in successive lots or shipments with respect to unspecified characteristics to the extent that the seller warrants that no known changes are to be made in raw materials or processing methods of this material without due notification of the buyer. . 28320 10-88 38733 RAW MATERIAL CHARACTERISTICS AND ASSIGNMENT REQUEST FORM 68-01-00 ..... .... _............... Code INTRA COMPANY CONFIDENTIAL This Side fir S-W and Affiliated Caapany Pareaantl Only TRADE NAME__!____________________________________ __. 3/12/70...... oate CHEMICAL mimf Basic Silicate White Lead 5 .Card No. 6801 Prev. Code FORMULATING PARAMETERS 3.00 Gai Cwt.@ 25 C 33*33.....Lb.-Gal. @ 25 C -"100 ----- 100 .... 100 .Wt. % NVM .Vol. % NVM .Wt. % Pig. 100 .. .Vol. % Pig. SUPPLIERS (Pfimtry) National Lead Company COOE vAiite Lead, Basic Silicate, Oncor 1j 5X OTHER CHARACTERISTICS ..................Coeff. of Exp. TOC Flash _______ Pt. F. ...................Price Lb. HANDLING Shipping Containers..-Safety Label Codes___ ________________ _ Age Limit Kone.. Protect from Freezing.____ ___ ___Protect from Moisture .... Flammable Material.TM--_____ Explosive Material--"2Hazardous Material. Xes SAFETY PRECAUTIONS AND OTHER HANDLING INFORMATION , Contains Lead. Avoid Breathing Dust. Wash hands after use USES Product Name Type or Rex......... ..Cl?----------------- ----------- ------- ----------- .--------------------------------------- ,, Line Item________________________Customer Specificationx---------------------------------._Experimental...... Reason for Assignment or Revision___To transfer to large card and assume control Similar Codes................... 680320 ____________ __Codes Which May Become Overstock Advantages Over Similar Material...._____________________ ________________________________ ..._______ Nat. Lead Test SPECIAL TESTS: #5 Lead Monoxide X126 . #6 Silicon Dioxide X127 #7 Sulfur Trioxide X128 INSTRUCTIONS 1. Fill out as completely as possible. Refer to Routine & Policy Bulletin No. 145. 2. Enumerate all tests on opposite side in consecutive order. 0007-SWP-0048437 The following test numbers are to be run routinely 3, U, 9 Tentative Reference Sample to be sent to Cleveland Tech. Service ................................. Person Requesting Assignment......... h. K. Morse ......... Laboratory Coordinator Approving H. Piel Received arid Approved in Cleveland Ry Tillinan/E. Gardiner _ 2*320 10-68 36735 Yes No x Oate 3/12/70 ? Chicago Forest | o\ Lab. Products | 00 i o h Date ----I-t----1--0-----7--0-----------------i! oo T S -W C ./S\ h b h e r w in il u a ms o CORPORATE PURCHASING OEPT. 101 PROSPECT AVE., N. W. CLEVELAND,-OHIO 44115 . FORM 11933 Sc mPECIFICATION FOR PURCHASED MATERIAL CODE. 68 01 OQ DATE 7/10/73 ^ CARD NO. ----------- SUPERSEDES SPECIFICATION DATED 3/12/70 CHEMICAL NAME AND/OR DESCRIPTION BASIC SILICATE WHITE LEAD TEST QUALITY CONTROL METHOD MININUM % J . . /^Avri j :v - i lA -i" V STANDARD MAXIMUM NORMAL QUALITY LIMITS 1, Specific Gravity 2. Oil Absorption j G/lOOg 3. Color \ 4. Residue 325 Mesh 5. Dispersability 4 Grind Clean TECHNICAL DATA 1. Lead Monoxide (PbO) % 2. "iSilicon Dioxide (Si02) % jlfur Trioxide (SO3) % 4. Moisture Loss at 105C ASIM D 153 ASTM D 281 3.90 14 4.00 16 ASTM D 332 ASIM D 185 ITM 421.4 Equal to Standard - - . - 5h JUh f Supplier's Method * 46. Supplier's Method * or ASIM D 718 46 Supplier's Method * 4 ASTM D 280 47.5 47.5 4.2 4.10 18 0.1% 49 49 4.4 2% * Test Methods can be Obtain ad fron National Lead Company NORMAL QUALITY LIMITS AND CRITICAL QUALITY LIMITS WILL PE RUN ROUTINELY iPECIAL TESTS AND/OR CHARACTERISTICS N15815.05 0007-SWP-0048438 'RACTICAL REQUIREMENTS: The material shall remain constant in successive lots or shipments with respect to unspecified characteristics o the extent that the seller warrants that no known changes are to be made in raw materials or processing methods of this material without lue notification of the buyer. \ FOAM 119SS . cooc * j 68 01 00 CARO 6 OATC . 7/10/7 FLASH FT, T.C.C. N/A -r FLASH FT. T.C.C. N/A .r SHIPPING - HANDLING - STORAGE INFORMATION LOWER CXPL. LIMIT........ u p p er c x p l . l imit FE0. STD. SIS COOES .Y VOL. N/A % ,vvot- N/A * 0 assaiHo a ^Ia r d m gp " none PPM VALUE TLV VALUE MQ/M3 LOSO SINGLE D(J3E;. MO/KG 0.2 Unavailable AGE LIMIT-MONTHS 36 PROTECT FROM 0 HEAT 0 FREEZING [3 MOISTURE (0 Lit GALS/100 LBS. If 77 *F LBS./GAL * 77F - COMPOSITION DATA NVM 1 GY WEIGHT n v m i ar v o l u me ~ 3,00 PIGMENT (OENTIFICATION 33.33 100 100 PIC-'MT COOE-6 DIGIT PIGVMT X BY WT. PIG'MT BY VI Basic Lead Silicate VEHICLE IDENTIFICATION ......... ^ ^ 68 01 00 100 100 VEH. COOE-6 DIGIT VEH. NVM % BY WT. VEH. NVM BY V N/A SOLVCNTS(S) tOENTIFlCATION ......... N/A N/A SOL.ISl COOE-6 OIOIT SOL.ISl X BY WT. N/A SOL. SI % BY VO N/A N/A N/A N/A SOILING PT. N/A F v a p o r PRES.(mm-Ho! VAPOR o e n . (AIR = 11 N/A N/A PHYSICAL DATA EVAPORATION RATE (ETHERS II (BUTYL ACETATES*; U N/A N/A PM N/A 9 MAX. (OLEFINSI MAX. % BY VOL. N/A AIR QUALITY 8 MAX. (C8 AROMATICS) MAX. X BY VOL. BRANCHED KETONCS-MAX. X BY VOL. N/A N/A TOTAL NON-COMPLYING MAX. X BY VO N/A COMPLIES TO PULE 66 YES 0 NO HEAVY METAL & WATER QUALITY DATA MATERIAL MAX. % BY MAX H2o SOL WEIGHT BY WEIGHT MATERIAL ANTIMONY Sb ARSENIC As LEAD Pb MANGANESE Mn AZIDE N3-1 MERCURY Hg BARIUM Ba NICKEL Ni CADMIUM Cd PHOSPHORUS P CHLORIDE CI-1 SELENIUM Se CHROMIUM Cr-3 SILVER Ag CHROMIUM Cr-6 SULFIOE S-2 COPPER Cu THALLIUM T-1 CYANIDE Cn-1 TIN Sn FLUORIDE F-1 ZINC Zn IRON Fe PERSON PtUutJMlNk* ASS IttNMtNT OTHER OATE MAX. % BY WEIGHT 44.1 MAX. H2o SOL BY WEIGHT MATERIAL Silicon Sulfur l a g o r a t o r y c o o r d in a t o r APPROVING MAX. % BY MAX H2o WEIGHT BY W0G 23.0 1.7 .01 .001 - l ab WILLIAM K. MORSE/dj //)/*& RECEIVED AND APPROVED IN CLEVELAND BY ' J. Tillman/ J. Woo 7/10/73 OATE 1/9/7U .--rP;^-D. GALAYEA................................... REASON TOR REVISION to Up Date Specification Ch-m. Ctc SUPPLIER _________________________________________________SUPPLIER'S CODE National Lead Company White Lead* Basic Silicate Oncor 45X 0007-SWP-0048439 . . - 'j r TECH. PROG: J0R1 .................... . The Sherwin-Williams Company coeoootATC PunooisiHa oerr i msspecrav*. aw. cuvsuvo. o hks'miis AwnitSSSSJB. ; -` PURCHASED MATERIAL. ' ? ~nno 68 oi 00 -- PATE : -.- ), A7/7Q \i .. ^HfMICAt. MAMC AMO/OK OCSCAIATtON . . ........ ... ... Basic Silicate White Lead Oncor U5X ' `t : r.: - iv rtm M'n ~ ~y ' ** * , SPECIFICATION DATED '.'TAO/H. " #'*A . SHERWIN-WILLIAMS QUALITY CONTROL ACCEPTANCE TESTS . t est " .: yam " ' : . /.j METHOD ' , * ' '* v MIKINUM * < STANDARD . . -' * .... .. '' .................. MAXIMUM ; PER CIASS CHAIRMN, A. OGURCHAK V~ NO CONSUMPTION :: ' ' : - . . ' . * - ' - : - .:**: ; .. ' * .. .. . *' '- _ ... .7 ' ; - - - '. .. * ... . .' . ' : ' - . * . .. . ' _ : ` ' o-' ' ' ` - .- ^15815.06 .. ' - . .- 0007-SWP-0048440 NORMAL QUALITY LIMITS AND CRITICAL QUALITY LIMITS WILL BE RUN;_______________________________________________________________ ________________ SPCCIM. TfSTS ANO/Oft CMAAACTCXISTtCS """ ' ' :' : '' "' . q JJ . D. L. Brenner , Chicago Chem. Ctgs. Lab . J. D. Baldwin/ J. Woo Cleveland Technical Center PRACTICAL REQUIREMENTS: The material shall remain constant in successive lots or shipments with respect to unspecified characteristics to the extent that the Sellerwarrants that no known changes are to be made in physical or chemical properties of this material without due notification in writing to the Corporate Purchasing Department of The Sherwin-WIIBams Company- o