Document jvOpmQ32a38v5yoxmNYZ6Jm2

Central Engineering Department Project Scope Report Solid Aroclor Expansion CEA 2080 New 20 M lbs./year Plant Anniston, Alabama Plant By: R. S. Yates Central Engineering Department January 14, 1969 0726018 TOWOLDMONOQ48806 DISTRIBUTION Organic Division 1. J. M. Smith 2. W. A. Kuhn 3. H. L. Williams 4. W. E. Voss Central Engineering 1. R. M. Kountz 2. R. S. Yates 3. 0. F. Bremer/P.K. Nunn 4. J. W. Campbell/B. W. Steketee/R. 5. L. R. Burchfield 6. F. J. Holzapfel 7. Central File 8. R. C. Herman 9. R. C. Herman 10. R. C. Herman 11. R. C. Herman . Degenhardt 0726019 TOWOLDMONOQ48807 CEA 2080 Date: 1/16/69 By: R. S. Yates TABLE OF CONTENTS 1.1 Project Scope Summary 1.11 Title 1.12 Synopsis and Project "Tone" 1.2 Process Technology 1.21 Process Description 1.211 1.212 1.213 Details of Process Yields and Raw Material Usage Process Documents 1.22 Raw Materials 1.221 Specifications 1.222 Sources 1.23 Products and By-Products 1.231 1.232 1.233 1.234 Quality Considerations Specifications By-Products Packaging and Shipping 1.24 Waste Streams 1.25 Personnel, Property and Public Hazards 1.3 ManufacturingFacilities 1.31 Description 1.311 General 1.312 Manufacturing Facilities 1.32 Design Capacity 1.33 Flexibility Requirements 1.34 Future Expansion 1.4 1.35 Physical Appearance 1.36 Storage and Shipping Requirements Utilities 1.41 Utilities Summary 1.42 Utilities Facilities Page No. 1 1 i 3 3 3 3 4 4 4 5 5 5 5 6 6 7 7 9 9 9 9 10 10 11 11 11 12 12 12 0726020 TOWOLDMONOQ48808 Appendices A. Equipment Information Summary D. Process Flow Diagram C. Equipment Arrangement Study D. Building and Site Requirements E. Description of Work by Code of Accounts F. Preliminary Schedule G. Project Loss Prevention Report 0726021 TOWOLDMONOQ48809 Page 1 1,1 Project Scope Summary 1.11 Title Aroclors - Increase Solid Aroclor Capacity - Organic Division at Anniston, Alabama Plant CEA 2080 1.12 Synopsis and Project "Tone" The objectives of this project are to a. Provide new facilities to increase solid Aroclor plant capacity from 9.6 M lbs./year to 29.6 M lbs./year. b. Provide an overall production capacity for solid Aroclors of up to 30% more than indicated in the latest sales forecast. c. Provide for an orderly expansion of the solid Aroclor facilities. d. Complete these facilities by December, 1969. New facilities to be added are: 1. Two batch chlorinator systems consisting of a single terphenyl feed tank, two chlorination tanks with heat removal systems and one inter mediate storage and blow tank. 2. An off-gas recovery system consisting of heat exchanger and surge tank to recover entrain ment lossss from both chlorinator systems. 3. One batch distillation system consisting of still pot, external circulating system through a gas-fired heater, condensing and receiving equipment, and a high vacuum ejector. 4. Sufficient piping tie-ins to insure good oper ating flexibility with the existing batch system. 5. Expand the existing control room to provide sufficient space for instrumentation for the new facility. 6. Expand the existing Therminol heating system to provide proper distribution of hot fluid to the new facility. 7. Add drowning facilities at the HCl plant to drown the extra HCl gas produced from the chlorinators. 0726022 TOWOLDMONOQ48810 Page 2 .8 A new elevator in Building 27. 9. A flaker for Aroclor 1268. Sales forecasts indicate that we will be out of solid Aroclor capacity in 1969. The plant is carrying out a debottlenecking program which will allow us to meet most of our 1969 requirements. The new facilities should be operational by December 1969 or earlier if possible. A preliminary schedule shows that if we can start definitive engineering in January, these new facilities will be available for start-up in December 1969. Full design capacity will not be necessary until after 1973. It is divisional policy in certain product groups to provide excess capacity over and above sales forecasts and we are providing a 31% excess capacity in these new facilities for 1973 based on the sales forecast of December 6, 1968. Low capital cost is important to this project, however, schedules must be met for a December 1969 or earlier start-up even at some increased capital cost. There are no items that could be deferred from this project to a later date. It is estimated that the cost of these new facilities will be: Capital Expense Total $ 950,000 50,000 $1,000,000 0726023 TOWOLDMON0048811 Page 3 1.2 Process Technology 1.21 Process Description 1.211 Details of Process Aroclors are the reaction products formed by the chlorination of biphenyl and/or terphenyls using an iron catalyst. The by-product HCl gas pro duced is absorbed in water to produce muriatic acid. Solid Aroclors are produced in chlorinator reaction vessels, air blown and distilled. They are drummed, flaked, or flaked and milled and packaged for shipment. Distillation residues are discarded as waste or sold as Montars. Aroclors, when used as plasticizers and that crystallize at ambient temperatures are con sidered solid Aroclors. Below is a list of the Aroclor grades that are considered solid Aroclors: Aroclor Starting Designation Raw Material Chlorination Level_____ Distilled 1268 Biphenyl 68% Yes 2565 25% Santowax C 7 5% Biphenyl 6 5% No 4065 40% Santowax R 60% Biphenyl 6 5% No 446 5 40% Santowax R 60% Biphenyl 65% Yes 5060 100% Santowax R 60% NO 5460 100% Santowax R 60% Yes 5042 100% Santowax R 42% No 5442 100% Santowax R 42% Yes We intend to make only Santowax R based Aroclors in this new equipment. 1.212 Yields and Raw Material Usage Yields are calculated for both chlorine and Santowax and/or Biphenyl. Based on cost standards of January 1, 1969 these are (% theory to standard): 0726024 TOWOLDMONOQ48812 Page 4 Aroclor On On On On Designation Chlorine Biphenyl Santowax C Santowax R 1268 73 73 2565 96 96.2 96.2 4465 73 73 73 5060 96 96 5460 82 85 5442 80.2 73 The yield on 5460 has not been demonstrated. Last year the standard yield on chlorine and Santowax R was 73.5% Lime and Ferric chloride are added to all products as follows? Lime Ferric Chloride Lbs./lOO Lbs. Aroclor 1.000 0.020 1.213 Process Documents "Standard Manufacturing Process for Aroclors Anniston Plant" September, 1966, M. J. Williams "Standard Operating Instructions for Aroclors Anniston Plant" November, 1968, M. J. Williams 1.22 Raw Materails 1.221 Specifications Raw material specifications, as listed below, are appended. Material Code Date Material 33500 2/26/57 Ferric Chloride Anhydride 83601 11/18/65 Biphenyl 82910 3/9/66 Santowax "C" 82602 3/2/66 Santowax "R" 82638 8/31/66 Chlorine Gas 38800 7/20/66 Lime Hydrate 0726025 TOWOLDMONOQ48813 Page 5 1.222 Sources Biphenyl Biphenyl is stored in horizontal tanks in the Biphenyl Area and pumped on demand into the Terphenyl Mix Tank. Ferric Chloride Received from the warehouse in 100 lb. kegs. Chlorine Received from tank cars and the chlorine plant. In 1969 the chlorine plant will be shut down and the entire supply will be from 44, 55 or 90 ton tank cars shipped into the plant. Liquid chlorine will be vaporized and trans ferred as a gas to the department area. Lime Hydrate Received from the warehouse in 50 lb. bags loaded on palettes. Santowax 11C" Received from the continuous biphenyl stills on demand through a transfer line. Santowax 11 R" Received from a 50,000 gallon storage tank, heated west of the HB40 department, on demand, through a transfer line. Santowax "R" is ob tained from the continuous Santowax still in the Biphenyl refining area. 1.23 Products and By-Products 1.231 Quality Considerations Aroclor 5460 has a color and softening point specification which because of the nature of the process gets out of control on occasion. Color is more of a problem than softening point. 1.232 Specifications Finished goods specifications, as listed below, are appended. 0726026 TOWOLDMONOQ48814 Page 6 Product Code 82616 82618 82619 82620 82622 82621 Date 3/11/66 3/11/66 3/11/66 3/11/66 3/11/66 3/15/66 Product Aroclor 1268 Aroclor 2 56 5 Aroclor 4465 Aroclor 5060 Aroclor 5460 Aroclor 5442 1.233 By-Products HCl gas is a by-product of the chlorination re action and can be absorbed in water to produce muriatic acid or sewered and neutralized with limestone. Residues from the distillation are drawn off to drums and sold as Montars or discarded. Listed below are data on the Montars. Montar No. Aroclor Softening Point Range Calcium Oxide 5 5460 6 4465 7 1268 8 5442 155-195C 135-190C 200 C 1.6% 2.0% The plant is considering the flakering of Montars in order to change the product form. Latest sales forecast, November 27, 1968, in dicates sales requirements for the solid Montars as follows for the year 1969: Montar 5 Montar 5 Montar 5 Montar 6 crushed. crushed. 180,000 dom. 400,000 inter.. 80,000 50,000 lbs lbs lbs lbs 1.234 Packaging and Shipping Material 1268 2505 4465 5060 5460 5442 Container Weights Weight - lbs. Container Form 200 ' 41 gal. fibre drum Flakes 50 and 500 50 and 500 50 and 100 5 and 40 gal. drums Solid 5, 40 and 55 gal. drums Solid paper bags Flakes 50 and 100 50 and 450 paper bags 5 and 40 gal. drums Flakes Solid 0726027 TOWOLDMONOQ48815 Page 7 1.24 Waste Streams Approximately 2200 gallons of Montar 5 will be produced daily with an approximate composition as follows: Chlorine Iron Calcium Oxide 57-59% 0.12% 1.6% Some of this material is sold, the remainder is put in drums and taken to the toxic dump. The plant has a project to pump these waste materials to Cleghorn's lake, a sump used for residue disposal. An additional 70,000 lbs. of HCl gas will be produced daily from this new plant and will have to be absorbed and sewered at the acid plant. If additional absorption capacity is required, a separate project will be sub mitted. . 1.25 Personnel, Property and Public Hazards Chlorine Gas Causes eye, skin and mucous membrane irritation. Maximum allowable concentration is 2 ppm. Concentra tions in the order of 15 ppm will cause throat irri tation. Cannister gas masks, Scott Air Paks or other similar equipment is required in strong concentra tions. Biphenyl A toxic organic chemical. Breathing fumes or vapors should be avoided. During processing the material is usually hot (100C or above) and can cause serious thermal burns in contact with the skin. Protective garments should be worn Jo aboid contact. Flash point of biphenyl is 235 F. Ferric Chloride Not toxic but presents an eye hazard. Normal pre cautions of wearing safety glasses should be followed. HCl Gas Fumes are toxic and hazardous to teeth, skin, eyes and mucuous membranes. in strong concentrations, rubber protective equipment should be worn. Maximum allowable concentration of HCl gas in air is 10 ppm. 0726028 TOWOLDMONOQ48816 Page 8 Santowax R Relatively non-toxic, however, the vapors are irritat ing to the bronchial tract. Prolonged breathing of vapors should be avoided. Material is generally, hot (150C or above) and can cause serious thermal burns in contact with the skin. Crude Aroclors Crude Aroclors are hot since all are handled in Therminol heated jacketed lines. They can cause' serious thermal burns in contact with the skin. - Still Bottoms or Residue ' Fumes from still bottoms are toxic. They are ex tremely irritating to the mucous membranes, eyes, and respiratory tract and should be avoided. They are hot (above 150C) and can cause serious thermal burns. Hydrated Lime Dust is irritating to the eyes and skin and any * material on the skin should be washed off with water. 0726029 TOWOLDMONOQ48817 Page 9 1.3 Manufacturing Facilities 1.31 Description 1.311 General The following information is included in the Appendix of this report: Equipment information Summary Process Flow Diagram Equipment Arrangement Study Building and Site Requirement Description of Work by Code of Accounts Preliminary Schedule Project Loss Prevention Report 1.312 Manufacturing Facilities A 2000 gallon mix tank for terphenyls with charge lines and supported on a 40,000 lb. hopper scale. Two 3100 gallon chlorination tanks with circulation pumps and heat removal systems consisting of two shell and tube heat exchangers and a Therminol surge tank and pump. An off-gas system consisting of heat exchanger and 2000 gallon storage tank to recover entrain ment losses from the chlorinator off gases with tailings pump. A 6500 gallon batch intermediate storage and blow tank with scrubber and transfer pump. A 7300 gallon still pot, 3500 gallon receiver with entrainment separator, still condenser and ex ternal gas fired heater with submerged centrifugal pump. A condenser control system consisting of two shell and tube heat exchangers and a Therminol surge tank and pump. A three-stage ejector with intercondenser, and aftercondenser and catch tank and sump tank. Additions to the present control room to provide space for additional instrumentation. A two-stage HCl gas drowning system. A new freight elevator for Building 27. Additions to the present Therminol system. 0726030 TOWOLDMONOQ48818 Page 10 1.32 Design Capacity Chlorination: Basis OST Rate Producing Aroclor 5060 6350 hrs./year 27.6 M lbs./year Distillation: Basis OST Rate Producing Aroclor 6350 hrs./year 20.0 M lbs./year 5460 After these additions are complete, plant capacity will be as follows: Present Capacity New Capacity Total Capacity 9.6 M lbs./year 20.0 M lbs./year 29.6 M lbs./year Basis: OST 6350 hrs./year OAY 7 3% Based on the December 6, 1968 Sales Forecast, (HD to RY) , excess capacity will be as follows: New Capacity Required Excess Capacity Excess Capacity 1970 29.6 M lbs./yr. 17.1 M lbs./yr. 12.5 M lbs./yr. 73 % 1973 29.6 M lbs./yr. 22.6 M lbs./yr. 7.0 M lbs./yr. 31 % 1.33 Flexibility Requirements Two complete and separate solid Aroclor systems will allow flexibility in our production runs. We will pro duce the larger volume requirement, Aroclor 5460 (82%) in the new units with the remaining solid Aroclors being produced in the smaller unit. Consideration will be given to incorporating the chlorinators into a continuous chlorination system at some future date. Both units will have the flexibility of being able to produce any of the solid Aroclor products. If fractionation is required to meet FDA standards, a separate distillation unit can be added to the existing system. 0726031 TOWOLDMONOQ48819 Page 10A .32 Design capacity As a supplement to the Design Capacity statements on Page 10, the following is added to show excess capacity of Aroclor 5460 only in the new facilities (based on the December 6, 1968, Sales Forecast, HD to RY): 1970 1973 New Capacity Required Excess Capacity Excess Capacity 20.0M lbs./yr. 14.1M lbs./yr. 5.9M lbs./yr. 42% 20.0M lbs./yr. 18.5M lbs./yr. 1.5M lbs./yr. 8% 0726032 TOWOLDMONOQ48820 Page 11 1,34 Future Expansion The present expansion will occupy an 18 foot wide area directly to the north of Building 27. There is suf ficient area to the north of this expansion to provide for two additional chlorination-distillation systems. In the meantime, work should proceed toward developing a continuous chlorination system which long range should provide greater flexibility in labor and equipment. 1.35 Physical Appearance We propose to make the top roof deck concrete, a contin uation of the surface we installed to the west of Build ing 27 on project OEA 4-488. Additional weather protec tion will be provided in the form of a panel enclosure on the north wall of the structure. 1.36 Storage and Shipping Requirements No additional storage facilities are contemplated. Re cently completed project CEA 1430 provided a 5500 gallon day tank for finished solid Aroclors. In addition, a new 6900 lb./hr. flaker with a 5500 gallon flaker feed tank has also been installed in a separate flaking and packaging building. Raw material storage for Santowax R and Biphenyl are adequate. 0726033 TOWOLDMONOQ48821 Page 12 1.4 Utilities and Services 1.41 Utilities Summary The approximate utility requirements are as follows: For ejector, lbs./hr. 450 For tracer and tankheating, lbs./hr. 250 Power, Installed HP 245 Cooling Tower Water, GPM 600 Potable Water, GPM 50 Natural Gas, Cu.Ft./hr. 2000 1.42 Utilities Facilities No additional utility facilities are required for this project. 0?2603<t TOWOLDMONOQ48822 V 0726035 ' 'i. r i Li' .,. V V \ *f('X ;-J TOWOLDMONOQ48823 - Monsanto Chemical Company ORGANIC CHCMtCA*.* qivivon FINISHED PRODUCT SPECIFICATION pboouct (Trade name) Biphenyl p aoouct (Cktmtal aamti Biphenyl CHEMICAL FORMULA PNOOULT COOt -M--C-T-M--O--O-tOmCMjTuITT SACK* COOt 135-000-03-09 ttp* Technical tvf* Technical IDMMfOII PECI OF 7/8/65 c12b10 | rCCIAL JO* NO. *WO* ANALT 1 l x 16 os. can f" ^ Issued 5/S/bl Anniston Plane *, By W. W. KlcNnar L Revised co add typ veluea 11-18-63 <> MOL *T. 156.20 vac Sale* * K 1 1 Characteristic* Roucina teats Appaarenca Crystallising point. *C Color, Gardner Limita White to pale yellow crystals 68.7 Min. 6 Max. General Teat (determined only on request) Biphenyl, X Napthalene, l 3 - Methylbiphenyl, % 4 - Methylbiphenyl, X Unknown, X Distillation Range, *C let drop - Dry Point Must Include 255*C Typical Values White crystals 68.0 1.3 99.9 0.001 0.05 0.02 <0.03 This specification for Internal ui< only 0726036 TOWOLDMONOQ48824 Monsanto FINISHED PRODUCT SPECIFICATION POOOuCt.O* 1AL. l . Moodv /s/ 2-1-66 . ; . Ault /s/ 2-22-66 - r >c h a. oiicir(9 t ure PNOOWCT Santouax C s'CAhV' ' " oou2t coot 1 j' ull Anniston l8u29ll.1l0oot Internal 3-9-66 7795-050-99-009 A0MNOV Alt MCACAftCM L. R. Stark // 2-3-66 - M. McEven /./ . . 1' -1 h OuAL.it y CONTROL (Chief Chemiit) 0. E. Dolln // 2-1-66 CHEMICAL , '-S7 ... . ( ric:ld information i Mrance 11 ing Point, C ho Terphenyl, 7* * ia Terphenyl, 7. i ,r i Terphenyl, 7. . rerphenyl, % i.enyl, 7, i Point, C r1 /ine, ppm . ir , ppm * ANAlTlIf 2 - 1 Pint Cana Liwr* lilvlp #y J. A. LlddLa 1-12-66 MCTHOO Brown, waxy aolid 350 Min. **10 **50 **26 **14 **0.1 **375 2.0 (Typical) 2.0 " G-l 064 064 06*. 072 064 114 ribution of iaoreera and quaterphenyla vary with operating condition. . Limited data is available; therefore, the limit* given are typical values <. ' i ) e characteristics. i roducc is mainly used aa a raw material for other finiahed products produced >r i 'on. t pecification is for internal use only. X Ri All other* Anolyted by requeii Only 0726037 TOWOLDMONOQ48825 Monsanto FINISHED PRODUCT SPECIFICATION n0OuCTI0N R. G. Moodv /a/ 1-31-66 *ue W. E. Ault />/ 2-22-66 AMOOUCT Santowax R *LAnT Anniston 3-2-66 piobuci cbbl 826.02 ihii ebbI 7795-000-11-009 vie Sale. i;r" . MillAM C H l. R. Stark /a/ 2-3-66 - M. McEwen /a/ 2-22-66 Qua lit v contmol (Chtet ChemteO 0. E. Dolin // 1-25-66 Mixed Terphenyls 2-12-62 - -.-.CTL.HH UNRESTRICTED INFORMATION (R> Appearance (R) Color (liquid), NPA (R) Upper Hold Point, #C (R) Lower Hold, C RESTRICTED INFORMATION Distillation Range, C, SOX (Uncorrected) Ortho terphenyl, X Meta terphenyl, 7. Para terphenyl, X Qua terphenyl s , 7. hm*li ror ANALvaia l x l pint cans LIMITS issuio v J. A. Llddle 1-11-66 MlT MOB Yellow white noncrystalline flaked solid 4.0 Max. 136 - 145 48 - 63 G-l 128 129 129 350 - 400 10.0 - Typical Value 54.0 - " " 27.0 - " " 9.0 - " " h k 'ut m , 4 n. !\ s,. , i It oihr ti A naty ted by te que il Only 0726038 TOWOLDMONOQ48826 Monsanto UATINIAC CODf 826.38 Chlorine Gas RAW MATERIAL SPECIFICATION Anniston 8-31-66 APPROVALS 04. 05. 27 b.low________________________________ R. G. Moody It/%. G. Moody - 8/11/66 *>OC UIIMINT H. L, Phillip, /,/H. L. PhllllDi - 8/15/66 giNim G(icmTiON L. R. Stark /s/l. R. Stark - 8/29/66 QUACITV CONTMM. fCMW C*MNM> 0. I. Dolls //D. E. Dolln - 8/10/66 CHlMCAC rOAMULA Greenish yellow gas Sept. 11, 1937 AMPCC roil ANAC V lit jGL^^aagUn^^ontaintr Cl, Mol. wt. 70.91 J. A. Llddle - 5/16/66 Typical Values UNRESTRICTED INFORMATION Material Supplied by Dlaaond Alkali Coapanv Assay, (Vol. X) Residual Gases (Vol. X) Moisture, ppa Non-volatile Matter, ppa 99.4 Min 0.5 Max. 40 Max. 40 Max. 113 113 Materlal Supplied by Depta. 56, 7 (Anniston) Assay (Vol. X) H2 (Vol. X) C02 (Vol. X) CO (Vol. X) N2 (Vol. X) 02 (Vol. X) 85.5 93.5 1.5 - 2.5 (3 Max.) 0.5 - 1.0 Nil 3.0 - 8.0 1.2 - 3.0 113 113 113 113 113 113 Aoulln* Af<*lyK, All olhtrt An*iyt4 by M#ual Anly. 0726039 TOWOLDMONOQ48827 Monsanto 38800 at. AMT Ilf* Hrdr.t* umm oion. RAW MATERIAL SPECIFICATION Ann1* Con 7-20-66 27. 26 wPPLiea Alebeator Line Co. . PRODUCTION APPROVALS AUIAACM R. G. Moody /s/R. G. Moody 6/9/66 PROCUMIMINT . P. Huall*r //. F. Hu.ll.r 7/13/66 Oualitv eoNtao*. ^CMpS CfcawdM) H. L. Phillip* /i/H. L. Phillip* 6/10/66 0. B. Delin /a/0. X. Botin 6/8/66 CHlMCAk OOtWA* White fine powder c*(0B)2 Hoi. vt. 74.10 Seot. II. 1937 C MftN ACTKRItTie UNRESTRICTED INPORMATIOW 1 lb, CAM Typie.1 iailpiU J. A. Llddl* 5/16/66 C.O (1) 73.00 MgO 01) 1.20 SlOj (I) 0.36 A1203 (X) 0.60 P203 (X) 0.30 Ignition Loot (X) C*(0B>2 (X Calcul.tod) 24.0* si.soW Screen Anelyala Through 200 aeab (l) Through 325 aeah (X) 99*8 94.5 120 Beale of Specification*: Supplier* typical enelyaie of product (5/23/66) u> C(0B)2 X - 1001 - [it0(X) + SlOj a) + AljOj a) + P203 D (HJ KnUrtt*, All ofApr* Anafrprf by **uppd mU)a 0726040 TOWOLDMONOQ48828 Monsanto OAOANIC ChIMICHI OIVtIION FINISHED PRODUCT SPECIFICATION FnoOuC T ION 1R*1.11G. Moodv /a/ 12-30-65 W. E. Ault // 3-2-66 CCNCAA. OttCNIATlOM Mixture MOOVCT ^o^lor 1268 pkooucV co "WleTlVT 11 8*2L6>.1c6wl Sales OO Ml-HMO_V_*_It___ 1040-340-04-11-16 |o**T. 127-S L. R. Surk // 3-8-66 OUALITV CONTAOk. ChtmleO 0. E. Dolin /s/ 12-29-65 CMKMICAi. rODMULA lAMAkl VO* ANAIVIII 'uo v 4-25-61________________________ 1 x 16 oz. Can or U.M. Bottle J. A. Liddle 11-30-65 UMTI MST MOO UNRESTRICTED INFORMATION (R) Appearance and color Color, Gardner White to off-white powder 6 Max. (R) Hold Point, "C 150 - 170 (R) Acid No., mg K0H 0.05 Max. RESTRICTED INFORMATION Screen Test, 7, retained on No. 16 mesh 0.1 Meat. No. 20 mesh 10 Max. Specific Gravity ca 25/25#C., Pycnometer 1.804 - 1.811 Loss <3 163C., 1 0.15 - 0.24 G-l 119 116 120 A R.iui.r. i ' n ... > n . . (. c vihin Analyzed by requett Only -------------------------------- 0726041 TOWOLDMONOQ48829 Monsanto FINISHED PRODUCT SPECIFICATION HOOUCTION WRL.CtG. Moodv /e/ 12-29-65 LwC..NCEAA.1.AOutICltAIP/IlO/H3-2-66 Mixture iurmicou c. or 61 UNRESTRICTED INFORMATION (R) Appearance end Color (R) Softening Point, *C (K) Acid No., ng KOH/g PRODUCT Aroclor 2565 prooucV 465| lWANnnPlfeVtoPnfKVlVl 826.18___ 13-11-66__________ 1040-390-04-009 APPROhViAiiAL*iicH QLU. ARLIT.YSCOtaNTrkROL// 3-8-66 Chemist) 3. E. Dolln // 12-29-65 jOPT. 127-S ut . Still__________ _____ AMPLl worn AHALVtll ISIWKO UMTS1 X 16 or. Can or W.M. gottla J. A. Liddla 11-M30T-N65p Black, brittle reeln 66 - 72 1.4 Max. G-l 115 116 'Ri Routine Analysis, A Cl others Analysed by request Only 0726042 TOWOLDMONOQ48830 Monsanto OROANIC ChCMICAl* OIVtUON FINISHED PRODUCT SPECIFICATION PRODUCTION ALII W. E. Ault // 3-2-66 CCNLAAL DCfCRtPTiOw Mixture Moover Aroclor 4465 Anniston PRODUCT CODI 626.19 MkH CODI lotFT. 127-S Sales 3-11-66 af fr oval* 1040-430-04-11-16 -009 RimiTN--------------------------------------------------------------------------- L. R. Stark /a/ 3-8-66 Oualitv CONTROL (Chlml ChemieO 0. E. Dolin /s/ 12-29-65 C MB MIC AL FORMULA iuPtRtoca *pic. op 4-25-61 CNARACTR,*T.C UNRESTRICTED INFORMATION (R) Appearance and Color (R) Color, NPA, Molten (R) Softening Point, *C Acid No., mg KOH/g AUPLI FOR ANALVDI* IDDUee DV L x 16 ot. Can or W.M. Bottle J. A. Liddle 11-30-65 UMITD MCTMOO Clear, light yellow resin 2 Max. 60 - 66 0.05 Max. G-l G-4 115 116 R ' Routim 4r.,ilysi>. 411 others Analysed by rcfuest Only 0726043 TOWOLDMONOQ48831 Monsanto FINISHED PRODUCT SPECIFICATION PHOOuCtlON W. E. Ault /./ 3-2-66 6cxc>. occirriON Mixture PKOOuCT Aroclor 5060 PtIM Annlaton " nrss&rzssr-- w.a.s 826.20 UCII coos Sales 1040-450-04-009 A*OV AC* AllfiMtH L. R. Stark // 3,-6r66 OVACITV CONTMOc (Chltf ChtmltO 0. E. Doltn // 12-29-65 C MB MIC AC FORMULA jO*T. 1 27-S iupikudu ipici, or _____ lM*b ro* iNACVtM 1 xliQZ. Canor tMI.-BotiUlJ. A, Liddle U-30-65 UNRESTRICTED INFORMATION (R) Appearance and Color (R) Softening Point, *C (R) Acid No. mg KOH/g Black, brittle reain 105 - 115 0.5 Max. C-l 115 116 othen An<iUttd by Only 0726044 TOWOLDMONOQ48832 Monsanto RROOUCT Aroclor 5460 (High Soluble Grade) ull. |oRT. I27-S FINISHED PRODUCT SPECIFICATION t-KOOUCTION Anniston 6Ic2f6r.f2s2Bi ` Sales 3-11.66 1040.480-04-009 *MOVAll MimtH-------- ------ -- -- ....... R. G. Moody /s/ 12-30-65 J.. R, SUrk /./ 3-8-66 QUALITY CONTROL {GHIll ChmmfO JL . Abucilot i^ItIiIon3:2-6fi__________ !_____________ 0. E. PolIn /./ 12-29-65________________________ hm,< Mixture 4-21-61 CHARACTER,.T.C AURIC FOR ANALTlII l x 16 ot. Can or W.M. Bottle J. A. Llddle 11-30-65 LIMIT* MCTHOO UNRESTRICTED INFORMATION (R) Appearance and Color Clear, yellow to aaber brittle resin or flakes G-l (R) Color, NPA, Molten 2 Max. G-4 (R) Softening Point, *C 98 - 105 115 (R) Solubility (25 g in 25 g. Acetone @ 25C.) 3 hour, Min. 117 Acid No., Mg KOH/gn. 0.05 Max. 116 Chlorine, X 58.5 - 60.6 093 RESTRICTED INFORMATION Hydrolysis Stability, ppx Cl 300 Max. H k-iutm, ' , i t.;hr' Anoly ted by -i-gucsi <.)nly 0726045 TOWOLDMONOQ48833 Monsanto FINISHED PRODUCT SPECIFICATION MRODon ION R. G. Moodv /a/ 12-29-65 141(1 w. 1. Ault /o/ 3-2-66 0 1 ML N 41 Dt#CWITlON Mixture MC L *T . lUl'tRICDEI 6tC. OF OUIUCTCAIIHC UNRESTRICTED INFORMATION (R) Appearance and Color (R) Color, NPA, Molten (R) Softening Point, C Acid No., mg. KOH/g enooucT WArAocVlo"r 54T"4*2* M&ftuef <mi------ |dct. 1 27-S dATnTntVisptonnrrTivi S8A2L6K.*2C1OBI SaUi_________ M3-M_ _ _ _ _ _ 1040-470-04-009-----------------------------------------Arrmov ALt KIHIWh ------------------- ---------------------------------------------------- L. R. StArk // 3-11-66 QUALITY CONTAOL (CMt ChAmttO 0. E. Dolln // 12-29-65 CHKMIC I4MFLC AO*! ANALYSIS IMuBD S v 1 x 16 o. Cn or W.M. Bottle J. A. Llddle 11-30-65____ LIMIT* MKTHOO Clear, yellow sticky resin 2 Max. 46 - 52 0.05 Max. G-l G-4 115 116 0726046 TOWOLDMONOQ48834 CTNlRAi L NO IN t I. RING DEARTMENT L QUIPMFNT INFORMATION SUMMARY ID lt UUH-MI NT mi NT IF 1. AT ION NUMflf lY J-/C/ Ol. SCRIA' T ION Of E UUIPMEN1 ITEM 77 #/**'*. sift // v OT V sue RATING MODEL. ETC / T.l X </-V - CONST R0C1 ion t SPERATCNO WEIGHT POUNDS i -- h&i E ST (MATED 1 t< .V A' y.v / - A- . /-- A /4vc / '/< rTvA/v- op /-/0/-OO/ 4l fi/e, 72r / , Affb 72* / /7So .. 7?*7* 7/1A/< /- A?/ * A"1 ? fcrA-r.K /Tt/'W '/ / j vr< hr. 7ft ' .. . . / /OHf/ziocXf'/l / Zc6 7/A XTib' HP & S/A&P- ZAP*7 -/277c'/W / At . , /-/`i /r />C/- * *=/. St>r*v' -. *. ' ! V 7TFC -V a- - /v A /./. i- At * 0726047 TOWOLDMONOQ48835 cf n 1 ttAl engineering DEdartment EQUIPMENT INFORMATION SUMMARY (. t [) f UUll'MC NT IOC NT 1 F 1C AT ION NUMflCH DC SCRIPT ION OF C QlllPMENT IT EM 7Z,.,.. rJf /+ '/.r, '/ o,, MODEL ETC CONSTRUCTION A AW; Ay' c . '/.r. - YWf'EERIGAHTTlNG POUNDS! REMARK i A /- * b X f ESTIMATED PRICE IH /-/Or ~Oc^/ , 7i-/>- //a. S*-i" / '*> , '"r 7rr< At /-/Or - /- iK o/-j /C.< / -V.V r fe.Mv.Vf. sVo-,' v/.c,, ,.r/ut. A S<9 "o/.' /Opto# ! /?, A/K 'sv/ '!> /vA/ w'/ - 6\ s/n / . 1,4 // i .. * A. . 0: a. / ,F< "" A - ./J .... 4/.'3b*s-A s - t> v / .// 7- -/ ../ h *. * G>; / A . ' ` '/ ' A ,1 HCAVICO /. . . .6 0726048 TOWOLDMONOQ48836 CfNlkAl engineering DEARTMENT rA ,rV> /* E QUIPMF NT INFORMATION SUMMARY G-j Gx'a .r /> ->r v A- 7", ` . 5-^(3 J / - * / y , A7/"/V h., Z',l- /_*> 7/;-. 'PER AT I NO WEIGH" POUNDS' -'v ' ' * - -r/ v' /.. -/ 4f /- AO/ -yV'" /*<*/"/ /9A "V v >/4 AsIf : 3rrr &//* \/a> V-i. Uh> ' A'* /* ' x 7 '/, - ' T/'-v <9/v ' - /- / ' - < V/~ <sK" /`vi'J A/ /. /AKX-V > -^v.;:A/'..4 V Avt* V /~7' js47o /K o: * .f Ar ^ ' /v,V V- - kv/a " /- /? k>.v -* v- 0726049 TOWOLDMONOQ48837 CENTRAL ENGINEERING DEPARTMENT EQUIPMENT INFORMATION SUMMARY / ^ -.r 'Vi*.' / s* ;/r 1 .1 .'{ cent qijipmc hi IOEN1 I r If ' ION numhck 'jiA/' s*ip. s<.A . /-/ -FF- 'Fa, * / /-t-e j -?ooc Sf* W >t.' a, -T-rr-f.. *Av. /<-. j3/`/CO ///? ~'i " ./si* -.- f'- |A</7 / -7- ' -/,'S ; / iff |A A..: > /-oc A/i///-if A '1 7/nK/r- /co gam /sb'p7 Putrm A// Avc 3*7''z-/o //Vf7 71^0 Si r. /- - At 2 l^f/ fW/. h,-; i-iio -oot '1o7oA. 7A - ,v' AsIP /-/// /pCKTl! '*/ :> C <jt\A F rrre 3', s/. fz/ l-/r'...1 +/'/jKMI - S'ICi <7~ to// 7vi- * - /it f - '/?' ' //,'. A ' v ,/>' A , ft/// / / / A A' 0726050 TOWOLDMONOQ48838 CInikai r Nf> i n t f ring DEPARTMENT ....... 'AT, . V. / 2- . 7 7EQUIPMENT INFORMATION SUMMARY " : 'A-r. ^ .- , i i n loyii'MtNT NUMII t fl rOUIPMFNI ITEM O' V MODE... ETC CONSTRUCTION 1PEPATINO POUNDS! HEM ARK i A s-s / i ESTIMATED i 7<r........ //..v/r. .?k'k. ' >< / /S&e*>i -A" M'*rG /Jvr c>- so A,,- A,?. <* sa. Af ' / \ - S-Ar, /-/A. -A' ' A n? Afio Ok , T/->< / . The\`n> >A/C L fix-i >' / Tr; < / 2.I& /2oo //a C/iQtfijh, ATTl \ 300 /o.'jl ''/ BlAOt' V So:> - i >7' ShVAs'tV Of'iS^rQH. <>AT'r k/f,u/t'r /S&:>4 8~ /'/13 -&,'>/ , 7#a. 4J//H l Ct> <a' />M- / 2/lp///6o rrrc // S/S /Z A'rSA -L O /-//V A A'A 'Jfttj'./****/'<;. ,'v/i ^ //V'."' Cl*,Tt\,r ,,-.S ~ / Soo e/U. C*Ki'!> -$71i 42"ax-Z/'>//f# / A2 /iv-A is *. A* 47ZJ- V/o*s r^;,. /A"j>,a ror*. .. /*tt. A- * * *>r ' ~ 9<SStP 5 h/$jy- 4 - /J' V ' - * > A\// 'A-K /V / " rfowK a' <v / *:. S''-'//*.< A A, 4 0726051 TOWOLDMONOQ48839 central engineering department tQUIPMENT INFORMATION SUMMARY '7'7. . / A, . /i a /a: 7f/Zr. roz/So l &>Osl~a. --------y 937 -i/'- l^y^A ^a-rr /- .' - - "7 'DERATING WEIGHT .POUNDS! REMARK S 9SZS .- ^ - -V,, " ~ S'#.-,: - / /-//# /- //& -< /-// / (- HA/i*.' ffijr- M. // Cftz. >/\! /tjfl fl>A)r* /t'-tfit ('a/TA. fFc /> fi Avs, I-X'. V '>/ 0 .* r, $>'.*>*? <A*. /v fv A af .A Grtn/ft'rfifl 3/C 4: /A7>r//7c.t V--f * a',- '.';V / ' //* *\/// 'rr A'.K .=7 . :" iron KCLOOTIO itKHTI OR T Cl T MATERIAL WHICHEVER II M C A VI l R toe* S/Wf a . /v> /-/ -l &vr. tor^f-T SToc |Ar* A>/TV- AV/. w *<yr A** 7P/Z rv,<-. ;-V A . -. ,/p . , A A .V A', / , ZJ .. / // / 0726052 TOWOLDMONOQ48840 CfNiHAi ENGINEERING DEPARTMENT EQUIPMENT INFORMATION SUMMARY -.11) E OUK'MfN IDIX1 II ll 10 NUMUFD / Sft. T /--'At ' A.'S> 'r. <S 'r 5>fr. !*.' ` POUNDS! \zh /-/<!.. /-122-6 1-12? Ttfcs^ni'r/ot- k At\'v *r TAa/A ^V<Ca f'v/iSr' S'iOtO* T/hfE&ttiA/ck/vMP {?; >* <r* otOO |**V/ v^V/',- '#/ l/V- 3*2-13 /, 4a& f37^rr 21>"&-A *iO/-r Ca*S;k ~ria. Jt,f2 \^7 /*">' - - rz^rif Ar AA . U /*A, Tjrrc /szir 1304r*rr- * 24 `t>/ . /y/v> rf/'r- , Y /-' - * Kyf,/ lA'i- " sp?j-*r- 0726053 TOWOLDMONOQ48841 CENTRAL ENGINEERING DEDARTMtNT EQUIPMENT INFORMATION SUMMARY r * / A- " CCl) EQUIPMENT IOENT IFIC AT ION NUMOEFt L/i. /)/. 0 *' ' DESCRIPTION OF EQUIPMENT ITEM OTV Si ZE RATING MODEL. ETC MATERIA.. OF CONSTRUCTION A/- V Aa. / <iX- ACFaI 7k r- ft /o::/ - ' /</), 1_T(/ },/ ; ' T ;".V O'-W /%roK` /)*. t-t ' / //////fo-fn* -S',-* / /S /< / - ^ / >PRATlNG WEIGHT .POUNDSI REMARKS rt/r.r j'i. // /-/ -< S estimated PRICE i 1 S' ^rrc AJ / -/if // Taa/a. / fSOO 6AL /2o*oe*/*o" ///CM &>0 A//&/*A>ft Su/l<3 - //i/ft /Vv'JA /''// . V >*> < /3y?r/ /*3 3 /#/ //>* v'r V /-nr. I-I-C- - < ff / ft-y ` /v>- V. *</ <-S'~ / /Zoof./2' ' ft? 7t'/ ra < /'. :/</ /A 3y<-fO / PlZ/fftW > TA -2'/>D x /O r- v y y-v *>' ^ >; / .'.rr ....... /-a' .* 7?/ .. /, - I lotnir: n no : : iiii'ini >. <o ii oocKiD ' * ll"U11FC H(IOH' nu(D Wl 1~ NORMAL CONftNTt 00 III' IS M| A VIEW /'/ / . . . 0726054 TOWOLDMONOQ48842 CiNlfMl L Nf.iNF [. ring DFAH T Mf N1 ( t QUlPMt NT INFORMATION SUMMARY "1 "'-.'uMiH r'" / /s' / Di sc nin <c>tj oi t qiiipmi i-n him f-j ; oi s si 7 r. RATINC.. MOOCI . ETC. MATERIAL 0< CONST RuCT ION / /rr /far * t./ /V/)7\ /.-. . * Sr eo* -- / TPERATING WEIGHT POUNhSI <? III MARKS <? > -r" / V. / % t t ST IMAT EO PRll ( i * A //fi rv^,-., - /.. S //c/)?ca: / ASoo.aa.) ^ (%a?vbA> ^rr/y. SCooa Cr/r - S0% A/ /bus r 7/u' & J/lTA -SSO rr-' ?7o V f/tfcD k//7A x 35'hihH //A7ufbi. 6S>'~ OO! $7fU. A'j S ftfA.'tT4` / {(IAr7/\`CA ........... .. - . .. -------------------------------------- -- -- ------------------------------- fa/*/ Stpf* Sy*7CA\ 4 - -------- .. ----------------------- -- A/2/ 3j//.l for At* S / /tor' /32 "as.- * 74 -A* a5/m. /0-/aor> AC/.'C 4vri Am 4W . /id s*t/ /* &770M /&% firms* nrrY A^v /ZOi!>0 cB~ tIOuHCI! N r mw * ` LS1IMA1I It ttL'Iilll f . E l1 INO H>T ! KltOOTIO NORM*l COMTCNTI ON Ttl' M*TIR(*t.. *HIC"IVER II MliVltfl 072*055 TOWOLDMONOQ48843 C'IMKAI ( NC-iNf 1 RING lif r'APHM N' /.' y . , . / [QUIPMFNT INFORMATION SUMMARY Si 2 E. HATING "A77/7. / /c ... /,, 2, 2- 7-^ . El>t (MAT t O Cr, a/. /' '' 4?W. / ' *'<? A / A/. Af"tV'i--' k l,, , M t*T ?r <LC- /> fi,. C -r/ ^ > - W k Aa .' aa//; a P> 46 7 Papa zy^./- a /-/ 8 *: ^"4 Pj(i , % 0j */4i ~ sT // . ' AX'* 7i-tV aSV/- I////V > '/a. r 4 A/?c/'* b/or> /-/A,, A- Z \n't.-\/ff- /A- ^v.-V/ Crs/Hs //t< C/\Z*>t`*S C* 42. 7*0d*/ZO%fffi\ A /26'6rf`;/ib'p&\ VotTH/i Av* /)v:3y-/o I ;62400 v/-/ " ^: |//2A. y//Jt/4/ '//> L> b>A=rr A/rnf^r 7&flaiec> W/PAi'.fyZ ? " . tvuX?s*r) /Ml rtctr* k- a ., /)/?>'' /4i\/i \Jr\pTr / PA // ; < , Ae<K #v,t. b(j") P // AC 0726056 TOWOLDMONOQ48844 I NG'Nf t klNC, m ''ARlMtNI *. . '- . tyUlPMtNT INfORMAllON SUMMARY /-/' /. -w.-.y ,'/ fYt/'> . r-. / 't.i'/- ' /C * /<V / V.C. Oy f Z0O A G>A.6t+ 'll' / /:- < tj. / Cjt. / -/*' ff-.t /) ft t t\> 3y?t)y,e. h/trn //vv* * a; fir if. a. /`MJ-r JAh AtffSJ s, f'tAj /tt//\ A l f /$ 'v/Mitr'*- Ch.Ct 'i.v Cnri ESTrMi! L U h'/z- zy>' ,, &/+// x -A set, *, /'itrtfi'i \6fir. Mo ,/ * //v ty/^itf'/)'t - yrt.: hott 7/ /' /- #<?> vrA^ /$r/.T<i \3\i>/'f,g A-' ^ U/A /*.; * * A> ficnl'/'t/ -t 3/,. <f : /` v /*/: ., 0726057 TOWOLDMONOQ48845 CENTRAL ENGINEERING DEPARTMENT EQUIPMENT INFORMATION SUMMARY ix/'/'A v..'.. . t At ".ne CCD OuiPMCnT lOENTiriCAl ION NUMBER RESCRIPT ION or EQUIPMENT ITEM OTY SUtE RATING MOOEL. ETC MATERIAL or CONSTRUCTION /- /3 7 *;; r , . e/a J S`u/\ A, - 7/iA/K / SCCD i h/\ -< .>*/ /CO. CV */36`/"* / /Z S-f 9-17-2 < / 'PER AT 1 NO WEIGHT .POUNDS) REMARKS & k % , -!-, .-V.T ESTIMATED PRICE 1 Si /-/?>& 1 /" ' 9.17; 7f/<A/CFF.A Mi*. / g. (**, rA `//rut^i. / W ucr/i.e /aca/ /-/a? THa&m'ttu- Sv/fte Thu* / 360 -V*a CtA&o* Cti. <t7`'oe*s/`'A'i - 776 C0!/~ A/ -f\ //0*T>K6 -` is/ ^/'/`--, * ** /JTA - fh/r'// ht/'..~7 /-/JO M>"ce- Cc/vf* i'rv'.tK /-/46- on/ rf(,7 ,r,, , THGA.A\IA/Cl Hu*).'-' /-/H T/i^/V'/v'A : r* ..... ........- / /CfrdPti/?'//it 3/ < /0 / 7 &#/>//*> /fM true Jew /tv . . - Stru /V W* -/*'>. ttfc /!/ , k.U / Gonocc- #.* 3///j. k' Z*\ * AI'../'- .J'" ' ,!\l IN ti. 70M ' *4 "- / 'V** V */* />..../jt r ' > r ,- - " ^ ".. v( R ,, r 072605a TOWOLDMONOQ48846 CENTRAL ENGINEERING DEPARTMENT EQUIPMENT INFORMATION SUMMARY ?0". / CCO EQUIPMENT IDENTIFICATION NUMBER /- /-^e DESCRIPTION OF EQUIPMENT ITEM S'jSCTO^ 7/1 //K P QTV Si Z E. RATING. MODEL. ETC MATERIAL OF CONSTRUCTION / TS&O </tx OtStCj 3*' Ofi4 firth >P CRATING WEIGHT .POUNDS! / REMARKS /eeo >. /l* />;t> >/r/* /S' /-/< " / tX, ESTIMATED PRICE i jt /- /F'.9 /-/43-OOI /fo/D/t / Ti/Cv/tro*!. / -/, fie * JTfiofi , /Z*r/r/t*, fb "<* r ` ssb" 4yv#a ^l/c 7yi-r / Soff/fonafr/i 1-/44 /-/4S /-/4C, /-/47 SaevftgrK /%*/*// Sec'**:./.* A. +"J'\ A^TS.'/v/<> / .`tMu/'V jTa. / Soa.1 % Ha foycsTt* fe' S(/'*, -,~./*r / 4g\ 24' -Vfr *>. , . r/r/ t,' /,, T , / .*>'< -4 /'*uyJ'~ >Tr- *> ^.v> TJrrc <- s* -V ,4 V 4/' *..' ____________1 0726059 TOWOLDMONOQ48847 CENTRAL ENGINEERING DEARTMENT EQUIPMENT INFORMATION SUMMARY "o rv rv r. / CED EQUIPMENT IDENTIFICATION NUMBER /-V e DESCRIPTION OF EQUIPMENT ITEM tftTA/7irK / SIZE. RATING MODEL ETC MATERIAL OF CONSTRUCTION /-/-6 / OPERATING WEIGHT .POUNDS' REMARKS /3 0, ^ h X s P1RSIC' E >Y Z-/4-9 7/Tf/CrV9/i/ . nSl/A / /?~ 7/tA/K / /-/So 7#iea; As'i/f/r * / V&Or/c/u. Ca/7/C;,-L'6s*`- /-/SO-0O/ f&ro/il > 7/td.'*t //V;5 ft*//* / /9<po OiAie' f, St.It . 2400'- A/.'v.'/V! a .,r' 4/ d%6**,A/f~ t///*TV '(**$*? tv/A*.1*/' /rwr fiswtr teo <so/-t //$' rt>/i 7a/Cut Momy Z>uJY OH'tSw 5m- y 5b>////smSi 7irrc V /-/."/ /3C ft /`/A'A. -r/. Z-/SI-/- / / Z4"Of- * So9 5'V <9$ " z.r/y M /tiv . " r / S/YZ//il> //>/ rrn V V X, . e.-yt /' 0 726060 TOWOLDMONOQ48848 CENTRAL ENGINEERING DEPARTMENT "^sy^je * EQUIPMENT INFORMATION SUMMARY -to o / ICDEEONTENIUQFMIUCIBPAEMTRIEONNT EOQESUCIPRMIPETNITONITOEFM QTY SIZMEO.DREALT, INETGC, CMOANTSETRRIUACLTOIOFN /- &SS 7 .)PPWOEEULINGAOHTSITNI G REMARKS `/S /S' "/-27-g? aK ESTIMATED PRICE * /- *S2 /VA<K. /> 7**/*; / 3000 CiAj. 9b -V a /&S~ W* S/ici- ZB 4oc> A/th So Asa; 1TACAOT /~OK S/SC^A.IA/CL -V A/npry /*//>-" /-/SB //S3.00I /-/S'3. 002 //3M> 3 /vtje/iiz e/z Sioro/Z, / 0'Z3NS1tK*o C*#Go*/ tSrseA. /bLU****** &oco + / /oz/fi//Sk>X/H /)/& CoHs/Ef, 4/* /br*Aft ?r xM 'a Z(/4'`4^6A Xt?OW &Z&1. An ConvEy//vf yer / *J*m fatiOov SrrtTL I-/SH- a /sy.oo/ /-/Air /-/s'S.ooj /- /AA A/ A ? 2)vsT fiu-CTc$, / CoA/rfoys, 2>o&r fi>ut7x>f< / / rfa/tAi, /Siowe* / / 7%ro<-. &//; / fatvK'YOfi. / J/3S3-4-30 M//fM U^ool. TjfaF ft/Sbire (MCE) StAKF* Oh/Mr tot/ ME>/4 tfior //to*/ yis/p/zfocAf/i #SS S/frA^o //ter /feo/j ^//p/s-fjo^pri 24 "w'>/r * SpATAPe/A Stt/ry AjczsxT V /ZeoiBs rrrt #\ /&? 4 /Vo 23// /V C/v/r /k A 4k *2>/t tMf/r *//ry Mr*t#r 7oo s V // %/a.Y S^ct, /V Sferv V$/4i/H v 7trrc /t /<ri*~r // 4/ rrrc 4/ jr ntg <Toa//A*Vf . V ' A 0726061 TOWOLDMONOQ48849 fon/fuiA SfQL HrsS**rewAx '/f' C*H,, esc-9 fa/ttc Cmo*- /SC4 Cm&A/A/f Ck. HZ. 9 70-? At* 0t S&6C ///*****.> Cmo* /* 4CJ zt-o z-o 3-J~ 4** 4/mX 74-/ s+co /itXTAK S' hHt<y,, S74-6 74/J./A/6S *-"a/oA 6m /at 1 /r /&* A* GM- ZfA* Z/seos/rr- Cfi 7k* C Jkess<j*M-4m / 11900 2, at" 3 4 S' 4 7 6 ` : 9 /o // ~ /2 //Zoo //zoo /s /S /s ~7s 32400 20 SO 3SCO 3*0 7000 ADO /OO 200 j1 ZSfOC 324oo 2S 3300 3SX> \ /OO /OO j_ _ _ 1 zs9t I742S 94SSO esc I74ZS 231 94S 946 ?4S 94S ?4S //too ~77~ 9tr `2/tO sSoS\ tiff* 42/00 2C/4S MO SMM 2/1?s 26/6i /3SO fi- /4SO 2/60 /4SO 2/6t 1 /oo /oo _ _ J100*00 33/0*0 -muo /2S zso /z-r zso /oofoo 33/0*0 /zs ZSO /ZS zso B-4 /o 94 U&, /?./ 8-4 mr* 7T7 /-O /OO 26 m /z 2-6 /z /40 /oo /to /s~ \2fO 2SO /to 'S zso zso / / / |7ftF\/-3S /-3S / / /3S\ /.3S / 0726062 TOWOLDMONOQ48850 TOWOLDMON0048851 <$>-* 1 I (0) *nu.far HarCK 1 "Ti (^24) 4tx Agw* %>/* &** Ssrtft GfLO*#/*raA. tret* 0**46* S**ro*4x (^> &SO 2000 * J00O * */rr Total. <S> (4> AGO /GO ?0O o-so /2 oo *4s fart.# SnuCrrj* totaeSrui (#> 0 /k*r i/A Oar/u. CstprY @> g> -2 8 / Total /2- 0726064 TOWOLDMONOQ48852 t&JUWL* **tch/#x . #xs. to,Qoo, COO * 37,900 *3S/3Knc# * C*e&*t*/S3*toU*3 * t&fOXXS V*e-**0 oso zoo 9-SO /oo /2-00HA3 8 Ht*9 ftWH. * Mr* esr fr* tfwi/tvra_____g&mn e^r*Ai *tMilx/vt Semxrnrur SrAw, '****#/ Ok*aahc 7/v /s/ox I Aw/^rc/v Aavt Antca fjtd bt*2i t/brs/un^Snarsw. Jj^jg A*oc<g* &f*s/s* OxsrtnAr/onj ~s?-- isrrXS*Tt3 t-v-A 2060 c V2 8 0726065 TOWOLDMONOQ48853 N *g>g-- 5CAW1. I" * I o`-0" 0726066 TOWOLDMON0048854 . eutr J ---f <+) Cf <Wr *v Jfc //f * *** fiHOUMD LEVEL. scale f"-. MMumww c*eloo sdAJ. r.io'-"'' (S w J> ob<d**** * 0726067 TOWOLDMONOQ48855 (F Tbikp Le.vt.i- 0726068 TOWOLDMONOQ48856 If 3 i/Jjfrf Jmt*Vm c/fjr- */v*6ik g*int*e*T AfcRAwttrf^T 5TUB/ SOU* **Q&rt>Kb(T#**0*J C.e^-u>to sofc* 'o'-o" I3h fk*4 i *f a. 0726069 TOWOLDMONOQ48857 Appendix D Building and Site Requirement A. Building Size Number of Floors - Three (includes ground and roof level) Area per floor - 1500 sq/ft. Bay Size - 20' X 18' - 2 required - 30' X 18' - 1 required - 12' X 18' - 1 required B. Type of Construction 1. structure - Open steel structure. Roof to be reinforced concrete. North wall to be enclosed with Monsanto Lustra span panels or equal. Second level floor to be grating. Finish on steel to be coating standard No. 502 or equal. One stair at the east end of the structure. 2. Rooms Control room ceiling will be acoustical tile. Control room floor will be terrazzo to conform to existing floor. Walls will be painted concrete block. 3. Personnel Service Facilities None required. 4. Elevators A freight elevator for moving bags of lime and rework to the operating floor is required. Capacity - 5000 lbs. Only one floor is served. 5. Heating and Ventilating None required. C. Electrical There are no flammable materials handled in the immediate oper ating area. Classification is water resistant. Normal grounding requirements. Lighting requirements - Allow sufficient lighting for opera tions at the ground, operating and roof level. 0726070 TOWOLDMONOQ48858 Provide two welding receptacles at each operating level, six required. Provide two small tool outlet receptacles at each operating level, six required. D. Maintenance Provisions The coil in the furnace, Item 1-128, has to be accessible for repair. The submerged pump. Item 1-134, in the still pot, Item 1-129, must be installed so that it is readily removable. E. Drainage No spacial materials are required for drainage. Drainage ditches will be constructed in the ground level concrete pad and a curb installed around three sides of the entire pad. F. Communications None required. G. Safety No safety showers or eye wash fountains are required. No explosion barricades are required. No blow out panels are required. H. Fire Protection No sprinkler systems are required. No fire wall, fire hose stations, fire alarms, or foam systems are required. No building steel fireproofing is required. I. Walks and Roads None required. J. Railroads None required. K. Parking Lots None required. L. Fences None required. M. Dock Facilities . 0726071 None required. TOWOLDMONOQ48859 N. Facilities to be Relocated The control room will be expanded and the existing chlorinator panel will be relocated into this new control room addition. O. Grading and Excavation The area to the north of Building 27 is a filled area and good soil is available at 12 to 15 feet from the surface. P. Site Covering Rock covering in the areas around the site location. 0726072 TOWOLDMONOQ48860 Appendix E Solid Aroclor Expansion Scope of Work 01 Equipment See Equipment Information Summary 02 Instrument Items See Instrument List and Summary 03 Setting and Testing Equipment Area accessible for truck and train unloading. High lift can be used to set larger units. The new elevator will be in stalled in Building 27. 04 Setting and Testing Instruments An addition to the present control room will be required to make space available for setting instruments. The new addi tion will be 20 ft. X 30 ft. 05 Piling None required. 06 Excavation For operating floor 100 ft. X 22 ft. X 1 ft. 2200 cu.ft. For elevator pit 360 cu.ft. 6 ft. X 10 ft. X 6 ft. For structural piers 7700 cu.ft. Mfg. Area 7 piers X 8 ft. X 8 ft. X 12 ft. = 5400 = 5400 Control Room 3 piers X 8 ft. X 8 ft. X 12 ft. = 2300 Backfill required 5000 cu.ft. Remove spoil - Sheet piling may be required for fehoring. 0726073 TOWOLDMONOQ48861 07 - Foundations For Structural Steel 10 pads X 6 ft. square X 1.2 deep with 12 ft. column 1.5 ft. square 700 cu.ft. Floor Slab - Reinforced Concrete 1100 cu.ft. 24 ft. X 90 ft. X 6" thick Equipment Pads 120 cu.ft. 10 items X 6" Thick X 6 ft. X 4 ft. Concrete Basin Within Floor Slab for drainage 450 cu.ft. 2 ft. wide X 1-1/2 ft. deep X 6" thick X 90 ft. long, 2 required Supports, platforms and Structures Equipment Supports 55 tons Grating Requirement 2000 sq.ft. Handrails 400 ft. Toeplate 400 ft. Wise. Structural Supports 8 tons Stair Requirement One complete stairway for two levels Control Room Building Frame Control Room Floor 30 ft. X 20 ft, X 6" thick 09 - Other Building Items Floor Covering for control Room 30 ft. X 20 ft. terrazzo to conform to existing floor Acoustical Ceiling for Control Room windows for control Room - Four Units 5 ft. X 4 ft. Doors for Control Room - Two Hollow Steel Units 3 ft. X 7 ft. 10 tons 300 cu.ft. 600 sq.ft. 600 sq.ft, 0726074 TOWOLDMON0048862 10 - Sprinklers None required. 11 - Piping Item Service Material Size 1-101 Sant R C.S. 2" X3" Biphenyl c.s. 2" Vent c.s. 3" X4" To It.103 Misc. c.s. c.s. 3 " X4 " 3" X4" Misc. c.s. 2"X3" Misc. c.s. 2"X3'' Therm.Ret. Steam Cond. c.s. c.s. c.s. 1" 1>5" 1" Rmks. Jacketed Traced Jacketed Length 75 ft. 75 ft. 35 ft. Jacketed Jacketed Hose Jacketed Hose Jacketed Hose - - 30 ft. 2 ft. 2 ft. 2 ft. 50 ft. 40 ft. 40 ft. Insul. Valves 1" 2 - Jctd. 1" 2 - CD3 1" 1 - Jctd. Vent l'1 1 - Jctd, -- - -- i" 3 - FA37 i" i" - 1-103 Chlor. Charge c.s. 3"X4" Jacketed 100 ft. 1*5" 1 - Jctd, 1-104 Relief c.s. 2" Relief c.s. 3" Chlorine c.s. 3" To It. 105 c.s. 3" X4" Jkt. S.. S.Inner Traced - Jacketed 50 ft. 50 ft. 60 ft. 30 ft. - 1 _ CA46 -- 4 - DE41I 2" i Jctd 1-105 To It. C,,S. Jkt. 3" X4" 106 S., S.Inner To It. 125 C.S. 3"X4" Sample C.S. 2"X3" Jacketed 50 ft. Jacketed 25 ft. Jacketed 30 ft. 1-106 To It. C.,S. J)ct. 3"X4" 104 S.,S.Inner To It. 116 c.s. 4" Jacketed - 25 ft. 25 ft. 2" 2 - Jctd 2" 1 - Jctd 2" 1 - Jctd 2" - No 2 _ FA42 072607S TOWOLDMONOQ48863 Item Service Material Size Rmks. Length insul. Valves 1-107 To It. 108 C.S. 4" 2 tracers 50 ft. 1*5" 1 - CA46 CO o To HCl Line 4" 2 tracers 50 ft. iy 2 - CA46 To It. 109 C.S. 4" 2 tracers 30 ft. 1*5" 1 - CA46 1-108 To It. 113 To It. 109 Drain C.S. C.S. C.S. 1-109 Vent Relief 200 psig steam In. Cond. Out TO It. 110 C.S. C.S. C.S. C.S. C.S. 3" - 20 ft. 1" 4" 2 tracers 15 ft. 1*5" i" - 20 ft. 2"X3" Jacketed 2" 1" - 25 ft. 25 ft. 50 ft. i" - 50 ft. 2" X3" Jacketed 30 ft. 1*5" 1*5" 1*5" 2" - 1 - FA4 2 1 _ Jctd. - 2 - FA37 2 - FA37 1 - Jctd, 1-110 To It. 101 C.S. 1-111 Vent Therm.In Therm.Out To It. 112 C.S. C.S. C.S. C.S. 2"X3" Jacketed 70 ft. 2" 2" _ 20 ft. 1*5" - 40 ft. 1*5" 1*5" - 40 ft. 1*5" 3" - 25 ft. 1" 2 - Jctd, _ 2 - FA37 2 - FA37 1 - FA42 1-112 TO It. 108 1-113 To It. Ill C.S. 3" C.S. 3" - 50 ft. 1" 1 - FA42 - 50 ft. 1" - 1-117 Relief Relief Chlorine To It.118 C.S. 2" Traced C.S. 3" - C.S. 3" - C.S. Jkt.3"X4" S.S.Inner ~ 50 ft. 50 ft. 100 ft. 30 ft. _ 2" i - CA46 - 4 - DE41I* 1 - Jctd, 0726076 TOWOLDMONOQ48864 Item Service Material Size Rmks. 1-118 To It. 119 C.S.Jkt. 3" X4" Jacketed S.S.Inner To It. 123 C.S. 3"X4" Jacketed Sample C.S. 2"X3" Jacketed Lenqth 50 ft. 25 ft. 30 ft. Insul. Valves. 2" 2 - Jctd 2" 1 - Jctd 2" 1 - Jctd 1-119 To It. C.,S. Jdt. 117 S.,S.Inner To It. 123 C.S. 3"X4" Jacketed 4" - 25 ft. 25 ft. 1-120 To It. 108 To HC1 Line C.S. C.S. 4" 2 Tracers 50 ft. 4" 2 Tracers 50 ft. 1-121 Vent To It. 122 Steam In Steam Out C.S. C.S. C.S. C.S. 4" . ' _ 4" Traced 14" 14" - 30 ft. 30 ft. 50 ft. 50 ft. 1-122 To It. 119 To It. 123 C.S. C.S. 4" 4" Traced 70 ft. Traced 30 ft. 1-123 To It. 121 TW in TW Out C.S. C.S. C.S. 4" Traced 40 ft. 6" ,3' - 50 ft. 6" ,3'` - 50 ft. 2" No 2 - FA42 14- i _ CA46 14" 2 CA46 _- No 2 - FA42 i" i" - NO 3 . FA4 2 No 1 " FA4 2 No 1 _ FA42 - 1 - EA46 - 1 - EA46 1-114 Vent C.S. 4" _ 30 ft. to It. 115 C.S. 4" Traced 30 ft. Steam In C.S. 14- - 50 ft. Steam in C.S. i4" 50 ft. 1-115 To It. 106 To It. 116 C.S. C.S. 4" 4" Traced Traced 70 ft. 30 ft. -- No 2 _ FA42 1" 1" No 3 . FA4 2 No i - FA4 2 0726077 TOWOLDMON0048865 Item Service 1-116 To It. 114 TW In TW Out Material C.S. C.S. C.S. Size 4" 6",3" 6" 3" Rinks. Traced " Length Insul. Valves 40 ft. No 1 - FA42 50 ft. 50 ft. - - 1 - EA46 1 - EA46 1-124 To It. 125 C.S. 2" - 60 ft. - - 1-125 Steam In C.S. 1*5" _ 60 ft. 2 2 - FA37 Steam Out C.S. 1*5" - 60 ft. 2 2 - FA37 Vent Saran Lined Steel 6" Traced 50 ft. NO " To It. 126 C.S. 3 " X4 " Jacketed 30 ft. 2 2 - Jctd. 1-126 To It. 129 1-127 Vent Drain 1-128 To It. 129 Gas In C.S. 3" X4" Jacketed 75 ft. 2 2 - Jctd. P.E. Saran Lined Steel 6" 3" _ 50 ft. _ 50 ft. _ C.S. 3 " X4" Jacketed 30 ft. 2" 2 - Jctd. C.S. 1*5" - 50 ft. - 2 - CD3 1-129 To It. 130 C.S. 18" -- 2" - To It. 134 C.S. 3" X4" Jacketed 40 ft. 2" 2 - Jctd. 1-130 To It. C.S. 16" - 30 ft. 2" - 131 To It. 129 C.S. 2"X3" Jacketed 10 ft. 2" Site Glass To It. 141 C.S. 2" - 30 ft. 1-131 To It. C.S. 3"X4" Jacketed 20 ft. 2" 2 - Jctd. 132 Site Glass To It. 141 C.S. 2" _ 40 ft. - 2 - FA37 0726078 TOWOLDMONOQ48866 Item Service Material 1-132 Vent C.S. Relief C.S. To It. 135 C.S. To It. 133 C.S. Steam In C.S. Steam Out C.S. Size Rmks 3"X4" Jacketed 4" - 3" X4" Jacketed 3 " X4 " Jacketed 1*8" - 1*5" - Length 30 ft. 30 ft. 40 ft. 30 ft. 60 ft. 60 ft. Insul. 2" 2" 2" 2" 2" Valves 1 - Jctd. 2 - Jctd. 2 - Jctd. 2 - FA37 2 - FA37 1-133 To It. 137 1-134 To It. 128 - 3" X4" Jacketed 110 ft. 2" 2 - Jctd, 3"X4" Jacketed 40 ft. 2" 2 - Jctd, 1-135 To It. 136 Steam In Steam Out Water In Water Out - " 3 " X4 " Jacketed 30 ft. 2" 2 - Jctd, 1" - 30 ft. 1" - 1" - 50 ft. 1" - 1" - 50 ft. 1" - 1" - 50 ft. 1" - 1-136 Steam In C.S. Water In C.S. Water Out C.S. Aftercond. Water Out C.S. Intercond. Vent C.S. 2" 2" 2" 2- 3" _ 30 ft. 1*5" - - 30 ft. - - - 40 ft. " - - 40 ft. " - 20 ft. " 1-139 Steam In C.S. 1*5" _ 50 ft. _ _ Steam Out C.S. 1*5" - 50 ft. - - Vent C.S. 3" - 20 ft. - - To It. 140 C.S. 2" - 30 ft. 1" 2 - FA42 1-140 To It. 131 1-141 TO It. 139 C.S. C.S. 2" 2" - 70 ft. - 2 - FA42 - 50 ft. 1" - 0726079 TOWOLDMONOQ48867 Item Service Material Misc. Therm 14 Conn. In C.S. Therm 14 Conn. Out C.S. Therm C.S. Size 1*3" iv 6" Rmks. - Length Insul. Valves 500 ft. l*s" 30 - FA37 ' 500 ft. l*s" 30 - FA37 - 500 ft. - 4 - FA37 12 - Ductwork A 6 ft. x 6 ft. cabinet will be required for housing drums for draw-off of residue product for still pot. 13 - Electrical Motors to be installed and wired: Number Horsepower 12 55 1 7H 2 10 3 15 2 20 1 25 1 30 1 50 Allow for remote pushbuttons and alarms for 10 motors. Lighting required in operating area: Ground Area# Operating Area# Roof Area# 18 ft. X 82 ft. 18 ft. x 82 ft. 18 ft. X 82 ft. 1476 ft2 1476 ft2 1476 ft2 14 - Site Preparation None required. 15 - Sewers 1. 50 ft. of 4" permanite sewer pipe with one tie-in to exist ing 8" sewer which runs west of Building 27. 2. 150 ft. of 304 s.S. guttering around the top of the new structure with 3-4" downspouts# each 30 ft. long 0726080 TOWOLDMONOQ48868 16 - Underground Mains None required. 17 - Yards. Roads and Fencing None required. 18 - Railroads None required. 19 - Insulation Piping - Refer to Code 11 Equipment - As below - material Standard #100 Weatherproof, Std. #65 Item 1-101 1-104 1-107 1-109 1-111 1-117 1-120 1-125 1-129 1-130 1-132 1-139 10 Pumps Area 250 ft2 200 ft2 50 ft2 250 ft2 80 ft2 200 ft2 50 ft2 550 ft2 550 ft2 150 ft2 350 ft2 80 ft2 Thickness 2" 2" i" 2" 1*S" 2" 1" 2" 4" 3" 2" ih2" Painting Coating Standard #502,, Epoxy System. All uninsulated piping, air, water, gas. Supports for Items 106, 113, 116, 119, 123, 128, 141, 142, 132, 135. 0726081 TOWOLDMONOQ48869 21 - Walls, lasonry, Roofs and Roofing Concrete roof deck for mfg. area - reinforced concrete, 20 ft. X 90 ft. X 5" thick Concrete roof for control room - reinforced concrete, 20 ft. X 35 ft. X 5" thick Concrete wall for control room - concrete block, 3 walls, total feet - 70 ft. X 15 ft. high Concrete enclosure for elevator - concrete block, 4 walls, total feet - 30 ft. X 25 ft. high Built up 4-ply roof for control room, 20 ft. X 35 ft. North wall of mfg. structure will have Monsanto Lustra Span panels for a distance of 80 ft. and height of 12 ft. in each level. 90 - Pismantlinq 1. North wall of Building 27, approximately 1500 sq. ft. of brick wall. 2. South wall of present control room, 450 sq.ft, of concrete block wall. 3. Shed to south of present control room, approximately 600 sq.ft, of transite roof and steel platforms inside shed. 4. Biphenyl heater on Still No. 1. This is a unit heater in the shed. 92 - Repairs Expense 750 cu.ft. 290 cu.ft. 1050 sq.ft. 750 sq.ft. 700 sq.ft. 1920 sq.ft. Replace existing head on Item 535. This is a 2000 gallon vessel and requires a new 78" O.D. carbon steel head. 93 - Relocation and Modification Expense 1. Remove and relocate Item 205, a 14' dia. X 10' high storage tank with coil and agitator. 2. Remove and relocate stairway to the north of Building 27. 3. Remove and relocate 10 ton stand-up tube air-conditioner which is now in the south section of the control room. 4. Remove and relocate a 20 ft. chlorinator panel from its existing position in the present control room to the new control room. 5. Remove the present 1268 flaker (24" X 48" unit) and replace with a new unit. This unit will be relocated to an area just east of the present flaker. 0726082 TOWOLDMONOQ48870 APPENDIX E - Amendment No, 1 Scope of Work - CEA 2080 07 - Foundations For Elevator Pit (Reinforced Concrete) 150 cu. ft Supports, Platforms and Structures Equipment Support For Item 152 6 tons Grating Requirement For Item 152 225 sq. ft Handrails 60 ft. Toeplate 60 ft. Stair Requirement One Stairway For One Level 11 - Piping Item 1-152 Service Material Size Charge C.S. 3"X4" Charge C.S. 2" X3 " Therminol C.S. Vent C.S. 1*5" 3"X4" Overflow C.S. 3"X4" Outlet C.S. 2"X3" Rmks. Length Insul. Valves Jacketed 125 Ft. 2" 1 - Jctd Jacketed 125 Ft. 2" 1 - Jctd - 200 Ft. 1*5" Jacketed 30 Ft. - 2 - FA5 - Jacketed 30 Ft. 1*5" - Jacketed 50 Ft. 1*5" 1 - Jctd 12 - Ductwork A 6 ft. x 8 ft. X 10 ft. hopper will be required under the new flaker. 13 - Electrical Use PVC coated conduit. 19 - Insulation Item 1-152 Area 320 ft2 Thickness 2" 90 - Dismantling ,2 A section of floor in Building 27 - Area 400 ft for 1268 flaker. 0726083 TOWOLDMONOQ48871 92 - Repairs Expense 5. Repair or replace section of floor at new 1268 flaker. 93 - Relocation and Modification Expense Remove Item (5) from original scope and replace with the following: 5. Relocate 18" I beam to south of control room. This beam is 40 ft. long and will be moved south approximately one foot. 6. Relocate 2 - 6" IPS tower water lines to south of control room - Total feet = 100. 7. Relocate miscellaneous 2" IPS pipe to south of control room - Total feet = 100. 0726084 TOWOLDMONOQ48872 APPENDIX E - Amendment No. 2 Scope of Work - CEA 2080 This amendment describes the work required to install a power pulverizer to grind flakes of Aroclor 1268. It includes a mill, conveying duct to dust collector, air lock to discharge material into fiber containers and a dust collector with blower. Instruments will be required at the dust collector. 03 - Setting and Testing Equipment Pulverizer will be located under the flaker unit. The dust collector and pulverizer will be located on support steel. 08 - Supports, Platforms and Structures Miscellaneous equipment supports, light steel 1 Ton 12 - Ductwork Install 75 feet of 6 and 8" duct for blower and pulverizer. 11 - Piping Install 100 feet of 1*5" IPS piping to filter for air. 13 - Electrical Motors to be installed and wired: Number Horsepower 1 10 15 1 Conduit run to dust collector controls. 20 - Painting Support steel with Std. #502 Epoxy System. 0726085 TOWOLDMONOQ48873 APPENDIX E - Amendment No, 3 Scope of Work - CEA 2080 Spares A pump, indentical to Item 1-134, is to be purchased and held as a spare in the storeroom. Item 1-134 is a special submerged pump, critical to the operation of the Aroclor plant, and is required to prevent losses due to pump failures. Size TDH Make 200 GPM 100 Feet Taber Heavy Duty 0726086 TOWOLDMON0048874 APPENDIX E - Amendment-No. 4 Scope of Work - CEA 2080 07 - Foundations For access to elevator 1 ft wide x 4 ft high x 40 ft 160 cu ft Retaining wall at west end of manufacturing area 1 ft wide x 2 ft high x 25 ft 50 cu ft Floor slab for elevator access 8 ft wide x 6" thick x 25 ft 100 cu ft 11 - piping 300 ft of 2" IPS 200 lb steam line, insulated 13 - Electrical Lighting for Control Room area 20 ft x 30 ft 600 ft2 15 - Sewers Add 25 ft of 4" permanite to existing 6" sewer in the HCl area. 90 - Dismantling Remove existing elevator after new elevator is installed. Dismantle 10 foundations in ground to north of Building 27: Size: 4.5 ft x 13.5 ft x 1.25 ft thick Dismantle 500 gallon jacketed tank with agitator at present 1268 flaker. 07260&7 TOWOLDMONOQ48875 93 - Relocation and Modification Expense 8. Relocate telephone lines to north of Building 27. 9. Relocate 100 ft of 2" IPS nitrogen line to north of Building 27. 10. Relocate 50 ft of 2" process lines from new pipe bridge to north of Building 27--two lines. 11. Relocate steam tracers and trap discharge to new condensate pig. 12. Relocate 3" IPS gas line in control room area - 30 ft. 13. Relocate 4" cast iron vent from toilet. 14. Relocate stove, sink, refrigerator and water cooler into new control room. 15. Relocate stairway to third level of Building 27 to ejector operating level. 16. Relocate No. 3 Blower to No. 4 Still Blower Tank. 17. Add 20 ft of 10 inch duct to existing tar blow stack. 18. Relocate and modify stairway outside of Building 27 at NE corner which will interfere with elevator. 0726088 TOWOLDMONOQ48876 TOWOLDMONOQ48877 TOWOLDMONOQ48878 Monsanto <pM nmi 6 locationi General Offices - St. Louis January 24, 1969 Project Loss Prevention Report 69-7 CEA 2080 "O : Mr. R. S. Yates cc R. E. Howard G. 0. Hunt P. K. Ward - Anniston S&PP Project File S&PP Location File COPIES TO THOSE PRESENT R. J. Green W. B. Howard R. M. Kountz W. E. Voss - Anniston R. S. Yates DATE AND PLACE OF MEETING Missouri. January 23, 1969, Creve Coeur, CEA 2080 Alabama. Expand Solid Arochlors, Anniston Plant, Anniston, This project is increasing the plant capacity for manufacture of solid arochlors from 9.6 to 29.6M ppy. The project capital is approximately $1.03M. Completion target is December 15, 1969. PERSONNEL 1. Chlorinated Biphenyl Content of Product An overall project objective is to minimize chlorinated biphenyl content in the solid arochlor 5460. This is needed for FDA approval of the material, since it is used in hot- melt adhesives in food packaging. It is also used in plasticizers. 2. Elevator It is planned to install an elevator to handle both freight and passengers. The elevator will have the capacity for 5000 pounds and will likely be hydraulically operated. It was agreed that the project manager will review the elevator design and safety con trols with Mr. George Gorbell. 3. Lime Addition Lime is added to the still pot from 50 pound bags. This size bag is considered safe for personnel handling. A, 07Z4091 TOWOLDMONOQ48879 R. S. Yates 2 January 24, 1969 MECHANICAL An external gas-fired heater is used for the still pot. Combustion safeguards are planned by the project; these will include a Honeywell protecto-glow unit. There will also be a pilot interlock. The combustion safeguards should be reviewed with Mr. George Ostroot when the heater design is further along. In addition, some process safety provisions will be incorporated in the heater. A high temperature sensing unit on the process material coming out of the furnace will shut down the burner on high temperature. If the circulation through the heater stops, an alarm will sound. Standard instrumentation will be employed for these functions. PROCESS1 1. Alarms and Interlocks The operation of the chlorinators will be sequence controlled. Chlorination starts at a temperature of about 150C. As the batch progresses the sequence controller steps the temperature upward so that, at the conclusion of chlorination of a batch, the tempera ture is in the range of 250-255C. The temperature will be recorded in the chlorinator; an alarm will be actuated at high temperature. It was agreed that the project will consider use of a differential temperature alarm, based on the desired temperature at any stage of the batch, rather than a high temperature alarm which must function at a temperature higher than the maximum batch temperature. It was believed that this type of alarming would be a better investment of money than the addition of a second high temperature alarm on the reactor, and located in the vapor discharge from the reactor. There will also be temperature detection in the arochlor circulating line on the chlorinator. A high temperature in this line will give an alarm and will also close the chlorine supply valve. The complete closure of the chlorine supply valve will not be possible because chlorine will come from tank cars rather than from the chlorine unit. If flow should cease in the arochlor circulating line there will be an alarm and the chlorine valve will be closed. There will also be an alarm if the therminol circulation should stop. V/-V v/j/ i' 0726092 TOWOLDMONOQ48880 R. S. Yates 3 January 24, 1969 Other alarms include the following: a scale alarm to prevent overcharge of the weigh tank: a low temperature alarm on the chlorinator at 120C; water coolant to the therminol cooler to prevent too low a water temperature; a signal when the batch is 0(W chlorinated in order to signal the time to initiate sampling; high (80C) and low (60C) temperature on the circulating therminol. The project is also considering installation of a nuclear instrument on the process circulating line at the chlorinator to determine density; it is hoped that this density figure can be correlated with softening point. If the correlation works out on a present plant test, the equipment will be installed. 2. Operating Time The operating time of the present unit is only about 74%. Downtime on a chlorine plant has been a part of the problem; the new purchased chlorine arrange ment should help this. Another part of the problem has been maintenance. It is also hoped that this can be im proved in order to improve the on-stream factor. 3. HC1 Scrubber In order to minimize the HC1 venting to the atmosphere the project will add equipment for improved HC1 absorption and scrubbing. 4. Gas Fired Heater Operation The firing rate on the heater is manually indexed on a flow controller on the gas to the burner. This type of control has proved adequate with the present plant installation and is believed to be adequate for the new heater. The project will also try to design the heater coils in such a manner as to simplify coil re moval for the furnace. The furnace coils can be expected to burn out approximately annually. This is considered a normal maintenance item and presents no major problems. 5. Residue Removal If the residue is removed from the system in the manner used at present, the fume hood venting provisions will be improved over those at present. The project also plans to try to develop a system for flaking the residue. BUILDING AND FIRE PROTECTION An 181 x 90' x 2 level bay will be erected adjacent to the north wall of Building No. 27. The construction will be open steel frame with reinforced fiber glass polyester wind-breaks, concrete slab roof and steel grate flooring at the first level above ground level. Hydrant #13 with hose house and hydrant #19 with attached monitor nozzle are adequate fire protection. No sprinklers or fire proofing are needed. 0726093 TOWOLDMONOQ48881 R. S. Yates 4 January 24, 1969 A 20' x 30' extension to the existing control room will be erected at the 16 ft. level. The construction will be con crete block walls and non-combustible roof. No fire protection is needed. LOSS EXPOSURE The maximum probable loss was considered to come from loss of the heater for the still pot as a result of explosion in the fire box. It was considered that approximately six days will be required to re-brick and repair the heater. A spare coil will be kept in stock. It was estimated that the repairs would cost about $10M. Six days were estimated to be sufficient for the repairs. The business interruption loss during this period of time would be approximately $45M. LOSS PREVENTION REVIEW CHECK LIST Attached to R. S. Yates' copy of this report is a copy of Form G-1425, Loss Prevention Review Check List, which can be used as a safety check list for this project. LOSS PREVENTION REVIEW BY PLANT The S&PP Branch of CED can not review design prints and construction steps in detail as this project progresses. S&PP requests plant personnel, in cluding plant safety personnel, to hold additional safety reviews at the plant, to follow the development of design prints, and to check the progress of construction in order to make maximum contributions from their experience with these operations to the CED personnel involved in execution of this project. SAFETY MANAGER G. O. Hunt will be Safety Manager for this project. Please contact him for additional safety reviews needed during design. d h.,' -s. .... R. J. Green bjr Attachment :; /'! ' /- ... W. B. Howard 1 /. 0726094 TOWOLDMONOQ48882