Document jm45pLB9ddmVZBnVa3kvQG8nO
STL Burlington Colchester, Vermont
Extended Data Package
SDG: 117522
Case Narrative Chain of C ustody........................................................................................................ Sample Report Summary - G eotechnical............................................................. Supportive Documentation - G eotechnical.......................................................... Sample Handling......................................................................................................... Last Page of this Document......................................................................................
1 2 12 34 39 43
Case Narrative
i
SEVERN
TRENT
STL
November 30, 2006
Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380
STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446
Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com
Re: Laboratory Project No. 26000 Case: 26000: SPG: 117522
Dear Mr. Young:
Enclosed are the analytical results for the samples that were received by STL Burlington on October 18th, 2006. Laboratory identification numbers were assigned, and designated as follows:
Lab ID
Client Sample ID
Sample Date
Sample Matrix
Received: 10/18/06 ETR No: 117522
691475 691476 691477 691478 691479 691480 691481 691481 DP 691482 691483 691484 691485 691486 691487 691488 691489 691490 691491 691492 691493 691494
DBCF01IPF0010041021 D B C F 0 1 IP F 0 0 2 0 0 4 1 021 D B C F 0 1 IP F 0 0 3 0 0 4 1 021 D B C F0 1IP W 0010041021 DBCF01IPW0020041021 DBCF01IPW0030041021 DOUF01IPF0010041021 DOUF01IPF0010REP D O U F 0 1 IP F 0 0 2 0 0 4 1 021 DOUF01IPF0030041021 D O U F 0 1 IP F 0 0 4 0 0 4 1 021 DOLIF01IPF0050041021 DOUF01IPW0010041021 DOUF01IPW0020041021 DL2F01MSW0010041021 D L 2 F 0 1 M S W 0 0 2 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 3 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 4 0 0 4 1 021 D L 2 F 0 1 M S W 0 0 5 0 0 4 1 021 DBCF01MSW0010041104 DBCF01MSW 0020041104
10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/21/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 10/22/04 11/04/04 11/04/04
TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE
Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal.
Leaders in E nvironm ental Testing
1.1
Severn Trent Laboratories, Inc.
STL
November 30, 2006 Mr. Charlie Young Page 2 of 2
In order to accommodate field length limitations in processing the data summary forms, the laboratory did, in certain instances, abbreviate the sample identifiers. Dashes have been removed from the client identifiers in this delivery group. The electronically formatted data provides the full sample identifier.
Lipids: There were no exceptions to the method quality control criteria during the analyses of these samples.
The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature.
If there are any questions regarding this submittal, please contact me at 802 655-1203.
C i n / 'r t "/-11/
Ron Pentkowski Project Manager
Enclosure
1.2
Chain of Custody
2
COPY - O W N A L f* * '
SOG *
f 2 S ^ 7
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAM PLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3117 Research Drive
State College, PA 16801
PAGE 3 o f S
PROJECT INFORMATION Client: W eston S o lu tio n s , Inc.
1400 W eston W ay, B ldg. 5-2 W est Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Ja i K esari email: .k e s a ri@ w e s to n s o lu tio n s .c o m
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
M 5E m s
S a m p le r:
Charles Young
P.O. #: Q uotation #:
I
SAMPLE ANALYSIS
ExyLIMS #
C lien t S am ple Ide ntificatio n
DL3 F01 IPF002
D L 3 F01 IPF003
041021 041021
DBC F01 IPF001
041021
DBC F01 IPF0Q2
041021
DBC F01 IPF003
041021
DBC F01 IPW001
041021
DBC F01 IPW 002
041021
DBC F01 IPW 003
041021
DOU F01 IPF001
041021
DOU F01 IPF002
041021
Collection Date
21 -O ct-04 21 -O ct-04 21 -O ct-04 2 1 -O ct-0 4 21 -Oct-04 21 -Oct-04 21 -Oct-04 21-O c t-0 4 2 1 -O c t-0 4 21 -O ct-04
Collection
Time 23:00 23:10 23:25 22:30 23:30 22:35 22:35 22:40 23:00 23:20
CHAIN OF CUSTODY
Cooler ID No.: li*- f
Rei in gu jstje d
Date Tim e
Received By:
10/22/04 12:00
Fed Ex
Cc
zOo. o3co
Sam ple Matrix Tissue T is s u e T is s u e T is s u e Tissue Tissue T is s u e T is s iie T is s u e T is s u e
C o ole r Tem p. (C):
Date T im e 10/22/04 12:00
t/i i A* JXI-
Com m ents
PROJECT REQUIREMENTS Results Deadline: Laboratory Report Options:
Sample Results Only Add Case Narrative Add Quality Control Summa'Y Add Calibration Summary Add RavO Data Other:
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3117 Research Drive
State College, PA 16801
PAGE 4 o f 4
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project M anage r: Jal Kesari em ;ail: i.kesariOwestonsolutlons.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
S a m p le r:
Charles Young
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sam|pie Identification | DOU F01 IPF003 0 041021 DOU F01 IPF004 0 041021 DOU FOT IPF005 0 041021 DOU F01 IPW001 0 041021 DOU F01 IPW 002 0 041021 DL2 F01 MS W O01 0 041021 DL2 FOT MSW002 0 041021 DL2 FOT MSW 003 0 041021 DL2 F01 MSW04 0 041021 DL2 F01 M SW 004 0 041021
Collection Date
2 1 -O c t-0 4 21 -O ct-0 4 22-Oct-04 22 -O c t-0 4 2 2 -O ct-0 4 22-Oct-04 22 -O c t-0 4 22-Oct-04 22-Oct-04 22-Oct-04
Collection
Time 23:35 23:45 0:00 0:05 0:10 0:20 0:25 0:25 0:30 0:35
X X X X X X X X X X
Sample
Matrix 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUS1rODY
Cooler ID No.:
Retinquisij^itBy^
Date Time
Received By:
10/22/04 12:00
Fed Ex
L.
Cooler Temp. (C):
Date Time 10/22/04 12:00
/f/j i/>z/a6
Grab Sample Composite No. of Containers
PFOA
Comments
X
X
X
X
X
X
X
X
X
X
PROJECT REQUIREMENTS
.O
Results Deadline:
Laboratory Report Options:
Sample Results Only
Add Case Narrative
Add Quality Control Summary
Add Calibration Summary
Add Raw Data
O th e r:
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T. 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE _1_ of _6
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project M anager: Jai Kesari e m itil: i.kesari@westonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
S a m p le r:
Charles Young
P.O. #: Quotation #:
Grab Sample Composite No. of Containers
Percent Lipids (STL)*
SAMPLE ANALYSIS
ExyLIMS #
Collection
Client Samipie Identification | | Date DBC F01 M S W 0 0 1 0 041104 4-NOV-Q4 DBC F01 M SW 002 0 041104 4-N ov-04 DBC F01 M SW 003 0 041104 4-N ov-04 DBC F01 M SW 004 0 041104 4-N ov-04 DBC F01 M SW 005 0 041104 4-N ov-04 DBC F01 MSF001 0 041104 4-N ov-04 DBC F01 M SF002 0 041104 4-N ov-04 DBC F01 IPF004 0 041104 4-N ov-04 DBC F01 IPF005 0 041104 4-N ov-04 DBC F01 IPW 004 0 041104 4-N ov-04
Collection
Time 19:15 19:20 19:23 19:25 19:27 19:40 19:45 20:00 20:05 20:00
X X X X X X X X X X
Sample
Matrix 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUSTODY
Cooler ID No.:
Cooler Temp. (C):
^--'Rellnqulshed/By:
Date Time
b /r/o * rfoo
... / / /
-- ^ ----------
Received By:
Date Time
FedEx
/ r -------r . .------
//eo
* Subsam ple o f m acerated tissue to be sent to STL for Percent Lipid analyses________
Comments
< O u_ 0. XX XX
XX XX XX
XX XX XX
XX XX
PROJECT REQUIREMENTS
Results Deadline: Laboratory Report Options:
__ S am ple R esults O nly __ Add Case N arrative __ Add Q uality C ontrol S um m ary
Add Calibration Sum m ary
__ Add Raw Data Other:
:|
3058 Research Drive State College, PA 16801
Phone: 814-272-1039 Fax: 814-231-1580
Loain
Login Group: L0003679
Login #: Project:
Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*:
3789 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 10/25/2004
10/23/2004
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
False True True True
* Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Am merman, Mark
Spread Sample:
Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program /
ROUTINE
Login Notes: Conform Notes:
Identification on the chain (DL2-F01-MSW004-0-041021) does not match the identification on the container (DL2-F01-MSW005-0041021). As per Charles Young, use the identification on the container (DL2-F01-MSW005-0-041021). MSA 10/25/04
Packaae PK0004480
Carton
Date / Condition
Packages / Containers
ShiDDer/ ID
Received Date: 10/25/04 10:45 Package & Contents Uncompromised
FEDEX 8479 6714 4761
TemD. Control/TemD.
Dry Ice
0 .0
Direction / Handled Bv
RECEIVED Ammerman, Mark
Container # C0048126 C0048127 C0048128 C0048129 C0048130 C0048131 C0048132 C0048133 C0048134 C0048135 C0048136 C0048137 C0048138 C0048139 C0048140 C0048141 C0048142 C0048143
Gross W eiaht 177.60 g 153.40 g 244.60 g 197.10 g 691.20 g 614.50 g 44.40 g 23.30 g 582.30 g 288.40 g 415.00 g 283.80 g 525.00 g 824.30 g 111.60g 150.50 g 87.70 g 174.60 g
E
Container TvDe 1 gallon zlploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
10/17/2006 I nnin rrt
Report Version: Oct 12 2006 9:14AM
D ona 4
C
6
Instance:
R0291646 Iiiiiiiii illmumilmumumumulimili
Login
Login Group: L0003679
Login #: Project:
Company Name: Submitted By:
3789 P0000760
Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
False True True True
Login Type:
Immediate Receipt of Samples
Started:
True
Date Start:
10/25/2004
Due Date:
Login Initiated*: 10/23/2004
Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Ammerman, Mark
Spread Sample:
Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program /
ROUTINE
Login Notes: Conform Notes:
Identification on the chain (DL2-F01-MSW004-0-041021) does not match the identification on the container (DL2-F01-MSW005-0041021). As per Charles Young, use the identification on the container (DL2-F01-MSW005-0-041021). MSA 10/25/04
Packaae PK0004480
Carton
Date / Condition
Packages / Containers
ShiDDer/ ID
Received Date: 10/25/04 10:45 Package & Contents Uncompromised
FEDEX 8479 6714 4761
TemD. Control/Temo.
Dry Ice 0.0
Direction / Handled Bv
RECEIVED Ammerman, Mark
Container# C0048144 C0048145 C0048146 C0048147 C0048148 C0048149 C0048150 C0048151 C0048152 C0048153 C0048154 C0048155 C0048156 C0048157 C0048158 C0048159 C0048160 C0048161 C0048162 C0048163 C0048164 C0048165
Gross Weiaht 257.40 g 203.50 g 221.40 g 380.30 g 228.70 g 198.30 g 140.10 g 613.40 g 429.60 g 417.10 g 372.90 g 263.60 g 301.40 g 263.30 g 177.80 g 730.50 g 1,256.60 g 113.40 g 105.20 g 55.30 g 53.70 g 52.70 g
dH
Container TvDe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfg, ID
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Paae 2 of 5
7
Instance:
R0291646
IIIIIIMIIIIIIM lllllllllllilll
Login
SamDle ID L0003679-0001
Container C0048126
Matrix SOLID
L0003679-0002
C0048127
SOLID
L0003679-0003
C0048128
SOLID
L0003679-0004
C0048129
SOLID
L0003679-0005
C0048130
SOLID
L0003679-0006
C0048131
SOLID
L0003679-0007
C0048132
SOLID
L0003679-0008
C0048133
SOLID
L0003679-0009
C0048134
SOLID
L0003679-0010
C0048135
SOLID
L0003679-0011
SOLID
C0048136
OOS Investigation #: OOS-04-071
L0003679-0012
C0048137
SOLID
L0003679-0013
C0048138
SOLID
L0003679-0014
C0048139
SOLID
L0003679-0015
C0048140
SOLID
L0003679-0016
C0048141
SOLID
Fraction Fish
Samples
Sample DL3-F01-IPF001 -0-041021
Fish DL3-F01-IPF002-0-041021
Fish DMC-F01-IPF001-0-041021
Fish DMC-F01-IPF002-0-041021
Fish DMC-F01-IPW001 -0-041021
Fish DMC-F01-IPW002-0-041021
Fish DMC-F01-MSW001 -0-041021
Fish DMC-F01-MSW002-0-041021
Fish DL2-F01-IPF001-0-041021
Fish DL2-F01-IPF002-0-041021
Fish DL2-F01-IPF003-0-041021
Fish DL2-F01-IPF004-0-041021
Fish DL2-F01-IPF005-0-041021
Fish DL2-F01-IPW001 -0-41021
Fish DL2-F01-MSF001-0-041021
Fish DL2-F01-MS F002-0-041021
1$ if ' -t
rHT'r i*
$6 c
g /'
<_ j
,0
la
in
|
.*
ta. <rg O 5
ss
Date SamDled 10/21/2004
Date Due
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/22/2004
10/25/2004
10/22/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 3 of 5
8
Instance:
R0291646
R0291646
L0003679-0017
C0048142
SOLID
L0003679-0018
C0048143
SOLID
L0003679-0019
C0048144
SOLID
L0003679-0020
C0048145
SOLID
L0003679-0021
C0048146
SOLID
L0003679-0022
C0048147
SOLID
L0003679-0023
C0048148
SOLID
L0003679-0024
C0048149
SOLID
L0003679-0025
C0048150
SOLID
L0003679-0026
C0048151
SOLID
L0003679-0027
C0048152
SOLID
L0003679-0028
C0048153
SOLID
L0003679-0029
C0048154
SOLID
L0003679-0030
C0048155
SOLID
L0003679-0031
C0048156
SOLID
L0003679-0032
C0048157
SOLID
L0003679-0033
C0048158
SOLID
L0003679-0034
10/17/2006 Login.rpt
SOLID
Login
Fish DL2-F01-MSF003-0-041021 Fish DL2-F01-MSF004-0-041021 Fish DL1-F01-IPF001 -0-041021 Fish DL3-F01-IPF003-0-041021 Fish DL3-F01-IPF004-0-041021 Fish DL3-F01-IPF005-0-041021 Fish DBC-F01-IPF001-0-041021 Fish DBC-F01-IPF002-0-041021 Fish DBC-F01-IPF003-0-041021 Fish DBC-F01-IPW001-0-041021 Fish DBC-F01-IPW002-0-041021 Fish DBC-F01-IPW003-0-041021 Fish DOU-F01-IPF001-0-041021 Fish DOU-F01-IPF002-0-041021 Fish DOU-F01-IPF003-0-041021 Fish DOU-F01-IPF004-0-041021 Fish DOU-F01 -I PF005-0-041021 Fish DOU-F01-I PW001-0-041021
Report Version: Oct 12 2006 9:14AM Page 4 of 5
9
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/21/2004
10/25/2004
10/22/2004
10/25/2004
10/22/2004
10/25/2004
Instance:
R0291646
R0291646
C0048159
L0003679-0035
C0048160
SOLID
L0003679-0036
C0048161
SOLID
L0003679-0037
C0048162
SOLID
L0003679-0038
C0048163
SOLID
L0003679-0039
C0048164
SOLID
L0003679-0040
C0048165
SOLID
Login
Fish DOU-F01-IPW002-0-041021 Fish DL2-F01-MSW001 -0-041021 Fish DL2-F01-MSW002-0-041021 Fish DL2-F01-MSW003-0-041021 Fish DL2-F01-MSW004-0-041021 Fish DL2-F01-MSW005-0-041021
10/22/2004 10/22/2004 10/22/2004 10/22/2004 10/22/2004 10/22/2004
10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004 10/25/2004
Login Reviewed By: ____________________________________________ Date/Time:
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 5 of 5
10
Instance:
R0291646
R0291646
SamDle ID L0003772-0001
Container C0049450
Matrix SOLID
L0003772-0002
C0049451
SOLID
L0003772-0003
C0049452
SOLID
L0003772-0004
C0049453
SOLID
L0003772-0005
C0049454
SOLID
L0003772-0006
C0049455
SOLID
L0003772-0007
C0049456
SOLID
L0003772-0008
C0049457
SOLID
L0003772-0009
C0049458
SOLID
L0003772-0010
C0049459
SOLID
L0003772-0011
C0049460
SOLID
L0003772-0012
C0049461
SOLID
L0003772-0013
C0049462
SOLID
L0003772-0014
C0049463
SOLID
L0003772-0015
C0049464
SOLID
L0003772-0016
C0049465
SOLID
L0003772-0017
10/17/2006
I n n in rn t
SOLID
Login
Fraction Fish
Samples
SamDle DBC-F01 -MSW001-0-041104
Fish DBC-F01-MSW002-0-041104
Fish DBC-F01-MSW003-0-041104
Fish DBC-F01-MSW004-0-041104
Fish DBC-F01-MSW005-0-041104
Fish DBC-F01-MSF001 -0-041104
Fish DBC-F01-MSF002-0-041104
Fish DBC-F01-IPF004-0-041104
Fish DBC-F01-IPF005-0-041104
Fish DBC-F01-IPW004-0-041104
Fish DBC-F01-IPW005-0-041104
Fish DOU-F01-IPW003-0-041104
Fish DOU-F01-IPW004-0-041104
Fish DOU-F01-IPW005-0-041104
Fish DL2-F01-IPW002-0-041104
Fish DL1-F01-MSW001-0-041104
Fish DL1-F01-MSW002-0-041104
Report Version: O ct 12 2006 9:14AM
P o n o A r.f 7
11
Date SamDled 11/04/2004
Date Due
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
11/04/2004
11/08/2004
Instance:
R0291811 IinillllIIIlllll HillHillHillHillMillllllINI
Sample Report Summary - Geotechnical
12
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691475 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
5.9
Printed on: 11/20/06 08:11 AM
13
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691476 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
4.9
Printed on: 11/20/06 08:11 AM
14
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPF0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691477 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Quai.
1 0.1
6.9
Printed on: 11/20/06 08:11 AM
15
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691478 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
9.5
Qual.
Printed on: 11/20/06 08:11 AM
16
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPW0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691479 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
4.1
Qual.
Printed on: 11/20/06 08:12 AM
17
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01IPW0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691480 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
3.6
Qual.
Printed on: 11/20/06 08:12 AM
18
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPF0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691481 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Quai.
1 0.1
0.4
Printed on: 11/20/06 08:12 AM
19
GEOTECHNICAL / GENERAL CHEMISTRY
Duplicate Sample Report Summary
Client Sample No. DOUF01IPF001OREP
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691481DP Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
Sample Result Cone. Qual.
0.4
Duplicate Sample Result
Cone. Qual.
0.4
RPD*
0
* Control Limit for RPD is + /- 20%, unless otherwise specified.
Printed on: 11/20/06 08:12 AM
20
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPF0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691482 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
1.8
Qual.
Printed on: 11/20/06 08:12 AM
21
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPF0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691483 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
3.8
Printed on: 11/20/06 08:12 AM
22
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPF0040041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691484 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
5.5
Printed on: 11/20/06 08:12 AM
23
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPF0050041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691485 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
0.3
Qual.
Printed on: 11/20/06 08:12 AM
24
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691486 Date Received : 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
1.9
Qual.
Printed on: 11/20/06 08:12 AM
25
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DOUF01IPW0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691487 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL 1 0.1
Cone. 1.0
Quai.
Printed on: 11/20/06 08:12 AM
26
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSW0010041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691488 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
1.4
Qual.
Printed on: 11/20/06 08:12 AM
27
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSW0020041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691489 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
1.3
Printed on: 11/20/06 08:12 AM
28
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSW0030041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691490 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
0.4
Qual.
Printed on: 11/20/06 08:12 AM
29
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSW0040041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691491 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
1.3
Printed on: 11/20/06 08:12 AM
30
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL2F01MSW0050041021
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691492 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
0.5
Printed on: 11/20/06 08:12 AM
31
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSW0010041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691493 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL Cone. Qual.
1 0.1
1.2
Printed on: 11/20/06 08:12 AM
32
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DBCF01MSW0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117522 Lab Sample ID: 691494 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/17/06
Units %
DF RL
1 0.1
Cone.
1.3
Qual.
Printed on: 11/20/06 08:12 AM
33
Supportive Documentation - Geotechnical
34
ST LS E V E R N
TRENT
PERCENT LIPIDS
35
Percent Lipids Calculations
D ate: Tim e:
11/17/2006 2200
A nalyst: E T R (s):
C lien t:
TPB 117507,117522
WESTN2
Sam ple ID
MB111706E 691404 691475 691476 691477 691478 691479 691480 691481 691482 691483 691484 691485 691486 691487 691488 691489 691490 691491 691492 691493 691494
691481DP
Sam ple
W eight
(g )
10.00 3.00 10.02 10.02 10.00 10.04 10.02 10.03 10.04 10.04 10.01 10.03 10.00 10.01 10.03 10.03 10.01 10.02 10.02 9.97 10.01 10.00 10.01
D ish ( D ish/R esidue
g)
1.0121 1.0083 0.9996 0.9966 0.9765 1.0164 1.0377 1.0373 1.0452 1.0456 1.0187 1.0432 1.0209 1.0010 1.0106 1.0343 1.0435 1.0170 0.9804 0.9957 1.0384 1.0332 1.0447
(g )
1.0118 1.0160 1.0592 1.0454 1.0454 1.1122 1.0788 1.0737 1.0490 1.0640 1.0569 1.0986 1.0239 1.0204 1.0203 1.0480 1.0567 1.0206 0.9930 1.0007 1.0501 1.0463 1.0492
Extract Final
V olum e
(m Ls)
10 3 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
A liquot U sed in
D eterm ination
( mLs )
1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
% Lipids
<0.1 0.8 5.9 4.9 6.9 9.5 4.1 3.6 0.4 1.8 3.8 5.5 0.3 1.9 1.0 1.4 1.3 0.4 1.3 0.5 1.2 1.3 0.4 #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117507117522MB111706E
36
11/20/2006
Percent Lipids Calculations
N-
CO
Date: Time:
11/17/06 2200
Analyst: ETR(s):
Client:
TPB
C V
117507,117522
WESTN2
Sample
Extract Final
Weight Dish ( Dish/Residue
Volume
Sample ID ( g )
g)
( g 6 (mLs)
MB111706E 10.00
Oi'L\
1 gii<g
10
691404 691475 691476 691477 691478 691479 691480
3.00 10.02 10.02 10.00 10.04 10.02 10.03
Tom
0.W 6
(3
O-flCfi l'lbtf 1 0 377
.>$7 3
T o IGo
f-0 > 7 2 _ 1-045*7
/04S*f
>/ ( Z .o lii
T7/?7//7T~^" iThk
10 10 10 10 10 10
691481
10.04
t.n^TO
10
< 691482 691483 691484 691485
10.04 [oH5l ' 0 0 10.01 l o t i n i - 0 5 > c 10.03 o n b
10.00 / -oZ ( f\ f . o i y 7
10 10 10 10
691486 691487 691488
10.01 (0010 i - i H 10.03 \ , o l o & i ' O Z O
10.03 \ m w
10
10 10
691489
10.01
lo h V i
10
691490 691491 691492
10.02 T W f o {CTL0&
10.02 V - W o H 0 79? <3 9.97 o - n s n l - o OO 7
10 10 10
691493
10.01 o l i H ( 1
10
691494 691481DP
10.00
10.01 l o u n n
fs
1. 7 3 /. o t i 2 ,
10 10 10
) (Lw m f
10 T 10
Aliquot Used in ------------- \
Determination
( mLs )
% Lipids
1 1 1 1 1 1 1 1 1 1 .1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117507117522MB111706E
37
\ l i / i 'V 706
STL BURLINGTON
8
\&4 CT'
3
-c. X -O
"9
V
r- P S' C
-S)- 'i > J ) X
-5
C^S' ^ -S
;3
03
"- - ' ^ ^ - C ' <r-C V ^ -C, -C - -C
-O <5y
c^STL Sample ID
rn
^7
S f)
XK>
< T ) Bottle ID
f t p p j j j ^ r ^ ~ > ^ . S ^ ^ ej, p 5 ,0 p>^J<5
AO. o< &n0 'J'RVmC AX xcK. 5- 5i. p_-\ ^D C^S tb. 'O'-t O pOp COoOO ^ o O ^ ^ Weigh 10gm sample into a 250ml wide
- O-^
r r~ r 'x ` " ' O mouth Jar
O
>D m .o. O> dm
HHDwZ
m TJO m H
? pi
S?8 5~ * -\ooc ' " "vJ 6*
-J A -o TnI vT\ P p*
P1
" ^ A d d 10gm N a2 S 0 4
Add 60m ls C H 2C L 2
U
^r O
CL
fc r
' ' T is s u e m iz e 3 m in.
.0*
^ i D e c a n t thru a N a 2 S 0 4 fun nel into a K -D set3 up
^ R e p e a t 2(X)
5-> ^H 5-?S ' C o n e , extract to 10ml
- J`-- ^
.......... - -......... - - ..........................
^ Filter extract thru a 0 .4 5 u m filter
_ 3ull 1.0m l for % Lipids. S e e % Lipids ^"C alcu lation s sheet.
Zmco 7mC^c-<o
CO73 --I
n
f*\ X
<s
00
on
0 1
oNO
I-
NO
I-
o
H it O
o fN
Sample Handling
39
9J
FedEx | Ship Manager | Label 7985 2242 2182
From: Origin ID: (814)231-8032 MarkAmmerman EXYGEN RESEARCH 3058 RESEARCH DRIVE
F e d ire .
STATE COLLEGE, PA 16801
SHIP TO: (802)655-1203
5 BILLSENDER
Kirk Young .
s
Severn-Trent Lab-Buriington
208 South Park Drive Suite 1
14 12CLSH M / i ' l
7208 SOUTH PARK DRIVE SUITE 1
O Colchester, VT 05446
PRIORITY OVERNIGHT
[)> 01 0205446 840 11 7985224221820201 FDE 133455337 290 1/1 36LB N 208 South Park Drive Suite 1 Colchester VT Kirk Young 06 TRK# 7 9 8 5 2 2 4 2 2 1 8 2 F0m
0 5 4 4 6 -VT-us ICE
XH BTVA
30544693110003217985224221822011
lltiliiftfi
7208 SOUTH PARK DRIVE SUITE 1
[)> 01 0205446 840 11 7922243774250201 FDE 133455337 290 1/1 31LB N 208 South Park Drive Suite 1 Colchester VT Kirk Young 06 30544693110003217922243774252015
STL BURLINGTON
SAM PL E RECEIPT & LOG IN CHECKLIST
Client: W f S T A / 3 .
Date Received: Q - 1 - G < V
Log In Date:
\ /\ 7 /o 4
ETR:
' Tim e Received: O Q V i i
SDG:
\ \ n Z S l *3
Received By:
Q
PrQiei* _____ 7 U O O _____________________________ # Coolers R eceived: 2 Sam ples Delivered By: (.Shipping Service o C ourier o H and O th er (specify)
List Air bill N um ber(s) of A ttach a photocopy o f the A ir Bill:
by
Signature: _ V v v --.L.-- PM Signature:
L if ) r S?
______________a X : / o & ___________ '
COOLER SCREEN Th ere is n o evidence to indicate tam pering Custody seals are present and intact Custody seal numbers are present If yes, list custody seal num bers:
vTivbiV. .Y E S X
no - N A ; <V V V V ' C O M M E N T S V -
7v
V
Therm al Preservation Type: W e t Ice o Blue Ice None p o t h e r (specify)
if.fc L
IR Gun ID: C ooler 1: Cooler 2: Cooler 3: Cooler 4:
(,, 2 '2 5 .0 -2 U .L ?
Correction Factor (C F ) *C Cooler 6 "C Cooler 7 C Cooler 8 "C Cooler 9
<t> "C C C ooler 11 "C C ooler 1 2 C Cooler 13 C Cooler 14
"C C o o ler 16 "C C ooler 17 "C C ooler 18 C Cooler 19 '
j C C 't *C C
Cooler 5
"C Cooler 10
"C Cooler 15
"C Cooler 20
.
C
U nless oth erw ise do cu m ented, the rec o rd e d te m p era tu re read in g s a re adju sted readings to a cc o u n t fo r the C F o f the IR Gun
E P A Criteria: 0 -6 C , e xc e p t fo r a ir a n d g e o s a m p le s w hich shou ld b e a t am b ien t tem p erature a n d tissu e sam p les, w hich m a y b e frozen.
S o m e clients req uire th e rm a l p re se rv atio n criteria o f 2 -4 C o r o th er such criteria. Th e P M m u s t n o tify S M w h en alte rn a te criteria is specified.
Sam ple containers were received intact Legible sam ple labels are affixed to each container
C H iftiN ^ ie U S fd D ^ C O C is present and includes the following inform ation for each container: Sam ple ID / Sam ple Description
-Y E S ': -'N O r 5 ',, ;N A &
X
X YES-y S N i N 3 I ^ ^ C M J V i E N T S ^ ^ ^ ^ i
X .
Date of Sam ple Collection
Tim e of Sam ple Collection
X
Identification of the S am pler , Preservation Type Requested Tests Method(s) Necessary Signatures Internal Chain of Custody (IC O C ) Required If yes to above, IC O C Record initiated for every W orksheet
Th e sam ple container m atches the C O C Appropriate sam ple containers were received for the tests requested Sam ples were received within holding time
X
K X
X
X
X YES? iN O i: NA
X X' X
i V 'g * 7 ' C O M M E N T S X ^ I K V # ,
^<3f
V y V X r''
Sufficient am ount of sam ple is provided for req uested analyses V O A vials do not have headspace or a bubble >6m m (1 /4 " diam eter) Appropriate preservatives were used for the tests requested pH of inorganic sam ples checked and is within m ethod specification If no, attach Inorganic Sam ple pH Adjustm ent Form
X X
X X X
A Ja
-gX c*
'V C rv n c r
\\< \ X
o r\
S o ,/* \.0 \e
j ;]
<i ''x'trij r-^i ^ C.C/,
E *T R g / t 'Vy. AVX Wy^V-KT/- $ --'C fe^'v
V o w w .-v .V ..^ ,
*1
S 'tfs C~ <? g x ,A ^ ..< g \e
*
\ rx H f \
\ c.O .s\ TTVK{ .S
4 b <r~ o l a \
Cj /?- \A ______________ f y riX L \ fagx.'vm blf-S
*
FSM002:10.26.05:2 STL Burlington
42
Last Page of this Document
43
