Document jgy8NeVYG6EYyk9r8eBj42x59
vA S i E ,*.N ALV513 REPORT Environmental Laooratorv
PPG Industries. Inc.. I.aKe Charles, L.a.
Derivatives TanK Cleanout. A'TS-uO
jcTuon of oample:
Sampled from drums at HVSA.
ample Jilector:
W. Cooper - G. Pre.iean
ample Methoa/Device:
Random arao - dipper
ate,'Time of Sampling :
8-1-90 1:35 pm
ate AIi Analyses Completed: 3-1-90
Report Submitted By: Date:
Garv Pre.iean 9-31-90
naI.YSIS RESULTS
?=t parameters
jnitauilify :
orrosivity a/a
>activ:tv
>, / -t
TCLF 'ox ic i: v
I mg/L )
N7A
/A pH.
inch/vr
. As
Ba ICd Cr Pb
M.
Se.
Standard 14 0 F 2-12.5 0.250 max
ab Log
5.0 max 100.1- max 1.0 max 5.0 max 5.0 max 0.2 max 1.0 max 5.0 max
1 ND 0.06 ND ND ND
_0.0006 ND ND ND
ther Parameters
. 0/ ii'jne detected
i
HYDROCARBONS 1%) -
Chioroethane
iVCJ LEC
Dicnlormethane
<-MeC12 )
i , 1-Dichloroethene
1 VDC )
1, 1 - Pichioroethane
( DCE)
1 , 9-Dichloroethene
cis/trans )
Tricnloromethane
7IRC13)
1.3-Dichloroethane 1.1.1-Trichloroethane
LEP.SL
(MC)
Tetrachloromethane
1CCJ,4 )
Tncnloroethene 1.1.2-Trichloroethane Tetrachlorethene
(Tnchlor )
JCJLJ
Perchlor
< 2-Tetrachloroethane lunsvm )
1.1.9.9-Tetrachlc roethane - (svm)
Pentachloroethane
Penta1
oara-Dichlorobenzene
1P-DCB)
Hexachloroethane
!HEMA)
riexacnloroPutaq lene
. HCBD
L'nttnown C1HC
Sample Mo 1930 Ii
i
i i ii
1 1 ...... i ii i!
PCBs
1
Heat Value
Chlorine
Water
Densitv
Ash
Sodium ;
1 I
PPJR
BTU/Lb
%
wt% a/mi
wt%
wt%
lotai C1HC
-----SL 021561,
%)
.isposai Metnc
Isftf" *
Profile No
NTS - 005.9
J1AMETER
METHOD USED
: n 11 a b l j. * t v
' n. a
. r r o s i v 11 " dH )
y'N /--a-
orrosivity inch/yr)
y\/.
____Penskv-Martens Closed Cup Tester ASTM Standard D-93-79
SW-84 6 Metnoa 9 04 0 pH measurement
Setafiasn Closed Cup Tester ASTM Standard D-i'278-7A
____ National Association of Corrosion Engineers Standard TM-01 -69
Other (Specify i |
1
i
Other
i
(Specify);
Other
i
l
(Specify)
eac tivit"
^v;/A
ne
[inaaave
nswer will .assif y 3i 3 t *r -active )
1. Normally unstable without aetonatin?'.' 2. Reacts violently with water?
3. Forms potentially explosive mixture with water? i. Cyanide or sulfide bearing waste which can generate toxic
j'ases, vapor or fumes under pH conditions between 2 and
12.5 ?
Capable of detonation or explosive reaction 1: subjected to strong initiating source or if heated under confinement? Readily capable of detonation or explosive decomposition or reaction at standard temperature and pressure? 7. Forbidden Class A, or Class B explosive as defined in 49CFR 173.51, 173.53, and/or 173.88?
TCLP* \/A
'Toxicitv
1 SW 84b
Parameter Method Parametei
is j Ba
! __ 4 1 Cr
Pb
H ! Se Characteristic
6010
Ae
6010
C1HC
6010 , Sodium
6010 1 dH
h010 1 7 4 70 1
I boio
Leaching Procedure
SW 846 i
SV 84b
j
Method Parameter Me(thod
J
6010 5030
1 PCE
! C1HC
LD-2571 LD-2 5 b 2A
3050.0010 Heat Value LD-2 3 b2E
90 4 5
Chlorine LD-2 5 6 2D
Water
LD-2 5 bb
Asn
LD-2561
1
moratory identification r aboratorv: PPG Lake Charles inalv?t(si: SGS Labs
Test Parameters Analvzed
Total metais
8- 20-90
TCLP metais
8- \ 7-40
TCLP volatiles, semi-voiatiles
and Date 9 -1-90
File larv
SL 021562
.S.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS-SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS.SOS-SOS.SOS.SSS.SQS.SaS.SOS.SOS.SOS.
SGSSGSSGS*SGS*SGS*SGS*SGS*SGS*SGS*SGSSG$SGS*SGS*SGSSGS*SG$SGS*SGS*SGS*8GSSGS$GS
i m
<a
SGS Envir nm ntal Lab ratories e9008-038
ca
o
ca
in
RESULTS - Sample ID* 1336 Der. Tank Clean-Out
o
SGS IDi E9008-38-6
in TCLP Metals
aca
ca Date Extracted* 8/13/90 Concentration in ppm (mg/L) in TCLP Extract
Ca</A> Date Analyzed! 8/17/90
(A
o (A EPA HW
a(A (A D004 (oA D005 (A D006 (aA D007 (A D008 o(A D009 CA D010
(oA 0011
(A
TCLP Metals
Arsenic Barium Cadmium Chromium Lead Mercury Selenium Silver
Result
HD 0.06 ND HD HD 0.0006 HD HD
Blank
HD HD HD HD HD HD HD HD
Method Detection Limit
0.2 0.02 0.03 0.04 0.1 0.0002 0.2 0.02
(A
o
(A
Total Metals
m
CA
Date Analyzed! 8/20/90
Concentration in ppm (mg/Kg) in sample
(A
o
(A
(A
a
(A
(A Antimony
a
(A
Arsenic
<A Barium
o
(A
Beryllium
(aA
(A
Cadmium Chromium
CA Lead
a
(A
Mercury
(aA
Nickel Silver
(A
(aA
Thallium
(A
Result
HD HD HD HD ND 36 41
2.7 25 HD HD
Blank
ND HD HD HD HD HD HD HD HD HD HD
Method Detection L:
20 20
2.0 2.0 3.0 4.0 10.0 0.09 10.0 2.0 30
(A
a
(A
ND denotes Not Detected at a level above the method detection limit.
(aA
CA
CaA
CA
m
CA
*
CA
G
CA
CA
a
CA
SL 021563
CA
G
M' of th SGS Grouo fSoei*t*
o* Surv#iHnc*
i*
3QS Environmental Laboratori--
B9008-03S
RESULTS - TCLP TOXICITY VOLATILES ass IQ I B9008-038-6 PPG IDi 1336 Dar. Tank Claan Out Date Extractedi 8/28/90 Data Analyzadi 9/01/90
concantratlon la ppb (ug/L) la TCLP Extract
Banxana Carbon Tatrachlorida Chlorobansana chloroform 1,4-Dichlorobanzana 1,2-Dichloroathana 1, l-Dlchloroathylana MathylathylXatona Tatrachloroathylana Tricbloroathylana Vinyl Chlorida
1336 Dar. Tank Claan Out
NO
NO NO 90 NO S3 NO 305 114
NO NO
Nathod Oataotlon
Limit
50 50 50 50 SO 50 50 100 50
50 100
TCLP Blank
NO NO HO NO NO NO NO NO NO NO NO
Blank Dataetloi
Liait 5.0 5.0 5.0 5.0 5.0 5.0 5.0 10.0 5.0 5.0 10.0
surroaata Standard Parcant Kaoovarv (at 0.050 au/LL
1336 Dar. Tank Claan Out
BUnfc
1,2-Dlchloroathana-d4 Toluana-dB
4-Broaofluorobanzana
101 % 95 %
101
98 % 101 %
112 *
SL 021564
ND danotaa M t Detected at a laval abova tha aathod dataotl a Halt!
Mamter of th* 808 Qreuo MM Mw m kiMMmi l8a8^o8a8fOsoooaa8asooooao800oaotaooo8800asOQ88a8oao80*8<lO^
8Q8 Environmental Laboratoriao RB8UIT8 - TCLP TOXICITY 5BKIV0LATXLNS
353 ID. 9008-038-6
B9008-938
PPG IDi 1336 Der. Tank clean Out
Date Extracted! 8/28/90
Date Analyzed! 9/01/90 Concentration in ppb (u?/L) m TCLP Extract
o-creeol e-creed p-creeol Creaol
1336 Dar. Tank Clean Out. _
HD
HD
ND ND
aii&JL ND ND ND ND
Method Qi&tsUaa. Halt
10.0
10.0
10.0
10.0
2 a 4-Dlnltrotoluene
HD
HD
10.0
Hexachlorobencene
HD
ND
10.0
Hexachlorobutadlene
ND
ND
10.0
Hexachloroatbaae ND ND 10.0
Nitrobenzene
ND ND 10.0
Pentachlorophtnol
ND
ND
so
Pyridine
ND ND 10.0
i 2,4,5-Trlohlorophenol
ND
ND
50
2 f 4 a 6-Trlchlorophenol
ND
ND
Surrogate Standard Percent Recovery (at 0.200 eo/L)
so
1336 Dar. Tank A&JOUX____
ftlA&fc
2-Fluorophanol Phanol-d5 2 a 46-Tribroeophenol Mitrobenzene-d5 2-Fluorobiphanyl
Terphenyl-dl4
59 % 17 %
69 \ 67 % 38 %
53 %
28 4 19 % 33 % 38 % 37 %
21 %
si
HD denatea Hot Dotoetod at a laval abava tha aathad detection Halt. {
3
Member Of the SOB QrOup ttcimm 4n+m am SwavNwm
C
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