Document jgoM2J96BZLJmqyJRgE1QbL39
CG 03- CODE KY-907-D
STANDARD HRS*
TIME
PROCESSES < ) KY-907-D <F)
APPROVED BY FWP 1O/8/80
9
<)
<)
<) ()
H
() -9 TYPED BY:
<)
FWP 10/8/80
CG CODE
PQ
14 YC002B 93
14 YC002B 93
14 YC002B 93
LOT
LBS
TOTAL EST'D WGT 6053
NON-BLEEDING
11 EQUIP 1 NAME : "KROLOR" YELLOW MEDIUM
1 USE 1 LBS
NCODE
ACCT LBS
203 1
RUN 60'<990 GAL) WATER INTO V-203 6 ADD c a u s t ic ! 4 i 7-D 1 20
it 1
1 RUN AGITATOR ON HIGH SPEED
111
205 1 2 1 WEIGH SODIUM SILICATE INTO DRUM & POUR IN 1 3 1 DUMP IN CHROME YELLOW 6 STIR 5 MIN
1 320 I 3 2-D 1 320 1 48X50 IYC -2-BI 2400
i 1 RECORD: START
11
11 1
1 1
FIN
! ----------- 1 -- 1 mil
4 ADJUST TO 75* <1275 GAL)
5 WITH AGITATOR ON LOW SPEED PUMP V-203 THRU
HOMOG AT 2400-2600 PSI INTO V-205
WHEN V-203 MT, WASH COLOR THRU HOMOG WITH MIN
HOT WATER AT 24OO-2600 PSI INTO V-205
7 RECORD:V-205 VOL.* 6 ADJUST TO 60*<2100 GAL)
8 INSPECT HOMOG STRAINER *. CLEAN IF NECESSARY
208 9 6
SV to
11
RUN ___ *<20 GAL) WATER INTO V-____, START AGITATOR *. INSTALL TEMP CHART
PUMP V-205 THRU HOMOG AT 4800-520 PSI INTO SV. RECORD: TIME START TOTAL MINUTES _____________
NOTE: IF HOMOG PRESSURE FALLS BELOW 4800 PSI, 3-WAY VALVE WILL RECIRCULATE SLURRY TO V-205 WHEN V-205 MT, RUN IN 5*<240 GAL) WATER & PUMP
THRU HOMOG AT 4800-5200 PSI INTO SV
349 &
384
12 13
14 15 16 17
WHILE HOMOG, RUN 6* <284 GAL) WATER INTO V-349 RUN 1000* WATER INTO V-384 & HEAT TO 110-12*F
WEIGH INTO V-384 6 PUMP TO V-349 RUN 1000* WATER INTO V-384 6 PUMP TO V-349 ADJ V-349 TO 17' <805 GAL) 6 STIR 15 MIN RECORD DENSITY: ______ G/ML <1.138-1.142)
3220
32-D
3220
SV 18 19
343 &
386
121 122
I
123
WHEN S-11 HOMOG COMPLETE, ADJ SV TO _,,*<2420 GAL) RECORD: PH _____ 6 ADJ TO 11.1-11.3 WITH CAUSTIC|
AT 5% <10 PARTS WATER TO 1 PART N-7-D) ASSUME 50%
SIPHON N-7-D INTO SV 6 RECORD: PH _____
HEAT TO 190-194*F IN 55-65 MIN 6 REC:HT _____*F 6 RECORD: _____*F
NOTE: STRIKE MUST BE STARTED IMMEDIATELY ON ON COMPLETION OF HEATING
WHILE HEATING SV, RUN 39' <1070 GAL) WATER INTO V-343
METER IN SULFURIC ACID FROM V-3B6
MK_____,_____ */GAL,_____ GAL
STIR
MIN UR LONGER
#****" t
7-D 27-D
481
Tfcauip
'TsiMJl"5' "CG 03 KY-907-D EST WGT 6053
USE I NLBS 1 CODE
USE LBS
25 WHEN S 20 HEATING COMPLETE, RECORD: PH_____
26 SET V--343 ACID PUMP AT 5? SETTING <225 MIN)
27 SET V-349 SILICATE PUMP AT 48 SETTING <180 MIN) 25 IMMEDIATELY METER IN V-343 6 V-349. MAINTAIN SV
sv AT 190-194KF DURING STRIKE
29 RECORD:
START
FINISH
MINUTES
V-343 ______
_______
______
V-349 ______
_______
______
V-343
V-349 SV NORMAL
TIME INCHES INCHES PH
PH
AT 20 MIN _____ (36)___ (15)___ _____(9.3-10.0)
4 MIN _____ (33)___ (13)___ . _(9.3-10.0)
1 HR _ . (29)___ (11>___ ___ _(9.3-10.0)
2 HR
. (19)___ ( 6)___ _____(9.3-10.0)
3 HR
. ( 8)___ ( 0)___ ____,,(9.3-10.0)
FINISH
. < )_,,_ ( 0)___ ___ ,,( 7.5-8.5)
NOTE: IF PH DROPS BELOW 9.3 IN FIRST HOUR, STOP
1l
PUMPS 6 SEE SUPV. IF FINAL PH IS ABOVE
11
11
8.5, ADJ TO 7.5-8.5
130 1 SIFT IN
ASSUME 117. 1.
,,l 27-D L
1 50 i 128-A1 50
385 131 1 RUN 40' <308 G) WATER INTO V-385 & HEAT TO
71
1 135--1 40*F
|32 1 DUMP IN t, STIR TO DISSOLVE FOR S-60
11t 11 1 1 280 1 15-AI 280
302 |33 1 ADD 17" <208 G) WATER TO V-302 8 134 1 ADD 6 STIR FOR 2 MIN FOR S 62
11 1 ASSUME 50% 1 100 1 7-D 1 50
135 1 DURING STRIKE PUMP INTO PT PT 136 1 PUMP IN 9 137 1 PUMP IN
38 STIR 10 MIN WITH LIGHTENING MIXER FOR S 42
1 558 1 62
1 62
1 169-AI 558 1 155-Ai 62
1 160-AI 62
356 10
139 140 |41 |42
I |43
44
45 46
DURING STRIKE RUN 18' (317 G) WATER INTO V-356
TURN ON STEAM ADJ TO 23" <403 G) AT 81-82*C PUMP PT MIXTURE FROM S 38 THRU UNDERSURFACE
DISTRIBUTORS AS FAST AS POSSIBLE RINSE PT WITH HOT WATER FROM HOT WATER MIXER
& PUMP IN SHUT OFF PUMP STIR 30 MIN AT 81-82*C FOR S 54 DO NOT SHUT OFF AGITATOR
DUP050105498
EQUIP
SV 4711 148
49 50 51 52 53
54
55 56 57 58 59 60 61 62 63
64
PAGE 3 CG 03 KY-*07-D EST WGT 6053*
T
USE | NLBS I CODE
WHEN V-349 H t T RINSFlN~wiTH~MlNiMUM"uATiR & SET PUMP AT ZERO SETTING
WHEN V-343 MT, RINSE IN WITH MINIMUM WATER &
TURN OFF PUMP MOTOR
HEAT TO 198-200#F IN 5-10 MIN CLOSE WATER LINE 6 DISCHARGE VALVES AT STEARATE
PUMP OPEN V-356 DISCHARGE VALVES TO STEARATE PUMP
INLET OPEN WATER VALVE AT STEARATE PUMP & RUN WATER
THRU HOMOG AT 2900-3100 PSI TO SEWER WHILE HOMOG WATER, OPEN HOMOG DISCHARGE VALVE
TO SV 6 CLOSE VALVE TO SEWER
IMMEDIATELY OPEN STEARATE PUMP DISCHARGE VALVE,
TURN ON PUMP & HOMOG V-356 TO SV AT 2900-3100
PSI. MAINTAIN SV AT 198~200*F.
WHILE HOMOG V-356 TO SV, SHUT OFF WATER VALVE
AT STFARATF PUMP ASAP
WHEN HOMOG COMPLETE, RINSE IN V-356 WITH HOT
WATER FROM HOT WATER MIXER
TURN OFF HOMOG & STEARATE PUMP
STIR 5 MIN AT 198-200F
SHUT OFF STEAM
RUN IN V-385 FROM S-32 & STIR 5 MIN
RECORD: PH______ <3.3-3.7)
IF NECESSARY, ADJ PH TO 3.3-3.7 (DOWNWARD ONLY)
& RECORD: PH_____.
RUN IN N-7-D FROM S-34 IN 4-6 MIN & STIR 5 MIN
RECORD: PH_____. (4.2-4.4) & IF NECESSARY, ADJ
TO PH 4.2-4.4 6 RECORD: PH_____. ASSUME 78%
(DILUTE 10 PARTS TO 1 WITH WATER) ASSUME 50%
SIPHON N-7-D INTO SV
DO NOT STOP AGITATOR
START
FINISH
OPERATOR
27-D 7-D
USE LBS
STEP 9
18
V-262 (20 RPM) 2" 24"
V-243,244,246,247 4'
47"
DUP050105499
r
cc 03 COPE KV-907-D
PKG
- OCT - p* 60
EST. WOT.
1853
37111
UBS.
PROCESSING INSTRUCTIONS: BATCH UNIT
1
PROCESSES
APPROVED BY
!
KY-Qn7-D (F)
FWK 12/12/7
|
Alf-prnafp
nro ip /u /7
REMARKS
TYPED BY
r.i 2/8/77___ emw031579 ma k imo n o t e s
FWP 03-15-79
TOTAL WGT. 6053#
"
AME: KR0L0R YELLOW - MEDIUM
INSTRUCTIONS
-PRESSING-
AT
ATE
IME
ELEASED BY
R ESS 0 OF CAKES
96 72
*ESS With
*SHTO 2000 ESTAFTER 3
0AD on 10 cars
\
)
AGITATION OHMS with 135-1 45F wator HOURS
PRESSLOAD STARTED CAKES USED
WATER ON HRS. WASHED OHMS 4
HRS. WASHED OHMS HRS. WASHED OHMS CAKE CONDITION
MIL.CARS LQApEP
2LELA.IH-LOSSES..
RECORD 1ST 2ND
NON-BLEEDING
3RD
4TH
STH
vMPLES
SLIVER TO
h.
Fnr color
Yv 24 HOURS AT
SAMPLED B~Y~ -DRYING-
180 F
0 LUMP: - OK
RiLEAS^fTBY-
WEv - SALTS - CONTAMINATE
NOTE:
MPLES LIVER TO
IY dr ted In 12*23, 80*97,
lk-1 59k sect ion\:
1
\
Itrv f&r 25 hrs\at 1&o \f
r>ec ordVsei ttions\ 1
\
fiN* 1 nVa idition&J hrs ^
\\ ADDITIONAL ORYING HOURS REOUIRED V v.
reciiii red'*i f anv.
NO. DRUMS
NO. CARS PULLED SAMPLED BY
LUMP WOT. RELEASED BY
-GRINDING-
l l 939 HSP 1/8" RP s c r e e n 3500 r p m
SCREEN
* X. TEMP.
170#p
.......................... MAX. TEMP.
"PM F
.......
____________________----------- -------- :----- -------------------E--X--P---L--A--I-N----L--O--S--S- ES
............--...
<MPLE
/WITHOUT MIXING
MPLEf 1 ENV & 1PT CAN
1 IVER TO
C. T L
DATE MIXED
___
SAMPLED BY
RELEASED BY DUP050105500
; JR& 03 Kr~793"Q
W&T 4380-S
l USE }' N- ! UJsJfcA i LBS i CODE 1 LBS
\\y\ .OPERATOR STEF' P
1
*Vt RECORD LEVEL 2LG5l P_% if <332 FOLLOW SOLUTION I
SV I | M&KE-UP PROCEDURE FOR N-27-D
1
SP I 1 S-^^JUST SV TO 58" (2980 0)
!
CP 11 9<***1?ECPfiI>
ADJ TO 11,1-11*3 WITH N-7-D AT- ]
I 1 33^10 PARTS WATER TO 1 PART N-7-D)
4 | L^fPHON INTO SV. RECORD: PH //XT
ASSUME 50%
12&X OPERATOR STEP PB
-fir-STEP 06/39* AFTER HEAT-UP RECORD: PH
-TCH 3FC20, 8FC10, % 8FC20 TO AUTO
PERATOR STEP PB
SP_^STEP 10/43..WHEN 3FCi0, 8FC10 & 8FC20 FLOWS l
E IN LIMITS, SWITCH 3FC10 TO AUTO & PB
|
11/44. WHEN 3FC10 & 3FC20 FLOWS ARE IN {
SWITCH 3FC20 TO REMOTE
|
PERATOR STEP PB
^
>- " j
DURING STRIKE RECORD:
I
SP STEP
V-243/V-244 13/46 <30 MIN) 1 4/47 (60 MIN) 1 5/48 <2 HRS) 1 6/49 <3 HRS)
RANGE
zi.f jlS?
99.,00--11 00,..>00
d AL 9.0-10.0
JQ? 9.0-10.0
TIME.
-~44ffo
n^ii mXmVm^w m mw
T>ro
16/49 <4 HRS) 17/50 (FINISH)
sifc 9.0-10.0 -~7L gL^.3^ 7.5-0.5
NOTE: IF PH NOT IN RANGE, NOTIFY SUPV &
IN LOG. IF FINAL PH >8.5, ADJ TO 7.5-8.5
RECORD; PH
ASSUME
27--D
Ei &h "in t 6~55'"Sa l "`d r u h
% FILL WITH WATER & STIR 2 MIN
ASSUME 50%
Xl 28
STEP 17/50 AFTER CHECKING^PH, OPERATOR PB.
STEP 23/53 RECORD PH
< 3.3-3.7)
IF NECESSARY AjW~PH (DOWN ONLY) TO 3.3-3.?
RECORD-- PH ffZ*
NOTE: DISSOLVE EXTRA N-15-A IN WATER At 135-1401
*F IN DRUM. USE 30 GAL WATER TO 50# N-15-A. |
FIR 5 MIN AFTER EACH ADDITION.
1
SIFT IN
j
OAH^SIPHON IN N-7-D FROM S 29 IN 10-12 MIN & STIR 1
LJ5 MIN
,_
i
T RECORD: PH%<j&H',0-4.2) * IF NECESSARY ADJ TO |
PH 4.0 -4.2 & RECORD: PH. ^gar--
(DILUTE 10 TO 1 WITH W(Wgr>
SIPHON N-7-D INTO SV
"
Op e r a t o r s t e p p b
>P STEP 24/54 - POUR IN &STIR
ASSUME 77% ASSUME 50%
15 MIN
1 ! ! 1 f
.OPERATOR STEP PB J?P STEP 60 - BATCH COMPLETE OPERATOR STEP PB
>, -
*i i 1
PV0F *7j0 f v-X4^
_'
15-A
j 150' 1 128-Af
I ?-D 1
X
\
! | 97B-Ai
150
START TIME SP STEP
FINISH TIME SP STEP
.i DUP050105501