Document jgkBoZR0kqO4GryJGvmRyNKQ
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APPROVED BY DATE: .FILE: SOP#3SAM.LAB
SOP 3 MAIN LAB SAMPLE LIST
MONDAY
TUESDAY
WEDNESDAY THURSDAY
FRIDAY SATURDAY SUNDAY
1 1l
t
11I11t
I1 11
11 t1lJl1
l1 ii iiii
Bomb 3 03 8 oz.
8 oz. 8 os.
----
Bomb 8 03. 8 oz.
\ # 2 EDO Product j # 1 EDC Rx Liq. ! It 3 EDC Rx Liq.
11 J TCE Storage ! DH Still Reflux
11 | none
1
! # 2 EDC Product ! # 1 EDC Rx Liq. | # 3 EDC RX Liq.
1111 none 1 tl
These are to be sent to the Main Lab on night shift. The dayshift will prepare the bottles for the night shift. Samples are picked up by the Storage Operator and delivered by him to the main lab. Other samples may also be requested by super vision. These samples must also contain the lab test needed on the label. VDCM storage samples for clearance require two 8-os. samples. These and other samples sent to the main lab are to be entered in the sample log book in the control room.
SL 010568
CONFIDENT!1^**
SOP 3
PAGE 2
DATE-
WRITTEN BY:
APPROVED BY: W
FILE: SOP3LAB.PRO
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! mmt&i OfMATORB IA108AT08Y AH?LIN!
! 'd*j PLANT AND MAIN LAB
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PLANT SAMPLING:
1. All samples are caught in plastic tottles with screw on lids except for coil samples.
2. The coil samples are the EDC product and the Transfer sample after the neutraliser.
FIRST ROUND:
1. Moisture samples
A. No. 1 Plant stripper feed and stripper reflux.
B. No. 2 Plant stripper feed and stripper reflux.
C. No. 2 EDC Product and Transfer after the Neutraliser.
D. ST 2 B-4 (Brought by transfer operator)
E. Recovery Still Feed, Recovery Product, TCE
stripper reflux, DH bottoms, VDC St. Reflux, Day Tank. 2. Gas Chromatographs
A. #2 Product - EC and TCE
B. #2 Still Bottoms - %EDC
C. Recovery Still Product - %EDC, %TCE, %Tri
D. Recovery Still Bottoms
E. DH Still Reflux
F. VDC Still Reflux G. TCE Storage H. TCE Stripper Bottoms
CONFIDENTIAL: Subject to Protective Order of ,14th Judicial District Court
No. 91-1.145
SL 010569