Document jgDbXONmMJmwRORMEKLNymwpN

DownloadRandom document
$ SGaotmiisnservices: PrinCtreed:ate1d90w2i/th20A1n0aly1s1t:p5tR9e:p0o0rAteMr PDraotjaecFtile Result Table w02a1r7'1s0\PSraOmRpciieSsLPoEnCgS wif 021710iong 1b Instrument Name _AP1 5000 [Samplefame TKioororr-o11 [UAicnqiueicisotnivoinaWlethed[|3P251F1C7H7n2s0t1e0x9L:o2n4:g11daPmM ZT Sample Type [Unknown| D[iWeownniFoavcotourme[[100000 || roi o|r mmo o [swe] erm | wa | [[RnaeasatuelPtesakSummaroyve |orn|AAnatEERT | riper| CleCaGeorne | woates PFOA 1 PENAT TacPFOA | ToPRNA | 424900200000 || 1120091365)||@0720893s1 | ) 0353 oi | No Ne eros1 PFOAT | worros | Pron | s2owtiioeo0|| 2s000@o2n||(e0ss0asme6i )| oan ozo ELLA | No | PFU 1 [eros 1 TICPFUA| [aceros | 179780 semi | 38s3s0s8p8e)n||wests st |s ow03o 1s6 | No Ne PPRrIaAt | T r5 sC c||P p20szF r 2zs00 O o|[sse0 oaaeroA n iss)|| arsaee | 0000s7ts 7 Sint +l0 Page 101 170 122 PASSombieServices- Printed: 19/02/2010 11:59:00 AM RCsummary [rroeer vrmoamn || owe|we e Smegw|gen]| [sermon [aon | sem | we wma | | [soma Pros amas || we |omem| we | wan| wwe | mw |ow|evsw| scorn [[soroers res swam|vm|we |amas | we |oemanawrsn|memm || wweoJmosaen| || | Jsowm|w| mw em| | 5 Golambin Analytical Services PrinCtreed.ate1d91w0i2t1h20An1a0ly1s1t:I5)R9e:p0o0rAteMr Quantitative Peak Review -- im Tw Eo A iai UA ea] B4a1se3lP0iFn1Oe1Ac613Mi0s0sed | Ba4s1e17l3.iC0n-3eP7cF2O0MAi0sased lg pes 3 HT FET 7 K1001011-011 =z = A ="| nd ed | Ba4s6e3l.Pi0En4eN19cA.10Mi0sased | Ba4s681i.3n0C4s-2P3cF.N0MAi0sased ge inn een z | i: i| B4as9e9Pl.iF0nOe8S001M0isased | B15as03e3Cl,i-0n/Pe3F0O0MSDisased | cB5a1s3e.Pi0Fn1D6eA5c.10Mi0sased | oBa5s1e15l30iCn4-e7P0F0OMAi0sased -| Fi Lo Ro || BasseslPsiFonUseR1AM9i10s0saed :| i 1 51635C0-2P7F0U0NA0a | Baseline Missed 2 os = ix = i | o5Ba9s9e.lPi0Fn6Oo0cS01M0isased | oBa5se01l32iC.n-e0P1F0OMD.Sia0ssed c IeL :3 IE< op b: E o61Ba3s.eP0lFi1nD5eO6Ac901Mi0sased | oB6a1s15e30Ci/-n1Po6Fc9D00MiADsased | cB6as6e3Pl0iE6nT1oAc901M0isased | B6a11se35lC0i-n/PeF1:O6M08iA0s0ased = | = Lrportgene| llTe| Be) < B7a1Ps3eF.liT0n6Ee6A9o.1Mi0sased | o B6a1s1e35lCi0-nPe1Fc6DMo9i0As.ased O Before O After Page 3f 170 126 5 ASnoalluymtibciaal Services pd PrinCtreed:ate1d9/w0i2t/h2A0n1a0ly1s1t:5R3e:p0o0rAteMr TfC oomn Ro Raattiimoo Cofnfiirmar tionmation------K1--001--0e1T1---H01-- 1a--ieat LX- 118 ==| i=- A ar f= T i =_ I 3kd i AA [== | oy 4130P3F6OA902 0a 463P0F2N1A920 Da BasWerlionneguPMeiasksed | B=asWeilionneg PMeiasksed | 499P.F0O99S020a 513P.0F/O22A69D.a0 B<asWeloinneg PMeiasksed|c BasWeloinnegoPMeiasksed = h5ss =| "| = 2 zl Fz[i SI i. 6P3.F02U60A.02 Da 59P9.F0D/9S9.20 0a 613P0F/D1G6A90Z 0a BaseWrloinngcePMeiasksed | BaseWlionneg PMeiasksed | c BasWeiloinneg PMeiasksed | 663.P01E16T9.A20 Da BWasreloinnegoPMeiasksed BY) 713P0E/T1e69A02 Da BasWeloinnegoPMeiasksed 0 Before O After Page 4 of 170 125 3 ASnoalmybtiicaalServices PrCinrteead.ted18w/i0t2h1A2n0a10ly4}p0R2se0p0ortPeMr ReDPsraotujaletcFitlTeable caEv22a11n7'Ts1i0P0SrosajhmercoptalrsbePsFSChsowritf Instrument Name __ API 5000 [[AScaqumipsliteiNoanmDeate K2Pi7r0gC2ok0tn7eo0tre5rx4os4rh4or6dAaTm [SiammepclteoTnyvpoemme |5Union|| [DilutionFactor [100 | [ioctl 135 | Weignttovoome [ooo | Results Summary "Rnaiyte Pak [rant T ron| sam "Anaiyie RT | 12s0an| sare "Cale. Gone " PrbrPoosA1 t | ToaCrPRmRA|| 6w220w000 || a3540o60)||ummseeantm| o00o8 | Ntoe SFraeotri | | wwoorrrmosn ||wsoarw [a| m wee| [aman| saoo or Ww | wo sero | vorron| wo [1am| wm | 0| w A Ze ZL 1sle Pa89gof1e63 126 AnalyticalServices" RCSummary rrses ne [[rreoossss [ros ne|ev[r go ma ien| snmeenm|| wamm || we ||owwwee| | w|e | amen|| we |wwem| - | Columbia 4 Analytical Services" Quantitative Peak Review = rg T= - | Fi | p.7 PriCnrteead:ted18w/i0h2/A2n0a1l0ys4t:0R2e0po0rPteMr K1001011-011 =I TT So =i i. 2130/P1F6B9A.0T Da _u Baseli1 nec Missed | 211730C1-7PF2E0A08 Basweloinnegc Missed | 263P0F12P1A910 Da Baseli1 ne Missed | 31153C0-/P2F7H0XD.Aa0 WBasaelipne. Missed a=| | =-"i Li o- i.m | 209P.F0B60S01 0a oBasine Missed | 4031.8001-10P3F.H0S0a cBaselineoMssed | 313.P0F2H69X.A0 1 0a Baseline Missed | 311530C-2P7F0H0XADa Baseline Missed gs bing ze ction pes Ming ea ol L EL i. i. 363P.0F/H1D69A.10 0a oBaseine c Missed | 315130C2-7PF0H0XA0a Baseline Missed | 39P9F.0H1X80S.010a Baseline Missed | 4013800/-1P0F3H00S a c Baseline Missed ithe owe es conn pea is iz iE i= Ath tel oh 4S63_.108/010-3P.F0H0Sa Baseline o Missed | 5151.30C4-7P0F.O0A a Baseline o Missed | 51S5_0143C7-0F0FD0A8 Baseline Missed | 51153.C0-/P4F7O0AD.a0 Baselineo Missed 0 Before 0 After Pag9e1of 169 128 8CoSloumibina services: PriCnrteeadt:ed18w/i0t2h1A2n0a10ly4R.02e0p0oPreMr r ion Rr atio Cr onfie rmatr ion e------------ K1001011-01e 1 eteee Tm [oi = = : | El oa fT re Beene| = Berm | SL Re JE _21B3Pa0Fs/B1e6Aol92M0iis0nsaeed | c2B6a3P0s2Fe1Pl8Ac0Mi2i0snsaeed | Ba209sp.0re1e9l9sc.0?MiiDsnaseed | Ba31s3P0Fe1HlG1uA9Mi02i0sn2seed Wrong Peak Wrong Peak Wrong Peak Wrong Peak 1 1 - bode ot F4 5 i= Tinapisodwide 363R0H/3P1A902 Da Baseline Missed | Ba30s9P.F0e/H9Xl9c.SM0i2iDsnaseed | Ba5S1_s31.3e0C4l.o7P0iMF0iD0nsAaseed | Wrong Peal. Wrong Peak Wong Peak NB PBA and PFPeA do nal have qualifying on ransitons O Before O After NA BaWsroenglcPMieiasnkseed Pa92gof1e69 129 LS CSooltusmebiravices: PrinGtreed:ate1a9w0i2th12A0n10ap11Rs:e50p:0o0rAteMr PrDoajteacFtile Result Table 0GE22v117a71I0kP0nragom1epdcbloePRsCLsoingt Instrument Name API 5000 [SRAaeemaapuuliiseiitaioomnn MDeaettehad||TiP2oFo1Ct7kon21e70l61e7x0C48--do83FnaIg1m ecionval TSE TeSacmnpolne vTyapme me [|5Union | wDeiilugthitoinaFaVcotlorume|T1.00 oes] a ERET ARreaisultPesakSummary ont | mon | sowow Hoye AT [ava] EmTw |oSew+Gonse| w | PENA 1 13C-PFNA 2665500 | 2.02 (2.06) 9569 0.067 No wont [earrrro|| weevsno [|ssssom|asozewo]|| ooeomm Wo = al? "P2 o Page sof 170 130 8Solumbia AnalyticalServices Greate wi AnalytReporter Printed: 19/02/2010 11:58:00AM Resummary soso entims [roz [sroron Prinz | S-130.Pr [ros2 [swerros Pron smoeron SrruamcProm [erosz prox [sworron [paz [reas [wrenn) [| res [weds|CH IA| Coins| Times | vow |we| mew| we | | ass| www|wo|sows| ve | [2oeaon| an |ow [ome | ow | [oma | 0 |w |ome [we | Jovan| som |we|owom| we | |avawm |seo| nN |wma | wo | [socom| ws [we[ome | we | |smeon| some | No|cms| we | [ooo [os | bwoo ||omasaoem|| vwees | Tsmam ml me Jomuss| 0 |we[omeam | wn | |ewasn|wwe | we|wmer | we | [swe | ar |ow [ome | we | [swe | an | we |ome | we | O CAnoalluymtbiciaal Services `Quantitative Peak Review - = or I = PrinCtreed:ate1d9/w0i2t/h2A0n1a0ly1s1t:p51R9e1:p0o0rAteMr K1001011-012 = 7m oBa4s1e3lP0i/Fn1Oe6AM91i0sDsaed | Ba4s11e37lC.i-0nP5e7F:2OM0Ai0sased | oB4a6s3ePl0En4Ne1oA9M01isDsaed | Ba4s6e1l83i0Cn4-e2Pc3F0NMAi0sased Sng pea elon -I tong pes i} Fz i. = Bas4e9l9Pi.0Fn/eO8S0(01M0isased | Bas15e03l3Ci..n0P8eF0:O0MSDisased | oB5a1s3e.Pl0Fi4eO69cA.M01is0saed | Ba5s1e1l53i0Cn4-e7P0cF0OMAiDsased T 3 ion 2 =: 1 er | Ba5s6e3lP.i0F/nU5eR1A9c.10MiDsased | oBa51s36eC5l-i0nP1eF2U7RMA0i0s0ased | oBa5s0e9.lP0iR/n8Oe0Sc.01MDisased | Bas5e013l3,i0Cn1-e8P0c.F0GMSiDsased ILow | _B6a1s3cP0iF/nD5eO6cA9M10iDssaed | 1 ey ilhen] oB6a1s153e0C/l-1n6Pe9Fo.DM0Os0Asaed | o6B6as3e0Pl6iFn1eT8c0M1iDsased | Ba5se11l35iC0n-e/PF1cD6MOD9iAsa0sed "sw J 71P3F.0T6O6A9.10 Da Baseline c Missed | 611530C/-1P6F9D00A0a Baselineo Missed O Before O After Page 7 of 170 132 LSCoS lumo bia services: Created with Analyps.t1R2eporter Printed: 19/02/2010 11:59:00AM Ton Ratio Confirmation K1001011-012 J im |== z7l] \ o= i =[LsAvai} ifs pnd an =S .E0). R pendriarn| =| JUN| =The pens 413.0P1F3O69A.20Da 4630P1E2N1A820 0a 499.P0F19O9S.20 Da 513P0F26D92A008 BWaosneglPMieiasnkseed | cBaWrsonegclPMieiasnkseed | BaseWlionnegoMPiesasked | Ba WsroengloPMieiasnkseed z pe = = F~aLhptt |iBZ=i) 3 3 7~ - i-i 563P,E0U2I6A902 Da Baseline c Missed | 509P.0R/O99S.20 Da o Baseline oMissed | 613.P0F11D6A9.02 0a oBaselinec Missed | 663.P0E/1T6I9.2A0 Da Baselinec Missed Wrong Peak Wrong Peak Wong Peak Wrong Peak ] 71P3F0T1e1A62900a BWarsoneg.lPMeiiasnkseed O Before OJ After Page 8of 170 iE LS SColoumibina services: CrweithAanalytstpRe1o3podrer Printed: 18/02/2010 4:02:00 PM FRDraeotsaeueFlitTlaeble GEa0tv2?1ai7oiiP0sosamndpaolbRrePsRsChSorwi Instrument Name API 5000 [`SAcaqumiseitaiomn Deate T |2118/2010o 35423 AMT [[meScioTanyvpaemlmep|J Ulnkneown s] n`AeccqutiisoitniVoanlMethod|15P6FCkinetexshdaomr [DWioliuatihotntFoactlourme|[ 1.00 000] ReERsauElpteEsrSum|m| arsyname | snes | FgaaleaAT| moons | cCaeere | edn r vost r|vr [woormrs|emoso|mssoeoeuo|| msewse | | on om " w wroas | racrra| sor [s|meewm| ow wo vwrsenss o[orrems|| msose [[sommee| wwe | en | wl wo sors | viorron| seo | szesn| wero o ay ioZrt 5 28 Page 83.01 169 136 8 Solumbia Lo \nalytical Services: Printed: 18/02/20104:02:00 PM RCSummary [ rs r ven||o owmo||w wa e ioeme m || vn e | FoTe rae [some smn|sen|we omen| 8 SAnoatluymtibciaalServices" PriCnrteead:ted18w/i0h21A2n0a1l0ys4tp01R2e50p0ortPeMr Quantitative Peak Review -I x = K1001011-012 =I g7 ps= ns in2 | io| i= | cBa2s1e3lP0i/Fn1Be6Ac9TM0isDsaea | oBa2s11e73l0Ci1n-e7PcF2MB0iA0s8ses | oB2a6so3Fi0Pn2Ge1A810Mi0s8sed | Ba3s1e15l3i0Cn-2Pe7F:0H0MXiADsased aap pea ops Wag, ei pga | i i- = cBa2s0o9Pi.rn0ee80sM0i1sDsaed | cB4as01e38l00i1-n0eP3cFM0HiS0sased | Ba3s1el3Pi0Rn2HeI6A9c 0|Mi0sased | Ba3s1e1l53i0Cn-2eP7cF0H0MXiA0sased m] Sr I El 0 Te ix- | =2 3 |- Fil B3a6s3eP.lF0i1Hn6ep8A.c 1MiDsased | yp B13a13se5Cl0-i2nPe7F0H0XMAi0sased | Bas3e0l9P.iE0nH/e8X0S.01MDisased | o B4a0s1e38l00i1n-e0Pc3F0HMSiDsased iuaggees sian ag = Ih d3 IF | oB4as0s_3e.1l08n100e3Fc.F0MHi0ssased | oBa5s11e53l0Ci4n.7ePo0FM0OiA0ssaed | 5s1_51034C7-0P0FD0Aa Baseline oMissed| c 511530C4-7P0F0OAa Baseline c Missed 0 Before OI After Page 95 of 169 136 4AACnoalluymtibciaal Services- Creat with Analy5s.t1R6eporter Printed: 18/02/2010 4:02:00 PM lon Ratio Confirmation K1001011-012 EFie TT =a iC [3ofp fepu)| 1; | hee| SL Roe 213P0r1e6i5s000 oBasoine Missed | ca2sp6i3en0p3g1eo60Mi0s0sed | B2as6ep9lir0ne9es50M0i8ssed | B3a1s3Pol0n1ee1or9t20i0a8sed 2 Wong Peak =Wiong Peak Won Pook Wiong Peak = il = Foe | i Et J-- 363P04H10A.2 00 cBastineo Missed | 26p6r0i85s0208 Baseline o Massed | oB$aSs1e15l0an4ce7Fo0rv0oi0gns0ed | NA Baseline o Missed won Peak Wrong Peak Wong Peak Wrong Peak NE. PBR and PFPeA do nat Fave quafying or Famions O Before OJ After Pa96gof1e69 15 Columbia PAY oi TI PrimCerde:ate1d90w2i7n20A1n0aly1s:t5p9R1:e70po0rAteMr DaFrtoageFeitle Result Table cT2a1a1771s100P:0nar.mo1pR0lae0sRLPoCngswit Instrument Name __API5000 [[S[AacmaupilseitNioanmDaete | [21K7i7o7o2t0o1r0i$0373521 Fi [jectionvial [a7 [SinajmecptlieonTVyopteoms [U nkoow |WeighttoVolume [ooo TRFesEauyltPseaSk um|moarny an| wm | FSraEER | maenn| iCeantBear e | | wowren [oros1 pron | | ovsrotrroons | | mwas moss [2araon| smom| som wm |ow| wo [rrunar ror | ocrrum| wom [smo| raseos [rv Taman] mes ven | om | aw | |wewe l| pPrrimoi | | v oreo e ||mwaar e [|seo osaesm|| me | oom mn o wo Prien worm| wae [omesn| 0| mh wo 4dy0 7 Sat Page 80 170 138 AnalyticalServices IRC Summary TFororn a sic pron [mcr ros sisorros Canam| wm | ow | wem i mam| seme | we |mwem| we | wa| 0 | mw | woo | we aan| mmo | we | owe wae | mem | ne | sway | we | prumaz wom| 5 |te| omewm |we| rook Sscrroon Pera sms |0 |we| owom| vaso|wa|n we| amen| we snow| om |we| mow | PASCAnoalluymtibciaal Services- Created wih AnalystpR1e9porter Printed: 19/02/2010 11:59:00 AM 3 - Ck 2 | Quantitative Peak Review =7 T= L- Z. LS K1001011-013 o Ed La41o3Pi0rs16o80vi0s8ed | oB4as71e03l08n.e7p2ME0GiA0ss8ed | Ba4s6e2l.Pi0en4eN15Ao.TM0s0s8ed| o S4a6s1e8l03in4Ce7.Fc30MAi0sased 7| =] =i =I cBa4s9o9Pi0rne2o0sM0ii0s8sed | B5a01s23.ce0.8lp0cE0MiGiS0snaseed | oS5a1sP3eFl0nO4e6Ac90TM0isased | oB51a135s00.e4PlF7MOii0DAsn0saeed I 2 tam ide |= - - Cl Ei 563P0r15u19.p10eDae] 561530C/.207FB 0U0nA0ea ] p59e9P0eF12S0B 010aid 5013300./p8F0G0S0 Baseline Missed | oBaselne Missed | Baseline Mased| oBaselne o Missed ig =8 i] - Ba5sP1e3rl1ion5oe8A9M01i0sased | oB6a11s3e5.i0pn1F6BM8oi0As0sed z7 =7 " ] Ba7sPe1l3Ei0Tn5eG8o910Mi0s8sed | o B6a11se35lCi0.n/ePF1B6Mo90sA0saed i sot i. | B6a62sP0eE6T1lA9oMi0Ti0snaseed | oB6as11e35l00n.e/F1BM60i9DAs0ased O Before O After Pa11gof1e70 140 8AnuamlybtiicaalServices Created with Analyps.t20Reporter Printed: 19/02/2010 11:59:00 AM : A Cp pi Ton Ratio Confirmation i = Ie- -zl . ef Egat | 4130P3F6OA920 0a 463P0F1N2A129Z0 Da BaseWlrionneg;PMeiasksed | oBaseWlrionnegcPMeiasksed | i! "ib = K10010117-013 i \ == A la | hee 499,P0F9O9S.200 513.P0F1D26A92.00a BaseWlrionnegoPMeiasksed | BaseWlrionnegoPMeiasksed tet fff 3 J = et |3 = pgs| bee Bhi | -i = ne| mentite cBa5s6e3Pl0iF1nU2eN6A90M2iDsased | 599.P0F1O99S.20 Da Baseline o Missed | 6P13F0D/1O6A920 Da 663P0/E1T69A20 Da Baselinec Missed| o Baselineo Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak se 71P3F.T0E1A629D.a BasWerlionnegc PMeiasksed 0 Before OJ After Page 1201170 14 LS CSoloumbaia services PriCnrteeadt:ed18w1i0t2h1A2n0a1l0ys4tp02R2e10p0orPteMr PRreDosajtuaelctFtilTeable E00w22a11n7'71'1s0S0PasrmohjpoeldcretstbsS\PhFoCrst. wif Instrument Name __AP 5000 [Samp Name K2i/1o8/u2i0100740.0%355 AM AcIqnjueicstiiotnioVniaMlethod| PFCkinetexShdoarmt [InSjaecmtpiloenTVyopleume || 5Unknown [DWieliugthiotntFoaVcotlorume[[100000 "ARoneanistyuiletPseaSk ummartyame [same |"AnAaigyieelRT|avons| GaGle GCone PFBAT Tsceron| sesso [124020| ses | ot = | | | No | Pres 1 | taoprrs | aseos00 | at9(e2e) | 130910 No PFHA 1 Ey Siees00 | 525531)| 274290 04s No [errpas CPR| stesso | 61562)| 7a | 0m | Mo [Pres 1 |1sorrrs| aseos00 |e2e32)| Tesat0 083 No ['sisopris | 13cPFOA| 4287300 |626631| 3590800 104 No S1acPFOR | 1cProA | aera| 75469| seaman w | ow | +S0o 21 Pa97gof1e69 142 [ogame nalytical Services: RCSUmmary om rmtne[wr0mn|| nen| PrCovedr10wei0t3h2As0n70at4t0ae2e0p0odre wg | prez Prroaz [poss | s-racpren [sore eww | em | we | awol|e | [oso | oem | wo |aes | ve | Toxes | wom |w | wow | vs | [raz| sso| wo |ssa | we | |saseso |soso| we|wsror | wo | Pa98gof1e69 ws OCoT lumbia rier PrCinrteead:ted18w/i0t2h/A2n0a1l0ys4t:p0.R22e0p8o0rPteMr Quantitative Peak Review == - 3=3 3 K1001011-013 -J [ =7 1 zl } 1= 1. isa) fey i. _21Ba3s0elP1iF6neB9A.T0Mi0sased | cB2a1s1e73l0Cn1-e7PcF2B0MAi0s8sed | Ba2s6e3lP0iFn2Pe1e9A01Mi0sased | Ba3se11l35iC0n-e1PcF2H7MX0DiAs0ased - 3 q zl = | i F =| G B2a0se0lP/iFn8Be0S01M0iassed | Ba4s0e13l8.i00n-1eP0c3F.HM0Si0sased | B3a1s3e0lP/iR2nHe5I.0A0M1i0sased | Ba3se11l35iCn-0eP2F:7HMX0i0As0ased ip : Wong pea Msg ea A | | io i- Fg B3a6s3eP.lE0in1He1p6A.901MiDsased | cBa31s13e5Cl0i-n2Pe7F0oH0MXiA0sased | Bas3e0l9P.iF0nH/eX8S001MiDsased | o B4a0s1e38l0i01n-e0P3oF0HMSiDsased lag es brag ea hip hg :H i3 o=l I boZ i3 i= | .=i oB4S0a3_.10s8/01e0-3lPc.MF0iiHsDSnsaeed | Ba5s11e35lC.i0-n4eP7F0MD.i0As0saed | Ba5sSe1_l51i03n4Ce7-c0FM0FiDsDAsaed | Ba511s530Ce4-7lPG0FMi0OiAsnDsaeed O Before OI After Page99 of 169 14a 4 Anoalluymtibciaal Services Created with Analyps2t 4Reporter Printed: 18/02/2010 402.00 PM Ton Ratio Confirmation ---- 3 11 K1001011-013 = 7 EE 3 | I 2! 2130P1F6B0A20 0a 2630P2F1P8E.A020a c Baseline Missed | o Baselinec Missed | 20P9.F0/B9S9.20 0a Baseline Missed | Wrong Peak Wiong Peak Wrong Peak EfFI u| wd =1 of i 313P0H1X1A90208 BaseWloinnegc PMeiasksed Tepid 36P3F0H13p1A920 Da 309P.0F19H9S.02Da 5S1_51034C7P0F0DDAa BaseWlrionnegoPMeiasksed | o BasWelrionnegoPMeiasksed | c BasWerloinneg PMeiasksed | NB PBA and PFPeA do nal have qualifying on ransiions 0 Before 0 After NA BasWerlionnegoPMeiasksed Ad4 Page 100 of 169 145 5AnSaolymtbicianl Services prinCtreeda:te1d91v0i2t7h2A0n1a0ly1s1t.p5R29e.5p0o0rAteMr FDartoamFeitle ResultTable T0022a11n77s1100P\riSeoadcnmiabpslPeRsCLSwoinfg Instrument Name __AP1 5000 [S[ `aAcmqpuin lseitNiaoj nmMeetheod[|32c[P/K51Fi7Co/ko2tti0o1nr0e19l0o:1e446x:L5do2nanPmgM vr|S[DaWimeluiptglihoetnFtTaoycVptoeolrume |[[10.0000Unknown| Results Summary naaatye Peak istame |sara|AnAaGiesRRTT | anate area CleeeGone PFNAT [eros Tacrros | eseszoio0|| 2 199@009)1||t@25o 4093a 9 | |itw todsteo| No Ne PFUOA1 | 13GPFUMA | 11280 |3s| 2T@ose e| 00s | No [Prost| 1acpros | mesa [meen| set 0025 No PFTeA TACPFDOA| 160790 | 547(550| Te4t 0078 +2 al ZLihvo Page 130f 170 148 Li Guma nalyticalServices: CoT voit nAnatr Reotde RCSummary posepuatiome sermon Prinz swoops | wren) [| awed | SEERA| Corton| 0 |vos| eso |ow |amww| we | [recon| ss|we|oso | we | [owas | 0 |w[ome | we | EB 8 [smorros Pron s_rsceron sce rosz pro: [sero Prinz prea |rovaoo|saan | we |emer| we | [20cm| wo |wo| wow| ow | [oo|rsamoon| wo |owa|rswe y| |swam| vem | we | emis | ne [oween| 0 | we|omen| ow | Jowuss[o|ow mem|e we | |asusy| wow | se |omer | we | sue| m0 [ esos| | we | [sees | ew |wo|omoam | wo wr age wor 170 48 CAnoalluymtbiciaal Services Created wih AnalypR2e7porter Printed: 19/02/2010 11:59:00AM = TB Quantitative Peak Review EE) K1001011-014 =a = |A Ey = | Ba4s1el2Pi0Fn1eO6A801Mi0s8sed | cB4o11s37eC0l-n3Pe7Fc2O0MAi0s8sed | oB4as6e2Pl0En4eN1oA.M10i0sased| oBa4s6e18l30iCn4-e2P3cF0NMAiDsased E| Exq Ip dg anp vnl Ba4s03Pe0Rn2O0S01M0i8ssed | cBa5s01e33i.Cn0-e6P0cF0OM0Ssased | cBa5s1e3iP0nF4ecD69A.1M0i0sased | oB5as11e35lC0n-e4PcF7DM0AiDs0ased = wm - EiI in3low onf f Hdl L c5a6s3eP0Fi5Un1R9Ao0M1s0saed | cB15a3s6eC5i-0n2Pe7F0uU0MR0sAsaed | oBa5s6e9Pi0Fn/De8S0c.M10i0s8sed | c Ba5s01e3l3iC0n-/eP8F0OM0Si0ssed i= al] LC 4 a il]1 oG6a1s2eP0iF/nD5gO6Ao9v01i0saead | oB16a13s5Ce0-i7Pn1eF6cO90M0Ai0s8sed | Ba6s6el3Pi0EnT6eA1.91M0is0sed | B6a11s5e3l0Ci-1nPe6F8D0MOiA0sased | -t 547 "| B7a1Pss3Fl0iT8nEe6A9oM01i0ssaed | B6a11s53e0Ci1-n1eP6Fo9DM00iA0s8sed 0 Before O After Page 1501 170 148 4 Solambia Analytical Services" Greated with Analyps2t8Reporter Prined: 19/02/201:059.00AM Ton RatioConfirmation TE = K1001011-014 ] TT Ek: i=, La ful lt [2 : hala JAC Led 413P0F3O6A820 Da Baseline _ Missed | 463P0E2N1A920 0a Baseline oMissed | 499P.0F/O99S.20 Da Baseline Missed | 513P0F26O92A0 Da Baseline c Missed Wrong Peak Wrong Peak = Wrong Peak Wong Peak oi =| i] Ju] Zep | i WET | me[TL i nities 563P0F1U2R6A902 Da Baseline o Missed | 509.P0F/9S9.20 Da Baseline c Missed | 613P0F/D1O6A902 Da Baselinec Missed | 663P0/F16T920 Da Baselineo Missed Wrong Peak WrongPeak. Wrong Peak. WongPeak Loe 71P3E.T0o1R623D0a BasWerlionnegP.eMaikssed 0 Before OJ After Page 16 0f 170 149 LSCSoluombiia services: PrCinrteead:ted18w/it0h2A/n2a0l1y0stp4R.26e29p0o0rPteMr DPraotjaecFtile E0w2a1n7'1s0PSraomjpelceasPhFoCrs wif IRnessturlutmTeanbtlNeame _ A0P2I1751000h0ort 0b [[AcSqacuaimusiestiiNtoianonmDeaettehod|| 2TPR7FI1CO6K02iT0G1nT0e7t40e77x%5S3h1doaArmWt l[SinaDfimleucattiiloonnTFVyaapcretaorme [ |[ Unio15 00 ] ]| [ `A ecM t[o 38 nvia |Weighttovolume [ooo | -- Results Summary ARnaarieyrie Peak ne |aes n|AaEiUeRnT|wanes| GaGleGeCloTne [wearer 1 =X PFBS 1 PFHAA 1 |PPHpA 1 Teor| Toe | 353000| 201980 wn No 180-PFHS | 4192000 | 4.19 (4.26) 170880 | 013 | No TaCPRRK|A 7074200 | 520(530)| sor | 042 | No | 13C-PFHXA| 7074200 | 614623) | 77424 025 No S1BOPFHS | 13C-PFOA| 4385900 | 623631)| 4192900 No S_13C-PFDA 13C-PFDA | 4585900 | 7.51(765) | 4585900 | 1.00 No a yo oA5 211810 Page 101of 169 150 8Sombie,Services" Created wih AnaisReporter Printed: 18/02/2010 4:02:00 PM RCSwmmary porepsctone roa pePenz [pron [pronz pas 5rceron [ocomoa [enemas[| aes |worn|SHH| cin| [aaa|wm| we | cw| ve | [2am |amo | ne [reo| ve | ves [saesen[am |we |owen | ve | [ome |aso |wo|amas | ves | Temes| wwe |wo| www| ve | [imam | wa | ne |eomm| we | [ozs | onam |wo|mmoern| | oe zor 00 pe LColR umbia services PrCinrteead:ted18v0it2h12A0n1al0ys4tp032R1e0p0orPteMr J : Quantitative Peak Review pou FJ 7 3 = i E213p0r1a6x9T00a | 21173.c0A 1P7F2E0A0a Baseline Missed | Baseline Missed K1001011-014 [7] 3| |= 23 i: io pe 263P0EP2O1R9T008 31135C0-2PF7X00A0a - | Baseline Missed | Baseline Missed I c2h09p.or03aL00| 0R a ep z 4l 013800-1p0F3r0iS0a | Er31n 3p0r26iL801B 08 p] J -- 31153002.7|P0F0H0a a oBaseninegs Missed | oBasellniegMissed | BaseolineeMissed | oBasea lineo Missed a- | -; == iI =| 363P.0r1H1p63A.01 Da Baseline Missed | cB3a1s15e3l0Cn2-e7.p00FMRi0sased | co B3a9s9pe.ri0n1e8c001MiDsased | oBa4s0e13i60n0e1-o0p3F0iMSi0sased = !3 = 3 = = = i A| |= EN i. Ba4sS0e3l10i1n81e00c350MisDsased | oB5a1s1e53l00n.4eP7Fc0OMA0ss0ed | cBSass5_e01i34nc7e.0c707M00iAsased | c B5a1s15e3l0i0/n.4eP7:F0O0MAiDsased 0 Before O After Page 103of 169 152 Columbia 4 Analytical Services Created with Analypst32Reporter Printed: 18/02/2010 4:02:00 PM Ton Ratio Confirmation im aw K1001011-014) 7 i.- | k=lo | lEL I = AL A] Spal) 213P0F/1E6A920 0a 263P0E2P1o9A02Da 26P9.F0E99S.20 Da 31P3F0/H1A12900a BasWelrionnegcPMeiasksed | Bas_eWlrionnegcPMeiasksed | BaseWlrionneg PMeiasksed | BaseWlrionnegc PMeiasksed EE 3 |= 3 oe f Tibspeitate 363P0F/H3p1A902 0a 399P.F01H9I9.S02Da 5S1_51.30CP4F7D0A0a NA c BasWeilionnegcPMeiasksed | BaseWlrionnegMPiesasked | BaseWlrionnegMPiesaks.ed | BaseWlrionnegMPiesasked NB PFBA and PFPEA do nol have qualiying on (ransiions 0 Before OJ After Page 104 of 169 153 LSCoSluombmia services: PriCnrteead.ted18w0i2h/2A0na1l0ys3y:p2R34e.3p0o0rtFeMr DPraotjaecFtile GE2v1Ta10SParmopRlaeRsPtRonCgE i InRessturlutmTeanbtleName__AcP2I1751000l0ong 10 [Sameame TRT0T01767% IRcauistionMetha |P2F71x7i7n2e0t1e0s9t5o4n.g29daPmM Injection Vial [39 [TSaemtploenTvypoerame[ |Unk 5 no] wn| |DWieaitgohntFtaocvtoowrme|[1os0o0 | | `RFesnultPsekSummary Haar te Cane rproonn | Torororn|| wwoaree [imaomm ]| osm ow | we bros | vores | smawo | 1w| a mewm| owe | PFUNA 1 1acPrUM| tet | asseon| oases|ous | {eras ssron| wae [en von Aeer 2081 Page 106of 170 156 4Columbia ~ AnalyticalServices' RCSummary Printed: 18/02/2010 3:24:00 PM [emo [mon|wm| we[men|e] ro: sme | ow |ow |anew|| [oronei [somo L[amemm | wwwWo |oommeonw || owve |wemern|wm| we nso || [rarse [sswmann||oaww || ewe|oowmeom||ve| LS Columbia services Quantitative Peak Review SE a 14 Tz 2 il || L GB4a1s3e.lP0i/Fn1Oe6.A9.10MiDsased | Ba4s11e37lCi0-n8Pe7F.2O0MAi0s0sed an cong i cl PrCinrteead:ted18w/i0t2h/A2n0a1l0ys3t2p4R..e30p5o0rtPeMr -- K1001011-015 Lo: ; Ll".| TE ETheen (I | | oB4as6e3lP0i/En4Ne1Ac910MiDsased | Ba4s6e81l.3i0Cn4-e2Pc3F.N0MAi0sased Le 1 5 wong 23 Lhd c B4a9s9eP.l0iF/nO8e0S.01MDisased | B5as01e33l0Ci/-n8Pe0Fc.OMSiDsased | Ba5se1l3Pi0nF4eD6cA910Mi0s2sed| oBa5s1e1l35iCn0-e4PoF7DM0ADis0ased - a =1 ga ise Zl -2 Rema[=T=l = =a 3A CBa5s63eP,l0Fi1nU5eR1A9c.01MiDsased | Ba5s6e15l30iC/n-2eP7F0U0MRiA0sased o J = ser Fl here Beceoo] LL B6a1s3e0lP/iFn5De6O9Ac01MiDsased | oB5a1s15e3.l0Ci/-n1P6eF9cD.0MOiADsased | oBa5s0e9Pl.iF0nD8eS0o0M1iDsased | E IE =P| hoseobe) i | Ba6s6e3lP0i/En6eT1Ac910MiDsased | oBa5s0e13l3.i0Cn1-e8P0oF.0OMSDisased LR Ba6se11l35iC0n-e/PF1oO6M00i0As0ased "i :1 = a 550 E=R ed | Ba7s1el3Pi0FnT8ee8Ao910Mi0s8sed | co B6a1s1e35lCi0-n/ePcF1D6OM9DiAs0ased O Before O After Pa108gof1e70 156 4 AnoalluytmibciaalServices- Created with Analyspt.3R6eporter Printed: 18/02/2010 3:24:00 PM fon Ratio Confirmation K1001011-015 RI = LC fz 3 nl Ee [Vs x0 | Zod gen LIAN A | m reise |i L A A | [| m ah e 4130P1F3O6A920 Da BaselcMiisnseed | 463P0F2N1A920 0a BaselciMinsseed | 499.P0F/9O9S.20 Da BaselcMiisnseed | 513P0F2D692A002 Basel.Miisnseed Wrong Peak Wrong Peak Wrong Peak Wrong Peak d wri | i L lth=f 2Treeifee|=Toei 563P,R0U26T9A02 0a cBaseline Missed 509.P0F/9O9S.02Da |, BaselciMinsseed | 613P0F/D1O69A020a BaselciMisnseed | 663P0F/1T269D0a Baselc Miisnseed Wrong Peak Wrong Peak Wrong Peak Wrong Peak { 713P.F0T/e1A629.0a0 BaWsroengolPMieiasnkseed 0 Before OJAfter Pa109gof1e70 157 8CoSloumobima services PrCinrteead:ted18w0i2th12A0n1al0y4s:tp03R2e:7p0o0rtPeMr DPraotjaecFtile 0w2a1r71s0SParmojpelcetssPshFoCrst wif InRessturlutmTeanbtleName __AoP211751000sh0ort rab [SampoName TRio0TGT07 [AcquisitionDate Liecion vir |1P23r/1C08R/2n0e1i0 e4H23o.r06dAamM T EE C -- [DwSiaolmgtplomenoTavycpoteuerme o1o0o0 || Tr sve | a [| ms|iy| ner| Results Summary ProA 1 Taceron | swsaoo | 126120| vet |oes| he rPreasnt1 | ora | s410s65w00 | 4[1s96e26a)|| a17m42o30 No . prs | worms| eo [sem| memo | om | to [StsoprHs | 19CPFOA | 4950500 | 622631)| 4196500 No SCPFOA | 13CPFDA | 4ssos00 | 7520765)| 4es0s00 No oe eCrA2S1gl Page 105 of 169 158 OE comme Createdwith AnalytReporter RCSummary reorrs [iy|msg won| [ras [sam |wen | we | am | | rwenie aemweenm|| woenn||ewe ||osmweam||ewm]| Tea To Tort LS RColoumtbiaa services Quantitative Peak Review =I a = PrCinrteead:ted18w/i0t2h/A20n1a0ly4}p.0R32e90po0rPteMr K1001011-015 =I = sm i= os | Fz i i weed 3B lhe Aad U B2a1se3lP0iF1nBe6A901Mi0sased | cBa21s13e7lCi0-n1Pe7Fc2B0MA0is8sed | Ba2se6l3PiE0nP2eE1Ao90Mi0s2sed | Ba3s1e1l53iC0n-2eP7F0.H0XMiADsased -= iE == CG -J gs a he - l=o ]i - a:-.| IA | Loo A. | cBa2s9e9lP.i0Rn/eB8S0M0i1sDsaed | cB4as01e38l00i1-n0eP3cFM0HiS0sased | oB3a1so3Pl0Hn2e6Ac9M01isDsaed | o B3a1s15e3l0Ci1-n2eP7F0H0MXiADsased = men RE = - bod = =| Ba3s6e3lP.i0E/nH1ep69A.10MiDsased I TE ol i=2 E 4S03_.108/010-3P.F0H0Sa Baseline cMssed | Ba31se13l5Ci0-n2Pe7F0MH0iXsADsaed Wap pea |i | oB5a11s35eC0l-4nPe7Fc0OM0As0s2ed | Bas3e9l9P.iF0n1He80X.01MiDsased ouagg peak i. | | oB5aSs1_e51l03i4Cn7e.0oFM0FiDDsAased | Ba4s0e13l80i0/n-1eP0.F3H0MSiDsased Mopne n - | | | o B5a1s1e53l0iC4n-e7P0oF0OMAiDsased 0 Before O After Page 107 of 169 160 4 CAnoalluymtibciaal ServicesTM Created with Analyps.t4R0eporter Printed: 18/02/2010 4:02:00 PM lonm Ratiom Confirmation[ow T 7 K1001011-015 2=} | --= |i=2 | ia.| 4 iHa.| fy a -aa - mr "h Il a5y } 2B1a3se0lPi1Fn6Be A9c20Mi0sased | cBa2s6o3Pl0iFn2Pe1OM9Ai02s0saed | Bas2e0l5Pi,nF0e9SM92i.0s0sed | B3a1se3Pl0Fin1He1X9A0M2i0s8sed Wrong Peak Wrong Peak Wrong Peak Wrong Peak Ld ess fo flee | 1 ipo 3P63r031a902 0a 39P9.r0i99s020 5115.004750.0A0a cBaseline c Missed | Baseline c Missed | oBaselin o Missed | NG PFBWAraonndg PPFePakeA da not Fave qWuraolnfyginPgeaokn ansons Wrong Peak 0 Before OI After ) Na Baseline Missed Wrong Peak 1 Page 108 of 169 161 7 goin AnalyticalServices Bietetse anf bose FDRreaeasriaele CGS2riramrdoocrnagmreang menthame__ 401300 [SampleName [Kiootor [AcquisDiatteion| 2/17/2010 016 10,0201 PM rection vate Sample Type [5 Unknown | [iectTsPooFCKnnetevxLonig daam r--|[DwiaugihotntFoavcotlourre|[01800 | [[ARnea=slyutletPseakSummaroyre | ore A[nRaTERT|| mpm ae| Cie.CoCoSne. | wonton PFOA 1 Pros | 13c-PFOA 3848900 | 1.23(1.36) 68449 0.379 No. Toros | sroeono [|azoroaorn| s|r_|s o|w w~o ra PFDA 1 13C-PFDA 2786800 Towam| | 0.00 (3.08) 00 || wmNIA -- No. prost| worros| ym [a|mwasm| om ~ Pprroim | wce|rrwesso|os[ooswneaesn]| 07 | wa | w~e prrenr| oeroon| res owes| o " ByAdd a Page 1001170 ez PAYSd Lo nalytical Services: Printed: 18/02/2010 3:24:00 PM RCSwmmary TN Cri wl err T Corraam | m we|w| ma waea|] | [ser |mam| own | we wan|| msm omen [srcososrn T|oa mess || 0 weu m ||s wwoo|| mowoemn || we | [[rruaes Tasmaeenm||w mn|eow |mwoowm|| we|| PASCAnoalluymtbiciaalServices Created with AnalypRdesporter Printed: 18/02/20130:24:00 PM p-- 5 1TT `Quantitative Peak Review = -- K1001011-016 ZA a ]3 Ba41s3Pe0Fn1O6A901M0ac0ed | oB4s11s37eC.l0-n3eP7Fo2O0MAs0sed | cB4a5se3Pl0En4Ne1Ac910M0is8sed | o B4a6s1e83liC0n-/eP4F2NMA3i0s0ased B4a9se9l.Pi0Fn8Oe0S.01M0sased | o5Be10s33eC0l-n8Pe0Fc0OMiS0ssed | Bas5e1l3iP.n0Fe4O6A9M.1i0sased | B5a11s35Ce0-l4PcF7iOM0DAins0aseed - eo aes oa Fo ena) - ~ "i || ssPsF0UsN1A90100 | Baseline c Missed 561530C/-2P7F0U0DA0a Baseline c Missed | 3a caombb] fo) of 599P0F8O0S.010a Baseline o Missed 50133.C0-8P0F0OS0a Baseline o Missed FT pr: ] 50 RE cB6a1s3eP0iF5nD6eO9oA.l01is0s8ed | oB61a13s5Ce0-/i1Pn6Fe9cD.M0Os0Asaed | oB6a6s3e.Pi0n6F1e9T. M1 i0 ssed | cB6as11e35lC0n-e/PF1D6MO9iDAs0ased J T~T lingnes | ucoa Bea hon Pe 713P.0F6T6e9A.01 0a | Baseline c Missed 61135C0-/P1F6D90.0A0a Baseline o Missed 0 Before 0 After 164 Page 11201170 LCE olumS bia services Created wit AnalypstaRseporter Pred 1802/201032400PM on Ratio Confirmation K1001011-016 A d1e fn |= m= LT ci Al = | =AA] :mele | -LTA 3S. ees oB4a1sP3eF9i3nO8e8A.o2Mi0 ssed | Ba4se6l3Pi0En2eN1Ao92M0s0s0ed| Ga4s9eP5lFn0eO0S5L20h0s8sed | B5a1s3Pl0Fe2D802AM0i0s0sed Wong Peak Wong Peak Wong Peak Wrong Peak 2 h: eal o=l ill i.1 Ba5s6e3lP.iF0n2eU6A5M.2i0s0saed | oBa5s0e5Pi.Rn0eO0S5M20i0sased| Ba5s1e3lPi0Fn1DeO8A5M02i0s0sed | B6a6se3Pl0iF1nTe65I.2A0s0e0d rong ea = Wong Peak wrong Peak = Wong Peak B7a1se3Pl0iFn1Te6ec0A20Mi0s8sed Wong Peak O Before O After Page 11301170 165 PASACnoalluymtbiciaal Services Created with Analy dEporter Printed: 18/02/2010 4:02:00 PM DPraotjaeFcitle 0Ew2a1n7's10PSraomcpeiPeFsCSshwair InRessturlutmTeanbtleName __AoP2I1751000s0horrc [Sample Name___ TK1001011-016 [injectionVolume[5 | Acquisition Method|P2F7C1x8n1e2t0e1x0s4n:3o2r.4.1dAaMm |DSialmutpiloenTFyapcet.or [100 | Injection Vial [lo [weigntoveumeJoo | `RRaesyueltPseaSk ummary Anais RT Gale Gone [Praat cere | sauoso |12e02n|am |oe r| te BE TcPRH| sews0 353| 0ot0s )| ots No ras opis | samo |areazn| 1s ne | Prar1 tacoma | soso |szGan| we | om| PrripA 1 CPF| 5605200 | 614629) | 45197 017 No peru | worms |smo [ome | temo | iw wo Ssopmis | moron | so |oz@an| seo | ose TM SACPFOA | 19CAFOA| 4320500 | 7.520165)| 4323500 ww | 4 ad , Lud! 1 Page 108 0f 169 166 nalyticalServices CrweithAanatReepordter RCSwmmary ffCoreaEs TEeoawYmnIso| wommTteT |r] | a] CmoEos om = TeaTe Tm [s[omees Tromi]ne|m | Tmow mma|] 8 kmbia AnalyticalServices- Created with Analysp!.R4e7porter Printed: 18/02/2010 4:02.00PM 3k JE | TL Quantitative Peak Review ~ K1001011-016 o:f 120 =- Es 3= 353 |- 5 = i i 2130P1F6B9A0T 0a 21173.C0-1P7F2B0A0a 263P0F2P1eA901 Da 31135C-0P2FH7xX00A0a cBaseline C Missed | cBaseline Missed | Baseline: Missed | Baseline o Missed "| = || = 209P.F0B8S001 0a 4013800/-1P0F3H0S0a 313P0E2H6AA90| Da 311530C-2P7F0H0XADa oBasoliongecgMipeassed | BaselilnuencaMissed | Baseltianep: eMissed | Baselpineuc Missed - | i El | Bl He Fi -- 363P0F/H1P6A901 Da 31135C0-/P2F70H0XA0a 399P.0H/8S0.01Da 4013800/-1P0F3H0S0a tBasealinye Missed | oBasetliinngse peMaissed | Baselunigne pe Missed | -BaselT ine . Missed 4S0_31.80010-3P.F0H0Sa 511530C4.7P0FD0ADa 5S15_.10347C0-.0PFDDAa 511530C4-7P0F0OADa Baseline oMissed | cBaselneoMissed | oBaseinecMissed | Baseline Missed 0 Before O After Bre Pa111gof1e69 168 4 Solambia Analytical ServicesTM PrCinrteeadt:ed18w/i0t2h/A20n10a4t:0B2e:p0o0rtPeHr fon Ratio Confirmation r= am = l= 124 | |= zaZ we--e f=|] ip=e K1001011-016 " a He i(sh 213P0/F1B6A920 0a 263P0F/2P1A802 0a 209.P0F/B99S.20 Da 313P0F/H11X9A.20Da Bas=eWlrionneg PMeiasksed | BaseWlrionnegcPMeiasksed | uBaseWliionnegoPMeiasksed | BasWerloinnegc PMeiasksed p-- - = |= | fom =i 1 - zl 363P0F/H31p9A02 0a 30P9.H09S902Da 5S1_51.034C7P0F0DDAa BasWerloinnegcPMeiasksed | BaseWlrionnegc PMeiasksed | oBasWorionnegc PMeiasksed | NB. PFBA and PFPeA do not have qualifying ion transitions. O Before OJ After Tihsde NA BaseWlionnego PMeiasksed Page 1120f 169 169 4 Analytical Services [[SFacqpuitseitNoanmbeate R2i1o1o72t0a1r0-01107.6357 37 SarmepcloenTVyopteume [5 Acquisition Method| PFCknetextdoanmg [DWieliugtihotntFoaVcotlorume[[100000 || Results Summary E sont |E mopron | Ewoso | 1220|sm | oe w | we | Pros ncrros| seme wm |om| Frost | noeros| samo |sotamn|ant| zis Loma PriCmesrweih2A0a1n0at11e5Re9po0drto0ehr RCSummary [[sroenro moe| ve | ve [ween| | wsesre ommaamw||o ws| [|oow mmeown|| ww|] [[ersoosrsros mmaamm||owown|| wveo[|moomaenn|||| [[rsoemrso oowwaomm|| o mn|w[oomoemn|| m| [rFoasis Toowmoamn||o v |wo[|mow moemn|| ww|| [[rsaeors vowmaeno||w me w | ve ewweosm| | we e | Page2601170 i" 8 Anoallyutimcabl Services Created with Analystp5R1eporter Printed: 19/02/2010 11:59:00 AM Quantitative Peak Review : Tm A= Fy5 a K1001011-017 3= >3 - i wo i 0 413P0F/1O6A901 0a cBaseloinngecpMeiassed | Li- om 499P.F0O8S00{ 0a Baseline Missed | 41137C.-0P37F2O0A0a BaselitniengpMeiassed Ep x A 15033C.0-/P80F.O0 SDa oBaselinec Missed 463P0E4N1A901 0a 4681.03/C42-3P.0FNADa | ccBoasnelignec Missed | ocBasoelninge cpeMaissed =- "|ol = i do ph l _ 513.P0F4D69A.01 Da 5151.30C4-7P0F.D0ADa | Baseline Missed | co Baseline o Missed 5 =! fi = = aE iqpl"aw is 3 563P0FU5R1A901 0a 1635C.-0/P2F7U0R0 A0a 599P.0F/D8S001 0a 50133.C0-8P0F.O0S.Da oBaseline Missed | Baseline Missed | Baseline Missed | Baselinec Missed ia= i. Ho i] = 523 4 613.0P1F5D6O9A.01 Da 611530C/-1P6F9D00A0a 66P3F0TG6A19100a 61135C0-/PF1D6OD9A0a cBaseinecMissed | cBaselinecMissed | oBasolnec Missed | Baseline Missed +4 oor J 713P.F0T6e6A901 0a 61135C0-/P1FD6O90A0a c Baseline Missed | Baselineo Missed O Before O After Page 27 of 170 172 LR Columbiaservices PriCmerde.ate1d91w0i2t3h20A1n0al1y:t553R2:e0po0rAter =lon Ratio 7 Confirmation 0 7 K1001011-017 lE3 A ied io[ o Ge :io[iO YnR R = ae 41Ba2s.e0Pli3Fn6Oe9Ao.2M0a0s8ed | B4a6s2s.l0Pi2nN1e8Ac.20Mi0ssed | Bas4e0l9Pi0Fn5Oe9S.20M0is8sed | B5as1elP3iF0neO2o28AM0i0s0ased Wong Peak =Wiong Peak =Wiong Peak Wiong Peak = = - 5 i i Sener | LF i. JRSET, cB5a6s3ePl0Fi2Un6Re9oAM02i0sased | B5a9s3e.Pl0iR9nOe9S.c20M0s3s8ed | oB6as1e3PlF0iD1nOe6cA0M20i0ssed | c B6a6se3Pi0En/eTo1A26M9i0s0ased Wiong Pea Wrong Peak = Wiong Peak Wiong Peak es B7as1eP3lFi0nTee10A62M9i0s0ased Wrong Peak O Before O After Page 2801 170 3 8 CSoolumbia services: Created with Analyspt.5R3eporter Printed: 18/02/2010 40200 PM Project DReastualFtilTeable Instrument Name E0v2a1n7'1s0SParmopjleecsiSshPorrCts iff 021710shortrdb API 5000 SampleName |KI001011-017 TnjsciionVolume `AcquisitionDate | 2/18/2010 442.73 AM Sample Type `AcquisitionMethod | PFCrinetexShdoarmt a [injection Vial a1 | Weighttovolume[ooo | EE] wre[oIas| Bo | weer| Results Summary Tate Peak Anatyie RT Cal Gone prea acpreA |swaz0| 123020| eer 008 wo [prr|e13actm | 6702200 | 3530000)| tas 02 No PFES 1 woes | awrioo [4te@e)| rome | oo | ne | PFHXA 1 PFHpA 1 PRIS 1 13C-PFHXA | 6702200 | 5.23 (5.31) 163070 0.18 No 1cPrrs | 610200 [61620| aamse | oes | we | 1eoPrHs | 31100 [024632| ass || oa No | S_1ICPFOA | 13CPFDA| 4924800 | 7.54(165)| 4924800 1.00 No AAet "7pa,t 19 ( Page 113of 169 174 AnalyticalServices: Created ith AnalyBi Rporter IRC Summary -- rfreenin T| ow | ow | e [|mom||| [[seoeerman [smmunm||oowmm||ww w wmomw|e] we|] BCoR lumbia services Created vith Analyt5R5oporer Printed: 18/0212010 40200 PM Quantitative Peak = Review er = 2 ~ =m - K1001011-017 sw lol =| iE i= pre] - He -- CT] ee A Ba2s1e3l0Pi1Fn69Be.A0 10Miassed | Ba2s11e37lCi0-n1Pe7F:2B0MAi0s8sed | 263P0F2P1e9A010a oBaseine Missed | 311530C1-2P7F0H0XADa Baseline c Missed ny 7a BT gee ; i i - jd I ed ne diz L ge 1 209.p0r/e8s000a 4108300-11P0F3H0S0a 313P0E2H6I9A0|02 31135C0-1PF2H7X0Aa0 B--alstelaignaeeeMsissed | oBaseA linec Missed | BasMeilcinae.peMissed | BaselMinngegceeMaissed 2| J py El 3 | i] i 363P0F/1H6D9A.01 Da CBaseine c Missed | 311530C/-2P7F0H0XA0a Baselinec Missed | 399P.0H/8S0.01Da Baseline c Missed | B4a0s1e38l0i0n1-e0PF3H0MSi0s8sed Ii i=3 3 == == = = 4S0_3.108/010-3P.F0H0Sa 51135C0-4P7F0O0A0a 5S1_51034C7-0PF0DDAa 511530C4-7P0F0OADa cBaseinec Missed | oBaselneoMssed | cBaselnecMissed | Baseine o Missed 0 Before O After Page 115of 169 178 7 Solumbia Analytical Services* Created ith Analypst.5R6eporter Printed: 18/02/2010 4:02.00 PA fon Ratio Confirmation K1001011-017 om =m 1 T -N if E io=o] lon | i~ 4 - i EE ee. 3 s | tem | SESS| eel| eee 2130P/F1E6A920 Da 263P0F1P2eA102 Da 209.0P/r9o8s.?0 0a 31F30H/A112900a BaseWlrionneg_PMeiasksed | B~asWeliionneguPMeiasksed | BaseWlionnegcPMeiasksed | BaseWlrionnegcPMeiasksed ioe iE tT i= | Tots 363P0F1H3p1A902 Da Baseline c Missed | 309P.E0/H9X9.S02Da Baseline c Missed | Ba5sS1e_5l1.i30nC/e4P:7FM0DiD.Asa0sed | NA Baseline Missed Wrong Peak Wiong Peak Wrong Peak, Wrong Peak NB_PFBA and PFPeA do nat ave qualfying on transifons 0 Before OJ After Page 116 of 169 7 4 lambia AnalyticalServices" PrinCtreed:ate1d9w0i2th1A2n0a1ly0d 1F1:p53o:0r0tAeMr Project DReastualFtilTeable Instrument Name Ewans ProjectsPFCs 002211771100li0SnagmpalbesLong if __API 5000 [SaAcmqpuliseitaiomn Deate |Rr2/a170/r200170i106.617.12 PH `Acquisition Method| PFCkinetexLong dam JSmaemsptloenvTyopneume [|U 5 nknown|| Oiltion Factor [100 | Results wv Summary | wo [EE | es| | rer | PFOS 1 | 1aceros | esseoo | 2050s)| a1zse0 No POAT TCPFOA| zes0 | 000s| 0 | wa No PFURA 1 | 1sceruma| 1sss20 [ass sn 0082 No PETA 1 PFTeA 13C.PFD0A| 303910 | 5.03 (5.08) va |we] 130PRDoA| 0mi0 |sso | sw | wa No #101A0 [i Lie Page 2001170 178 Lostmn m consR rlsStr RESummary Craperenvn [ron [mr0ia||n wenw|eer]Seagn|| cvi- n|| oz rman| wm |ow |omem| a ETa Hw [eerrim |smam| | we ~ fs ww [ow | vo |omom| =] w--orn mum|wwe |we [mman| Tw Ton |ww [we | omew| ws EEI - rm sror 0 8 AnaalymtbicialServices" PrinCtreed:ate1d9/w0i2t1h2A0n1a0l1y1d:i55R9e9:p0o0rAteMr =| | Quantitative Peak Review IF) EE Haof Fl Ba4s1e3l.Pi0F/n1Oe6A9c.10Mi0sased | oB4a1s1e73l0Cn3-e7PcF2O0MAi0s8sed A ape 205 } 5 a deyBo] 2 B4a9se9l.PiF0nO8eS0(10M0isased | 50133C0-/P8F0O0S0 cBaselnecMssed 7 pol} ow | K1001011-018 Tz =| | oB4as6e3Pi0En4eN1A9c 01MiDsased | c 461830C4-2P3F0NA0a Baseline Missed = ovo Beene = - i - i| A hese J ; | o5B1as3e0lPi4FnD6eA9c10M0is8sed | c B5as11e3l5iC0n-e4P:F7OM0ADis0ased zz ass | = - A I 4 2 -l| ass ocE i [- LA] i 563P.F0U51N9A.01 0a oBaseline c Missed | 561530C/-2P7F0U0RA0a Baseline Missed | 509P.R0O8S001Da Baseline Missed | 50133,0C/-8P0F.0OSDa Baselinec Missed = ai iran ea a f- ip iJ i 3E)I iolEl 613P.0F/D5O69A.01 Da Baseline Missed | 6151.03/C1-6P0F.D00A0a Baselinec Missed | 66P3.F061A9.10 0a cBaselinec Missed | 61135C0-/PF1D6080A0a Baseline o Missed iLew i| 713P.F0T6O6A9TDa 61153C0-/P1F6D90.A0a0 Baseline o Missed | Baselinec Missed 0 Before OI After Page 31of 170 180 5 AGnlaulymtbiciaal Services- Created wilh Analyps.t6R0eporter Printed: 19/02/2010 11:50:00 AM Ton Ratio Confirmation K1001011-018 3gSaas CJo 1J al - 413,0P3F6O9A.20 0a BaseliMinsseed | 463,P0F2N19A.20 0a oBaseloMiisnseed | 499P,F0O9S92.00 Baseline Missed | 513P.F02O6A9.00a BaselMiisnseed Wrong Peak Wrong Peak Wrong Peak Wrong Peak == i =i - le = = = izChath a.Lo_ aldr e il e I= [se 563P.F02U6I9A.020a Baseline c Missed | 59P9F.0O9S9.20 Da Baseline o Missed | 513P.0F/D16O9A.020a Baselinec Missed | 663,P0F11T6I9.A20 0a o Baseline Missed Wrong Peak Wrong Peak Wrong Peak Wrong Peak 2a 713P.F0T1eA629.00a BasWerlionneg.PMeiasksed O Before OAfter Page 32.01 170 181 8 AmnaliytiacalServices" Created with Analy} 5Re1porter Printed: 1810212010 40200 PM Project Data File 0Ev2a1n7'1s0SParmopjleecsiSohParrCts wif InRessturlutmTeanbtleName__A0P2I15701000shoartb [SampleName 2K1i8G1b2i0o110ro4:1581:45 AM Sample Type `Acquisition Method| PFCkinelexShdoarmt DiutionFactor [100 [jec[tezonviar |Weihttovolume ooo `Results Summary Channtaiyiepea||smme[same T[naFiyEiEe TRT| opener | CauelCyonc | prea 13CPFBA | St0s00 | 1230120| 101120 010 | | vers No = PFHpA 1 1ICPFHXA| 6964500 | 524 (531)| 162880 No [oer| omesoo |ote6zy|sm | oe o | m S_13C-PFDA wTio0| 7550165| 47s | 100 No Ao ZF2i!P` glo Page 117 01 169 182 Lm Cre iot ntase eRepodrter ReSummary poepstone [rien[| ave wouter |Sg cots Frese [tamu [wow | ne |ieonoo| ves | [prez | emeso[wow[we | rooms | ves | Pres: ema [wee | wo | ames| ve | Prana smeen | ms |we|owen| ve | Prronz [owe [| mao | no| some | ve | pprasz [omen| ome | wo| awww | ve | ocormn | sam| soo|we|swoem[we | scema |sues | ess | we [amir| we | Page 10100 ps 8 Glumbin Analytical Services PrCirnteeadted18w/i0th22A0n1a0ly4!0pR26e03p0ortPeMr `Quantitative Peak Review = = 3 Eg K1001011-018 J 33 s Bg | L i: 3| i -2B1a2sPe0ir1nos6n8Cv0ii0n8sed | Ba2se11l7ai0cn.1eP7Fo2BMA0s0sea | B2a6se3ple0ip2nee1.00Mi0s8sed | oB3asr1e5lan0e2c7eM0i0s0ased == | iA= Lo ea iL a. c2a0s5pi0rn6eo0sM0Ti0s8sed | oB4a0s13e8l00-n1pe0Fc3Fi0MS0is8sed | Ba3se1lP3i0Rn2eA68T0Mi0s8sed | oB3as11e35l0n0.e2PcF7HM0iDAs0ased 1 ie =1 tye i == iwi io| i=M Ba56Pc3.ri01oo16n8o.M10t0saed | oB3a1s15e3l0n2Ce7Po0MH0iAsDsaed | oBe3s0ep9l0rn8ie0sc.0M|0is8sed| cBa4s0e13l60i0n1ep0F3H0MSi0sased "f| h=e i=i i =| a 4s0_3108100P3F0H0sa Casale oMiseed a | oB5a1s15e30i04.n7p0MF05iAsDsaed | =|SS_11530c4.7F0F0o0Aa Baseline Missed ol | =) 5115304.7p0F0ADco a 0 Baselne o Missed 0 Before O After Page 119.01 169 184 SAnoalluymtibciaal Services p.6s PriCnrteeadt:ed18w/i0t2h/A2n0a1l0ys4t:0R2e:p0o0rPteMr --fon-- Ratio e Confirme ation K1001011-018 N TE 2 PJ N1A | E o : 1 1se fooEf E 2130P1F6BA920 Da oBaselMiisnseed | 263P0F2P1E9A0202 BaselcMiisnseed | 20P9.F0/E9S9.20 Da cBaselc Miisnseed | 31P30H/A1129D0a cBaselo Miisnseed <Wong Peak Wong Peak Wrong Peak Wrong Peak :5 . oa 5 5z foe =-- [= Paapitudts 363P.E03H1p9A.02 0a oBaseline Missed | 309P.F01H9X9.S02Da BaselwMiisnseed | 5S1_51034C7P0F0DDAa Baselc iMinsseed | NA Baselc iMisnseed Wiong Peak Wong Peak Wong Peak Wrong Peak NB PFBA and PFPeA do nl have qualfying on Transitions O Before OJ After Page 120 of 169 185 3 Golam AnalyticalServices Reteeit sta65otre RreaavaaTate SoGaToro1FsooanRmysonigt umn hame__ op 3500 [SampleName --TRiooiori078 ET (`Acquimsitioen Metch1od&|t62P1F7C7h2o0i1n0e1ln0e2x4L4dov3anmPgMar|DiwSlaeumgtpihloteniFToaycvpteoourme Jom | | py ene Results Summary Analyte Peak |oes [ET `Analyte RT pron vorron |ww|1w :30| [pprrousar | evorrrros|| owvoom|[aawwaaoonn|| Front iorron | moon omam| prt | orto| mo [asm| PROS 1 13C-PFOS | 9540700 | 3.89 (3.87) mparro || owoeerroooens|| wwmw [[osoweasms| Pret | cero| wom |owssn| arenes| CH Calc. Conc. | w_e-- a sso | are " wowmw | |oowm| w 0 | wa| w mrEEam | we 6173 002s | No o[w | a wwe | 0 | wa | we Lreecen?e as [-- Ten nalytical Services mii Created withAnalyh poner `wesummary Trnapereni|mwsry| an wean |oe gi | icons| [sois.pron Tormnz wo [emam| aw|awew| we | omow| w bros: [sisorros roam| --_-- 2am| wow |we |swa| rve m| Sows oro sm|awmm| we | vee | asus| wm | wo| warm | we | 8 SAnoatluymtibciaal Services- Created with Analypst.6R7eporter Printed: 18/02/2010 3:24.00 PM Quantitative Peak Review im Tw 8 =A :A "| K1001011-019 T =7 | f= 205 = 413.P0F1O69A.01 0a 411730C3-7P2FO0A08 Baseline c Missed| oBaseline Missed | 463.P0E4N19A.10 Da Baseline Missed | 4681.30C/4-2P3F.N0ADa c Baseline 0 Misoed 499P.F0O8S001 Da 15033C.0-/P80F.O0 SDa Baseline: Missed | oBaselince Missed | 513.P0F46D9A. 1 Da 511530C4-7P0F0OADa Baseline Missed | o Baseline. Missed 2daedeWfI EE Z Lc " a " h = = he promsgea] Ue - | 563P0F/U5N1A901 Da cBaseline oMssed | 561530C1-2P7F0U0RADa oBaselnec Missed | 509.P0F/D80S.01 Da Baseline Missed | 50133.0C/-8P0F.0OSDa Baseline c Missed - Was pes Woo wang = Ll A3 vo Ld 5. 1 |- 520 " 6130P1F5D6O9A01Da cBaseineoMssed | 61153.C0/-1P6F9D.00ADa oBaselineoMssed | 663P06F1T9A.T00a cBaselnecMissed | 6113500-/PF1D6oD9A0a oBaseline Missed ~ - a8 pr 713.P0F6T6O9A.01 0a 61153C0-/P1F6D9O.DAa0 Baseline o Missed | o Baselineo Missed 0 Before O After Page 124 of 170 188 LSS AnalyticalServices- pCireeated0w3ith3An0al1y 0F3db3o02rt4er fon Ratio Confirmation K1001011-018 Tw 7 =7 = | || | == o\ o=l | za| TDA| Seen Ba1se3l0Pi3FneO8A320M0is8sed | Wong Peak B46a30Ps2FN1sA8c20Mii0s8sned | Wong Pea B4as9e9lPi0Fn9eOS0M20i8ssed | Wiong Peak c B5a1se3Pl0iFn2eD892A0Mi0s8sed Wong Peak 2 7 -2!Lnfran i[ -| 2 ii=z =i7 Ba56s3Pt0Fi2U6nA902Mi0sased | oBa5s6e3Pi0Fn9Oe8S.o20Mi0saed | Wong Peak Wong Peak Ba5s1el3Pi0FnD1eO8A9M02i0s8sed | Wong Peak Bas63e.P0l/i1F6n9T.e0 2Mi0sased Wiong Peak = B7as1eP3lFi0nT/eE1oA62M0i0s0ased = Wong Pea 0 Before OJ After Page 12501170 189 /AnlaulymtbiicaalServices Created with Analyspi.6R9eporter Printed: 18/02/2010 4:02:00 PM Project Data File 0E2w1a7n1'0s\PSraomjpelctessPShFoCrst wit IRnessturltumTeanbtleName __ 021710hort API 5000 db [[S[aAcmapuilseiNtoanmDeat--eTk|io27o19i7a20r10i5o0s778 Al Sample Type `Acquisition Method | PFCKinetexShdoarmt [infectionVial Tes || WDeiliugthiotntFoavcotmourme[[ 700ooo]| m i Resul-- ts TSuo-- mTmar-- y ----e-------- eee-- eee------e [nBaiaytend Peak [stm [same [RAEnaEisERRTT T mraenes|GCalEe CEone | weamnova = 13CPFBA | 5210000|1.26(1.27) No [preeas| racer| esoram|ssecoon| terse 021 No 160PFHS |s4s2|4020000200)| 197950 014 No | PrHXA1 1cPRa | soereon [52563| zoo | om | me | [prrpat | racer| eesrao0 [s1629| eooat 022 No [pers 1 | tsoprrs| sssos0 omen| smo |os| we [sacproa | raceron| sina| 7ss(es| arras[ en wo | we | xa zStu5sie Page 121 of 169 190 ee AnalyticalService Cote: CrweithAanaltytepodrter ISRuC mmary [rosmani rom||m me |e we||Sn mEom|_|| [[eersoemrom||mwwwamw||swwe[o[[aesmrommn|]ewvem| 4 SAnoalluymtibciaal Services" Created with Analyspt.7R1eporter Printed. 18/02/2010 4:02.00 PM Quantitative Peak Review = 7i TE F- Esl | j Ki001011019 "[ TEE - | Foi [ol 2130/P1F6B9A.|0 0a oBaseline Missed | 211730C1-7PF2B0ADa Baseline C Missed | 2630PF2P1e9A0|0a Baseline Missed | 31135C0-1PF2H7X0DA0a Basiec Missed 4| : -y 62% - 1 A 535 - = Ih a. | 266.P0F/8B0S.010a cBaseline c Missed | 4013800/-1P0F3H0S.Da Baseline c Missed | 313P.0F/2H6A9.01 0a Baseline Missed | 31135C-0P2F7HX0DA0a c Baselinec Missed lL - } ol iW dng | ol 363P.0F/H1p69A.01 0a 311530C1-2P7F0H0XADa cBaseline c Missed| cBaselie c Missed bJo= 675 phooET i= Fl aii .l=i dpe | 399P.F0H/X8S001Da | Baseline Missed bal ge I ali=!] = - 4013800/-10P3F0HSDa | Baselinec Missed p=poof oa il 4s61300/1e03r0sDa 51510340.7p0F05ADa 5s1_51.034c7F070o0na 130.PF5A 5150470D0a uBaseinec Missed | Baseline oMissed | Baseline cMssed | o Baseline c Missed 0 Before O After Page 123 of 169 192 LSCSoluombaia services: PriCnrteead:ted18w0i2th12A0n1a0ly4:0A2B:p0o0rtPeMr Ar ols ME = lon Ratio CTornfirmation 3 7 = K1001011-019 I i. |- 21P3F0B16A3200a BaseloiMinsseed | 263P,F0P21e9A02 0a Baseline Missed | B2a09sP,Re0E9Scl92.Mi0i0snseed | Wrong Peak Wrong Peak Wrong Peak TR = = ot = i | | mosis fn Te aA dren oB3a3P0sF3He1p9oAi0M2in0saseed |oBas30e9P.i0Hn/9eY9cS.0M2iDsased | coB5S1a5_.1s031C4e7-c0Pl.MF0iDns0Asaeeq | NE PF EWraonndg PPeFaPkA do nol Fave QWuraolnlgynPgeaokn Tarsilons Wrong Peak Ba31sP3Ee.H0Alc1AMi12i8Dsn.saeed Wrong Peak Dispute NA BaselinesMissed Wrong Peak 0 Before O After Page 124 of 169 193 4 Solambia AnalyticalServices Greated with Anlyspi.7R3eporter Printed: 18102120130 24:00PM Project Ewans ProgaisiPFCs Data File 021710\SamplesLong wif Result Table 021710i0ng.10b Instrument Name __API5000 [SampleName T1001011-020 Acquisition Method [injectionVial Jae = Injection Volume [5] Sample Type | WeighttoVolumeJos | Results Summary fTinaiyte Peak shame |sarea| FAiTgEsRRT| nay area GaaleiCmone _| Mod-es? PFOA1 I= [Prosi [ proAt | 13C-PFOA | 3984000 | 123(136) | 94eas0 | 4700 | No | aes0600|205208)| 17292 00s No | 1ICPFOS | 8043300 | 209209)| 371500 | 0447 No 13C-PFDA | 2639100 | 000(3.06) o | wa No |--pros 1 {pFTiat {PFTeat 13C-PFOS | 8043300 || 3.93(3.87) 2601 0023 [cproon| woos [stoeom| am | wa | | 13c.prDon| 14050 |5.73551) 5 Too 0 No Ne | wo | Aa0 IZ hr Page 126 of 170 194 / Soumbla AnalyticalServices PrCinrteead:ted18w/i0t2h/A2n0a10ly3:2A6:p00orPeMr RCSUMMGry [ros va |wor| | aoa | | [ovemn oman|| wo| mom| | [ocroeors [oamoamm||wom||owwe ||mmeoewn||Cew || E rmleTommom| 0 |E w |oT mow|E nw | [[rroosss [oommeomn|00 || we [|oowmoemm|| mn || rs sw | we |ow | omom| wo ] 4 GAnoalluymtibciaal Services PriCnrteeadt:ed18w/i0t2h/A2n0a1l0ys3tp:27R4e:5p0o0rtPeMr `Quantitative PeakReview wm v= = K1001011-020 pl z 3 - == 205 il- -- -- bo ae " geen) c4B1a3se0Pl1Fin6OeA9:01M0isased | Ba4s1e13l7Ci0-n5eP7Fc2OMA0is0sed | cBa4s6e3lP0iE4nN1eAc90TMi0sased | cBa4s6e1l83iCn0-o4PcF2NM3Ai0s0ased : Ll = A 2 3A = A- Bas4e9l9Pi.Fn0Oe6S0u10MiDsased | oBa15s03e3lCi.-n0Pe8F00OMSiDsased | Ba5s1e3l.Pi0Fn46De9cA.1MiDsased| cB5as11e53l0Ci4-e7Pc0F0OMAiDsased LZ se |~ S pr od - uBa5s6Pe3F.l0iU/vR5e1A9.01Mi0sased | oB1a6s3c5Cl.-i0Pn2Fe1oU0N0MAi0sased I a -- a0 oii i i: i 5 Joe CB6a1s3ePl0Fi1nD5eO6Ac901MiDsased | B6a11s53e.lC0i/-n1Pe6F9D.0OMDiAsased z = f=T ag i; | Bas5e9l9.Pi0nF/eD80Sc.0M1s0saed | c B5as01e33l.iC0n-3e0P.cF0OMSiDsased 4000 Peak yg pe iow | - 519 = | Ba6s6e3lP0iF6nT1eG9A.01MiDsased | Ba6se11l35iC0n-e/PcF1D6MO9iDAsa0sed = PE A am |= 713.0P/F6T6O9A.01 Da 61153.C0-/PF1D6O9A.0a0 Baseline o Missed | Baseline o Missed O Before O After Page 128 of 170 196 LSCSoolsuembrivaices: Created with Analy7R6eporter Printed: 18/02/20103:24:00 PM El Z lonER Ratio Confirmation= = I aw 2M EN 0 = K1001011-020 lo |z 413P0F13O6A920 0a 463P0F2N1A29Z0 0a 493P0F8O9S.20D8 513.P0F26D82.A0 0a _ BasWelrionnegcPMeiasksed | oBasWerloinnegcPMeiasksed | BasWerlionnegCPMesiiscsed | BasWelrionneg PMeiasksed =z ntalfi o El| i -| fo egaggies | "pgp [| ewspagasagias| Lempert 56P30F/2U60.20 0a 50P9r00O9S9.2008 613P.0F1O16O9A.020a 663P.0E11T2630.0a CBaseWlrionnegMPiesasled | oBasWerloinnegoPMeiasksed | BaseWlrionneg PMeiasksed| oBas<eWlirnoeng MPeiaslsed 71P3F0T1eA62900a < BasWerlionnegcPMeiasksed O Before OJ After Page 1200170 197 8AnSaollyutmibciaalServices" Created with Analy7R7eporter printed: 1810212010 4:02:00 PM DParotjaecFtile E02v1a7r1t0s:PSraompRlCeIsSsPhFoCrSt wit RIenssutrlutmTeanbtlNeame __A0P2!15701000shoartb [[S`aAcmapulseitNoanmDaete | 2[R/i1c9o21001107-502100: Al [inSjaemcptlieonTVyopeume[5] Acquisition Method| PFCneiexShordam 700 [nie[cs+ionvia|Wegniovoiume [om ReASnaslytuEe ltPseaSk um|mnaray me| ams |AnaRiyEteTRT| pnts | GlCeHGSone | aan PFBA1 | 13cprea | sterso0 | 122(1.27) 89084 0.10 No [Prreat | 1scrrrua| eesetoo| 353060| 139s40 oz No Pros 1 180-pFHS| 3063000 | 420626)| 201600 016 No [roar osm |sown [erom| om |ox| pris 1 100PFHs |des|60 256032 | sr |oa| : Aaw Ioah " 2/19 Page 125of 169 198 AnalyticalServices rRCSOOMary Crwein AanattReepordter mens own|mn| mem| ow] [[seccoomns [|msomemm ||ssoowm||ewe[omsamn||ew]] Golumbia Analytical Services" Quantitative Peak Review . 7| dl T|E z: 3 PrCinrteead:ted1w8i0th2A2n0ai1y0bi24:B08e2p:0o0rPteMr K1001J0I 11-020 o B2a1s3elP0i/Fn1Be6Ac910MiDsased | Ba2s11e37lC.i-n0e1P7Fc2B0MAi0sased | oB2a6se3Pi0Fn2Pee1A90M0is8sed | c B3a11s5e30lC7i-n2Pe7F:0H0MXiADsased I | | ii o2B9as9e.lPi0Fn8Be0S(01M0i5ssed | o B41a0s83e0l0i1-n1Pe0cF3H0MSi0sased | oB3a1s3eP.i0H2n5oA9c.0M|i0s0sed | o B3as11e3l5Ci-0neP2F7HMX00iAs0ased 4 J 5 = Ba3s6e3lP0iF1n1He6Ac90M1i0sased | oB31a13s5Ce0i-n2Pe7Fc0H0XMAi0sased | B3as0eP9l.Fi0ne8001MiDsased | c B4a0s13e80li0/n-1eP00F3H0MSiDsased A gs bre LE . = | - i i) Ii =! il Ba4sS0e_3l1.i80n01e-0oP3M.Fi0Hs0Ssaed| cB5a1s15e30lC/n-4eP7cF0MO0iAs0saed | cB5aS1s_3e.1i034nC7e0-c.F0MDi0Asased | oB5a1s15e30iC4n-e7Pc0F0OMAiDsased O Before O After Page 127 of 165 200 7 Solumbia Analytical Services* Created with Analypst.8R0eporter Printed: 18/02/2010 4:02:00 PM Ton Ratio Confirmation K1001011-020 i | 3 2 T7 z pole | tA) J Tr 213P0F/1B6A9200a 263P0E2P1E9A020a 2690P/F9B9S.02 Da BasWerloinneg PMeiasksed | BasWeilionneg PMeiasksed | c BasWerlionneg PMeiasksed Ba TT . oo i |=r ds 313P0FH/I1A1020.a0 | c BasWerlonneg.PMeiasksed Tipe 363.P0/F3H19p.A0 2Da 309P.F0/H9I9.S02Da 5S15_.01/347C0.P0FD0Aa BasWeloinnegcPeMaiks.sed BasWeilionnegGPMeiasksed BaseWlrionneguPMeaiks,sed NB. PFBA and PFPeA do nol have qualifying on transiions. 0 Before 0 After NA y BasWeilionnegcPMeiasksed Page 128 of 169 201 / Solumbsia AnalyticalServices" PrCinrteeadt:ed18w/i0t2h/A2n0a10ly3s:P2R4p:o00rtPeMr Project Data File E0w2a1n7'1s0P\rSoajmepcltessPLFoCngswif! IRenssutlrtumTeanbtleName __ 0AP2I1751000i0ong.1b [SampleName __|KQi00066M4f06 201772010 11:17:36 PM [mectionVotume SampleType [ [Un5 kno] wn| `Acquisition Method|PFCkinetexLong dam Dilton Factor [100] injectionVial 50 WeitogVohlutme [000 | Results Summary [[nnaaiyate Peak [ismome [sama |T AAnEaMEiRsT[RT avapeaes | CoaleoCoone Modified? PFOA 1 13CPFOA | 4027100 | 127(13)| 2838 No | PFNA1 PFOS 1 13CPFNA| 2474900 | 2.07 (2.08) ht A ogy | No 13CPFOS | 8130300 | 208208)| 88793 07 | No PFDAT 1oProA | zumo0 [omaos| 0 | Na No PFURA 1 1CPFUA| 132050 |3sse0s)| toste |os| No PFOS 1 | 13cpros seseen| mm oss | No PFDA 1 13C-PFDOA 4.54 (4.55) a CE ors No PETA 13C-PFDOA| 146830 | 5.16(5.08) No Zz = 218 iw Page 1o5f1070 202 5 lumpia ticalServices" PrCinrteead:ted18w1i0t2h1A2n0a1l0y3Bt24AR0p0orPtAer RCSummary [ AnaytePoak Namo [sPreoAm2 en [errrm [rsoommses [remram RTEpRT)| Ama |Moditeay|CHSIETHRN|Ral Conims| mom| 000(1.38) oow r |[ we Jonw ]|ews e || Comoaawn||s0n || wweo||ooomaemm|| w || T|ommaom||wowem|| wwe[Jommwreann|| we|] [somoomw||wa0rs ||wvoe[ooewmn|| ww|| [[rcooscso Toemsmaenm|| w0en||ewe|ommownw| || | r[J mrosa e [amen s|s|e we[[n ooooom| |e w| e | Page 151of 170 203 Columbia 8 Roam services: PriCnrteeadt:ed18w0i2th12An0a1l0ys3:t2R68:B0o0rtPeMr EE Tw 3 Quantitative Peak Review = | 7 iDm=t ow |ST KQ1000664-062 Le 41P30F1O169T0 0a caseinec Missed | 411730C3.7PF2O0R00 oBaselnecMssed | 463.P0E1N1A8.|0 Da oBsselnec Missed | 4681.301C2P3.F0A0a oBaselnec Missed ER] hizE . = 207 i: i: - - 7 : 3 os el [| mre Tv id nea | 459P.F0/O8S0.100a Baseline Massed | 5013.30C1-80P.FOSDa cBaselnecMissed | cB5a1s2eP.iF0nD4eA6c91M.s0s0ed | cBa5s1e15l30iCn4-e7Pc0F0OMAi0sased 5 aan 2a gps - fingpea EC = Loni 3 i= i= 5P63F01U519T0 Da oBaseine Missed | 56153.c0-2p1F0U.n0A0a oBsselnec Missed | 599P.R0O8S00 0a cBaseinecMissed | 50133.00.16207.38Da oBaseine c Missed = viz "hog umes "sungpe lii| = ast ffEf o1 i -I=l se i|| Ba6s1e3l.Pi0F1nD5e8O9Ao.M01i0sased | o B6a1s15e3.l0Ci/-n1eP6F5MD.i00sA0saed | oBa6s3e.P0iE6nT1eA9cT.M0i0s8sed | o B6a1s1e53lC.i-n0eP1Fo6D5MODi.Asa0sed = To Zl Lp FT Yo 713.0P18E6T9.A0 0a 61153C.-0P1F6B9o.0A0a oBaseine c Missed|o Baselinec Missed O Before O After Page 1520f 170 204 LColb umbiaservices PrCirnteeadt:ed18w0it2h12A0n1a0ly3t.24e:p00orPeMr lon Ratio Confirmation KQ1000664-06 1 ESyy = a3 i= oz = = 2 = d [i=| nat Thee | Cen| SAY Loe, 413.P0F5O6A9.0 0a oBaselne o Missed | 463.P0E2N1A92.00a Baseline c Missed | 495P.F0O99S0208 Baseline o Missed | B5a1s3e.lP0iFn2e6D862.A0Mi0sased < Virong Peak a Wong Peak Wrong Peak Wrong Peak Ll = Ea 2 cf |i = = i- hme| oBa5s63eP.l0iF1nU2e6A9cA.20Mi0sased | oBa5s9o3Pi.R0nO9eS9c2.0Mi0s8sed | oB6a1se3Pl.Fi0Dn1Oe6cA5.M2i0sased | Ba6s6e3l.Pi0n1E1e6Tc9.A20Mi0sased = Wrong Peak Wrong Peak < Wrong Peak Wiong Peak i 1 Nem o B7a1s3ePl.Fi0nT1e6eo9A.ZM0i0sased <Wrong Peak O Before O After Page 153 of 170 205 OSColumbia services [--.- Printed: 18/02/2010 4:02:00 PM PJ aewveotae CEGoomvonr csaaanmimr aearoint Mmeaame tp 500 [SampleName |K2a11t8o/o20o1e0s6&:0068:10 AM. A ecionvoume Sample Type [5 Unknown. | [`AcquiisitjionMeethocd[|8PtFCionetnexSvhodraitm ar [WewhttoVotums 700 [000 | R[aeTsapauglratos Snuim|marsiyenrrea|[ smens| R1a 2E0R0T2Y0 [ tyes| wwonsly [w~oos orn| oun[sso| wm | om [we | Pros1 | ores o[wwons[a[wseew|| swee [| owao| ~we | Frnt own [oom| ww | wa | w [srwsotre || wToeroeeerosn || wserno[aommeens|| esemen | oe = ccrron | orion| wo | rom| wome | | we | oF LIglo ae ar188 xs ASolymbleS,ervices Created with Anal Reporer Printed: 18/02/2010 4:02:00 PM RCSwmmary ([rorr r[opreens mez PFHpA 2 cceorren [rasan | saw | me wm |ow [moon | | oowmeenn||oo w[oomww eenn||wn]| 6.13(6.22) 35089 No | 3.331290) YES om | some | ne mm | m w-e | 5 Goma Analytical Services- PriCnrteeadt:ed16wi0t2h2A0n1a0ly4s.P0R2E.p0o0rtPeAr = Tw Quantitative Peak ReviEeE w 7 -- KQ1000864-06 i I oo B | E xI: fioz| uK m filL _ < G2o1s3e.Pi0Fn1oB69Ac.T0Mi0sased | o B2a1s17el3.iC0n-4eP72F0BMAi0sased | oB2a6sPe3Fl0Pn2ee1cA910M0ss8ed | Ba3s1e1l53i0Cn-2eP7F0=H0MXiA0s8sed i E EA B c2o0a5s,tP0i8Rn0Be.Sc01M0aased | oB4a0s31e.80l0/n-1Pe0Fc3H.MS0s0s8ed | o3B1as2eP0lH2ne6Ac01M0i0ssed | B3a1s1e35lCi0-n7ePcF2H7MX0iDAs0ased rg -- ER TE i= i i== :i Loosen LR PT RA A Ba2s6e2lP0iF/nH1ep6Ac90M1i0s8sed | Ba31s1e3l5Ci0-n2Pe7F0H0XMiA0s8sed | oBa3s9eP5Rl.Hn0Xe8S0c01M0issed | Ba4s0e1l38i00n1-e0Pc3F0HMSi0sased 7 i I pe i zl 2 i= 2 3 zl = = cB4aS6s3_.t10i81n010-e3Po.FM0HsDSsaed | oB5a11s35eCl0-n4Pe7Fc0MO0iAsDsaed | oBSaSsi_e51i03n4Ce-7cP0bF0iDDsAsaed | Ba511s530Ce4-7lPo0FM0iDiAsDnsaeed 0 Before O After Page 151 of 169 208 SAnGaollyutmicbaila Services- PriCnrteead:te1d8w0i2h12A0n1a0lp4y.0oR28e0p0ortPeMr Fe Li lon Ratio Confirmation Ih2 fo oe 3 Z KQ1000664-06 eee cB2a1s3el0Pi/Fn1Ee6Ao520Mi0s8sed | oB2a6se2Pi0Fn2Pe1Ec9AM02i0ssed | oBa2s0e5Pl,Rn0Ee9Sc82.M0is0sed | cB3a1s3P0Re1H1loA6Mi20i0sn8seed Wrong Peak = Wrong peak = Wrong Peak Wiong Peak = J ci } z= Perdis o3B6a3seP0iF3nH1ep9cA0M2i0sased | Ba3s0s9P,iF0nH98I.MS0i20sased | Ba5sSe1_l51i3n0eC4P7MFiD00sA0saed | NA 0Saseo lMinsseed NB PFBWAraonndg PPFePaekA Ga nol have WquraolniginPgeaokn ans ons. Wrong Peak Wrong Peak 0 Before OJ After Page 15201 169 200 LS RCooltumibmiia services: Created with AnalystiR8florter Printed: 18/02/2010 3:24:00 PM DParotjaeFcitle GE2a1r7s1P0rSoaamopPersCtsointg IRenssutlrtuTmeanbtleName_ AG2P1!7150000o00g100 gor |i |we [| a| og | er | |[SRacmapuliesaomnDeats TR2G1r7o206078861.15%GEEPTHC [SamspleTeypeto[[ 5nvaooranm]e A -- i TT C-- X `Acquisition Method| PFCKnetexLodnagm [Dilution Factor [100 | - FRevsulPtesakSummary ART Sic Gore - stant rot eon| wooo [asm|sw | re es | ror| zoom| zoe| soo |wm| ros raarron | arn [zviam| vows | mew | me | [rromt II) " [roms | oro| rams | ssiaon| ssowo | zee 0 sro PFDS 1 acre|vom [sss| [iscpros | or23700 | as1aen| ww | 113s3000 | mom11.000 | wNoo itz (gle Page 14801170 210 | um lyticalServices: CrweithAanattReepordter Printed: 18/02/2010 3:26:00 PM `RCSwmmary rroon:ms[[wwinn|[ rom |e 0|[av gwaow|wn wme|| raz 20s| teen [[oromsse [oewwaasn|| mu0m || wwoe||oommeomw|| wwee || [sere avam |wae|woman| ow ] [[ rmsemorwor m ||wo memnn||w[ voo|mvowaem rn||oen|| [ross ewan|wom | we|owes | we | [rr osm|sme | vo | wen|e | & ACnoalluymtibciaalServices PriCnrteeadt:ed18w/i0t2h/A2n0a1l0y3st:i2R68.f0l0orPteMr Quantitati7v%e Peak Review 7 =- A i= i Peers ae o B4a1s3ePl0i1Fn1Oe6A<9T0Mi0saced | oB4a17s3e.Cl0-n3Pe7F2O0MAi0s0sed = Cl i= pl KQ1000664-05 z A}. i= pou -- | cB4a6s3eP,l0iE4nNe1Ac3.1M0i0sased | o B4a6s81e.3l0iC1n-4e2P3oF.N0MAiDsased =2 iE pi IE a i N - Ba4s9i9p.nr0go80s-01MDiased | oBa5s01e33i.C0n-1eP0cF0OMS0issed | cBa51s3e.lP0iF4nO6e9Ac.10Mi0sased | c B5a1s15e.3l0iC4n-e7Pc0F.D0MAi0sased x El i ii A Ba5s6e3lP.iE0nU5e1R9AM.10is0saed |oBa5s61e53l.Cn0-e2P7Fo0UM0RiA0sased i- i=E J zl < B6oP1s3Fe0lD/n5Oe6Ac910MiDsased| cB61a13s5C.e0-l1P1n6Fe3Dc.0M0sA0saed | oBa5s05eP.i0Fn1Oe8Sc0M01i0sased | c50B133a.C0s1-8Pec0FlMOiSiDsanseed i7= iE he xl | oB6a6s3eP0iF/n6Te1oA9MT0i0sased | oB6as11e35lCi0n-1ePF6D9MOi.0Asa0sed 7 Lo = =xt le Ar - a er 713P.0F6T6E9A.01 0a Baseline oMissed | oB6a1s1e53lC.n-0eP1Fo6D9OM.i0As0ased O Before O After Page 148 of 170 22 8An5aollyutmibciaalServices- PiGnreda:ted18w/i0t2h1A20n1a0if3t:2R6e.p0o0rter F fTon RRatio Confirmatioo n y eeeKQ1000664-0e 5 ee eee Tw 33 > 3 = |Doak fi| = B sl: El Io = Eh oBa4s1e2l.Pi0Fn3O6e5cA.20Mi0ssed | oBa46s3e.lP0iE2n1N9eA.c02Mi0sased | B4as9e9Pli,Rn0Oe5Sc82.M0is0sed | B5a1se3lP0i2Fne6O92A.M00aase Wiang Peak Wang Peak WongPeak Wrong Peak a Ty cBa5s6e3Pl0Ri2Un6eR9oA.02Mi0sased | < Wong Peak i =| = 1 1 B5as9e9PliF0nO5eS9c20M0i8ssed | oB6as1e3Pl0Fi1Dn6GecA90M2i0sased| o B6a6se3Pl0iF1nTe6oA920pi0sased Wrong Peak = Wrong Peak < Wrong Peak = B7a1se3Pl0Fin1Te6e0A020Mi0s8sed Wong Peak 0 Before 0 After Page 1401 170 a 4 Solumbia AnalyticalServices PrCinrteeadt.ed18wi,t0h2A1n2a0l1y0s4t.R0230o0rPeMr Project. Ewan's Projects\PFCs RIenDsastutarlutFmiTleeanbtleName __Ac0P22111751T00i0\0S0asmhprloaerbsShort wiff [SampieRams TRGo0068608 [25 [npectonVorame [5 | "Acquisition Method| 2P/F1C8K/i2n0e1t0ex5S:h5o8r:t36dAaMm SE ampleC Type E[E Unknown| [iec[t46onvial [Wegntiovoume [oo | rRR=vessulPtes[akSuemmanry e|oes[eAnrdieyRT| mvs| CgatuelColne" [wear EX orton | sso | rar| veo |wo| rrro| nrmta | omen [amas| emo| wo | we | [Prat TacPra| sr2es0 | 522630| 12013000 020 prron1 | sore| om |sviem| me No 0 sreorms | rcrron| arsss0 | 621630| 3838000 00 SISCPFOA | 1SCPFOA| 4759500| 7500165)| 4759500 00 u | i oo" glt EA Page 145of 169 2 4 Ss,Services: Created with AnayBi Reporter Printed: 18/02/2010 4:02:00 PM. RCSwmmary (rere |[nere | gn| Proaz [rows [sr wamz ||wwea me||m wmee ||owoomm|| evees || Prinz [orzo |wenn|wo |awe | ve [sseremron Toomom||oamne||wwoe ||oomaannm| | wem] 215 5 Gomis PrCereda.ted18w0it2h/2A0na1l0y4s0t2R,&0o0rter Analytical Services BE SBS PI = Quantitative Peak ES Review -- 7 KQ1000664-05 i- isEl i== i| o21a3p0r1ne69d.M0n0s8ed | 21T7a0c7P73F.E0 08 casing Med | c2a6p3sr0sp2ie1ei00Mi0ssed | 3113500p7F0A00a oBaseineo Missed in ie rr ie i i i= i. ca2m6e6ip0nre0s0oT0M0ses | oB4a0s13e8i00n1Pe0oF3li0iSs0sed | oB5as1e3Ple0ir2ne6o80M0is8sed | 4115300720F0A08 oBaseine o Missed i= | i- i| o2o63P0rn/H1G6Ae9v01in0caed | ca5s11si5c0np2g7io0M0ni0saed | cGa3ps6er6i0nie8s0c01M0s8seg | oB4a0s19ei00n10e1c053M70i0s3sed id (2 El i of4ss5s1i3i00n1g005o5N0isBnased | oB5as1ti5ia0np4i7M0is0s0ed| oB5a51s5e10i31n40e75o070M0s5nsaed | oB5as1ao5i0cn4ep7o0i0Mi0s0sed 0 Before O After Page 1471 168 216 PAS ACnoalluymtibciaal Services Created ith Analpy9R6eporter Printed: 18/02/2010 4:02:00 PM Tm Tw lon Ratio Confirmation ; 4 | =3 | i = lL |S ; - 7 KQ1000664-05 | T == h=e oB2a1se3Pi0Fn1eE6Ao8Z0Mi0ssed | oBa26s3eP.l0Fi2Pn1oe9o.A2M0isased | B2as0e5l.Pi0nF9eE9So20M0issed| c B3as1oPl3iH0ng1Ao1M290is0ased Wiong Peak Wrong Peak Wrong Peal o Wang Peak Er) : Fo i I] Cen fr Ie fl = | Tigre oBa3s6e3Pl0iRn3He1Gc9A02Mi0sased | oBa3s9ePl9i,En0eH9MS9i.2s00sed | Wrong Peak Wrong Peak B5as1s5_e.l10i34neC70Po,F0MOi0Asased | Wrong Peak NE. PFBA and PFPeA do not have qualifying ion transitions. O Before 0 After NA Baseline o Missed Wrong Peak Page 148 of 168 a7 8CRooluutsmbeiravices: CrweithAanaltystReBfodrer Printed: 18/02/2010 3:24:00 PM Project Twas ProecisPrCs InDReassttuarluFtmilTeeanbtlNeame __ 0cA2P21I1T75110000l\0oSnagmaoplesLong wiff [Sample Name KaT0oo00 0eei7 0s7% [A`cAqcuqiusiistitiioonnDMaettehod ||2P7F7C2K07n0et10eSxLEodEnaFgmI Sample Type [DWieliugthiotntoFaVcotlourme| [10.0000 FiRreasiusltPseakSummarwyine [sa A[nsEeTRY | es | iseeEan | wearer | Pron 1 TSPFOA| ae3s0| 1250139)| 4m000 | 24300 No EX T3CPRNA| 2766800 | 208208)| 12547000 "1700 no PrUnA 1 Pros 1 PFDoOA 1 Tort TaCPRUMA| 121680 | 396405)| T3cPros| 8esseon| 306 (en| 13C-PFDOA | 142700 4.59 (4.55) rorro| ao [swoen| 3056600 24000 No 9503600 a700 No 1777000 20.600 mw |ma | wm o | 5Sl? Fu pel Page 138of 170 216 8ASnoalluymtibciaalServices:_ Created vith Analy Rborter Printed: 18/02/2010 3:24:00PM JRCSummary [rove | ovum| me| we | mere| | [soma amas| 0| ooo | | [rsovoem [|sswaamm||momw||ewe w| eowem||e [rsowms n |asmeoarm ||wnwn || || eswoemm|| wwer || [ross oman|on| we |omen | ow [sorsceroon rr | [re [soem |wn| | emem| ow | Columbia LS foe iemiseriies 7 [4 Quantitativezs Peak Review 7 i3 i| ol h- wher --, o B4a1s3ePl0iF1n1Oe6AM9i10sDsaed | oBo41s13e7lC.i-0nPe37Fc2OM0Ai0s8sed PrCinrteeadt:ed18w1i0t2h1A2n0a1l0y3s:t2R4:0b0itPeMr 3 El ee = z KQ100"]0664-073% f== I "3 he x : w| -- - | oB4as6e3iP0nE4eN1cAh9M10i0s8sed | oc B4a6s18e3l0iC4n-e2Pc3F0NMAiDsased == i=cl i -| :i wo --] hey ly oBa4e9i9P.i0Fn1eO3S0M.i10sDsaed | oBa5s01e33l.Ci0-n6eP0cF0OMSiDsased | cBa51s3e,lP0iF4vD8e9Ac.h10is0saed | 511530C4-7P0F0OADa Baseline o Missed - Hi i | ~| =| Ll-; he Lc| i= id pn - 4 Ba5s6e3lP,i0Fn1U5eR19Ac.10MiDsased | = nian ea cB15a63s5eCnt.i0-n1P2e7Fc0U0MAi0sased | cBa5s9e9Pl.iO0n8Se0cT0Mi0sased | agen oc B5a0s13e3.i0Cn/-e8P0cF.0OMSDisased Guang a hl i =i i3 I 613P.F0D1O39A1 0a Bessie o Missed | 16135C0-1P6F9D.00ADa cBaselnec Missed | Ba6s6e3l0P/iE6n1Te9As0 1DMiassed|o B6a1s1e53l0Ci-1neP6oF8D0M0iADsased i| i =3 | 713P0F/T8O6A910 Da o Baseline o Missed | = B6a1s1e53l.Ci0-n/ePoF1D6OM9iA0.sa0sed 0 Before O After Page 1400 170 20 3 olumbia Analytical Services PrCinrteead:ted18v/it0h2A20n1a0if3.W26o00rPeM RR Sa LZ = Tm = lon Ratio Confirmation == | 4- KQ1000664-03 i3 = al = iFe o4B1a3s.e0Pl3Fn6Oe9Ao.M20i0ssaad | Wang Peak cB4a6s3e.Pi0F2nN1e5Ac.Z0Mi0s8sed | < Wrong Peak o4B9as9e0Pli9Fn8Oe.Sc20s0s8ed | c Wang Peak B5a1s3Pi.F0e2Oo62A9Mi.0s0ased = Wiong Peak pofl f E = =| - i. feemtpeeL I: |o oBa5s63eP.l0Fi2nU6eR9cA.0M2i0sased | 599P,F0O96S.2008 cBasoine Missed | oB6a1s3lP0iF/nD1eO6o8Al02i0saed | Ba6s6e2l0Pi/nF1e6T9.A20Mi0sased Wrong Peak Wrong Peak =Wong Peak Wong Peak iI I! =F 71P3F0T/e1A62080a BasWerloinnegcpMeiasksed O Before O After Page 141. 170 BE