Document jDNqQrjMnbBBa4Vd4yQ8egoN

46 CODE RT-53-1 -D 'mJj s Jm JJ2K88 < DATE ) ( LOT~) EST * WT * LBS. PKG ___ ' PROCESSES APPROVED BY: ( > RT-531-D (P> EWK 08/02/82 COMTYP JOB NAME:- 40RT531DMP STANDARD HRS. _______ TIME J3a h s.sssssssesssas: NAME: NAPHTHANIL RED LIGHT AIN 4-NITR0-2-AMINOTOLUENE FOR S6 IN 3-HYDRQXY-2-NAPTHYLAMIDE FOR SI 8 AN, DRESS, CLOSE 24r'CLARIF PRESS - ` 15 FRAMES J^0N 29' (700 G) WATER INTO V-_ KRUN IN HYDROCHLORIC ACID FROM V-324 M___ J._______ , j^BQfip IN FROM SI >^NITR0t 2-AMIN0T0LUENE ! USE I LBS. SEMI-BLEEDING I ACCTN-CODE | LBS 504-C 1 150-C J I Yj&5tL i3_d~ 1 28-D | 182 5(M-c~MEs GA A##r STIR 15 MIN TO W 8 TO 42* (1470 G) AT eg . f : . - . lg*551 9 ^TFHON IN SODIUM NITRI 7-1 MIN M----- -/fflV--- -r \&3Z II >SflR 5 MIN & RECORD: CR__dr__(+>, KI_;Jr_(+) i ^NUTE: (1> IF CR-, KI- ADD 204 `AS IS' i INCREMENTS HYDROCHLORIC ACID ASSUME 32% i--_ RECORD: CR;( + ) KI__________ ___(+> i. (2) IF CR+, KI- ADD 104 *AS IS* INCREMENTS i SODIUM NITRITE ASSUME 33% RECORD: CR__^^__U->.KI_______( + > 11 IR 10 MIN AT-3eM*F MAINTAINING +CR, +KI OR SI3 RECORD: TIME START, MISC 112 I^S0JRRY DICALITE FILTER AID IN 40.GAL WATER I 3 i \Sm DRUM & PRECOAT CLARIF PRESS I DV I'ia/'l WHEN si 1 STIR COMPLETE 4 J14^SlN DICALIXE FILTER AID 10 15 L^jTR 30 MIN AT DEG F ASSUME 33% I ____ {^MAINTAINING +KI FOR S23. UNCORD: START^,^____ KI___ < + > '. j". 3(3 16 WATER INTO V-Gr ;?/3 I 17 [/'SWJRRY TRISULPHOIL SOAP D IN 25G WATER & I _ l/WJUR IN I 3&L 18 KtfUMP IN 3-HYDR0XY-2-NAPTHYLAMIDE FROM S2 it I J^SflR 30 MIN OR LONGER TO WET. _LOT L^r Ec ORD: START^wfek- -JKJL3L.^ \X3A- [ #32.3 57-a lift: :| - 725-A | 138%f 28-D |_____ | I 725-A 1___ __ I , I 777-A- 1 I 777-A- I 10 725-A I______ - 57-A |____ _ I 39-A I 3^L |- 150-C I 536 NOV 191 COMTYP JOB NAME : 40RT531 BMP PAGE 02 DATE PRINTED: 9/14/82 EQUIP MENT I PAGE 2 OF 3 CG 40 CODE RT-531-D <P> USE | I ACCT LBS | N-CQDE { LBS , 19 Viwk 12* <144G) WATER INTO V-302 20 yfWE IN SODIUM HYDROXIDE ASSUME 50% 84 } " IN ACETIC ACID THRU METER & STIR 3 MIN -5LX-1 22 J^KECORD PHJ2*JE*<6..7-7*5) IF NECESSARY ADJ TO I 6*>-7.5* ACETIC ACID ASSUME 70% ;____-- l ORD PH_^._ SODIUM HYDROXIDE ASSUME 50% --_____i 7-D 30-D 30-D 7-D | 42 i | 63 |_____ RN ON V-323._ AGITATOR 8, ADD ICE, THEN 2X330 | SHUT OFF AGITATOR 23A | ^eff(p DV. THRU CLARIF PRESS INJO DV USED IN f S 23* MAINLINING TEMP AT3*4fefcF. RECORD: TOTAL MIN_52S-i.,,_ l^fOTEi DO HOT USE V-303 - TOO SMALL i 24 j^WffEN S23A CLARIF COMPLETE WASH DV <S4) I J^fNES PUMP & PRESS FOR 20 MIN OR TO A -CR i^PEST ON A SAMPLE OF TOTAL PRESS EFFLUENT M^ICHEVER COMES FIRST. COLLECT WASHINGS IN (S23) RECORD: START_&^__,,CR_^._<-OR+> J 25 J.WREN S24 IS COMPLETE TEST DV(Sg3) ASSUME 33% ___-- I IJS^RECORD: KI_.__< + > TEMP^Jl I-<40-45* F) . 26 rjrfBIGH SULFAMIC ACID IN RUBBER BUCKET AND r rifv'IgSE IN AND STIR 5 MIN* 15 } 27 URfCORD: KI__r^_. MUST BE - 6 IF NECESSARY I I ADjLTO -KI,WITH SULFAMICsdftCID _______i 28 C**ffj TO 551* Cl925 G> AT^^8?DEG F 1X330 | 57-A I 725-A t___. - 57-A i 395-D I -15I 395-D I___ 57-A i__,,^ 260 8 9 >/3 260 10 <3300 &>. WATER INTO V-260 /<+ i'9:7yD> /L, SI8 STIR COMPLETE, POUR IN SODIUM ^MpROXIDE-IN 3-4 MIN* ASSUME 50% i^EAT TO 128-132 DEG F AFAP 6 STIR 5 MIN TO .V0TSSOLVE* STOP AGITATOR* 1 ^ ------------------------ -------------- . HATELY RUN V-^/La FAP INTO Cv Ln O ITATION IN CV. RECORD: STARTX3-_ TOTAL MIN J/.___ In ACETIC ACID THRU METER 6 STIR 5 MIN M____________ PHiJter<10.5~1?70> ASSUME 50% CCESSARY ADJ TO PH 10*5-11.0 iD: PH//V# ASSUME 70% JN IN V-302 AFAP >320 I 3/1 *.! 1 f 7-D i 160 30-D 7-D 30-D 210: "7 1 TO 78-82 DEG F AND RECORD: 5.Jl _^_DEG F AND REC.jgjV____DEG F WHEN SS8 COMPLETE, COUPLE DV UNDERSURFACE IN 65-70 MIN. MAINTAIN CV AT 78-82 DEG F RECORD : SlMtf&ygjtiJ TOTAL MIN _________ STIR 5 MIN, DISCONNECT TRANSFER LINE AT CV 6 RECORD: DlAZO__zlT___, < +/r>. . BASE-.jf__(MUST. BE +> PH_j '.<4.2-4.6) v*> IF NECESSARY STIR TO - DIAZQ RECORD: S'StmTOTAL MIN_____ RECORD; DIAZO MUST BE - ' BASE ____MUST BE + PH ,,J&3.___<4.2-4.6) V. DUP050061192  CO&TYP JOB NAME : 40RT531DMP PAGE 03 e q u ip "!-"''!- ~ . ; MENT J ) PAGE 3 OF 3 CG 40 CODE RT-531-D (P) niSC j*FT~AbD 30G WATER AT 130-140* TO BRUM FROM HOT 11 1 1 WATER MIXER ADD BLANCOL N 6STIR FOR S43 DATE PRINTED: 9/14/82 u s e ""T"" --J~a 5c t LBS l N-CODE l LBS 43 i 567-B I 43 260 POUR IN N-567-B SOLUTION FROM 542, 12 HEAT TO 194-196 DEG F IN 55-60 MIN A#D RECORD: HT_/_f$Z___DEG F AND REC_Z^C_DEG F WHEN. S44 HEATING COMPLETE,' RUN IN ALUMINUM SULFATE SOLUTION THRU BADGER METER. NOTE: 36 15-D 86 'RINSE IN LINE AFTER N-115-D SOL*N RUN IN. 'STIR 30 MIN AT 194-196 DEG F FLOOD TO 80* (7928G) AND STOP AGITATOR II i! START FIN. OPTR II II II I. i .11 II II ___________ " ______________: --3B&G___ _____ ,' __________ ^_____; -- I DUP050061193 DUP050061194 ! i DUP050061195