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R226 3287 #3 Dupont-11418 Rass 3287 - TRADE SECRET Study Title H-25425: Subchronic Toxicity 90-Day Gavage Study in Rats with One-Generation Reproduction Evaluations Volume 2 of 5 Laboratory Project ID: DuPont-11418 `TEST GUIDELINES: U.S. EPA Health Effects Test Guidelines (OPPTS 870.3100 (AUG-1998) --_ AUTHOR: Susan A. MacKenzie, V.M.D., Ph.D. D.AB.T. STUDY COMPLETED ON: August 1, 2003 "PERFORMING LABORATORY: E.L du Pont de Nemours and Company Haskell Laboratory for Health and Environmental Sciences `Elkton Road, P.O. Box 50 Newark, Delaware 19714-0050 Wonk Request Nower: {JY SERVICE CODE ones [EY -- wae Company Sanitzed. Does no contain TSCA CBI ~F 22 3 2 BT Ta I 3 emma F$ESgfymEf AF R t o m nny Bor 8 pi i} e 9A5E% |i i iMo --_ 8 5 | 5f 5Z3RgF ii--Fi! 11: 2 2ih1 ' EER Po ig 31 3f%e : i iiH =i gEEg! |; 5GoSiE : gi id 22 | Boi: i i id]q 8 0 , nTiil EdEEEEEE id 533 iz z g o, C0E E iaha ailt Eahi aign ilnn gor HTEEREEEEREL I 59 l iB [F e o BE fg F s Oe E OEl iz CompanySantas. 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P2e 3 8Zzg } CiaE Pog is dSia nainn ifs i FoRRRRR gy i Pos lpgat FEO ~4#z6] foo 128 iE 4 Company Sailzad, DosnotcontTSaCAiGnE! ~3 Hl 35 g= BT Te a. 25g f Lae5, c EgE N5 i pgEEL g BBBEE jLiemei i ~) Sg gEFaEEsEgii| CT iIiifta iggz e55s80 i iF azz : 523 iE i 252 H41 &SsB ii iH iis : 5i 4 2g68 8 :: iPidi L/ 2 8 ; bC} p OEiks hi nia | i4 3 zg :POE pbPsE iEI sToEtH a53 i iPE52EEig: EH Company Santas. bossnotcaTrsoaCo ~ og 3 3 :2 2 3HE8S0RE-- T 23 2 f igiaitei | i: g BSEorE& 0iz eL p m iie fig -- g 8g9a45t8 [|i I r I5E : i1 F TEE gg i cg }| iEBH ] IH 2 5| i g8 ;i {2 ii J si :J. g2 : | i g 14. i gis igz 5 <5 g I P lego E:E 535 Eg P0E, o ii riigs iia8s iPL F E PiEEEE feiilgd is -- CompanySaized.DossnotcontTSaCAicnr ~ : FEL : EET a. EF 2 BgiaimT e BE dim i Sg ggsEHLE T fr ~ 8 Szogggdgze | i |i [i5ihn %. = 55 13 03s82 D_| ji iss 548 ' | Eg 4 g zi i/ Ts ii i 28 qgi :| 5if 4 S3 08g g EL i o E HH E5E2 Pi oE8gis E|edilggk S| PEF ig a CompanSanaa. DoesrtconT50an0n1 ~3 3g g :Eigen os. gir-- 2 game | 2FTEeE3eLIHlI N TIiH Zg8z g0g84p58g HIBT leilggi CET R s a ~ gg5g99g zg 1|| iif i iI3oH = 4yg& 585888} --| 4a I5 2 ggE2zE ii iiE 14 gfze. :| iii i}l g2g 8g2! | i 51i2 H: g=i || i hixH : Ezl= BE i bi op ia i Core dE ~ i%8z = | : ePe ER ik CompanySaiz. DooteconstinTSOACE! ~ 3 a 2 zz BTh(BEE s5%a) EE5 igigiAEs --i oBogr E 3 tie gi----itig 5 83 i 5 3. Fei: ~ | :Bg8g3k% 4ge8m 1 | igi (13T] ielofENR ||iT = nH831i3f,3y 4 i: gg ih # i 5 532 | 1 92 2 82z5g% || || iiEE & i i idg S i i iad g 78 ! ih 2 gS Eo ir2 ICor idein: 849d)3 18: iE CompanySaid. onsotcosntain TSACBI ~3 3:3 i3 S5ELpa-- t fs hiv i glgBogeh nm EmTmo hi ~ | 8g8a8g i | i ihHi] % y= giz Foil i52 3 5 32) | i ' id 2 gz2 ; = 2g | i if 4 5og:g : ia gd 2%! ! if &{4 8a |ic :| i3: : iLE Cro il IjEE 2 ; i i ge igd Ey EEE ~~ 48 Conant, gostriTSA ~ 93 . 2Z EE -- 2 tisk! | Eg2 hi igiEin ly eee} Eon [EViam ig 3Z8o0r HiBTom IP S T L t 0k 2a8 iisH ~~ 8 e gig Pi OEi5 i {E5N8 ig|l o=g sS5Ez0 i--! i23 i 2 Bogozxz |! iHi 1 Eg 5s i iiE gd 28 : & 3 : 2ga i. iiCo fiil dl i i joy 25 I 8 . L LE o iE 207 ris 0h 2 PoE ppd ~ i398 LBC 3g 28 4 . Company Said. Does otconTtSGiACnEN ~= Zz . BE Zz o8 aanEna2s%l gSEg g5 8giT z|--T i ZBz E3 GEEE ra i 2 giag i I El E Emi Boas oi 3 . ~ gg g84882.1 iF iH:H 8 fg 2 588 i 14 FfEg EC !| iisi : i583 1." 1h 108 0 by 28 ; i 223 g8 S8i00%2 38 --_ EE | i I ifd 1 is iFihgs PoE hye EEG =8 Company Sanilized. Doesnot containTSA GBI ~8 3 3 FEL -- 3 ie g t 1 zal ig i%EE Le | 2% igighs | i sili --, BR 2Tem iH] ag gZgezgptg iH SELiEITRH-- ES -- 5g iNn EB Boe lly i : ~ 8g In : i3 z2 5s8oi3zs | --i 14I2H3 172 8 1 te |i qd| 2: 52 8 3] 2138%] ~ 33 =| 24 : i Cob igre 4 iE 9 | i i iH % g i| i "REiH gg i 3 g ii a8 i i15d%s : 2 H- HE 15 E ia [TT ---- ~~ 5 5 : FEL -- g 2 iogi3 gnidesi| e, mii g 83 1 8 IL i: BEE om--u - EEC ggz i | ii] &; Ei E2 g55i8g F-- E 5i25812 & z2 i 183 ped 25 6Zz a5 ! : q8 i z 17 || iiii |; 3i52 Cop i2t3 eg | PiEg ogiliinl of, rile 3 Por oiE fed 49 i LaF in 23 GompaySantags, Boner NY ~ 3g z 3 J 2% dik 2 8 if iy : 8 5 igiziEm I gE phir i inBb {E AI RE ER TT rs --i3 : s3i6g0 HBln my| TTT= -- g ggiEggQ | iiiE F i| j5i5e2 28 oz 258 3 3 828 --| ia ia iIoC2 gozgZc2E i :i iiHt i gg. 4 25 ` ii } iE 4g i of it Cd : Cokes e ' i 4 g g | fbe p Bflabis iidw: 12i%2 2 PIi ogo2 PE EE BEUAERSTRD 1d Ze EE iE ~ 28 23 Company Sod.Go rtconTaSCiA n ~z g: g2 3 FZzELgi EE C7 33 gigT |Ly gE g2E i Eh nek gl oiy i conii g REE id ~ |g gael1 ig ii i fg = 5533%80 --i 5 iE {g Fe20 | ii ih 15k 1 gel | af 3 1 F22EEz8| ii| 1ii2g g Z2 e ; H | E IIH . g gd i PoeElE 3] 22534 ~ Eg aby Ealing i PF PEE BeiiEl CompanySate. pons contac ~3 3 7 2 1 F fi zg Big T TE5m85i1 g8 e wm on || ggz 225 g g0is[5%tu os|t-- a-- l; $g FB i (ETE E gGEor Bll iLF LIyH eee if ggggSaggE!i | i iy1i]] : - 45g3e5o80 1-- iiz idF4 o8g%if i | 4 5i 228 | i ii g g $eg || {Fe oslii] 9 42 8E8l ! ||i [gIEfEREdBiEdT H1o: Le Hi ilHsi 5352 8 EO E LLzE fgihtid Lis 42% Eog Edr,Et #6) ifs i% = | Company Sanitized. Does not contain TSCA CBI ~3 z 2 PEL : E 3 igizii des | ,i gE fam = BE ETT io i ~ | OEH8G (Hi ggzaE fem | o1 h iHs ee2----i3 i 8 1 gig PoE jak ifg 0483:55| --| {E3d% ' [ 2 Ez N; }: ygiis i 2| | ion of< g8 i } godtBEE in Hoo: H2E4 ~ 22 =| gp EEE CEr E E Cig ComprSard. aannToon ~ 3 3i az = :zz igTlifeal| za ff | $F [5-- gE 5 igiZ zife|s ,| 5 8g2oEgoB steT m li.H : egogae2xo8 TiL ilZetli| g 13 iiiPEt ~ |fz8g32zLo iFP | iii;a 8 E3 R | :| iEEt #7 g%F i i H gg! | pt] 2: g2d Z5 ii ii H EREE g E4R g | :i Ey ii%ds iqd iZ ; :PogfEi - Kk g fy BE 533 ggEs PPrE Bg EEon H3r PEE E HEelE id MH ii E ig ~8 Company Santee, Doss nt contin TSCA Ca ~ 5 a g zz gi RE 2 } Sid -- i 85EBo8Rb iHEam C m|---- Er 1I3H - glig t -- i 5hi 3 13j 4"5E22R5%2E i| i=B Hi Eg .3 |; og:g, PLo uifri g ! LL i i 1 . 2z:s ggii Pb Pd EE RpEid 2 iE 5g5l 5 gE, fr iieE giek i3f oProopeHEE #6) i PEF i ~i `CompanySanitized. DoesnotcontTSaCAiCBnI ~3 g2 i po bs zg og Big T 7jsi1 z29a E g 5Lpute $Eo2m iEtlieam Liy 88Z8o5r i2H limT o0Pr8og ~ :ggCgaEcL i 1i igEHHi] 4 12ES:gE83gE8| -- iF | Hii3Ht iF ogzz i 2 f27e2 | |: iiff i1 4Ezg | 4iz i. 02 ol if . i |boi ing 2 5 ag i IiEg iii:. 3 2 og ii; i 49 ~i Coit | emmiena e | CompanSantee. oesconanTSCAGBI ~ 3% z : : gm gE 53 LHaEni--i gZz z5 iEp NEEER iIf] 5 82E Toi ~ | gggs i1f ` iHiE 8 = 558 123 1% 3 fa 3g g5 f El Bi 4 gg 8 || Se0g2: SE 8 H2 o: CFop a | ; jsf i HH I] i% Iig i{3j3 lf P HoEE :i bHEM lige (EE dl ig g; : CompanSanaa. owscon5aGn81 TM I 2:2 :Zz z i5g7 (8=%F | g 8 een| ge5 ligizii des | i g 88 i fam --, 3 gEE ii ~ 88gE92L55 0 | if i | | 5iiiH } 3 of 5 828 i ' |il o5z 8:838 | |i 1if%f 4i40 ges gg i :| iiHEH 1 i | 11 g 2245 |baniiss 5 g3 8 82 ii oF, P`gfEog OEEBE ifOEisEniy 1 pam ~ 293 8 ire in CompanySri. Sees TORG1 ~% Z3 : z BBEEEE g@ e i| FEL EE Lez r3: g aHiiRTE Ti os PE fom | 3" "oid : gBoE4sH8 |T| ii)1mei e------------ l3i . ~ giz | i : [| E=RIg5E8 @ : i3t: ' EEH EREia !} 1533 : 2zg | i 5 isk 3 gg! i RE 4 gs ! feos ii 1 82 op dine 2 5! HEE Cy ET bodnui ke 2 8| PE og RR iE EE Ea fl 0 pidEni i223 23 #3 ~ 4 Zgz iPog Dg Eden {8 g3 fEBEIEEEREEEes Bby oi FEE(ErE g EE iiNsT Company Saizd. Does ot conTtSGaAiGHn! ~= i ~ |g 1d : Z:z og (iggi sqfm12 sas! gg2 g ipigirfe -- 3 di A & Boia if g5 g2aBs BflaT m PsRai,d J E32 fF | 8 : ii f8a z982&g8 i | | -- || i3inha EEL i: Zgge| i fsgz !| iigf E i aif: 5 Ei 4 ii PiEE ow Bieed : gl 2 if 1 I w5 o:g or lyiBllo e i28y iCoE E Ete e 4% fi 2 E72 ~~ ZE3& Company Santis. Dossroc5AaG2 ~= 3 3 2 = fg 0 FEL | Egg iE Ef 3Sogp inEe B BOR SBEorC 8OH(lE%iT haEemioEo 2:ig --~ : goe4gs8g Ti(iZiiTc TiE51E 852 | if < gzS gosaEgE | iF iiigast 3' 3 3 sz i 2 gz2 : i& i HE 37 | 41 g8 E: E EEBE 34i. &2 a | 5: gl! 5 g BoC i 22g i ~ 33 : i |i i(2H3 iIRr 512 PE Eeo a ii4kE | ie 3% lily fi i2gigh =| GompanySanized Dowsso contain TSCA Gal z :i 10iiag]i ----t 1ggm%x 1 z2s% |i s 3%aplaam i4 gBoEr lLa Li --------iF ~ |:g gSat g oFg o| i| ; fig He 17% 0 : gi Hl 1P o:gz1 | i iJEiins i= Pi . no: i32d 2 i: 49 IH28 rank PoE ioiirayi gi ionb Pod ig get id PRE i ampsisrtins ms ~g Z2 g 3 BT gh 1 zee| s3 ipi igigm|erEF, 2 | ob Em if i gggSfgoEr:E E BL yET . oo i1E2 ~ J EEsga 5 3& i. ifg =85858s i iiy yI3 5| gqi 23! iBil us ~ 2LE4 8 0 dry 2:Eli :i gliiis Sgs &= i: HLE E zi 5 8 P|| o[pEr ERdHEH g&2 ii iE E i dg5.8:[32 Poe opge d RE iE CompanySantzs. Dooteotss TSCAGt ~4 2i 2 2 Frain Ty F3 Eog liig q-- gdE -- CsC l 3 pa gE Bor ig] i~y--i------ii ga4r8 ( TiZirT i1f3y ~ lesesg| i0f | iin : Jog: -- Hh 3i Z4F o5g8i8 A ;i i%3 iE i 322 | i [1] 33: g8 sz i || iZs 8152 . 1 ] 5g 8}| ii o. piilE Poi : 25 z| i gig i223% gag i: Pli gE3SbE82 2 P08 ie gids 2 1 ifgeidd ~ 2393 a| i 8% igs ig [EP -------- ~2 <3 ligz igi i38 | 2 EEL I -- 5 imizifes | i sli -- Bob 28o8r8 oiETi=m iE i08L T lm FET iF a8 Cy OE --_ g EL | i ] j= S2E 0 h HH 3 I HE | i HIE i i is 4 24 | H 9 gg! 5 Z5i i i i%s EH i g8 i I 43 8 i |NH fil : dos ps z bai Poy ER BEE 2 2 PoE oie iid Pog i feigd 28 i182 ii ~ Z& 3 CompanSatan, oes conan3AG1 ~ og ] 8 g iF HB : Spm zr ge FT g 3 igi idee | ! i $F RET, Bor B 0idle ig 5gg2f2r L A pew --t Ei4g --~ 8 g85cz i | HI i cgi Fo i iH 4 $ E fg 2 E = Lo | IiE] ' iz 3 ZSz g i ! is ii 2{332 4 28 gE Co JE PoE dF CE B4 o:g LE dn yi: BEE HH Poilaad ~ 8d bE iE =8| CompanySnitz. Doe econ 50mCo ~3 3 2 1 8 iE : Nm EL iE gi EE m 232s0! gE5 EipiziiEegs | | SBEE3a H ifT Ef oi g oF0E8gE8g i(ZEL heFaRii 0 Frogi1E58 ~ | B E gsc F 5 J Sg i iii3f *i i 58 -- IE di F Bg2z8z | ii iify : EL J 38 g !i | |i i IinEd ;8 Fa } i ii IM] 4 2 Log iE 535 i ~ 2i8z 8] g |iPog iPEE EELFLEEM CoE ia ee | PEE ids CompanySanitized. DoesnotcontTSaCAiC8n1 ~ Z 3 :2 Z og fi jERE B SE -- B=o3B igigisEy | oRitis|h i i g 82o5r5 Iilg F Ih o1i =iid: --_ 4 ga5z 85E ff | i 85 if | ijPayg ik . 1:82 g #g sgziEf 0I HifH moo :3 | of: 1 ga g5 i| iifi | gi i i153 4 5 2i ; od i gi ' Hq 123 235s g ~i 5 z i posi: g i E25 PF8 iiEE Eiseiks f: e 1L2EFE IR CompanySaiz. Doss otsaanTSA Got ~3 i 3 : ELie gi 3+T 9 |-- 2aa2. 3 insite| | B$o2B 0 ECasn| | i g girE 11 ToEori Egegge 1 ~ 8 gig iif ih ; iig 45852:88 | 311 g & 83% EE ;! iigH 3 8c5 E5 i i| iii:d 24 Z5 | ii iitEs g$8q g27 4.| EIi Lo i(Eik . 5:2 %g ii 2i3: gi P | EE HH RPdEFERE if i i2 2 PE iPs ER21Eh Pdi Ea ~ E2g34 e ; ie i Eih Company Saiizad Doesnot conta 780A G1 LL : :& ggggigf GBLE Ee i E 5 jE ~ |g Bu EH REET g gogig (Zl eFRi 7 2iE JEf 228338 PoiF i iaHe lise -- 2 Z iz | i IES 17% bk 2J] 8 Ss 2 :8i i5EA- Lgfl g ! 68 : i i F || hIi ig efeF il%y fs iiE 1 _ $3 CoE pga SL : :' : ConanSoi. sos omen 3 : g zg fn gE Er fr! eg 53BoE gijigi | i i 5 8Se8r5 34 FiT oi:f 3 EpaEx --i--i--iid= ~ |iZ8c835ga2e i i] i -- iiH31h3 .3 1982 0% oal F2 EsREzs i i| EHeh | | ie i FFg |it g4h] . I4 08 orba igo: Cb4 1ge0d ~ 3344% teh Compass. os scm560 ~ i 2 : EEE ze PEL gE re Eg 35 h igizii fEs |s--i EB ofail dFi ia|ei!i fag Lo ---- 0 gd 289 |1 iix g |i i(3 --~ i 85% | 5 S28 qo i 3 7 3 EZR | ` 3 2 z2 i H+ | fE d | : iE : g8 | 13 i 3 sg 8 | 25 | i. i53 if T 5 n g i ogiI i2i g Poy E ohG,E Proj] te --~ 4a iE ik =8 . 3 . ` CompanySota. Dooteonss TSCAG1 ~f 3 : T E TeREhL s+ ZgiztzEg La wiaT nE _!I1 || 2 TE asi .: gE i "k | |i Cl : oa | i13 hgito | H"i i: 2 5232 :| | iIi ) |i : o 3te e :| i8% i | | ol | 134 5 gg : g5 }i I: 533 Lo z :sg | poi G1l] oo|inki5: i 5 | LAE . CompanySanz.DoesrotcontainTSCACE 2 2 3g i2g 57 aBEB 1F3T eee gEEE 0 ahie F PTRI I Ep S e IH | 0 I Ei i ~ | ger 1 i 112052588 -- | Fg aa 0 og: d gz! | It iE | ii : 2 8i HE i i fxg : gH og poo g8 oo i 24 PF [I i { 223 BEE 1% 152 ~ 29 :fodid L2 iiz oman, vert ~3 83 3 FE zgEu Lgsrie -- faF g3S H pati el T,i EF o&oiAiTiam if : ZEoriiB nEFeT fa.ry ES. 1 ~ | 88 | iH : |g i 3 B88 | =i d F o2g2z8z | ;; iTn 1 iz sl1 o8z EE 8 tZwHoof ~i piggt EPS Bi Cd pis iE E ih Com DaoRrTAeS ~ 3% i | joe -- a E g 2g8il fo g 3 gigi 2 RE iLy So Bgr8 E Fie TT.i gpg em ET CER ~ | 8 ia Co iE i gg EF Hi |g 822 | | a [ 2 ILi i| iig 8 8!i ii 4 FER | 5 {flaigff El 1 28 | iia 3 250 0 gp iil I2 g |PeooBaFd it is gs PE dds if: goof ? it iE 19 CoE Ded EE ih --~ 24 =| ? . CompanSete. Does conanSGAGBI ~f zz g PEL(B87o1a85l| 5os mem oe an |: 3 2 ipisiges | p; GB OEiem| i a B%E TT oa EfggFegERRE ERSis CE 2h52 ~ f =g 88538z2g | ii || EIiEH 5. [ 4 Fai z i| iiH i gEa id ;i it ifs 1 if diay IE Comb gd2 EF | ifinFLERyE . iz1 2sg : Pd o5p pdeBeEdllaEildy 2i:2 55 Z Loy hE jh i il PoEoigeaie df I ii E s ih ~i Compo Std. ossconTaSAn1 }3 z 3 3 cory 1g iss | 2 i igpiga SEE | 8,3 88% 0 Bi ----1 fh 22 in 0a --_ 4= 895o8f | ii 5 838 | iF! ii:H i :3 1Bf 8B32y1| i--i &EN ai4 g3s% i H &&| } i4H : 3g 58 :| Pgoi1E2% Cyi 24oF ii Pij opioei biEd3 | gl iiKH i ~ if 2 Pp Eg dl 82 i roiiEildei ESH3EHE1H50 Lier Conny Sart. one can TsoRG1 ~ Z2 4 2 z Bi i5EE | cod : I SSE li--e igizides | i 8EO3S E0iieHwFm--1IH 8gpl 8% ieiili iiy SjEiEe L-- kod ` sgaez 0 ii ; : i 1 35 oZoz 43 ~ fF 0 Fa2 i gi g8s i 8a i iI f -- GE : |i ibyis J i] |ip Pi iid iE D8 E ii i IiHH] J ------ ~ 5 3 i 8 d Big 7g8e -- 1| 2=r . gz ge i F8REBiiEiTS :it 5fg8Bi%9l=2 z-l I4 --Hi----ihf2 ggeerE i og i3 4} ~ 58:g5 -- 1 =i $ Hg: IeEes53ieg8 i| i| Eis ~ Z1| 4i I.3 55 2 E2H #9) Ff i ;i 4igd := :Lik5 gE i Epoo bod g le EE i giiEN g5i5 78 iE if CompanySaas continTSCAG1 ~i | 4. ; 2 gl 588 aoolf ES : cs 2 & 2 4 382 2 J| -- a Ff 28 q. i gl :3 8 g2 i for weet x3 |= : 33 E2 fexeo anes5 5 zz ig 3 : FY a [a i fa 222 ~ #493 u2f 8 |i3 RBHE 55,, 5 . Company Saniizd. Dossncoontain TSOA GBI ~ 2 2 z g2 o a 0 oi qi$8cs5 SB5ag8 i28=; S4 LYE $38 i:g a8s : 8. 2 | f FERRE ~ 1:1, gE 8 1= lass : 8 |. 5 8 Besa z 5 S og i 1 5 EE glgzFon8e:8 i3d] 5 gE B22. 3: 3 58 ~ #3 8 #2 wolZS885% wu EN nog5f4R5E%E: 3552 ofpifE sats ig aalE3315 sisis Eg2ii43sn8% gHeiadl gdiioen Hides anatiy 8gh2l/F5e3R8s7y =f. : : CompanySis. oss continT50AO31 ~ i5i zg2 = 2 g3 4 [E1s1e g fz f g8aa 8 orn] $S > aces i 1H go 5 = og 588 aoosld } ~ 48 i g | 8 |. 2 3 g f.ga mooa| : is g 2 3:i 88 CA lus f : I C3O 5 ag er H25H/2 dE : 2F z 3 &=z uEollt3 552 ~ 4] #5 5 3B88o 78 CompanySanize. Dossno contain TSCA GBI ~3 ) A 2 fs BE FS I % 3r % 3i5ag i8i3 HE 2z Ssoo:z :oz :oz oozg E3s fm amen g i S A Ba ~ 3: iE Hg 82" 8a" 83 83 44 33 : z: _ gid g 8 2 8 8 8 8 8; % ]Z| HH fu Eee ids z ood 3don a2 e@ ed fei ? 5% $3 23 85 28 ER 5 aa I FEE] i ! Poi 13 <4 pBEaEF0%OFFfEfR OtBl|g iETd 2 8 5 ge Zt 3 IH CompanySins GocerescToSArOeB ~3 Sfe oarwmf sof of of a gig 1i3 3 ss s82 3 Bs g e1s8 345d 3d5s <473 33 33 iER iiss : is 5 a = = =a oa C2g] 2 i - g 8 8 8 8 8 gE . ~ 3% f: 3588s ied VE ge ie i:3 3g mls3q ] 5z s~s~ 3= 8= s-5 8-|;E%3e% | : i 5 R 3 T wPn Rws N on Con w% eai o EE4 52 3 i4 49 ~i P5OF> O3 RF> OR OR|8 iO&i7 i ae 2g 5 i2 f> LI i id [EE -------- ~Z i . a gs BOBEHEE =; g i: o 38 Eo. mum a a a 2 is d B 5% RR EMEERR 3g g i 3 a8 saad 1: EE 3 3 2 3 is ~ f 25g5 R3x, B shiEegE ais 4 I . z 2 . 1x zf 1 8 : :133 7%- 333 G.2.2.3:0% dizBL omigeEden i[ sd 3 8 3s 3 gE3 E z y og. i 5802 - 53233 F 332 ~FF3 N &BlF;EosBoa3 ~ &5i i io.e CompanySonics. Dons conTSCAnGE ~ 3z oa od g E8T sacengdI Fi 2 HE Sg =o ooo ii E, Z3on8on3es3 u28f ig Ado diag 8 g fq od F s R5 EE ~ | Es. F300 ff 25 Io =doad ddd 2 4 g gz : zg1 z& o-oo op3i313 H 2 BE. s 3 3z 3 s3aSeianiosd z i, 8cadsdgd BEd 5 z 2&4 i$l 2E. i55324%3 2%: g2i 58, T2 o: =if 1of3l - 43 i [$ 08i RF BfgFooye is : ii ! i4 ~ a48329 s PFsI LE2 Company Saiz. Dons otcontain TSOA Gol ~% : Tisai g 5 ER EERE OS g i Z g 22 5% BeFS BgTn EssRaEq 352 2 So ds a: o gg 23 %@ we an ne 1% 3 --_ igd 3E 2 ; gs gREREREY 2 1. i : =o o-oo 2 as 5 2 3 2 8 JE, 1: Eis 4 8 5B $ 58 . siIi2% id it - z 3 25 22g s 88 3 5 - z lf 2 F Fp i ii;f i 3 2d bE ~ &3 : = gE Ee Company Saiz. Does notcortSOsAiGnBI ~3 3 52 zzso ,.23 0&% z3..33 E B8E 2dg42%% 388% e23Z = : o i "~~ gii 2 2 gg 3 3 IE E% ge#8 2233722 3s53nod3ad f4y5 3 is J 28. 22.28 6 : _ gg = Sao oa iEe ; i2 : ZE : i: de dd gE a on a3 2) i: : ooo siad 3 3 3 3% is EBfge zadea03o5aiaina ioReEs i ag HE.3 - i253 g B5 iagde f=7o1 fA %cfei i3s I3 38d8 8 2 233 33%3 _0 : i= Company Sartzd. Does not contain TSCA GBI ~ 5 Ssoz od E isi se5aat8a.a8n. gfF 2g 2 Soa ao2 a ] i i 8 TTT i3 = iz ~ == x 25 % o a==a c8i2 a3ier8 ed3 ig 4S3 fd FF ds oanoa st ge Fa :: 2 3z HE || g 2g ~ = ~5 ~3 223% k5 3 %& & 21 5Z ho EwS Eof HonHanITIogL8 ig IER oHfZ ss os5 sliis d2 5 f3f io: d i: . 5 Z t H3L% i ~ 4EH ig i} | 122 Bs o.Ef2 J ------ ~ 3z z g 3 z 2 3 8 3 $5 2 g Sood HI i Z 3223 Fi 2. 3585 83% & #8 353 d88 SE 42 3 ~ 52 32 233 2 | 2S. srsioaorely 3 E fg 3533323 Los os ' g 3 BR i got c yif $g 142 . $ rl LE 53 Eog 12 gfa f n3 H3oo:2 3 i= ~ & EBoEoe Pg Eo. CompanySaitzad. Doss ot conTtSaCAiOnBI ~ al y 48 85 85 38 iS EY ToT g. 5 3 oe. COE of of Eg i: FE RE EE ET ~ [fered id ; SEE g = 85 83 8% us lEiioi =5 gis ag Eom EJoL28.a8 33 33 yEiE IF . i1:$ 5 FO oM 2 gEFudaR al: 1H] o5fB a:i T1.%i3rbg5oslfasfpiidHdnigiieeittdsye I Fgp R SBEE E OB;E8Fy gy iif iE 8 82 HE 2 BMd RYE2 3 ~i `CompanySanitized. DoesnotcontainTSCA CBI 8 2 8 %% a0 gag Asay ; 14 oe 5 18 228 weg i Fr TEER RR "z - go. .z +3 3:38 3.3 s: & ~ g4 L3 B EEE| EE zi | ZZ 5g 32g g5 cce, 5g35 o2sGF eEf2IB5a;8 gBaRe3ra.n323 84 E8 Cf J1 2 oe igEi aiEi 3 :4 5 24 3] 345] ~ E2s4 PEON ERIE HE RHEE EE gis 3 gid ES ECE to. 85% 53: CompanySanitized. Doesnot conTtSaCAiCBnI 29H020-5DD4a2y5G;GaavvSaauggbeceSShvttouunddiyyciTinnoRRxaaittcssitwwyiitthhOOnnee-GGeenneerraattiioonnRReepprroodduuccttiioonnEEvvaalluuaattiioonnss --~ TABLE 65 DDuuPpoonntt--1111441188 MEANESTROUS CYCLE PARAMETERS AND PRECOITAL INTERVAL INP, FEMALERATS eee eee eseeeeeeeeeee Dose. oPferDcaeynst PoferDcaeynst oPferDceanyts Mean Cycle in in in Length Preecaonital Interval Group (mg/gk/day) N _Bstrus Diestrus Procstrus (days) (days) 11-0 20 3a 568 08 v-0 10 20 308 EY EY vi-o 00 20 ane 608 as vizio 1000 20 26% 62 128 a Standard deviation is presented in parentheses. 210.9% 4100.3) 4.20.0) 4.30.0) 3.00.4) 2.90.7) 3.00.5) 2.80.5) Therperewceorietanlo isnttaetrivsatlicbayllJyoncskighneiefriec-aTnetrpsttrevnadstesitn e(sptr<ou0s.0c6)y.cle length or --~ --_ -_-- wo. `CompanySanitized. Doesnot conTtSaCAiCnBI 25425: Sobehvonic 90-DayGavage Study TinoxRitcsitwyithOne Generation Reproduction Evaluations DuPont-11418 ~~ TABLE66 MEAN PUP NUMBERS AND SURVIVAL: F) GENERATION DoMsAeMI(EReNaAfLigG/RdOaUyP):s 11-0 TVG0-0 V1I00D V1E00E0 wo19 at 19 19 MEAN ouBER OF puPS/LITTER Born na me ms 13 bBaoyrn4AlPirveeculling nBeoamse nmea 112a DDaayy 74 Posteulling 25 17 1s 1.8 ne 17 16 1 Day 14 78 77 16 9 Day 21 Mean wnER OF MALS U7P8S/LITI1ER7 16 9 sBoormn Alive a6e6 6612 161 11.s6 DDeayy 44 pPorsetccuulllliinngg 3ss5 3680 4607 470a Dey 7 39 38 40 40 Day 1 as 3s 40 ao Day 21 ss 38 a0 40 ~ Born HEANER0FmoLEF6UPsS/LITT6E0R 571 67 Born alive Day 4 Precutling 66ss 6s0s" 5s1a e6r7 Dey 4 Fosteunling ao 3s a6 3s Day 7 59 3s aE 3 Day 14 58 3s 36 3s Day 21 somvnvaL (8)35 3s 36 39 Sex Ratio (mates) 0.49 0.53 0s 0.53 GHeesatnat%ioBnornInAdleixve 1w0o0.o0 9953.80 1s00a.0 19090..00 0-4 Day viability 99.6 99.5 100.0 95.3 Lactation Tndexd $9.3 1000 99.3 100.0 . 3Litter= s1u9rvfiovralDeay 4 Freculling to Day 312,00.00-4 Da1y00V.i0abil1i0t0y.,0 100.0 : b eLPaecrtcae3tn5itodnluietItnFedoerxsa,mdieasnldsievxeLeirtdetdeprhuavSiunrgvivaatlleast one live pup. . 4 HDoearnonp:ercleinttterssurbvoirvnalwiftrhomaDaylea4stPoosntecuplulipngalitvoeDoany iDay 21. horSeeawnerpeerncoensttabtoirsntiaclailvle,y s0i-g4nidfaiycavnitabtirleintdys, ionr nluascbteartioofn piunpdse.x sbeyx ratio, herSSeuornwvceihrvheaelenroebyTsetCraoptcsihtsrrtaainc-atAlemlaiytt:asigpgen<itfe0is.ct0ai5nb.t t<re0n.0d5s. in gestation index and litter -~. StatGiasttaicasreweprreespeenrtefdomfeodr oinnfcoormmbaitnieodn pounplsy per litter only. Male and female a CompanySanitized. Does notconTtSaCAiGnal ~i 13 3 z I d fc |i: 2 aa - {3 Ezy, p33 - "any i EB ~ 3] iz igf4 i: igl BZ E 2ofan oasais8 ' H Eofef oo oof 2 2 EYi3 ~i 2 E38 gE 3 ' F2E g2l28 2 spf , 8 SElp 2 EFiELEiIiEly S CompanySaiize. Doss netcontTSaCAiCanl 25425; Subchronic Toxicity 90-Day GavageStudy inRatswithOne-GenerationReproductionEvalustions DuPont 11418 TABLE68 MEAN PUP WEIGHTS: F, GENERATION DOMSEATE(RmNgA/Lkg/GdRaOyU)P:: 110-0 1w0-0 1v0i0o v1i00o0 Woo19 19 19 19 MEAN PUP WEIGHTS (grams) bay 0 6800 120.) 7.20.8) 650.6 Day 4 Preculling 11.215) 12.2 (17) 1222.0) 10.9 (0.7) Day 4 Bostculling 11.2 1.6) 12.3 (1.8) 12.2 (2.1) 10.9 (0.7) ay 7 16.504) 19.320) 19.5 @7 17.6 2.0) Day 14 3.90.0 38.43.00 39.2(4.0) 37.2 3.6) Day 21 0.6065) 62.7(4.4) 63.6(6.0) 60.7 (5.7) MEAN MALE PUP WEIGHTS (grams) ay 0 710. 7.40.6 1.40.8 680.7 Day 4 Preculling 1171.6) 12.5 (L7) 12.4 2.0) 11.2 (1.6) Day 4 Posteulling 11.6 (17) 12.5 (17) 12.5 (2.0) 11.2 (1.7) ay 7 19.0025) 19.82.00 19.9 (2.5) 18.2 2.0) Day 2 38.6 (6.0) 39.031) 39.9 (3.8) 38.0 (3.6) Day 21 61.9 (6.3) 60.214.9) 65.2(5.6) 2.7 (6.2) ~ MEAN FEMALE PUP WEIGHTS (grams) Day 0 6600.6) 7.0 0.1) 7.00.8) 6.40.7) Day 4 Preculling 10.9 (1.4) 11.9 (1.8) 11.8(2.1) 10.5(1.7) Day Bosteulling 10.5 (1.5) 12.0(1.8) 11.9(2.2) 10.5 (1.8) ay 7 18.0023) 18.9.2) 1880.9) 17.10G.0 Day 14 3.20.8 37.72.90) 38.4082) 36.4 03.5) DDaayta21summarized as: 58.M5ea(6n.5)(Sta6n1d.a0r(d8.0D)evia6t1i.o8n()65.0) 58.7 (5.3) TherSequwaerreemneoanss:tatpis<ti0c.0a5l.ly significant trends by linear contrast of least : Note: HSatlaetiasntdicafelmaalnealdyasteas awreereprceosnednutcetdedfoorn itnhfeorcmoamtbiionnedonplyu.p weights. --_ . `Company Sanitized. Donotecontsain TSCA CBI ~Z 322 FI i 2 gE enol zg s 9 RN Eg 18g 2 wegelf } |: : ~ gd 22ER 8zd 1 : 3 | 2 Hea manly 3:3 2gdz | 2i: 2 len "eaclE z z i i 5 gd Bf 2 ER 58 3 E2E2] XE 28 | g 8g [2 i 2HL8 By ge aaBde)}|} Company Santas. Goesso cont5a6iGn1 3i3 Pa8.. : : BEE, oof =Fg % 5 z2a 8# ve82 enald& 2 5g2 94 Zi: 5 ~ | 38d, i 3 zea "eal : I 3| 5 5| 2 i: 2 223] 2 ~2 =] : Ho? 2g 3 2H dr i FEEALN 8 sil} sds & = CompanySntzsd, Dooteotsi TSCAOt ~3 3 gg 5% 8% RE 1 . 2 33.33 +3 2 gz e& 13d8 agfd egd egaa &; 2 ~ | gie FEEEH 1 2 | 1 8 2 2 8 3 3 k2 ij ZEBg : ia5:4 : :2 gZ z a2 2 3 oa f: 3 3 3 3F s eT 2 ainle g 8 1. = EaE REEER p ld J g ick .d 5 HE : giz ia 7 8 2553g) 4 it ~ 4%) &3 B $85 a F n 0& F To lFgF o i oss a FR g i= :5 FE. CompanySaitzad.Dossnot contTSaGAiGenl ~3 z 23: 21 ES 82 2 82 3g : 3 EoufEs Ea E i3d z Soa ad Ee 8 i; 9 oF 83 oF 8 wi =a v3 9 a3 2g FE ] = 208% et gu gH xd ~~ | iS5E5 HT "TR Sg 5 9 .3 : 2: z2 3g a E 9 E =a Ea EEYYE 0%4 4%4 oF4 ws3 |7 58 3 : : 2 37 ES 2 23 % 0 EE & 2 i3 a88 a 3% zi FL 3 oa 8 If; 3g : i 2g 8 iigss ~~ 2g438 25 2 CompanySnitz. GoesconsomnCo ~3 EHEMECE CEL : i ZS $8 sv guIIeEngn oo z 32333 Bg5 da EERE af af oF of oF PN |g5 : x3 v: fg =z 3 j g 5 i B8 7Ho F(RT iSdWd3iSiElRaGe fifs | agzd 3 z2s2 2 24 ~8 3 E 3o.0303aa0s g23 8&8 8 a 3 osfi i3 tlg f &|8 2 i Pi Company Sanitized. Do note conts ain TSCA C81 ~3 g BE ev 90 ac gngn) 3 i g we J2 m2 a3 i2a3 :5 ii -- sf3 , H F2E 23f3S3 =z Jz gs $7 8 30 sd gx s gf 23 3: d|F B7E. Ae ddaA dfg 8% 88 mn Se ad Tow 3 EE & & g H4:d g 252 %53 : 12 2f8a Tosh g3 Eg umn eo 4 8 AL8 i28 Pi ~ #3 i: CompanSanta.Doe stconanToonco ~ i BR dd ad 39 ad gd | i 2 2< 2zaz3 2ozod8 2 8 Z af +o a% 55 o3 2 IF 54 gg de ge 8 i &= g3 % 2 a a3 * --_ ?3 Z:2 z [HHig adednn oaaddda wgode en ga<eei <ggd ea 8 vc : 22 i %z z 8 ~~~~ : s2 g8 o 2 2 432 of F3a33 5[3i8% Zg| 2Efe d+ ad an dn 48i%gs $ g0i.s 8 * 38 fgidz = ia kN 3 =3 38 49 ~ i 24 Eo. 9 8% 20s 2 FE FF FE FF OEE Ed i FI oF Company Sanitzed. Donotecontsain TSCA CBI ~3 3 a. shed oeboasoed i sf 59 93 5% 33 2 2 3 3 == ~~ ~ 2Zl3 s 3 3 0% es en gs es ES om EERE IE i 3-~ 2aA 2~~3 3 551g --- E eo E p+ aB3 oE h 2E 8 25Noa I2 . ; i 2 = sd ssa: a. 8 lo oo oo oo oo oo 5 & i4 23 HO5F 2a3 ~3 z5 E3 o. oa 8 08% ely ifdi 1 g.0 H 3 8 oa o: a1f0f i3i iis 27 Pic CompanySete. Doecon30s81 ~ 3 I 1:33:49 : Boma i gg ai : a, 2 we 2 <5 2 eS 3 WF ab3 $ EEE i i 5 3 8 | 2: : ~ 88 LzQ f7 g d@r% uadd ea Ed e3 de on) mel 2 a{ z I oS -2a I 3a 3aI 3a I 3al :3 : Ede dS edad ad nd BiEd g| z a 23 i: 4& fios=: CEiE: E3 E i io ~ EgLl, 22 oa 83 FREER T8RF5f IZF I : id : . 3 CompanySantzed. DocsnotcontTSaAiGanl : EE SS &5 Se ee aq H z 318238 & ._ 32 3% 33 83 33 & 7 #8 2333333533 3 z 22333 ~ 4 g BS So oc oo oo sso a 2 i IF : 3 2 2 2 2So3 3~~3 3o g o3 i . sigEaiiaysl : TE 2g 9%5 He Jo oo oo oe oo 8 & id] - 5 3| BE i z2 0% i Posi Yossi 2 uh oo 88 I 2 g a23 $F FFF ORE) oe Pi ~ 224 : a8 CompanySailzed. Doss otcontTSaCAiCnat 02-5D4a2y5G:avSauglbeeShtvuondiycinToRxaitcsitwyithOneGenerationReproduction Esluations --~ TABLE 79 DuPont 11418 SUMMARY OF DEVELOPMENTAL LANDMARKS IN F; RATS PREPUTIAL SEPARATION - Fy MALE RATS OBSERVATIONS 202 (Days) GRovP: xN1umber oEfER-a1ts withVlGiven SVigInL OSE (mg/kg/day)N: 19 110 10190 110900 a1s7 a1a3 a16s a1as VAGINAL PATENCY - F, FEMALE RATS GRovP: FuImTber ofT-Ra1ts witVhEGLiven VSiIgnL DOSE (mg/kg/day)N: 190 1i0t) 1090 10100 OBSERVATIONS --~ AGE (Days) 3 16 31a4 a15s n1o5 Datasummarized as: WSetaanndard Devi-ation - a A"gIendwiavsiducaallcCulliantiecdalasObfsoelrlvoawtsiounssi,ngDedvaetlaoppmreensteanlteLdanidnmatrhkes,ApapnenddiMxo,rtality TDeastta dfaoyr +F, 2M0aldeayasnd= FAegmeal(edaRyas)t.s: Ther(ep<wer0e.05n)o. statistically significant trends by Jonckheere-Terpstra test --~ Tas `Company Sanitized. Doesnotcontain TSCA CBI ~3 z g 2 2 5 2E % E 5 2 FFs EEE 2 ig on 2% 58 8% BE 38 3%5 = cTogs a $9 nS S 68 ne.ne B : osii33s 33e 33 J &2 E . 33333353 3 8 gia ghad ss ides ddA g 28 7 Bz: FE J pple EREREDR i : 8 i gsi 3 4 iH g EEF fy gg gd 3 fF 8 81 . Company Santas. DoerocontTSaAiGno 3 g 2 5 8 8 & = g 8 i1s 55 ogNOEoak O5R5 OaN5 37 O5BEos ~ gIEf sR EREH BE : 1I4 E: g J FEg Sa ola 2a Ea da f3o GO 2a 88 =OE2E 2Es OE98 5: 5 3 :3 Eg9-i B38OE83 O8H8 8o8HoE3o8 S Zy ga g3 O38 RE88 33 aRf H8 : ii3 i ~i i po-&go.F2 8Toy38 C8E8 3 HE BRI I ign Gh hhh on FR 3 Of OM OE OH HOH CompanySante. ossotc Tso ~3 32 g o 1s uh og Eos si zg i z i503 35 3 | TE om oB os oBE Ea a i gs gar =e of , To 5%: ss 5 3 5 4 2 * i F g zgPho sFfOEaf oTst Eos Los of 1 gi = gs =F 3 i si od 3 ii 8: sg 8 3 3 3 g3iz. 33% 88% Eg8 H2 O8E3H 3st OosRY 3$ ZgcE:. 82 ga : 5" 1 igs } 513 gf LiEi 5 Fs kh ood os ks |i 2 Ep oC ER Fo aE End --_ 3 geal af MoM oH Ou 3! CompanySantis. Gossret com5a0iGno ~3 " 3 2 = L838 FSRlEo- Ies2 33L3% Ee3%s 383 3e%m oBEo : ZL 3388 BEE _EgE fgggsiiio: ~ | & gE i i = 22 5.555.85 187 :z2] ffm 8< ; -fg 972 2338 2338 2333 2a82 : gi 1 z: J i] L333 g g Ho Jn go cs ee ns gl| 5 133 --~ a294) 28 EZ H3 ft g Feiif2 Er 5 g o3 8 F f : 8 % i Company Sanitzed. Dossnot contain TGA Cl -- 3 o 3 2< 5 33 3 g -iByg 2iO2F N58%8 aO3nBB=oge d gp f 3oHEE ~ SE 3 . 3 sf sf os 2 88 33 38 38 G3 fJg &= 8 5333 ; EH Zz 23 8 M3 en : g z i 2:2 P=E 8 8%. 3 sos ous g dei. 3202 325 & . 22 32 2] 24 ~ &iM3sE i sg gz = s oR "sn pE 8sa8i3if id32 iFOHEzEoHoE Bu ig?3BE Company Sait. Donotscatsain SOA Gal ~3 33 g z =4 Te pp BEB ) 8:% 35 3 4d @ I o3 jg: ae ~ 3 FoF oad J 0 Eo:Thn F BT EI E : z El i : a Eekh oslid 3 g Fr c Tid ~ a3 gs ik 5 3% FI [SS ~ 2 : i i 5eo fei o=aep + | 8i = i | 5 oat i g Ri bog ~ 2 2 aE i i j2 $ Je2gS tafe ofPdBE 8 .51 ia qs Ed 2 ii zgh i [PI d 9 ai i . 33 i i [I] CE 232s ~3 H LH ye BE dE Company Saiizod DoesntcontainTSCAGot ~ a t i i i gEa iifsel; o - oc so || 2 i |i lgef oe 0 ooo 0 i ~ 1 285= LEH IRA i: 3 gi g Pog 4 Sf i 2 E.81 | | 1z g5 ughl {a if -8 3 HZEs 37] ~ 322293 8i : gd ii HFIf Hsgeaatgiri8s FaiiaElga I. fg iPl8 gi[I f 5 00% Company Satzsd. Does otcotTaSCiAGn1 ~ 33 3 ii i| ii ii g2 ikgoi. | 2Ed |i =i | g Non i: 53 Z2 i Pi oda a p 7 ..0.. [I i - 8 [I HI EE LPgE 3qd EI 38 i. Pf si |i 1dod 1232] siiiExfrliio d 3. ' : CompanySizes. SonsrtconanTso co ~ po 2 io gb 2 BRR} i Fd :g fgaiid| zh, ~~ 5&8RZ) i P iR d gf2 S2i0. og I e5 i 8g .di iE gEEgxE8f | 33 2 & aogi og gI g o3f EiEiRt. PfoiirEE ~ &343 BEiie2i0fg . 3 ! CompanySatz. oes ocr TSCAGO! Sloi ro oTio uik ~ legsE g i - : IF: 3 5i i gciun g fl f3di9 Eg a ad: 5 TIE PEE PoPolg LdEk Lid i Seng [oLn He fled }!|i Hhhhi i A ~i ghgrRR RRITRE LE j Po 3 gq i d Lo Sind :i = ei i =i Bi Ph S2 udi Lad: a. oiid i58 : Eleaf cigo Pi wal a. :; i ouh LS HE LoGgk 3 Eg i 1 eh 3| zzill 8 g sie H1 oifnx, W0H H TH g $a3g 2 RdI, ETmTig p BPH g Bg p ofEE dfs HET | Wha oreie i HH Pa b gfpHl FIgHE sg gShp HidEs CompanySiz.ooes consi sca ~~ g 1 : i HE Lio Ll Tait Lie 5 8E HieE ii F igT]Eg ~ f E 82EaEfl liislda < 4 gid ian 4 | gS SH aal3idl Pid PPEEE ic . 8 Ki i gu i giHI } i i23 giPoEaii iH REE EE ii gHEREARE ~i Big" Bio: Compass, bore8Gs ggq ii. iHdg Ea iis Poa ih fiiiss ihianl iat Pia 2 : iz a | i 2 1 gi Pi ida I TH jE i3: i5 3d ~ 24 g ii gg ii t, 2i fEiE,S fle dy Hig g ialfa B85 OE23 4 . PR . ---- ~3 i i 3 ! ! i fg 5EgeE5ldT. T2 TCC gr. Z.iggiizoI:c g dF: 8 gesin oo oom wiiigdd eo iE 8 HBiE. d HE ighld --~ B8 E8g .EsifR77c2o iE jigos a <7 3 cid id i bios 8 .8i : J C8E&gRaaLleii gi BH ai Pii3dg: iisf PPaEsn i.e i g i007 23] 4 i8 1 2 Eig 2 n B41 8 2 2g gi 2.8 Foi LH 1a Company Sots, boss con3a0 n ~ ii i }i z i ii j ig SERRE =Iqsihcoooc nooom EiiE iyd i427: [HE Sol E 2 iE ssossLL ieidg:i : 2 J1 i 32 2 i 2 28 ~ if5 giB5n1 8 ae 8 5.5! %9 Eifi: g 8z i|i } iad iainfal i 8% Es . Pi ew BaEn gf 8{i8g87i fo fae Bg gHigE8 i ge if ifEelilg 2 og SHige EEgh gf ggiif 3 ] [---- ~3 {Pd e | if z Tesi iJ Zo Lil ~ JE2Th gz oo hIgEh Eid PE 85 j i728 3 i 1 gss il iEsBns EI IH EH i8] i3 3 2i} ~i 830851i iiPsaaew doo giPg ifai ig 20 Fa gHiEgRfEeiigds Be fB is . corpses ema `H9205-4D2a5y;GavSaugbechSrtoundiyc iTnoxRiactistywithOneGeneration Reproduction Evaluations --~ Dupont-11418 ~~ FIGURES --- CompanySanitized. Doesnotcontain TSCA C81 9H02.5D4a2y5:GavSaubgeehSvtoundiyciTnoxRiactistywith OnGeeneration Reproduction Evaluations --_ FIGURES EXPLANATORY NOTES DuPont.11418 CriticalDates Day 72 Last day data from the male and female rats designated for reproduction evaluations were reported with the subchronic toxicity animals. Body weights and clinical observations collected during the cohabitation and post-mating periods are reported in the Reproductive Toxicology section; Dose volumes administered during the cohabitation and. post-mating periods are documented in study records. Day 90 Last day of test substance administration for male and female rats designated for one-month and three-month recovery periods. Day 91 Last day of body weight and food consumption data collection for male and female rats designated for the subchronic toxicity evaluation Last day of test substance administration for male rats designated for the, subchronic toxicity evaluation. Day92 + Male rats designated for the subchronic toxicity evaluation were sacrificed. ~ Last day of test substance administration for female rats designated for the subchronic toxicity evaluation. Day93 Female rats designated for the subchronic toxicity evaluation were sacrificed. Day 126 Last day of body weight and food consumption data collection for rats designated for the one-month recovery period. Last day of food consumption data collection for rats designated for the three-month recovery period. Day 127 Male and female rats designated for the one-month recovery were sacrificed. Day 182 Male and female rats designated for blood fluorine level evaluation were sacrificed ' Ee CompanySanitized. Doesnot conTtSaCAiGnBI ~ 3i FE 53 153833t 23 [Bice ow - i. : 1 Rk : lL 8 2 hd db 22h 2 g oop _ 3 2 iIz 38 EE 5 3 sig WeX S itz 1X ie q2 x a8 < | B T TRE : ig : 7 . 4of 7g 3 23 _ i28s 2 gz } NWY |[ L5i:g WyN 3 TEE i Ng 3 la 5 I: 8 [= 4 CEEEEeea ! - gREEE5 RronEfpoEg wE re RERE CompanySaritzsd Dooteconssi TSAOt z 3I 2 :z : a5 ~ Jn g25 e83 2 a2 23 8a 3 2z J2z 3 : $2 22 HE i ~3 #8 i =2 E>E5S3] 3 2332 228 REAL 1% [ TH FER nLaby 22 2 g QaX le if 3 n8 N\ 31 W\W Tt .- %\x 5 $ Fi2 E N5 Nk fs lo5Ce23 I'E 3 gs a re | o2 lg | "To [ X * -- :- wtApoo wmo CompanySantas. DoesotconsiTSCAG1 : z3d3 i Essg Baa z3g z g ~ 2a Ei| H E 1: &iS : --{ | | i 21 : ey 5 : i 2 id i Tf fos 5% 2 i (BY) yuan dup quasog i g 2 E588 Dosw z 5= F i3 : Z =J + 3 E02 8 E2 he 232 v ER] : rr |= 43 z 3i Hig Z ii 1 at 5 i EEEEEEEE 1 i (50 uttdiaqnos Company Santis. Goes ot catTSaCAGnBI Z 83: 8 z "2 Hi5543 S2icasmg --{ 1 3 ] j g PR HE 1 i2 8 8&8 23 gz 53g &8 25 (3%) wiuang duo qupury CompanySaites. Doss otcata TSCAGB ~3 2 ai 2 gE zE ~ d gh 2g Eg]% iF 2 i 3 g ghi z & i ig 3 ~ 34 iilEE Ecst Gooa i |& of2 ; 5ge3 ' i z 3 i = ac JR HEINER (@) wavans dup quipugy CompanySanized. Does not contSCaAiGn1  zg 2g 2z 3g 52z= ggz ~~ J g8 i3E g 8 2 z g g HI2g z 2 Eg S2|3 ~ #3 =8 Hi F[E7E8S EgEaEanE gFy 2 --1] 1 24 iPY i g7 ii C1 - F Priae mels 1 3 000 2 fon many eng Company Saized. DoesntcontainTSCA Gal ~3 Ig 2 :8i 3 45 3 & 42 i3: 3 HEH r --~ 4244] Z| 28s8g 2 < 23 23 3 5 2: gg i ooam i: -- g 2g &g -- z5 8 g2 E5 z & a2 4 xE . g:z 8-- a (soswasjo woprn 5 |& 1 b 2 . PE] : 8 7i2 3 3z2 i 33i. : z i CompanySenta, Does etcaTSEnGS! ~3 : 3 :5 zg Ei =& &g /pe g2 23 gj 28g 3 ils23d Gaam ; % . i i3 -- I =r2 fd| ii ' i 54 5 :i 53 i 3 _ EiE : 2 3 a 2 z2 g. E i ao :F 2 LL] 5 2 gs: 8es:8z8sonms CompanyStd. conconanTSACo ~3 5z3 g := g 4 3gZ :< ] = rd . g2 2@) N55T285Ed3 233 ScHaEmE ---- [3 2 --| I 32 .J Cos g Lr <; 2 3 $ i: 5 i 33 ~ 2435 = 4 = 2 2: g EEE Cg g Is 8 Sg 83 :838:z868- = SwaJonanmy CompanySats. oss cont TSCACo H.25425: Subchronic Tosicity 90.Day Gavage Study in Rats with One-Generation Reproduction Evaluations --~ DuPont 11418 --_ APPENDICES [Ce -- Company Sanitized. Doesnot contain TSCA CBI 9H-02-5D4a2y5G:evSaugbcehSvtoundiyc iTnoxRiactistywith OneGeneration Reproduction Evaluations ~~ i APPENDICES Duron 11418 EXPLANATORY NOTES Critical Dates Day 72 Last day data from the male and fernale rats designated for reproduction evaluations were reported with the subchronic toxicity animals. Body weights and clinical observations collected during the cohabitation and post-mating periods are reported in the Reproductive Toxicology section; Dose volumes administered during the cohabitation and post-mating periods are documented in study records. Day 90 Last day of test substance administration for male and female rats designated for one-month and three-month recovery periods. Day 91 Last day of body weight and food consumption data collection for male and female rats designated for the subchronic toxicity evaluation. Last day of test substance administration for male rat designated for the subchronic toxicity evaluation. Day92 o Male rats designated for the subchronic toxicity evaluation were sacrificed. ~~ Lathsetsudbacyhroofnitecsttosxuibcsittyanecvealaudamtiinoin.stration for female rats designated for Day 93 Female rats designated for the subchronic toxicity evaluation were sacrificed. Day 126 + Last day of body weight and food consumption data collection for rats designated for the one-month recovery period. Last day of food consumption data collection for rats designated for the three-month recovery period. Day 127 Male and female rats designated for the one-month recovery were sacrificed. ' Day 182 Male and female rats designated for blood fluorine level evaluation were. sacrificed. . Abbreviations `gmagn/mkigd=aymg=/kggr/admasy/animaliday Note NAbMse(nncoet omfeadsautareidn)dimcaatyesbtehereapnoirmteadl iwfaasn naontimaalilvediaetdthoenttihmeeodafydaotfa2 csoclhleedcutiloend;weighing. -- ES Company Sanitized. Doesnotcontain TSCA CBI H-25425; Subehvonic Toxicity 90-Day Gavage Study in Rats with One-Generation Reproduction Evaluations --~ DuPont-11418 ~~ APPENDIX A ANALYTICAL DATA --~ -- `Company Sanitized. DoesnotcontainTSCA CBI 9H0.2-5D4a2y5:GavSaugbcehSrtoundiyc iTnoxRiactistywithOne-Generation Reproduction Evaluations Dupont-11418 --_ SamTpalblee I. RecoveryofH:25425 Added to Dosing Vekicle "mg/ml F.25425 Percent ES Fave No1m9i6al ___ ML easuraed s No7misnal RReeccoovveerryy 227107 116815 52 RecoveRy 245 192 Mean 78442442, cv.e% RecoveRy 191 164 859 RReeccoovveeRryy 129074 1177.41 8884.11 Mean 8c6v0.22%0, RReeccoovveerryy 118998 119715 99256. RecoveRy 192 m Mean 98298137, Processed withhomogeneityconceniation verification samplesfomdosingcpvre.paarned on est da2y (October 17,2002). --_ P(rOoccteosbseerd23w,i2t0h0h2o)m.ogesitylconcentation verification samples from dosing prepared ontestday PPrroocceesssseedd wwiitthh ccoonncceennttrraattiioonn vveerriiffiiccaattiioonn ssaammpplleessffrroommddoossiinngg pprreeppaarreedd oonntteesstt ddaayy4826((Naomvueamrybe9r,22600,3)2.002). ~~ - ow Company Sanitized. Does not contain TSCA CBI 0F--2D5a42y5G;avSaugbcehSrtoundiyc TinoxRiactistywith One-Genersion Reproduction Evaluations DuPont 11418 --~ TableSIlamHopmloegeneity/Concentration Verimfigc/amtiLonFa-n2d54St2a5bilityof H-25425 in Dosing SPuesrpceennstions Type Test day Nominal `Measured Nominal Homogeneity CovTroL i, NDA) i. Top 2 136 680 MDLE 2008) 187 95 Bottom 2008) Mean: 210740:+0.34 (5170.000%) Tor 2008) c1v90.19% 950 MbLE 2008) 208 1040 Bottom 2008) Mean: 221034512 (11020.605%) Top 20 1c8v7.e% 95 MBoorbriows 2200 191818 %95.05 Mean: 189 2.1 (04.5%) cv.1% 5 Horo 22000088)) 183 217 91s 1085 ~~ Testda9y 20 196 980 `Homogeneity ConrmoL. MoTDoip Borrow 000 NDA) -- 2200008)) 119877 99855 2008) Mean: 119921+ 005 95.5 960%) cv.2% T Abllereewpoertteddreesueltesdcorrected based on recovery ofthe spiked sample (refer 0 Table I). cToheeffaivcieernatgeofvmaeraisautrieodnocfoncoepn,trmaitdidolne,,aavnedrabgoettpoemr.centofnominal (i parentheses), standard deviation, and Stabilitysamples held 5 hours a room temperature. --~ - ws Company Sanitized. Does not contain TSCA CBI 9H02-5D4a2y5G:avSaugbecShrtoundiyc iTnoxRaitcstywithOneGenerationReproduction Evaluations DuPont11418 ~~ "Table IIL. Concentration VerificationofH-25425 in Dosing suspensions Preparation Day mg/mL H25425 Percent Sample Type Testday 42 Nominal Measured Nominal `ConcentraCtioonntVreroilfication 00 NDB) on 20010 235 7s 20020 Mean: 236 2320.10 1180 as.) cv.04% 2010 205 1025 010 8 1040 Mean: 2c0v7.01.%16 (103.5) 2001 002 190 13 950 965 Mean: 192521 cv.1% #60) Test day 86 --~ ConcentratCioonmVaelrification 00 NDB) tn 20010 203 1015 20020 204 1020 Mean: 2c0v4.o0s.%01 (102.0) 20.16 196 980 2010 218 109.0 Meano: 2cv0.772%15 (103.5) 20-10 2010 20 0 1045 101s . Mean: 2c0v6.2a.%40 (103.0) . DuDpelnioctaestenosadmeptleecstepd,er level were smalyzed. Mean, SD.andcalC.Vc. ulated to verify uniformity of mixture. AMlelarneproersutletdfroersualntaslcyosrerseoctneddubpalsiceadtoensarmepcloevse.ryofthe spiked sample (refer to Table I). -- --_--_-- Company Sanitized. Does not contain TSCA CBI 9H0a-sD4a2ys;GavSaubgeehSutoundiyc TinoxRiacttywithOne Generstion Reproduction Evaluations -- Representative AnalFyitgiucrael1Calibration Curves 3000 Equation for the fitted linc: Jap] Y= 52267455 43155285 FX R-Squared = 09970 Dupont 11418 g 2000 255 150 fu -- 50 ! vz 3 4 5 8s 7 8 9 Concentration, mg/mL Figure la: Cmaelaisburrateimoennctusr(vsequsahroews)infgorlicnaelairbrfaittiloinnseo)ltuotiroenpsliocfatHe-p2e5a4k25hediiglhutted with THF over a concentration range of 1.897 to 8.672 mg/mL. --_ ----0---- `Company Saniized. Does not contain TSCA CBI L25e05, Storey pment ~~ Figur2e RepresentativeHPLC/GPC/RL Chromatography Chromatograms R TO R : P preReps HPLCo IGROR chroo0m00tic.dginrspianin25625 ~~ rr i RIDTA,RIDA,RefrInadec xSitgnail(v 112e602 508010) | . | | re 2 Rpeptresrent HPLGomIaGnoPf396C1myIaRlt]s ern soon ss So, Ss ety Ast i Oe etn Rion Eins Dirtias ~~ Fi2g(countirnueed) Representative HPLC/GPC/RI Chromatography Chromatograms gq ~ igre 2:ReoprescnaoievneHaiPiLioCnIoGPO9I000hmmrootmsooHgmEoSf52.00mTitnm.edsousrinegousmenesinndoif d EE 8 || | - 0 ENrs2mosonbil4 saevteon5s1o9fen00am 8 T oIL e 15-- h To msedc14o_meienin P------ H25425; Subchronic 90-Day Gavage Study Toxicity in Rats withOne Generation Reproduction Evalustions --~ Dupont 11418 --_ APPENDIX B INDIVIDUAL DOSE VOLUMES -- 5 ~ Company Saritized. Does notcontain TSCA CBI 9102D54a2y5G:avSaugbeehSrtoundcy iTnorRiactistywithOneGeneration Reproduction Evaluations -- INDIVIDUAL DOSE VOLUMES DuPont 11418 EXPLANATORY NOTES Critical Dates Day 72 Leavsatludaatyiodnastawefrreomretphoertmeadlewiatnhdthfeemsaulbechrraotsnidcestiogxniacitteydafnoirmraelps.rodBuocdtiyon weights and clinical observations collected during the cohabitation and Dpoosste-mvaotliunmgepseraidomdisniasrteerreepdodrtuerdinign tthheecRoehparboidtuactitoinveanTdoxpiocsotl-omgaytisnegction; periods are documented in study records. Day 90 Last day of test substance designated for one-month aadnmdintihsrterea-tmioonntfhorremcaolveeraynpderfieomdasl.e rats Day91 Last day of body weight and food consumption data collection for male and female rats designated for the subchronic toxicity evaluation Last day of test substance administration for male rats designated for the. subehronic toxicity evaluation. Day92 Male rats designated for the subchronic toxicity evaluation were sacrificed. ~ Last day of test substance administration for female rats designated for the subchronic toxicity evaluation. Day 93 Female rats designated for the subchronic toxicity evaluation were sacrificed. Day 126 + Last day of body weight and food consumption data collection for rats designated for the one-month recovery period. Last day of food consumption data collection for rats designated for the three-month recovery period. Day 127 Male and female rats designated for the one-month recovery were sacrificed. Day 182 Male and female rats designated for blood fluorine level evaluation were sacrificed . Abbreviations mg/kg = mg/kg/day Note Absence of data indicates the animal was not alive at th time of data collection. --~ ET me -- `Company Sanitized. Doesnotcontain TSCA CBI ~ FE Yi a ll 2 = :i : ef i [22 z 150 ppp ea eer 00 F obbibibLbnhMLRbLb Lbb RbRELLLL LLL LLLRo omnia 80 8 joEf 2 0 [EE : CETINTIIIIIE: EIOEECLeIEOrNSEeCR:E ;[2 E: pppppppppppepepeeeep epesa pene 5W2o 3 2: ororoorooonoooonoonooninins 8i .8 i= :E2 ~ JE:r orroorrrrmTmIoITIeIeRRsIrIIrIrIIrIIeseIIeI SSe55f i8 :E Aor3 prrrrremeeesccoeeeoespespeeeeer 5of1f 0 i coroooropnImIIInIIOOIIIOIIOIGIIeNIrGeE CY PfES errr i SRIEDRIICIEIDDIIDEDEDEMEIIIIDDDOEOENY 5CY i 5 6! oonmoommonmmppnmmenmmaninnnssmnmann. 5d | SINIIISIINIIIITIIIIITt IGRIr IIIIOe REEIe IEET OHY Hy ~ i{ Company Snized. Doss na ona TSCA OBI --_ . --- i 8: --~ 15,8 SLELLER FF gle? PE c [82 creer 2060 EEE . frseelli f 2 creer 2,8 ::2 ceerer ges 24 |F 8 co conn 4 ff 5od 58 freeeillig6 rorrree OH monn s8d errr 82,48 5 E CompanySates. Does ot ats TSCACl ~ ~~, ~ 23323235538823333335833538308398388 z FE iittala PE B Fle? NY i ems: a_ 3 i (fE 8,2 5 CLCRLITIR IIE. mmm. rpmremeieeei epee hbk bbR bE verre CICELLODIERLOIIIRLOLONIINNEERE. 8,8 i 8g 5 4g3 R[2E 5oPE8;BS|E 3 8 +} 1 3 gE [tH HR AAA : : CompanySatan. Does contSGiAGnB --~ } ~~ ' ~~ i 825222555522228852282022020200222282228 , 2 ssn perrRE PEEPpEEEEppp per deSsFl]HL EEfEeEef gt 553 CENTRIST IRL LIER fs 8,8 H CLIIIIL IIITY ] cms 5 CF |2g errors eHsE |2[B8 perros. [3A 1 f CELIO (. EprIITIII ) 2,8 meres Hg Ez Company Sanitized. Does not contain TSCA CBI ~ ~~ ~ 233333222223220a2a2sa0as00000000000208 zz ex SHS REE oppressors m-- CEILI REET ERRRTTIILTILIILIIIIIIIIIIIIIIIIID CLELELEREIERLLLEEROREEIIERIIONANLEL LrErLpDLp UEEITCENSECp IICERNNRIICs E IIRERite conn li E4E: 8iF[EE ; ,8 : i ge 0 | offZ [E o8C g oELoIEIIITILILILIIIIIIIIIIIIIIIIIIIEEE 1o]h & 4 fti p r e = 8 Hlo i CompanySonias. DoeracenaTso1 cozoeoeiFtRIfol; EEEeE Feil ossasd 5 : cereeee 8. |g : ree 2 H: I | 53 mmm td wom 42 szingr osgf4 ainininine s CompanySaritcad Doss ncaaTSGA Gat ~ --~ * $5558552255303350800305335335533358853 gf [8% BEPESRAEEMDISSe=TEv ERE, o 5 [oF FcoArRrrmmnArnAoAnoArArRooRRoAoAnAnAnonnAeRnRrnAnSen 18 5S"Edl)0b, FCBiEF 2 5 [iattast cians riiitt einai ETEEIEEREIIIEENISEEDIIIINEITIONIT srrprorprrerroreeceeeeeeseesoeeese mmm 5 i 5,8 24 2 5i 1 SITU - 8 V3 z : Gompany Sanitzd. Does not contain TSCA CBI --_ ~ 45 ~ gs$3e8a5n8a5s% 2 fLElEEEd perpen 3d HgIEN banainiin iEElEEE 5 2 coommn prpnngy errr Baauuay SeEe8fs2:ff35|[E3 FEE Eg : Sxe8g 32 2%2 EE oe H Laalini rere BaauuEy peeeeer 1 BsEOfE |G = 5e iF 508 0 pny Evdf preeene 52,08 g serene 3%2 corer : v :H [A ---- : ~. 5 &y% igs eerrremrereeereee pLoRnInnnITnEIRI III RRIIITA, cere Snub shekaachuaaaneIuAIALan Te er corrosion PE FEE o. E :: oli of bf LbhmL unb aanh IA b Nb A An RBa IRAN RBRn E 5s SOLER rornrmS remL eeeE eesS eesees 3H : ~~ ; CorrySos. consti ~ ~. f ~ 22222222222220222222222222022022222 & Z|8% oseoismrmmmsrprsmmensmzonzomozmenznes 4fgE.3R%E8 LfCF [[leBifEg Fed rSEeRpLeIIrRSe IIDIIITp DITIIOEe INICINNe IINIID 5%8.86 0 6 [[2B5E3 herr TET eeeey OF8 o: g8 2 rnp reprny F : serereeseneee e. e bE g 5 |g i sree 5sf @ :JF i SEDLDNIIDUVITIETIUIIIDIIIOEIIIENGD 8F rsh 7S,F8 nmr eer ppsprresenenyy SP2 z Company Santzad. Dossne contin TSA Cal il -~ : - 3 33333599000558535385235535533558888888 & zg ex 3RIIBSEISTFTBIZILBIRRZIIZEN: 5,T i L:ire TIIDr IEDELEELIIENr IIIONORIRICr CIONANNENCS 3s LEQFF :iEEtss i ig NE E32 F oprorrrTrarrIoIIIIITORIIIIILInIIININ :: 3i 0 fe 1 5,8 i 8 Lbhuboesstnsavsuanannutnakshaseuhuiaye corerrerrmpprrsmrrr rere 04 mre. Lf4 58 [|8B SoLpDSpDEsREsRCeLCnENReIRtaneRRnniEmLnnniieiintinniestt 0% I : [2 srrepprrrr ree 3 2 5 . SCITEIERRIIIIIIIIIIIIILIEbNNREIINALED % Ey 2O,F1 very OH pprppspppppEEep Erp bg f Prestttttetttimapit rapt iaiit a tiine gf g : Gompany Satz. Does nt conan TSCA CEI -- . --~ 5 : ~ SEE cspreinet preeees annie Cpr eee TL IF i iles o8=y S 8,8 oER[lEe2g 3 FEE "E 2opf ff t5 i fEzBE = 2%8 z< ni 4 | ie BLIrEruuns fo: &|2 bf igEE mmm gt oF 2 Ef 0: g -- I corre 58,08 UT 5| poz 5wd spewene 80,48 5 g CompanySante.Does not contTSaCAiCnl ~~ :~~, rr no20a2sszagazs 2 = HH HE HEH LEE rin ttettsoe ot tEI5L,A00IN RE NIL epEpRApprprpr-- Li! c ifiE:E : copper 8 i SL CELE Spy.. oo : - H YY b WH 5S ow RSA . g 2 Gompany Sanitzed. Doss ntcotan SGA GH! --- : = 2 ~~ scusndsr 2 7 5 LeRisse FR fof |2s8E% gle? 52 ' 1] wom : : 2,8 ] papErEoNsNnEr wvu EE i= worpEms &2f sgs whombNE z ppp ge o EE Q roones OH i 2 mommy sd2 women OH : 8,5 PTR A g = CompanySaitzad. oneotcosntin 0AGol ~ ?' --_ RISER IR REE os jes SRSSUISEISISSNMSUSIUIRASSIRERans : Hi copsrommnronzonnzoonsoninanioanz 4LEx R6 GRC ElEef Sy Y HH : vigf,8 iS FT. 8 i: prpprsp esse spypr ee seseseey 6308 55 [[8E prrpp irrre Erprrrepp eops rvoryy O083 3 I|g ELENSLURLERE REELotEERE NLELEREERLEY : romp perpe yen s GH2 i ersmniy. . O8 8,1 EEE ESE NEESER ENE gf PIERRIIRIERIERIIIEERIEERIEERSYRERSSEY 80,d1 Ef 8,1 pnpnoRnIIIIIERRIIIRRLIIIONRLIIL % : Company Snitz. Doos not contain TSCA Cal ~~ ~~, LLL soosasannansssanananas LL itisia sopppsee eps eens CONDITLCTICIRITICIEIEIETIRINSILIILT 2 Erol oy TI get = r Hi lie 2 zz 2i : 5: FE sepsis ed QF 2,8 jis fatetittinisnsisititistiitinaigy Pa Company Sanitized. Donote contsain TSCA CBI ~ 5338580008005 300000000000000030308838883 8 52 ps3xH emmy | OL sCr ieR r n CL reveRree: HE [EE SEfl fgekb ila Coor prmpeesepesseneeen w 30 l; em. Hf BA EmaLAA vee 2--- 838CFfR ~ CECHIICRISUIITIIOI LILeY ee M 3 | 4' - a.0 een conn emmy <1 fg - : CompanySanitized. Doesnot contain TSCA CBI ~ 8 ~ tritins 4 SREBRER < z 8,8 was mmr gSweeiit 2IEH : lo % Flee s |E3 3i[szfpEg souoooa oF 2 woe 8,8 =: ome L2Hf:EJB[2 LELEIeIeT E ge EFEE : 5f propnpr oe 8 & peppner [oidH ef 2 prnnze TwEdS o2 = CompanySanted. Does not contain 750A Gat --~ ' ~ 3 $35300E 000I0E00N0E00EE0RE0EE 00P0RR0ERESRNRN ERCRRRRRRRRETRRRSERRE * fgg SEE jrtteittttttdttiititnsiitdittitiittdl: ILL HE 5 : pM upppppE spepS epssspE pussssS pepesneney L50E8 E E[HEEEE jetddinndistictbttittisisitiinitainita 8 by 5 2 SP UTTIRIP RIIRITP IIRIILS IEIODEIIIp ERIy ONON. LY spspmevsmmrmeepnesnevznennevnezy esses. O8F2F g2E LoEd oz |fgF iE E +8o1 EfF SRLDIIDNTTORDERICTSTOSORIREIDODIONIT ed SgrrnnipnnnIIrITIITIIRRIDIIIIIIOIILIL 3 se DRLRIEDITIRIRIEREOEECIOSIIIRRSIONINIIC 8 o* 6, DRIDESDERITUILERERRECURIIIISISIIDINIID 8,8 SEE & CEL IIRL I I RN ssE npeny 78 z e-------- CompanySanitized. Doesnot conTtSaCAiCBnI -- 3 _ ~~ ee fmt $58%3%8 E o2 lfdF pone L2 EE]sf 1EfEi2Ee7 Lakblin i E28 sens E 2%E0 F: IE2R7 woLo t2e.i8 oF 3 wsoepprnney 2g,E8 i=: powsens poorer 2725 E EJE gE 28 fF tt sagas susmses susmmsn Eg SEF 8,8 ef 5,8 20d $ &f wowwnny 378 i CompanySaiizad, Does not con7t5a0AiGn1 -: - sozzansazassansanzesianzanas i i5 iE NERENLEEEREIRESEEISEEEIINRCIEREIRLNELDSIEIEIIINL &3 83| prnnnomssnonmnnEnInr 8S i1 28 i: - Cone pERuRImmeEREERRENNEIORRRIEIRIINIS : PELUIINNIIUIIIRRNERRTIIRIERNRNINLLY : o LORLr RDCROILCLIEIDREILEECRERIRLREISIIRRIIsEeRpRpIeInSeIrIrITr g o 5f % i2g 5f=:F SENTRIILIIIIDIIIERINIERRIRVREReIrOIeNsY 40: Jf oo 5i DERIRIRLIEIIIETILIILINL oe SERREEERIRIRIILLLY I. uf| LEERRERRSSELELIRLIILLD oe htt tittttatn tntF td tn ts yo| jt tttttthtittttt ttdtaniT tide T e sie | o i = `Company Sanitized. Doesnot contain TSCA CBI ~~ # ~~. - $3293585588553332355555255535885388 Pigs smmrpmmmmmosmmmmmeszsensonseeeeny Ji sovennmnpnonmmmnnnpnopeonzenanany sf JER 8 S pomppmsuuussyy 2 =: a5 0 2 sr spmpsnsepspp ss NomhoRbhNNNEROWH RF EORRLNHENEUNOWI aE 50 [2 51 55 poppmommmmmRERERnnmnbnnOnIIIERERY o8f borospssmesse usy 22,08 8 BEEMEENENERRELRELES SELES EEEEEEES SY 2 g ; Company Saiize. Dossnotcont75a0AiGn1 ~ sFgagHgasAgEmtE sipasssasamcsimsesamcassssinazzaannse iaEiseaassaanasmzaassEsannsisiafi ra slf p{ [5|%8= -- EEEEIILEII-- LIIIRIIEI-- IIILILLEY--:gi] fPl iit susmmsmmssren ene E5R04A [ER rE 2g,%8. S LS SSTry T,Ef ES semis ee 93 18 [|8 ~, neo: |E RSpEeepppppprpppspprprpppRpsReorreney 58 :EF |B 2,5 BE EEREIE IEIEEEP 88 SupsEEsEuNsERESsLsLsESLSESSESESSESESES 5S H ~ i (CompanySanitized. DoesnotconTtSaCAiCBnI --_ . ~ ? ~ anise Hh op pes es sezieyry Shs fed Foon fin swomneone SPE 0 5 [E2E Cen 8 ?2 ne een od i; aunnseyr waeee 3g ] [iiI EZ HPEE .. BiH enn 2 FC coves Z 2 supmusy 5 z = Company Sarid. ossnotamanTSCAGE! 93333235595335055005088 3 semmrernmenmennennn i aSadl S2RIINANNASES NIRA 2NIURRSILABILS - = :2 fElTie spss 0 8 [ER eobeve sss 48 S[8 Cs ELLUomm IIe RLs 2 J;E spmpmprroemsenes 8 g2 w1u [8 ~ wenn 08 } sppmpeppmm----------ery 5;$,7]8 3 mI 58 8 8 smear oer H oF gfg - = Compan Santas. oes conT5a0AnG1 sevens igs] Ef aK i ALehaini Te A : ' poner gr of fe spsmonn 528S =5 cwoeree E = 1B ~~ ememem sdf1 fF| ; I 5 woe 4 ovens swowppnann 83%8 i Compan Sonics,boetscansa SoA G1 BE3833H 33882I 3R0R0nnsI nnsnsaR nsanss fskxt se com si mos s { Pe3e5lOfEl3e6 seems oosews T ppsmesspssspssssssssinussns.huny goHf [[EEEE 2g,g8 z: IIELIUEIIIIITEIUIILIIA Ie IS f ;E ppm 2of11 Of| ~~ SENIEINIENIv IIIRNs LII Is ES B ge E iF j WE g oe 22 eH or 2 = ; CompanSantas. oes conTann01 LI f ~ sozzaas AESERRECEIIRBEINERELERRESE AE 0TEIER pLeopnrsrrespneemreRmRmrmLmyvrnrnsepnsu zsm nnapnes ny DLINDIENDIIIRIIIDIREENRLRIILIYDIRSRRODDSIIIINoLwLnLsS prRTeT Senay me 3 7 : L. HH SEg6 Ro HlB[igE2 E e37%8E0:T EAfEE[7EE 2,8 - STE 3: no wr fettdisiodsiipimiuasnistsinnnssninssrssstintseesneueneaesyy 504 3[I [2 eommssssssnpppnensseossny goHs 1 [|6g [Rtttnsdiiiiaisistnnsisastteseniasy : poppssEES EE sEE Rsy sE pppmEssERusE ELLE E2 f i 650 8 sppsEsLsLLsEE RLsLsL E 20 1 itn taednd 2 Lo : DERDEDDUDNIRIRDIIDRDIRRRIIRLNIIRENT Company Sanitzed. DoesnotcontTSaCAi0n81 ~ g2ocnssansasanoasasansaasasnsaansnaas 2 = sai] SeNlNLNiEbNiNiNlNeNiNiNiEiNiELIbLiN eatE liE llS inEiE NliER lEnS 48 a8 88 ifs i= 3i fpf isp rinpmunramRoEnRIIIIIERRIRRTIRERIOIIY 8% HE B . 8 S rmILIIIIIIERIORIb IIeIy R : 2 | feetittttttitetbtitttiebiottetbpt H Pf eos |f SORRLOIDERLLREELLEENSERERRERRERINER Ef 5 CE ~, smerny. wf 1 ' 8 snr fF gf 2,8 suznmnanmasTRmNIIImnnamImnnNnznaun #E sppensppesEsEEEsEEsSsESEsESseEy 2gd, v ~ Comrades ekTan ~ oo; -- 2383338 gf [8% 5 :le2 FL ev 8 $ElEsEg mnie TI 2 sowwene fg5g25 26 0 B[E 5 [EE amnaninn = meme ef8 fSb mo ne 4 5ff fg Lis 5 mom TI F 2 Cl ot Ei W g 8,8 one Labial 2 Hg 5 5 CompanySorts. Doe recot Toco ~ ~ : ~ $385550800553555000055550000088355288 2 EH sreermierssesstersnerenveereney e3I% fRElEe SEL LEEL LaE bbaR LL nlE . i ti} wrens of80:4 JIEEER ERpEyEmEmEEsunLs sR ESSERE sree S--RLC-- CITI_RIU-- IIN-- E i --L --L --R-- RReN--Ini-- Eiy LIIEIIRIIRORIIEITINIIIRERNERRENLRYLYY LnsnmmIinuIIIToTIIIIIIURIININIIILNY vevprnere 22 e8Z 5 H 24 l 8 [0 nh ET .8 E : f+ 4 5of 51 sonrsppprerser revere g sSIeIvErDIrRsNrIeRIsNrRmIrREvReIRr RRIBLRIILRy IIRILLNY 2 :: E CompanySatz. Does notcont15a0AiGnBI ~~ . _i gaasase fEE sens | A !flief sowswes al Eg 275 0 EEE Lp =< me: m 2eo hb z g mmm 4 2 g2 vores oH 8 popes ge fF SE fff we 42 pone 4 1 g pitta 2 z Compa Srtin boutconn scm ~~ a SEESSRIEECRCSCICCECHBEBCOERSRIEENIE & 1 oR spInninunmniiinninmsacEanaeneee 8i oS 5fF JEIg ~ ` sm. sovpssmissssss pens EEE EEEEEE PulLbbbaunouanrab uns nab oR no a summonses eb 2. 2 ot : OE : LftygEIf %i 7 HoFf 5 8 g ' 4 cmnosvsenrmsosnsnnIRnInnrny befy ita.ssittctititieinirotbrerootiiroli 84| 8,8 ressarcisseistesiintirn roo|l SrmmENCusSEESEESEESSSEEEESeeSy 5,8 S08 s ~~ : CompanySnitz. Dossne containTSCAO31 83335380222 0ass z EH smmmmmmnmmsseserereeeeeeeeneene 5% ERE . . - Ef q QLLTIIIININNIIIIDIRIIINIIIIIINLILIIY ; Lf E frittitididsnttitetitttitidtit tii] i 2,8 Fa SRIRIIIINIIIIIIIIINII IEEE, 2 8 : = -- wovenenn 24 5 [F SRDTIRRIIIIIIIIIIITIINLL ESL, 2 8 : 3 [teresatitterrrreriritrsroootSi i Tmerrr irerstnanaenra E58 rovprpemmeass OH foIoimnnnnLInIIIINITIIRNNIIOILESS & 2 A : CompanSees, Sos361 --~ : - 232222222028222200000200000020a00s 33EI3RETEEREREE EER EREENEEEE RR NEREEE ` 2g |g% :i SUTIN IISA ANY | 8 i [ef pssstsnennany = 3 JE DEIRENRRRIERIRRERERRRRREEaansasenay serpentine over LsIoZRvINrIIeIImIEmIReIIsIRsIImERmIEnRInEeTEsReS Reayneyy SIINIIIIIIIRNIINIIIRETIIETIREEIRRIIENY eopprmm ry------ 2d B B2e6 [8 HI B: |3 : SH 5,8 sr oF sennnIIIIIIIIIIATIEIRLIERRIYII 5,1 SPELSISRNIEISIENSINIEIIIEISTEIEANRNIDELRRRISRIEIIREREENRSLENEEREENNLEYEYS hSTiE gv : CompanySanlzed. Does etcont78a0AiGBnI snail ffs SRERREY 1 ref ae peppery = 3 LE EB 275 flsg = le pers we 2 cSeare ne | : ~~ sowwere g5eBf: ffF g' 8 |I . 8 senor od 5,8 meee of | : 2,8 wry 5 z Compan Sant. oescon3a0n01 - SEESIICIIRGIITILcIRCICLIRRMARE 1 [JES EA ini 1Eke me wovpeneeney Lo2f12 EfEFE we wn #48 i> povrmmenevonns OH : ~~ 4 we : i ror featur 8 i EE | 5 smerny 8oF 6g 5 vopemponeoens OHg ; CompanySri. ss consaonn _ WUE f I (8% women a + 88 J i llEeef EEE sunny NT 2 penrnennne over HgTE , [iJE fiisz ` rovren 8 2|B wane 3 FJ 2 ~ RF ovr 2 sme =2 ~ g 8,8 sony ed g CampaSatzad. DossrotconanTSCAOo : ' ~ seassEsssnnaisasssmssssssensssasa2z SERERREREEESISRERIECEIREY ; bf [sk ; nEEEENEEEESSEELSLSLSIEISLSIaSeSy 8 3LE0R gg: f; leed FER 353 bormohbnmannloe = a - 5,8 smeeenenmamirey 2 sosvumnusmsnuoy SPE == o 2 |i H amnmnmeimmezzzy "+fEgN:[|8 rE RgL.8 = snnmmmienre B@fE creprsvmeene SH : minsrenniiize: ef8 minnie s2 d minsmoanenz 5,8 ef 2 : Company Santzed. Does not conan 750A Cot ~ ~ g + ~ 3582222322285 nanassnsansazanngas | 2 ES mmm . $0 z 8 gE. 8 convreseemeeene p3,C%8 4,8 cinpmmmmmnt @f comsunspsspsuss 2.2 SPE tof lig RC oF [F E[EESTE o i : z proessdittetiodE LIE i sma "55423 Ef 2 moomoo 5 ef I. g EM of mosses ef 8 moennmnnen ef purl Ef 5 z CompanySaiizsa. Dossnot contTsacAiGont | . SAIIR LIR Se ait nIIEIIIIIIIIIRIIIRERRRRSRLIRNILRRLL i le su F5a1t5 d1l552h peppespenreeery 240 8 [BR mr "proeessiy ' Fo mmmtpsnonanier 5@ 24 == Hs [8 pe LRnTIDIIIIERET #0 % : su propevensnennnn 53 s F O [fEF repre me pppoe sd1 s- oe sppemponssnenns 2,h8 g = Company Saiz. Donotscontsain 750A Gol - oo # ' -- ensse+ vf Jes SUSRRER s 7 Io % same {LE fg sopsnen 375 lin 5 [FE eawmala :< TAL2 : wrens nr ff pan.&f2 xiE weeee poumpy fF f 51 F EC 2 womens woown woe Of ms 7E4f :2 CompanySit. bosmeteorosm sR eg fi cPouppeevnppeoreens t5 L20)4 :i2lB |i3g - EEE mwr mommy f=efz` vf :[[EmRE wor : prone B-oEf :| ips 5 : . cossoneeonecns B 2 BIf on cveroreerers g4e1 f|F J' posnposneony PH8 1{ wrermpnn 2 --~ H CompanySanta. Goes otcontain 5A Go - : -- ? - EgsaaagnEEiestEir2 fB f2leEnE sz 15e5d) Cfefl LE: 2f2E8E cogzp sf [ER ) I1| :g ee maps scorsweens vere ] 8 z i fffERB ge O;oEFE fH gf Ea : CompanySanitied. Doss mot contTSaCAiCnEH FSFE IIMPRITEESR RINRR STRESS & J HE sPeeT rsT ivi} Pcl pit RTRREEILII net; [EF fs : wevppmenpnners OH2 :5 vopppppppprrey 2S,081 =E pomspnpnemrneee [oHa1 | _ e pompm rpopmosnnaers 3g%g iF E|g : sovssevenineey L3E sovewmoon 53,H8 5 ~ = CompanySanitized. Doesnot contain TSCA CBI ~~ --_ 2 ' $S E 55555E 5223t5g e03n22i0E 5n2e 5i5R5i R0R05R23i R25E80E8E 8R88E3 [ feettiE rrtit-- octl wLTnEuLpRpIpInEwInIeNnCsLeLeSe rrp mLEeRNnEoRs 8 = 1LEiEE HES HH Lf g' Elie EE2E2 [E2E 2 FH. i 4: g : lz 2 pinnae = fog |B eLIvTnReRmneieneneo 15 poetasd eas it 5E of ta] puns 8 v ~ : CompanySanitized. DossnotcontTSaCAiCnBI 1 EAINSEARUSHERERREEALE os i: ou e eresH 1 | LEE : , z FREESE RSSaENSULERRNRIRRERITRRSBLIRAS s 2 8 ils oo. : gE Loa i . Pow : ur rvsorrmenens fr2e0t FiEfEy nhinbinshsanobable Cg ::<< smn 2d : ge | wrppmomymaz of H oi 2 womens H E2 E x H2 ~~ = CompanySaiz. Gon conanTSoACa TEs mv: [ef coven 5= 82,2 EElEig SREEIL Tgfegseto iyr g[fEE2 pgp wd 3 [Eg . z sen aff |B 2,8 2: spun td 5 comeres 3.%2 BBE cee #8 ~8 5g suposed &i 2 Company Saiized. Dootscontsain TSE GBI supp B g3zzz22222E 2s3ssasaaE nzanzaazanR gsssazazay SESICSNNICIENISRNIStIsEIenIteneIeest # LEoH i0 orsneosensuoonnanyeneneerennneeee:. BECTfFE[BEE - SEITIEeRrIrrTiII- TE Sp2 7;z , s2ozoessososssessrooorasessestasezzseseaseeCoS Bcf fEF rT ----22,I ' CITEITIIIII rrr irerrry 2h rorvrrrover LEIEESILEITIITILISIssEbCSIITIanIIIISISE LE SSEESIEEIISIIIIISIeSEECIIaLISIIIIIISE 5 Frittatat 5,8 rossperrrrssyrmeraresrrssrarrerrrenarer OH Company Sanz. Donotecontsain TSCA Ct ~~ ~y ; --~ g283e228r7 fffies8 tg J leg ReRpeeeSoies 3&8pa3 z5ColFe2zg sees gEedBi [52 iEE : sesss 5 ME H$ : i sooo gesgee geese senor 9 iiE E ny FE ff 5 of 8,28 vf feelin1 gon 2oErYgd corer OH8 6 sepper = Hg : Company Sarzed, Doesnt contain T8GA Gol sessssermrensasnorosnsasessosanaess soeh, lff s[EF ha =z oosoossrrnosossrorosoossnsssssssoey nif [EE CTIIIIDIIIIIIIIIELIIIIIIIIIseeIeLs Boy f 8 F . - ee rore r enon over sons ~ 0 fg 2: Company Sanitized. Does not contain TSCA CBI ~ ' ~ 55355550000000500000003500505550080 EEZEGITRATUARNEICASERANERRATEARASES cSeEoSnCeIsEnErIrEeTnEreInEcEeInEsEeCnIsOeCnzNeEnRnIoEnNcIeEaNcEe fsooofogeosIoorriisIognionosgoioiszsissoinosisoiszsiszsesssincs:ss : gsoesesrzesissiosceseostonoenestir rtddditttdnitidtitdtitittddititc 1 | 4S0 pell "EnEo ge te 2,3 SEE al] 2 : 2 i4 | EiEF lEloEe Li [2EESFE i 2 3 spo0oserrosrassssossnsunsnsssane TEN wid fIooooornoInooooooonTIoRIooTonIne nig me gf SILCISIIECIRCLOOCREITEIIRCIILILCIIE ve 5 EILIIIIIIIITILCIIIEIIIIIISILEIIIIoE E 8,8 LoILSSIIISIIIIIISIoSSISIISIIIIISiSE d Eg. 88 TOILSSIIISIIIIIISIOSSISIISIIIIISISE 28 rorrosrrrorrrrrrorssarerorrrrrares LH2 ; : Company Sanilzed. Doss not contain TSCAG81 ~ 333gsasannsssaasagazansasssasasasansass 7 2 gx sezszssssnssseznennenmnencennzenzenie feof ffx oC [8 ssememnmsnnneeneesnennenzezeazzes L 5408 453 [EB sesssonrszissosssssissrsssssoronurroree sissssssssisecsssssssissssgssssssssiy soosssssesnosnosesssosiozozoszsnozozase UM8 ?2 nef of 5E gp IF off fF ~~ i sBsEssEsItoHsSsersoocesiioosronoosoooooaeset oo2 fF H I..| senssrsecnImmsnnzosEIoIonooInionIan 5nf seessrecenisrirrrirosrosrerserrrerzery 5<M eotipnserionIiiInIegiogIonooIIioion: of2 esterscorimiiinnsneCiogionosTiionion: 8R,f8 2 ~~ = CompanySatins. Doroscomtsain TSCA GB . ~~ ~ senpes 0 jes feof Plie ciornsesgx oo5 fl E5 E[2E8 Tees fF cozee FTE EEE o 5 Corser OH { cess ccoorzgseeee core cies pipe mpg 14 5 54151iJIfFF 8 8 0 |fFg nodig f 8 md 81 re 5,8 1 "osooi w 5 : orrssosooTnnIInIITIE ERTS LITER LLL i * : Hi ft essssnppmegiinisnetiicoioiisnnsnoiz se [F2E 5.8 |F ~ : Company Secs. Dons containTSoACa ~ H530i835g2 f 2 ogsl8z comm LilfC iEEEs i 2 seen rs&p8 d 8 Az E1|= s] 8 2S eweme 2Hg eee 1 SELNIL Ff ge oP E1BE sfrorenrsr of 8! i : were Ig reer 58 monn of moro5,8 crore 51 od E CompanySantis. DocscontinTsoAG1 reds iiintniitninssittieiinsniei i iI 2% s Te sa & 0g |5: EfB t CLLR ER EERIE = i error OH < SOLCLPLTLLELECRECROOOTEEIITININIISL S82 i = ~ COLCLBLICRLEETERCREDIEETIEIELIEIE 2 2 Te verre 4 EP 5 COCRUOPTLORCORLOORORLILEREILELLILI. pm ---- eel ~ S83E532E22C22S22N22N22I22E2E2E2E2RE2E2ER2R2R2E2RR2E2E2E2ER2R2ER22 |2 =2 Lfg E|E8% < le remesmrommoressnennannnneny. froedfffEE . I - IE- 2,8 SF S H se A | senpemmomoemmmeCrmnnriorer 6<d8g f|F 61:HH8 ~. commen sd bf Chott toaea 5i BA TOTTI EL EE 8 8,8 ceoeroromsrrezronsooooooonoeroin vd I aOE TECLIIIIITIIT. 5P,8 CompanSans, oss conanA01 ~. POSSTIpERErroInTITTIIIIoIonnnIIIIIIIIT RE aEEE PoooCrr oor onnnEIrooneToonlinrIionis ue 5 EH R1F5T5 2= errs COLLCRIDTORCOLCICIILTENISIELEIIRIEIIED Hoebbbihbbshbebiiibbibbbabhohbbhbbbl oki Fe > Crm 5,8 REECIILDEDIRIRILICCCCELSDRLRLLTOTIIIIIL vd H CompanySaiz. Bons conanTSoACo -- To ". ages wi 2 aERtE fg, ilie crzzrz ge Sf CT [ef 1 28 55550 Ceprrre 28 Ep Ea :2 2,0 prAoseroe G8 i5: aid rcenrprre 2 iEkE 5o,d2 ;BORE eee g ren 5,8 prrnnr NOR 5y CompanySaiz. Dossno contain TSCA Gel 160 v0.1 em os sony oc fans ~ og 3 2 sr TEIIUIRIIIIIIIIIIIIIIIINIIINIING 2 3 IIIIIIIITIIIIIIIIININNICNINNNNNINGNNNE 1 fr IIIIIIIIIIIINIIINANNCONIONIINONOONINNNE He pa IIIIIIIIHHISIIIIINNIIIIANIIIANINIL 3 fr TIIIIITHIISNIIINIIININIIANIIINNLG 2 ~ ga ; : amaennnnantenatastnn nase ntasant tate 2 i ; 19] H 1 pe TITER i fp SITIES i 8% Eff pi 42 pe IIITIIIIIIIIII:TIIIEIIA BE: pe CITIIIIIIIIIIIIIIIIIIIIIIIINIINGIN 2 IP 2 onianenniesesenesssnnnnanannne ~ $493 i : ZERSgATIRRRRIRRAEsanSsESSssRRzgEsLganR 160 051 veoussee `pesAunduos ~ 2 5.8 31333 Ht 5 5 IIE FE ga III iz ga mI Hi , F TE Pe. i iz oo 3 I fd 5 ope unm 3 draws 5 2 Es rida : LE 3 oa 3mmne ig] ifzy men gr 33003 .$ i : N 223 : > FPef) AInanadne i iFe IN fl. 2Y5i%: CQh E ~ 5583:: ii am 180 VOSL uieuoo jou $90 "pezniues Aueduwog wl 3 3 sn IIIMSITIITIIIISIIIRIIIRS fx TIIIIIIIIIIIIIIIIANIIIIINIINISNNNNY Hi H sa IEIIIIIIIIIIIIIIANIIIIIIIINISNINEN Hi pa IITIIIIIIIIMIIIIIINIIIIIIIIINNNGG 1 se IIIIIIIRIIIATIIITIITINIG ~~ | 23RopEr FOEELLDININENIHINIINT aH: 3 58 i i 3 8 IIIIIIIIIINIIIIIIIIIIANIIIANNGD i He 3 82 g Bil poh pe GDIIIIIIININIIIIIIIIEINIIIIIIIGNONE 180VoR sae SessKovtun ~ oe : gp TSIEN &'z N gr IITIIIIIIIIIINNSIIIIIIIIIIAANINNN 5 fa TIIIIIIIIOIIRIINIIIIIIIIANIANIININ 5 gr IIIIIIIIIIIINISIIIIIIIIINIANINNAN i fr TITIES Hi sr INTIIITIIIIIIIINIINIIIINNS ~~ f 8ifpe INTIINTIIIIINNISITIRIRIIIIIANIININD 4 qf ok 3 ITI ART g = &F 5 fo TINIE Pil pope CIIIIIIIIOOOINIIRIINIAIMIAINIIANMNAIININNOINN 4 fo Ey, H2ERCcLEFoon Ml Fh conEspENgTen ig : i sgagipraiaduisiadacnusitieatusagae 60 v1 ence ous `emsfear ~~ og : 3 IRIIIIIRIERRIIIEIIIIITIIRNITINE EF efary TIIIIITIIIITIITIOIIIIIEIIIIIIANIN fr CONNIIIIIIIIIIIIIIILIIIIIIIIIIIIN 1 _ jg EEE ] {f5 p T IEI TAN : If. mms 8 Fi fr CoINIIIIIIIIIIIIIIIIIIINIIIIIIIIIID : 1 pe3 IIIIIIIIIIIIIIIIIIIIIIIIIINIIIINIEIN i & 3 B5:38 fR e | Cg IIITIIINIIIIIIIIIIIIIIIIIINIRMITGEHID cel $885 83):MY, lic:8 ommenmenmamenIaIasIIIAnIdnIIIILA EE i 1 gEagsgsugsiacuagigesasatutay 160 vOs1 tues ou sen `pres Ase ~3 3 ga mE &s = EREERA] i 3g we i Add ea III HC 82 s 5 Jamal al IE 8% RA. gl OF EY i oz &d oZ| f8 oes mmm 13 iPy & [OEEEE g &% g 5 ne . g La] * HERR iy: fis 229H:i Ei]: gal 8 FF asgs 4 $. 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Hi o go iiER a ge 3| I 5 AEy mI mmm z2 PIER "mmemn g 5% S p= an 82 Hi : EgeE:ppssid don i BL IL #8 2 23 ii sagas % -- ` . 185 081weeas0 pee Areas TMg sa SUTIIISTIIILIIIIIANIIIIIANIIIIIIIIIINNI i } i B es SIIIIIIITIIIIIIIIIISIIIIIAIIIII i 3p TINTING &F ~ 1h J gz EMIIIIIIIIIIINIIINEIN g sa SNIIIIISIIIIIIIIIIIIIIITIANIIIIIIII 3| PEg 54i 05FaL0L s ARRARARe IRIERIANm EAAEEA en 7 i 52 & gHEpI fEoHl ppc s fg 872 8, {| 28: Lic dasa TIT S EITIIIIIIEIZEII NIIEZnD mneT ouTeanneTT ee onrmnmn =8] 2 & 38388EELEILLILLEIT8IL88E! PE -- ~ | 3 PO i go Sm i po mm % ps mm 5% Hi ~ gH weeny LIRR di E1 , wm 3: BE sree &7 g 2 5: i. mum 2: g 5 222) 80 Wee o2 ivoin 8513 =zg| & 333353 388328 H ] 160 v0 useosusens pres Artes a ES AAG AR AAA AAAAAA A A A A pr ITIIIIIIIISIIIIIIIIIIIIAIIIIIINNN 1] gs SITIIIIIIIIIIIIIIIIITIIEIIINNG Hi] fs IIIIIIIIIATIIIININNIIIIIINIINIIN 3 M ITI RI Ps FR : o| 3 ope TEImmTTIIEIICIIIIIIIONN 3 : po TIIIICTIITIIIIIIIIIIIIINNIN 5i } o oo g p i IITIIIIIIIIIIIIIIIIIIIATIIIIIIN : : 25 Hi $310 FICE noEEuRsERaRRenaTeRenEeEIsEEIaEnnEtEneEeEsRnETEaaEnn] . eee 22 3 LE ABA PID ~~ | z 3.2 STATI TIRE 1 fe SIIHIIIIIIIIITIINIIIINIIIII 53 po SITTING Hi fa STITT 1 ipa STIIIIIIISIIIIININIING ~ 8 : gl : HE nAensInIeIgeIeIeRTAaNTaANNTAaRneAnAENaIeNaENTAaAeAnAAATAGaAAAtAS 7 3 :1 i pa 5i Hp CETIIIIIIIOITIIIIIIIIIIIINIIIN TITTIIIIIISIIIIIIIIIIIIII Gg 4 SH, kLre, sommmTIEIIIIIINIIITIIN 31M LF seas 2% Ric } 189 VOLutes ou00g pezmues Ausiuco rr | 5 po He TIOOIHIIIIIIIIIITININ] ki AR AIaIR RnR AAAARAARIAAAAS AAA ~ | L|i epo Col EF, snaasanmenaIOIIIANIIINIINIIINIINANIIIEI gf 2 | pa GmAmIaAuInNaNnIaInInIeInIyIaIeIaAaNnInOeNeIaITITIIeNInNnERaNnANtINN Le - - : 3 By . a3fpi ; 7ge2, 4 IHIIININITIIITIAIIIINIwIeInmImRaInIanENNaNnST 23 1M. og conroonIIIISANIIIIINNINIANDIIIINNEE 3t J 3 851 1 1 EEggacimesspecnaniactennniiieees ~| 3 5.0 birrins Ez gp mm HH gs 033 2 Hi] pa SII i ~ ii 2 g@ pIaInIe 5 5i i z gogo -- SIEEED i BE : ga SII i 1 3 ge SII rc gil pp, IEEE" i i gid 23 2 Pye Emma i: Ria PEL EE I, 23: 2 gegese 8 " ' ] , 160osewesss prinnue ~= 3 Bs iviniviArAn hy jp po TUITE 1 pr TUITE r~ i 1 : fF ope TOIIIRIEIINININEIS : 5; i i aqsrenennnaniainaeyyassaneinavessesany g i 3 ik hd dd hd 2 8Z 5 go TIIIIITITINIIEIIIIIIHINGG gn } iIL.HH sem ; an . 2 HPE.iepe SIIIIIIIIIIIINSTIIINIIIIIIIIIIINS HIM gi: 160vosL mos10 50 pemmues undue ~| 2 ge III 5 i i fe smn 3 ps IIE He ~ { I :igsn Z fi 9neIIY 42 1gs &4 sa SF LL 2235} 5 5gE1 3 1 AG Ze: Jee ~3: IRIN SII: mmm AA Fv Bas gsazaz i i ` [EO -------- ~ =| 18 ImIENNNaIA AAA AAA AA A po IITIIIITRIIIIIIIIIIIINIIII 3 i AIEIAiNNANAA AAA AAA AAA AAA i A IARAlAIn AANA AAA Add dA ~ i fay em : i ! 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L5LLi ae EE ER 3 i a g sessty ~ 49 i 8i & i ssazsz i gags 8; . iss pA ~~ =| i pe ISTE He] ps TTI 1 pe TIITIIISINNN Hi pe SmI x fHeN III ~ | 1H of :8 pr 2wEnInIeInMyInEsIaInIaInEeEnDn RE i2 OE ge mwnEnmeInEsIeIaZaIeEaZnEnZy fe TIMING i fF . : of gis z2: 3i 43 : 23 i &F pe hammIIIwZneInInIeNaEe Pos o Fonre n em iIa Ian 3& Co gprassnasgassessgsssceszaagogpEsi i 1 zagadeasagesasesess 180 VOSL umu00o29390 peznes Ausdued : jp SATIRE Hi 8 SIIATIIIIINANI HH ge SOIIIIIII 1 gs ITIAIIIIIIMANI He bE Ar ~ i al i pe :1 fr !7 5 ,0 iF RIIIATIITIIANI IAIIASIAIIIAANI reAnEmAeRaInRaMvIvReEnEnEnRe gr IIIIIIIIIINON . g H2e $25 go DITION ER ER EN BEAD F ~ 45: : n ' . 183 081 ute1s0 3900 `perms Ausdueo 3 5 5 SIIIIIINIIINN: Hi] eo SIINIIINIIINN 1 HE jo TEE ge SIIIIIINIIIIN 5% I wns hiked WI ig 85 3F Fr Adana Eil fF i EF AAndAAAAedddAa 3 & Asrirledd 3 gr SIIIIIIINIII 25 fd 48 mn gr SIIINIINIIIIN fcxxken . 82 : 23:pogpei TEEImIEIINIG man side Co 1! gr STIIIIIIIIIIIIIIINNNIIIINIAIIANNIAN 28 3 $y xn 83 i i I 5523seREgRatansattaasRtantataRtae 189 VOS1UIeU00Jou 530 "paznesAuedwog ~~ a 2 ga i [> He [ER] oz pe a Hi 8 ------- 2 g BE ~ 52 82 re i2Hl 8 &. F A i of ir g| Ea $5. 2 ---- : 3= &F Hgix CEI : . nae 22)582 f8a0y 8 ne FE E4% iEEd:TAR fis 5 canens 2384: FE: ~ 83:5 ia 28] 2 & i gga 33 : 180 OSL UIejuod jou 530 "pazniues Auedwog ~ of EE pe. ~ ] He | gop i 5 F df OF gi HH & pe S Fr FY] og TIMING TEED mmm IEIIIIIIEN . 0EIIIIIIIIIN amnMeneseTaTien 31333 5 21353 : fio 130 | +wav]we : eneee i: ps ommmmmm 130 8: hte: ~~ gs 0 Va aREnSmTIEEEIRIIAILLINARIAISRLATIRLIRAAL [ES ~a 3 ---- 53 bs i --~ i 5 | 12 p eWeEn 2 3 , 83 | I A i Ey 3 gs Sn i 2 Cops am S8 i : : 138 mE 5 fog Ed Ae If 2 fie 28 i CF ~ 33: % {asa 120vosLU0910 5500 puesusu 3 ~~ =| g 2 jp an iz ge EI iz , BF ReEmmn ~ LI i 5 iops III HI ananansanacanes i fs : 8 TIIIININIII 23 pr $g Hi] Fal; ge iz i g 3 TLITIIIIIIIIN : IENIIIIIIININIS i I s Fumi 2g 3 fis = asl 59] &3= . : : : 180 VOSLuI10uu500000 "perme ucuon --~ a 3 52 8 aga 82 ji em 8 rik RS] --~ i: 2 2 raesnenesenenn = i8 8EF oi&8 AAA 1sl 8E keg IA%IREERGGGAGEEE 5:5 EERRREERRM RNIN] i 3 2 Gan , Sf + FF : 2B3ip ge E nneeI aenE esgnN ens L5H 5 iERE 2 SPs Fn --~ aSE9:: 3 8258) i gHz : 252933235290 53R825455R05R085RRRASE | gSEgRaAgasRsaasncaaniaanNsaunaiannAinRaRiaaRnaiRiaiRnaaktRis PACH TARA ~~ | Z3 jy Tm jg Tm ~i i 1mIsIIaNNIII 3 : EF gfikpe mmm 5 fs SOTIIIIIIIIENA <Q b$i8: E1EE1mEsEsRIEasEaa:Eses : 333m ? 11333 $3333 ssn . d 28, h pe smmmmmmen r3EC1 T.:ofP cA osmo aE 3 88 sm Tama 3g4e)l 12 Fp sgn : em onEr TRATIONS REI ORnSY 189 VoL uu ou 000 "peznues Aces ~= 3 I] 55d ~~ g B8 E in & 3 gs 3 !x i fs mm i fin i in fg In $s &8 a l 23 ke 5 pn 23 E iP. a fo . . dE382 8 =8l & & fai $ sszane 888882 180 VOS1 ured10u S900 "pazIues Aueduoy H902-5D4a2y5G:avSaugbcehSrtoundiyc iTnorRiacistywithOne Generation Reproduction valuations -- EE DuPont 11418 --~ APPENDIX C INDIVIDUAL BODY WEIGHTS --~ E 180 VOL U1EIu0010u S000 "PoznIuES Aueduog 0H2-5D4a2y5:GavSaugbeelSotnuidcy TinosRiactistywithOneGeneration Reproduction Evaluations DuPont 11418 INDIVIDUAL BODY WEIGHTS EXPLANATORY NOTES Critical Dates Day 72 Last day data from the male and female rats designated for reproduction evaluations were reported with the subchronic toxicity animals. Body weights and clinical observations collected during the cohabitation and `post-mating periods are reported in the Reproductive Toxicology section; Dose volumes administered during the cohabitation and post-mating periods are documented in study records. Day 90 Last day oftest substance administration for male and female rats designated for one-month and three-month recovery periods. Day91 Last day of body weight and food consumption data collection for male and female rats designated for the subchronic toxicity evaluation. Last day of test substance administration for male rats designated for the subchronic toxicity evaluation. Day92 o Male rats designated for the subchronic toxicity evaluation were -- sacrificed. Last day of test substance administration for female rats designated for the subchronic toxicity evaluation. Day 93 Female rats designated for the subchronic toxicity evaluation were. sacrificed. Day 126 Last day of body weight and food consumption data collection for rats designated for the one-month recovery period. Last day of food consumption data collection for rats designated for the three-month recovery period. Day 127 Male and female rats designated for the one-month recovery were sacrificed Day 182 Male and female rats designated for blood fluorine level evaluation were sacrificed. . Abbreviations . `my/kg = mg/kg/day Note Absence of data indicates the animal was not alive a the time of data collection. ~~ =m [ER ---- a --~ J 2 L2G: FE 0 SEEIGESINNNENNssnTE h2y .3 dmeanrsiaaEnsnEenniessdesniesedssedse4 creissedssaisdossisgsassgdnsgeisndciiasgnedes i i.2 @928ennennontanan ean yn naenesasnss $3 3 i i& {HN 23 gop i al a 23 ; : 7 ggafipdsasziadiiacdadididaiiicisinensaz fF. gumannanesnraescasdeaiienannesvananegs 3ED J RSREARRRRe IANnRNRAgRrNBTEa SAdRNsIeANnRg CRnAReBg EEaRAsZnEAgNd n NEs NE fe } s IEnIIIIIIIIIIIIsIIIIIyIIani ay ARgSisnRggIngssIdsrangns dannynancy 3EEzsssasmrauzssscaseassassansanneanes 180 vs.UIH100030900 pzmes Aueduuog TM3 3 3f ia 32 i2.p5o fads: ~ 2. aomune joi g % 8.7 gagdsd 73 Eg3 g TTT o.oo B2 i. 3 H SE2 i Eo?3 gR3Ah3RsRgRd iF 2 . fo heen f3o. mun iz gRRA%E ~ 2494% =gl & * 4: a2Egaes= 2 838833 3 . 180 OSL uewwo Jou s80q "peznues Aueducy : a 2 . a%esgeqsvencussniseasyvecatvateecte 3 B27 #denensAusaIneaataeuIIeaitnatenas: 3 Lo 3o2m33m39m30n00u80n0an0 3n02n93nmREmTAaRTnERnREsS ga EEE 5825988 jLpo nmmemmuenmmSEnIuSSwEAnToaREaTEmTEsINnINm ~ 5 $4. senanszemessnsasanasnsanaaacasnaess .5 gBoLeUsIRiAsSsSgUcRaRnIsEsIfAiSfNfIsRsSsNiIsSsfgSrEgRuIdLsAdAuLdIsE 4 8: i 13 1 SlI. $ gggy 3 i --~ 24% ggl 2 if 3 .2.0 gAiUdGeEdAeEsEsRiIRRrNEEvssSnneEsZsseeevvzisesvsassRssamocnniannnazsEs or | _ sasencsurecsrasssacarancanvivestann fo; ARRARRERNNESRIERAZAERARERRNIZERIARER 04 2 entnannanesnesseasaassananenenasy fo; I RRGEERRRARNARIARRENRAIRNRARREIRANAY TEPRL EEEEERE EEE EER EERE E OH] E3ESSEOIREEEEI0ERIREERRLERRERRIREE 180 VIUSIEIN0J0DU $30Q "PazHiUES AuedwoDd ~~ 3 zAa J .i3 m sgpoizsm psetaonzmsecnessasasnsniigesEsssiainnaivnesssaaesnsniadnacge iF i& 31.7 anseanmenanesiyoasaanncaeenoyn gzsadessiisivangissusiaednaiees if ~ $5. woeusnizassnesnassssessnennoeneunas f i iif 88 IEi fs3u5mRamzmRdrnensEasseensaegusnsassReInRasnaannaiasAtaEnE gl, if ommended | - se3lg 4 x 0 2 gmanesiannianemunazaaissaanaeniy fey B ARASHARRRARIGIGRINAIINANANEAAAANEER =g| 4 FERE S EERFREE EEE EE LEEREEE OVS vorou Seog PeuD i pp me 3 fe FoREFm ATICTHELnNInNTnALIAIRNImALRINARNGIIILNIRAANTIGNS i . safndqgmdmznasgndaassaannzdacansoasgnaaassidedassastsaagncdmaagnegdiaennness Le nESHULRnonumNnnn gq if |i 0 3 1] . f3r% HIEIBNEEEINEaAmRzAaRAaNmAaNaAmRAaNiRzAeRAnRiAaRsAsNReAnNiIaRAsNnNaAcReR 180 vot. row sony pee Amd ~= g 8 2 if ; 33 Yt: zum FE 3 gps i& J PI EEE 8 i if IES zzsass i "if g if z 123 2% ~ a5l35 & fg oto3 oF g RARER Tos; sagas its Se ~7 3 : 23 FErReRyE 2a2p3t8s is a3 on 35888 He 3588 3i ~~ I 1 3i 3 ii2.5 spiedcsedsssgssnscdasesndedss fis GEtduenanan 23i ande5sd 4? Hd qd if EERE3, mimes : #4. 1 1H i 1. 3 i o $58R52A88Rn RRRTRAREZAa REININAANLn AEANRINNCRS gg: dsniianhnannnetntnnnt ST STRAY ~~ =| 3 1 Eo gnomes Ly! gets fa queen: 3i pda7 230833 3i ~ 11. omnes 3 Ii i i FERRE] on J : 3 fr mm Evans 13, cHE 2 --~ i 34s 1 9 p dite 7;. aaases . : ' svi ~~ 2 3 3. 3i = 3 esses ERE g38a3 i2 ~ 8 snansgsneeveane 3 4i < i He | FE ~3 Fez srssmspmsasennessnamnnasssanaanncs HOVER OST Pr any i z, iz ] is an 2 3 35 8 is 3 3fRreaeR 3 FE3ER ~~ J fBii. ssmge ssse usgnat $3 | i 5 3 3 3azAasaRgEaEEE I1 :bey mGRmSRmESmARRaIGnEEmNC 2 reurenavtaananieiiaiesesemmenanyy - g2. iF 3 $552 is3 b dInAnNaSceNRIssRRiSiAiRiRIaIdAiLIaCiAdRiIIiRvRndIeRsaNmiIosAnNsaAvaaLdeE PEI BE32BBE52E250088082288882 588888388 180 voSLUetio3 ou 000 perme Ausdued ~~ = ; i 291% ggdaa nae 8388 i: wa mm , games damn 3i 3g ji ~ 13 acnsnenneecanes 3& di nmin 4 if 4 LS. EE ame 4 sane ne 33 3 323 R 3 BRGuNI EARRRIIRGRLN ICERERIRIIRT RRIRASIERY 28 ity EE g93auissagasyuanyanntannaaastananaey 180 OSL e090 a0 pozues Aca ~~ og g2 . fo wmmeas if ia $5 seamen ESE ir :23 dGeeaan ~ LI i& i 1g 3 2a5 EBEEREE NE 522 2 ~ F2EEE33 ;z ie Tae H5iE 8e3gsedaass : 180vos.umes 3000 puns undue rm 2 q i. 57 2% BRBLR ii sshiesz He fe i: wos Hh - ~~ f1is mas : : Hy REES ? ji 2 i z 2 1fo asa S| zgl & IREISEETITRSIARIPEGAE RS 3333285 8583 358 E5R3 RT2 ERA2 ERA2 RTI8 ER vosmes es ~~ gl 51 is kiife ii o7 iz jie ~ HHEER 4: | >23 3 LEE] | i IP Ll =g| & iicaam IT: # 383888 159eescn `ern tay ~ =| ie 3 8388 1] gdgas j ig gl Fie] LE 1 3388 jor Bg, 1 gm iss bir #9|\8 Ee srigRRanRtEneRAIRETERAaEEEEE 180voseoo uss00 pres und i ~ 3 3 wo wo i 8i i& HH i& 3 ~8 ii, 7 ii g 10ii 38 &8 228% 53 BuEn you i, 1 $f if.q7 : S2 HE:tse 45 225%! $233 8 5252 3a8= i : Ys Toros 3i 3i | in ~~ 3i mn . 4 ii: i i if sui f2283 . 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