Document gm43MY0kMe3gJJmYNzJkgKoV
SEVERN TRENT
STL
STL Chicago 2417 Bond Slreel University Park, IL 50465
Tel: 70S 534 5200 Fax: 708 534 5211 www.stl-inc.com
SEVERN TRENT LABORATORIES ANALYTICAL REPORT
JOB NUMBER; 232883
Prepared For:
Weston Solutions/ Inc:
1400 W e s t o n Way
. Building 5-2
..
'Weist;viChestieri;iiiPA193-8 0'-14 99
.
P r ojectCprif idential Dec.atur t":iFC.:..Investigation
..Attention.-:".. Jai Kesari ...
Date: 12/30/2004
Title: Project Manager E-Mail : r w r i g h t @ s t l -i n c ,com
This R e.po r t Cant a in s
Leaden in Environmental Testing
Date STL Chicago 2417 B o n d StreetUniversity Park, IL 60466
PHONE; (708) 534-5200 F A X ..: (708) 534-5211
Pages
Severn Trent Laboratories, Inc,
WET CHEMISTRY DATA PACKAGE CONFIDENTIAL DEJOCAB#TU23R28-8F3C INVESTIGATION
Data Summary.................................................................1 Chain of Custody.......................................................... 18 Case Narrative..............................................................22 Raw Data.......................................................................24
STL Chicago is part of Severn Treni Laboratories, Ine,
S J M P L t ' I M r O R M A T : - ! D'M" Date; 12/30/2004
Job Number. 232833
Customer... Weston Solutions, Inc. Attn...... Jai Kcsari
Project Number........ : 20004891
Customer Project ID___ : CONFIDENTIAL DECATUR Project Description.,+.: Con-fidehtial Decatur - FC Investigation
Laboratory sample ip
232883-1 232883-2 232883-3 232883-4 232883-5 232883-6 232883-7 232883-8 232883-9 232883-10
customer Sample ID. . DF09-SBC-131R-0-0000 DF09-SB-131R-Q-0050 DF09-SEC-131R-0-0050 DF09-SEC-131R-0-010 DF09-SEC-131R-0-0160 DF09-SBC-131R-0-0150 DF09-SBC-131R-0-0200 DF09-SEC-131R--25 DF06-SE-133B-0-0050 DF06-SB-133B-0-0160
Sample
Date
.Time . . . \Date-
T ime
Matrix
Sent?led
Sampled .v;;: Received ....Received
Soi l
12/09/2004
11:55
12/17/2004
10:00
Soi L
12/09/2004
12:05
12/17/2004
10:00
Soil
12/09/2004
12:15
12/17/2004
10:00
Soi 1
12/09/2004
12:30
12/17/2004
10:00
Soil
12/09/2004
12:40
12/17/2004
10:00
soi 1
12/09/2004
13;00
12/17/2004
10:00
Soi 1
12/09/2004
13:25
12/17/2004
10:00
Soil
12/09/2004
13:45
12/17/2004
10:00
soi 1
12/10/2004
09:15
12/17/2004
10:00
Soi l
12/10/2004
09:13
12/17/2004
10:00
Pago 1
1
STL Chicago is part of Severn Trent Laboratories, Enc.
Job Number: 232883
CUSTOMER: Weston Solutions, Inc.
Customer Sample ED: DF09-SEC-131R-0-0000 Date Sampled...... :12/09/2004 Time Sampled...... :11:55 Sample Matrix..... :Soil
TESTHETKQD Method
Lloyd Kahn
:PARAMETER/TE ST !'DESCRI P T EON
% Solids Determination % Sol ids, Solid % Moisture, Solid
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LABORATORI
TEST
RESULTS
PROJECT CONFIDENTIAL DECATUR / .
Laboratory Sample ID: 232883-1 Date Received....... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 ATTN: Jaf Kesari
:SAMPLE: RESULT O ELGS:
51.5 13.5
240 D
MDL
0.10 0.10
79
RL: 03 LUTI OH u n i t s ; BATCH DT . .DAT.E/TIME TECH1
0.10 0.10
137770 137770
12/21/04 1522 da j 12/21/04 1522 da j
3T0
mg/Kg 137664
12/21/04 1014 els
* In Description = Dry Wgt,
Page 2
STL Chicago is part of Severn Trent Laboratories, Ine.
Job Number: 23833
CUS1OntK: Weston Solutions, the.
Customer Sample ID: DF09-SB-131R-0-0050 Date Sampled...... :12/09/2004 Time Sampled...... :12:05 Sample Matrix..... :Soil
*r!-\ -T.EST'.M:E:T:HO:D:::
PARAMETER/TEST DESCRIPTION
Method
% Solids Determination % Sol ids, Solid % Moisture, Solid
Lloyd Kahn
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
co
LABORATORY
TEST
RESULTS
HRUJtC1: LUNrJDtNJIAL .utCAI UK.
Laboratory Sample ID: 232SB3-2 Date Received...... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 .A M R : Jai Ke s a n
i:! v-
!TT=-^r.
SAMPLE RESULT Q FLAGS
80.7 19.3
1300
L
; L
DILUTION
u n i t s ; . BATCH DT d a t e /t j m e TECH
0.10 0.10
0.10 0.10
1 1
%
137770
12/21/04 1525 daj
%
137770
12/21/04 1525 da|
SA
330 1
mg/Kg
13764
12/21/04 0957 els
[n Description = Dry Wgt.
Page 3
!
STL Chicago is part of Severn Trent Laboratories, [no.
Job Number: 232883
CVSTOMERs;Ueston Solutions , Inc.
Customer Sample ID: DF09-SBC-131R-D-0050 Date Sairpled...... :12/09/2004 Time Sairpled...... :12:15 Sample Matrix..... :S di l
TEST METHOD Method
Lloyd Kahn
PARAKETER/TEST DESCRIPTION
% Solids Determination % Solids, Sol id % Moisture, Solid
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECAT.LJR -
Laboratory Sample ID: 232883-3 Date Received........ :12/17/2004 Time Received........ :10:00
Date:12/30/2004 ATTN: Jai Kesari -
SAMPLE RESULT . $ FLAGS::
78.7 21.3
i
1100
0.10 0.10
67
RL DILUTION. . UNITS- BATCH DT DATE/TIME TECH
0.10 0.10
1 1
%
137770
12/21/04 1527 daj
137770
12/21/04 1527 daj
260 1
mg/Kg 137664
12/21/04 1030 cts
* In Description = Dry Wgt.
Page 4
_____________
STL Chicago is part af Severn Trent Laboratories, Inc.
* ]n Bescri pti on = Dry Ugt.
Page 5
STL Chicago s part oi Severn Treni Laboratories, Ine,
Job Number: 232583
CUSTOMER: Weston Solutions, Irte.
Customer Sanale ID: DF09-5BC-131R-0-0160 Date Sampled...... :12/09/2004 Tjne Sampled...... :12:40 Sample Hatrix..... :Soil
TEST METHOD-
PARAMETE R/TEST DESCRIPTION :
Method
% Solids Determination % Solids, Sol id Y> Moisture, Solid
Lloyd Kahn
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT : CONFIDENTIAL DECATUR
Laboratory Sample ID: 232383-5 Date Received....... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 ATTWi' Jai Kesari'
SAMPLE RESULt
79.7 20.3
500
FLAGS
MOt:
0-10 0.10
12
r di lut sow UNITS :: . BATCH D T : DATE/TIME TECH
0.10 0.10
;137770 i137770
12/21/04 1532 da j 12/21/04 1532 da j
45
mg/Kg -137664
12/21/04 1124 c ls
* In Description = Dry Ugt.
Page 6
STL Chicago is part of Severn Treni Laboratories, Ine.
Job Nunber: 232683
CUSTOMER: Weston Solutions, Dnc ;
Customer Sariple ID: DFO9-SBC-131R-Q-O150 Date Sampled...... :12/09/2004 Time Sampled...... :13:00 Sample Matrix..... :Soil
. TEST METHOD:
' PARAHETER/TEST DESCRIPTION
Method
% SoLids Determination % Solids, Solid % Moisture, Solid
Lloyd Kahn
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
F*
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECA TOR
Laboratory Sample ID: 232883-6 Date Received........ :12/17/2004 Time Received........ :10:00
SAMPLE- RESULT <3 F U G S ' ' ::m o l . '
79.4 20.6
0.10 0.10
740 60
' RL
0.10 0.10
1 1
230 1
Date:12/30/2004 ATTN: Jai Kesari
UNITS BATCH. DT DATE/TIME TECH
%
137770
12/21/04 1535 daj
%
137770
12/21/04 1535 daj
mg/Kg 137664
12/21/04 1139 c Is
* In Description = Dry Ugt.
Page 7
00
STL Chicago is part of Severn Trent Laboratories, Enc.
Job Number: 232803
CUSTOMR:. Weston :S o lu tio n s , Inc :
Customer Sample ID: DF09-SBC-I31R-0-0200 Date Sampled...... :12/09/2004 Time Sampled...... :13:25 Sample Matrix..... :Soil
TEST METHOC
Method
Lloyd Kahn
:PARANE TR/TST.D ESCRIPTION
% Solids Determination % Solids, Solid % Moisture, Solid
Total Organic Carbon (Soils? TOC Average Duplicates, Soil'd
LABORATORY
TEST
RESULTS
PROJECT:!CONF IDENTAL DECATUR
Laboratory Sample ID: 232883-7 Date Received....... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 : ::ATTN: Jai Kesari
SAMPLE RESULT-
FLAGS
74.1 25.9
810
MDjJ
0.10 0.10
58
RL DILUTIESJ UNITS BATCH B.T DATE/TIME TECH
0.10 0.10
1 1
%
137770
12/21/04 1537 daj
137770
12/21/04 1537 daj
230
mg/Kg 13764
12/21/04 1215 els
* In Description = Dry Wgt,
Page fl
ff)
STL Chicago is part of Severn Trent Laboratories, Inc,
Job Number: 232383
CUSTOMER: Heston Solutions, Inc;
Customer Sample ID Date Sampled__ ,,_ Time Sampled..... Sample Hatrix....
D F09-SEC-131R-0-025 0 12/09/2004 13:45 Soi l
TEST METNCC Method
Lloyd Kahn
:PARAMETER/TE ST ;;0ESCRI PT IOH
% Solids Determination % Solids, Solid % Moisture, Solid
Total Organic Carbon [Soils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample 10: 232883-6 Date Received...... : 12/17/2004 Time Received....... : 10:00
Date:12/30/20D4 ATTN: Jai. Kesari
.SAMPLE RESULT
78.6 21.4
370
FLAGS
MDl
0,10 0.10
61
RL DILUTION: UNITS EATH: DT DATE/TIKE TECH
0.10 0.10
137770 137770
12/21/04 1540 daj 12/21/04 1540 da j
240
mg/Kg 137664
12/21/04 1235 els
* In Description - Dry Ugt,
Page 9
STL Chicago is part of Severn Trent Laboratoriesr Inc.
Job Number: 232883
CUSTOMER: Ueston.Solutions, Inc.
Customer Sample ID: DF06-SE-133B-0-005D Date Sampled..... : 12/10/2004 Time Sampled..... : 09:15 Sample Matrix.... : Sai l
TEST METHOD Method
Lloyd Kahn
PABAMETER/TEST DESCRIPTION
% Solids Determination Si Sol ids, So lid % Moisture, Sol id
Total Organic Carbon (Sails) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample fD: 232883-9 Date Received...... : 12/17/2004 Time Received...... : 10:00
Date:12/30/2004 : ATTN: Jai Kesari
;:SAMPLE- .RESULT ' Q FLAGS
81.7 18.3
850
' HDl -
0.10 0.10
66
'.SL -D-ILU7ION UNITS ..BATCH' DT DATE/TIME 'TECH-
0.10 0.10
1 1
%
137770
12/21/04 1542 da j
%
137770
12/21/04 1542 daj
260 1
mg/Kg 137664
12/21/04 1047 els
i
1i________________
* In Description = Dry Ugt.
Page 10
STL Chicago s part oi Severn Treni Laboratories, Ine,
Job Number: 232583
CUSTOMER: Weston Solutions, Irte.
Customer Sanale ID: DF09-5BC-131R-0-0160 Date Sampled...... :12/09/2004 Tjne Sampled...... :12:40 Sample Hatrix..... :Soil
TEST METHOD-
PARAMETE R/TEST DESCRIPTION :
Method
% Solids Determination % Solids, Sol id Y> Moisture, Solid
Lloyd Kahn
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT : CONFIDENTIAL DECATUR
Laboratory Sample ID: 232383-5 Date Received....... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 ATTWi' Jai Kesari'
SAMPLE RESULt
79.7 20.3
500
FLAGS
MOt:
0-10 0.10
12
r di lut sow UNITS :: . BATCH D T : DATE/TIME TECH
0.10 0.10
;137770 i137770
12/21/04 1532 da j 12/21/04 1532 da j
45
mg/Kg -137664
12/21/04 1124 c ls
* In Description = Dry Ugt.
Page 6
STL Chicago is part of Severn Treni Laboratories, Ine.
Job Nunber: 232683
CUSTOMER: Weston Solutions, Dnc ;
Customer Sariple ID: DFO9-SBC-131R-Q-O150 Date Sampled...... :12/09/2004 Time Sampled...... :13:00 Sample Matrix..... :Soil
. TEST METHOD:
' PARAHETER/TEST DESCRIPTION
Method
% SoLids Determination % Solids, Solid % Moisture, Solid
Lloyd Kahn
Total Organic Carbon (Soils) TOC Average Duplicates, Solid
F*
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECA TOR
Laboratory Sample ID: 232883-6 Date Received........ :12/17/2004 Time Received........ :10:00
SAMPLE- RESULT <3 F U G S ' ' ::m o l . '
79.4 20.6
0.10 0.10
740 60
' RL
0.10 0.10
1 1
230 1
Date:12/30/2004 ATTN: Jai Kesari
UNITS BATCH. DT DATE/TIME TECH
%
137770
12/21/04 1535 daj
%
137770
12/21/04 1535 daj
mg/Kg 137664
12/21/04 1139 c Is
* In Description = Dry Ugt.
Page 7
00
STL Chicago is part of Severn Trent Laboratories, Enc.
Job Number: 232803
CUSTOMR:. Weston :S o lu tio n s , Inc :
Customer Sample ID: DF09-SBC-I31R-0-0200 Date Sampled...... :12/09/2004 Time Sampled...... :13:25 Sample Matrix..... :Soil
TEST METHOC
Method
Lloyd Kahn
:PARANE TR/TST.D ESCRIPTION
% Solids Determination % Solids, Solid % Moisture, Solid
Total Organic Carbon (Soils? TOC Average Duplicates, Soil'd
LABORATORY
TEST
RESULTS
PROJECT:!CONF IDENTAL DECATUR
Laboratory Sample ID: 232883-7 Date Received....... : 12/17/2004 Time Received....... : 10:00
Date:12/30/2004 : ::ATTN: Jai Kesari
SAMPLE RESULT-
FLAGS
74.1 25.9
810
MDjJ
0.10 0.10
58
RL DILUTIESJ UNITS BATCH B.T DATE/TIME TECH
0.10 0.10
1 1
%
137770
12/21/04 1537 daj
137770
12/21/04 1537 daj
230
mg/Kg 13764
12/21/04 1215 els
* In Description = Dry Wgt,
Page fl
STL Chicago is part of Severn Trent Laboratoriesr Inc.
Job Number: 232883
CUSTOMER: Ueston.Solutions, Inc.
Customer Sample ID: DF06-SE-133B-0-005D Date Sampled..... : 12/10/2004 Time Sampled..... : 09:15 Sample Matrix.... : Sai l
TEST METHOD Method
Lloyd Kahn
PABAMETER/TEST DESCRIPTION
% Solids Determination Si Sol ids, So lid % Moisture, Sol id
Total Organic Carbon (Sails) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample fD: 232883-9 Date Received...... : 12/17/2004 Time Received...... : 10:00
Date:12/30/2004 : ATTN: Jai Kesari
;:SAMPLE- .RESULT ' Q FLAGS
81.7 18.3
850
' HDl -
0.10 0.10
66
'.SL -D-ILU7ION UNITS ..BATCH' DT DATE/TIME 'TECH-
0.10 0.10
1 1
%
137770
12/21/04 1542 da j
%
137770
12/21/04 1542 daj
260 1
mg/Kg 137664
12/21/04 1047 els
i
1i________________
* In Description = Dry Ugt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 232883
CUSTOMER : -Weston:Solutions, fnc
Customer Sample ID: DF06-SB-133B-0-016Q Date Sampled.......:12/10/2004 Time Sampled.......:09:13 Sample Matrix..... :Soil
TEST ME7HCC Method
Lloyd Kahn
;PARAWETEW TEST ;DESCRIPTI0H
% Solids Determination K Solids, Solid % Moisture, Solid
Total Organic Carbon CSoils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL CATR
Laboratory Sample ]D: 2328S3-10 Date Received....... : 12/1772004 Time Received....... : 10:00
Date:12/30/2004 ATTN: Jai Kesari
SAMPLE RESULT
83.9 16.1
460
FLAGS
:MDb
0.10 0.10
53
RL DILUTION UNITS BATCH ; 0T DATE/7TME TECH
0.10 0.10
137770 137770
12/21/04 1545 da j 12/21/04 1545 da j
210
mg/Kg 137664
12/21/04 1246 els
* In Description = Dry Wgt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 232883
CUSTOMER : -Weston:Solutions, fnc
Customer Sample ID: DF06-SB-133B-0-016Q Date Sampled.......:12/10/2004 Time Sampled.......:09:13 Sample Matrix..... :Soil
TEST ME7HCC Method
Lloyd Kahn
;PARAWETEW TEST ;DESCRIPTI0H
% Solids Determination K Solids, Solid % Moisture, Solid
Total Organic Carbon CSoils) TOC Average Duplicates, Solid
LABORATORY
TEST
RESULTS
PROJECT: CONFIDENTIAL CATR
Laboratory Sample ]D: 2328S3-10 Date Received....... : 12/1772004 Time Received....... : 10:00
Date:12/30/2004 ATTN: Jai Kesari
SAMPLE RESULT
83.9 16.1
460
FLAGS
:MDb
0.10 0.10
53
RL DILUTION UNITS BATCH ; 0T DATE/7TME TECH
0.10 0.10
210
137770 137770
mg/Kg 137664
12/21/04 1545 da j 12/21/04 1545 da j
12/21/04 1246 els
* In Description = Dry Wgt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 232883
LABORATORY
CHRONICLE
Pate; 12/30/2004
CUSTOMER: Weston Solutions, Inc.
V PROJECT: CONFIDENTIAL DECATUR-
ATTN: Jai Kesari
Lab ID: 232BB3-1 METHOD
Method EDD LLoyd Kahn
Client ID: DF09-SBC-131R-0-0000 DESCRIPTION % Solids Determination Electronic Data Deliverable Total Organic Carbon (Soils)
Lab ID: 232BB3-2 METHOD
Method Lloyd Kahn
Client ID: DF-SE-131R-0-005 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-3 METHOD
Method LLoyd Kahn
Client ID: DF09-SBC-131R-0-0050 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-4 METHOD
Method LLoyd Kahn
Client ID: DF9-SBC-131R-0-0100 DESCRIPTION % Solids Determination Total Organic Carbon (Sails)
Lab ID: 232883-5 METHOD
Method Lloyd Kahn
Client ID: DF9-SBC-131R-Q-0160 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-6 METHOD
Method Lloyd Kahn
Client ID: DF09-SBC-131R-0-150 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-7 METHOD
Method LLoyd Kahn
Client ID: DF09-SBC-131R -0-0200 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-8 METHOD
Method LLoyd Kahn
Client ID: DF09-SC-131R-0-0250 DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-9 METHOD
Method Lloyd Kahn
CLient ID: DFO-SB-133B--0O5O DESCRIPTION % Solids Determination Total Organic Carbon (Soils)
Lab ID: 232883-10 Client ID: DF6-SB-133B-0-0160
METHOD
DESCRIPTION
Method
% Solids Determination
LLoyd Kahn
Total Organic Carboh (SoiLs)
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1522
1
1 137664 137664
12/21/2004 1014
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PRP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1525
1 137664 137664
12/21/2004 0957
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1527
1 137664 137664
12/21/2004 1030
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1530
1 137664 137664
12/21/2004 1103
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #()
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1532
1 137664 137664
12/21/2004 1124
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1535
1 137664 137664
12/21/2004 1139
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1537
1 137664 137664
12/21/2004 1215
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/09/2004
RUN# BATCH# PREP BT #(S>
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1540
1 137664 137664
12/21/2004 1235
DILUTION
Date Recvd: 12/17/2004 Sample Date: 12/10/2004
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1542
1 137664 137664
12/21/2004 1047
DILUTION
Date Recvd: 12/17/2004 Sample Date; 12/10/2004
RUN# BATCH# PREP BT #<S)
DATE/TIME ANALYZED
1 137770 137770
12/21/2004 1545
1 137664 137664
12/21/2004 1246
DI LUT ION
Page 12
12
Job Number.: 232883 CUSTOMER :/Ueston: Solut ions; Tnc.
QUALITY CONTROL RESULTS project; confidential Decatur '
Report Date.: 12/30/2004
Test M e t h o d .... ,,..: Method .......... ..... :Method Oescription..% Sot ids Determination : Parameter. .,.;.r;r. ; % Sol ids
...
Batch........ : 13777P .. Equipment Code...-.:
QC Lab ID
Reagent
MB 137770-001
Units %
QC Result
QC Result
0.1000 U
True Value Orig. Value
A n a l y s t . : da j . . . Test Code..: :SsbLTo
QC Calc. F * Limits
Date Time 12/21/2004 1500
.Test .Method.. . . . . : Lloyd Kahn
.Method.Description.: Total organic carbon (Soits>
Parameter..
: Organic Cardon, Tot..(TOC)
QC Lab ID
Reagent
Units
ICV 137664-002 I04LSTTC2 MB 137664-003 LCS 137664-004 IQQFSTLK3 LCD 137664-005 I0FSTLK3
mg/Kg mg/Kg mg/Kg mg/Kg
QC Result
QC Result
1731.98 32.00
5172.65 3614.82
U
ccv 137664-016 I04LSTTC2
CCB 137664-017
CCV 137664-016 I04LSTTC2 CCB 137664-017
mg/Kg mg/Kg mg/Kg mg/Kg
2038.04 32.00
2032.44 32.00
U
u
Batch. . ...:iJ :137664' ' ' Equipment Code,.'; :.:T0C4
.Analyst,,,: C l S
. Test Cade.: TOC
rue Value 2000.00
4780.00 4780.00
2000.00
2000.00
Orig. Value 5172.65
QC CaLe. F * Limi ts
Date
Time
87 % 85-115 12/21/2004 0326 12/21/2004 0829
108 % 53-140 12/21/2004 0852 76 % 53-140 12/21/2004 0900 35 k
102 % 85-115 12/21/2004 1202
12/21/2004 1208 102 % 85-115 12/21/2004 1545
12/21/2004 1548
Page 13
* %=% REC, R=RPD, A=ABS Diff., D=% Diff.
13
.0 0 A 'L I T Y ' A S S U R A N C E R E FE R EMC E S AND
M Et H0b S
ESN :o t
Report Date: 12/30/2004
REPORT COMMENTS 1> All pages of this report are integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sampLe results are reported on a "dry weight" basis except when analyzed for
Landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted anaLyticaL method(s) meet the requirements of NELAC, Lab Cert. ID# 100201 5) According to AOCFR Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sampLe collection. When these parameters are not indicated as field (e.g. pH Field) they wore not analyzed irmiedistely, but as soon as possible on laboratory receipt.
Glossary of flags, qualifiers and abbreviations Cany number of which may appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated limit.
Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection limit. B Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is Less than the RL, but greater than or equaL to the methoddetection limit. Inorganic Flags (Flag Column)
ICV,CCV,ICB,CCB,I5A,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower control Limits. * LCS, LCD, MD: Batch QC exceeds the upper or Lower control limits. + MSA correlation coefficient is less than 0.995, 4 MS, MSD: The analyte present in the original sampLe is 4 times greater than the matrix spike concentration; therefore, control limits are not applicable. E SO: Serial diLution exceeds the control limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting limit or had a negative instrument reading lower than the absolute value of the reporting Limit. N MS, MSD: Spike recovery exceeds the upper or Lower control limits. U A(GFAA) Post-digestion spike was outside 85-115% control limits. Organic Qualifiers (Q - Column) U Analyte was not detected at or above the stated limit. ND Compound not detected. J Result is an estimated value below the reporting limit or a tentatively identified compound (TIC). Q Result was qualitatively confirmed, but not quantified. C Pesticide identification was confirmed by GC/MS. Y The chromatographic response resembles a typical fuel pattern, Z The chromatographic response does not resemble a typical fuel pattern. E Result exceeded calibration range, secondary diLution required. F AFCEE:Result is ah estimated value below the reporting limit or a tentativelyidentified compound (TIC) Organic Flags (Flags Column) B MB: Batch QC is greater than reporting Limit. * LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lowercontrol Limits. EBl, EB2, EB3, MLE: Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a diLution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Manually integrated compound. P The lower of the two values is reported when the % difference between the results of two GC columns is
Page 14
Q U A L I T'Y ' i S U R A U C M E T H 0 D S !'
FE R E n c E s and notes
Report Date: 12/30/2004
greater than 25%. Abbreviations AS Post Digestion Spike (GFAA Samples - See Nate 1 below) Batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set CAP Capillary CoLumh CCB Continuing Calibration Blank CCV Continuing Calibration Verification CF Confirmation analysis of original Cl Confirmation analysis of A1 or D1 C2 Confirmation analysis of A or D2 C3 Confirmation analysis of A3 or D3 CRA Low Level Standard Check - GFAA; Mercury CRI Low Level Standard Check - ICP CV Calibration Verification Standard Dil Fac Dilution Factor - Secondary diLution analysis D1 Dilution 1 D2 Dilution 2 D3 Dilution 3 DLFac Detection Limit Factor DSH Distilled Standard - High Level DSL Distilled Standard - Low LeveL DSM Distilled Standard Medina LeveL EB1 Extraction Blank 1 EB2 Extraction Blank 2 EB3 DI Blank ELC Method Extracted LCS ELD Method Extracted LCD 1CAL Initial calibration ICB Initial Calibration Blank ICV Initial Calibration Verification IDL Instrument Detection Limit ISA Interference Check Sample A - ICAP ISB Interference Check Sample B - ICAP Job No. The first six digits of the sample ID which refers to a specific client, project and sample group
Lab ID An 8 number unique laboratory identification LCD Laboratory Control Standard Duplicate LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest MB Method Blank or (PB) Preparation Blank MD Method Duplicate MDL Method Detection Limit MLE Medium Level Extraction Blank MRL Method Reporting Limit Standard MSA Method of Standard Additions MS Matrix Spike MSD Matrix Spike Duplicate ND Not Detected PREPF Preparation factor used by the Laboratory's Information Management System (LIMS) PDS Post Digestion Spike (ICAP) RA Re-analysis of original A1 Re-analysis of Di A2 Re-analysis of D2 A3 Re-analysis of D3 RD Re-extract ion of dilution RE Re-extraction of original RC Re-extract ion Confirmation RL Reporting Limit RPD Relative Percent Difference of duplicate (unrounded) analyses RRF Relative Response Factor RT Retentioh Time
Page 15
Q U A L I T Y A -S S U R A N C E H E T H O D S
references
N D OTE S
Report Date? T2/30/20Q4
RTW Retention Time Window Sample ID A 9 digit nimber unique for each sample, the first
six digits are referred as the job number
SCB Seeded Control Blank
SD Serial Dilution (Calculated when sample concentration exceeds 50 times the MDL)
UCB Unseeded Control Blank
S5V Second Source Verification Standard
SLCS
Solid Laboratory Control Standard(LCS)
PHC pH Calibration check LCSP pH Laboratory Control Sample
LCDP
pH Laboratory Control Sample Duplicate
HDPH
pH Sample Duplicate
MDFP
Flashpoint Sample Duplicate
LCFP
Flashpoint LCS
G1 Cel ex Check Standard Range C M
G2 Gelex Check Standard Range 1-10
G3 Gelex Check Standard Range 10-100
G4 Gelex Check Standard Range 100-1000
Note 1: The Post Spike Designation on Batch Qc for GFAA is designated with an "S" added to the current
abbreviation used. EX. LCS S=LCS Post Spike (GFAA); MSS=MS Post Spike (GFAA)
Note 2: The HD calculates ah absolute difference (A) when the sample concentration is less than 5 times the
reporting Limit. The control limit is represented as +/- the RL.
Page 16
16
CHAIN OF CUSTODY
CHAIN OF CUSTODY/ANALYSIS REQUEST FORM 3,3^88S
Severn Trent Laboratories
T: 708-534-5200
F: 708-534-5211
2417 Bond Street
University Park, IL 60466
PAGE / of
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 W eston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai Kesari em ail: i.kesari@ twestonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED 1
Sampler:
T Frinak, A Murphy
R.O. #: Quotation #:
Grab Sample Composite No. of Containers
TOC
SAMPLE ANALYSIS
ExyLJMS # . 1: -
r 3
4-
G 7
fc
V
" =: l O
Client Sample Identification DF09 SBC 131R 0 0000 DF09 SB 131R 0 0050 DF09 SBC 131R Oi 0050 DF09 SBC 131R 0; 0100 DF09 SBC 131R : 0 0160 DFG9 SBC 131R 0 0150 DFG9 SBCi 131R 0 0200 DF09 SBC' 131R 0 0250 DF06 SB 133B 0 0050 DF06 SB 133B 0 0160
^ Collection
Date
9-Dec434 9-Dec-04 9-Dec-04 9-Dec-04 ; 9-Dec-04 9-DeoG4 9-Dec-Q4 9-Dec-04 10-Dec-04 10-Dec-04
Collection
Time
11:55 12:05 12:15 12:30 12:40 13:00 13:25
X
2L ~x"
X IX
X
13:45
X
9:15 * x " 9:13 X
1
1
1 1 1 1 1 1 1 1
Sample
Matrix
SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL SOIL
|
j
CHAIN OF CUSTODY
Relinquished S
Datp
ffM/oH
TV
Cooler ID No.: |
|
Time
Received By: Fed Ex
v0 u -
Cooler Temp. (C): Date Time
tto o
Comments
X X X X X X X X X X
PROJECT REQUIREMENTS
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data _ i Other:
;
|
| 1
Sample Lot#:
Sam pie No. / _ .-fs-f
l IL S
!- ( &
Analysis
/UL
STL Chicago Internai Sample Custody Transfer Record
Client:
Relinquished by:
l j
Received by: ^ //
v & rC
D ate
Time
Comments
> -3f
H
CHi-22-11-001/01/99
rpjsckl
Job Sample Receipt checklist Report
Job Number.: 232883
Location.: 57222 Check List Number.: 1
Description.:
Customer Job ID.... :
Job Check List Date.: 12/17/2004
Project Number.: 20004B91 Project Description.: Confidential Decatur - FC Investigation
Customer...... : Weston Solutions, Inc.
Contact.: Jai Kesari
Questions ?
(Y/N) Comments
V2
Date of the Report. 12/3/204 Project Manager___ .: rew
Chain-of-Custody Present?..... ...,.............. . Y
Were samples dropped off at or picked up by STL?. . N
Custody seal on shipping container?.............. . Y
...If "yes", custody seal intact?...... ......... . Y
custody seaLs on sample containers?............. . N
...If "yes", custody seal intact?................
Samples iced?.................................
Y
Temperature of cooler acceptable? 4 deg C +/* 2) . Y 2.7
Samples received intact (good condition)?....... . Y
Volatile samples acceptable? (no headspace).....
Correct containers used?......................... . Y
Adequate sample volume provided?................. . Y
Samples preserved correctly?................... . . Y
Samples received within holding-time?............ . Y
Agreement between CQC and sample labels?........ . Y
Radioactivity at or below background levels?.... . Y
A Sample Discrepancy Report (SDR) was needed?___ . N
If samples were shipped was there an air bill #?. . Y
Sample Custodian Signaturc/Date..... .
.Y
Page 1
20
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Total Charges
CASE NARRATIVE
STL Chicago Wet Chemistry Case Narrative
Client: Weston Solutions, Inc. Job#: 232883
Date Rac'd: 12/17/04
1, This narrative covers the analysis of the samples in the above Job # for TOC by the Lloyd Kahn Method. The samples were analyzed for TOC in duplicate by furnace combustion and nondacisidpiefrisciavteioinnftroarreedmdoevteecintioorngaonnica cDaorbhormn,aannndPdhroyeinngix. 8N0o00coTrrOeCctioannawlyazserm, aadfete,rtherefore, for moisture content. The average of the sample bums is reported.
2. The method-recommended holding time of 2 weeks was met. Refer to the Laboratory Chronicle Page for dates of sampling, receipt, and analysis.
3. Tmheet aTcOceCptcaanlciberactriiotenricau.rve and the initial and continuing verification standards and blanks 4. The method blank was less than the reporting limit. 5. The LCSs were within acceptance limits, although the first attempt was very low and the
RPD between the repeated LCS and the LCD was high, at 35%. 6. The matrix QC was not done on samples from this Job#. 7. tOhne tfhuernfaircset watittehminptthfeoralslaomttepdleti2m3e28w8i3n-d1o,wth,eanadnatlhyestrfeasiuleltd, aton ienrsreorntetohuessnamonp-ldeebteocatt, iwntaos
not reported. The analyst spilled the sample boat during the second analysis of sample 232883-7, so that burn was discounted.
Wet Chemistry Section Manager
Date 23
RAW DATA
RUN LOG
***
<V2 )
12/30/04 12;45
Total Organic Carbon (Soils) Method Code,.: TOCS Batch Code...: 137664
S t a t u s ...... Batch Date... Batch Time...
RVUD 12/21/04 958
User Name..... : els QC Code....... : TOCS CaLc Code......: TOCS
Location Code.. Equipment Code. Import Code___
57222 TOC4
TEST CODE
TTTTTTTTTTTTT
O 0OO 0DC ccI1 1 cccC CcC S ssCC C
23 4AAA 2A sSS
VV V
V 2A
234 2 2
SAMPLE: Grp Pos 11
Sample ID ___ICAL_I04LSTTC1_
Pi Luti on
TEST POS Date / Time
1234 56 7 1 1 12 2 2 789 0 12
0
- "*
12
___ICV_I04LSTTC2_
12/21/04 0826 0
13
___MB__
12/21/04 0B29 0
14 15
___LCS_I00FSTLK3_ ___LCD_I00FSTLK3_4
12/21/04 0852 0
12/21/04 0900 it
16
23Z884_1^S___
12/21/04 0910
0
17
232884_1_S_MS_I04LSTTC2_6
12/21/04 0936
0
18
232884_1_S_MSD_I04LSTTC2_6
12/21/04 0943
0
19
1 10
1 11
1 12
232883_2_S___ 232883 1 S 232883_3_S___ 232883,,9_S___
12/21/04 0957 12/21/04 1014 12/21/04 1030 12/21/04 1047
0 0 0
0
-
1 13 232883_4_S___
12/21/04 1103
0
1 14 232883_5_S___
12/21/04 1124
0
1 15
1 16
232683,,6mS___ ___ C C V J 0 4 L $ T T C 2 _
12/21/04 1139 12/21/04 1202 0
0
... -
1 17 ___CCS__
12/21/4 1208 0
1 18 1 19
232883^7_S___ 232883_8_S___
12/21/04 1215 12/21/04 1235
0 0
-
1 20 232883J 0 _ S ___
12/21/04 1246
0
1 21 232885_1_S___
12/21/04 1328
0
1 22 232885_2_S___
12/21/04 1344
0
1 23 2328S5_3_S___
12/21/04 1406
0
1 24 232885^4^5___
12/21/04 1443
0
1 25 232885_5_S___
12/21/04 1504
0
... .
1 26 1 27
232885 6 5 232885_7_S___
12/21/04 1516 12/21/04 1530
0 0
1 28 ___CCV_I04LSTTC2_
12/21/04 1545 0
Page 1
25
##* RUN LOG
(V2 )
1 2 /3 0 /0 4 1 2 :4 5
Page 2
26
trk* QC Stimary
***
(V2 )
T o t a l O r g a n ic C a rb o n ( S o ils )
M e th o d C o d e B a tc h C o d e . s t a t u s ______ .
TOCS 137664 . : RVUD
B a tc h B a tc h
D a te .. T im e ..
U s e r N a m e .. .
: 1 2 /2 1 /0 4 : 958 : e ls
QC c o d e . . . . . , , : TOCS C a l c C o d e .................... : T O C S L o c a t io n C o d e .. : 5 7 2 2 2
G r p S m p S a m p le ID
Pos T e s t Result
Know n
O r ig in a l
12
IC V 1 0 4 L S T T C 2
1 TOC
1 7 3 1 .9 8
2000
13
___ MB__
1 TOC
-1 .8 0
14
15 17
______L C S _ I 0 0 F $ T L K 3 _ ______L C D _ I 0 0 F S T L K 3 _ 4 2 3 2 8 8 4 _ 1 _ S _ M S _ I0 4 L S T T C 2 _ 6
1 TOD
5 1 7 2 ,6 5
1 TOC
3 6 1 4 .8 2
5 TOCAV2 2 3 4 9 . 7 5
4780 4780 2000
5 1 7 2 .6 5 6 9 3 .6 7
18
2 3 2 8 8 4 J _ S J 1 S D _ I0 4 L S T T C 2 ^ 6
5 TQ C AV 2 1 9 5 5 .9 9
2000
6 9 3 .6 7
1 16 1 17
___ CCV_I04LSTTC2_ ___ CCB__
1 TOC 1 TOC
2 0 3 8 .0 4 -1 .8 8
2000
1 2 8 ______C C V _ I 0 4 L S T T C Z _
1 TOC
2 0 3 2 .4 4
2000
1 29
_____ C C B ____
1 TOC
-2 .9 0
R e p o rt D a te :
1 2 /3 0 /0 4
E q u ip m e n t C o d e .: I m p o r t C o d e ______ :
T0C 4
A l t e r n a t e QC Res
87
F QC R e s
2 3 4 9 .7 5
108 76 1 2 8 .7 9 1 .3 102
35 27
102
F
*
Page 1
27
*** RAU TEST DATA
(V2 )
Total Organic Carbon (Soils)
M e th o d C o d e B a tc h C o d e , S t a t u s .................
TOCS
137664
B a tc h D a te . B a tc h T im e .. . U s e r M a rn e ...
1 2 /2 1 /0 4 958 e ls
SAMPLE:
Grp P o s
S a m p le ID
11 12
ICAL I 0 4 L S T T C 1 ICV I 0 4 L S T T C 2
13
MB
14
L C S I0 0 F S T L K 3
15
LC D I0 0 F S T L K 3
16 17
232884 232884
1S 1 S MS
I0 4 L S T T C 2
6
18 19
232804 232883
1 S MSD 2S
0 4 L S T T C 2 6
1 10 2 3 2 8 0 3 1 S
1 11 2 3 2 0 8 3 3 S
1 12 2 3 2 8 0 3 9 S
1 13 23 28 83 4 S
1 14 2 3 2 8 8 3 5 S
1 15 2 3 2 0 0 3 6 S
1 16
C C V I0 4 L S T T C 2
1 17
CCB
71 1 8 2 3 2 8 8 3 S
1 19 2 3 2 8 8 3 8 S
1 20
23 28 83 10 S
1 21
232885 1 S
1 22 232885 2 S
1 23
232885 3 S
1 24
232885 4 S
1 25
232885 5 S
1 26 232805 6 S
71 2 7
232885
S
1 28
C C V I0 4 L S T T C 2
1 29
C C B ___
Q C C o d e ............................. : C a l c C o d e ..................... : L o c a t io n C o d e .. :
TOCS TOCS 57222
D ilu t io n
TO C m g /K g
TO C 2 m g /K g
Report Date: 12/27/4 16:35
E q u ip m e n t C o d e .: i m p o r t C o d e ______ :
T0C 4
T0C 3 m g /K g
T0C 4 m g /K g
T0C AV 2 m g /K g
1 7 3 1 .9 8
"1.S0
5 1 7 2 .6 5 3 6 1 4 .8 2 8 1 3 .5 1 2 3 4 9 .7 5 1 9 5 5 .9 9 1 5 5 3 .4 1 2 6 5 3 .6 9 1 2 6 3 .3 3 8 6 8 .9 2 0 2 7 .7 0 9 3 8 .2 9 8 1 6 .9 1 2 0 3 8 .0 4 -1 .8 8 0 7 3 .1 9 3 4 6 .2 9 4 3 2 .4 4 6 4 0 1 .3 7 1 6 7 1 .6 4 8 0 0 .7 8 8 3 5 .7 5 1 1 3 4 .8 6 6 4 0 .6 9 9 0 8 .9 6 2 0 3 2 .4 4 -2 .9 0
5 7 3 .S4
1 0 1 4 .9 1 2 1 0 2 .7 8 1 0 0 8 .7 8 6 2 6 .4 5 5 4 4 .3 3 5 3 .8 5 6 5 9 .0 9
7 5 0 .3 3 3 9 1 .5 6 4 9 7 .0 5 5 7 5 0 .3 0 1 3 1 0 .5 9 8 1 2 .4 1 7 9 2 .5 9 8 5 6 .9 3 1 0 1 6 .3 7 1 0 6 0 .0 9
6 9 3 .6 7 2 3 4 9 .7 5 1 9 5 5 .9 9 1 2 8 4 .1 6 2 3 7 8 .2 4 1 1 3 6 .0 6 8 4 7 .6 8 6 8 6 .0 1 4 9 6 .0 7 7 3 0 .0 0
8 1 4 .2 6 3 6 0 .9 3 4 6 4 .7 5 6 1 1 5 .0 4 1 4 9 1 .1 2 8 0 6 .6 0 8 1 4 .1 7 9 9 5 .8 9 8 2 8 .5 3 9 8 4 .5 2
1Pago
28
*** RAU TEST DATA
CVS )
Total Organic Carbon (Soils)
M e th o d C o d e . B a tc h C o d a ,. S t a t u s ______ . _
TOCS 137664 RVW D
B a tc h B a tc h
D a t e . ..: T im e .. . .:
1 2 /2 1 /0 4 958
U s e r N a m e .-,, : c ls
SAM PLE:
G rp P o s
S a m p le ID
11 12 13
IC A L 1 0 4 L S C 1 IC V 4 L S T T C 2 MB
14 15
LC S LC D
I0 0 F S T L K 3 I0 Q F S T L K 3
16
232884 1 S
17
2 3 2 8 8 4 1 S MS I0 4 L S T T C 2 6
18
2 3 2 8 8 4 1 S M SD I0 4 L S T T C 2 6
19
232883 2 S
1 10 2 3 2 8 8 3 1 S
1 11 2 3 2 8 8 3 3 S
1 12 2 3 2 8 8 3 9 S
1 13 2 3 2 8 8 3 4 S
1 14 2 3 2 8 8 3 5 S
1 15 2 3 2 8 8 3 6 S
1 16
C C V IQ 4 L S T T C 2
1 17
CCS
1 18 1 19
232883 7 S 232883 8 S
1 20 2 3 2 8 8 3 10 S
1 21
232885 1 S
1 22
232885 2 S
1 23
232885 3 S
1 24
232885 4 S
1 25
232885 5 S
1 26 1 27
232885 6 S 232885 7 S
1 28 1 29
CCV CCS
I0 4 L S T T C 2
Q C C o d e . . . .................: C a l e C o d e ..................... : L o c a t io n C o d e .. :
TOCS TO C S 57222
D ilu t io n
T0C AV 3 m g /K g
T0C AV 4 m g /K g
Report Date: 12/27/04 16:35
E q u ip m e n t C o d e .: Im p o rt C o d e .. . . :
TOC4
TO CRl ug
T0C R 2 ug
TO C R 3 ug
8 6 .5 9 B 9 -0 ,2 8 8 4 1 7 8 .9 7 3 6 9 1 .8 1 6 4 3 5 .8 7 5 9 1 8 3 ,5 1 5 1 1 4 1 .4 1 7 8 7 8 .1 3 6 6 1 7 8 .3 2 8 3 8 5 .7 7 9 9 6 7 .7 7 5 5 6 1 .9 1 2 2 7 5 .1 5 7 1 7 3 .9 3 0 7 1 0 1 .9 0 2 0 -0 .3 0 0 7 8 4 .8 3 3 1 2 7 .2 5 3 4 4 1 .4 2 8 1 1 7 8 .8 8 5 8 5 5 .6 6 5 6 3 3 .6 3 2 7 3 0 .9 2 2 6 6 2 .6 4 4 Q 3 8 .9 5 3 9 5 8 .7 1 9 1 1 0 1 .6 2 1 9 -0 .4 6 4 8
3 6 .2 0 9 4
7 2 .5 6 6 3 1 3 2 .6 8 5 3 8 4 .9 3 8 9 6 2 .8 9 2 6 5 3 .5 0 7 8 4 3 .5 0 9 4 5 3 .2 5 4 5
5 8 .9 0 1 0 3 4 .9 2 6 9 4 8 .1 1 4 7 1 2 4 .2 0 6 5 4 8 .3 6 0 8 3 2 .3 3 4 1 2 9 ,6 4 2 9 5 0 .0 4 4 7 6 0 .0 6 7 7 6 5 .9 3 7 5
Page 2
89
*** RAW TEST DATA
<V2 )
Total Organic Carbon (Soils)
M e th o d C o d a .. : B a tc h C o d e .. .: S t a t u s . . .................:
TOCS 137664 RVU>
B a tc h D a t e . . . : B a tc h T im e . . . : U s e r N a m e ..,.:
1 2 /2 1 /0 4 958 e ls
SAMPLE:
rp Pos Sample ID
11 12 13 14 15 16 17 1S 19 1 10 1n 1 12 1 13 1 14 1 15 1 16 1 17 1 16 1 19 1 20 1 21 1 22 1 23 1 24 1 25 1 26 1 27 1 2S 1 29
I C A L I0 4 L S T T C 1
ICV I 0 4 L S T T C 2
MB
L C S IQ Q F S T L I3
LC D I0 0 F S T L K 3
232884 232884 2328S 4
1S
S HS1 I 0 4 L S T T C 2 6
HSD1 S
I 4 L S T T C 2 6
232883 2 S
232883 1 S
232883 3 S
232883 9 S
232883 4 S
232883 5 S 232883 6 5
C C V I 4 L 5 T T C 2
CCB
232883 7 S
232883 8 S
232883 23288$
10 S 1S
232885 2 S
232885 3 S
232885 4 S
232885 5 S
232885 6 S
232885 7 S
C C V I0 4 L S T T C 2
CCB
QC C o d e ...
- TOCS
C a lc C o d e . * * b . . TO C S
L o c a t io n c o d e . . : 5 7 2 2 2
D i L u tio n
T0C R 4 US
U T1 9
Report Date: 12/27/04 16:35
E q u ip m e n t C o d e .; 0 C 4
Import Code m . :
U T2 s
W T3 S
UT 4 S
0 .0 5 0 .1 6 . 3 4 6 0 .0 2 5 4 0 .0 4 4 1 0 .0 7 8 1 0 .0 7 2 3 0 .0 5 0 3 0 .0 6 7 2 0 .0 6 7 9 0 .0 7 8 0 0 .0 7 4 8 .Q 8 0 1 0 .0 9 0 5 0 .0 5 0 .1 6 0 .0 9 6 6 0 .0 7 8 7 0 .0 9 5 8 0 .0 2 7 6 0 .0 3 3 3 0 .0 4 2 0 0 .0 3 7 0 0 .0 5 5 2 0 .0 6 0 8 0 .0 6 4 6 0 .0 5 0 .1 6
0 .0 6 3 1
0 .0 7 1 5 0 .0 6 3 1 0 .0 8 4 2 0 .0 7 6 1 0 .0 9 8 3 0 .8 0 8 0 .0 8 0 8
0 .0 7 8 5 0 .0 8 9 2 0 .0 9 6 8 0 .0 2 1 6 0 .0 3 6 9 0 .0 3 9 8 0 .0 3 7 4 0 .0 5 8 4 0 .0 5 9 1 0 .0 6 2 2
Page 3
30
*** RAU TEST DATA
***
Total Organic Carbon (Soils)
Method Code..
B a tc h C o d e ... S t a t u s . . .................
TOCS
137664
RVUD
B a tc h D a te .. . B a tc h T im e ... U s e r N a m e ______
1 2 /2 1 /0 4
956
c ls
SAM PLE:
G r p P o s Safiple I D
11
IC A L I0 4 L 5 T T C 1
12
IC V I0 4 L S T T C 2
13
MB
14 15
LC S LC D
I0 0 F S T L K 3 _ I0 0 F S T L C 3
16
232684 1 S
17
2 3 2 8 8 4 1 S MS I0 4 U
16
2 3 2 8 8 4 1 S MSD 1041
19
232883 2 S
1 10 2 3 2 8 8 3 1 S
1 11 2 3 2 8 8 3 3 S
1 12 2 3 2 8 8 3 9 S
1 13 23 2 6 8 3 4 S
1 14 2 3 2 8 8 3 5 S
1 15 2 3 2 8 8 3 6 S
1 16
C C V I0 4 L S T T C 2
1 17
CCB
1 18 23 2 6 6 3 7 S
1 19 232883. 8 S
1 20 2 3 2 8 8 3 10 $
1 21 1 22 1 23
232885 232885
15
2$
232885 3 S
1 24
2328S5 4 S
1 25
232885 5 S
1 26
232885 6 S
1 27
232885 7 S
1 28
C C V I0 4 L S T T C 2
1 29
CCB
O C C o d e ...............................: T O C S
Calc TOCSC o d e .................... :
L o c a t io n C o d e ..: 5 7 2 2 2
Dilution
DLFAC N/A
TCS mg/Kg
3 .2 0 0 0
1.0000
4 .6 2 4 3 6 .2 9 9 2 2 .9 6 5 1 2 .0 4 8 7 2 .2 1 3 0 2 .6 2 7 3 2 .4 5 5 9 2 .1 0 3 9 2 .0 7 6 6 1 .8 4 8 6 0 .3 6 0 3 1 .8 6 8 1
1.00003 . 2 0 0 0
1 .6 2 7 5 1 .9 0 5 9 1 .6 6 1 5 6 .5 0 4 1 4 .5 5 8 4 3 .9 1 2 0 4 .3 0 1 1 2 .8 1 6 9
2 .6 6 8 9 2 .5 2 3 7 3 .2 0 0 0
1.0000
(V2 )
Report Date: 12/27/04 16:35
E q u i p m e n t Code.: T O C 4
I n j j o r t C o d e ----------- :
TCS2
mg/Kg
TC SAV 2 m g /K g
TICS
m g /K g
Page 4
31
Calibration Report Print Date/Time: 2004/12/21 7:53:52
Cal. Curve ID:
SOILCURVE
Created:
12/13/200413:36
Calibration Factor (m): 9.841 e+04
Y Intercept (b): -250134
r-squared:
0.99935
Standard ID Y X Expected Measured Message
Date &
Raw Data ug C ug C
Time
0 ugram C
-8891 0.000 2.451 No Sample Det 12/13/2004 11:24
10ugramC
911065 10.000 11.800
12/13/200411:42
20 ugram C 1853385 20.000 21.375
12/13/2004 11:48
40 ugram C 3745719 40.000 40.605
12/13/200412:04
120 ugram C 11194916 120.000 116.302 Endpoint Time 12/13/200412:28
200 ugram C 18654032 200.000 192.099
12/13/200412:46
300 ugram C 29462156 300,000 301.928
12/13/200412:59
400 ugram C 39451668 400,000 403.439 Endpoint Time 12/13/200413:19
Multiple Analysis Report Print Date/Time: 2 00 4/l2/2t 15:53:46
Sample ID
Result Std. Dev. RSD Mode ALT
ICV
86.5989
TC
ICB-MB
-0.2884
TC
LCS
51.5042
TC
LCS................................ 178.9736............. ...TC ..
LCD
91.8164
TC
232884-1
35.8759
TC
232884-1............... ........... 36.2094...
...........TC
232884-1 ms
-0.3194
TC
232884-1 ms
183.5151
TC
232884-1 msd........ ................141.4178...
...........TC
232883-2
78.1366
TC
232883-2
72.5663
TC
232883-1............... ........... -0.2423...
. ...TC .
232883-1
178.3283
TC
232883-1
132,6853
TC
232883-3........................... 85.7799...
...........TC
232883-3
84.9389
TC
232883-9
67.7755
TC
232883-9........ .................. 62.8926...
...........TC .
232883*4
61.9122
TC
232883-4
53.5078
TC
232883-5........................... 74.1571...
...........TC .
232883-5
43.5094
TC
232883-6
73.9307
TC
232883-6........................... 53.2545...
...........TC .
CCV CCB
101.9020 -0.3007
TC TC
232883-7........................... 84.8331..,
.......... TC ,
232883-7
17.4619
TC
232883-7
58.9010
TC
232883-8........................... 27.2534...
.......... TC .
232883-8
34.9249
TC
232883-10
41.4281
TC
232883-10.............. ............48.1147...
...........TC
23288S-1 232885-1
466.7505 178.8858
TC TC
232885-1................ ...........124.2065...
...........TC
232885*2
55.6656
TC
232885-2
48.3608
TC
232885-3................ ...........-04558...
. ...TC ..
232885-3 232885-3
33.6327 32.3341
TC TC
232885-4................ ...........309226...
.......... TC .
232885-4
29.6429
TC
232885-5
62.6440
TC
232885-5................ ...........50.0447...
.......... TC .
232885-6
38.9539
TC
232885-6
60.0677
TC
232885-7................ .......... 58.7191...
232885-7
65.9375
.......... TC . TC
CCV
101.6219
CCB........................ ........-0.4648..............
TC ...TC ..
33
Detailed Analysis Report Print Date/Time: 2004712/2115:54:02
Sample ID: ICV Method: boat Calr Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12210820
y
Timestamp: 12/21/2004/08:26 j
Sample Type: Cal. Verificaiipn y
Rep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 86.5989 86.5989 8271924
0.942 1.939 282
Sample ID: ICB-MB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode; TC Filename: 12210827
Timestamp: 12/21/2 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 '0.2884 -0.2884 -2611
1.505 1.483 120
Last Message: No Sample Detected
= = = = = = ^ = = = = TM ^ 5 : ? 5 K : i i S = i i * = = = = = = = = = = = = S = = = = = = = = = = = = ^ x a ^ SSSWS
Sample ID: LCS \
.
Method: boat \ (
Cal. Curve: SOILCURVE-' ^
Operator ID: CAROL \ \
[
Mode: TC Filename: 12210836
Timestamp: 12/21/2004 08:41 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 51,5042 51.5042 5094^09
1.930 2.930 235
Sample ID: LCS Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210845
Timestamp: 12/21/20 Sample Type: Sample
08:52
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 178,9736 178.9736 17638262
1.819 2,818 370
Sample ID: LCD Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210855
Timestamp: 12/21/20 Sample Type: Sample
R ep# p p m C u g C Raw Data Beginning Ending Integration Baseline Baseline Time
1 91.8164 91,8164 9061265 1.951 2.949 265
Sample ID: 232884-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TO
Filename: 12210904
'
Timestamp: 12/21/200*09:10
Sample Type: Sample ^
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 35.8759 35.8759 3556254
1.793 2.792 276
Sample ID: 232884-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210910
Timestamp: 12/21/2004 09:14 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 36.2094 36.2094 3589071
2.138 3.136 201
S'
Sample ID: 232884-1ms
Mode: TC
Method: boat \
^ v Filename: 12210919
Cal. Curve: SOILCURVE. ^
Timestamp: 12/21/200409:22
Operator ID: CAROt, Q " . l a
Sample Type: Sample
\1
Rep # ppm C ug C Raw Data Beginning Ending Integration
\ Baseline Baseline Time
1 -0.3194 -0.3194 \-S 6 6 9
1.449 1.328 120
Last Message: No Sample Detected
Sample ID: 232884-1 ms Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210927
Timestamp: 12/21/2 Sample Type: Sample
Rep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 183.5151 183.5151 18085186
1.339 2.487 480
Last Message: Endpoint Timeout
Sample ID: 232884-1 msd Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210938
Timestamp: 12/21/21 Sample Type: Sample
09:43,
Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time
1 141.4178 141.4178 13942461 2.833 3.829 276
Sample ID: 232883-2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12210952
,
Timestamp: 12/21/2004 |Q9:57y
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 78.1366 78.1366 7715061
1.667 2.667 267
Sample ID: 232883-2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12210958
Timestamp: 12/21/2004 10:03 Sample Type: Sample
R e p # p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 72.5663 72.5663 7166895
1.886 2.880 262
= = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = = ^ " -- = = = = = = JT-- r ; ^ : = = = = = = =
Sample ID: 232883-1 \ p , i | f Mode:
TC
Method: boat
r ^ \ } Filename: 12211004
Cal. Curve: SOILCURVE $ V / y Timestamp: 12/21/2004 10:07
Operator ID: CAROL
^\ jM T Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 -0.2423 -0.2423 1918
1.363 1.396 120
Last Message: No Sample Detected
Sample ID: 232883-1 Method: boat Cal, Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12211008
Timestamp: 12/21/200410:14
Sample Type: Sample
\
R e p# ppm C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 178.3283 178.3283 17574762
2.128 3.125 319
Sample ID: 232883-1 Method: boat CaL Curve: SOILCURVE
Mode: TC Filename: 12211016
Timestamp: 12/21/2004 10:22
Operator ID: CAROL
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 132.6853 132.6853 13083108
2.104 3.102 285
Sample ID: 232883-3 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211025
Timestamp: 12/21/2 Sample Type: Sample
Rep # ppm C ug C
1 85.7799 85.7799 2.959 273
Raw Data Beginning Ending Baseline Baseline Time 8467224 1.965
Integration
Sample ID: 232883-3 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211036
Timestamp: 12/21/2004 10:41 Sample Type: Sample
R ep# p p m C ugC Raw Data Beginning Ending Integration
Baseline Baseline Time
1 84.9389 84.9389 8384461
1.541 2.540 276
Sample ID: 232883-9 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211042
Timestamp: 12/21/2<Xj4*1fr4J/ Sample Type: Sample
R ep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 67.7755 67.7755 6695443
1.925 2.923 268
Sample ID: 232883-9 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211048
Timestamp: 12/21/2004 10:53 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 62.8926 62.8926 6214923
1.941 2.940 260
Sample ID: 232883-4 Method: boat Cal. Curve: SOILCURVE
Mode: TC
_
Filename: 12211058
Timestamp: 12/21/2004^11:03
Operator ID: CAROL
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 61.9122 61.9122 6118446
1.640 2.638 269
Sample ID: 232883-4 Method: boat Cal. Curve; SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211106
Timestamp: 12/21/200411:11 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 53.5078 53.5078 5291377
1.765 2.764 251
Sample ID: 232883-5 Method: boat Cal. Curve; SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211119
Timestamp: 12/21/201 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 74.1571 74.1571 7323449
1.692 2.689 277
Sample ID: 232883-5 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211125
Timestamp: 12/21/2004 11:30 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 43.5094 43.5094 4307455
2.029 3.028 235
Sample ID: 232883-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211134
Timestamp: 1 2 /2 1 /2 0 0 yfl :39 Sample Type: Sample i
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 73.9307 73.9307 7301163
2.255 3.248 251
Sample ID: 232883-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211141
Timestamp: 12/21/2004 11:45 Sample Type: Sample
Rep# ppm C ugC Raw Data Beginning Ending Integration Baseline Baseline Time
1 53*2545 53.2545 5266458 2.383 3.381 234
Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TO Filename: 12211156
Timestamp: 12/21/20! Sample Type: Cal. Verifn
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 101.9020 101.9020 9777878
1.546 2.545 299
Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID. CAROL
Mode: TC Filename: 12211205
Timestamp: 12/21/2 Sample Type: Sample
Rep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 -0.3007 -0.3007 *3828
1.695 1.637 120
Last Message: No Sample Detected
Sample ID: 232883-7 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211210
Timestamp: 12/21/2 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 84.8331 84.8331 8374055
1.692 2.692 289
Sample ID: 232883-7
L
Mode:
TC
Method: boat
ilename: 12211218
Cal. Curve: SOILCURVE \ f Cj
Timestamp: 12/21/2004 12:22
Operator ID: CAROL
V\ ^ L Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 17.4619 17.4619 1744159
1.962 2.959 208
Sample ID: 232883-7 Method: boat Cal. Curve: SOILCURVE
Mode: TC Filename: 12211225
Timestamp: 12/21/2004 12:30
:=?i:3iii======
39
Operator ID; CAROL
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 58.9010 58.9010 5822114
1.961 2.955 260
Sample ID: 232883-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211230
Timestamp: 12/21/2 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 27.2534 27.2534 2707724
2.428 3.425 219
Sample ID: 232883-8 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211235
Timestamp: 12/21/2004 12:40 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 34.9249 34.9249 3462668
2.224 3.223 246
Sample ID: 232883-10 Method: boat
Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211242
Timestamp: 12/21/200412:46 Sample Type: Sample l
Re
p # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 41.4281 41.4281 4102640
6.401 7.396 184
Sample ID: 232883-10 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211247
Timestamp: 12/21/2004 12:52 Sample Type: Sample
R ep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 48.1147 48.1147 4760651
2.162 3.161 249
Sample ID: 232885-1 \ ^
Method: boat
\6
Cal. Curve: SOILCURVE U'V
Mode: TC Filename: 12211315
Timestamp: 12/21/2004 13:21
Operator ID: C^ROL
1* Sample Type: Sample
\ (t
Rep # ppm C \ug C Raw Data Beginning Ending
\ Baseline Baseline Tima
1 466.7505 466.7505 45957920
2.150 3.150
Integration 345
Sample ID: 232885-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211323
Timestamp: 12/21/21 Sample Type: Sample
R ep# p p m C u g C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 178.8858 178.8858 17629628
2.645 3.644 280
Sample ID: 232885-1 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211331
Timestamp: 12/21/200413:36 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 124.2065 124.2065 12248724
2.282 3.282 265
Sample ID: 232885-2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12211339
/
\
Timestamp: 12/21/2004 13:44
Sample Type: Sample l /
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 55.6656 55.6666 5503725
2.209 3.208 245
Sample ID: 232885-2 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211351
Timestamp: 12/21/2004 13:56 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 48.3608 48.3608 4784873
1.633 2.632 248
Sample ID: 2328i Method: boat Cal. Curve: SOILCUR Operator ID: CAROL
Mode: TC name: 12211358
Timestamp: 12/21/2004 14:01 Sample Type: Sample
3S E3
41
Rep# ppm C ugC (paw Data Beginning Ending Integration \ W* Baseline Baseline Time
1 -0.4558 -41.45& -19085 2.015 1.541 99
Sample ID: 232885-3 Method: boat CaL Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211402
Timestamp: 12/21/2004/14:06 Sample Type: Sample ( /
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 33.6327 33.6327 3335504
3.333 4.328 201
Sample ID: 232885-3 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode; TC Filename: 12211431
Timestamp: 12/21/200414:37 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 32.3341 32.3341 3207714
1.637 2.636 285
Sample ID: 232885-4 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12211438
S'
Timestamp: 12/21/2004/14:43
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 30.9226 30.9226 3068810
1.838 2.837 230
Sample ID: 232885-4 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211450
Timestamp: 12/21/2004 14:55 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 29.6429 29.6429 2942870
1.708 2.706 269
Sample ID: 232885-5 Method: boat Cal. Curve: SOILCURVE
Mode: TC Filename: 12211459
Timestamp: 12/21/21
15:04 /
42
Operator ID: CAROL
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 62.6440 62.6440 6190454
1.827 2.825 243
= = = = 3t= = = = = = ii= = = = = t3 2tff--= = T !3 ;= = = = = = = = ic = = = = = 2 i= = = = = S rsa S = ^ = = = = = a:= t3 ;S Jiit S = ^ !Ittt3 JfiS iJS
Sample ID: 232885-5 Method: boat Cai. Curve: SOILCURVE O peratorio: CAROL
Mode: TC Filename: 12211505
Timestamp: 12/21/2004 15:10 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 50.0447 50.0447 4950579
1.771 2.768 224
Sample ID: 232885-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211512
Timestamp: 12/21/2' Sample Type: Sample
15-16
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 38.9539 38.9539 3859158
3.971 4.970 199
Sample ID: 232885-6 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211517
Timestamp: 12/21/2004 15:22 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 60.0677 60.0677 5936929
2.520 3.516 242
Sample ID. 232885-7 Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC Filename: 12211524
Timestamp: 12/21/2 Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 58.7191 58.7191 5804212
1.978 2.976 289
:Ess;ss^s:s2r;==
Sample ID: 232885-7 Method: boat
Filename: 12211530 Cal. Curve: SOILCURVE
Mode: TC Timestamp: 12/21/2004 15:35
43
Operator ID: CAROL
Sample Type: Sample
Rep # ppm C ug C Raw Data Beginning Ending Integration
Baseline Baseline Time
1 65.9375 65.9375 6514565
2.105 3.104 263
Sample ID: CCV Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12211538
^ "-
Timestamp: 12/21/^004 15:45
Sample Type: Cal. Verification
R e p # p p m C ugC Raw Data Beginning Ending Integration
Baseline Baseline Time
1 101.6219 101.6219 9750314
1.707 2706 386
Sample ID: CCB Method: boat Cal. Curve: SOILCURVE Operator ID: CAROL
Mode: TC
Filename: 12211546
//
Timestamp: 12/21/200^15:48 /
Sample Type: Sample i
S
R ep# p p m C ugC Raw Data Beginning Ending Integration
Baseline Baseline Time
1 -0.4648 -0.4648 -19973
2.407 2.111 120
Last Message: No Sample Detected
tl Chicago
Page No.:_
110
TOC in Soils
Book No.:. 7y 7 77 T ~
Method; Lloyd Kahn
/ 3 CYInstrument Phoenix 8000 (T0C41 LabNet Batch:
C a lcu la tio n :
Date of Standard Curve. / - / / 3 /? ? :
TOC (mg/kg) ug C / gram* sample
Book # 7 7 7 7 page # / & (
MS. MSD Known Cone, (mg/kg) * 100 ug C / grams sample
MS, MSD Observed (mg/kg) * ug C / grams sample
MS, MSD Rec. * (observed mo/ko - avtr sample result (mo/koll x 100
known concentration in mg/kg
Standard Traceability; (Note; Working Standards are prepared daily from the noted Stock Solutions.)
Stock I (Curve) 7 7 ? </Z S T t C / Stock II (ICV/CCV) T o ^ ^ T T V ^
LCS Source ID ^ O O True Value
/<- Acceptance Range 7 7 --/ 7 ^ 7 ^
Sample ID;
Sample Weight (g)
S 2UJtO4Jcc1t--0s7'M"A7-nbbtCrt---oooOO~0Os-..\-ooL,,o*c0n7.asjOc0o7-.d.jjOn2J*oorcXo\-Soi3ujs0jHf?/H/tiQ_j.
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Comments;
. -7//'<f..n'\Ls.nrV%,,'if--. fj\)
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/ STO w 237?,7^ /&*/ \V^.7 7? 5T.77 U^3,/Z J"?/ ^
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Prep Analyst\ Analyst: Reviewed by:_
/it'l/,
Date: o / % f a / f ; g e ' l : oC` Date: / C - / 2 l / f \
Date:
ffa jC H
CHI-23-12-OSS/S-OS/01
STL Chicago
Page No.:
Hi
TOC in Soils Method: Lloyd Kahn
Book No.:
7 ^7
7 6GInstrument Phoenix 8000 fTOC4> LabNet Batch: / ^ /
fljc u Ia tio n e :
Date of Standard Curve:
^
TOC (mg/kg) = ug C / grams sample
Book # __ _ Paae #
MS, MSD Known Cone, (mg/kg) 100 ug C / grams sample
MS, MSD Observed (mg/kg) = ug C / grams sample
MS, MSD Rec. * fobserved mo/ko - ava. sample result (mo/koll x 100
known concentration in mg/kg
x ''
Standard Traceabllftv: (Note: Working Stai)dard3 areptepared daily from the noted Stock Solutions.)
Stock I (Curve)_______
f(iC V /C C V )___________________
LCS Source ID _____
__________ Acceptance Range___________________
03 5 8 3 - ^Sample ID:
Sample Weight (g)
ugC
5g*r?S>. 3S&Y
Comments:
ldc-eCic?-l0/~ T3--7
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Data:
/p.n / 7 ------- ------------ Date:
7
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i>fz7Jo1
CHI-l2-12iS7B-05roi
, ??
112
STL Chicago
Page No.:______ _
TOC in Soils
Book No. " ^ 7 Z Z
Method: Lloyd Kahn
Instrument Phoenix 8000 (TOC41
LabNet Batch:
C a lc u la tio n :
Date of Standard Curve:.
TOC (mg/kg) ug C / gram* sample
Book #._________ Pi
MS, MSD Known Cone, (mg/kg) - 100 ugC/ grams sample
MS, MSD Observed (mg/kg) * ug C / grams sample
MS, MSD Ree, (observed mg/kg - evo, sample result (mo/koll xlOO
known concentration in mg/kg
Standard Traceability: (Note; Working S tanfl^in^re-pfpared daily from the noted Stock Solutions.)
Stock I (Curve)_____________ M ^ -S t c k II (ICV/CCV)
LCS Source ID _______ /ff^ ^ L C S True Value___________ Acceptance Range
Sample ID:
Semple Weight (g)
ugC
0. C
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Prep Analyst Analyst: Reviewed by:
Date:
/('* * '* '
Date: S j z / - t / e - r ___
Date:
CH*22-ia4s5^-0V0l
k-kic RAW TEST DATA
***
<VZ )
% Solids Determination
Method Code..: SOLIDS Batch Code...: 137770 Status....... : RVWD
Batch Date...: 12/21/04 Batch Time...: 1613 User Name :daj
SAMPLE:
Grp Pos Sample ID
11
S MB
1 Z Z3Z854 1 S
1 3 232854 1 S MD 2
1 4 232S54 2 S
1 5 232854 3 S
1 6 232854 4 S
1 7 232854 5 S
1 8 Z3Z854 6 S
1 9 232854 7 S
1 10 232883 1 S
1 11 Z3ZB83 2 S
1 12 232883 3 S
1 13 232883 4 S
1 14 232883 5 S
1 15 232883 6 S
1 16 232883 7 S
1 17 232883 8 S
1 18 Z3Z883 9 S
1 19 232883 10 S
Report Date: 12/30/04 14:01
QC Code.........:SOLID Calc Code..,...: %S0L Location Code..: 57222
Equipment Code.: Import Code____ :
Dilution
%SOLID %
IWOT g
FWGT g
DRYWT g
WETWT g
0.0 90.8 90.5 92.9 96.9 80,7 64.6 90.2 92.8 81.5 80.7 78.7
00.5 79.7 79.4 74.1 78.6 81.7 83.9
10.3968 10.4604
10.3606 9,7569 10.3573 10.2764 9.8329 9.9714 9.8362 10.6880 10.0708 10.2327 10.3243 9.8972 10.2487 9.8008 10.0221
9.9579 9.9156
0.0021 9.4959 9.3765 9.0681 10.0335 8.2968 6.3556 8.9989 9.1307 8.7103 8.1227 8.0579 8.3140 7.8848 8.1393 7.2667 7.8733 8.1327 8.3147
1.3079 10.7975 10.6788 10.3639 11.3240 9.5734 7.6396 10.2898 10.4039 9.9816 9.3991 9.3349 9.5877 9.1714 9.4233 8.5454 9.1619 9.4233 9.6047
11.7026 11.7620 11.6629 11.0527 11.6478 11.5530 11.1169 11.2623 11.1094 11.9593 11.3472 11.5097 11.5980 11,1838
11-5327 11.0795 11.3107 11.2485 11.2056
Page 1
48
*** Raw test d a t a
***
(V2 >
% Solids Determination
Method Code..: SOLIDS Batch Code...: 137770 Status....... : RVUD
Batch Date...: 12/21/04 Batch Time...: 1613 User Name___ : daj
SAMPLE:
Grp Pos Sample ID
11
S MB
1 2 232854 1 S
1 3 232854 1 S MD 2
1 4 232854 2 S
1 5 232354"3 S
1 6 232854-4-S
1 7 232854 5 S
1 8 232854 6 S
1 9 232854 7 S
1 10 232883 1 S
1 11 232883 2 S
1 12 232883 3 $
1 13 232883 4 S
1 14 232883 5 S
1 15 232S83~6~S
1 16 232883 7 S
1 17 232883 8 S
1 18 232883~9-S
1 19 232883 10 S
QC Code........: SOLID Calc Code...... : %SOL Location Code,.: 57222
Di Luti on
TARE g
ASHWT g
1.3058 1.3016 1.3023 1.2958 1.2905 1.2766 1.2840 1.2909 1.2732 1.2713 1.2764 1.2770 1.2737 1.2866 1.2840 1-2787 1.2886 1.2906 1.2900
Report Date: 12/30/04 14:01
Equipment Code.: Import Code____ :
FASHUT 9
%MO]ST
%
100.0
9.2 9.5 7.1 3.1 19.3 35.4 9.8 7.2 18.5 19.3 21.3 19-5 20.3 20.6 25.9 21.4 18.3 16.1
%ASH %
Page 2
49
