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Heavy Still Bottoms Sample
May 1991 LCDavts
I. Attach bomb to fittings and tighten.
2 Check to sure the septum fitting is tight Hand tighten only. 3. Make sure bomb valves are closed.
4. Close valve "G".
5. Close valve 'A' and open "B".
6. Open valves 'D", T, "F", "H", and "C".
7. Feel tubing to be sure it Is warm and flowing.
8. Carefully open the bomb valves. Watch for leaks around septum.
9. Close valve T,^.
10. Circulate for minutes.
II. Close the outlet then the Inlet valve on the bomb.
12 Open valve T
13. Close valve "D" and allow to depressurize to bottoms line.
14. Close valve "H".
15. Close valve "B". 16. Carefully open valve "G" to relieve pressure.
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17. Carefully disconnect bomb.
12 Run Q.C. according to directions.
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19. Log results per previous Instructions.
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20. Reinstall bomb for next sample.
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