Document gabXNgr0xmn2Q5XJkeOQgegQa
SEVERN TRENT LABORATORIES ANALYTICAL REPORT
JOB NUMBER: 244964
Prepared For:
Weston Solutions, Inc. 1400 Weston Way Building 5-2
West Chester, PA 19380-1499
Project: Confidential Decatur - FC Investigation
Attention: Jai Kesari
Date: 03/23/2006
Signature Name: Richard C. Wright Title: Project Manager E-Mail: rwright@stl-inc.com
Date
STL Chicago 2417 Bond Street UcSveas iia Park, IL 60466
PHONE: (708) 534 5200 FAX..: (708) 534 5211
This Report Contains (_____) Pages
STL Chicago is part of Severn Trent Laboratories, Inc.
SA M P LE IN F O RM A T ION Date: 03/23/2006
Job Number. Customer... A t t n ......
244964 Weston Solutions, Inc. Jai Kesari
Project N u m b e r ......... Customer Project ID.... Project Description....
20004891 CONFIDENTIAL DECATUR Confidential Decatur - FC Investigation
Laboratory Sample ID
244964-1 244964-2 244964-3 244964-4 244964-5 244964-6 244964-7 244964-8 244964-9 244964-10 244964-11 244964-12 244964-13 244964-14 244964-15 244964-16 244964-17 244964-18 244964-19 244964-20 244964-21 244964-22 244964-23 244964-24 244964-25 244964-26
Customer Sample ID DF09-SS-0006-0-0000 DF09-SS-0006-0-0003 DF09-SS-0006-0-0010 DF09-SS-0007-0-0000 DF09-SS-0007-0-0003 DF09-SS-0007-0-0010 DF09-SS-0007-DB-0010 DF09-SS-0008-0-0000 DF09-SS-0008-0-0003 DF09-SS-0008-0-0010 DF09-SS-0009-0-0000 DF09-SS-0009-0-0003 DF09-SS-0009-DB-0003 DF09-SS-0009-0-0010 DF09-SS-0010-0-0000 DF09-SS-0010-0-0003 DF09-SS-0010-0-0010 DF09-SS-0011-0-0000 DF09-SS-0011-0-0003 DF09-SS-0011-0-0010 DF09-SS-0012-0-0000 DF09-SS-0012-DB-0000 DF09-SS-0012-0-0003 DF09-SS-0012-0-0010 DF09-SS-0013-0-0000 DF09-SS-0013-0-0003
Sample Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil
Date Sampled 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006 03/09/2006
Time Sampled
08:32 08:34 08:55 07:55 08:00 08:15 08:15 09:10 09:25 09:40 10:00 10:05 10:05 10:10 10:23 10:27 10:38 10:55 11:00 11:11 11:23 11:23 11:26 11:35 11:40 11:46
Date Received 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006 03/10/2006
Time Received
10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20 10:20
Page 1
STL Chicago is part of Severn Trent Laboratories, Inc.
SA M P LE IN F O RM A T ION Date:
Job Number. Customer... A t t n ......
244964 Weston Solutions, Inc. Jai Kesari
Project N u m b e r ......... Customer Project ID.... Project Description....
20004891 CONFIDENTIAL DECATUR Confidential Decatur - FC Investigation
Laboratory Sample ID
244964-27
Customer Sample ID
DF09-SS-0013-0-0010
Sample Matrix
Soil
Date Sampled
03/09/2006
Time Sampled
11:50
Date Received
03/10/2006
Time Received
10:20
Page 2
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0006-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:32 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-1 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 24000
|Q 'FLAGS ' ll I II I
MDL 420
I RL I 1800
IDILUTION I UNITS II I1 I mg/Kg
I BATCH IDT ' DATE/TIME ITECH
III
I
1176370 I I03/21/06 1 2 0 6 i l s
* In Description = Dry Wgt.
Page 3
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0006-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:34 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-2 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4700
|Q 'FLAGS ' ll I II I
MDL 440
I RL I 1900
IDILUTION I UNITS II I1 I mg/Kg
I BATCH IDT ' DATE/TIME ITECH
III
I
1176370 I I03/21/06 1 2 2 2 i l s
* In Description = Dry Wgt.
Page 4
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0006-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:55 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-3 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4000
|Q 'FLAGS ' ll I II I
MDL 250
I RL I 1100
IDILUTION I UNITS II I1 I mg/Kg
I BATCH IDT ' DATE/TIME ITECH
III
I
1176370 I I03/21/06 1 2 3 5 i l s
* In Description = Dry Wgt.
Page 5
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0007-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 07:55 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-4 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4000
|Q 'FLAGS ' ll I II I
MDL 220
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 950 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1 3 3 0 i l s
* In Description = Dry Wgt.
Page 6
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0007-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:00 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-5 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 5300
|Q 'FLAGS ' ll I II I
MDL 220
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 930 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1 3 4 6 i l s
* In Description = Dry Wgt.
Page 7
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0007-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:15 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-6 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1800
|Q 'FLAGS ' ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 750 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1 4 0 l t l s
* In Description = Dry Wgt.
Page 8
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0007-DB-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 08:15 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-7 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1700
|Q 'FLAGS ' ll I II I
MDL 190
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 800 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1424 i l s
* In Description = Dry Wgt.
Page 9
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0008-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 09:10 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-8 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 7600
|Q 'FLAGS ' ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 720 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1440 i l s
* In Description = Dry Wgt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0008-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 09:25 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-9 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 7300
|Q 'FLAGS ' ll I II I
MDL 200
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 850 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1453 i l s
* In Description = Dry Wgt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0008-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 09:40 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-10 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 3700
|Q 'FLAGS ' ll I II I
MDL 210
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 890 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1506Icls
* In Description = Dry Wgt.
Page 12
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0009-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:00 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-11 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4800
|Q 'FLAGS ' ll I II I
MDL 180
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 780 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1 5 1 8 i l s
* In Description = Dry Wgt.
Page 13
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0009-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:05 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-12 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4400
|Q 'FLAGS ' ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 730 I1
I I mg/Kg
III
I
1176370 I I03/21/06 1 5 3 0 i l s
* In Description = Dry Wgt.
Page 14
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0009-DB-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:05 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-13 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 3200
|Q 'FLAGS ' ll I II I
MDL 190
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 820 I1
I I mg/Kg
III
I
1176497 I I03/22/06 0838 i l s
* In Description = Dry Wgt.
Page 15
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0009-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:10 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-14 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4000
|Q 'FLAGS ' ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 720 I1
I I mg/Kg
III
I
1176497 I I03/22/06 0 9 l 2 c l s
* In Description = Dry Wgt.
Page 16
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0010-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:23 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-15 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 4900
|Q 'FLAGS ' ll I II I
MDL 190
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 810 I1
I I mg/Kg
III
I
1176497 I I03/22/06 0 9 4 6 i l s
* In Description = Dry Wgt.
Page 17
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0010-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:27 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-16 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 2500
|Q 'FLAGS ' ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 740 I1
I I mg/Kg
III
I
1176497 I I03/22/06 0 9 5 9 i l s
* In Description = Dry Wgt.
Page 18
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0010-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:38 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-17 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1300
|Q 'FLAGS ' ll I II I
MDL 98
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 420 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 0 1 6 i l s
* In Description = Dry Wgt.
Page 19
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0011-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 10:55 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-18 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1800
|Q 'FLAGS ' ll I II I
MDL 110
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 490 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 0 2 9 i l s
* In Description = Dry Wgt.
Page 20
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0011-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:00 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-19 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 3900
|Q 'FLAGS ' ll I II I
MDL 180
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 750 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1407 i l s
* In Description = Dry Wgt.
Page 21
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0011-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:11 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-20 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 2500
|Q 'FLAGS ' ll I II I
MDL 92
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 400 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 0 5 2 i l s
* In Description = Dry Wgt.
Page 22
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0012-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:23 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-21 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1400
|Q 'FLAGS ' ll I II I
MDL 120
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 520 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 1 0 6 t l s
* In Description = Dry Wgt.
Page 23
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0012-DB-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:23 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-22 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1400
|Q 'FLAGS ' ll I II I
MDL 100
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 440 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1127 i l s
* In Description = Dry Wgt.
Page 24
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0012-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:26 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-23 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 2400
|Q 'FLAGS ' ll I II I
MDL 100
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 450 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1143 l l s
* In Description = Dry Wgt.
Page 25
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0012-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:35 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-24 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 1300
|Q 'FLAGS ' ll I II I
MDL 79
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 340 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 2 1 2 i l s
* In Description = Dry Wgt.
Page 26
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0013-0-0000 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:40 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-25 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 950
|Q 'FLAGS ' ll I II I
MDL 86
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 370 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 3 2 2 i l s
* In Description = Dry Wgt.
Page 27
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0013-0-0003 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:46 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-26 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 750
|Q 'FLAGS ' ll I II I
MDL 74
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 320 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1 3 3 6 l l s
* In Description = Dry Wgt.
Page 28
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF09-SS-0013-0-0010 Date Sampled..... : 03/09/2006 Time Sampled..... : 11:50 Sample M a t r i x .... : Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn
!Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B O RA T O R Y
TE ST
R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID Date Rece i v e d ...... Time Rece i v e d ......
244964-27 03/10/2006 10:20
Date:03/23/2006 ATTN: Jai Kesari
| SAMPLE RESULT I | 700
|Q 'FLAGS ' ll I II I
MDL 66
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 280 I1
I I mg/Kg
III
I
1176497 I I03/22/06 1354 i l s
* In Description = Dry Wgt.
Page 29
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
LA B O RA T O R Y
CHR ON IC LE
Date: 03/23/2006
| CUSTOMER: Weston Solutions, Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
| Lab ID: 244964-1 | METHOD | EDD | Lloyd Kahn
Client ID: DF09-SS-0006-0-0000 DESCRIPTION Electronic Data Deliverable Total Organic Carbon (Soils)
| Lab ID: 244964-2 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0006-0-0003 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-3 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0006-0-0010 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-4 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0007-0-0000 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-5 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0007-0-0003 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-6 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0007-0-0010 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-7 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0007-DB-0010 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-8 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0008-0-0000 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-9 | METHOD | Lloyd Kahn
Client ID: DF09-SS-0008-0-0003 DESCRIPTION Total Organic Carbon (Soils)
| Lab ID: 244964-10 Client ID: DF09-SS-0008-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-11 Client ID: DF09-SS-0009-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-12 Client ID: DF09-SS-0009-0-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-13 Client ID: DF09-SS-0009-DB-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-14 Client ID: DF09-SS-0009-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-15 Client ID: DF09-SS-0010-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1
1 176370 176370
03/21/2006 1206
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1222
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1235
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1330
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1346
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1401
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1424
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1440
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1453
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1506
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1518
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176370 176370
03/21/2006 1530
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 0838
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 0911
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 0946
DILUTION
Page 30
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244964
LA B O RA T O R Y
CHR ON IC LE
Date: D3/23/2006
| CUSTOMER: Weston Solutions, Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
| Lab ID: 244964-16 Client ID: DF09-SS-0010-0-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-17 Client ID: DF09-SS-0010-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-18 Client ID: DF09-SS-0011-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-19 Client ID: DF09-SS-0011-0-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-20 Client ID: DF09-SS-0011-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-21 Client ID: DF09-SS-0012-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-22 Client ID: DF09-SS-0012-DB-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-23 Client ID: DF09-SS-0012-0-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-24 Client ID: DF09-SS-0012-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-25 Client ID: DF09-SS-0013-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-26 Client ID: DF09-SS-0013-0-0003
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244964-27 Client ID: DF09-SS-0013-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 0959
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1016
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1029
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1407
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1052
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1106
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1127
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1143
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1212
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1322
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1336
DILUTION
Date Recvd: 03/10/2006 Sample Date: 03/09/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 176497 176497
03/22/2006 1354
DILUTION
Page 31
QUA L ITY A SSU RA N CE M E THO D S RE FEREN CE S A N D N O TE S Report Date: 03/23/2006
REPORT COMMENTS 1) All pages of this report are integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for
landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 5) According to 40CER Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt.
Glossary of flags, qualifiers and abbreviations (any number of which ma y appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated limit. < Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection limit. B Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the methoddetection limit. Inorganic Flags (Flag Column) A ICV,CCV,ICB,OCB,ISA,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower
control limits. * LCS, LCD, MD: Batch QC exceeds the upper or lower control limits. + M S A correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater
than the matrix spike concentration; therefore, control limits are not applicable. E SD: Serial dilution exceeds the control limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting limit or had a
negative instrument reading lower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or lower control limits. Wf AS(GFAA) Post-digestion spike was outside 85-115% control limits. Organic Qualifiers (Q - Column)
Analyte was not detected at or above the stated limit. Compound not detected. Result is an estMiated value below the reporting limit or a tentatively identified compound (TIC). Result was qualitatively confirmed, but not quantified. Pesticide identification was confirmed by GC/MS. The chromatographic response resembles a typical fuel pattern. The chromatographic response does not resemble a typical fuel pattern. Result exceeded calibration range, secondary dilution required. AFCEE:Result is an estMiated value below the reporting limit or a tentatively identified compound
(TIC)
B MB: Batch QC is greater than reporting limit. +- LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits.
EB1, EB2, EB3, M E : Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is b elow the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not
obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Manually integrated compound. P The lower of the two values is reported when the % difference between the results of two GC columns is
Page 33
QUA L ITY A SSU RA N CE M E THO D S RE FEREN CE S A N D N O TE S Report Date: 03/23/2006
greater than 25%.
Abbreviations
AS Post Digestion Spike (GFAA Samples - See Note 1 below)
Batch
Designation given to identify a specific extraction, digestion, preparation set, or analysis set
CAP Capillary Column CCB Continuing Calibration Blank
CCV Continuing Calibration Verification
CF Confirmation analysis of original
C1 Confirmation analysis of A1 or D1
C2 Confirmation analysis of A2 or D2
C3 Confirmation analysis of A3 or D3
CRA Low Level Standard Check - GFAA; Mercury
CRI Low Level Standard Check - ICP
CV Calilbration Verification Standard
Dil Fac Dilution Factor - Secondary dilution analysis
D1 Dilution 1
D2 Dilution 2
D3 Dilution 3
DLFac
Detection Limit Factor
DSH Distilled Standard - High Level
DSL Distilled Standard - Low Level
DSM
Distilled Standard - Medium Level
EB1 Extraction Blank 1
EB2 Extraction Blank 2
EB3 DI Blank
ELC Method Extracted LCS
ELD Method Extracted LCD
ICAL
Initial calibration
ICB Initial Calibration Blank
ICV Initial Calibration Verification
IDL Instrument Detection Limit
ISA Interference Check Sample A - ICAP
ISB Interference Check Sample B - ICAP
Job No. The first six digits of the sample ID which refers to a specific client, project and sample group
Lab ID An 8 number unique laboratory identification
LCD Laboratory Control Standard Duplicate
LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest
M B Method Blank or (PB) Preparation Blank
MD Method Duplicate
MDL
Method Detection Limit
MLE
Medium Level Extraction Blank
MRL
Method Reporting Limit Standard
MSA
Method of Standard Additions
MS Matrix Spike
MSD
Matrix Spike Duplicate
ND Not Detected
PREPF
Preparation factor used b y the Laboratory's Information Management System (LIMS)
PDS Post Digestion Spike (ICAP)
RA Re-analysis of original
A1 Re-analysis of D1
A2 Re-analysis of D2
A3 Re-analysis of D3
RD Re-extraction of dilution
RE Re-extraction of original
RC Re-extraction Confirmation
RL Reporting Limit
RPD Relative Percent Difference of duplicate (unrounded) analyses
RRF Relative Response Factor
RT Retention Time
Page 34
QUA L ITY A SSU RA N CE M E THO D S RE FEREN CE S A N D N O TE S Report Date: 03/23/2006
RTW
Retention Time Window Sample ID A 9 digit number unique for each sample, the first
six digits are referred as the job number
SCB Seeded Control Blank
SD Serial Dilution (Calculated when sample concentration exceeds 50 times the MDL)
UCB
Unseeded Control Blank
SSV
Second Source Verification Standard
SLCS
Solid Laboratory Control Standard(LCS)
PHC pH Calibration Check LCSP pH Laboratory Control Sample
LCDP
pH Laboratory Control Sample Duplicate
MDPH
pH Sample Duplicate
MDFP
Flashpoint Sample Duplicate
LCFP
Flashpoint LCS
G1 Gelex Check Standard Range 0-1
G2 Gelex Check Standard Range 1-10
G3 Gelex Check Standard Range 10-100
G4 Gelex Check Standard Range 100-1000
Note 1: The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current
abbreviation used. EX. LCS S=LCS Post Spike (GFAA); MSS=MS Post Spike (GFAA)
Note 2: The M D calculates an absolute difference (A) when the sample concentration is less than 5 times the
reporting limit. The control limit is represented as +/- the RL.
Page 35
