Document gaN5bxbN61yaQBKnRz34YZ4VG
Septexuber 27, 1965 Supersedes Formula No Dated June 7, 1965
TEX-993
PLAINTIFF'S EXHIBIT
AC.m TEXAS PLANT FORMULA
ONE DAY WALLBOAR'O idf.m COMPOUND TEX-993
DESOi; IPTi'ON OF PRODUCT' - For use in aiL applications in the reinforcing and concealing oi joints, except the final finish.
FOjiiiliLA
Raw Material^
Source
R.M. Spec.
Sodium Citrate* Natrosol 250 HXR
(Fine Grind) Gslvatol 20-30 BP Gelva D-702 Clay, ASP-100 Asbestos 7RF-9 / TEX-33 Petro-AD Yellow Oxide #2087
Open Market
Hercules Powder Shawinigan F.esins Co. Shawinigan Resins Co. Minerals Chemicals Co. Phillip Carey Co, Bestwail Gypsum, Acme The Thoruley Co. C. K. Williams Co.
134
170 162 161 167
9
143 139
aVary to adjust setting time.
Working Consistency - Refer to Plant Testing Procedure Wo, 32.
%
0.125
0.50 1.50 3.00 3.00 4.50 87.075 0.100 0.200
100.0001
Specification
- Maximum 62
Minimum " 58
Average 60
Setting,Time
Refer to Plant Testing Procedure No. 6 (slow set).
Specification
- Maximum 3 hrs ,
45 mins.
Minlmuia 2 hrs.
45 mins.
Average 3 hrs. 15 mins.
Working Properties - Refer to Plant Testing Procedure No. 33.
Specification
- Must be plastic and buttery working; free of grit or coarse particles.
Bonding Properties - Refer to Plant Testing Procedure No. 35.
sp. ecification
- After compound has dried, tape shall delaminate when peeled back.
Crack Resistance
Refer to Plant Testing Procedure No. 37.
Specification *
- There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ Denotes change in this reissue.
DAM: se
SGP 0018381
March 4, 1966 Supersedes Formula No. TEX-993 Dated September 27, 1965
ACHE r TEXAS PLANT FORMULA ONE DAY WALLBOABD JOINT COMPOUND TEX-993
DESCRIPTION OF PRODUCT - For use lu all applications in the reinforcing and concealing of joints, escept the final finish.
FORMULA
Raw Material
/ Sodium Citrate* Natrosol 250 HXR (Fine Grind) Gelvatol 20-30 BP Gelva D-702 Clay, ASP-100 Asbestos 7RF-9
/ TEX-38 Petro-AD Yellow Oxide #2087
Source
Open Market
Hercules Powder Shawlnigan Resins Co. Shawinigau Resins Co. Minerals Chemicals Co. Phillip Carey Co. Bestwall Gypsum, Acme The Thornley Co. C. K. Williams Co.
R.M. Spec.
134
170 162 161 167
9 143 139
..% .
.25
0.50 1.50 3.00 3.00 4.50 86.95 0.100 0.200
*Vary to adjust setting time.
100.000%
/ Working Consistency - Refer to Plant Testing Procedure No. 32.
Specification
Maximum 60
Minimum TM56------
Average 38
/ Setting Time iwwinai jrf . Specification
- Refer to Plant Testing Procedure No. 6 (slow set)
Maximum 4 hrs.
30 mins.
Minimum 3 hrs.
30 mins.
Average 4 hrs.
Working Properties - Refer to Plant Testing Procedure No. 33.
Specification
- Must be plastic and buttery working; free of grit or coarse particles.
Bonding Properties
-----1- ~r ~ ini --ipnTri ii mi mii Irwrin'~ir ~r i~i~i |~
Specification
Refer to Plant Testing Procedure No. 35.
After compound has dried, tape shall delaminate when peeled back.
Crack Resistance - Refer to Plant Testing Procedure No. 37.
Specification
- There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ Denotes change in this re-issue.
DAMsse
SGP 0018382
December 26, 1967 Supersedes Formula No. TEXDated1 June 14, 1967
ACME, TEXAS PLANT FORMULA ONE DAY WALLBOARD JOINT COMPOUND TEX-993
DESCRIPTION OF PRODUCT
For use in all applies fcions in the reinforcing and concealing of joints, except the final finish.
FORMULA Raw Material
Source
R.M. Spec.
Percent
Sodium Citrate* Natrosol 250 HXR
(Fine Grind) Gelvatol 20-30 BP Gelva D-702 Clay K-70 Asbestos 7RF-9 TEX-38 Petro-AD Yellow Oxide #2087
Open Market
Hercules Powder Shawinigan Resins Co. Shawinigan Resins Co. Magcobar Minerals Co. Phillip Carey Co. Acme Plant The Thornley Co. C. K. Williams Co.
*Vary to adjust setting time.
134
170 162 161 167
9 143 139
0.25 .
0.50 1.50 3.00 3.00 4.50 86.95 0.10 0.20 100.00
WORKING CONSISTENCY - Refer to Plant Testing Procedure No. 32.
Specification:
Maximum
Minimum
Average
60 56 58
SETTING TIME Specification:
- Refer to Plant Testing Procedure No. 6 (slow set)
Maximum
Minimum
Average
4 hrs .
3 hrs
3 hrs. 30 mins.
WORKING PROPERTIES Specification:
- Refer to Plant Testing p- ocedure No. 33. Must be plastic and buttery working; free of grit or coarse particles.
BONDING PROPERTIES Specification:
- Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specification:
- Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ Denotes change in this reissue.
DRGrkkt
SGP 0018383
January 5, 1968 Supersedes Formula No. TEX-993 Dated Dec. 26, 1967
ACME, TEXAS PLANT FORMULA ONE DAY WALLBOARD JOINT COMPOUND TEX-993
DESCRIPTION OF PRODUCT - For use In all applications in the reinforcing and concealing of joints, except the final finish.
FORI''.'LA
Raw Material
Source
R.M. Spec.
Percent
Sodium Citrate* Nat rosol 250 HXR
^Fine Grind) Gel /atol 20-30 BP Gel a D-702 Clay K-70 Asbestos 7RF-9 TEX-38 Petro-AD Yellow Oxide #2087
Open Market
Hercules Powder Shawinigan Resins Co. Shawinigan Resins Co. Magcobar Minerals Co. Phillip Carey Co. Acme Plant The Thornley Co. C. K. Williams Co.
*Vary ,to adjust setting time.
134 0.25
170 0.50 162 1.50 161 3.00 167 3.00
9 4.50 - 86.95 143 0.10 139 0.20
100.00
- c*m-
WORKING CONSISTENCY Specification:
Refer to Plant Testing Procedure No. 32.
Maximum
Minimum
Average
60 56 58
**SETTING TIME Specification:
-
Refer to Plant Testing Procedure No. 6 (slow set)
Maximum
Minimum
Average
4 hrs.
3 hrs.
3 hrs. 30 mins.
WORKING PROPERTIES Specification:
Refer to Plant Testing Procedure No. 33. Must be plastic and buttery working; free of grit or coarse particles.
BONDING PROPERTIES Specification:
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specification:
Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
/ **REMARKS
- Shipments to The Flintkote Co. shall have a set of 1% to 2\ hours (2 hr. average) tested at the consistency shown in ASTM Designation C474.
-/ Denotes change in this reissue
JRW:kkt
SGP 0018384
June 24, 1968 Supersedes Formula No. TEXDated Jan. 5, 1968
ACME. TEXAS PLANT FORMULA
ONE DAY WALLBOARD JOINT COMPOUND TEX-993
DESCRIPTION OF PRODUCT - For use in all applications if the reinforcing and concealing of joints, except the final finish.
FORMULA Raw Material
Source
Sodium Citrate* Nutrosol 250 ;XR
(Fine Grind) Gclw.tol 20-30 BP Gelva D-702 Clay K-70 Asbes tos 7Ft.- -9 TEX-38 P e t r o-AD Yellow Oxide #2087
Open Market
Hercules Powder Shawinigan Resins Co. Shawinigan Resins Co. Magcobar Minerals Co. Phillip Carey Co. Acme Plant The Thornley Co. C. K. Williams Co.
* Vary to adjust setting time.
R.M . Spec.
134
170 162 161 167
9 -- 143 139
Perc ent
. fO 0.-25r
0.50 1.50 ^ 3.00 C. o 3.00 4.50 86.95 0.10 0.20 100.00
WORKING CONSISTENCY Specification:
Refer to Plant Testing Procedure No. 32.
Maximum
Minimum
Average
60 56 58
SETTING TIME Specification:
Refer to Plant Testing Procedurei No. 6 (slow set) .
Maximum
Minimum
Average
3 hrs.
2 hrs.
21; hrs.
WORKING PROPERTIES Specification:
Refer to Plant Testing Procedure: No. 33. Must be plastic and buttery working; free of grit or coarse particles.
BONDING PRO ERTIES Specification:
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specification:
Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
REMARKS
Shipments to The Flintkote Co. shall have a set of \\ to
2J2- hours (2 hr. average) tested at the consistency shown
in ASTM Designation C474.
-/ Denotes change in this reissue.
JRW:kgc
SGP 0018385
February 12, 1070 Supersedes Formula 993 Dated 6/24/68
ACME, TEXAS PLA XT FORMULA
SPEED SET JOINT COMPOUND (YELLOW! TEX-993 (60 Minute and 2 hour working cement)
DESCRIPTION OF PRODUCT - For use in reinforcing and conceiling joints and nailheads.
-/ FOKMliT.A
Raw Material
Function
R.M. Spec.
:Sodium Citrate Natrosoi 25 HXR Gelvatol RS-6219 Gelva GP702 Asbestos 7RF-9 Defoamer Mill TEX-38 Yellow Oxide
Retarder Thickner Adhesive Adhesive Fiber Filler Defoamer Plaster Pigment
134 170 162 167
9 196
139
f Adjust quantity according to set time requirements.
Percent
0.1 0.2 3.0 1.0 3.5 0.1 91.9
.2 1GG.0
Lbs/Beitch
2 4 80 20 70 2
1838 4
2C00
J2 oi.
/L 2 2 i a 3 oz
7 a S'** & * & 4-2 2. / /<? a . 6 S3 t S 4,; l 13 Fez:
WORKING CONSISTENCY Spec ifications:
Refer to Plant Testing Procedure No. 32.
Maximum
Minimum
Aver e
60 56 58
SETTING TIME Specifications: -
WORKING PROPERTIES Spec ifications:
Refer to Plant Testing Procedure No. 6 (slow set)
Maximum
Minimum
Average
110 mins. 3^ hours
70 mins, hours
90 mins. 3 hours.
Refer to Plant Testing Procedure No. Must be plastic and buttery working; coarse particles.
JoO-n . free of grit
or
BONDING PROPERTIES Specifications:
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specifications:
Refer to Plant Testing Procedure No. 37.
There shall be no large fissure craclks in cka
and
very few, if any, cracks in the thin;net naif of cna
wedge.
-/ Denotes change in this reissue.
EDO:dek
SGP 0018386
February 27, 1970 Supersedes Formula 993 Dated 2/12/70
ACME, TEXAS PLANT FORMULA
SPEED SET JOINT COMPOUND (YELLOW) TEX-993 (60 minute and 2 hour working cement)
DESCRIPTION OF PRODUCT:
For use in reinforcing and conceiling joints and nailheads.
FORMULA Raw Material
*Sodium Citrate Cellosize QP 100,000 Gelvatol RS-6219 Gelva GP702 Asbestos 7RF-9 Defoamer Mill TEX-38 Yellow Oxide
Function
Retarder Thickner Adhesive Adhesive Fiber Filler Defoamer Plaster Pigme nt
R.M.Spec.
134
162 167
9 196
139
Percent
0.1 0.2 3.0 1.0 3.5 0.1 91.9
2 100.0
Lbs/Batch
2 '2
4/03 i'o
60 22 20 7 70 2 0
6' f 4-
2 /2
1838 6P3
4,, / 2000
<F,
* Adjust quantity according to set time requirements.
WORKING CONSISTENCY: Specifications:
Refer to Plant Testing Procedure No. 32.
Maximum
Minimum
Average
60 56
58
SETTING TIME: Specifications
Refer to Plant Testing Procedure No. 6 (slow set)
Maximum
Minimum
Average
110 mins. ^ ------ ^3% hours
70 mins. 2\ hours
90 mins. 3 hours
WORKING PROPERTIES: Specifications:
Refer to PlantTesting Procedure No. 33. Must be plastic and buttery working; free of grit or coarse particles.
BONDING PROPERTIES: Specifications:
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE: Specifications:
- Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ Denotes change in this reissue.
ED0:dek
'=
SGP 0018387
June 29, 1971 Supersedes Formula 993 Dated 2/27/70
ACME, TEXAS PLANT FORMULA
SPEED SET JOINT COMPOUND (YELLOW) TEX-993 (60 minute and 2 hour working cement)
DESCRIPTION OF PRODUCT:
- For use in reinforcing and conceiling joints and nailheads.
/ FORMULA;
Raw Material Yellow Oxide
Function Pigment
R. M. Spec. 138
*Sodium Citrate Natrosol 250HXR
Retarder Thickner
134 170
Gelvatol RS-6278C
Adhesive
162
Gelva GP702 Asbes tos SG210 Asbestos 7RF09
Adhesive
Fiber Filler Fiber Filler
167 -
9
Mica p80H
Anti-Cracking Agent 11
Defoamer Mill
Anti-Foaming Agent 196
Vanicide TEX-38
Fungicide Plaster
126 -
^Adjust quantity according to set time requirements.
Percent 0.20 0.10 0.20 2.25 0.50 0.50 2.25 4.00 0.05 0.05 89.90
100.00
Lbs/Batch 1.500 0.750 1.500 16.875 3.750 3.750 16.875 30.000 0.375 0.375
674.250 750.000
WORKING CONSISTENCY: Specifications
- Refer to Plant Testing Procedure No. 32.
Maximum
Minimum
Average
62 58
60
SETTING TIME: Specifications
- Refer to Plant Testing Procedure No. 6 (slow
Maximum
Minimum
Average
110 mins . 33 4- 3% hours
70 mins. 2\ hours
90 mins. 3 hours
WORKING PROPERTIES: Specifications
BONDING PROPERTIES: Specifications
Refer to Plant Testing Procedure No.33. Must be plastic and buttery working; free of grit or coarse particles
- Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE: Specifications
Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ Denotes change in this reissue.
EDO:dek
SGP 0018388
May 10, 1973 Formula TEX-993 NEW
ACME, TEXAS PLANT FORMULA SPEED SET JOINT COMPOUND WHITE TEX-993
(1 Hour Working Cement)
DESCRIPTION OF PRODUCT - For use in reinforcing and concealing joints and nailheads. To be supplied to Chicago plant only.
FORMULA
Raw Material
Function
RM Spec Percent Lbs/Batch
Natrosol
Water retention
170
.40 3.000
Vancide
Fungicide
126 .10 .750
)
Gelvatol 5000
Adhesive
162
1.50
11.250
Attagel 40
Bulking agent
8
4.50
33.750
Mica P80-H
Anti-cracking agent 11
8.00
60.000
Defoamer Mill
Anit-foaming agent
--
.10 .750
Denscal
Plaster
--
84.57
634.275
Potash (-100 mesh
k2so4)
Accelerat or
-- .75 5.625
Com. Retarder
Retarder
.08 .600
100.00
750.000
-vAdjust quantity according to set time requirements. Increase amounts for longer working formulas.
WORKING CONSISTENCY
- Refer to Plant Testing Procedure No. 32.
Specifications
Maximum 60
Minimum 55
Average 58
SETTING TIME Specifications
- Refer to Plant Testing Procedure No. 6 (slow set)
Minimum: 1-1/4 hr.
Maximum: 1-3/4 hr.
WORKING PROPERTIES Specifications
- Refer to Plant Testing Procedure No. 33. Must be plastic ana butcery wording; rree of grit or coarse particles.
BONDING PROPERTIES Specifications
- Refer to Plant Testing Procedure No 35. After compound has dried, tape shall delaminate when peeled back.
C^RACK RESISTANCE Specifications
- Refer to Plant Testing Procedure No. 37. There shall be no large fi&sure cracks in the wedge and very few, tf any, cracks ir. the thinner half of the wedge.
WNG:elz
7^>
/4 3
SGP 0018389
July 25, 1973 Supersedes TEX-993 Dated 5/10/73
ACME, TEXAS PLANT FORMULA SPEED SET JOINT COMPOUND WHITE TEX-993
(1 Hour Working Cement)
DESCRIPTION OF PRODUCT - For use in reinforcing and concealing joints and nailheads. To be supplied to Chicago plant only.
FORMULA
Raw Material
Function
RM Spec Percent Lbs/Batch
Natrosol Vancide Gelvatol 6000 Attagel 40 Mica P80-H Defoamer Mill Denscal Potash (-100 mesh
K2S04) * Com. Retarder
Water-retention Fungicide Adhesive Bulking agent Anti-cracLing agent Anit-foaming agent Plaster
170 126 162
8 11 ---
Accelerator Retarder
--
.40 .10 1.50 4.50 8.00 .10 84.59
.75 .06
3.000 .750
11.250 33.750 60.000
.750 634.425
5.625 .450 ;
100.00
750.000
^Adjust quantity according to set time requirements. Increase amounts for longer working formulas.
WORKING CONSISTENCY
Refer to Plant Testing Procedure No. 32.
Specifications
Maximum 60
Minimum 55
Average 58
SETTING TIME Specifications
Refer to Plant Testing Procedure No. 6 (slow set)
Minimum: 1-1/4 hr.
Maximum: 1-3/4 hr.
WORKING PROPERTIES Specifications
Refer to Plant Testing Procedure No. 33. Must be plastic and buttery working; rree of grit or coarse particles.
BONDING PROPERTIES Specifications
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specifications
- Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ denotes change WNG:elz
* 7^
9- */- 73
^4 /l -fT7
SGP 0018390
March 7, 1974
Supersedes TEX-993 Dated 7/25/73
ACME, TEXAS PLANT FORMULA SPEED SET JOINT COMPOUND WHITE TEX-993
(1 Hour Working Cement)
DESCRIPTION OF PRODUCT - For use in reinforcing and concealing joints and nailheads.
FORMULA Raw Material
Function
RM Spec Percent Lbs/Batch
Methocel 228 Vancide Gelvatol 6000 Attagel 40 Mica P80-H Defoamer Mill Denscal Potash (-100 mesh
K2S04) Com. Retarder T.P. Blend Talc
Water retention Fungicide Adhesive Bulking agent Anti-cracking agent Anit-foaming agent Plaster
170 .26 .62
8 11 --"
Accelerator Retarder Slip Agent
---
*Adjust quantity ac cording to set time requirements, for longer working formulas.
.20 .10 1.50
5.50 8.00
.10
78.79
1.500 .750
11.250
41.250 60.000
.750
590.925
.75 . .06
5.00
100.00
5.625 .450
37.500
750.000
Increase amounts
WORKING CONSISTENCY
- Refer to Plant Testing Procedure No. 32.
Specifications
Maximum 60
Minimum 55
Average 58
SETTING TIME Specifications
WORKING PROPERTIES Specifications-'
Refer to Plant Testirg Procedure No. 6 (slow set)
Minimum: 1-1/4 hr.
Maximum: 1-3/4 hr.
- Refer to Plant Testing Procedure No. 33. Must be plastic and buttery working; free of grit or coarse particles.
BONDING PROPERTIES Specifications
Refer to Plant Testing Procedure No. 35. After compound has dried, tape shall delaminate when peeled back.
CRACK RESISTANCE Specifications
- Refer to Plant Testing Procedure No. 37. There shall be no large fissure cracks in the wedge and very few, if any, cracks in the thinner half of the wedge.
-/ denotes change WNG:elz
SGP 0018391
SGP 0018380