Document gXwqg25GXv0wnKL87bLdr0OG
/& 01
CODE YE-698-D
Z-bLQ/l < DATE )
L&H18, _ IM
_________ /' 5527* LBS.
< LOT )
< EST WT )
PROCESSES ( ) YE-698-D <T)
APPROVEP'BYT , FWP 10/15/82 ,
CGMTYP JOB NAME: 01YE698DMT
ELEN
98, '----- --- (CODE)
(LOT)
(POUNDS)
EQUIP | HENT |
I
NAME: MOLYBDATE ORANGE
PREP 1
') +V*OBTAIN SODIUM SULFATE FOR S-13
I 2 CALCULATE i, SET ON BADGER METER E)R S-16
I (NITRIC ACID WEAK)
JUtjjt'Je?...%
(TT/OBTAIN SODIUM CHLORIDE FOR S-33
4-j^OBTAIN SODA ASH FOR S-37
JgT\ OBTAIN SODIUM SILICATE FOR S-39 *
nV^OBTAIN SODA ASH FOR S-43
--TuBTAIN ANTIMONY TRIOXIDE FOR S-46
USE LBS
84
m **^n:0rSU* 734 146 237 350 70
1 ACCT N-CODE 1 LBS
1 08-A ! 84
33-D 1 6 4-A 1 734 3-A 1 146
32-P ! 237 3-A 1 350
711-B j 7
351 I
WEIGH SODIUM CHROMATE INTO V-351.
| OPTR_____ , MKlj^i,
I
OPTR
MK ,
'/I&7. / _____%
10-D 1 1885
359 1 VTWEIGH IN SODIUM MOLYBDATE ^LOTION
3I t
. OPTR:_____, m &K, T-&V&,
Il
L.OPTR _____, MK _____ T-____ ,
423-D
302
358 RRUN 10* <50 G) WATER INTO V-358 4 iKLL'RUN V-359 INTO V-351 6 PUMP IN V-351
ADJ TO 55* (2600 G)
:IFT IN N-10B-A FROM S 1
TR 5 MIN & RECORD: PH__/A$L<9.0-1 0*0)
ADJ TO PH 9.8-9,9 6 RECORD: PH_Z7-
<CAUSTIC SODA SOLUTION)
ASSUME 50% ASSUME 66% 1CZ
D N-33-D FROM S 2 USING BADGER METER
ADJ^TO 66" <3121 G) AT 67-69*F
RECORD: VOL&.(?_" 6 _J_7*'
| STIR 5 H*N 6. RECORD : Fh 4Z&<?:.4-?*6) &
I G/ML /UP-SuSli 1 *080-1 *083)
I NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
LIST & ATTACH. TAKE 1 QT SAMPLE
7-D 33-D
31
RUN 2* <996 G) WATER INTO V~*_JkXT RECORD N-41-D STORAGE TANK TO PUMP FROM. l *`-` CIRCLE ONE: 42 41 411 420 424 425 20. CHECK WITH CU SUPV: i WSTORAGE TANK MUST CONTAIN AT LEAST 2376 | GAL: 402=49", 410=25", 411=48", 420=25",
i 424=25*, 425=31" I ^STORAGE TANK MUST HAVE STIRRED AT LEAST I 2 MIN SINCE LAST ADDITION OR ADJUSTMENT I . ^STORAGE TANK MUST BE ISOLATED UNTIL ALL y PUMPING FOR THIS BATCH IS COMPLETE
2T I SET METER FOR 300 G 6 PUMP TO SV
**
LOT*: . EQUIP MEN! |
SV 122 c In t
I
I 123 I
f
124 I
CQMTYP JOB NAME: 01YE698DMT
PAGE 2 '
DATE PRINTED:1/I 5/62.
USE N- ACCT LBS CODE LBS
AT APPROX 100 G WHILE CONTINUING TO PUMp T CHECK PH & DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING & SEE SUPV.
* PH:_____ (2.2-3.7)
* DENSITY: _________C/ML <1.270-1.328) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
DENSITY _______ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21. CIRCLE DENSITY & SETTING IN TABLE BELOW.
**** TABLE #**
1 1 G/ML SETTING 1 G/ML SETTING 1 G/ML SETTING 1
! 1 1.270 1 673 1 1.291 1534 | 1 .312 1410 |
1 | 1.271 1670 1 1 .292 1527 | 1.313 1404 |
i i 1 .272 1 663 1 1.293 1521
| 1 .314 139? |
i i 1.273 1 656 1 1.294 1515 | 1 .315 1394 |
i i 1.274 1649 1 1 .295 150? | 1 .316 1388 i
i i 1 .275 1641 1 1.296 1503 | 1 .317 1383 |
i i 1 .276 1634 1 1 .297 1497 | 1.318 1378 |
i i 1.277 1627 1 1.298 1490 | 1 .319 1372 1
! 1 1 .278 1620 1 1 .299 . 1484 J 1 .320 1367 |
1 1 1 .27? 1614 I 1 .300 1478 f 1.321 1362 |
1 i 1 .280 1607 J 1 .301 1473 | 1 i 322 1357 |
i i 1 .231 1 600 1 1.302 1467 | 1 .323 1351 i
i i 1 .282 1 593 1 1 .303 1461 | 1 .324 1346 |
i i 1 .283 1 586 1 1 .304 1455 1 1 .325 1341 |
i i 1.234 1580 1 1 .305 1449 | 1.326 1336 |
i i 1 .285 1573 1 1 .306 1444 | 1.327 1331 i
i i 1 .286 1566 1 1 .307 1438 | 1 .328 1326 |
i i 1 .286 1566 t 1 .307 1438 I 1 .328 1326 |
1 ! 1 .287 1559 1 1.308 1432 1 1 .329 1543 |
1 1 1.288 1553 1 1 .30? 1427 I 1 .330 1537 I
! 1 1 .28? 1 546
1 1 .310 1421
| 1 .331
1532 J
1 I 1 .290 154 1 1 .311 1415 1 1 .332 1526 |
125
126 I 127 I 28
129 I 1301
SET METER 4, PUMP_______G (RECORD FROM TABLE)
|
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY |
30 SECONDS
|
ADJ LEAD NITRATE TO 76' (3625 G) AT 67-69*F.
|
RECORD:____ ______,F
|
STIR 5 MIN 6 RECORD PH: ___ _ (2.2-3.7)
|
IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 667. |
6 RECORD PH: ____ ASSUME 50% |
NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING 1
RECORD: _______ G/ML (1.143-1.144) IF OUT OF SPEC!
FILL OUT CHECK LIST & ATTACH.
.
|
STIR AT 67-69KF FOR S-31 . TAKE 1 GJT SAMPLE.
|
41-D 57-A
33-D 7-D
I I 5110 |____
I |______ |___ _
I
|
* DUP050059967
Hfesuip'
. i4%^u,;'
COMTYP JOB NAME: 01YE698DMT
. ;. ` 7^S'
- ';
PAGE 02
P fTEsiRIfEii10fl6f2
I LBS | CODE i LBS
AT APPROX 100-G WHILE CONTINUING TO PUMP, CHECK PH 6 DENSITY. RECORD BELOW. IF NOT RANGE, STOP PUMPING G SEE SUPV.
l_----- ----I____;____I____ '
I 1,1
Ii
I
>-&*. <2.2-3.7) '
* DENSITY: }3&P G/ML <1^27-0-1 .328)
IF S-22 OK G WHEN S-21 COMPLETE, RECORD
DENSITY
G/ML ON TRAPPED SAMPLE
M END OF S-21 PUMPING,. >
USING DENSITY FROM S-23, FINDiMETER SETTING FOR
SECOND PUMPING IN TABLE BELOW.- NOTE: TABLE
ACCOUNTS FOR 30 G ALREADY PUMPED IN S-21.
CIRCLE DENSITY & SETTING IN TABLE BELOW.
***# TABLE ***
[' T': - :v ' -
1 1 G/ML 1 I 1.270 111.271 1 I 1.272
1 11.273 1- 1 1.274
1 11.275 1 | 1.276 1 1 1.277 1 | 1.278 1 |1.279 ! I 1.280 1 J 1.281 I 11.282 | 11.283
I 11.284 1 11.285
1 11.286 I 11.287 I |1.288 1 |1.289
1 11.290
SETTING ,| G/ML SETTING I G/ML
1644 1 1.291 1504 1 1.312
1637 1 1.292 1487 1 1.313
1630 | 1.293 1491 1 1.314
1623 ! 1.294 1485 1 1.315
1616 I 1.295 1479 1 1.316
1609 I 1.296 1473 1 1,317
1602 I 1.297 1467 I 1.318
1595 1 1.298 1461 1 1.319
1588 1582
1575
1 L455 1 1.320 in .300 "'"'T44lh I 1.321 tSTarsr*' 1444 1 1.322
1568 1 1.302 1438 1 1.323
1562 1 1 .303 1432 1 1.324
1555 1 1.304 1426 1 1..325
1549 1 1.305 1420 I 1.326
1542 1 1.306 1416 1 1-.327
1535 1 1.307 1410 1 1.328
1528 I 1.308 1 404 1 1.329
1522 i 1.309 1399 1 1.330
1515 1 1.310 1393 I 1.331
1510 I 1.311 1387 I 1,332
SETTING 1 1382 1 1376 1 1371 i
1367 1 1361 J
1356 1 1351 1 1345 | 1340 j 1335 | 1330 | 1324 1 1319 j 1315 |
1310 1 1305 1 1300 1
1295 1 1290 1 1285 1 1280 |
11 1J 11 11 11 11
1. 1 I1 1I
1I 11 11 11 11
11
11 1I 11
I1 11 11
11
2SPTSET METER G PUMP
(RECORD FROM TABLE)
|
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY |
SECONDS
j
ADJ LEAD NITRATE TO 3625 G (76"-242/245 G 74.5" I
247) AT 67r69F
|
^RECORD:___ Lpjf_._*-F G ICE CONSUMED (3304/BL.OCK) | 330&Z
' STIR 5 MIN G RECORD PH:
<0 (2.2-3.7)
j
1|
USE TITRIMETER TO ADJUST N-41-D PH *#*#
|
1 'Ml IF NECESSARY APJ JE41 PH 3.0-3.1
ASSUME 66% 1
RECORD PH:
ASSUME 50% I
Tt E; DILUTE/N-7-D 10:1 WITH WATER BEFORE ADDING]
129"T RECORD: MMJL- G/ML (1 .143-1.144) IF OUT OF SPEC I
| i JPILL OUT CHECK LIST G ATTACH.
I
J 30 KJfTlR AT 67-69F FOR S-31 . TAKE 1 QT SAMPLE.
!
L-
\V *
DUP050059968
LOT: . EQUIP MENTI
CQMTYP JOB NAME: 01YE698DMT PAGE 03
DATE PRINTED: 10415/82 I USE | N- IACCT I LBS | CODE | LBS
II
I
1,23 I
I3KT
OBTAIN 1 QT SAMPLES OF S-18 & S-30 SOLUTIONS 6 TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
7*1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0.1O ML N-10-D (IF YES, FLUSH ALL'*'--T
`K
EQUIPMENT S REPEAT TITRATIONS) * DO NOT f oS, P >c / JJ
PROCEED IF N-10-D TITRATION IS OUT OF RaWg F---
ADJUST V-358 FOR A TITRATION PH OF 2TfrQ- TB 2*20)
FROM FINAL IN-LINE TITRATION, RECORD LOWEST
I ~7jf~
PH St ML N-1S-D
2b=-&&t \
WHEN S-31 TITRATION OK , STRIKE V-358 THRU
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN
si A
^
RECORD: START
TOTAL MIN />T___
INTUOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
BUBBLES APPEAR IN SIGHT GLASSES
iIMMi EDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
15 MINUTES
RING S 33, WASH IN V-358
STTIR 2 MIN G RECORD PH_._fli.6L_< 1 .8-2*5)
F'BXS, 4* (MUST BE + )
STIR TOTAL^OF 15 MIN FROM S-33 &
______I.
RECORD: TEMP_.2/.__*F (67~73*F) N-3-A. FROM S-4
3 M IN IN N-32-D FROM S-5
2 MIN
IN LIQUID ALUM USING BADGER METER
3 MIN 6 FLUSH ALUM LINE WITH WATER
IN N-3 FROM S-6
STIR 4 MIN FOR S-48
'
734 115-DI
9
367
RUN IN HYDROCHLORIC ACID USING WEIGHT
CONTROL PANEL
MK .J___ >
MK ______ , __________7.
DUjjU'NG S-44 SIFT N-711-B FROM S-7 INTO V-390
WITH AGITATOR ON IN 1-2 MIN
STI&.1-2 MIN TO MILKY SOLUTION
28-D 28-D
105
WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
FCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
FOAM SUBSIDES*
IN BLANC FIXE N
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP'OF PAGE 1
. RECORD: CODE_________, LOT _
I^TL^flR 20 MIN,/
l^g^RECORD : PH,,,,4ftl?__ ( 5 * 8-6 * 0)
|3 I IF Jl&CESSARY, ADJ TO .PH 5*8-6 .0
ASSUME 50%
6 RECORD: PH-____________
ASSUME 66%
FLOOD TO 153" (7298 G) 6 STOP AGITATOR
128-AI 330
7-D)_____ 33-D |_____
STAR
FINISH
OPTR
DUP050059969