Document gE5Yn4yNRjxbxNn26NEZKwo2a
CC: W. D. Lawson, F&F, WMm. G. T.Vaala, F&F, Wilm. F. D. Chapman, F&F, Wilm. j. C. Richards, F&F, Wilm. J. A. Klacsmann, F&F, Wilm. P. 1. Poindexter, F&F, Wilm. 0. H. Bullitt, Jr., Laboratory P. J. Graham, Exp'l Sta. G. 1. Mulholland, Flint G. R. Maher, F&F, Wilm. A. B. Naselow, F&F, Wilm. 1. S. Baker, F&F, Wilm. A&l and Trade Sales
File: 3320
Marshall Laboratory July 21, 1969
J. O. GRAVES (23) DIRECTOR OF PRODUCTION F. & F., WILMINGTON
ft l C j- ; v r r,
C. W. THEOBALD DIRECTOR OF RESEARCH DIVISION F. & F. , WILMINGTON
I96S
. lil& fli
R. N. SANGER (4) TRADE SALES MANAGER F. & F. , WILMINGTON
MARSHALL DEVELOPMENT LABORATORY SUPPLEMENTARY RELEASE LETTER NO. 2149-A COMMERCIALIZATION OF CUSTOM COLOR SYSTEM BASED ON BENNETT'S DECORATOR COLORANTS
RELATED RELEASE LETTERS: R. L. #2149, 2149-B, 2149-C .
\.
........---- -
h i--.............................
........... ..............
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...
PROPOSAL AND EXTENT OF RELEASE:
This letter proposes manufacture and national sale by Consumer Paint of Lucite Custom Color Wall Paint light and deep tint bases. The proposed formulations are based on HG acrylic latex (RC-11008) and utilize colorants manufactured by Bennett's.
This is part of a series of proposals that will update our Custom Color system. Companion proposals on "Lucite" Custom Color Interior Enamel and on 639 Line Alkyd Custom Color Paints will complete the program.
This release is being written at the request of Marketing in advance of completion of laboratory and alignment programs to provide lead time for marketing plans and is subject to satisfactory completion of these programs.
-2 -
MANAGEMENT DECISION REQUESTED:
Management should consider the fol lowing points in making a decision on this proposal:,
1) The adoption of this proposal will update our Custom Color System both technically and commercially.
2) The formulas proposed in this release are designed for use with Bennett's colorants. Adoption of this proposal will obsolete existing white base paints.
3) Durability, application properties, manufacturing reproducibility, and stability experience with the proposed formulations is limited.
4) The proposed deep base formulation has been difficult to adjust and control for tinting strength because of low TiC)2 level.
5) The proposed formulations represent a major quality change for "Lucite" CC Wall Paint. This change will update.the Custom Color Wall Paint to the quality of present 392-401 quality.
6) Testing and Control Procedures have been revised to improve testing reproducibility but have not been completely validated.
7) The proposed formulations are deficient in that some colorants can be washed from the surface of the tinted paints even after several days drying. However, no apparent change in the paint surface is observed after washing.
TECHNICAL OPINION:
The Laboratory recommends approval. An adequate background with respect to durability, application properties, and stability is considered essential for any major consumer paint line. In this case, our background is less than that previously considered adequate. However, the background that has been developed on the light base has been acceptable.
The risk associated with the light base is reasonable to assume because the formulation closely resembles current quality "Lucite" Wall Paint. The proposed deep base formulation involves a relatively higher risk since we have,little experience with this type of formulation. The poor tinting strength precision identified earlier also increases the risk with respect to color matching ability.
We feel that these products are improvements over the current "Lucite" Custom Color Wall Paints. The Technical Concept is sound and we believe this proposal presents only moderate risk.
PRODUCT DESCRIPTION:
The proposed bases are updated versions of 392-091 and 392-092 Custom Color Wall Paints. The formulations combine the technology of 392-401 "Lucite" Wall Paint with some of the formulating changes incorporated into the 392-601 paint proposed in R. L. No. 2165.
DUP030022766
-3
Color and Hiding:
The color and hiding of the proposed formulations matches the color and hidingJF'siayiBd<3r.ds;sapRl!ediby; Bennett's. These formulations will match the color chips of the Bennett color system when properly tinted.
Stability:
Package stability in terms of viscosity and package conditions is limited to four weeks on proposed formulations and has been satisfactory.
Tinting strength stability has been satisfactory for the proposed light base. Stability of the deep base is also satisfactory.
Competitive Situation:
The proposed "Lucite" CC bases are considered equal to competition in color matching to standard chips.
TABULATION OF COMPOSITION:
*
The composition of the proposed light base is shown next to the current and proposed shelf qualifies in Table I. Table ILcompares the light base with the deep base.
DUP030022767
-4 -
Code
Ingredient
392-401
RC-11008
Acrylic Latex, 46% Solids 1.796
<5-1117
Hydrocarbon Emulsion
1.113
50% Solids
W-1012
MontmorilIonite Clay
.099
W-1014
w-ion
Calcined Clay
.314
Calcined Diatomaceous Silica .642
W-90
Calcium Carbonate, Whiting .615
W-1008
Aluminum Silicate
-
W-192
Fine Extender, Zeolex 80
.089
W-129/W- 199 Titanium Dioxide
2,269
Ti Pure2 R-901/TiPure"R-992
KW-8714
Titanium Dioxide, "TI Pure" -
R-931
G-l111
Methylcellulose, Thickener, .028
4000 cps.
G-21
Thickener L, Thickener
-
G-l 95
Solium Polyacrylate
.001
H "632
Odorless Mineral Spirits
.120
H-658
Deofamer, Polyglycol P--1200 .034
H-609
Non-ionic Surfactant, 99% .042
H-657
Anionic Dispersant, 25%
,061
H-454 G-796
Phenyl mercury Oleate, 10% .030 Phenylmercury Proprionate -
VM-5648
10% Pot. Pentachlorphenol
.121
Soln.
H-372
Reodorant
,003
H-514
Ethylene Glycol
.415
H-506
Water
3.155
G-782
Defoamer
.020
H-284
Ammonia, 28%
.018
G-12
Soya Lecithin
.102
Shading Bases
Trace
392*445 Light Base
3.052 **
.097 .301 .614 .588
-
.117 1.74
392-601 2.080
Changes
0) 0)
.091 .281 .734 ,292 .296
-
(2)
(2) (2) (2) (2) (2)
-
.029
2,515 .011
(2)
m -
.117 ,030 .038 .054 .030 .121
.300
-
-
.018 .029 .117 ,002 -
(3)
(4) (4) (4)
(5) (5) (5)
-
.410 3.387
.005 .026 .091 Trace
-
.900 3.587
.020 .018 .102 Trace
(6) (7)
Gallon Weight Weight Solids % Volume Solids % Pigment Vo (urns %
11.087 50.5 34.0 45,0
10.80 46.99 31.31 43.87 .
11.400 47,6 29.0 55.0
DUP030022768
-5 -
Explanation of Changes; Table I
{
(1) Hydrocarbon emulsion dropped in order to upgrade film properties.
(2) These changes reflect the rebalancing of the pigmentation to achieve a match for color and tint strength to the Bennett Standard,
(3) Polyacrylate thickener, which causes rapid recovery of the gel structure, not required since this property is no longer desired.
(4) Surfactants and dispersants rebalanced.
(5) Fungicides used for can preservation believed adequate. G-769 replacing H-454 on equal mercury level due to its greater safety in handling,
(6) Reodorant being dropped since it is believed that the odor level of all acrylic system is acceptable without any masking agents.
(7) Difference in quantities of water in each formulation reflects the volume of solid differences.
(8) G-782 level lowered to improve color compatability.
"'D
DUP030022769
-6
TABLE II
Code
Description
392-445 Proposed Light Base
392-446 Proposed Deep Base
RC-11008 Acrylic Latex, 46% Solids 3.052
2.869
W-1012 MontmorilIonite Clay
.097
.095
W-1014
w-ion
Calcined Clay
.301
Calcined Diatomaceous Silica .641
.351 .701
W-90
Calcium Carbonate, Whiting .588
1.051
W-192
Fine Extender, Zeoiex 80
.117
W-129
Titanium Dioxide
1.74
.587
H-454
Phenylmercury Oleate
.030
... .. mm-. .
G-796
Phenylmercury Proprionate
---
.002
VM-5648 10% Pot. Pentachlorphenol Soln.
.121
MMMMi
G-1111 B-632
Methylcellulose, Thickener 4000 cps
Odorless Mineral Spirits
.029 .117
.042 ,118
H-658
Defoamer, Polyglycol P-1200 . 03^
.034
H-609
Non-ionic Surfactant, 99% .038
.042
H-657
Anionic Dispersant, 25%
.054
.062
H-514
Ethylene Glycol
.410
.427
H-506
Water
3.337
3.699
G-782
Defoamer
.005
.005
G-12
Soya Lecithin
.091 .103
H-284
Ammonia, 28%
.026
.030
Shading Bases
Trace
Trace
Gallon Weight Weight Solids Volume Solids Pigment Volume Concentration
10.80 46.99% 31.31% 43.87
10.22 42.76% 29.78% 41.14
Changes 0)
(2) (2) (2) (2) (3) (3) (3) (3)
(4)
(5) (5) (5)
(5)
DU P030022770
-7-
Explanation of Changes: Table II
(1) This change results i,n lower volume solids. (2) Pigmentation isrebalanced to match tint strength of Bennett's standard.
(3) H-454/VM-5648 used in light base because of effects on dispersion. (4) G-l111 increased to maintain viscosity at lower volume solids. m Surfactant levels rebalanced.
REPRODUCIBILITY:
Reproducibility of the proposed formulations has not been established. One hundred gallons of a light base prototype was successfully completed. Scale up of 100 gallons prototype deep base was unsuccessful because of adjustment problems.
Formulations of the current light base have been made in the laboratory with no difficulty. We do not expect unusual scale up problems with this base.
Formulations of the current deep base have also been made in the laboratory. Tinting strength testing of this formula has not been as precise as previously considered necessary.
CONTINUING LABORATORY WORK:
The laboratory will establish stability of the bases manufactured in scale up batches and will be responsible for development of instrumental shading techniques.
A new Test Method will be written outlining procedures for testing tinting strength of Custom Color bases ( TM-71-S).
Preferred testing and adjusting procedures will be developed in cooperation with Plants Technical.
COST INFORMATION:
The bulk mill costs of the proposed formulations are listed together with the costs of the old system and that of "Lucite" Wall Paint Systems. These costs are unofficial and are provided for guidance only.
392-091 "Lucite" CC Light Base ( Present ) 392-445 "Lucite" CC Light Base ( Proposed ) 392-401 "Lucite" Wall Paint ( Present ) 392-601 "Lucite" Wall Paint ( Proposed R.L. 2165 ) 392-092 "Lucite" CC Deep Base ( Present ) 392-446 "Lucite" CC Deep Base ( Proposed )
$1.60 15/16 gal. 1.44 15/16 gal. 1.63 gal. 1.72 gal. 1.17 7/8 gal . 1.03 7/8 gal.
MANUFACTURING PROBLEMS:
The 392-446 Deep Base has been revised to eliminate adjustment and control problems. However, alignment of this material is not complete and further revision may be necessary. Control limits for tinting strength of the base may be revised.
No material representing the present quality Light Base has been manufactured. We do not expect the present quality to act different than the prototype so no problems are anticipated.
DUP030022771
8- -
NEW OR UNUSUAL TOXICITY OR OTHER HAZARDS: There are no known unusual toxicity hazards involved in this release.
All materials have been classified with respect to handling hazards.
LABEL INFORMATION; Label analysis will be required for all of the proposed white base paints.
The;mercury present in these paints is below the .06% level that requires a hazardous, warning label . Label directions and cautions should be the same as the current quality. Information for calculation of label analysis will be forwarded to Plants Technical when formulas are scaled up.
Three of Bennett's colorants contain lead pigments. Paints using these paig.me.nts will require a warning label as required by local ordinance or when the permissible level as defined by U.S.A. Standards Institute Z 66.1 is exceeded.
SIMPLIFICATION; Approval of this release will favorably affect simplification. G~1117
Hydrocarbon Emulsion has been eliminated in conforming to 392-601 formulating changes. In addition, ingredients used only in 392-091 and 392*-092"paints will be obsoleted.
PATENT INFORMATION; There are no known patents which conflict with the manufacture and sale
of the proposed latex wall paint formulations identified as 392-601, 392-445 and 392-446, the latter two a light base and deep base, respectively, for coloring with Bennett's colorants. Each of the paints are formulated with the non-iminated acrylic latex HG designated RC-11008. The carboxyl equivalent of the HG polymer is within the claimed teaching of the licensed Rohm & Haas U.S.P. 2,795,564 and consequently this HG latex is subject to royalty payment. Substitution of an iminated latex will require definition of the patent status, although no patent conflict is currently recognized in such a substitution.
CONFIDENTIAL INFORMATION; The information contained in this letter should be considered "For Du Pont
Use Only."
FORMULA CARDS; Formula cards for the 392-445 and 392-446 paints together with the 548-992
and 548-993 dispersions proposed in this release are attached to the Production and Research copies of this Release.
CONFORMANCE TO AIR POLLUTION CONTROL DIRECTIVE; These paints conform to APCD.
DUP030022772
CTR/smw
-9MARSHALL DEVELOPMENT LABORATORY
CHARLES T. RIVEN BURGH "
DATE_ DATE
DUP030022773
Ip! frit ?<v?J
. 0 i 0 USS ` 4 f&U
392 ! **w \ **. p'tuc
TRADE SALES INTERMEDIATE
CT RIVENBURGH/CLH
:
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1YM TEKP
! R.L..L 2149-A
s t XT2 1
jte44D.|WlLM TRADfc j Cote* f WHI Tt {,'b.&p.[ 9413-8^
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'392-H-8384 T--6-3-69
%Cesr. fP
---- T.C.CB7. ?
-Of- B.F,1 ASSIGN PfcRM COOC TO 392-H-8384
1 tuw |PHILA-DL 1tm JCWS-RFC
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30? I TINT SIR. STD, TM~7l~S
Qu al STO. 392--OOI-P
|c_Sm| s e e TESTING
3 X -D <; 392-445 s G W X 42.6 = GMS
H"T T F PILOT COLORANT F * 21.6
TiT)
USE 2~X0U~7 FOR STANDARDIZING COLORIMETER. USE
TJ1i'4ll
s t a n d a r d s s u p p l ie d b y l a b o r a t o r y , .a l l s h a d in g h it s t o b e DETERMINED BY COS
42C VOL S3l TT575 '
TFT c o mpu t er
P:r o g',"r'1ammed n 1
If s .v m.1 43.10%
M323L a
NOT TO BE USED FOR OTHER THAN EXPERIMENTAL RELEASE LETTER IS APPROVED //
TI
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1 [cSHTTrSw PURPOSES UNTIL
$2-9 ! Ge
JWl ~TXS 1 feUE "LUCITEO CC LIGHT BASE
| tan |
2 30 Pat Kw
| 89-92 KU
\ ftxt
231 CSST
637 VST
1
634 &
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WATER 8 i.SE PiilNT ORDER OF ADDITION
AVOID Ut INECESSART CONTAMINATION, DO NOT AGITATE iASES; AND VM-5751 BEFORE USING,
3041 53
TJ7
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638
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53:34 ADD SlITHt IUT FREEFALL OR AGITATION
6.39 U MIX 5 .MINS,
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12-:07 ADO WHItl NIXING, MIX 15 MINS,
TXT
548 992
596:63
TXT
H
506
67-46
TXT
H
514
30:82
TXT
H
284 ss
0:97
647 STS'1
USE H 306 TO h
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649 T C Ml X i 5 MINS 6Ei ORE ADDII 0
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00 NpTJ OSMP. MIX HR.:AFrtR EACH ADD. "Y" ADJUST PH
S k i TH IH'284 I REQUIRED //
-4-
TOTAL
1078:00
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N42517.01
DUP030022774
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V;"5 tai) .OSS
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COLOA WILM TRADE
< P03M C-T RIVEW8URGH/CLH
R.L.-1 2149A
9413-28
r 0 - ffcviwa C T RIVEN8URGH/CLH 'Oo Rrw4 392 -H-8386 T~6~3~69~P
iJDST. FP rtter p.
Pl ast PHILA AH*. CWS-tPG
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I t in t STRENGTH STD 'TM--71-5
j iT ff 392-446 * G H X 39.8 GMS-
nl r r PILOT COLORANT P = 21,6 GMS.
ur E 0 USf 2-XOOI-7 FOR STANDARDIZING COLORIMETER. USE STANDARDS
H3jS R SUPPLIED 8V LABORATORY. ALL SHADING HITS TO EE DETERMINED
)I 7 1 b y cos n
ST -G 2
0
fi;
4 20 Vet. SUL 29.78%
521 COMPUTER PROGRAMMED //
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NOT TO BE USED FOR OTHER
>2 3. T i RELEASE 1$ APPROVED //
CHI
H
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--1 ft 0.
THAN
41.14 % ! EXPERIMENTAL
Wr.SM. 4276% PURPOSES UNTIL
WTfe^l,,tUC;T1 CC PEEP BASS. wt | 88-92 H.U C*U. WT jfljgg
ORDER OP ADD I TION MOST AH[NATION, DO NOT USE k BEFORE USING.
CHS ) 7&7&f
ADO WITHOUT FREEFALt OR AGITATION.
ADD *FIL< MIRING. MIX 15 WINS,
MIXING. MIX .30 MINS. mr WITHHOLD ANY H-.506
sjJJ !
fa O'* tj;. /. fa n t > [
- - . . -.....J t J --V ---..... :------ 4-ADD -8fH 11 i mTx Tn G, *00 NOT USE
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di F LOW Aco dip TO: 5 LfS./lGO GAL, VH-5751 AT FOR EACH l, XU fISC RISE NEEDED. "X" IE
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324 H ti NOT TO BE USED FOR OTHER THAN EXPERIMENTAL PURPOSES UNTIL
325
RELEASE LETTER IS USED //
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WELL 8 EEQRE US IN I. RINSE TANK WITH LETDOWN HATER. IF BATCH
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100:00
|
DUP030022776
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JT10N: TH? 5 IS FOR 4ATEft PAINT. ORDER OF
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]
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