Document g267MXMo7QbdD6KjRLJDLegYQ

I MICROBIAL INHIBITION (DEHYDROGENASE ACTIVITY TEST) TEST SUBSTANCE Identity:A mixturecontainingperfluorooctanesulfonawthei,ch may alsobe referretdoas PFOS, FC-95,oras a component ofFC-203. (IOctanesulfoniaccid)(CAS # 27!95-39-3). Remarks: The 3M productionlotnumber was notnoted.The testsample isFC-203. Currentinformatioinndicateistisa mixtureof 1.34% PFOS, 35% diethyleneglycolbutylether,37.85% water,20% ethyleneglycol,2.66 % Sultonefoamer,3% sodium octylsulfate0,.1% sodium laurylsulfatea,nd 0.05% tolyltriazole. The followingsummary appliesto a mixture with incompletely characterizedconcentrationsof impurities.Data may not accurately reflectinhibitionby the fluorochemkat component of the testsample. METHOD: Method: Not noted. GLP: No Year completed: 1973-1974 Analyticalmonitoring:% Transmittance Statisticamlethods: Resultswere determinedby calculationfthe% transmittanceand comparison withthe blank. Test organism source: Not given Contact time: Not given. RESULTS Nominal concentrations: Blank control0,.01,0.1,0.5,1,5,and 10% conc. Element values: Not given. CONCLUSIONS No conclusionsgiven. Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St. Paul,Minnesota,55133 DATA QUALITY ReliabilityK:limischranking= 3. Study lacksdescriptioannd recordsof the method followed.Sample puritywas notpropedycharacterizeadnd the study lacksanalyticaclonfirmatioonftheamount offluorochemicaplroportioninthe solution. REFERENCES The studieswere conductedby the3M Company, EnvironmentalLaboratory, St.Paul,MN, Lab Request Numbers 2034, 2036,2093,1973-1974. OTHER Last changed: 6/27/00 FORM 10620-PWO cc: LAB REQUEST BOOK - 42-5W Water and Wastewater REQUEST FOR LABORATORY WORK TO: ENVIRONMENTAL ENGINEERING LABORATORY- File: LabRequestNo.BUILDING 53-6N Requestor Lab Personnel Name: DOLIP- 30-CC'A Request Date P1.0jectNo.-?;-45740Prob.No. 08 Code# Description..Fc---2o"S + L -32 -f3 Sample Date: Date Needed: HoldSampleFor_Days EstT.ime:- Hrs Date Rec'd.Sam le: Analyst: y v, R Date Completed: Hrs.Spent: Sample Description Total Hardness,mg/i as CaC03 Calcium Hardness,mg/i as CaC03 "P" Alkalinitym,g/i asCaC03 "M" Alkalinity,mg/i as CaC03 PH Sulfate,mg/l as S04 Nitrate,mg/i as N03 ifh-loridem,g/i as Cl Silica,mg/l as Si02 Fluoride, mgll as F brtho Phosphate, mg/l as P Total Phosphate, mg/i as P Total Chromium, mg/i as Cr @ex. Chromium, mg/l as Cr Total Cyanide, mg/i as CN Ferrocyanide, mg/l as CN iron, mg/i as Fe -Manganese, mg/i as Mn Surfactant, mg/l as LAS Thenol, mg/l BOD, mg/l ZOD, mg/l (Short, Long, Dilute) Total Suspended Solids,mg/l Mt)( VolatileSuspended Solids, mg/l"' Turbidity, mg/i Silica Total Solids,mg/l Total Volatile Solids,mg/i Conductivity, mhos Total Bacteria,No./100 mi Total Coliform, No./100 ml Tecal Coliform, No./100 mi Fecal Streptococcus, No./100 mi Ammonia Nitrogen, mg/l as N Tjedldahl Nitrogen, mg/i as N Oil and Grease, mg/l T T-C Comments: p7C -2 03 L;,rAutw- 640 1 7b Tr a R! vtc P. 16i1'rt1 ,4 71 A Of. 0.1% clot7le 93 71 64.5 L-3243 1 % Tr 70 71 75 16to tpq it-041%te White - Environmental Engrg. Lab Conar Environmental Engrg. Lab Pink Environmental Engrg. Lab Goldenrod - Requesters CopV F(@lim 10620-PVVO cc: LAB REQUEST BOOK - 42-5W Water and Wastewater REQUEST FOR LABORATORY WORK File: LabRequNeo.st TO: ENVIRONMENTAL ENGINEERING LABORATORY- BUILDING 53-6N Requestor Name: . 1'r.uject 7 Description: "-J Request Prob.No. !@@ te Code SampleDate:- DateNeeded: HoldSampleFor_Days EstT.ime: Sample Description TotalHardness,mg/ias CaCO3 Calcium Hardness,mg/i as CaC03 "P" Alkalinity, mg/i asCaCO3 "M" Alkalinitmyg,/iasCaC03 pH Sulfate,mg/i asS 4 Nitrate,mg/i asN03 Chloride,mg/iasCi SilicaM,g/lasSi02 Fluoridem,g/l asF Ortho Phosphate,m()'/@a[asPP@, TotalPhosphate,mg/las P ToialChromium, m!j/alsCr Hex.Chrom-i-u-m-,-/mgI a-Csr TotalCyanide,mg/iasCN Ferrocyanidem,g/i asCN Iron, Ias Fe n Surfactantm,g/las LAS Phenol,mg/l BOD, mg/i COD, mg/i(Short,Long,Dilute) TotalSuspended Solidsm,g/i VolatilSeuspended Solids,mg/i Turbiditym,g/iSilica TotalSolidsm,g/i TotalVolatilSeolidsm,g/l Conductivitym,hos TotalBacteriaN,o./loomi TotalColiform,No./100mi FecalColiform,No./100mi FecalS*LrePtococcuNso,./100 mi Ammonia Nitrogenm,g/lasN KiedldahlNitrogenm,g/ias N Oiland Grease,mg/i A cN d0 Hrs. 0 Lab Personnel Date Rec'd. Sample: '80 Analyst: I'1z0 y 11 Date Completed: Hrs.Spent: c -i jq Comments: 644 c Environmental Engrg.Lab Canor EnvironmentaElngrg.Lab Pi-nk- EnvironmentaElngrg.Lab Goldenrod RequesterCso3py.rC-aqrtmminPianper PRODLXT ECOLOCilCAL ASSESSMENT L.6. tt,. tS REQUEST FOR UKDORATORY WMK RE@UESTOR LABMTORY 1FC -z-03 I- (Fc-zP(/ NAmr-.: REOUEST DATE. F'RA)ECT 140.: CODE NO.: SAMPI-E DARF.: DATE NEEDLO: PROS. NO.: DATE RECE IVF.D SAMP LE: Z -z 1 4- AHALYST: DATE COWLETED: HOURS SPW: 15kw Di@SC@IFTION: PURPOSE OF TTSTS: BIOASSAY Freshwater.F@lsh': @larine Fish,.., isms Aquatic Plants l.ar-dPlan@us birds. Mammals LEACMBILIT"Y Parent Material PH COD mg/a BOD"M /a BOD, ultimate GC Bioassay Other Leachat6 PH COD mg/9 ROD BOD-, ultimate TOC Bioassa). Other PH)Sli.'AL1, PR("PERTIES -)f.,.t)mbuSLi,.c)-nal/g BTU/ Ib. A,;ii ro s Lvene.,;s w U'l,ION 'Ou Een Ul).Cue 0 rilt:i@ ';o itCC 16"IU, 'it! L)7', i!it c nce idat iun P o Rec N-cI.,iibI itv ty x -F-7 7- SAMPLE T .77%,.@- P" Ovk F(-- Eli,4P1(r'.j"TN-F'-I14TLA,FNGR. LAB File: Page N,). WORI(, SHEET Date: Ana 1 7t ' Hrs.' Ivy Lo 67 4 77. ?,?43 Fc -LO(a 7t. 10 74 2 -71" 2f ti -74, 5@ q 4ily 74. O-TZO <Q V s #1L, OOZ-71 Reviewed by: 5 12'0.@*tv SAM P'Lii: LlE S 1,1 Vr I CNVIRO@:t%L-'-%T,'%ELNGR. LAB File: Pz,,geNo. WORK Sf&,L-T D-ate: tl7q Aiialyst:__ Hrs. L6 16 34 -3(o 14 46' C 37 .37,S e--@. 74.?1 o4 @m7 Ok -M-o7m140 Reviexqed by: