Document evvVLO5eE4M0y2yLaYNagw4qE

Inspection Entry Date/Time Inspection Exit Date/Time Regulatory Program Type of Inspection EPA REGION 6 Enforcement Division INSPECTION REPORT 05/09/2024 1:00 PM (CT) 05/09/2024 4:00 PM (CT) RCRA Focused Compliance Inspection (FCI) Announced: No Access: Granted Facility or Site Name Facility/Site Identifier Facility/Site Physical Address City, State, Zip Code County/Borough Generator Status NAICS Type of Operation Geographic Coordinates Specialized Waste Services, Inc. TXD980870257 403 W Brentwood Channelview, TX 77530 Harris Very Small Quantity Generator (VSQG) 484110, 484220, 532412, 562991 Specialized Waste Systems, Inc. is a tank wash out facility. They are registered transporter and transfer facility for hazardous waste 29.7786, -95.14427 Additional Persons Participating in Inspection: Name Title Organization Dedriel Gardner Inspector EPA REGION 6 John Penland Inspector EPA REGION 6 Anshul Paripati Contractor Eastern Research Group (ERG) Email Gardner.Dedriel@epa.gov Penland.John@epa.gov Anshul.Paripati@erg.com Phone (281) 983-2133 (214) 665-9717 (571) 535-1503 Lead Inspector: Cameron Tanaka Cameron Tanaka Date: 2024.07.25 23:23:05 -04'00' Digitally signed by Cameron Tanaka ERG Cameron.Tanaka@erg.com 07/25/2024 (703) 633-1632 ext. 11632 Page 1 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 SECTION I - INTRODUCTION Site Entry and Purpose of the Inspection Type of inspection: Focused Compliance Inspection (FCI) The Port of Houston and surrounding facilities were selected for inspection based on an Environmental Justice and Regional initiative to evaluate facilities at ports receiving or transporting Resource Conservation and Recovery Act (RCRA)-regulated hazardous wastes, and/or have an International Convention for the Prevention of Pollution from Ships (MARPOL) Annex V Certificate of Adequacy (COA) issued by the U.S. Coast Guard (USCG). This report is based on information supplied by the facility representatives, inspector observations, port related facilities, and records including photographs taken (see Appendix 1), verbal or written statements made during or after the on-site inspection, and/or materials shown, demonstrated, or submitted to the EPA during or after the on-site inspection. In addition, information gathered prior to or after the inspection from a review of EPA, State, and public records may be included in this report. Attendees Title/Organization Lead Inspector/ Contractor/ERG RCRA Inspector/ Contractor/ERG Inspector/Enforcement Officer/EPA Region 6 Inspector/Enforcement Officer/EPA Region 6 Name Phone Email Opening Closing Conf. Conf. Cameron Tanaka (703) 633-1632 Cameron.Tanaka@erg.com N/A N/A ext. 11632 Anshul Paripati (571) 535-1503 Anshul.Paripati@erg.com N/A N/A Dedriel Gardner (281) 983-2133 Gardner.Dedriel@epa.gov N/A N/A John Penland (214) 665-9717 Penland.John@epa.gov N/A N/A Page 2 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 Facility General Description Tenant/Area Specialized Waste Systems, Inc. Inspection Date 05/09/24 Process Description Specialized Waste Systems, Inc. (SWS) is a tank wash out facility. They are registered transporter and transfer facility for hazardous waste. They operate their own trucks as transporters and their transfer area only keeps waste for 10 days. They also operate a wastewater treatment plant, but they bring their treated wastewater to Southwest Shipyard. SWS does not have a MARPOL COA. Area of Concern Yes Page 3 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 SECTION II - OBSERVATIONS Tenant: Specialized Waste Systems, Inc. Section: 2.1 Date: 05/09/24, 1:00 PM Contains AOC: Yes Contains CBI: No Lead Inspector: Cameron Tanaka Attendees: Nicole Rudolph (Tech Services Manager) and Sean Chavira (Waste Profiler) SWS is a subsidiary of TAS Environmental Services and acts as a tank washout facility for tankers, roll-offs, and bulk containers. The facility does not maintain a MARPOL COA but is registered with the USCG as a mobile transporter (see Appendix 8) and with EPA as a VSQG, transporter, and transfer facility (EPA ID TXD980870257). The facility operates its own trucks to pick up waste and to ensure that the containers being received are RCRA-empty. Ms. Rudolph stated that if a container is not RCRA empty, they will drum up the heel and send it back to the customer. The facility consists of a wastewater treatment plant (WWTP), a transfer area, and a roll-off area. Ms. Rudolph stated that the facility is extremely cautious about what material is allowed through their WWTP as the facility does not own a permit to discharge, but instead discharges through Southwest Shipyard. The facility representatives stated that the facility does not generate hazardous waste but does generate used oil and sends it to Select Environmental Mansfield, a used oil recycler. Ms. Rudolph also stated that the company has another facility on the Houston Ship Channel (EPA ID TXR000086206) that acts as another 10-day facility for overflow or if this facility's 10 days are up and the waste needs to be held longer prior to disposal. Observations and Areas of Concern (AOCs) are organized by section below along with facility responses where relevant. Transfer Area The inspection team first observed the transfer area, the process of the trucks dropping off containers for washout and the resulting sorting process. The transfer area contained roughly 100-200 drums and 50-100 boxes that had been delivered and were awaiting washout. There were no issues found by the inspection team. Roll-off Area The inspection team then observed the roll-off area which mostly holds the containers that have finished the washout process and are waiting to be delivered. During the time of the inspection, there were roughly 60 roll-offs in this area. While walking through the area, the inspection team observed a waste area, labeled CS 107, which contained drums and totes, many with unknown material. Upon further inspection, the drums and totes were found to be not RCRA-empty and, after questioning the facility representatives, it was determined that the facility was storing waste they did not generate or sign manifests for (see Appendix 1 - Photo 1-6). SWS may be receiving hazardous waste in the form of non-RCRA empty containers without a permit and/or accepting hazardous waste as a transporter from generators without a manifest. EPA will be conducting further follow up regarding these observations. The inspection team also observed universal waste batteries without proper labeling (see Appendix 1 - Photo 7) [AOC #1 - SWS did not label batteries being managed as universal waste properly - 40 CFR 273.14(a)]. In Ms. Rudolph's third follow-up email (see Appendix 4), she provided an explanation for the non-empty RCRA drums and documentation of corrective action for the universal waste batteries (see Appendix 5). In this follow-up email (see Appendix 4), Ms. Rudolph also provided verification of the material contained within the drums and totes (see Appendix 6). The inspection team did not observe any other AOCs at the time of the inspection. A closing conference was conducted at approximately 3:10 pm with SWS personnel. During the closing conference, the inspection team requested documents from SWS, which Ms. Rudolph provided as attachments to her three follow-up emails (see Appendix 2, Appendix 3, and Appendix 4). The requested documents and their associated appendices are Page 4 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 listed as follows: Their hazardous waste transfer manifests from April 2024 (see Appendix 7). A description of the contents of the containers with unknown materials (see Appendix 6). Confirmation of MARPOL COA status (see Appendix 8). Their incoming container inventory for the past three months (see Appendix 9). Documentation of accumulated heels of hazardous waste drums for the past six months (see Appendix 10). Manifests and documentation of hazardous waste going to their secondary transfer facility (see Appendix 11). Standard operating procedures (SOPs) for container and tank cleaning (see Appendix 12). The inspection team noted no issues with these documents. Page 5 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 SECTION III - RECORDS REVIEW No RCRA regulated records were reviewed during this focused onsite inspection. SECTION IV - APPARENT AREAS OF CONCERN The presentation of Area(s) of Concern does not constitute a formal compliance determination or violation. Tenant: Specialized Waste Systems, Inc. AOC #1 - SWS did not label batteries being managed Citation: 40 CFR 273.14(a) as universal waste properly. Section: 2.3 Page 6 of 8 Specialized Waste Systems, Inc. SECTION V - FOLLOW UP Inspection Date(s): 05/09/2024 Follow-Up Any facility follow-up items are as discussed in each facility's observations in Section II. Documents or files provided by the facilities were transmitted via email and included responses to AOCs or provision of documents requested. Communication Log During and after the inspection, additional information was emailed to EPA including: 1. 05/24/24 SWS email #1 - Nicole Rudolph sent an email hazardous waste transfer manifests from April 2024, clarification of their MARPOL COA, their washout container inventory for February through April 2024, and their SOPs for container tank cleaning. 2. 05/24/24 SWS email #2 - Nicole Rudolph sent an email providing documentation of hazardous waste going to their Miller Rd facility for February through April 2024. 3. 05/28/24 SWS email #3 - Nicole Rudolph sent an email providing verification regarding the drums of unknown material that were observed during the inspection, documentation of the accumulated heels of hazardous waste drums for the last six months, and an explanation regarding the AOC for receiving and managing nonempty RCRA containers without a permit. Page 7 of 8 Specialized Waste Systems, Inc. Inspection Date(s): 05/09/2024 SECTION VI - LIST OF APPENDICES Appendix 1. Photograph Log Appendix 2. Follow-Up Email #1 from SWS Appendix 3. Follow-Up Email #2 from SWS Appendix 4. Follow-Up Email #3 from SWS Appendix 5. SWS Corrective Action - Non RCRA Empty Containers and Universal Batteries Appendix 6. SWS Description of Contents of Containers with Unknown Materials Appendix 7. SWS Hazardous Waste Transfer Manifests from April 2024 Appendix 8. SWS Confirmation of MARPOL COA Status Appendix 9. SWS Washout Container Inventory Feb, Mar, Apr 2024 Appendix 10. SWS Documentation of Accumulated Heels of Hazardous Waste Drums for Last 6 Months Appendix 11. Documentation of Hazardous Waste Going to SWS's Secondary Transfer Facility Appendix 12. SWS SOPs for Container and Tank Cleaning Page 8 of 8 APPENDIX 1. PHOTOGRAPH LOG UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 1 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04188 Date of Photo: 05.09.2024 Time of Photo: 14:42 hrs Photographer: Anshul Paripati Description: Overview of waste area, CS 107, where facility is storing waste that they did not generate or sign manifests for. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 2 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04189 Date of Photo: 05.09.2024 Time of Photo: 14:42 hrs Photographer: Anshul Paripati Description: Close-up of label on black drums in the far back left of photo 1 in CS 107. All four of the drums have the same label. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 3 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04190 Date of Photo: 05.09.2024 Time of Photo: 14:47 hrs Photographer: Anshul Paripati Description: Close-up of black drums from photo 2 in CS 107. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 4 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04191 Date of Photo: 05.09.2024 Time of Photo: 14:47 hrs Photographer: Anshul Paripati Description: Overview of a row of three drums from photo 1 in CS 107. The blue and leftmost black drum have labels while the rightmost black drum does not. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 5 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04192 Date of Photo: 05.09.2024 Time of Photo: 14:47 hrs Photographer: Anshul Paripati Description: Close-up of the label on the black drum shown in photo 4 in CS 107. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 6 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04193 Date of Photo: 05.09.2024 Time of Photo: 14:47 hrs Photographer: Anshul Paripati Description: Close-up of the label on the blue drum shown in photo 4 in CS 107. UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Photograph Log Photo No. 7 Location: Specialized Waste Systems, Inc City: Channelview County/Parish: Harris State: Texas Photo Name: DSC04194 Date of Photo: 05.09.2024 Time of Photo: 14:54 hrs Photographer: Anshul Paripati Description: Close-up of unlabeled used batteries in CS 107. APPENDIX 2. FOLLOW-UP EMAIL #1 FROM SWS Appendix 2 Page 1 of 3 Appendix 2 Page 2 of 3 Appendix 2 Page 3 of 3 APPENDIX 3. FOLLOW-UP EMAIL #2 FROM SWS Appendix 3 Page 1 of 3 Appendix 3 Page 2 of 3 Appendix 3 Page 3 of 3 APPENDIX 4. FOLLOW-UP EMAIL #3 FROM SWS Appendix 4 Page 1 of 2 Appendix 4 Page 2 of 2 APPENDIX 5. SWS CORRECTIVE ACTION - NON RCRA EMPTY CONTAINERS AND UNIVERSAL BATTERIES CORRECTIVE ACTIONS EPA Observations for Response: "Receiving and managing non-empty RCRA containers without a permit" TAS believes their process is consistent with industry standard practice. Our process is as follows: We receive containers based on last contained documentation. After receipt and prior to washout, the container is evaluated for any residual heel that would not make the container "RCRA Empty". This information is communicated to the customer, and they are made aware that the waste is to be managed by the generator. Once approval from the customer is given, the heel is removed by manual means and containerized for the generator to dispose of. In no way is the heel altered during this transfer of containers. No water or chemicals are added and no treatment occurs. The heel is physically and chemically the same in the drums as it was in the container that it was removed from. As a transfer facility, we inform the generator that they must remove the heel containers within ten days. The generator is responsible for creating manifests and shipment of rejected materials. Only after the removal of residual heel, to make the container RCRA empty, will the facility start the washout process. "Universal waste batteries not labelled as universal waste" This issue has been corrected. Please see picture below for verification. Appendix 5 Page 1 of 1 APPENDIX 6. SWS DESCRIPTION OF CONTENTS OF CONTAINERS WITH UNKNOWN MATERIALS 2. Verification of the drums we saw with unknown material summary. DRUM 1: BLACK DRUM: 1-25-24 - 1000-SCS ON TOP. This drum was heel from a product removed from a trailer that was hauling "FUEL OIL, PYROLYSIS" product. This material is profiled to Systech Environmental to be utilized as a fuel and is not a solid waste per 40 CFR 261.2(c)(2)(ii). When we receive final approval, this drum will be shipped out in our next load to Systech. SEE DRUM 1 VERIFICATION PACKAGE FOR FURTHER INFORMATION. DRUM 2: BLUE DRUM: 3109/IRONCLAD/04-23-2024 ON TOP. This drum is a heel from a nonhazardous solid box that went to a Subtitle D Texas landfill. SEE DRUM 2 VERIFICATION PACKAGE FOR FURTHER INFORMATION. DRUM 3: BLACK DRUM: 05/08/24 MARTEST FULL (MIX) ON TOP. This drum is nonhazardous solid waste material removed from filters that contained molecular sieve to remove water from a synthetic base oil stock. SEE DRUM 3 VERIFICATION PACKAGE FOR FURTHER INFORMATION. Appendix 6 Page 1 of 47 DRUM 4 & 5: BLACK DRUMS: VB-22027 MOBILE MINI These drums are a heel from a flammable sludge of Xylene and Petroleum Distillates. SEE DRUM 4-5 VERIFICATION PACKAGE FOR FURTHER INFORMATION. DRUM 6: BLUE DRUM: 3109/IRONCLAD/04-23-2024 ON TOP. This drum was going to be used for a job at Kohl's. When the drum wasn't used, the label was inadvertently left on. Later, someone grabbed it to place unused absorbent from broken bags to protect it from the elements. We have removed the absorbent, bagged it up and spray painted the label so there will be no more confusion. BEFORE: AFTER 1: AFTER 2: TOTES - VINEGAR (ACETIC ACID) - SEE ATTACHED SDS: These totes are vinegar (aka ace c acid) We were transpor ng them as a product for a customer that no longer want the material. We are in the process of profiling the material for disposal as a nonhazardous waste. Appendix 6 Page 2 of 47 DRUM 1 INFORMATION Appendix 6 Page 3 of 47 SAFETY DATA SHEET Fuel Oil, pyrolysis Section 1. Identification GHS product identifier Product code Other means of identification Product type : Fuel Oil, pyrolysis : SDS#: 1749 : Not available. : Liquid. Recommended use of the chemical and restrictions to use Product use : Not available. Area of application : Industrial applications. Supplier's details : INEOS Olefins & Polymers USA 2600 South Shore Blvd. #500 League City, Texas 77573 e-mail address of person responsible for this SDS Emergency telephone number (with hours of operation) : rcspolymers@ineos.com : USA:1 (800) 424-9300 Outside USA:+1 703-527-3887 (CHEMTREC) Section 2. Hazards identification Classification of the substance or mixture GHS label elements Hazard pictograms : H225 H332 H340 H350 H361 H373 H304 : FLAMMABLE LIQUIDS - Category 2 ACUTE TOXICITY (inhalation) - Category 4 GERM CELL MUTAGENICITY - Category 1 CARCINOGENICITY - Category 1A TOXIC TO REPRODUCTION (Unborn child) - Category 2 SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (blood system, liver, thymus) - Category 2 ASPIRATION HAZARD - Category 1 Signal word Hazard statements Precautionary statements : Danger : H225 - Highly flammable liquid and vapor. H332 - Harmful if inhaled. H340 - May cause genetic defects. H350 - May cause cancer. H361 - Suspected of damaging the unborn child. H304 - May be fatal if swallowed and enters airways. H373 - May cause damage to organs through prolonged or repeated exposure. (blood system, liver, thymus) Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 4 of 47 : SDS#: 1749 Version : 4 1/19 Fuel Oil, pyrolysis Section 2. Hazards identification Prevention : P201 - Obtain special instructions before use. P202 - Do not handle until all safety precautions have been read and understood. P280 - Wear protective gloves. Wear eye or face protection. Wear protective clothing. P210 - Keep away from heat, hot surfaces, sparks, open flames and other ignition sources. No smoking. P241 - Use explosion-proof electrical, ventilating, lighting and all material-handling equipment. P242 - Use only non-sparking tools. P243 - Take precautionary measures against static discharge. P233 - Keep container tightly closed. P271 - Use only outdoors or in a well-ventilated area. P260 - Do not breathe vapor. Response : P314 - Get medical attention if you feel unwell. P308 + P313 - IF exposed or concerned: Get medical attention. P304 + P340 + P312 - IF INHALED: Remove person to fresh air and keep comfortable for breathing. Call a POISON CENTER or physician if you feel unwell. P301 + P310 + P331 - IF SWALLOWED: Immediately call a POISON CENTER or physician. Do NOT induce vomiting. P303 + P361 + P353 - IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water or shower. Storage : P405 - Store locked up. P403 - Store in a well-ventilated place. P235 - Keep cool. Disposal : P501 - Dispose of contents and container in accordance with all local, regional, national and international regulations. Supplemental label elements : - Eliminate sources of ignition. - Avoid spark promoters. - Ground/bond container and receiving equipment. - These alone may be insufficient to remove static electricity. - Avoid contact with skin and clothing. - Wash thoroughly after handling. Hazards not otherwise classified : - Static accumulating flammable liquid can become electrostatically charged even in bonded and grounded equipment. - Sparks may ignite liquid and vapor may cause flash fire or explosion. - Prolonged or repeated contact may dry skin and cause irritation. No ingredient(s) of unknown acute toxicity is intentionally used in this product. Section 3. Composition/information on ingredients Substance/mixture : Common name and : synonyms CAS number/other identifiers Mixture Not available. Ingredient name Other names % CAS number Fuel oil, pyrolysis styrene toluene benzene Fuel oil, pyrolysis styrene toluene benzene 99-100 <1 <0.5 <0.5 69013-21-4 100-42-5 108-88-3 71-43-2 Any concentration shown as a range is to protect confidentiality or is due to process variation. There are no additional ingredients present which, within the current knowledge of the supplier and in the concentrations applicable, are classified as hazardous to health and hence require reporting in this section. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 5 of 47 : SDS#: 1749 Version : 4 2/19 Fuel Oil, pyrolysis Section 4. First aid measures Description of necessary first aid measures Eye contact : Immediately flush eyes with plenty of water for at least 15 minutes, occasionally lifting the upper and lower eyelids. Check for and remove any contact lenses. Get medical attention immediately. Inhalation : - Move exposed person to fresh air. - If not breathing, if breathing is irregular or if respiratory arrest occurs, provide artificial respiration or oxygen by trained personnel. - Loosen tight clothing such as a collar, tie, belt or waistband. - Keep person warm and at rest. - Get medical attention immediately. Skin contact : - Call 911 or emergency medical service. - In case of contact with liquid, warm frozen tissues slowly with lukewarm water. - In case of contact, immediately flush skin with plenty of water for at least 15 minutes while removing contaminated clothing and shoes. - Dispose of contaminated clothing and shoes. - Do not remove clothing adhering to skin. - Keep person warm and at rest. - Wash clothing before reuse. Ingestion : - If swallowed, do not induce vomiting. - Never give anything by mouth to an unconscious person. - Aspiration hazard if swallowed. - Can enter lungs and cause damage. - Get medical attention immediately. Most important symptoms/effects, acute and delayed Potential acute health effects Eye contact : No known significant effects or critical hazards. Inhalation : Harmful if inhaled. Skin contact : Defatting to the skin. May cause skin dryness and irritation. Ingestion : May be fatal if swallowed and enters airways. Over-exposure signs/symptoms Eye contact : No specific data. Inhalation : Adverse symptoms may include the following: reduced fetal weight increase in fetal deaths skeletal malformations Skin contact : Adverse symptoms may include the following: irritation dryness cracking reduced fetal weight increase in fetal deaths skeletal malformations Ingestion : Adverse symptoms may include the following: nausea or vomiting reduced fetal weight increase in fetal deaths skeletal malformations Indication of immediate medical attention and special treatment needed, if necessary Notes to physician : Treat symptomatically. Contact poison treatment specialist immediately if large quantities have been ingested or inhaled. Specific treatments : No specific treatment. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 6 of 47 : SDS#: 1749 Version : 4 3/19 Fuel Oil, pyrolysis Section 4. First aid measures Protection of first-aiders : - No action shall be taken involving any personal risk or without suitable training. - If it is suspected that fumes are still present, the rescuer should wear an appropriate mask or self-contained breathing apparatus. See toxicological information (Section 11) Section 5. Fire-fighting measures Suitable extinguishing media : SMALL FIRE: In case of fire, use water spray (fog), foam, dry chemical or CO. LARGE FIRE: Use water spray, fog or foam. Move containers from fire area if this can be done without risk. If tank, rail car or tank truck is involved in a fire, ISOLATE for 1600 meters (1 mile) in all directions; also consider initial evacuation for 1600 meters (1 mile) in all directions. - Fight fire from maximum distance or use unmanned hose holders or monitor nozzles. - Cool containing vessels with flooding quantities of water until well after fire is out. - Withdraw immediately in case of rising sound from venting safety devices or discoloration of tank. - ALWAYS stay away from tanks engulfed in fire. - For massive fire, use unmanned hose holders or monitor nozzles; if this is impossible, withdraw from area and let fire burn. Unsuitable extinguishing media : Do not use water jet. Specific hazards arising from the chemical Hazardous thermal decomposition products : Highly flammable liquid. - Flammable or combustible, may be ignited by heat, sparks or flames. - Vapors may form explosive mixtures with air. - Vapor may travel a considerable distance to source of ignition and flash back. Special exposure hazards - Many gases are heavier than air and will spread along ground and collect in low or confined areas (sewers, basement, tanks.) - Vapor explosion hazard indoors, outdoors or in sewers. - Runoff to sewer may create fire or explosion hazard. - Containments may explode when heated. - Many liquids are lighter than water. : No specific data. Hazardous combustion products: carbon dioxide carbon monoxide Special protective actions for fire-fighters Special protective equipment for fire-fighters : Promptly isolate the scene by removing all persons from the vicinity of the incident if there is a fire. No action shall be taken involving any personal risk or without suitable training. Move containers from fire area if this can be done without risk. Use water spray to keep fire-exposed containers cool. : Fire-fighters should wear appropriate protective equipment and self-contained breathing apparatus (SCBA) with a full face-piece operated in positive pressure mode. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 7 of 47 : SDS#: 1749 Version : 4 4/19 Fuel Oil, pyrolysis Section 6. Accidental release measures Personal precautions, protective equipment and emergency procedures For non-emergency personnel : - No action shall be taken involving any personal risk or without suitable training. - Evacuate surrounding areas. - Keep unnecessary and unprotected personnel from entering. - Do not touch or walk through spilled material. - Shut off all ignition sources. - No flares, smoking or flames in hazard area. - Avoid breathing vapor or mist. - Provide adequate ventilation. - Put on appropriate personal protective equipment (see Section 8). - Structural firefighter's protective clothing will only provide limited protection. For emergency responders : If specialized clothing is required to deal with the spillage, take note of any information in Section 8 on suitable and unsuitable materials. See also the information in "For nonemergency personnel". Environmental precautions : - Ensure emergency procedures to deal with accidental gas releases are in place to avoid contamination of the environment. - Avoid dispersal of spilled material and runoff and contact with soil, waterways, drains and sewers. - Inform the relevant authorities if the product has caused environmental pollution (sewers, waterways, soil or air). Methods and materials for containment and cleaning up Small spill : - As an immediate precautionary measure, isolate spill or leak for at least 50 meters (150 feet) in all directions. - Keep unnecessary personnel away. - Stay upwind/keep distance from source. - Keep out of low areas. - Ventilate closed spaces before entering. - Eliminate all ignition sources (no smoking, flares, sparks or flames in immediate area). - Ensure that the equipment is adequately grounded. - Do not touch or walk through spilled material. - A vapor suppressing foam may be used to reduce vapors. - Absorb or cover with dry earth, sand or other non-combustible material and transfer to containers. - Use clean non-sparking tools to collect absorbed material. Large spill Note: see Section 1 for emergency contact information and Section 13 for waste disposal. : Consider initial downwind evacuation for at least 800 meters (1/2 mile). - Dike liquid for later disposal. - Water spray may reduce vapor but it may not prevent ignition in closed spaces. - Keep away from heat, sparks, open flames and hot surfaces. - No smoking. - Ensure that the equipment is adequately grounded. - Do not touch or walk through spilled material. - Contaminated absorbent material may pose the same hazard as the spilled product. - A vapor suppressing foam may be used to reduce vapors. - Cover with dry earth, sand or other non-combustible material. - Use only non-sparking tools. Note: see Section 1 for emergency contact information and Section 13 for waste disposal. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 8 of 47 : SDS#: 1749 Version : 4 5/19 Fuel Oil, pyrolysis Section 7. Handling and storage Precautions for safe handling Protective measures : Advice on general : occupational hygiene - Put on appropriate personal protective equipment (see Section 8). - Do not get in eyes or on skin or clothing. - Do not ingest. - Avoid breathing vapor or mist. - Use only with adequate ventilation. - Wear appropriate respirator when ventilation is inadequate. - Do not enter storage areas and confined spaces unless adequately ventilated. - Keep in the original container or an approved alternative made from a compatible material, kept tightly closed when not in use. - Store and use away from heat, sparks, open flame or any other ignition source. - Use explosion-proof electrical (ventilating, lighting and material handling) equipment. - Use non-sparking tools. - Take precautionary measures against electrostatic discharges. - To avoid fire or explosion, dissipate static electricity during transfer by grounding and bonding containers and equipment before transferring material. - Empty containers retain product residue and can be hazardous. - Do not reuse container. - Eating, drinking and smoking should be prohibited in areas where this material is handled, stored and processed. - Workers should wash hands and face before eating, drinking and smoking. Conditions for safe storage, including any incompatibilities : - Store in accordance with local regulations. - Store in a segregated and approved area. - Store in original container protected from direct sunlight in a dry, cool and wellventilated area, away from incompatible materials (see Section 10) and food and drink. - Eliminate all ignition sources. - Separate from oxidizing materials. - Keep container tightly closed and sealed until ready for use. - Use appropriate containment to avoid environmental contamination. Section 8. Exposure controls/personal protection Control parameters Ingredient name Exposure limits Fuel oil, pyrolysis styrene None. ACGIH TLV (United States, 3/2017). TWA: 20 ppm 8 hours. TWA: 85 mg/m 8 hours. STEL: 40 ppm 15 minutes. STEL: 170 mg/m 15 minutes. OSHA PEL Z2 (United States, 2/2013). TWA: 100 ppm 8 hours. CEIL: 200 ppm AMP: 600 ppm 5 minutes. NIOSH REL (United States, 10/2016). TWA: 50 ppm 10 hours. TWA: 215 mg/m 10 hours. STEL: 100 ppm 15 minutes. STEL: 425 mg/m 15 minutes. benzene ACGIH TLV (United States, 3/2017). Absorbed through skin. TWA: 0.5 ppm 8 hours. TWA: 1.6 mg/m 8 hours. STEL: 2.5 ppm 15 minutes. STEL: 8 mg/m 15 minutes. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 9 of 47 : SDS#: 1749 Version : 4 6/19 Fuel Oil, pyrolysis Section 8. Exposure controls/personal protection OSHA PEL Z2 (United States, 2/2013). TWA: 10 ppm 8 hours. CEIL: 25 ppm AMP: 50 ppm 10 minutes. NIOSH REL (United States, 10/2016). TWA: 0.1 ppm 10 hours. STEL: 1 ppm 15 minutes. OSHA PEL (United States, 6/2016). TWA: 1 ppm 8 hours. STEL: 5 ppm 15 minutes. toluene OSHA PEL Z2 (United States, 2/2013). TWA: 200 ppm 8 hours. CEIL: 300 ppm AMP: 500 ppm 10 minutes. NIOSH REL (United States, 10/2016). TWA: 100 ppm 10 hours. TWA: 375 mg/m 10 hours. STEL: 150 ppm 15 minutes. STEL: 560 mg/m 15 minutes. ACGIH TLV (United States, 3/2017). TWA: 20 ppm 8 hours. Appropriate engineering controls Environmental exposure controls : - Use only with adequate ventilation. - Use process enclosures, local exhaust ventilation or other engineering controls to keep worker exposure to airborne contaminants below any recommended or statutory limits. - The engineering controls also need to keep gas, vapor or dust concentrations below any lower explosive limits. - Use explosion-proof ventilation equipment. : Emissions from ventilation or work process equipment should be checked to ensure they comply with the requirements of environmental protection legislation. In some cases, fume scrubbers, filters or engineering modifications to the process equipment will be necessary to reduce emissions to acceptable levels. Individual protection measures Hygiene measures : Eye/face protection : Skin protection Hand protection : Body protection : Other skin protection : - Wash hands, forearms and face thoroughly after handling chemical products, before eating, smoking and using the lavatory and at the end of the working period. - Appropriate techniques should be used to remove potentially contaminated clothing. - Ensure that eyewash stations and safety showers are close to the workstation location. Splash proof safety goggles complying with an approved standard should be used when a risk assessment indicates this is necessary to avoid exposure to liquid splashes, mists or dusts. Chemical-resistant, impervious gloves complying with an approved standard should be worn at all times when handling chemical products if a risk assessment indicates this is necessary. Personal protective equipment for the body should be selected based on the task being performed and the risks involved and should be approved by a specialist before handling this product. When there is a risk of ignition from static electricity, wear antistatic protective clothing. For the greatest protection from static discharges, clothing should include anti-static overalls, boots and gloves. Personal protective equipment for the body should be selected based on the task being performed and the risks involved and should be approved by a specialist before handling this product. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 10 of 47 : SDS#: 1749 Version : 4 7/19 Fuel Oil, pyrolysis Section 8. Exposure controls/personal protection Respiratory protection : - Wear positive pressure SCBA when ventilation is inadequate - Use a properly fitted, air-purifying or air-fed respirator complying with an approved standard if a risk assessment indicates this is necessary. - Respirator selection must be based on known or anticipated exposure levels, the hazards of the product and the safe working limits of the selected respirator. - All respirator use must comply with OSHA 29 CFR 1910.134 Section 9. Physical and chemical properties Appearance Physical state Color Odor Odor threshold pH Melting point Boiling point Flash point Evaporation rate Flammability (solid, gas) Lower and upper explosive (flammable) limits Vapor pressure Vapor density Relative density Solubility Partition coefficient: noctanol/water Auto-ignition temperature Decomposition temperature Viscosity : Liquid. : Amber. : Hydrocarbon. : Not available. : Not available. : 12 to 88C (53.6 to 190.4F) : 191C (375.8F) : 21.1 to 60C (70 to 140F) Pensky-Martens. : Not available. : Not available. : Lower: 1.1% Upper: 5 to 7.8% : 12.3 kPa (92 mm Hg) [37.8C] : 0.75 to 3.6 [Air = 1] : 0.87 to 0.91 (Water = 1) : Insoluble in the following materials: cold water. : 2.13 to 2.76 : >200C (>392F) : Not available. : Not available. Section 10. Stability and reactivity Reactivity : Flammable liquid and vapor. Avoid all possible sources of ignition (spark or flame). To avoid fire or explosion, dissipate static electricity during transfer by grounding and bonding containers and equipment before transferring material. Chemical stability : Stable under recommended storage and handling conditions (see Section 7). Possibility of hazardous reactions : Under normal conditions of storage and use, hazardous reactions will not occur. Under normal conditions of storage and use, hazardous polymerization will not occur. Conditions to avoid Incompatible materials : Avoid all possible sources of ignition (spark or flame). Do not pressurize, cut, weld, braze, solder, drill, grind or expose containers to heat or sources of ignition. Do not allow vapor to accumulate in low or confined areas. : Reactive or incompatible with the following materials: oxidizing materials Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 11 of 47 : SDS#: 1749 Version : 4 8/19 Fuel Oil, pyrolysis Section 10. Stability and reactivity Hazardous decomposition products : Decomposition products may include the following materials: carbon dioxide carbon monoxide Hazardous combustion products: carbon dioxide carbon monoxide Section 11. Toxicological information Information on the likely routes of exposure : Routes of entry anticipated: Oral, Dermal, Inhalation. Symptoms related to the physical, chemical and toxicological characteristics Eye contact : No specific data. Inhalation : Adverse symptoms may include the following: reduced fetal weight increase in fetal deaths skeletal malformations Skin contact : Adverse symptoms may include the following: irritation dryness cracking reduced fetal weight increase in fetal deaths skeletal malformations Ingestion : Adverse symptoms may include the following: nausea or vomiting reduced fetal weight increase in fetal deaths skeletal malformations Delayed and immediate effects and also chronic effects from short and long term exposure Short term exposure Potential immediate effects : Not available. Potential delayed effects : Not available. Long term exposure Potential immediate effects : Not available. Potential delayed effects : Not available. Potential chronic health effects General : May cause damage to organs through prolonged or repeated exposure. Prolonged or repeated contact can defat the skin and lead to irritation, cracking and/or dermatitis. Numerical measures of toxicity Acute toxicity estimates Route ATE value Inhalation (vapors) 11.2 mg/l Information on toxicological effects (Listed for the components where information is available.) Acute toxicity Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 12 of 47 : SDS#: 1749 Version : 4 9/19 Fuel Oil, pyrolysis Section 11. Toxicological information Product/ingredient name styrene benzene toluene Result LC50 Inhalation Vapor LC50 Inhalation Vapor LCLo Inhalation Gas. LCLo Inhalation Vapor LD50 Intraperitoneal LD50 Intraperitoneal LD50 Intravenous LD50 Oral LD50 Oral TCLo Inhalation Gas. TCLo Inhalation Vapor TDLo Oral LC50 Inhalation Gas. LCLo Inhalation Gas. LCLo Inhalation Gas. LD50 Intraperitoneal LD50 Intraperitoneal LD50 Oral LD50 Oral LDLo Intravenous LDLo Oral LDLo Oral LDLo Oral TC Inhalation Gas. TC Inhalation Gas. TC Inhalation Gas. TC Inhalation Gas. TCLo Inhalation Gas. TCLo Inhalation Gas. TCLo Inhalation Gas. TCLo Inhalation Gas. TCLo Inhalation Vapor TCLo Inhalation Vapor TD Oral TD Oral TD Oral TDLo Dermal TDLo Intraperitoneal TDLo Intraperitoneal TDLo Oral TDLo Oral TDLo Parenteral TDLo Parenteral TDLo Subcutaneous TDLo Subcutaneous LC50 Inhalation Gas. LCLo Inhalation Gas. LCLo Inhalation Gas. LD50 Dermal LD50 Intraperitoneal LD50 Intraperitoneal LD50 Intraperitoneal LD50 Intravenous LD50 Oral Species Mouse Rat Human Guinea pig Mouse Rat Mouse Mouse Rat Rat Rat Rat Rat Human Human Mouse Rat Mouse Rat Rabbit Dog Man Rat Human Human Mouse Mouse Mouse Rat - Female Rat - Female Rat Rabbit Female Rat Mouse Rat Rat Mouse Mouse - Male Mouse Mouse Female Mouse Mouse Female Mouse Mouse Female Mouse Mouse Rabbit Rat Rabbit Mouse Mouse Rat Rat Rat Dose 9500 mg/m 24 g/m 10000 ppm 12 mg/m 660 mg/kg 898 mg/kg 90 mg/kg 316 mg/kg 5000 mg/kg 100 ppm 1500 g/m 8600 mg/kg 10000 ppm 2 pph 20000 ppm 340 mg/kg 2890 g/kg 4700 mg/kg 3306 mg/kg 88 mg/kg 2000 mg/kg 50 mg/kg 52 g/kg 150 ppm 10 ppm 1200 ppm 300 ppm 300 ppm 50 ppm 150 ppm 1200 ppm 1 g/m 670 mg/m 2400 mg/kg 52 g/kg 10 g/kg 1200 g/kg 5 mg/kg 1200 mg/kg 6500 mg/kg 18250 mg/kg 4 g/kg 670 mg/kg 1100 mg/kg 600 mg/kg 400 ppm 55000 ppm 4000 ppm 12124 mg/kg 640 mg/kg 59 mg/kg 1332 mg/kg 1960 mg/kg 5000 mg/kg Exposure 4 hours 4 hours 30 months 14 hours 4 hours 24 hours 7 hours 5 months 5 months 15 months 8 hours 6 hours 6 hours 6 hours 24 hours 24 hours 6 hours 24 hours 24 hours - - - 24 hours 40 months 4 hours - Date of issue/Date of revision : 09/20/2018 SDS # : SDS#: 1749 Version : 4 10/19 Appendix 6 Page 13 of 47 Fuel Oil, pyrolysis Section 11. Toxicological information LD50 Route of exposure unreported LD50 Route of exposure unreported LD50 Subcutaneous LDLo Oral TCLo Inhalation Gas. TDLo Oral - : Not available. Irritation/Corrosion Mouse Rat Mouse Human Mouse Mouse Female 2 g/kg 6900 mg/kg 2250 mg/kg 50 mg/kg 400 ppm 9 g/kg - - 7 hours - Product/ingredient name Result Species Score Exposure Observation styrene benzene toluene Eyes - Moderate irritant Rabbit - Eyes - Severe irritant Rabbit - Skin - Mild irritant Rabbit - Skin - Moderate irritant Rabbit - Eyes - Moderate irritant Rabbit - Eyes - Severe irritant Rabbit - Skin - Mild irritant Rat - Skin - Mild irritant Rabbit - Skin - Moderate irritant Rabbit - Eyes - Severe irritant Rabbit - Skin - Moderate irritant Rabbit - Skin - Moderate irritant Rabbit - Skin - Mild irritant Eyes - Mild irritant Eyes - Mild irritant Rabbit - Rabbit - Rabbit - - : Not available. Sensitization Specific target organ toxicity (single exposure) : Not available. 24 hours 100 - milligrams 100 - milligrams 500 - milligrams 100 Percent - 88 milligrams - 24 hours 2 - milligrams 8 hours 60 - microliters 24 hours 15 - milligrams 24 hours 20 - milligrams 24 hours 2 - milligrams 24 hours 20 - milligrams 500 - milligrams 435 mg - 0.87 mg - 0.5 minutes - 100 mg Name Category Route of exposure Target organs styrene toluene - : Not available. Specific target organ toxicity (repeated exposure) Category 3 Category 3 Not applicable. Not applicable. Respiratory tract irritation Narcotic effects Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 14 of 47 : SDS#: 1749 Version : 4 11/19 Fuel Oil, pyrolysis Section 11. Toxicological information Name Fuel oil, pyrolysis styrene benzene toluene - : Not available. Aspiration hazard Category Category 2 Category 1 Category 1 Category 2 Route of exposure Not determined Not determined Not determined Not determined Target organs blood system, liver and thymus hearing organs blood system hearing organs Name Fuel oil, pyrolysis styrene benzene toluene Result ASPIRATION HAZARD - Category 1 ASPIRATION HAZARD - Category 1 ASPIRATION HAZARD - Category 1 ASPIRATION HAZARD - Category 1 Potential acute health effects Eye contact : Inhalation : Skin contact : Ingestion : No known significant effects or critical hazards. Harmful if inhaled. Defatting to the skin. May cause skin dryness and irritation. May be fatal if swallowed and enters airways. Mutagenicity Product/ingredient name Test Experiment Result benzene - : Not available. Carcinogenicity Classification OECD 471 Bacterial Reverse Mutation Test 473 In vitro Mammalian Chromosomal Aberration Test OECD 474 Mammalian Erythrocyte Micronucleus Test OECD 475 Mammalian Bone Marrow Chromosomal Aberration Test Experiment: In vitro Subject: Bacteria Experiment: In vitro Subject: Mammalian-Animal Experiment: In vivo Subject: Mammalian-Animal Experiment: In vivo Subject: Mammalian-Animal Positive Positive Positive Positive Product/ingredient name OSHA IARC NTP styrene benzene toluene - 2B Reasonably anticipated to be a human carcinogen. + 1 Known to be a human carcinogen. - 3 - +: Listed - : Not applicable. IARC 1 Carcinogenic to humans IARC 2A Probably carcinogenic to humans IARC 2B Possibly carcinogenic to humans IARC 3 Not classifiable as to its carcinogenicity to humans IARC 4 Probably not carcinogenic to humans Reproductive toxicity Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 15 of 47 : SDS#: 1749 Version : 4 12/19 Fuel Oil, pyrolysis Section 11. Toxicological information Product/ingredient name Fuel oil, pyrolysis styrene toluene Maternal toxicity Positive Positive Positive Fertility - - : Not available. Teratogenicity : Not available. Development toxin Positive Positive Species Dose Exposure Rat - Male, Female Rat Rat - Female Dermal Inhalation Inhalation: 750 ppm NOAEC 6 hours 20 days; 6 hours per day Section 12. Ecological information Ecotoxicity Product/ingredient name styrene benzene toluene - : Not available. Result Acute EC50 1400 g/l Fresh water Acute EC50 720 g/l Fresh water Acute EC50 4700 g/l Fresh water Acute LC50 52 mg/l Marine water Acute LC50 4080 g/l Fresh water Chronic NOEC 63 g/l Fresh water Acute EC50 29000 g/l Fresh water Acute EC50 1600000 g/l Fresh water Acute EC50 9230 g/l Fresh water Acute LC50 21 mg/l Marine water Acute LC50 5.28 ul/L Fresh water Chronic EC10 >1360 mg/l Fresh water Chronic NOEC 98 mg/l Fresh water Chronic NOEC 1.5 to 5.4 ul/L Marine water Acute EC50 12500 g/l Fresh water Acute EC50 11600 g/l Fresh water Acute EC50 6000 g/l Fresh water Acute LC50 5500 g/l Fresh water Chronic NOEC 1000 g/l Fresh water Species Exposure Algae - Pseudokirchneriella subcapitata Algae - Pseudokirchneriella subcapitata Daphnia - Daphnia magna Crustaceans - Artemia salina Fish - Pimephales promelas Algae - Pseudokirchneriella subcapitata Algae - Pseudokirchneriella subcapitata Algae - Selenastrum sp. Daphnia - Daphnia magna Neonate Crustaceans - Artemia salina Fish - Oncorhynchus gorbuscha Fry Algae - Scenedesmus subspicatus Daphnia - Daphnia magna Fish - Morone saxatilis - Juvenile (Fledgling, Hatchling, Weanling) Algae - Pseudokirchneriella subcapitata Crustaceans - Gammarus pseudolimnaeus - Adult Daphnia - Daphnia magna Juvenile (Fledgling, Hatchling, Weanling) Fish - Oncorhynchus kisutch - Fry Daphnia - Daphnia magna 72 hours 96 hours 48 hours 48 hours 96 hours 96 hours 72 hours 96 hours 48 hours 48 hours 96 hours 96 hours 21 days 4 weeks 72 hours 48 hours 48 hours 96 hours 21 days Persistence and degradability Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 16 of 47 : SDS#: 1749 Version : 4 13/19 Fuel Oil, pyrolysis Section 12. Ecological information Product/ingredient name styrene benzene toluene - : Not available. Test 301F Ready Biodegradability Manometric Respirometry Test 301C Ready Biodegradability Modified MITI Test (I) 301C Ready Biodegradability Modified MITI Test (I) Result >60 % - 28 days 100 % - 14 days 100 % - 14 days Product/ingredient name styrene benzene toluene - : Not available. Bioaccumulative potential Aquatic half-life - Photolysis - Dose - - Inoculum - - Biodegradability Readily Readily Readily Product/ingredient name Fuel Oil, pyrolysis styrene benzene toluene - : Not available. Mobility in soil Soil/water partition coefficient (KOC) Mobility Other adverse effects LogPow 2.13 to 2.76 0.35 2.13 2.73 BCF 13.49 11 90 : Not available. : Not available. : No known significant effects or critical hazards. Potential low low low low Section 13. Disposal considerations Disposal methods : Do not puncture or incinerate container. Disposal of this product, solutions and any byproducts should at all times comply with the requirements of environmental protection and waste disposal legislation and any regional local authority requirements. The generation of waste should be avoided or minimized wherever possible. Empty containers or liners may retain some product residues. This material and its container must be disposed of in a safe way. Dispose of surplus and non-recyclable products via a licensed waste disposal contractor. Disposal of this product, solutions and any byproducts should at all times comply with the requirements of environmental protection and waste disposal legislation and any regional local authority requirements. Avoid dispersal of spilled material and runoff and contact with soil, waterways, drains and sewers. Refer to Section 7: HANDLING AND STORAGE and Section 8: EXPOSURE CONTROLS/PERSONAL PROTECTION for additional handling information and protection of employees. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 17 of 47 : SDS#: 1749 Version : 4 14/19 Fuel Oil, pyrolysis Section 14. Transport information DOT Classification UN number UN1993 UN1993 IMDG UN proper shipping name Flammable liquids, n.o.s. (Fuel oil, pyrolysis) RQ (benzene, Toluene) Transport 3 hazard class(es) FLAMMABLE LIQUID, N.O.S. (Fuel oil, pyrolysis). Marine pollutant (Fuel oil, pyrolysis) 3 UN1993 IATA Flammable liquid, n.o.s. (Fuel oil, pyrolysis) 3 Packing group II Environmental Yes. hazards Additional information DOT Classification IMDG IATA II II Yes. Yes. The environmentally hazardous substance mark is not required. : This product is not regulated as a marine pollutant when transported on inland waterways in sizes of 5 L or 5 kg or by road, rail, or inland air in non-bulk sizes, provided the packagings meet the general provisions of 173.24 and 173.24a. Reportable quantity 2222.2 lbs / 1008.9 kg [299.46 gal / 1133.6 L]. Package sizes shipped in quantities less than the product reportable quantity are not subject to the RQ (reportable quantity) transportation requirements. Limited quantity Yes. Packaging instruction Exceptions: 150. Non-bulk: 202. Bulk: 242. Quantity limitation Passenger aircraft/rail: 5 L. Cargo aircraft: 60 L. Special provisions IB2, T7, TP1, TP8, TP28 : The marine pollutant mark is not required when transported in sizes of 5 L or 5 kg. Emergency schedules (EmS) F-E, S-E Special provisions 274 Remarks Packaging instructions: P001 Tank Instructions : T7 : The environmentally hazardous substance mark may appear if required by other transportation regulations. Quantity limitation Passenger and Cargo Aircraft: 5 L. Packaging instructions: 353. Cargo Aircraft Only: 60 L. Packaging instructions: 364. Limited Quantities - Passenger Aircraft: 1 L. Packaging instructions: Y341. Special provisions A3 Special precautions for user : Transport within user's premises: always transport in closed containers that are upright and secure. Ensure that persons transporting the product know what to do in the event of an accident or spillage. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 18 of 47 : SDS#: 1749 Version : 4 15/19 Fuel Oil, pyrolysis Section 14. Transport information Transport in bulk according to Annex II of MARPOL and the IBC Code : Not available. Section 15. Regulatory information Additional regulatory information may be available through our website, at www.ineos.com. U.S. Federal regulations : United States inventory (TSCA 8b): All components are listed or exempted. Clean Water Act (CWA) 307: benzene; toluene Clean Water Act (CWA) 311: styrene; benzene; toluene Clean Air Act Section 112 (b) Hazardous Air Pollutants (HAPs) : Listed Clean Air Act Section 602 Class I Substances : Not listed Clean Air Act Section 602 Class II Substances : Not listed DEA List I Chemicals (Precursor Chemicals) : Not listed DEA List II Chemicals (Essential Chemicals) : Not listed SARA 302/304 Composition/information on ingredients : No products were found. SARA 304 RQ : Not applicable. SARA 311/312 Classification : FLAMMABLE LIQUIDS - Category 2 ACUTE TOXICITY (inhalation) - Category 4 GERM CELL MUTAGENICITY - Category 1 CARCINOGENICITY - Category 1A TOXIC TO REPRODUCTION (Unborn child) - Category 2 SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (blood system, liver, thymus) - Category 2 ASPIRATION HAZARD - Category 1 HNOC - Defatting irritant HNOC - Static-accumulating flammable liquid Composition/information on ingredients Name % Classification Fuel oil, pyrolysis styrene 99-100 <1 ACUTE TOXICITY (inhalation) - Category 4 CARCINOGENICITY - Category 1B TOXIC TO REPRODUCTION (Unborn child) - Category 2 SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (blood system, liver, thymus) - Category 2 ASPIRATION HAZARD - Category 1 HNOC - Defatting irritant FLAMMABLE LIQUIDS - Category 3 ACUTE TOXICITY (inhalation) - Category 4 SKIN IRRITATION - Category 2 EYE IRRITATION - Category 2A CARCINOGENICITY - Category 2 TOXIC TO REPRODUCTION (Unborn child) - Category 2 Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 19 of 47 : SDS#: 1749 Version : 4 16/19 Fuel Oil, pyrolysis Section 15. Regulatory information benzene toluene SPECIFIC TARGET ORGAN TOXICITY (SINGLE EXPOSURE) (Respiratory tract irritation) - Category 3 SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (hearing organs) - Category 1 ASPIRATION HAZARD - Category 1 HNOC - Defatting irritant <0.5 FLAMMABLE LIQUIDS - Category 2 ACUTE TOXICITY (oral) - Category 4 SKIN IRRITATION - Category 2 EYE IRRITATION - Category 2A GERM CELL MUTAGENICITY - Category 1B CARCINOGENICITY - Category 1A SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (blood system) - Category 1 ASPIRATION HAZARD - Category 1 HNOC - Defatting irritant <0.5 FLAMMABLE LIQUIDS - Category 2 ACUTE TOXICITY (oral) - Category 4 SKIN IRRITATION - Category 2 EYE IRRITATION - Category 2A TOXIC TO REPRODUCTION (Unborn child) - Category 2 SPECIFIC TARGET ORGAN TOXICITY (SINGLE EXPOSURE) (Narcotic effects) - Category 3 SPECIFIC TARGET ORGAN TOXICITY (REPEATED EXPOSURE) (hearing organs) - Category 2 ASPIRATION HAZARD - Category 1 HNOC - Defatting irritant SARA 313 Product name CAS number % Form R - Reporting requirements styrene benzene 100-42-5 <1 71-43-2 <0.5 Supplier notification styrene benzene 100-42-5 <1 71-43-2 <0.5 SARA 313 notifications must not be detached from the SDS and any copying and redistribution of the SDS shall include copying and redistribution of the notice attached to copies of the SDS subsequently redistributed. California Prop. 65 WARNING: This product can expose you to Benzene, which is known to the State of California to cause cancer and birth defects or other reproductive harm. This product can expose you to chemicals including Styrene, which is known to the State of California to cause cancer, and Toluene, which is known to the State of California to cause birth defects or other reproductive harm. For more information go to www.P65Warnings.ca.gov. Ingredient name Benzene Toluene Styrene No significant risk level Yes. Yes. Maximum acceptable dosage level Yes. Yes. - Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 20 of 47 : SDS#: 1749 Version : 4 17/19 Fuel Oil, pyrolysis Section 16. Other information Hazardous Material Information System (U.S.A.) Health *3 Flammability 3 Physical hazards 0 Caution: HMIS ratings are based on a 0-4 rating scale, with 0 representing minimal hazards or risks, and 4 representing significant hazards or risks. Although HMIS ratings and the associated label are not required on SDSs or products leaving a facility under 29 CFR 1910.1200, the preparer may choose to provide them. HMIS ratings are to be used with a fully implemented HMIS program. HMIS is a registered trademark and service mark of the American Coatings Association, Inc. The customer is responsible for determining the PPE code for this material. For more information on HMIS Personal Protective Equipment (PPE) codes, consult the HMIS Implementation Manual. National Fire Protection Association (U.S.A.) Health 3 Flammability 1 0 Instability/Reactivity Special Reprinted with permission from NFPA 704, Identification of the Hazards of Materials for Emergency Response Copyright 1997, National Fire Protection Association, Quincy, MA 02269. This reprinted material is not the complete and official position of the National Fire Protection Association, on the referenced subject which is represented only by the standard in its entirety. Copyright 2001, National Fire Protection Association, Quincy, MA 02269. This warning system is intended to be interpreted and applied only by properly trained individuals to identify fire, health and reactivity hazards of chemicals. The user is referred to certain limited number of chemicals with recommended classifications in NFPA 49 and NFPA 325, which would be used as a guideline only. Whether the chemicals are classified by NFPA or not, anyone using the 704 systems to classify chemicals does so at their own risk. Procedure used to derive the classification Classification Justification Flam. Liq. 2, H225 Acute Tox. 4, H332 Muta. 1, H340 Carc. 1A, H350 Repr. 2, H361 (Unborn child) STOT RE 2, H373 (blood system, liver, thymus) Asp. Tox. 1, H304 On basis of test data Calculation method Calculation method Calculation method Calculation method Calculation method Expert judgment History Date of issue/Date of revision Date of previous issue Version Key to abbreviations : 09/20/2018 : No previous version. :4 : ATE = Acute Toxicity Estimate BCF = Bioconcentration Factor GHS = Globally Harmonized System of Classification and Labelling of Chemicals IATA = International Air Transport Association IBC = Intermediate Bulk Container IMDG = International Maritime Dangerous Goods LC = Lethal Concentration LC50 = Lethal Concentration Fifty LCL0 = Lethal Concentration Low Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 21 of 47 : SDS#: 1749 Version : 4 18/19 Fuel Oil, pyrolysis Section 16. Other information LD50 = Lethal Dose fifty LDL0 = Lethal Dose Low LogPow = logarithm of the octanol/water partition coefficient MARPOL = International Convention for the Prevention of Pollution as modified by the Protocol of 1978. ("Marpol" = marine pollution) PEL = Permissible Exposure Limit TC = Toxic Concentration TCL0 = Toxic Dose Low TD = Toxic Dose TDL0 = Toxic Dose Low TD50 = Toxic Dose fifty TLV = Threshold Limit Value UN = United Nations WEEL = Workplace Environmental Exposure Level From Ships, 1973 References : HCS (U.S.A.)- Hazard Communication Standard International transport regulationsHazardous Substances Database (HSDB) : toxicology data file on the National Library of Medicine's (NLM) Toxicology Data Network (TOXNET). Registry of Toxic Effects of Chemical Substances (RTECS) Commission de la sant et de la scurit du travail, Service du rpertoire toxicologique (CSST) : information on chemical products used in the workplace including WHMIS classification. National Toxicology Program (NTP), Department of Health and Human Services: Report on Carcinogens International Agency for Research on Cancer (IARC), List of Carcinogens Occupational Safety and Health Administration (OSHA) (29 CFR 1910.1001-1052) National Institute for Occupational Safety and Health; NIOSH Pocket Guide to Chemical Hazards. Aquatic Toxicity Information Retrieval (AQUIRE) Sax's Dangerous Properties of Industrial Materials Other special considerations : Refer to OSHA standard in 29 CFR 1910 for additional information. Indicates information that has changed from previously issued version. Notice to reader To the best of our knowledge, the information contained herein is accurate. However, neither the above-named supplier, nor any of its subsidiaries, assumes any liability whatsoever for the accuracy or completeness of the information contained herein. Final determination of suitability of any material is the sole responsibility of the user. All materials may present unknown hazards and should be used with caution. Although certain hazards are described herein, we cannot guarantee that these are the only hazards that exist. Date of issue/Date of revision : 09/20/2018 SDS # Appendix 6 Page 22 of 47 : SDS#: 1749 Version : 4 19/19 DRUM 2 INFORMATION Appendix 6 Page 23 of 47 Appendix 6 Page 24 of 47 DRUM 3 INFORMATION Appendix 6 Page 25 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 Date of issue: 10/6/2015 Revision date: 3/23/2022 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1. Product identifier Product form : Substance Trade name : Molecular Sieve-type 4A EC-No. : 930-915-9 CAS-No. : 1318-02-1 REACH Reg No : 01-2119429034-49-**** Formula : Unspecified Synonyms : Aluminosilicates, zeolites / Zeolites / ZEOLITE / Zeolite, cuboidal, crystalline, synthetic, non-fibrous / Zeolite (insoluble inorganic) / Zeolite, cuboidal, crystalline, synthetic, non fibrous, thermally produced 1.2. Relevant identified uses of the substance or mixture and uses advised against 1.2.1. Relevant identified uses Main use category : For drying of industrial gaspurification of gas of raw materials in separation plant (while removing water and carbon dioxide and some hydrocarbons) 1.2.2. Uses advised against Restrictions on use : No information available 1.3. Details of the supplier of the safety data sheet Only Representative: REACH24H CONSULTING GROUP Address: Paramount Court, Corrig Road, Sandyford, Dublin 18, Ireland E-mail: Info@reach24h.com Manufacturer: Address: E-mail: Telephone: Fax: Shanghai Hengye Molecular Sieve Co., Ltd. No.12,Guangda Road,Fengxian District, Shanghai 201414, P.R.C. jianwei@hyms.com.cn +86-21-57568588-8001 +86-21-57568970 1.4. Emergency telephone number Emergency number : 8621-57568588 SECTION 2: Hazards identification 2.1. Classification of the substance or mixture Classification according to Regulation (EC) No. 1272/2008 [CLP] Not classified Adverse physicochemical, human health and environmental effects To our knowledge, this product does not present any particular risk, provided it is handled in accordance with good occupational hygiene and safety practice. 2.2. Label elements Labelling according to Regulation (EC) No. 1272/2008 [CLP]Extra labelling to displayExtra classification(s) to display No labelling applicable 2.3. Other hazards This substance/mixture does not meet the PBT criteria of REACH regulation, annex XIII This substance/mixture does not meet the vPvB criteria of REACH regulation, annex XIII SECTION 3: Composition/information on ingredients 3.1. Substances Name Product identifier Silicon Oxide (Synthetic) Sodium Oxide Aluminum Oxide 3.2. Mixtures Not applicable (CAS-No.) 7631-86-9 (CAS-No.)1313-59-3 (CAS-No.)1344-28-1 % Classification according to Regulation (EC) No. 1272/2008 [CLP] 60 Not classified 40 Not classified 40 Not classified 3/23/2022 EN (English) 1/6 Appendix 6 Page 26 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 SECTION 4: First aid measures 4.1. Description of first aid measures First-aid measures general : In all cases of doubt, or when symptoms persist, seek medical attention. First-aid measures after inhalation : Remove person to fresh air and keep comfortable for breathing. Get medical advice/attention if you feel unwell. First-aid measures after skin contact : Gently wash with plenty of soap and water. Take off contaminated clothing. First-aid measures after eye contact : Remove contact lenses, if present and easy to do. Continue rinsing. Rinse cautiously with water for several minutes. If eye irritation persists: Get medical advice/attention. First-aid measures after ingestion : Call a poison center or a doctor if you feel unwell. Rinse mouth. 4.2. Most important symptoms and effects, both acute and delayed Symptoms/effects : No information available. 4.3. Indication of any immediate medical attention and special treatment needed Treat symptomatically. SECTION 5: Firefighting measures 5.1. Extinguishing media Suitable extinguishing media : Water spray. Dry powder. Foam. Unsuitable extinguishing media : No information available. 5.2. Special hazards arising from the substance or mixture No information available 5.3. Advice for firefighters Precautionary measures fire : Eliminate all ignition sources if safe to do so. Evacuate personnel to a safe area. Ensure adequate ventilation, especially in confined areas. Firefighting instructions : Keep upwind. Complete protective clothing. Protection during firefighting : Do not attempt to take action without suitable protective equipment. Self-contained breathing apparatus. Complete protective clothing. SECTION 6: Accidental release measures 6.1. Personal precautions, protective equipment and emergency procedures 6.1.1. For non-emergency personnel Protective equipment Emergency procedures : Wear personal protective equipment. : Ventilate spillage area. 6.1.2. For emergency responders Protective equipment : Do not attempt to take action without suitable protective equipment. For further information refer to section 8: "Exposure controls/personal protection". 6.2. Environmental precautions Avoid release to the environment. 6.3. Methods and material for containment and cleaning up Methods for cleaning up : Sweep up or vacuum up the product. Avoid raising dust. Other information : Dispose of materials or solid residues at an authorized site. 6.4. Reference to other sections . For further information refer to section 13. SECTION 7: Handling and storage 7.1. Precautions for safe handling Precautions for safe handling : Avoid dust formation. Ensure good ventilation of the work station. Wear personal protective equipment. Provide good ventilation in process area to prevent formation of flammable vapour. Handle in accordance with good industrial hygiene and safety practice. Hygiene measures : Do not eat, drink or smoke when using this product. Always wash hands after handling the product. Keep away from food, drink and animal feeding stuffs. 7.2. Conditions for safe storage, including any incompatibilities Storage conditions : Store in a well-ventilated place. Keep cool. Store in tightly closed containers. Store in a dry area. 7.3. Specific end use(s) No information available SECTION 8: Exposure controls/personal protection 8.1. Control parameters Zeolites (1318-02-1) DNEL/DMEL (Workers) Long-term - systemic effects, dermal 2.5 - 3 mg/kg bodyweight/day 3/23/2022 EN (English) 2/6 Appendix 6 Page 27 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 Zeolites (1318-02-1) Long-term - local effects, inhalation 3 mg/m DNEL/DMEL (General population) Long-term - systemic effects,oral 1.25 - 1.5 mg/kg bodyweight/day Long-term - systemic effects, dermal 1.25 - 1.5 mg/kg bodyweight/day Long-term - local effects, inhalation 0.0033 mg/m PNEC (Water) PNEC aqua (freshwater) 3.2 mg/l PNEC aqua (marine water) 0.32 mg/l PNEC aqua (intermittent, marine water) > 1 mg/l PNEC (Soil) PNEC soil 600 mg/kg dwt PNEC (STP) PNEC sewage treatment plant 95 mg/l 8.2. Exposure controls Appropriate engineering controls: Do not breathe dust. Provide local exhaust or general room ventilation. Provide adequate ventilation to minimize dust concentrations. Hand protection: Protective gloves Eye protection: Safety glasses Skin and body protection: Wear suitable protective clothing Respiratory protection: In case of insufficient ventilation, wear suitable respiratory equipment. Dust mask Environmental exposure controls: Avoid release to the environment. SECTION 9: Physical and chemical properties 9.1. Information on basic physical and chemical properties Physical state : Solid Colour : Grey. Odour : odourless. Odour threshold : No data available pH : 9 - 11 Relative evaporation rate (butylacetate=1) : No data available Melting point : 1414 C Freezing point : Not applicable Boiling point : 2900 C Flash point : Not applicable Auto-ignition temperature : Not applicable Decomposition temperature : No data available Flammability (solid, gas) : Non flammable Vapour pressure : No data available Relative vapour density at 20 C : No data available Relative density : Not applicable Density : 0.5-0.9g/cm Solubility : insoluble in water. Log Pow : No data available Viscosity, kinematic : No data available Viscosity, dynamic : No data available 3/23/2022 EN (English) 3/6 Appendix 6 Page 28 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 Explosive properties Oxidising properties Explosive limits 9.2. Other information No additional information available : No data available : No data available : Not applicable SECTION 10: Stability and reactivity 10.1. Reactivity The product is non-reactive under normal conditions of use, storage and transport. 10.2. Chemical stability Stable under normal conditions. 10.3. Possibility of hazardous reactions No dangerous reactions known under normal conditions of use. 10.4. Conditions to avoid Avoid creating or spreading dust. Incompatible materials. Moisture. 10.5. Incompatible materials Strong acids. Strong bases. 10.6. Hazardous decomposition products Under normal conditions of storage and use, hazardous decomposition products should not be produced. SECTION 11: Toxicological information 11.1. Information on toxicological effects Acute toxicity (oral) Acute toxicity (dermal) Acute toxicity (inhalation) : Not classified. : Not classified. : Not classified. Zeolites (1318-02-1) LD50 oral rat > 5110 mg/kg bodyweight LD50 dermal rabbit > 2000 mg/kg bodyweight LC50 inhalation rat (mg/l) Skin corrosion/irritation Serious eye damage/irritation Respiratory or skin sensitisation Germ cell mutagenicity Carcinogenicity > 3.35 mg/l/4h : Not classified : Not classified : Not classified : Not classified : NOAEL 60 mg/kg bw/day (nominal), no effects. Reproductive toxicity Zeolites (1318-02-1) NOAEL (male) STOT-single exposure STOT-repeated exposure Aspiration hazard : Not classified >= 2 : Not classified : Not classified : Not classified SECTION 12: Ecological information 12.1. Toxicity Ecology - general Acute aquatic toxicity Chronic aquatic toxicity : The product is not considered harmful to aquatic organisms nor to cause long-term adverse effects in the environment. : Not classified. : Not classified Zeolites (1318-02-1) NOEC fish EC50 Daphnia EC50 96h algae NOEC (chronic) NOEC chronic fish 680 mg/l Pimephales promelas 2808 mg/l (24h)-Daphnia magna 18 mg/l Desmodesmus subspicatus 32 mg/l (21d)-Daphnia magna > 86.7 mg/l (30d)-Pimephales promelas 3/23/2022 EN (English) 4/6 Appendix 6 Page 29 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 12.2. Persistence and degradability Zeolites (1318-02-1) Persistence and degradability 12.3. Bioaccumulative potential Zeolites (1318-02-1) Bioaccumulative potential 12.4. Mobility in soil Zeolites (1318-02-1) Ecology - soil 12.5. Results of PBT and vPvB assessment Component Zeolites (1318-02-1) 12.6. Other adverse effects No additional information available No information available. 0.59-0.95 No information available. This substance/mixture does not meet the PBT criteria of REACH regulation, annex XIII This substance/mixture does not meet the vPvB criteria of REACH regulation, annex XIII SECTION 13: Disposal considerations 13.1. Waste treatment methods Waste treatment methods Sewage disposal recommendations Product/Packaging disposal recommendations Ecology - waste materials : Dispose of contents/container in accordance with licensed collector's sorting instructions. : Disposal must be done according to official regulations. : Dispose in a safe manner in accordance with local/national regulations. : Avoid release to the environment. SECTION 14: Transport information In accordance with ADR / RID / IMDG / IATA / ADN ADR IMDG IATA 14.1. UN number Not regulated Not regulated Not regulated 14.2. UN proper shipping name Not regulated Not regulated Not regulated 14.3. Transport hazard class(es) Not regulated Not regulated Not regulated 14.4. Packing group Not regulated Not regulated Not regulated 14.5. Environmental hazards Not regulated Not regulated 14.6. Special precautions for user Overland transport Not regulated Not regulated Transport by sea Not regulated Air transport Not regulated Inland waterway transport Not regulated Rail transport Not regulated 14.7. Transport in bulk according to Annex II of Marpol and the IBC Code Not applicable ADN Not regulated Not regulated Not regulated Not regulated Not regulated RID Not regulated Not regulated Not regulated Not regulated Not regulated 3/23/2022 EN (English) 5/6 Appendix 6 Page 30 of 47 Molecular Sieve-type 4A Safety Data Sheet according to Regulation (EU) 2015/830 SECTION 15: Regulatory information 15.1. Safety, health and environmental regulations/legislation specific for the substance or mixture 15.1.1. EU-Regulations No REACH Annex XVII restrictions Zeolites is not on the REACH Candidate List Zeolites is not on the REACH Annex XIV List Zeolites is not subject to REGULATION (EU) No 649/2012 OF THE EUROPEAN PARLIAMENT AND OF THE COUNCIL of 4 July 2012 concerning the export and import of hazardous chemicals. Zeolites is not subject to Regulation (EC) No 850/2004 of the European Parliament and of the Council of 29 April 2004 on persistent organic pollutants and amending Directive 79/117/EEC 15.1.2. National regulations Listed on the AICS (Australian Inventory of Chemical Substances) Listed on IECSC (Inventory of Existing Chemical Substances Produced or Imported in China) Listed on the EEC inventory EINECS (European Inventory of Existing Commercial Chemical Substances) Listed on the Korean ECL (Existing Chemicals List) Listed on NZIoC (New Zealand Inventory of Chemicals) Listed on PICCS (Philippines Inventory of Chemicals and Chemical Substances) Listed on the TCSI (Taiwan Chemical Substance Inventory) Germany Reference to AwSV 12th Ordinance Implementing the Federal Immission Control Act - 12.BImSchV : Water hazard class (WGK) nwg, Non-hazardous to water (ID No. 805) : Is not subject of the 12. BlmSchV (Hazardous Incident Ordinance) Netherlands SZW-lijst van kankerverwekkende stoffen SZW-lijst van mutagene stoffen NIET-limitatieve lijst van voor de voortplanting giftige stoffen - Borstvoeding NIET-limitatieve lijst van voor de voortplanting giftige stoffen - Vruchtbaarheid NIET-limitatieve lijst van voor de voortplanting giftige stoffen - Ontwikkeling 15.2. Chemical safety assessment A chemical safety assessment has been carried out No chemical safety assessment has been carried out : The substance is not listed : The substance is not listed : The substance is not listed : The substance is not listed : The substance is not listed SECTION 16: Other information Abbreviations and acronyms: ADN European Agreement concerning the International Carriage of Dangerous Goods by Inland Waterways ADR European Agreement concerning the International Carriage of Dangerous Goods by Road IATA International Air Transport Association IMDG International Maritime Dangerous Goods RID Regulations concerning the International Carriage of Dangerous Goods by Rail EC50 Median effective concentration LC50 Median lethal concentration LD50 Data sources Training advice Median lethal dose : ECHA reference. Loli. : Normal use of this product shall imply use in accordance with the instructions on the packaging. SDS EU (REACH Annex II) This information is based on our current knowledge and is intended to describe the product for the purposes of health, safety and environmental requirements only. It should not therefore be construed as guaranteeing any specific property of the product. 3/23/2022 EN (English) 6/6 Appendix 6 Page 31 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 1 of 9 ______________________________________________________________________________________________________________________ SAFETY DATA SHEET SECTION 1 PRODUCT AND COMPANY IDENTIFICATION PRODUCT Product Name: SPECTRASYNTM 100 Product Description: Synthetic Base Stock Intended Use: Base oil COMPANY IDENTIFICATION Supplier: EXXONMOBIL CHEMICAL COMPANY SDS - LOC. 106 22777 Springwoods Village Parkway Spring, TX 77389-1425 USA 24 Hour Health Emergency (800) 726-2015 Transportation Emergency Phone (800) 424-9300 or (703) 527-3887 CHEMTREC Product Technical Information (832) 624-8500 Supplier General Contact (832) 624-8500 SECTION 2 HAZARDS IDENTIFICATION This material is not hazardous according to regulatory guidelines (see (M)SDS Section 15). Other hazard information: HAZARD NOT OTHERWISE CLASSIFIED (HNOC): None as defined under 29 CFR 1910.1200. PHYSICAL / CHEMICAL HAZARDS No significant hazards. HEALTH HAZARDS High-pressure injection under skin may cause serious damage. ENVIRONMENTAL HAZARDS No significant hazards. NFPA Hazard ID: HMIS Hazard ID: Health: 0 Health: 0 Flammability: 1 Flammability: 1 Reactivity: 0 Reactivity: 0 NOTE: This material should not be used for any other purpose than the intended use in Section 1 without expert advice. Health studies have shown that chemical exposure may cause potential human health risks which may vary from person to person. Appendix 6 Page 32 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 2 of 9 ______________________________________________________________________________________________________________________ SECTION 3 COMPOSITION / INFORMATION ON INGREDIENTS This material is defined as a mixture. No Hazardous Substance(s) or Complex Substance(s) required for disclosure. SECTION 4 FIRST AID MEASURES INHALATION Remove from further exposure. For those providing assistance, avoid exposure to yourself or others. Use adequate respiratory protection. If respiratory irritation, dizziness, nausea, or unconsciousness occurs, seek immediate medical assistance. If breathing has stopped, assist ventilation with a mechanical device or use mouth-to-mouth resuscitation. SKIN CONTACT Wash contact areas with soap and water. If product is injected into or under the skin, or into any part of the body, regardless of the appearance of the wound or its size, the individual should be evaluated immediately by a physician as a surgical emergency. Even though initial symptoms from high pressure injection may be minimal or absent, early surgical treatment within the first few hours may significantly reduce the ultimate extent of injury. EYE CONTACT Flush thoroughly with water. If irritation occurs, get medical assistance. INGESTION First aid is normally not required. Seek medical attention if discomfort occurs. SECTION 5 FIRE FIGHTING MEASURES EXTINGUISHING MEDIA Appropriate Extinguishing Media: flames. Use water fog, foam, dry chemical or carbon dioxide (CO2) to extinguish Inappropriate Extinguishing Media: Straight Streams of Water FIRE FIGHTING Fire Fighting Instructions: Evacuate area. Prevent runoff from fire control or dilution from entering streams, sewers, or drinking water supply. Firefighters should use standard protective equipment and in enclosed spaces, self-contained breathing apparatus (SCBA). Use water spray to cool fire exposed surfaces and to protect personnel. Hazardous Combustion Products: Oxides of carbon, Smoke, Fume FLAMMABILITY PROPERTIES Flash Point [Method]: >270C (518F) [ASTM D-93] Flammable Limits (Approximate volume % in air): LEL: N/D Autoignition Temperature: N/D UEL: N/D Appendix 6 Page 33 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 3 of 9 ______________________________________________________________________________________________________________________ SECTION 6 ACCIDENTAL RELEASE MEASURES NOTIFICATION PROCEDURES In the event of a spill or accidental release, notify relevant authorities in accordance with all applicable regulations. US regulations require reporting releases of this material to the environment which exceed the applicable reportable quantity or oil spills which could reach any waterway including intermittent dry creeks. The National Response Center can be reached at (800)424-8802. PROTECTIVE MEASURES Avoid contact with spilled material. See Section 5 for fire fighting information. See the Hazard Identification Section for Significant Hazards. See Section 4 for First Aid Advice. See Section 8 for advice on the minimum requirements for personal protective equipment. Additional protective measures may be necessary, depending on the specific circumstances and/or the expert judgment of the emergency responders. SPILL MANAGEMENT Land Spill: Stop leak if you can do it without risk. Absorb or cover with dry earth, sand or other noncombustible material and transfer to containers. Recover by pumping or with suitable absorbent. Water Spill: Stop leak if you can do it without risk. Confine the spill immediately with booms. Warn other shipping. Remove from the surface by skimming or with suitable absorbents. Seek the advice of a specialist before using dispersants. Water spill and land spill recommendations are based on the most likely spill scenario for this material; however, geographic conditions, wind, temperature, (and in the case of a water spill) wave and current direction and speed may greatly influence the appropriate action to be taken. For this reason, local experts should be consulted. Note: Local regulations may prescribe or limit action to be taken. ENVIRONMENTAL PRECAUTIONS Large Spills: Dike far ahead of liquid spill for later recovery and disposal. sewers, basements or confined areas. Prevent entry into waterways, SECTION 7 HANDLING AND STORAGE HANDLING Prevent small spills and leakage to avoid slip hazard. Material can accumulate static charges which may cause an electrical spark (ignition source). When the material is handled in bulk, an electrical spark could ignite any flammable vapors from liquids or residues that may be present (e.g., during switch-loading operations). Use proper bonding and/or ground procedures. However, bonding and grounds may not eliminate the hazard from static accumulation. Consult local applicable standards for guidance. Additional references include American Petroleum Institute 2003 (Protection Against Ignitions Arising out of Static, Lightning and Stray Currents) or National Fire Protection Agency 77 (Recommended Practice on Static Electricity) or CENELEC CLC/TR 50404 (Electrostatics - Code of practice for the avoidance of hazards due to static electricity). Static Accumulator: This material is a static accumulator. STORAGE The type of container used to store the material may affect static accumulation and dissipation. Do not store Appendix 6 Page 34 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 4 of 9 ______________________________________________________________________________________________________________________ in open or unlabelled containers. SECTION 8 EXPOSURE CONTROLS / PERSONAL PROTECTION Exposure limits/standards for materials that can be formed when handling this product: When mists/aerosols can occur the following are recommended: 5 mg/m - ACGIH TLV (inhalable fraction), 5 mg/m - OSHA PEL. NOTE: Limits/standards shown for guidance only. Follow applicable regulations. No biological limits allocated. ENGINEERING CONTROLS The level of protection and types of controls necessary will vary depending upon potential exposure conditions. Control measures to consider: No special requirements under ordinary conditions of use and with adequate ventilation. PERSONAL PROTECTION Personal protective equipment selections vary based on potential exposure conditions such as applications, handling practices, concentration and ventilation. Information on the selection of protective equipment for use with this material, as provided below, is based upon intended, normal usage. Respiratory Protection: If engineering controls do not maintain airborne contaminant concentrations at a level which is adequate to protect worker health, an approved respirator may be appropriate. Respirator selection, use, and maintenance must be in accordance with regulatory requirements, if applicable. Types of respirators to be considered for this material include: No protection is ordinarily required under normal conditions of use and with adequate ventilation. For high airborne concentrations, use an approved supplied-air respirator, operated in positive pressure mode. Supplied air respirators with an escape bottle may be appropriate when oxygen levels are inadequate, gas/vapor warning properties are poor, or if air purifying filter capacity/rating may be exceeded. Hand Protection: Any specific glove information provided is based on published literature and glove manufacturer data. Glove suitability and breakthrough time will differ depending on the specific use conditions. Contact the glove manufacturer for specific advice on glove selection and breakthrough times for your use conditions. Inspect and replace worn or damaged gloves. The types of gloves to be considered for this material include: No protection is ordinarily required under normal conditions of use. Eye Protection: If contact is likely, safety glasses with side shields are recommended. Skin and Body Protection: Any specific clothing information provided is based on published literature or manufacturer data. The types of clothing to be considered for this material include: No skin protection is ordinarily required under normal conditions of use. In accordance with good industrial hygiene practices, precautions should be taken to avoid skin contact. Appendix 6 Page 35 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 5 of 9 ______________________________________________________________________________________________________________________ Specific Hygiene Measures: Always observe good personal hygiene measures, such as washing after handling the material and before eating, drinking, and/or smoking. Routinely wash work clothing and protective equipment to remove contaminants. Discard contaminated clothing and footwear that cannot be cleaned. Practice good housekeeping. ENVIRONMENTAL CONTROLS Comply with applicable environmental regulations limiting discharge to air, water and soil. Protect the environment by applying appropriate control measures to prevent or limit emissions. SECTION 9 PHYSICAL AND CHEMICAL PROPERTIES Note: Physical and chemical properties are provided for safety, health and environmental considerations only and may not fully represent product specifications. Contact the Supplier for additional information. GENERAL INFORMATION Physical State: Form: Clear Color: Colorless Odor: Odorless Odor Threshold: Liquid N/D IMPORTANT HEALTH, SAFETY, AND ENVIRONMENTAL INFORMATION Relative Density (at 15 C): 0.85 [In-house method] Flammability (Solid, Gas): N/A Flash Point [Method]: >270C (518F) [ASTM D-93] Flammable Limits (Approximate volume % in air): LEL: N/D UEL: N/D Autoignition Temperature: N/D Boiling Point / Range: N/D Decomposition Temperature: N/D Vapor Density (Air = 1): N/D Vapor Pressure: < 0.013 kPa (0.1 mm Hg) at 20 C [In-house method] Evaporation Rate (n-butyl acetate = 1): N/D pH: N/A Log Pow (n-Octanol/Water Partition Coefficient): N/D Solubility in Water: Negligible Viscosity: 1284 cSt (1284 mm2/sec) at 40 C | 102 cSt (102 mm2/sec) at Oxidizing Properties: See Hazards Identification Section. 100C [In-house method] OTHER INFORMATION Freezing Point: N/D Melting Point: N/D Pour Point: < -20C (-4F) [In-house method] SECTION 10 STABILITY AND REACTIVITY REACTIVITY: See sub-sections below. STABILITY: Material is stable under normal conditions. Appendix 6 Page 36 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 6 of 9 ______________________________________________________________________________________________________________________ CONDITIONS TO AVOID: Excessive heat. High energy sources of ignition. MATERIALS TO AVOID: Strong oxidizers HAZARDOUS DECOMPOSITION PRODUCTS: Material does not decompose at ambient temperatures. POSSIBILITY OF HAZARDOUS REACTIONS: Hazardous polymerization will not occur. SECTION 11 TOXICOLOGICAL INFORMATION INFORMATION ON TOXICOLOGICAL EFFECTS Hazard Class Inhalation Acute Toxicity: (Rat) 4 hour(s) LC50 > 5200 mg/m3 (Aerosol) Irritation: No end point data for material. Ingestion Acute Toxicity (Rat): LD50 > 5000 mg/kg Skin Acute Toxicity (Rabbit): LD50 > 2000 mg/kg Skin Corrosion/Irritation (Rabbit): Data available. Eye Serious Eye Damage/Irritation (Rabbit): Data available. Sensitization Respiratory Sensitization: No end point data for material. Skin Sensitization: Data available. Aspiration: Data available. Germ Cell Mutagenicity: Data available. Carcinogenicity: No end point data for material. Reproductive Toxicity: Data available. Lactation: No end point data for material. Specific Target Organ Toxicity (STOT) Single Exposure: No end point data for material. Repeated Exposure: Data available. Conclusion / Remarks Minimally Toxic. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 403 Negligible hazard at ambient/normal handling temperatures. Minimally Toxic. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 401 423 Minimally Toxic. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 402 Negligible irritation to skin at ambient temperatures. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 404 May cause mild, short-lasting discomfort to eyes. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 405 Not expected to be a respiratory sensitizer. Not expected to be a skin sensitizer. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 406 Not expected to be an aspiration hazard. Based on physicochemical properties of the material. Not expected to be a germ cell mutagen. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 471 473 474 476 Not expected to cause cancer. Not expected to be a reproductive toxicant. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 415 Not expected to cause harm to breast-fed children. Not expected to cause organ damage from a single exposure. Not expected to cause organ damage from prolonged or repeated exposure. Based on test data for structurally similar materials. Test(s) equivalent or similar to OECD Guideline 407 408 Appendix 6 Page 37 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 7 of 9 ______________________________________________________________________________________________________________________ OTHER INFORMATION For the product itself: Synthetic base oils: Not expected to cause significant health effects under conditions of normal use, based on laboratory studies with the same or similar materials. Not mutagenic or genotoxic. Not sensitizing in test animals and humans. The following ingredients are cited on the lists below: None. 1 = NTP CARC 2 = NTP SUS --REGULATORY LISTS SEARCHED-- 3 = IARC 1 5 = IARC 2B 4 = IARC 2A 6 = OSHA CARC SECTION 12 ECOLOGICAL INFORMATION The information given is based on data available for the material, the components of the material, and similar materials. ECOTOXICITY Material -- Not expected to be harmful to aquatic organisms. PERSISTENCE AND DEGRADABILITY Biodegradation: Material -- Expected to biodegrade slowly. SECTION 13 DISPOSAL CONSIDERATIONS Disposal recommendations based on material as supplied. Disposal must be in accordance with current applicable laws and regulations, and material characteristics at time of disposal. DISPOSAL RECOMMENDATIONS Product is suitable for burning in an enclosed controlled burner for fuel value or disposal by supervised incineration at very high temperatures to prevent formation of undesirable combustion products. REGULATORY DISPOSAL INFORMATION RCRA Information: The unused product, in our opinion, is not specifically listed by the EPA as a hazardous waste (40 CFR, Part 261D), nor is it formulated to contain materials which are listed as hazardous wastes. It does not exhibit the hazardous characteristics of ignitability, corrositivity or reactivity and is not formulated with Appendix 6 Page 38 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 8 of 9 ______________________________________________________________________________________________________________________ contaminants as determined by the Toxicity Characteristic Leaching Procedure (TCLP). However, used product may be regulated. Empty Container Warning Empty Container Warning (where applicable): Empty containers may contain residue and can be dangerous. Do not attempt to refill or clean containers without proper instructions. Empty drums should be completely drained and safely stored until appropriately reconditioned or disposed. Empty containers should be taken for recycling, recovery, or disposal through suitably qualified or licensed contractor and in accordance with governmental regulations. DO NOT PRESSURISE, CUT, WELD, BRAZE, SOLDER, DRILL, GRIND, OR EXPOSE SUCH CONTAINERS TO HEAT, FLAME, SPARKS, STATIC ELECTRICITY, OR OTHER SOURCES OF IGNITION. THEY MAY EXPLODE AND CAUSE INJURY OR DEATH. SECTION 14 TRANSPORT INFORMATION LAND (DOT): Not Regulated for Land Transport LAND (TDG): Not Regulated for Land Transport SEA (IMDG): Not Regulated for Sea Transport according to IMDG-Code Marine Pollutant: No SEA (MARPOL 73/78 Convention - Annex II) Product Name: POLYOLEFIN (MOLECULAR WEIGHT 300+) Ship type: 2 Pollution category: Y AIR (IATA): Not Regulated for Air Transport SECTION 15 REGULATORY INFORMATION OSHA HAZARD COMMUNICATION STANDARD: OSHA HazCom 2012, 29 CFR 1910.1200. This material is not considered hazardous in accordance with Listed or exempt from listing/notification on the following chemical inventories: KECI, PICCS, TSCA AICS, DSL, ENCS, IECSC, SARA 302: No chemicals in this material are subject to the reporting requirements of SARA Title III, Section 302 SARA (311/312) REPORTABLE GHS HAZARD CLASSES: None. SARA (313) TOXIC RELEASE INVENTORY: This material contains no chemicals subject to the supplier notification requirements of the SARA 313 Toxic Release Program. The following ingredients are cited on the lists below: None. Appendix 6 Page 39 of 47 Product Name: SPECTRASYNTM 100 Revision Date: 30 Mar 2018 Page 9 of 9 ______________________________________________________________________________________________________________________ 1 = ACGIH ALL 2 = ACGIH A1 3 = ACGIH A2 4 = OSHA Z 5 = TSCA 4 --REGULATORY LISTS SEARCHED-- 6 = TSCA 5a2 11 = CA P65 REPRO 7 = TSCA 5e 12 = CA RTK 8 = TSCA 6 13 = IL RTK 9 = TSCA 12b 14 = LA RTK 10 = CA P65 CARC 15 = MI 293 Code key: CARC=Carcinogen; REPRO=Reproductive SECTION 16 OTHER INFORMATION 16 = MN RTK 17 = NJ RTK 18 = PA RTK 19 = RI RTK N/D = Not determined, N/A = Not applicable THIS SAFETY DATA SHEET CONTAINS THE FOLLOWING REVISIONS: Section 01: Company Mailing Address information was deleted. Section 01: Company Mailing Address information was modified. Section 01: Product Identification Product Name information was modified. Section 07: Handling and Storage - Handling information was modified. Section 07: Handling and Storage - Storage Phrases information was modified. Section 14: IMO ANNEX II Ship Type - Header information was modified. Section 15: SARA (311/312) REPORTABLE GHS HAZARD CLASSES information was added. Section 15: SARA (311/312) REPORTABLE HAZARD CATEGORIES information was deleted. ----------------------------------------------------------------------------------------------------------------------------------------------------The information and recommendations contained herein are, to the best of ExxonMobil's knowledge and belief, accurate and reliable as of the date issued. You can contact ExxonMobil to insure that this document is the most current available from ExxonMobil. The information and recommendations are offered for the user's consideration and examination. It is the user's responsibility to satisfy itself that the product is suitable for the intended use. If buyer repackages this product, it is the user's responsibility to insure proper health, safety and other necessary information is included with and/or on the container. Appropriate warnings and safe-handling procedures should be provided to handlers and users. Alteration of this document is strictly prohibited. Except to the extent required by law, republication or retransmission of this document, in whole or in part, is not permitted. The term, "ExxonMobil" is used for convenience, and may include any one or more of ExxonMobil Chemical Company, Exxon Mobil Corporation, or any affiliates in which they directly or indirectly hold any interest. ----------------------------------------------------------------------------------------------------------------------------------------------------- Internal Use Only MHC: 0, 0, 0, 0, 0, 0 DGN: 2030728CUS (554326) PPEC: A ----------------------------------------------------------------------------------------------------------------------------------------------------Copyright 2002 Exxon Mobil Corporation, All rights reserved Appendix 6 Page 40 of 47 DRUMS 4 AND 5 INFORMATION Appendix 6 Page 41 of 47 Appendix 6 Page 42 of 47 TOTE INFORMATION Safety Data Sheet SECTION 1. Product identifier/Name: Synonyms Product Use: Manufactured by: Emergency Number: SECTION 2. GHS Classification PRODUCT AND COMPANY Vinegar White Distilled Vinegar (120 to 300 Grain / 12% to 30%), White Distilled Vinegar - Organic (120 to 300 Grain / 12% to 30%), White Distilled Vinegar IP Non GMO (120 to 300 Grain / 12% to 30%), Vinaigre Blanc (120 to 300 Grain / 12% to 30%), Crystal Select Vinegar (120 to 300 Grain / 12% to 30%), WaterWhite Vinegar (120 to 300 Grain / 12% to 30%) Food Fleischmann's Vinegar Company, Inc. 12604 Hiddencreek Way, Suite A Cerritos, CA 90703 USA Telephone: (562) 483-4600 CHEMTREC: 1-(800) 424-9300 or 011-(703)527-3887 HAZARDS IDENTIFICATION Skin Corrosive 2, Eye Irritant 2A, Hazardous to aquatic environment WARNING Hazard Statements H320: Causes eye irritation H315: Causes skin irritation H332: Harmful if inhaled H402: Harmful to aquatic life Precautionary Statements P261: Avoid breathing fumes/mist/vapors/spray P264: Wash exposed skin thoroughly after handling. P280: Wear protective gloves to avoid prolonged exposure. P304+P340: IF INHALED: Remove person to fresh air and keep comfortable for breathing. P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. P273: Avoid release into the environment Appendix 6 Page 43 of 47 SECTION 3. Chemical name Acetic acid Water SECTION 4. Eye contact Skin contact Inhalation COMPOSITION /INFORMATION ON INGREDIENTS Concentration 10% - 30% 70% - 90% CAS 64-19-7 7732-18-5 FIRST-AID MEASURES Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Immediately call a POISON CENTER Iofrodnoscktionr;/wphaysshicwiainth. plenty of soap and water. If skin irritation occurs, seek medical advice/attention. If on clothes; remove/take off all contaminated clothing. Rinse skin with soap and water. Remove to fresh air and keep in position comfortable for breathing. Ingestion Intended for ingestion, however if swallowed in large quantities, water may be consumed to dilute. Rinse mouth. Do NOT induce vomiting. Immediately call a POISON CENTER or doctor/physician. SECTION 5. FIREFIGHTING MEASURES Extinguishing media N/A Specific Hazards N/A Special Fire Fighting Methods N/A SECTION 6. ACCIDENTAL RELEASE MEASURES Personal precautions, protective equipment and emergency procedures Protect skin and eyes from exposure. Avoid breathing vapor LARGE SPILLS PROCEDURE: Contain spilled material. Large spills may be neutralized with dilute alkaline solutions of soda ash or lime. Avoid runoff into storm sewers and ditches that lead to waterways. Treat or dispose of waste material as a weak acid in accordance with all local, state/provincial, and national requirements. SMALL SPILLS PROCEDURE: Water may be used to dilute. Treat or dispose of waste material as a weak acid in accordance with all local, state/provincial and national requirements. Environmental Precautions Prevent entry to sewers and public waters. Notify authorities if liquid enters sewers or public waters. Appendix 6 Page 44 of 47 SECTION 7. HANDLING AND STORAGE Precautions for safe handling Provide good ventilation to prevent formation of vapor. Avoid breathing vapors, contact with eyes, skin and clothing. Conditions for safe storage, Keep container closed when not in use. including any iInnccoommppaattiibbilleitpiersoducts Strong oxidizers, metals, strong bases. SECTION 8. EXPOSURE CONTROL/PERSONAL PROTECTION Chemical Name Acetic Acid ACGIH TWA STEL 10ppm 15ppm OSHA PEL TWA STEL 10ppm; N/A 25mg/m3 IDLH 50ppm 125mg/m3 Appropriate engineering controls: Hand protection: Eye protection: Skin and body protection: Respiratory protection: Emergency eye wash stations should be available in the immediate vicinity. General room ventilation should be maintained for operator comfort. Rubber gloves should be worn to avoid prolonged exposure Chemical goggles or face shield. General clothing is adequate Wear NIOSH/MSHA approved respiratory protection in enclosed areas SECTION 9. PHYSICAL AND CHEMICAL PROPERTIES Physical state: Liquid Odor: Strong Vinegar Odor threshold: No data available pH: 2.1 - 2.8 Melting point: Vinegar @ 30F (Acetic Acid @ 62F) Boiling point: 215F @ 760 mm Hg and 100 grain Flash point: N/A Evaporation rate: No data available Flammability (solid, gas): N/A Upper/Lower Explosive Limit N/A Vapor pressure: 1.4 mm Hg @ 300 grain and 70F Relative vapor density at 20 2.1 (Air = 1) C: Relative density: No data available Density: 1.01 to 1.04 (water = 1) Solubility: Complete Appendix 6 Page 45 of 47 SECTION 9. PHYSICAL AND CHEMICAL PROPERTIES Partition coefficient No data available Auto-ignition Temperature No data available Decomposition Temperature No data available Viscosity No data available SECTION 10. STABILITY AND REACTIVITY Reactivity Chemical stability Possibility of hazardous reactions Incompatible materials Hazardous decomposition products No data available Stable under normal conditions Contact with strong oxidizing agents or strong bases may result in the release of heat. Water reactive materials, acetic anhydride, caustics, oxidizing materials, carbonates Carbon dioxide. Thermal decomposition may generate corrosive vapors. SECTION 11. TOXICOLOGICAL INFORMATION Routes of entry Symptoms (acute) Delayed effects Inhalation, ingestion and skin contact Respiratory irritation No data available Acute Toxicity: Chemical name Water Acetic Acid CAS 7732-18-5 64-19-7 Oral LD50 Rat 90000mg/kg Dermal LD50 Inhalation LC50 Mouse 5620ppm Carcinogenicity Mutagenicity Teratogenicity Sensitization Reproductive No evidence of a carcinogenic effect No evidence of a mutagenicity effect No evidence of a teratogenicity effect No evidence of a sensitization effect No evidence of a Reproductive effect SECTION 12. ECOLOGICAL INFORMATION Overview Persistence Bioaccumulation Mobility in soil This material is not expected to be harmful to the environment Biodegradation No data No data Appendix 6 Page 46 of 47 Other adverse effects No data SECTION 12. Chemical name Water Acetic Acid ECOLOGICAL INFORMATION CAS Ecotoxcity 7732-18-5 No data available 64-19-7 Aquatic LC50 (96h) Fathead Minnow 79mg/l Aquatic EC50 (24h) Daphnia 47mg/l Section 13. DISPOSAL CONSIDERATIONS Waste disposal recommendations: Dispose in accordance with local, state/provincial , and national requirements SECTION 14. TRANSPORT INFORMATION Transportation of Fleischmann's Vinegar's products covered by this SDS are subject to conditions set forth in Special Permit DOT-SP 16198. Specifically, the SP provides that "food grade" (as defined by the FDA) bulk vinegar with up to 30% acetic acid that meets the exemption conditions stated in the SP will not be a 49 CFR 171.8 hazardous substance. Additional guidance can be found in SP DOT-SP 16198 or by contacting Fleischmann's Vinegar. * DOT-SP 16198 is solely applicable to Fleischmann's Vinegar's products and transporters of those products. SECTION 15. Chemical name Acetic Acid SECTION 16. Issue Date: Prepared by: REGULATORY INFORMATION CAS 64-19-7 Section 313 no Section 304 RQ 5000lb CERCLA RQ 5000lb Section 302 TPQ no CAA 112 (2) no OTHER INFORMATION 7/31/2015 Fleischmann's Vinegar Company Appendix 6 Page 47 of 47 APPENDIX 7. SWS HAZARDOUS WASTE TRANSFER MANIFESTS FROM APRIL 2024 Appendix 7 Page 1 of 35 Appendix 7 Page 2 of 35 Appendix 7 Page 3 of 35 Appendix 7 Page 4 of 35 Appendix 7 Page 5 of 35 Appendix 7 Page 6 of 35 Appendix 7 Page 7 of 35 Appendix 7 Page 8 of 35 Appendix 7 Page 9 of 35 Appendix 7 Page 10 of 35 Appendix 7 Page 11 of 35 Appendix 7 Page 12 of 35 Appendix 7 Page 13 of 35 Appendix 7 Page 14 of 35 Appendix 7 Page 15 of 35 Appendix 7 Page 16 of 35 Appendix 7 Page 17 of 35 Appendix 7 Page 18 of 35 Appendix 7 Page 19 of 35 Appendix 7 Page 20 of 35 Appendix 7 Page 21 of 35 Appendix 7 Page 22 of 35 Appendix 7 Page 23 of 35 Appendix 7 Page 24 of 35 Appendix 7 Page 25 of 35 Appendix 7 Page 26 of 35 Appendix 7 Page 27 of 35 Appendix 7 Page 28 of 35 Appendix 7 Page 29 of 35 Appendix 7 Page 30 of 35 Appendix 7 Page 31 of 35 Appendix 7 Page 32 of 35 Appendix 7 Page 33 of 35 Appendix 7 Page 34 of 35 Appendix 7 Page 35 of 35 APPENDIX 8. SWS CONFIRMATION OF MARPOL COA STATUS MARPOL Certificate of Adequacy through the USCG if applicable. We are not and approved USCG facility for MARPOL Annex I, II, or V, but we are approved by the USCG as a mobile transfer facility. Appendix 8 Page 1 of 1 APPENDIX 9. SWS WASHOUT CONTAINER INVENTORY FEB, MAR, APR 2024 EQUIPMENT# 20649 VB0725113 RT2225038 RB21525 R250334 HOSES DVB568 RBM RT251190 RT250617 VAC253061 VAC259155 RB31454ML RBM250456 RB35057ML VB2540 VB2544 RBM250705 RBM250463 V250391 VB2225048 RT251530 2954 V251118 V250460 36 2777 7173 7231 23453 RT251725 V250745 RT250735 RT251664 5075 1426 VAC253049 V250149 V250170 RBM250401 RBM250489 2979 RBM250770 RBM250563 RT251965 R250237 2980 RBM250703 RBM250603 1828 2954 20 2777 DATE IN 2/1/2024 1/30/2024 1/31/2024 2/1/2024 2/1/2024 1/30/2024 1/15/2024 2/1/2024 2/1/2024 2/1/2024 1/11/2024 1/12/2024 1/29/2024 1/29/2024 1/29/2024 1/30/2024 1/30/2024 2/1/2024 1/29/2024 1/30/2024 1/30/2024 2/1/2024 2/1/2024 1/11/2024 1/30/2024 2/1/2024 2/1/2024 1/31/2024 2/1/2024 2/1/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/1/2024 2/2/2024 1/30/2024 2/2/2024 2/1/2024 1/31/2024 1/30/2024 1/29/2024 1/30/2024 2/1/2024 2/1/2024 1/30/2024 1/30/2024 1/31/2024 1/29/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 DATE WASHED 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/3/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/3/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/1/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 Appendix 9 Page 1 of 44 BILLED TO LEL REPUBLIC REPUBLIC DOW WM AEIS SCS CLEAN HARBORS SPRINT SPRINT CIMA CIMA CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CIMA CIMA CLEAN HARBORS CLEAN HARBORS SPRINT REPUBLIC SPRINT PCI SPRINT SPRINT CIMA PCI CENTERPOINT CENTERPOINT EEW SPRINT SPRINT SPRINT SPRINT SCS SET CIMA SPRINT SPRINT CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS WM CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS SOLENIS PCI TAS PCI WASH TKT # 128863 129057 129145 129202 129206 129084 137576 129184 129203 129214 137522 137550 129368 129370 129371 129080 129083 129198 129374 129079 129056 129179 129201 137508 129087 128868 129180 129129 129199 129178 128897 128886 128916 128898 129205 128881 129069 128890 129209 129148 129397 129388 129394 129183 128867 129395 129396 129174 129375 128903 128907 128888 128909 EQUIPMENT# T132 310 2777 5115 5017 T562 RBR250850 R250093 R250125 R250034 CHIU258657 CHIU258633 CHIU258731 1409 CHHA25122 CHHS25036 CHIU258740 CHHA25154 CHIU258749 CHIU258751 RBM250088 CHIU258268 HT2571 CHIU258645 CHHA25115 RBM250500 CHHS25018 CHIU258739 CHIU258738 CHIU258758 CHHS25010 CHIU258746 CHIU258706 FRC501082 DW2 20768 SLD255387 VB2515 RT2568 LT1007 RB2125242 RB0025032 RT2125058 RT2225027 GF6019 SLD251447 RBR250860 ZIPU106982-4 1832 RT252052 RT251460 RT251425 RT251194 DATE IN 2/2/2024 2/2/2024 2/3/2024 1/30/2024 1/23/2024 1/26/2024 1/31/2024 1/31/2024 1/31/2024 2/1/2024 2/2/2024 2/1/2024 2/1/2024 1/31/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 2/1/2024 1/31/2024 2/2/2024 1/31/2024 2/1/2024 2/1/2024 1/31/2024 2/1/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/1/2024 2/1/2024 1/24/2024 2/2/2024 2/2/2024 1/31/2024 2/2/2024 2/2/2024 2/2/2024 1/31/2024 1/31/2024 1/31/2024 1/30/2024 2/2/2024 2/2/2024 1/26/2024 1/26/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 DATE WASHED 2/2/2024 2/2/2024 2/3/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/2/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 Appendix 9 Page 2 of 44 BILLED TO SET NRG PCI SCS SCS AMERICAN ACRYL DOW WM WM WM CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS WM CIMA LEL CIMA CIMA CIMA KURARAY REPUBLIC REPUBLIC REPUBLIC REPUBLIC NRG INTERGULF IRONCLAD THIRD COAST CAMIN CARGO SPRINT SPRINT SPRINT SPRINT WASH TKT # 128884 128910 128921 129093 129404 129287 129163 129170 129172 129200 128919 129211 129191 129166 129197 129196 129195 129208 129189 129190 129117 128918 129137 128873 129188 129167 129192 128895 128878 128883 128882 129213 129193 129225 128875 128877 129177 128900 128920 128891 129159 129158 129160 129066 128915 128906 129320 129337 128927 128937 128938 128930 128942 EQUIPMENT# 1833 1830 RT251992 R250171 TA172 1828 1832 N35034 RT253 DVC250566 29 RB20026 DWRT2534 DSC250327 LR1111 PT1065 RBR2520211 RBR250230 VT4036 VT4012 SLD252907 DVB2125016 RT2125076 DVB2225078 SLD259677 RT251013 RT252508 RT250136 RT250567 RT250481 RB0025048 RBM250674 CHHS25045 VB2539 VB2545 VB2537 SLD251886 SLD259060 14305 RT251345 RT250829 RT251831 PT1035 HOSE T003 PT1030 1830 1832 1833 1828 6027 2954 RT251661 DATE IN 2/5/2024 2/5/2024 2/2/2024 2/1/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 1/31/2024 2/2/2024 2/5/2024 2/1/2024 2/1/2024 1/31/2024 2/5/2024 1/26/2024 1/26/2024 2/2/2024 2/1/2024 2/5/2024 1/31/2024 2/1/2024 1/31/2024 2/5/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 1/31/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/5/2024 2/5/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/5/2024 2/3/2024 2/6/2024 2/7/2024 2/6/2024 2/6/2024 2/6/2024 2/2/2024 2/7/2024 2/6/2024 DATE WASHED 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/5/2024 2/6/2024 2/7/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/7/2024 2/6/2024 2/6/2024 2/6/2024 2/2/2024 2/7/2024 2/6/2024 Appendix 9 Page 3 of 44 BILLED TO NRG INTERGULF SPRINT WM SET THIRD COAST NRG CIMA CIMA CIMA CIMA CIMA CIMA CIMA CIMA LION IRONCLAD IRONCLAD SCS SCS INTERGULF REPUBLIC REPUBLIC REPUBLIC SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT REPUBLIC CLEAN HARBORS CLEAN HARBORS CIMA CIMA CIMA CIMA CIMA CLEAN HARBORS SPRINT SPRINT SPRINT LION AEIS SES LION TAS INTERGULF INTERGULF THIRD COAST NRG PCI SPRINT WASH TKT # 128960 128962 128917 128870 128934 128932 128941 128951 128953 129151 128905 128955 128872 128869 129144 129128 129343 129342 128885 128864 128950 129153 128865 129122 128943 129003 128974 128964 129005 128981 129000 129165 129008 128983 128980 128997 128946 128935 128977 128994 128979 128975 128991 128933 128924 128963 129013 128996 128999 128985 134528 129014 128995 EQUIPMENT# RT250579 RT2525 N49132 F06083 FT21008 A5285C FRC589140 MT7055LG BERM BERM BERM BERM 1436 2853 2954 2777 RB21180 FRC502095 RBM250555 RT250692 1832 1830 T76 2954 1828 T023 VB2512 CHHS25007 CHHA25001 D425 D322 CHIU258655 RB22060 37 RT250998 RT250759 RT251216 RT250819 V251088 DVC259063 DVC259042 CHIU258760 5135 VAC259159 VAC252126 VAC259027 SLD259289 VAC253051 R250185 RT1342 RB21354 145 RT NEG AIR BOX / HOSES DATE IN 2/5/2024 2/5/2024 1/30/2024 1/30/2024 1/30/2024 1/30/2024 1/25/2024 1/26/2024 1/30/2024 1/30/2024 1/30/2024 1/30/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 1/26/2024 1/26/2024 1/31/2024 2/6/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/6/2024 2/6/2024 2/6/2024 2/7/2024 2/7/2024 2/2/2024 1/26/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/5/2024 1/31/2024 1/31/2024 2/6/2024 2/6/2024 1/26/2024 1/23/2024 1/26/2024 2/7/2024 1/29/2024 2/7/2024 1/26/2024 1/26/2024 1/30/2024 2/7/2024 DATE WASHED 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/2/2024 2/2/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/6/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 Appendix 9 Page 4 of 44 BILLED TO SPRINT CIMA DOW DOW DOW DOW WM MAVIRO DOW DOW DOW DOW SET PCI PCI PCI IRONCLAD WM CLEAN HARBORS SPRINT NOV INTERGULF SET PCI THIRD COAST SES CIMA CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS IRONCLAD CIMA SPRINT SPRINT SPRINT SPRINT SPRINT CIMA CIMA CLEAN HARBORS SCS STOLTHAVEN STOLTHAVEN STOLTHAVEN WM STOLTHAVEN WM IRONCLAD IRONCLAD SET SET WASH TKT # 128956 128961 129058 129089 129059 129088 129277 129309 129090 134531 134530 134529 129006 128971 128966 129004 129310 129341 129173 128982 129048 129038 129031 129037 129028 129022 129012 128988 128989 129019 129030 128896 129346 129018 129023 129024 129033 129034 128928 129121 129150 129007 128993 129238 137640 129297 129025 129355 129041 129312 129313 129097 129029 EQUIPMENT# 5011 RB1825068 RB2125210 7253 7146 4 7110 7268 6168 25RT-167 RB0025037 RB0025051 RB2125312 RB2125201 RT2125089 25RT-126 RB2125160 SLD250037 RT250502 V250819 V251022 SLD259197 SLD251007 2777 20 1832 VTR-05 1830 1828 1824 30 VAC250032 23 CHHT25011 CHIU258759 CHIU258627 CHIU258745 RB31155ML RB29884ML RB31109ML CHIU258726 CHIU258763 CHIU258750 VAC250317 FRC502104 FRC588072 PT1055 R250095 R250313 5175 5129 5125 VT4047 DATE IN 1/24/2024 2/6/2024 2/6/2024 2/7/2024 2/6/2024 2/6/2024 2/5/2024 2/5/2024 2/7/2024 2/6/2024 2/7/2024 2/7/2024 2/7/2024 2/6/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/9/2024 2/9/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/9/2024 1/23/2024 2/8/2024 2/5/2024 2/5/2024 2/5/2024 2/6/2024 1/29/2024 2/1/2024 1/30/2024 2/5/2024 2/5/2024 2/5/2024 1/23/2024 1/25/2024 1/26/2024 2/8/2024 2/8/2024 2/8/2024 2/6/2024 2/6/2024 1/31/2024 2/2/2024 DATE WASHED 2/8/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/7/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/9/2024 2/9/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/9/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/6/2024 2/8/2024 2/6/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/6/2024 2/6/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/6/2024 Appendix 9 Page 5 of 44 BILLED TO SCS REPUBLIC REPUBLIC CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC INTERGULF SPRINT SPRINT SPRINT SPRINT SPRINT PCI TAS INTERGULF CENTERPOINT SULZER TURBO THIRD COAST CAMIN CARGO CIMA CIMA CIMA CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS STOLTHAVEN WM WM LION WM WM SCS SCS SCS SCS WASH TKT # 129222 129010 128986 129047 129002 128978 128947 128944 129026 128987 129016 129021 129039 128970 129020 129032 129046 129035 128677 128679 128681 128690 128691 128698 128695 128685 128689 128666 128670 128674 128696 129425 128693 128957 128929 128959 128973 129369 129182 129071 129194 128931 128939 137638 129276 129300 129049 128692 128694 128967 134526 129125 128908 EQUIPMENT# TA172 SCP258972 25230310 SCP258430 25230314 RT251285 T532 CHIU258764 RB0025026 DVB1925002 T022 7178 RT250841 V250343 V250906 1833 1832 VB2528 VAC253296 2954 LT1007 T171 1409 20724 1828 20618 HXS300 VB2564 VB2524 VAC259036 V251156 RT251672 RT250549 V250003 RT250937 RT250888 SLD253697 CHVT0870 CHIU258745 RBM250596 25 16 SCRUBBERS DRT2509 RBR250368 RBR251391 RT2125079 RB0625176 RT2225031 RT2125027 101 54 HOSES 54 HOSES RB21169 DATE IN 2/8/2024 1/31/2024 1/31/2024 1/31/2024 1/31/2024 2/8/2024 2/2/2024 2/6/2024 2/8/2024 1/30/2024 2/9/2024 2/9/2024 2/9/2024 2/8/2024 2/8/2024 2/9/2024 2/9/2024 1/8/2024 1/22/2024 2/10/2024 2/8/2024 2/9/2024 2/9/2024 2/10/2024 2/9/2024 2/10/2024 2/9/2024 1/11/2024 1/15/2024 1/23/2024 2/2/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/8/2024 2/1/2024 1/31/2024 2/9/2024 2/5/2024 1/31/2024 1/31/2024 2/2/2024 2/6/2024 2/2/2024 2/1/2024 2/6/2024 2/9/2024 2/5/2024 1/31/2024 2/2/2024 DATE WASHED 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/8/2024 2/7/2024 2/8/2024 2/8/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/10/2024 2/9/2024 2/9/2024 2/9/2024 2/10/2024 2/9/2024 2/10/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/2/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/8/2024 2/1/2024 2/1/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/9/2024 2/1/2024 2/9/2024 2/9/2024 2/6/2024 2/6/2024 2/5/2024 Appendix 9 Page 6 of 44 BILLED TO SET DOW DOW DOW DOW ADVARIO AMERICAN ACRYL CLEAN HARBORS REPUBLIC REPUBLIC SES CENTERPOINT SPRINT SPRINT SPRINT INTERGULF INTERGULF CIMA CIMA PCI KURARAY AMERICA SET SET LEL THIRD COAST LEL CLEAN HARBORS CIMA CIMA CIMA SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CIMA VAPOR POINT DOW DOW DOW REPUBLIC REPUBLIC REPUBLIC REPUBLIC LIQUID POWER 220 MAXBOX SET WASH TKT # 128675 134536 134537 134538 129168 128678 128904 128972 129051 129065 128699 128719 128700 128682 128680 128739 128731 137824 128443 128740 128667 128710 128725 128742 128738 128741 128697 137521 137573 129423 128887 128730 128717 128714 128734 128733 128701 129052 128874 129140 128736 128952 129171 129143 128879 129011 128876 128866 128969 128737 128954 129157 128893 EQUIPMENT# RBR250850 23 VAC250996 VB2510 VB8025 VB8017 VB8034 VB8003 VB8039 VB8019 7233 6156 7172 6080 5148 VT401 310 VTR05 1833 HOSES/FITTINGS RBR2520640 5101 V250226 VB1925240 5035 5163 4130 RB21212 VAC259029 VB2518 VB2556 RT251810 1828 2954 ML25453 TA172 1426 HOSE PT036 29 7268 1831 6125 6126 36 T002 R250353 WM NO# VT5902 VT5253 PT1055 RT2547 RBR250199 DATE IN 1/31/2024 2/12/2024 1/23/2024 1/26/2024 1/30/2024 1/22/2024 1/22/2024 1/22/2024 1/22/2024 1/22/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/6/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/8/2024 2/6/2024 2/12/2024 12/12/2023 2/9/2024 2/9/2024 2/9/2024 2/12/2024 1/26/2024 1/22/2024 1/26/2024 2/12/2024 2/13/2024 2/13/2024 2/12/2024 2/13/2024 2/13/2024 2/10/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/12/2024 2/12/2024 2/13/2024 2/6/2024 2/9/2024 2/9/2024 2/14/2024 2/13/2024 2/13/2024 DATE WASHED 2/2/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/8/2024 2/8/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2/12/2024 2//12 2/12/2024 2/12/2024 2/12/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/14/2024 2/14/2024 2/14/2024 Appendix 9 Page 7 of 44 BILLED TO DOW CIMA CIMA CIMA THIRD COAST CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT NRG NRG CENTERPOINT NRG SCS SET CENTERPOINT CLEAN EARTH SPECIALTY CONS. SET DOW SCS SPRINT REPUBLIC SCS SCS THE DOW DOW CIMA CIMA CIMA SPRINT THIRD COAST PCI SPRINT SET SET AEIS LION CIMA CENTERPOINT THIRD COAST CENTERPOINT NRG CIMA SES WM WM REPUBLIC REPUBLIC CIMA CIMA THE DOW WASH TKT # 129163 128755 129401 129348 129392 128449 128473 128448 128477 128481 128761 128784 128779 128783 134527 128764 128776 128772 128765 128744 128669 134535 128762 138207 128727 128708 128720 128756 129326 128486 129344 128750 128811 128805 128780 128797 128788 128743 128824 128812 128831 128823 128830 128825 128768 128757 128798 129001 128726 128729 134544 128822 128826 EQUIPMENT# RBR250612 MT7060 5127 MT7049 5111 LT1007 VB1925323 VT5025 SLD250777 5133 5089 5049 VAC259037 RT250956 RT251179 VB0825199 VB1925129 7260 1832 1824 1833 1828 1831 1829 1833 1833 6153 1828 SLD251447 SLD259042 1409 D327 7163 1833 7219 1828 1824 1830 VT223 VT206 5068 25 2777 5015 D327 5072 29 VB2530 RT2555 VB2546 VB2554 VAC259114 SLD253437 DATE IN 2/13/2024 2/14/2024 2/12/2024 2/13/2024 2/13/2024 2/13/2024 2/13/2024 2/9/2024 2/13/2024 2/13/2024 2/13/2024 1/29/2024 1/26/2024 2/14/2024 2/13/2024 12/6/2023 12/13/2023 2/13/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/13/2024 2/13/2024 2/13/2024 2/2/2024 2/6/2024 2/14/2024 2/14/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/14/2024 2/14/2024 2/15/2024 1/23/2024 2/15/2024 1/24/2024 2/15/2024 1/16/2024 2/15/2024 2/15/2024 1/16/2024 2/2/2024 2/13/2024 DATE WASHED 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/13/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/13/2024 2/14/2024 2/14/2024 2/13/2024 2/13/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/13/2024 2/13/2024 2/13/2024 2/2/2024 2/7/2024 2/14/2024 2/14/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 Appendix 9 Page 8 of 44 BILLED TO THE DOW MAVIRO SCS MAVIRO SCS KURARAY REPUBLIC REPUBLIC CIMA SCS SCS SCS SHELTON SPRINT SPRINT REPUBLIC REPUBLIC CENTERPOINT WM WM CAMIN CARGO THIRD COAST ADVARIO ADVARIO ADVARIO INTERGULF USALCO THIRD COAST INTERGULF INTERGULF SET LEL CENTERPOINT TAS NRG THIRD COAST HERITAGE INTERACTIVE SOUTHWEST SET SET SCS CIMA PCI SCS LEL SCS CIMA CIMA CIMA CIMA CIMA CIMA SPRINT WASH TKT # 128803 128839 128745 128828 128809 128802 138245 128722 128821 128795 128813 129359 129304 128836 128807 137322 138246 128792 128845 128842 128840 128862 128493 128501 128500 134542 134541 134543 128926 129009 128498 128855 128532 128547 128546 128544 128537 128539 128531 128533 134545 128847 128518 129415 128520 129229 128519 134518 128545 128524 134517 128899 128790 EQUIPMENT# SLD252157 RT250770 RT250739 RT252222 RT252060 RT251792 5066 TSH308001 TSH309011 RB21515 5101 RT0025038 VB2558 VB2520 VB2527 7267 PT036 SHORTY 3047 PT1065 1828 TA171 RT250126 VB27585 WELD # 202962 LVT104 1828 22048 1000 RT250587 V250376 RT252550 SLD259095 VB8031 2802 CHHS25024 CHIU258747 14311 25 RT2546 VB2555 VB2514 RT251686 RT252019 RT250874 RT250782 RT252511 RT250139 RT2125068 DVB2225113 TB0525251 VB1225043 VB1925341 DATE IN 2/14/2024 2/14/2024 2/13/2024 2/14/2024 2/14/2024 2/15/2024 1/23/2024 2/14/2024 2/14/2024 2/14/2024 2/14/2024 2/16/2024 2/15/2024 2/15/2024 2/15/2024 2/16/2024 2/17/2024 2/17/2024 2/17/2024 2/17/2024 2/16/2024 2/16/2024 2/15/2024 1/11/2024 1/11/2024 2/16/2024 2/16/2024 2/16/2024 2/15/2024 2/12/2024 2/12/2024 12/11/2023 2/12/2024 2/15/2024 2/14/2024 2/14/2024 2/14/2024 2/16/2024 2/16/2024 2/15/2024 2/15/2024 2/6/2024 2/16/2024 2/16/2024 2/15/2024 2/14/2024 2/14/2024 2/12/2024 12/20/2023 12/12/2023 2/12/2024 2/12/2024 2/14/2024 DATE WASHED 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/16/2024 2/17/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/17/2024 2/17/2024 2/17/2024 2/17/2024 2/16/2024 2/16/2024 2/16/2024 2/15/2024 2/15/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 Appendix 9 Page 9 of 44 BILLED TO SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SCS WM WM DOW SCS REPUBLIC CIMA CIMA CIMA CENTERPOINT LION PCI PCI LION STOLTHAVEN SET SPRINT INTERGULF INTERGULF KR INDUSTRIAL THIRD COAST SET SCS SPRINT SPRINT SPRINT SPRINT THIRD COAST SET CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CIMA CIMA CIMA CIMA SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC WASH TKT # 128491 128835 128820 128860 128490 128502 129411 128859 128844 128857 128495 128563 128548 128536 128540 128569 128576 128577 128574 128572 128571 128556 128527 137498 137489 128655 128658 128654 128523 128767 128747 137215 128774 128504 128841 128856 128497 128643 128660 128542 128529 128984 128650 128645 128510 128853 128834 128766 137899 136636 128751 128769 128846 EQUIPMENT# DSC250417 SLD259102 SLD252207 WM NO # T449 T620 T827H RT953 RT2526 RB21060 T650 5142 5136 5086 FRC590033 SLD252016 SLD259198 VB23639 222188 290172 VB574 VB16100 VB567 VB506 280750 VB2559 VB1925196 23 PT1065 1832 RT401003 7263 TB4016 7178 1828 RT252665 2954 PT1035 WELD #V23476 VB2551 CHIU258656 CHIU258631 5132 5044 VB12010 RBR2520230 5161 5069 62 HOSES 29 RT250911 V250407 VB1925153 DATE IN 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/15/2024 2/7/2024 2/9/2024 2/13/2024 2/12/2024 2/15/2024 2/15/2024 2/15/2024 2/15/2024 2/16/2024 2/16/2024 2/14/2024 2/13/2024 1/26/2024 1/3/2024 1/3/2024 1/26/2024 1/10/2024 1/10/2024 1/11/2024 1/10/2024 12/29/2023 1/10/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/14/2024 2/19/2024 2/20/2024 1/24/2024 1/23/2024 2/12/2024 2/14/2024 2/16/2024 2/15/2024 2/19/2024 2/19/2024 2/14/2024 2/15/2024 2/9/2024 2/19/2024 2/16/2024 2/19/2024 12/12/2023 DATE WASHED 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/16/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/20/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/19/2024 2/20/2024 2/20/2024 2/19/2024 2/16/2024 Appendix 9 Page 10 of 44 BILLED TO REPUBLIC CIMA CIMA WM AMERICAN ACRYL AMERICAN ACRYL AMERICAN ACRYL DOW DOW DOW CLEAN HARBORS SCS SCS SCS CIMA INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF INTERGULF CIMA REPUBLIC CIMA LION NOV CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT THIRD COAST SPRINT PCI LION CIMA CIMA CLEAN HARBORS CLEAN HARBORS SCS SCS SET IRONCLAD SCS SCS MAXBOX CIMA SPRINT SPRINT REPUBLIC WASH TKT # 128562 128559 128558 128656 128543 129015 128724 128810 128775 128530 128505 128507 128517 128657 128647 128494 128829 129294 137706 137697 129327 137891 137876 137471 137863 137649 137869 128588 128617 128612 128627 128629 128622 128585 128597 128852 128579 128630 129438 129421 128770 128837 128555 128522 128606 128600 128858 128528 128716 128599 128646 128605 138208 EQUIPMENT# T5257 BERM 12X50 RT2561 29 36 LT1007 VT401 2777 1828 7171 1833 ML25162 5123 RB2125247 T627H 1833 VT4021 5115 BERM 50240049 RT5619 SCP511236 BERM RT250440 RT252090 1 HOSE 6" T668H T598 T614 T740 SS141 25 SLD251607 36 SLD259204 5183 5157 5078 5129 5184 VB15094 V27055 RB21081 RT2030 RT251575 RT250110 1426 15 HOSES 89601 2954 VB2552 OT2514 VTR05 1833 IM152 DATE IN 2/20/2024 2/15/2024 2/19/2024 2/20/2024 2/16/2024 2/19/2024 2/16/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/19/2024 2/20/2024 2/20/2024 2/21/2024 2/21/2024 2/21/2024 2/20/2024 2/19/2024 2/21/2024 2/20/2024 2/20/2024 2/19/2024 2/20/2024 2/20/2024 2/20/2024 2/12/2024 2/21/2024 2/21/2024 2/19/2024 2/21/2024 2/20/2024 2/19/2024 1/29/2024 2/16/2024 2/20/2024 2/19/2024 2/21/2024 2/19/2024 2/21/2024 2/22/2024 2/21/2024 2/20/2024 2/22/2024 2/21/2024 2/22/2024 2/22/2024 2/21/2024 2/9/2024 2/22/2024 2/22/2024 2/22/2024 DATE WASHED 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/20/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/20/2024 2/21/2024 2/21/2024 2/21/2024 2/20/2024 2/21/2024 2/21/2024 2/20/2024 2/21/2024 2/21/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 Appendix 9 Page 11 of 44 BILLED TO REPUBLIC CIMA CIMA CIMA CIMA KURARAY SET PCI THIRD COAST CENTERPOINT NRG THIRD COAST SCS REPUBLIC REPUBLIC SULZER TURBO SCS SCS IRONCLAD IRONCLAD IRONCLAD SPRINT SPRINT AEIS AMERICAN ACRYL AMERICAN ACRYL AMERICAN ACRYL CLEAN HARBORS CLEAN HARBORS CIMA CIMA CIMA SPRINT SCS SCS SCS SCS SCS SET SET IRONCLAD IRONCLAD SPRINT SPRINT SET SET BRENNTAG PCI CIMA CIMA VAICO ENVISTA PCI WASH TKT # 128632 128516 128625 134985 128664 128608 128566 134957 134982 134960 134981 134968 128616 134964 134978 135007 134991 135021 134974 138623 134993 128640 128638 128611 128633 134975 134984 128785 135016 134995 128628 135029 128639 128591 129378 128662 134963 128603 135012 128596 134997 135042 134999 134959 135055 134992 135046 135056 135003 128728 135064 135083 135088 EQUIPMENT# RB20043 RB23036 RT2847 RBR2520828 T809H T311 5138 V250327 V250556 HOSES / FITTINGS 146 46 VAC258044 VB8014 RT2125033 RT2125080 RB2125166 F19004SC RB0525256 VB1925163 RB0825370 VB1925309 RT401148 SFM6011 RBR2520201 RBR2520840 DVB578 FRC501075 CHIU258735 V250743 V250584 CHIU207004 V251082 RT251638 V250384 V250999 V250397 RT251497 RT251609 V250250 V250813 V250615 V250219 V250452 V250827 V251045 V250212 V251020 VB2560 DSC259026 SLD259997 RT2577 65096 DATE IN 2/20/2024 2/20/2024 2/21/2024 2/20/2024 2/16/2024 2/20/2024 2/16/2024 2/22/2024 2/22/2024 2/22/2024 2/21/2024 2/22/2024 2/21/2024 2/7/2024 2/7/2024 2/7/2024 2/12/2024 2/21/2024 2/23/2024 2/19/2024 2/22/2024 2/23/2024 2/23/2024 2/22/2024 2/23/2024 2/22/2024 2/23/2024 2/19/2024 2/14/2024 2/8/2024 2/12/2024 2/23/2024 1/19/2024 2/23/2024 1/26/2024 1/22/2024 2/8/2024 2/23/2024 2/22/2024 2/7/2024 2/2/2024 2/2/2024 2/12/2024 1/19/2024 1/26/2024 2/2/2024 1/18/2024 1/26/2024 2/20/2024 2/22/2024 2/22/2024 2/22/2024 2/15/2024 DATE WASHED 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/22/2024 2/7/2024 2/7/2024 2/12/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/22/2024 2/22/2024 2/22/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/22/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 Appendix 9 Page 12 of 44 BILLED TO IRONCLAD IRONCLAD IRONCLAD IRONCLAD AMERICAN ACRYL AMERICAN ACRYL SCS SPRINT SPRINT SET SET SET CIMA THIRD COAST REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC IRONCLAD IRONCLAD IRONCLAD IRONCLAD NRG ADVARIO CLEAN HARBORS SPRINT SPRINT CLEAN HARBORS SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT CIMA CIMA CIMA CIMA CIMA WASH TKT # 134983 134973 135020 128642 128648 134962 128653 135038 135040 135070 135004 135035 135030 129036 134534 134533 134540 135009 135120 128620 135037 135123 135119 135063 135106 135062 135901 128589 128854 129053 128748 135098 128422 135104 129290 128470 128683 135094 135061 129042 128902 128901 128758 128390 129291 128889 128372 129318 128631 135036 135053 135052 128508 EQUIPMENT# VT207 TA172 1409 PT1030 CHIU258742 12000 V250770 V250338 V250864 V250265 23 1828 2817 SHORTY RB20066 5128 5139 HOSE 6" RB23038 1828 VB27108 F06015 5092 5112 5103 5163 R250185 R250016 R250034 R250009 R250241 R250199 T010 2853 2777 VB27120 V250599 BERM 12X50 5091 5151 5143 VB8008 VB8001 VB8038 VB8007 V305 8466 1828 T022 TA172 T132 VB656 VB2529 25 DATE IN 2/23/2024 2/19/2024 2/23/2024 2/23/2024 2/14/2024 2/23/2024 1/9/2024 1/26/2024 2/12/2024 2/8/2024 2/23/2024 2/23/2024 2/23/2024 2/22/2024 1/26/2024 2/17/2024 2/22/2024 2/20/2024 2/23/2024 2/20/2024 2/21/2024 2/22/2024 2/20/2024 2/14/2024 2/22/2024 2/23/2024 2/23/2024 2/20/2024 2/22/2024 2/22/2024 2/22/2024 2/26/2024 2/26/2024 2/26/2024 2/19/2024 2/9/2024 2/15/2024 2/22/2024 2/22/2024 2/21/2024 2/21/2024 2/19/2024 2/22/2024 2/22/2024 2/16/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 1/26/2024 2/21/2024 2/24/2024 DATE WASHED 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/22/2024 2/22/2024 2/22/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/23/2024 2/22/2024 2/23/2024 2/23/2024 2/21/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 Appendix 9 Page 13 of 44 BILLED TO SET SET SET PCI CLEAN HARBORS CLEAN HARBORS SPRINT SPRINT SPRINT SPRINT CIMA CAMIN CARGO PCI SET SCS SCS AEIS IRONCLAD SPECIALTY CONS. SET SET SCS SCS SCS SCS WM WM WM WM WM WM PCI PCI PCI SET SPRINT CIMA SCS SCS SCS CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT SET REPUBLIC THIRD COAST PCI SET SET INTERGULF CIMA CIMA WASH TKT # 135124 128618 135103 135897 128496 135097 137849 129319 128760 128684 135099 135895 135090 135034 129317 128575 135080 134954 135101 134965 135026 135069 134979 128848 5163 135896 135105 134987 135047 135059 135073 135905 135904 135909 128610 128713 128515 134554 134553 135023 135015 128595 135077 135045 134548 135916 135934 135922 135918 135914 129328 135000 135903 EQUIPMENT# 5127 LT1007 5015 SST702001 V250304 V250667 V250588 V250693 V251076 R250211 PT1030 PT1035 1828 VB15180 CHVT0852 2954 V250623 V250616 FRC501054 FRC503183 39 TA168 HV220 N47904 TA132 DV799 SS125 T166 36 VB2225020 VB2225022 QV25135 VB16037 4 PIECES PIPES 19 PIPES 8 PIPES 10 PIPES 97 HOSES VB8012 37 HOSES 5 HOSES 64 HOSES SST708021 BERM 25230086 RB22001 5120 BERM 12X50 4 ROLLERS VB2538 T5203 T816H T759H T901 RB22088 DATE IN 2/26/2024 2/23/2024 2/22/2024 2/14/2024 1/24/2024 1/26/2024 2/12/2024 1/29/2024 2/8/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 1/3/2024 2/19/2024 2/27/2024 1/26/2024 2/12/2024 2/16/2024 2/19/2024 2/23/2024 2/23/2024 2/23/2024 2/22/2024 2/23/2024 2/23/2024 2/23/2024 2/2/2024 2/27/2024 12/11/2023 12/11/2023 2/26/2024 12/11/2023 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/19/2024 2/12/2024 2/12/2024 2/21/2024 2/26/2024 2/9/2024 2/27/2024 2/26/2024 2/21/2024 1/12/2024 2/27/2024 2/22/2024 2/23/2024 2/27/2024 2/28/2024 DATE WASHED 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/26/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/26/2024 2/27/2024 2/22/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/23/2024 2/26/2024 2/23/2024 2/26/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/27/2024 2/28/2024 2/28/2024 2/27/2024 2/16/2024 2/16/2024 2/23/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 Appendix 9 Page 14 of 44 BILLED TO SCS KURARAY SCS WM SPRINT SPRINT SPRINT SPRINT SPRINT WM LION LION THIRD COAST REPUBLIC CLEAN HARBORS PCI SPRINT SPRINT NTE NTE SET SET SET SET SET NRG MAVIRO IKON CIMA REPUBLIC REPUBLIC SHELTON INTERGULF SAGE SAGE SAGE SAGE SAGE THIRD COAST MAXBOX MAXBOX MAXBOX CIMA DOW WM SCS CIMA CIMA REPUBLIC AMERICAN ACRYL AMERICAN ACRYL KURARAY IRONCLAD WASH TKT # 135915 135110 134994 128843 129220 129288 128782 129373 129054 135961 135971 135972 135973 137698 128598 135949 129315 128763 128554 128587 135108 135900 135091 135054 135093 135902 135102 128892 135970 137222 137223 135919 137212 134561 134560 134559 134558 134557 134562 128753 128754 135017 135925 128709 135979 135908 135024 137551 135950 135074 135107 135967 135990 EQUIPMENT# 6128 T751H 2954 23 PT1030 310 TA168 1831 1828 1826 1830 FRC521002 5173 5135 5076 5165 5022 CV090 TA168 T76 1409 RT251247 SS HOSES TRAILER 1828 7018 310 1828 RBR251307 DVB27038 10300401 A5347 VT5252 VT5253 CHIU258752 5074 790093 OT25549 1055 RB22071 RT401225 T022 152 RT3220 1409 PT1035 SS146 VB2511 RT252069 V250542 V250026 RT251408 V250078 RT250238 DATE IN 2/28/2024 2/23/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/19/2024 2/16/2024 2/17/2024 2/14/2024 2/16/2024 2/15/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 1/4/2024 2/26/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/28/2024 2/8/2024 2/9/2024 2/27/2024 2/20/2024 2/23/2024 2/14/2024 2/14/2024 2/23/2024 2/20/2024 2/15/2024 2/16/2024 3/1/2024 3/1/2024 3/1/2024 2/29/2024 3/1/2024 3/1/2024 2/29/2024 2/29/2024 2/23/2024 2/22/2024 1/23/2024 2/21/2024 2/22/2024 2/21/2024 DATE WASHED 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/28/2024 2/27/2024 2/26/2024 2/27/2024 2/23/2024 2/27/2024 2/27/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/29/2024 2/23/2024 2/22/2024 2/15/2024 2/27/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 Appendix 9 Page 15 of 44 BILLED TO TAS REPUBLIC PCI CIMA LIONS PILOT SET NRG THIRD COAST THIRD COAST ELLWOOD ADVARIO SCS SCS SCS SCS SCS COMMERCIAL FUEL SET SET SET SPRINT MAXBOX THIRD COAST CENTERPOINT NRG THIRD COAST DOW DOW DOW SET REPUBLIC REPUBLIC CLEAN HARBORS SCS CLEAN HARBORS SPRINT CIMA SET DOW PCI PCI DOW SET LION CLEAN HARBORS CIMA SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT WASH TKT # 135986 135126 135994 135992 135991 136000 136001 136006 135998 136003 136005 128607 128652 128578 128499 128661 128550 136013 136030 136019 136011 137734 135936 134563 136035 136032 136020 135996 129050 128712 135955 128634 135113 128838 128849 135095 134567 128521 128644 136037 135659 136044 136031 136047 135655 136033 136021 135115 135079 137629 135010 135084 135018 EQUIPMENT# V250887 5133 T12138 VT5901 VT5900 LT1007 CHHA25161 2777 T132 V250369 RT251476 V250986 V250389 5172 VB12066 VAC253062 SLD251026 VB2548 VB2540 VAC252306 VB2561 VB25-1 CHVT0644 R250165 R250238 10300411 RT21089 RT2150 RT250954 R250171 V251029 V250841 V250988 V250816 V250910 V251018 V250402 V250876 PT036 PT1040 2853 CHIU258632 2817 SHORTY 1828 1833 RT401190 RT3219 HT4312 A6381B 7003 7266 7221 5108 DATE IN 2/22/2024 2/29/2024 2/28/2024 2/9/2024 2/9/2024 3/1/2024 2/12/2024 3/2/2024 3/1/2024 1/5/2024 2/26/2024 2/19/2024 2/22/2024 2/27/2024 2/28/2024 3/1/2024 3/1/2024 3/1/2024 2/15/2024 3/1/2024 1/23/2024 3/1/2024 2/23/2024 3/1/2024 3/1/2024 2/29/2024 2/29/2024 3/1/2024 2/21/2024 3/1/2024 2/19/2024 2/19/2024 2/22/2024 1/30/2024 2/21/2024 2/22/2024 2/19/2024 2/19/2024 3/4/2024 3/4/2024 3/4/2024 2/12/2024 3/4/2024 3/4/2024 3/4/2024 2/29/2024 2/29/2024 3/1/2024 2/28/2024 3/4/2024 3/4/2024 3/4/2024 3/1/2024 DATE WASHED 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/2/2024 3/2/2024 3/1/2024 3/4/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/1/2024 3/1/2024 3/1/2024 3/1/2024 3/4/2024 3/4/2024 3/4/2024 3/2/2024 Appendix 9 Page 16 of 44 BILLED TO SPRINT SCS GREEN ROCK REPUBLIC REPUBLIC KURARAY CLEAN HARBORS PCI SET SPRINT SPRINT SPRINT SPRINT SCS NRG CIMA CIMA CIMA CIMA CIMA CIMA CIMA CLEAN HARBORS WM TAS DOW DOW DOW SPRINT WM SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT LION LION PCI CLEAN HARBORS PCI THIRD COAST SOLENIS DOW DOW IRONCLAD IRONCLAD CENTERPOINT CENTERPOINT CENTERPOINT SCS WASH TKT # 135078 136034 135999 128705 128711 136043 128787 135665 135652 137757 135912 128592 135041 135958 136010 136040 136050 136041 128506 136049 129400 135660 135118 135651 136048 136029 136022 135661 135011 135663 128615 128604 135050 129076 135022 135068 128614 128593 135678 135685 135668 128786 135667 135683 135673 136017 136025 136038 136008 135684 135688 135686 134566 EQUIPMENT# T5016 5140 5136 5050 CHIU258757 CHIU258658 CHIU258641 27714 CU90 TSH309010 TSH309001 5013 LT1007 FRB173 A4182B A982B FT21010 FRB21005 T173 T172 5141 R250255 2 FILTERS PODS V23637 TSH308011 VT5025 T5014 SLD250037 VAC253336 CHIU258654 CHIU258638 SLD257007 V250299 RT252067 V250913 5035 V250788 V250325 V250695 V250499 V250895 5040 1828 4 1833 1832 PT1040 PT1055 FRC503353 FRC589089 TB4953 RT401154 T765H DATE IN 2/29/2024 3/4/2024 2/27/2024 2/29/2024 2/13/2024 2/13/2024 2/13/2024 3/4/2024 3/2/2024 3/4/2024 3/4/2024 2/28/2024 3/4/2024 2/20/2024 2/28/2024 2/28/2024 2/27/2024 3/1/2024 2/2/2024 3/5/2024 3/4/2024 3/5/2024 2/23/2024 1/26/2024 3/5/2024 2/22/2024 2/22/2024 3/4/2024 2/16/2024 2/12/2024 2/13/2024 2/9/2024 2/6/2024 2/27/2024 2/19/2024 2/28/2024 1/30/2024 2/22/2024 2/22/2024 2/22/2024 1/30/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/6/2024 3/6/2024 3/1/2024 2/28/2024 3/5/2024 3/5/2024 2/19/2024 DATE WASHED 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/4/2024 3/5/2024 3/1/2024 3/5/2024 3/5/2024 3/5/2024 3/6/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/5/2024 3/6/2024 3/6/2024 3/5/2024 3/4/2024 3/5/2024 3/5/2024 3/5/2024 Appendix 9 Page 17 of 44 BILLED TO REPUBLIC SCS SCS SCS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CIMA NRG NRG NRG SCS KURARAY IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IKON SET SCS WM VAPOR POINT INTERGULF NRG REPUBLIC REPUBLIC CIMA CIMA CLEAN HARBORS CLEAN HARBORS SPRINT SPRINT SPRINT SPRINT SCS SPRINT SPRINT SPRINT SPRINT SPRINT SCS THIRD COAST CENTERPOINT CENTERPOINT CAMIN CARGO LION LION NTE NTE DOW DOW AMERICAN ACRYL WASH TKT # 136014 135671 135951 136015 128794 128817 128818 135681 134564 135672 135682 135997 135669 128637 135988 135987 135977 135664 128880 135696 135677 135693 135096 129293 135695 135032 135033 135687 128565 128771 128793 128702 128965 135953 128586 135993 129078 135049 135039 135075 129074 135713 135720 135701 135694 135707 135727 135728 136042 136002 135697 135712 128619 EQUIPMENT# T644H 1436 1832 1833 1826 1828 2954 5038 VAC253060 SLD259113 SLD259047 SLD253937 29 RBR250647 RT2151 RB2325040 CHVB0636 SCV112 VAC259042 VAC250996 V250354 RT252651 V614S LT1007 5132 T652 RB0025072 TSH308001 25 HOSES QV25123 BERM C503296 RB2125206 BERM 25230308 RT250859 RT250922 VB2541 37 1833 1828 T901 PT1055 N49109 FRB21013 RT251373 VB2522 VAC251016 VAC253044 VB2512 VB2518 BERM SCP510921 BERM SCP510545 SPILL BERM SCP510691 3 BERMS DATE IN 2/22/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 2/22/2024 2/19/2024 2/7/2024 2/9/2024 2/13/2024 3/6/2024 3/5/2024 3/6/2024 3/6/2024 1/10/2024 3/5/2024 2/23/2024 2/26/2024 1/26/2024 3/7/2024 2/26/2024 3/6/2024 3/5/2024 2/27/2024 3/7/2024 3/5/2024 2/20/2024 2/23/2024 2/19/2024 3/7/2024 3/5/2024 2/21/2024 2/21/2024 2/16/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 1/18/2024 2/16/2024 2/15/2024 2/19/2024 2/16/2024 2/19/2024 2/27/2024 2/22/2024 2/20/2024 3/7/2024 DATE WASHED 3/5/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/6/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 Appendix 9 Page 18 of 44 BILLED TO AMERICAN ACRYL SET A-ONE CHEMICALS CHEMSTATION OXBOW THIRD COAST PCI SCS CIMA SPRINT SPRINT INTERGULF CIMA IRONCLAD IRONCLAD REPUBLIC INTERGULF LIQUID POWER SHELTON SHELTON SPRINT SPRINT SET HERITAGE SCS AMERICAN ACRYL REPUBLIC NRG SHELTON SHELTON REPUBLIC REPUBLIC SET SPRINT SPRINT CIMA CIMA SPECIALTY CONS. THIRD COAST KURARAY LION IRONCLAD IRONCLAD SPRINT CIMA CIMA CIMA CIMA CIMA SET IRONCLAD IRONCLAD IRONCLAD WASH TKT # 135082 135730 135733 135734 135744 135743 135725 135087 128580 129040 128703 128804 135745 135706 135740 135729 137866 135692 135898 135921 129333 135765 135935 135736 135711 135969 135778 135717 128635 135899 128590 135751 135723 135006 135019 128568 135770 135780 135784 135757 135758 135775 135762 128369 128567 128549 128624 128659 128602 135956 135057 128636 135774 EQUIPMENT# BERM SCP507281 HOSES AND BERMS 3 BERMS 3 BERMS N49094 F05546 A3553C A6395 A1128 RBR252038 N48260 VB16226 VB16255 RT22018 5088 5085 5029 11774677 QV25150 R250227 PLASTIC HOSES (9) T609 T547 T640H T700H T812H T5020 VT5213 VT5239 RT2125051 DVB1925059 RT0325045 RT2125061 RT042516 VB1225053 VB1925248 VB1925026 RT2225041 RB2125062 RT0025017 D327 2809 5177 5175 5155 5119 5166 5137 2494RB BERM 511233 T132 1828 PUMP / HOSES DATE IN 2/28/2024 2/28/2024 2/27/2024 3/5/2024 2/27/2024 3/7/2024 3/1/2024 2/19/2024 3/7/2024 3/8/2024 3/7/2024 3/8/2024 2/20/2024 3/8/2024 3/8/2024 3/7/2024 2/19/2024 2/27/2024 2/26/2024 3/8/2024 3/1/2024 2/22/2024 2/28/2024 2/9/2024 3/7/2024 2/20/2024 2/20/2024 3/7/2024 3/7/2024 5/19/2023 2/7/2024 2/13/2024 3/7/2024 2/13/2024 12/29/2023 2/12/2024 2/8/2024 2/13/2024 3/7/2024 12/28/2023 3/7/2024 3/7/2024 2/16/2024 2/19/2024 2/16/2024 2/20/2024 2/16/2024 2/23/2024 3/7/2024 2/21/2024 3/8/2024 3/8/2024 3/9/2024 DATE WASHED 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/7/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/6/2024 3/6/2024 3/6/2024 3/6/2024 3/7/2024 3/6/2024 3/7/2024 3/7/2024 3/8/2024 3/8/2024 3/9/2024 Appendix 9 Page 19 of 44 BILLED TO IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD SET SET DOW SCS SCS SCS SHELTON SHELTON WM SHELTON AMERICAN ACRYL AMERICAN ACRYL AMERICAN ACRYL AMERICAN ACRYL AMERICAN ACRYL REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC LEL DOW SCS SCS SCS SCS SCS SCS DOW SET SET THIRD COAST ADVARIO WASH TKT # 136009 135989 135982 135714 135983 135761 136045 128621 135776 135804 135777 135790 134986 135785 135799 135756 128613 135957 135920 135802 135654 135058 135995 128715 135747 134958 134961 135748 135749 133830 129027 128815 135771 128827 137658 128746 128665 128816 135779 138045 135760 135763 134547 128601 134546 134972 134550 135100 135772 135027 135792 135798 135806 EQUIPMENT# 1297 V250414 VDB25051 310 RB2025033 CHHT25006 CHRT26645 V250074 RT251023 VDB25171 RT253 OT3014 VB2565 VB2543 6008 VAC259162 SLD255407 SLD251857 SLD254857 SLD251036 SLD254917 SLD254987 SLD253877 VB8032 VB8002 VB8041 VB8024 VB8036 VB8026 VB8040 VB27199 5098 RT2125016 6093 6023 2859 2777 T172 6167 RT2225037 R250367 DVB661 DVB568 36 RT250629 RT252596 RT250760 RT251286 RT251116 RT251283 RT251357 1833 FRC502090 DATE IN 3/8/2024 1/23/2024 1/26/2024 3/8/2024 3/6/2024 3/8/2024 3/8/2024 1/23/2024 3/5/2024 3/7/2024 3/8/2024 2/14/2024 2/15/2024 2/15/2024 2/26/2024 3/1/2024 3/7/2024 3/7/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 2/13/2024 2/21/2024 2/21/2024 2/21/2024 2/21/2024 2/22/2024 2/27/2024 2/21/2024 2/19/2024 2/22/2024 2/21/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 2/13/2024 3/11/2024 2/26/2024 2/22/2024 3/8/2024 1/19/2024 1/18/2024 1/18/2024 1/18/2024 1/18/2024 1/18/2024 1/19/2024 3/11/2024 2/27/2024 DATE WASHED 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/9/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/8/2024 3/6/2024 3/8/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/11/2024 3/7/2024 Appendix 9 Page 20 of 44 BILLED TO MILLER SPRINT SPRINT SPRINT REPUBLIC CLEAN HARBORS CLEAN HARBORS SPRINT SPRINT CIMA CIMA CIMA CIMA CIMA CENTERPOINT CIMA SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT PILOT CENTERPOINT CIMA SCS REPUBLIC HERITAGE HERITAGE PCI PCI SET CENTERPOINT REPUBLIC WM NRG NRG CIMA SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT EVITA NTE WASH TKT # 135789 137630 129302 135803 135724 135788 135793 129407 135704 135769 135801 128492 128525 128541 135945 135657 135768 135767 135786 135797 135796 135787 128801 135014 135013 134996 135002 135048 135968 135001 128594 135076 135028 135813 135819 135807 135812 135814 135820 128814 135818 135947 135086 135795 128386 137626 137625 128355 128352 128354 128385 135811 135960 EQUIPMENT# R250064 RT2125071 VB2529 VAC258039 6121 DVB654 DVB27017 3080 VB22076 RB23057 R250185 R250285 VB27637 RBR22015 36 25 RBR250768 QV25-119 1409 2954 VB2528 1823 1833 1833 1828 RT401237 A6845-C A4196-B A6369-B T901 SHORTY 2777 VB2546 D322 5151 5111 1828 VB2517 5117 PT1035 1823 A4803-B A784-B RT20006 29 VB2519 SCV68 RBR2520076 RBR251648 RT401086 VB15191 TB4960 RT4189 DATE IN 3/12/2024 2/15/2024 2/29/2024 3/1/2024 3/12/2024 2/26/2024 2/21/2024 2/21/2024 2/26/2024 3/12/2024 3/12/2024 3/11/2024 2/26/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 2/23/2024 3/12/2024 3/12/2024 3/11/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/6/2024 3/6/2024 3/6/2024 3/12/2024 3/13/2024 3/13/2024 2/29/2024 3/13/2024 3/12/2024 3/11/2024 3/13/2024 2/29/2024 3/6/2024 3/13/2024 3/13/2024 3/5/2024 3/5/2024 3/13/2024 3/13/2024 3/12/2024 3/13/2024 3/13/2024 3/13/2024 3/12/2024 3/12/2024 3/13/2024 3/13/2024 DATE WASHED 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/12/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 Appendix 9 Page 21 of 44 BILLED TO WM REPUBLIC CIMA CIMA CENTERPOINT NRG NRG NRG INTERGULF IRONCLAD WM WM SHELTON CIMA CIMA CIMA CIMA SHELTON SET PCI CIMA CENTERPOINT BUDWEISER CAMIN CARGO THIRD COAST DOW IRONCLAD IRONCLAD IRONCLAD KURARAY PCI PCI CIMA CIMA SCS SCS SHAWCOR CIMA SCS LION NRG IRONCLAD IRONCLAD IRONCLAD CIMA CIMA CENTERPOINT DOW DOW DOW IRONCLAD IRONCLAD IRONCLAD WASH TKT # 135832 128512 136027 135658 135833 134555 134551 135031 135926 135840 135829 135817 135942 135852 135846 135838 135848 135109 135841 135839 135810 135859 135836 185861 135854 135845 135737 135738 135739 135834 135863 135868 136016 135873 135826 135815 135885 136036 135731 135894 135461 135718 135698 135867 135869 135855 135889 135893 135872 135862 135849 135871 135882 EQUIPMENT# RBR2520227 WM GREEN BOX WM COMPACTOR SCRUBER RT401003 RT401203 RT401054 37 TA-168 T-172 2777 PT1035 SVT245 310 5113 5101 A4192-B 1833 1829 5092 IM-169 5123 5157 R250034 SLD259334 CHIU258732 D316 ML25374 RT2225055 RT2125070 VT2510 RT400011 RT401143 RT401148 RT3212 TB6248 VB27173 A4799-B RT3220 RT401005 RT4495 5030 25 CHIU258647 T21023 HOSES/ FITTINGS 3 BASKETS WITH FITTINGS 2853 T171 1828 1832 1826 5060 DATE IN 3/13/2024 3/11/2024 3/13/2024 3/12/2024 3/13/2024 3/12/2024 3/12/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/13/2024 3/5/2024 3/14/2024 3/14/2024 3/13/2024 3/14/2024 3/12/2024 3/12/2024 3/12/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/12/2024 2/12/2024 3/7/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/12/2024 3/12/2024 3/5/2024 3/14/2024 3/14/2024 3/14/2024 3/7/2024 3/14/2024 3/14/2024 3/14/2024 2/3/2024 2/3/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/5/2024 DATE WASHED 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/13/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/8/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/14/2024 3/12/2024 3/15/2024 3/15/2024 3/15/2024 3/13/2024 3/14/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 Appendix 9 Page 22 of 44 BILLED TO IRONCLAD WM WM SHELTON CENTERPOINT IRONCLAD IRONCLAD CIMA SET SET PCI LION SET KIWO SCS SCS IRONCLAD BRENNTAG BRENNTAG SCS SET SCS SCS WM CIMA CLEAN HARBORS CENTERPOINT SPRINT REPUBLIC REPUBLIC REPUBLIC IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD DOW DOW DOW SCS CIMA CLEAN HARBORS SCS SAGE SAGE PCI SET NRG NRG THIRD COAST SCS WASH TKT # 135891 135824 135887 135847 135457 135858 135837 135469 135468 135465 135474 135476 135480 135481 135464 135886 135709 135493 135497 135866 135498 135825 135860 135853 135477 135487 134571 135486 135827 128778 135750 135484 135471 135479 135463 135842 135844 135710 135482 135504 135470 134568 135500 135488 135472 134570 134572 135516 135523 135517 135534 135519 135702 EQUIPMENT# 1831 7219 7217 7163 7233 QV25137 RT401098 VB12026 BERM 25230291 HOSES/ 5 BERMS 3 BERMS T23032 T21014 10300414 CHIU258630 CHIU258710 CHIU258755 CHIU258756 CHVT0677 CHIU258761 WELD# 173670 RT2225049 RT2125065 RT2125057 RT251193 RT252570 RT251033 VAC259027 5105 5173 5161 5154 5127 5091 5142 5103 5112 29 2777 1828 VB12196 VB14069 1833 1832 ML25146 ML25064 1 DVB27021 V498 A827 B A4798 B 10300419 RB21364 DATE IN 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 2/26/2024 3/15/2024 3/5/2024 3/8/2024 3/13/2024 3/15/2024 3/13/2024 3/12/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 2/26/2024 3/15/2024 12/28/2023 2/8/2024 3/12/2024 3/7/2024 2/8/2024 2/8/2024 2/21/2024 2/23/2024 3/14/2024 3/14/2024 3/11/2024 3/12/2024 3/12/2024 3/13/2024 3/13/2024 3/12/2024 3/13/2024 3/15/2024 3/18/2024 3/18/2024 2/27/2024 2/27/2024 3/18/2024 3/18/2024 3/14/2024 2/26/2024 3/18/2024 2/22/2024 3/2/2024 3/5/2024 3/5/2024 3/18/2024 3/18/2024 DATE WASHED 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/15/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 Appendix 9 Page 23 of 44 BILLED TO LEVITATED CENTERPOINT CENTERPOINT CENTERPOINT CENTERPOINT SHELTON DOW SET SET IRONCLAD IRONCLAD SCS SCS CENTERPOINT CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS REPUBLIC REPUBLIC REPUBLIC REPUBLIC SPRINT SPRINT SPRINT SHELTON SCS SCS SCS SCS SCS SCS SCS SCS SCS CIMA PCI NRG NRG NRG UNIVAR HERITAGE SPRINT SPRINT PCI NRG SET IRONCLAD IRONCLAD DOW DOW WASH TKT # 135527 135515 135514 135508 135531 135943 135510 135722 135791 135460 135513 135876 135835 135529 135511 135506 135512 135521 135917 135507 138044 128687 135828 135781 128676 128671 135005 135125 135478 135505 135808 135831 135830 135880 135865 135851 135879 135520 135547 135554 135984 135985 135556 134573 135501 135907 135550 135089 135666 135716 135719 135538 135540 EQUIPMENT# RT2118 RB21054 RT401223 T901 LT1007 CHVT0593 RBR251013 RBR250517 RT20026 DV306 ML25313 1832 1823 8713 R250093 RT2225034 5181 ML25120 VB2578 A6363 B 6006 6174 6079 HOSES / PUMP 5071 RB21060 RB22255 TB400003 10300417 RT2040 6162 VB1925129 VB1925150 6020 RBR2520389 RBR2520845 R250218 2777 RB21217 RB20073 VAC250040 VAC250447 VAC259043 RT251346 HOSES/PUMP 6111 CF 6019 6080 6047 6175 SCV 120 1823 37 DATE IN 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/15/2024 2/23/2024 3/18/2024 3/18/2024 3/18/2024 3/14/2024 2/2/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 2/12/2024 3/16/2024 2/26/2024 3/13/2024 2/20/2024 3/19/2024 3/18/2024 3/19/2024 3/19/2024 3/16/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/18/2024 3/18/2024 3/18/2024 3/14/2024 3/19/2024 3/19/2024 3/19/2024 3/20/2024 3/20/2024 3/20/2024 3/14/2024 3/20/2024 3/13/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 DATE WASHED 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/18/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/20/2024 3/20/2024 3/20/2024 3/19/2024 3/19/2024 3/19/2024 3/19/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 Appendix 9 Page 24 of 44 BILLED TO DOW DOW SHAWCOR KURARAY KURARAY CLEAN HARBORS DOW DOW DOW DOW SPRINT NRG CAMIN CARGO REPUBLIC WM REPUBLIC SCS SPRINT CIMA IRONCLAD MARTIN MARIETTA MARTIN MARIETTA MARTIN MARIETTA SET SCS DOW DOW WM DOW MARTIN MARIETTA MARTIN MARIETTA REPUBLIC REPUBLIC NRG MARTIN MARIETTA MARTIN MARIETTA WM PCI DOW DOW SHELTON REPUBLIC CIMA SPRINT ADVARIO MARTIN MARIETTA MARTIN MARIETTA MARTIN MARIETTA MARTIN MARIETTA MARTIN MARIETTA CENTERPOINT HERITAGE CIMA WASH TKT # 135551 135549 135544 135541 135509 135121 135539 135542 135555 135462 128911 135596 135592 135589 135578 128777 135537 135913 135892 134980 135572 135558 135567 135546 135535 135575 135594 135591 135600 135570 135557 135553 135552 135494 135601 135598 135595 135603 135631 135615 135466 135602 135864 135611 135637 135613 135621 135622 135645 135646 135626 135633 135640 EQUIPMENT# 1833 ML25579 RB23036 81 HOSES VB27250 RT6037 RBR2520855 RBR250413 T817 H RB2007 RB22025 RT6188 RBR251366 R250199 T176 36 VAC250357 RT2125059 VB8035 RT250874 RT250334 RT251044 RT251945 RT251793 RT251672 RT251661 RT251347 7152 1828 1833 23 7187 RBR2520315 5083 VB16216 5059 5062 RBR251537 RT401004 ZIPU264395-8 RT2225027 RB22073 RT22018 QV25105 5 BERMS RBM250397 1832 7263 1828 BERM SCP511158 BERM SCP511226 BERM SCP511244 BERM 0383 DATE IN 3/20/2024 2/26/2024 3/19/2024 2/3/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/13/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/21/2024 3/20/2024 3/20/2024 3/21/2024 2/29/2024 3/7/2024 3/21/2024 3/21/2024 3/20/2024 3/21/2024 3/21/2024 3/20/2024 3/21/2024 3/20/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/20/2024 3/19/2024 2/27/2024 3/15/2024 3/20/2024 3/22/2024 3/22/2024 3/14/2024 3/7/2024 3/23/2024 3/22/2024 3/13/2024 3/19/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/20/2024 3/22/2024 3/21/2024 DATE WASHED 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/20/2024 3/21/2024 3/21/2024 3/21/2024 3/18/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/22/2024 3/22/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/21/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/23/2024 3/22/2024 3/22/2024 3/22/2024 3/23/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 Appendix 9 Page 25 of 44 BILLED TO WM SPRINT MARTIN MARIETTA SAGE DOW IRONCLAD IRONCLAD IRONCLAD REPUBLIC IRONCLAD IRONCLAD IRONCLAD DOW WM SET CIMA REPUBLIC REPUBLIC THIRD COAST SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT CENTERPOINT MONUMENT KURARAY CIMA CENTERPOINT IRONCLAD SCS IRONCLAD SCS SCS DOW DOW THIRD COAST REPUBLIC IRONCLAD IRONCLAD SHELTON IRONCLAD WM SPECIALTY CONS CENTERPOINT THIRD COAST IRONCLAD IRONCLAD IRONCLAD IRONCLAD WASH TKT # 135610 135929 134574 134576 135614 135649 135650 135648 135459 135129 135130 135647 135632 135161 135628 135625 135131 136028 134565 135150 135158 135638 135136 135134 135641 135148 135642 135160 135147 135143 135132 135145 135128 135562 135963 135530 135620 135195 135185 135483 135773 135198 135189 135881 135599 135191 135177 135192 135172 135183 135619 135188 135144 EQUIPMENT# VB8025 6144 6086 LT1007 QV25-127 PT1050 VT5025 T5019 DB175084 DSC250776 SLD257007 SLD259077 5135 RT252597 T901 RT251634 5115 T15169 CHIU258736 T12126 VB2510 5167 R250198 R250125 R250342 R250337 R250009 R250241 R250121 BERM 25230289 5176 1829 1409 2853 V923 VB22086 VB8024 R250331 V251419 RT250832 5057 5163 5041 5054 A6349 B A6374 B 5077 A6352 B 23 1831 1828 1426 7147 DATE IN 3/5/2024 3/21/2024 3/21/2024 3/19/2024 2/26/2024 3/22/2024 3/18/2024 3/19/2024 3/21/2024 3/21/2024 3/22/2024 3/22/2024 3/22/2024 3/21/2024 3/22/2024 3/22/2024 3/20/2024 3/18/2024 3/20/2024 3/22/2024 3/19/2024 3/20/2024 3/22/2024 3/22/2024 3/21/2024 3/22/2024 3/22/2024 3/21/2024 3/21/2024 3/21/2024 3/22/2024 3/25/2024 3/25/2024 3/25/2024 3/22/2024 3/22/2024 3/25/2024 3/25/2024 3/21/2024 3/22/2024 3/6/2024 3/12/2024 3/21/2024 3/8/2024 3/19/2024 3/19/2024 3/12/2024 3/19/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 DATE WASHED 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/23/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/22/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 Appendix 9 Page 26 of 44 BILLED TO THIRD COAST MARTIN MARIETTA MARTIN MARIETTA KURARAY SHELTON LION REPUBLIC REPUBLIC REPUBLIC CIMA REPUBLIC REPUBLIC SCS SPRINT KURARAY SPRINT SCS SCS CLEAN HARBORS CLEAN HARBORS CIMA SCS WM WM WM WM WM WM WM DOW SCS SULZER SET PCI DOW DOW CENTERPOINT TAS SPRINT SPRINT SCS SCS SCS SCS IRONCLAD IRONCLAD SCS IRONCLAD CIMA BRENNTAG THIRD COAST SET CENTERPOINT WASH TKT # 135691 135140 135139 135571 135944 135196 135543 135582 135138 135133 135180 135179 135173 135157 135176 135166 135616 135545 135643 135168 135580 135630 135190 135178 135141 135169 135171 135163 135142 135162 135175 135208 135203 135200 135182 135194 135209 135214 135135 135167 135746 135850 135159 135805 135581 135564 135843 135568 135210 135216 135218 135217 135224 EQUIPMENT# 310 N37391 VA206 DB1625010 R250260 RT250702 QV25138 VAC253063 CHIU258646 CHIU258762 CHIU258754 RT252019 A4189 97 HOSES 53 HOSES TA172 SS HOSES ML25147 1828 1829 SLD250477 SLD259200 SLD253357 RB0325391 2857 DVB1925062 1831 1832 SLD259213 PT036 2777 XCR-05 RT252225 327 CHHS25009 CHVB0322 CHIU258712 CHIU258729 RT252224 SLD251907 SLD251527 RT252497 FRC590004 F08097 T5013 A6350 B A5285 C F07392 A6361 B A5664 B BERM DVB2225115 RT2125082 DATE IN 3/25/2024 3/20/2024 3/20/2024 3/21/2024 3/25/2024 3/22/2024 3/13/2024 3/14/2024 3/21/2024 3/21/2024 3/21/2024 3/25/2024 3/19/2024 2/27/2024 2/27/2024 3/25/2024 2/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/25/2024 3/7/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/15/2024 3/20/2024 3/21/2024 3/20/2024 3/25/2024 3/26/2024 3/26/2024 3/25/2024 3/22/2024 3/19/2024 3/20/2024 2/29/2024 2/20/2024 3/7/2024 3/19/2024 3/18/2024 3/22/2024 3/19/2024 3/19/2024 DATE WASHED 3/25/2024 3/21/2024 3/20/2024 3/25/2024 3/25/2024 3/22/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/25/2024 3/6/2024 3/12/2024 3/25/2024 2/29/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/26/2024 3/27/2024 3/27/2024 Appendix 9 Page 27 of 44 BILLED TO NOV IRONCLAD LEL REPUBLIC WM SPRINT SHELTON SHELTON CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS SPRINT IRONCLAD MAXBOX MAXBOX SET MAXBOX SPRINT THIRD COAST HERITAGE SPRINT SPRINT SPRINT REPUBLIC MAVIRO REPUBLIC NRG NRG SPRINT LION PCI MAVIRO SPRINT MAVIRO CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS SPRINT SPRINT SPRINT SPRINT ADVARIO REPUBLIC REPUBLIC IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD ADVARIO REPUBLIC REPUBLIC WASH TKT # 135219 135127 135604 135154 135223 134577 135888 135473 135153 135165 135164 135211 135597 135976 135974 135205 135936 135239 135253 135248 135231 135230 135242 135225 135220 135753 135254 135246 135243 135241 135232 135228 135201 135207 135522 135605 135152 135644 135202 135252 135251 135222 135170 135593 135627 136024 134988 135759 135583 135548 135184 135573 135577 EQUIPMENT# RT2125044 RT2225042 RT2225035 RB2025090 RB0825322 DSC259007 DSC259037 T12104 310 1832 29 1826 PT1070 PT1060 PT1045 1829 2853 RBR2520830 2450 VB13520 RT400014 RBR251489 T22049 5004 5007 5089 5072 RBR251161 RT4168 HOSE RACK 6133 6008 BERMS VB2513 FRC503333 F16017 5149 HOSES PT1035 CHVT0339 5124 TA172 5122 T901 LVT001 RBR2520003 RT2125075 RT12126 RT1208 RT2125077 SLD250037 WM GREEN BOX R250240 DATE IN 3/19/2024 2/27/2024 3/7/2024 3/26/2024 3/26/2024 3/1/2024 3/4/2024 3/5/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/26/2024 3/25/2024 3/27/2024 3/27/2024 3/25/2024 3/27/2024 3/26/2024 2/26/2024 3/26/2024 3/26/2024 3/27/2024 3/19/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/26/2024 3/28/2024 2/27/2024 3/14/2024 3/27/2024 2/21/2024 3/27/2024 3/28/2024 3/27/2024 3/5/2024 3/27/2024 3/27/2024 2/15/2024 3/28/2024 3/11/2024 3/28/2024 DATE WASHED 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/1/2024 3/5/2024 3/25/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/27/2024 3/26/2024 3/27/2024 3/27/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/27/2024 3/27/2024 3/27/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 Appendix 9 Page 28 of 44 BILLED TO REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC IRONCLAD ADVARIO HOOVER CIMA THIRD COAST PCI LION LION BRENNTAG PCI IRONCLAD IRONCLAD DOW IRONCLAD IRONCLAD SCS SCS SCS SCS SCS DOW IRONCLAD IRONCLAD NRG CENTERPOINT CIMA CIMA CIMA CIMA SCS AEIS LION CLEAN HARBORS SCS SET SCS KURARAY REPUBLIC IRONCLAD REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC WM WM WASH TKT # 135574 135966 135782 135227 135226 135656 135676 135690 135291 135264 135275 135286 135280 135268 135292 135284 135276 135271 135255 135199 135279 135270 135215 135258 135245 135930 135238 135249 135257 135579 134578 135259 135273 135269 135283 135263 134579 135240 135294 135954 135485 135260 134556 135261 135300 135287 135700 135282 135293 128514 135313 135821 135319 EQUIPMENT# WM GREEN BOX WM 25 YDS BOX 126 RT250892 DB1225015 DVB1925058 RT2225031 1829 1828 R250289 F16012 1436 25 36 1832 2777 2777 RT2125078 VB2225034 R250153 N48976 1833 1831 29 F19005 ML25143 RT0025035 RT12128 RT2125069 RT2225050 RT5449 RT251646 RT250783 RT251664 6020 RBR2520058 6088 T749H T705H 5086 5069 VT4020 RT2225048 RT1283 RT12120 RT12124 RT2125062 RT2125064 RT2225045 VB2225048 RT2125067 SLD252447 R250283 DATE IN 3/28/2024 3/28/2024 3/27/2024 3/20/2024 3/4/2024 3/7/2024 2/15/2024 3/28/2024 3/28/2024 3/28/2024 3/27/2024 3/28/2024 3/26/2024 3/27/2024 3/28/2024 3/28/2024 3/28/2024 2/6/2024 3/20/2024 3/11/2024 2/26/2024 3/28/2024 3/28/2024 3/28/2024 2/16/2024 2/26/2024 3/28/2024 3/28/2024 3/19/2024 3/5/2024 3/26/2024 3/25/2024 1/4/2024 3/20/2024 3/28/2024 3/27/2024 3/29/2024 3/28/2024 3/28/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 2/9/2024 2/16/2024 2/27/2024 3/13/2024 2/15/2024 3/29/2024 3/29/2024 DATE WASHED 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/28/2024 3/29/2024 3/29/2024 3/29/2024 3/28/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/27/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 Appendix 9 Page 29 of 44 BILLED TO WM WM SET SPRINT REPUBLIC REPUBLIC REPUBLIC BRENNTAG BRENNTAG WM CIMA SET CIMA CIMA CAMIN CARGO PCI PCI REPUBLIC REPUBLIC WM IRONCLAD THIRD COAST NRG CIMA REPUBLIC SPRINT REPUBLIC REPUBLIC REPUBLIC REPUBLIC DOW SPRINT SPRINT SPRINT CENTERPOINT IRONCLAD SHAWCOR REPUBLIC REPUBLIC SCS SCS SCS REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC WASH TKT # 135302 135315 135256 135609 135670 135752 128511 135322 135321 135303 135272 135306 135244 135285 135314 135309 135295 128998 135635 135816 135946 134581 134580 135305 128557 135933 135297 135312 135576 135699 135237 135221 137719 135623 135307 135288 135324 135308 135311 135325 135341 135335 135234 135326 135337 135336 128732 128564 135965 135877 128513 135327 135345 EQUIPMENT# VB27585 7147 RT252505 RT252693 RT251763 1829 HOSES/ PUMP 5003 DB1925039 VB1925127 T132 D423 FRC589030 1426 3 BASKETS WITH FITTINGS 1 RACK 51 HOSES 5192 RT2125026 RT2125032 25 40121 7233 7127 1826 1832 ML25139 1409 RT0025029 RB2225139 RT250772 ML25383 RT2509 7269 T901 PT1035 R250211 5134 1409 1826 1426 SLD257069 RT251948 ML25589 ML25442 T829 H T675 H T827 H RT102558 RB2125064 5167 36 N48980 N49109 DATE IN 2/28/2024 3/29/2024 1/8/2024 3/21/2024 3/20/2024 3/29/2024 3/29/2024 3/27/2024 3/29/2024 3/4/2024 3/29/2024 3/30/2024 3/27/2024 4/1/2024 2/3/2024 2/3/2024 3/23/2024 2/9/2024 2/20/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 2/26/2024 4/1/2024 3/30/2024 12/20/2023 1/26/2024 2/26/2024 3/20/2024 4/2/2024 4/1/2024 4/2/2024 4/1/2024 3/22/2024 4/2/2024 4/2/2024 4/2/2024 3/20/2024 3/20/2024 2/26/2024 3/13/2024 3/28/2024 3/21/2024 4/1/2024 2/20/2024 4/2/2024 3/30/2024 4/2/2024 4/1/2024 4/1/2024 DATE WASHED 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/29/2024 3/30/2024 3/28/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/1/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 Appendix 9 Page 30 of 44 BILLED TO SHELTON CENTERPOINT SPRINT SPRINT SPRINT NRG SET SCS REPUBLIC REPUBLIC SET LEL NTE SET SAGE SAGE SCS REPUBLIC REPUBLIC CIMA CLEAN HARBORS SHAWCOR CENTERPOINT THIRD COAST NOV SPRINT SET REPUBLIC REPUBLIC SPRINT SPRINT SPRINT CENTERPOINT KURARAY LION WM SCS SET THIRD COAST SET SPRINT SPRINT SPRINT SPRINT AMERICAN ACRYL AMERICAN ACRYL REPUBLIC REPUBLIC REPUBLIC SCS CIMA IRONCLAD IRONCLAD WASH TKT # 136004 135328 128368 135137 135624 135340 135329 135266 135333 135680 135332 135347 135265 135351 134587 134586 135197 128735 124955 135368 135354 135365 135360 135353 135358 135923 135359 135349 137901 129298 135906 135612 135394 135362 135380 135369 135186 135390 135393 135395 135608 135618 135928 135884 135318 135146 135356 134956 135391 135346 135381 135350 135355 EQUIPMENT# A2934 CB RBR2520201 RT339 RT947 6130 6075 6021 RT401223 N49045 T809 H T701 H DVB2225083 T15161 RT1771 2777 T759 H T14133 F15005 5065 RBR2520806 RBR2520183 RBR250956 RBR251535 RBR252405 VB15136 VB1925142 RT0025039 DVB2125017 5026 132 172 UP21002 1832 UP21003 ML25584 RT20039 FRC501032 37 ML25162 RBR2520326 HR03 A6381 B 10300418 RT2151 RBR250226 RBR2520076 RB0025048 RBR250492 RB23046 2666 T781 H RBR2520299 5196 DATE IN 4/1/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 3/29/2024 4/1/2024 4/2/2024 4/1/2024 2/23/2024 4/2/2024 4/3/2024 4/3/2024 4/2/2024 4/2/2024 4/3/2024 3/25/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 3/22/2024 2/29/2024 3/28/2024 2/23/2024 3/27/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/2/2024 4/2/2024 4/2/2024 4/3/2024 4/3/2024 4/3/2024 4/4/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 3/31/2024 4/3/2024 4/2/2024 DATE WASHED 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/2/2024 4/1/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/2/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 Appendix 9 Page 31 of 44 BILLED TO IRONCLAD DOW DOW DOW AMERAPEX ALLIED WM CENTERPOINT IRONCLAD REPUBLIC REPUBLIC REPUBLIC SCS DOW PCI REPUBLIC SCS CIMA SCS DOW DOW DOW DOW DOW DOW REPUBLIC REPUBLIC REPUBLIC SCS SET SET IRONCLAD SPECIALTY IRONCLAD SPRINT SPRINT ADVARIO CIMA THIRD COAST DOW CIMA IRONCLAD NRG DOW DOW DOW REPUBLIC DOW DOW DOW AMERICAN ACRYL DOW SCS WASH TKT # 135363 135376 135383 135392 135379 135384 135389 135334 135366 135385 135361 135122 135399 135404 135403 135387 135382 135406 135213 135437 135414 135420 135423 135449 135174 136012 135298 135111 135278 135431 135440 135409 135436 135444 135388 135398 135400 135407 135416 135442 139653 135438 134583 135424 135433 135456 135434 135452 135429 135435 134584 135453 135370 EQUIPMENT# 2216 10300417 A4320 RT2519 RBR2520476 FT21015 310 7017 1831 736 RT401237 6086 F06104 HOSES AND MANIFOLDS RT4191 RBR251381 RBR250109 RT5342 RBR250773 2592 RBR2520315 RB23042 RBR2520775 1828 310 6084 6174 10 6004 6087 VB1925308 RBR250674 1426 2853 RT2040 2777 VB1925151 RB23070 2777 23 TA 168 5020 RB21104 RT251725 RT251153 70006 VT5239 RB0825161 VB1925259 RB2025195 VB1925043 BERM 12 X 50 2 BERMS 12X50 DATE IN 4/3/2024 4/4/2024 4/3/2024 4/4/2024 4/4/2024 4/2/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 3/27/2024 4/3/2024 4/3/2024 4/3/2024 4/3/2024 4/4/2024 4/3/2024 4/3/2024 4/4/2024 4/3/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 3/13/2024 4/4/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 2/1/2024 4/4/2024 4/6/2024 4/5/2024 4/5/2024 4/3/2024 4/4/2024 4/5/2024 4/2/2024 4/5/2024 4/4/2024 4/4/2024 4/5/2024 4/4/2024 4/2/2024 4/3/2024 4/4/2024 DATE WASHED 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 3/29/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/4/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/6/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 Appendix 9 Page 32 of 44 BILLED TO DOW CENTERPOINT IRONCLAD CIMA DOW IRONCLAD CENTERPOINT CENTERPOINT NRG TAS CENTERPOINT SHAWCOR IRONCLAD IRONCLAD DOW DOW DOW DOW DOW DOW DOW DOW DOW THIRD COAST VPS NRG CENTERPOINT NRG ADVARIO ADVARIO REPUBLIC DOW SET PCI DOW PCI REPUBLIC DOW PCI CIMA SET SCS DOW SPRINT SPRINT CLEAN HARBORS REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC CIMA CIMA WASH TKT # 135448 139654 135447 139665 139651 135377 139673 139572 139626 139675 139570 139672 139647 135281 135432 135422 135455 135418 139643 135428 135412 139644 135430 139591 139620 139353 139615 139598 139586 139609 135878 139574 139606 139578 139583 139584 129187 139660 139357 139605 139611 135443 139657 139577 135373 139604 139642 139652 139622 139627 135378 135411 139664 EQUIPMENT# SST701003 T901 VT4048 5147 VT4016 5185 SCP511173 BERM 10X50 SCP511140 BERM 10X50 4 BERMS 10X50 SCP511237 BERM 10X50 50240246 50240250 50240247 50230406 BERM 10X50 50240253 BERM 10X50 FRB227 RBR251448 RBR251142 N5265 RB20006 RBR2520348 1990 RBR2520845 N40844 RB22151 RT2150 N36731 RBR251214 2494RB RB23071 RBR2520389 RB20066 RBR251093 RB23069 RB23047 N36492 1975 RB23036 RBR2520638 RB22142 RT4189 RT2125 RBR251180 VB8017 VAC252126 VAC258005 VAC2502516 VB27171 RBR2520200 RB23057 RBR2520036 N48297 RT6209 RT6059 V427 DATE IN 4/4/2024 4/4/2024 4/5/2024 4/6/2024 4/4/2024 4/5/2024 4/3/2024 4/3/2024 4/2/2024 4/1/2024 4/1/2024 4/5/2024 4/5/2024 4/4/2024 4/4/2024 4/5/2024 4/4/2024 4/3/2024 4/4/2024 4/5/2024 4/4/2024 4/5/2024 4/5/2024 4/5/2024 4/3/2024 4/4/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/4/2024 4/4/2024 4/5/2024 4/5/2024 4/4/2024 4/5/2024 4/6/2024 4/6/2024 4/6/2024 4/6/2024 4/6/2024 4/4/2024 4/8/2024 4/5/2024 4/5/2024 4/4/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/4/2024 4/4/2024 4/4/2024 DATE WASHED 4/5/2024 4/5/2024 4/5/2024 4/6/2024 4/5/2024 4/6/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/5/2024 4/6/2024 4/6/2024 4/6/2024 4/6/2024 4/6/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 Appendix 9 Page 33 of 44 BILLED TO CIMA KURARAY SCS SCS SCS SCS IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW CENTERPOINT CIMA SHELTON SHELTON IRONCLAD DOW DOW DOW DOW DOW DOW IRONCLAD WASH TKT # 139666 139662 139608 139354 139571 139621 135446 135451 135386 135367 135364 139617 139597 139681 139679 139581 139680 135415 139655 139590 139576 139595 139351 139623 135417 139646 139580 139582 139592 139625 139650 139573 139579 139593 139659 139352 139356 139364 139355 139365 139358 139667 139381 139624 139599 139677 139387 139388 139370 139377 139658 139645 139676 EQUIPMENT# RBR250929 VB1925170 RB0025026 2112 RBR251536 RBR2520370 RB21046 RB23058 R250146 ML25180 VAC259162 RT2164 RBR251647 RBR251508 RB22256 RBR250999 RB23050 1832 1829 DVB2125013 350264 L1805 PT1070 1824 1830 1828 310 DVB683 DSC255177 DSC259060 RT2524 N48313 ML25163 1 BERM SCP511225 ML BOX NO # R250222 N49043 RB23035 1832 VB27111 VB15205 VB14006 VB15153 T132 1831 RB20028 RBR250037 ML25463 ML25428 2851 DW VB VB14030 VB21033 2777 DATE IN 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/3/2024 4/6/2024 4/6/2024 4/4/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/6/2024 4/4/2024 4/4/2024 4/3/2024 4/3/2024 4/8/2024 4/8/2024 3/29/2024 4/4/2024 4/2/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 2/21/2024 3/5/2024 4/4/2024 4/5/2024 4/8/2024 4/8/2024 4/5/2024 3/29/2024 4/2/2024 4/3/2024 4/9/2024 3/27/2024 3/29/2024 3/28/2024 3/26/2024 4/9/2024 4/9/2024 4/8/2024 4/8/2024 3/19/2024 2/23/2024 4/9/2024 3/28/2024 3/29/2024 4/9/2024 DATE WASHED 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/3/2024 4/5/2024 4/5/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/8/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 4/9/2024 Appendix 9 Page 34 of 44 BILLED TO IRONCLAD REPUBLIC REPUBLIC DOW DOW DOW DOW DOW WM THIRD COAST SHELTON DOW DOW DOW DOW DOW DOW CAMIN CARGO NOV REPUBLIC HOOVER SCS LION THIRD COAST NRG THIRD COAST ADVARIO SCS REPUBLIC REPUBLIC CIMA IRONCLAD THIRD COAST INTERGULF WM WM IRONCLAD DOW SBM LIFE SET SET SET DOW SET NRG IRONCLAD IRONCLAD SPRINT SPRINT SCS SET SET PCI WASH TKT # 139389 139380 139375 139379 135426 139359 139363 139669 139385 139376 139368 139369 139361 139670 139661 135413 135425 139383 139384 121182 134588 135402 139374 139382 139402 139398 139396 139399 135025 135721 139575 139596 139395 139393 139603 135338 135375 135427 139434 135277 135344 135299 135233 139411 139420 139405 139401 135561 135116 139432 135310 135343 139409 EQUIPMENT# T172 FRC508385 SLD251156 1829 RT1342 1828 VAC250526 RT2525 5090 5149 RB2325028 25RT167 DVB1825039 RB2125171 DVB2125010 RB20073 N37391 N26847 RBR251430 R250372 R250279 RBR250612 RB23045 1409 T76 29 V250250 V250265 V251022 PCI 1826 7260 6148 6067 1831 310 PT036 1826 1831 5113 5123 1824 5130 T21047 T12170 T821 H SST702006 T901 10300395 V250917 RT2125084 RBR250437 RB22092 DATE IN 4/9/2024 4/5/2024 2/12/2024 4/10/2024 4/9/2024 4/10/2024 4/9/2024 4/9/2024 4/8/2024 4/6/2024 4/9/2024 4/9/2024 4/4/2024 4/8/2024 3/5/2024 4/9/2024 4/9/2024 4/9/2024 4/10/2024 4/9/2024 4/10/2024 4/8/2024 4/9/2024 4/10/2024 4/10/2024 4/9/2024 4/5/2024 4/5/2024 4/5/2024 4/10/2024 4/10/2024 4/9/2024 4/8/2024 4/8/2024 4/10/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/10/2024 4/5/2024 4/11/2024 4/6/2024 4/9/2024 4/9/2024 4/5/2024 4/10/2024 4/9/2024 3/26/2024 4/10/2024 4/5/2024 4/11/2024 4/10/2024 DATE WASHED 4/9/2024 4/8/2024 4/9/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 Appendix 9 Page 35 of 44 BILLED TO SET NTE SPRINT THIRD COAST IRONCLAD BRENNTAG CIMA CIMA SCS SCS REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC DOW DOW DOW DOW WM WM DOW DOW SET SET CIMA SPRINT SPRINT SPRINT PCI THIRD COAST CENTERPOINT STOLT TANK WM NRG CLEAN HARBORS LION EASTON EMERGY SBM LIFE SCS SCS NRG SCS IRONCLAD IRONCLAD REPUBLIC CIMA KURARAY DOW SPRINT REPUBLIC DOW DOW WASH TKT # 139408 139588 128773 139436 139412 139466 139428 139433 139371 139366 139407 139423 139671 139394 135708 139426 139417 139427 139450 139419 139454 139397 139416 139438 139451 139421 139618 139619 139613 139455 139461 139429 139391 139390 139457 139486 139490 139472 139482 139437 139610 139488 139360 139406 139431 139600 139444 139418 135250 139462 139614 139478 139449 EQUIPMENT# RB21164 N37352 VB8008 RT2125079 12X50 BERM 2 BERMS 12 X 25 2 BERM 50240248 50240249 VA163 TB5196 42 HOSES 1" 40 HOSES 1" 35 HOSES 1" 39 VALVES 36 PIPES 15 FITTINGS 29 PIPES 2" 1060 1070 RB20042 RT5763 30 RBR2520238 RT5752 RBR251084 R250041 R250155 L6747 T16122 V250135 VB8004 CHVB0445 VAC253266 N49038 39 HOSES 1" 30 VALVES 25 7169 310 2777 1826 RT2125048 T575 VT5213 T725 H FRC502108 T11015 1826 1 BASKET 34 HOSES 3 FITTINGS 1 BASKET 45 HOSES T10294825 ML25213 ML25462 A5659 B DATE IN 4/8/2024 4/10/2024 4/3/2024 4/4/2024 4/10/2024 4/9/2024 4/10/2024 4/11/2024 4/11/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 4/10/2024 4/10/2024 4/9/2024 4/9/2024 4/12/2024 4/12/2024 4/11/2024 4/12/2024 4/12/2024 4/12/2024 4/5/2024 4/9/2024 4/10/2024 4/3/2024 4/10/2024 4/12/2024 4/5/2024 2/3/2024 2/3/2024 4/11/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 3/26/2024 4/11/2024 4/9/2024 4/4/2024 4/11/2024 4/11/2024 4/12/2024 2/3/2024 2/3/2024 4/11/2024 3/14/2024 2/22/2024 4/5/2024 DATE WASHED 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/11/2024 4/10/2024 4/10/2024 4/10/2024 4/10/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 4/12/2024 Appendix 9 Page 36 of 44 BILLED TO DOW DOW PETRA NOVA REPUBLIC CIMA CIMA IRONCLAD LEL CENTERPOINT SAGE SAGE SAGE SAGE SAGE SAGE SAGE LION LION DOW DOW CIMA DOW DOW DOW WM WM SCS IRONCLAD SPRINT NRG CLEAN HARBORS SHELTON IRONCLAD SAGE SAGE CIMA CENTERPOINT NRG PCI SBM REPUBLIC REPUBLIC REPUBLIC REPUBLIC ADVARIO IRONCLAD SULZER SAGE SAGE IRONCLAD SPRINT SPRINT IRONCLAD WASH TKT # 139403 139458 135410 139678 139439 139410 139446 139487 134589 134597 134592 134593 134594 134595 134596 134591 139510 139509 139424 139413 139494 139520 139491 139512 139524 139503 139601 139415 139460 135445 139448 139497 139587 134500 134601 139489 139523 139525 139517 139516 135235 139492 139422 139663 139471 139481 139495 134598 134599 139483 135491 135065 139616 EQUIPMENT# 2120 2642 131 FITTINGS RB23061 RB21098 RB21075 44 HOSES 1" RB20041 RBR2520111 RB22073 1880368 A.M. A 6849GB CHVT0833 RT401126 1832 1833 7178 1828 310 1825 R250316 LT1007 DVB2125012 T10073 R250045 A4182 B A6500GB CHVT0723 CHVT0813 CHVT0674 CHVT0782 RBR250413 2829 ML25116 ML25125 FT21002 RB23043 RB23053 RBR250832 FRC589101 18 FITTINGS 4" 50 HOSES 1" 42 HOSES 1" PT1070 2120 2777 2063 VTC VACU0015 SCV120 RB21213 36 HV1092 RB23049 DATE IN 4/13/2024 4/13/2024 2/3/2024 4/13/2024 4/13/2024 4/13/2024 2/3/2024 4/15/2024 4/15/2024 4/8/2024 4/15/2024 4/10/2024 4/2/2024 4/12/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/12/2024 4/12/2024 12/19/2023 4/4/2024 4/10/2024 4/3/2024 4/10/2024 3/6/2024 4/3/2024 4/8/2024 4/10/2024 4/15/2024 4/10/2024 4/16/2024 4/16/2024 4/4/2024 4/16/2024 4/15/2024 4/12/2024 4/12/2024 2/3/2024 2/3/2024 2/3/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/12/2024 4/16/2024 4/16/2024 4/16/2024 4/12/2024 4/16/2024 DATE WASHED 4/13/2024 4/13/2024 4/13/2024 4/13/2024 4/13/2024 4/13/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/13/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/15/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 Appendix 9 Page 37 of 44 BILLED TO PCI DOW SAGE DOW DOW DOW SAGE DOW DOW DOW CLEAN HARBORS IRONCLAD CLEAN HARBORS CENTERPOINT NRG NRG CENTERPOINT CENTERPOINT CENTERPOINT STOLT WM KURARAY REPUBLIC CLEAN HARBORS WM IRONCLAD IRONCLAD CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS DOW DOW SPRINT SPRINT IRONCLAD DOW DOW DOW ADVARIO SAGE SAGE SAGE LION PCI PCI MILLER MAVIRO CIMA DOW CIMA MAVIRO DOW WASH TKT # 139526 139527 134603 139530 139529 139531 134605 139542 139543 139404 139544 139447 135372 134602 139533 139535 139545 139548 139551 139552 139506 139507 138156 139649 139456 135450 139445 135726 135405 139386 139440 139553 139459 140199 140200 139668 139569 139554 139498 139505 134610 134608 134609 140211 140212 139556 140208 139504 139562 139558 140203 139515 139565 EQUIPMENT# RB22074 RB22025 TA 168 TB4014 7233 1826 310 7011 21 6003 FRC509059 ML25195 ML25121 ML25449 ML25272 ML25346 ML25233 DWRT2573 DWRT25131 SLD259377 7200 7009 1831 RBR251156 CHVT0748 VT4013 7021 25 1832 1828 1824 736 5142 T901 T21022 5144 VB2521 N35032 RT251776 VB8001 VB0825199 RT12108 5027 ML25056 ML25176 5083 7252 6141 1832 1426 ML25454 1828 1831 DATE IN 4/16/2024 4/16/2024 4/16/2024 4/15/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/15/2024 3/15/2024 2/27/2024 4/12/2024 3/15/2024 3/15/2024 3/14/2024 4/1/2024 4/3/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/16/2024 4/16/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/15/2024 4/17/2024 4/17/2024 2/23/2024 3/15/2024 4/16/2024 4/17/2024 4/18/2024 4/18/2024 4/18/2024 2/26/2024 4/18/2024 4/18/2024 DATE WASHED 4/16/2024 4/16/2024 4/16/2024 4/15/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/16/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/17/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 Appendix 9 Page 38 of 44 BILLED TO DOW DOW SET CENTERPOINT NRG HERITAGE CHALLENGER CENTERPOINT ADVARIO ADVARIO SHELTON SPRINT SPRINT SPRINT SPRINT SPRINT SPRINT WM WM SHELTON EIF EIF THIRD COAST DOW CLEAN HARBORS SCS CENTERPOINT CIMA JONES THIRD COAST CAMIN CARGO TAS SCS KURARAY IRONCLAD SCS CIMA DOW SPRINT ZEON REPUBLIC REPUBLIC SCS SPRINT SPRINT SCS CENTERPOINT KURARAY KURARAY SET SPRINT THIRD COAST SPECIALTY WASH TKT # 139560 139561 139557 134604 140201 140225 140223 140215 140209 140210 139536 135533 135981 139502 135525 135526 135499 135352 135419 140232 140240 140254 140235 140204 139555 140253 140239 140237 140250 140229 140252 140226 140214 139567 134606 139564 140244 140246 140231 140242 139549 140241 134613 135117 135532 140202 140257 140279 140295 140288 135910 140274 140276 EQUIPMENT# T21035 T15153 T22001 ML25470 ML25248 ML25140 25 VT5239 T739 H T814 H T5013 RT2535 RBR2520529 RB22076 25235 172 36 VB2524 FILTER POT 3" R250095 R250150 ML25158 7223 ML25180 FSC200027 ML25133 25RT172 2829 37 RB23052 R5470 RB20057 RBR250647 RB22071 ART2590 N48192 RT1816 RB23072 RB21217 RB21507 RT2527 R250299 R250329 WM NO# 30 YD WM NO#40 YD RT12121 RT12129 1 PALLET 17 HOSES 1" 1 PALLET 17 HOSES 1" 1 PALLET 17 HOSES 1" 1 PALLET 23 HOSES 1" 1 PALLET 22 HOSES 1" 1 PALLET 14 HOSES 1" DATE IN 4/17/2024 4/16/2024 4/13/2024 3/14/2024 3/14/2024 3/14/2024 4/18/2024 4/18/2024 4/9/2024 4/12/2024 4/16/2024 4/17/2024 4/18/2024 4/17/2024 4/19/2024 4/19/2024 4/18/2024 4/17/2024 4/18/2024 4/18/2024 4/18/2024 3/14/2024 4/19/2024 4/19/2024 4/17/2024 2/22/2024 4/18/2024 4/20/2024 4/19/2024 4/12/2024 4/12/2024 4/12/2024 4/16/2024 4/15/2024 4/16/2024 4/12/2024 4/16/2024 4/16/2024 4/16/2024 4/18/2024 4/17/2024 4/16/2024 4/16/2024 4/19/2024 4/19/2024 4/18/2024 4/17/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 2/3/2024 DATE WASHED 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/18/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/20/2024 4/19/2024 4/19/2024 4/20/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 Appendix 9 Page 39 of 44 BILLED TO IRONCLAD IRONCLAD IRONCLAD SPRINT SPRINT SPRINT CIMA REPUBLIC REPUBLIC REPUBLIC REPUBLIC WM DOW DOW CIMA SET CIMA CIMA MARTEST WM WM SPRINT CENTERPOINT THIRD COAST CIMA SPRINT REPUBLIC PCI CIMA DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW DOW WM WM WM WM WM REPUBLIC REPUBLIC SAGE SAGE SAGE SAGE SAGE SAGE WASH TKT # 134611 134607 139532 135503 135489 135490 140294 140262 139425 139501 140224 140238 140261 140256 140300 140299 140285 140243 140271 140289 140268 135502 140313 140309 140230 135044 140283 140316 140303 139513 139519 139521 139559 139534 140205 139518 139566 139568 140206 140278 140255 140216 140197 140308 140307 140259 140227 134616 134615 134617 134618 134619 134620 EQUIPMENT# 40210 166538 VAC251736 VB11677278 CHVB0303 VB8043 VB12074 DVB1925046 CHVT0881 CHVT25057 CHVT0876 RB032016 RB1720001 RT12125 5088 RT251441 CF6063 TA168 1824 1829 1830 PT1070 TA168 ML25591 ML25077 1426 FRB313 A 5296 C 1601 30 HOSES 1" R250021 R250180 RT22020 RT2026 VB1925138 VB1925250 VB1925318 RBR250631 T661 H T614 URT177907 VB1925323 VB1825009 VB1225055 VB0725113 DVB1925012 VB1925192 5078 5181 10300401 5076 VB1925163 7130 DATE IN 4/17/2024 4/18/2024 4/12/2024 4/12/2024 4/2/2024 4/17/2024 4/12/2024 4/19/2024 4/2/2024 4/12/2024 4/15/2024 4/18/2024 4/19/2024 4/17/2024 4/18/2024 4/18/2024 4/18/2024 4/19/2024 4/18/2024 4/18/2024 4/19/2024 4/22/2024 4/22/2024 3/14/2024 2/26/2024 4/22/2024 4/4/2024 3/28/2024 3/22/2024 2/3/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/23/2024 4/22/2024 4/23/2024 4/23/2024 4/23/2024 4/20/2024 4/22/2024 4/11/2024 4/11/2024 4/11/2024 4/15/2024 4/11/2024 4/16/2024 4/18/2024 4/18/2024 3/25/2024 4/17/2024 4/22/2024 4/23/2024 DATE WASHED 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/19/2024 4/22/2024 4/18/2024 4/18/2024 4/19/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/22/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 Appendix 9 Page 40 of 44 BILLED TO CLEAN HARBORS REPUBLIC SHELTON REPUBLIC CLEAN HARBORS THIRD COAST PCI REPUBLIC CLEAN HARBORS CLEAN HARBORS CLEAN HARBORS REPUBLIC REPUBLIC REPUBLIC SCS SPRINT SPRINT SET NRG NRG NRG LION SET SPRINT SPRINT SET IRONCLAD IRONCLAD IRONCLAD SAGE WM WM CENTERPOINT CENTERPOINT REPUBLIC REPUBLIC REPUBLIC CIMA REPUBLIC REPUBLIC UNIVAR REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC SCS SCS IRONCLAD SCS REPUBLIC CENTERPOINT WASH TKT # 140248 140286 139500 139508 135374 140249 139499 140306 135371 139496 139537 140284 140297 140233 140287 140267 140266 140304 134622 134621 134623 140330 140333 135492 135938 140329 139648 135301 135187 134624 140320 140334 140332 140322 140351 140318 140341 140358 140213 140315 140328 139475 139469 139468 139550 139485 140198 140260 140277 135204 134612 140335 140371 EQUIPMENT# 7158 7189 A5808 5065 VB1925136 RB2125068 VB1925145 VB1925135 5077 5143 F1058 VB2545 4048 5029 36 1832 DBR259027 1828 2974 1833 5135 5116 5059 V1233 LVT001 FRC502165 FRC509174 30 1426 3109 V250438 VB15022 RBR251262 2917 5166 PT1060 R250202 RBR2520407 BERM 25230047 BERM 0379 BERM 25230314 FRB277 F06104 BERM 25240171 BERMS 50240023 25240034 BERM 25230097 7197 LV304 1828 2777 7221 7241 7154 DATE IN 4/23/2024 4/23/2024 3/20/2024 4/11/2024 4/23/2024 4/22/2024 4/22/2024 4/22/2024 4/18/2024 4/11/2024 4/22/2024 4/22/2024 4/23/2024 4/18/2024 4/23/2024 4/23/2024 4/22/2024 4/23/2024 4/23/2024 4/23/2024 4/19/2024 4/5/2024 4/19/2024 4/12/2024 4/23/2024 4/10/2024 4/19/2024 4/24/2024 4/24/2024 4/16/2024 2/1/2024 4/23/2024 4/23/2024 4/23/2024 4/19/2024 4/23/2024 4/23/2024 4/23/2024 4/15/2024 4/15/2024 4/15/2024 4/8/2024 4/23/2024 4/15/2024 4/23/2024 4/19/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 DATE WASHED 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/23/2024 4/16/2024 4/19/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/23/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 Appendix 9 Page 41 of 44 BILLED TO CENTERPOINT CENTERPOINT IRONCLAD SCS REPUBLIC REPUBLIC REPUBLIC REPUBLIC SCS SCS PCI CIMA SCS SCS CIMA HERITAGE CENTERPOINT NRG PCI THIRD COAST SCS SCS SCS PCI REPUBLIC NTE NTE CIMA SET DOW SPRINT DOW DOW DOW SCS LION WM DOW DOW DOW DOW INTERGULF IRONCLAD IRONCLAD IRONCLAD IRONCLAD SHAWCOR LEL JONES PCI SHAWCOR NRG CENTERPOINT WASH TKT # 140363 140348 135607 139473 140337 140317 140324 140326 140293 139470 140325 140321 140338 140258 140369 140357 140336 140364 140356 140347 140312 139585 140305 139511 140353 139443 140302 140372 140373 140207 129210 140340 140361 140362 140298 140344 140345 140346 134614 139539 139541 139392 140367 139540 140368 140311 140379 140380 140393 140396 140388 140387 140383 EQUIPMENT# 2120 310 V305 FMI129 DV487 FMI108 RT953 VB1925326 VB1925241 VB1925197 VB1925214 VB1925226 VB1925203 VB0025002 VB1925257 VB1925309 V250290 RT2125086 RT0025020 RT2125058 R250360 R250206 DWRT2574 SLD253437 SLD250406 SLD252437 6162 6008 727 SCP258211 T172 1829 7222 R250312 D387 168 HOSE 2777 RT2125036 VB0825102 VB2225022 VB1925253 RB20020 29 SVT701 25 27714 36 1829 ML25359 1832 V250304 ML25124 DATE IN 4/24/2024 4/24/2024 4/24/2024 4/23/2024 4/23/2024 4/19/2024 4/25/2024 4/23/2024 4/23/2024 4/24/2024 4/24/2024 4/24/2024 4/24/2024 4/23/2024 4/24/2024 4/23/2024 1/24/2024 4/10/2024 3/27/2024 4/10/2024 4/24/2024 4/24/2024 4/17/2024 4/25/2024 4/25/2024 4/25/2024 4/24/2024 4/23/2024 4/25/2024 4/12/2024 4/25/2024 4/25/2024 4/25/2024 4/23/2024 4/17/2024 4/25/2024 4/23/2024 4/26/2024 4/10/2024 4/17/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 3/12/2024 4/26/2024 3/19/2024 2/26/2024 DATE WASHED 4/24/2024 4/24/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/24/2024 4/25/2024 4/25/2024 4/25/2024 4/25/2024 4/22/2024 4/25/2024 4/24/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 Appendix 9 Page 42 of 44 BILLED TO PCI ADVARIO IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC SPRINT REPUBLIC REPUBLIC REPUBLIC WM WM WM CENTERPOINT CENTERPOINT CENTERPOINT NRG CENTERPOINT MILLER PCI SET CAMIN CENTERPOINT WM MAVIRO SET AEIS PCI REPUBLIC REPUBLIC REPUBLIC REPUBLIC DOW CIMA EEW CIMA MILLER CIMA SPECIALTY SPRINT THIRD COAST SPRINT SPRINT WASH TKT # 140381 134628 140375 140366 140370 140310 140406 140350 140359 140374 140385 140390 140382 140365 140397 140339 129226 139465 135262 139467 140389 140384 140228 140410 140402 140413 140394 140352 140403 139522 140400 140407 140414 140360 140245 140399 140343 140416 139464 140247 140435 140445 140418 140434 140429 140440 140419 140438 140443 135856 139907 135566 135911 EQUIPMENT# V250583 V251044 VDB25251 LT805990TW RBR2520776 BERM 0117 BERM 25240249 N49127 A6473 PT22020 F16015 F15001 SLD251567 SLD258001 6048 VT4048 DB1925046 2777 SVT702 VT601 VB1925188 3022 VB1925233 2891 VB2225037 V250807 2777 5017 ML25588 ML25458 ML25582 ML25284 DVB2225082 VDB25197 7223 RT2125013 RT2125068 RT2125023 RT2225055 DVB1925067 R250310 36 T530 DVB2225078 DVB2225094 102955232 T5221 T5217 25RT136 RT0025024 RT2125046 RT2425008 RB1825070 DATE IN 3/19/2024 1/29/2024 4/26/2024 4/24/2024 4/26/2024 4/26/2024 4/25/2024 4/26/2024 4/25/2024 4/25/2024 4/22/2024 4/22/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/27/2024 4/27/2024 4/27/2024 4/26/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 1/9/2024 4/29/2024 4/17/2024 2/22/2024 4/23/2024 3/13/2024 2/26/2024 2/23/2024 4/26/2024 4/29/2024 2/16/2024 4/16/2024 4/12/2024 4/16/2024 4/11/2024 4/29/2024 4/29/2024 4/23/2024 4/15/2024 4/15/2024 4/11/2024 4/26/2024 4/25/2024 4/2/2024 3/30/2024 4/3/2024 4/16/2024 4/30/2024 DATE WASHED 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/26/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 4/27/2024 4/29/2024 4/29/2024 4/24/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/29/2024 4/22/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 Appendix 9 Page 43 of 44 BILLED TO SPRINT SPRINT SPRINT IRONCLAD PCI IRONCLAD IRONCLAD IRONCLAD IRONCLAD IRONCLAD CIMA CIMA SPRINT SPRINT SPRINT SCS REPUBLIC PCI EEW EEW REPUBLIC PCI REPUBLIC PCI REPUBLIC SPRINT PCI REPUBLIC SPRINT SPRINT SPRINT SPRINT REPUBLIC SPRINT CENTERPOINT REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC WM CIMA REPUBLIC REPUBLIC REPUBLIC PCI REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC REPUBLIC WASH TKT # 135584 129383 140424 140398 140439 140428 140412 140430 140409 140411 140319 140323 140433 140432 140421 140415 140444 140450 139902 139905 140442 139903 139904 139908 139906 137848 139910 140251 135043 135114 135883 135940 135112 140426 139919 128651 140222 139514 140220 139477 139915 139921 140342 139546 139547 139493 140446 140404 135397 135348 135454 140218 139923 EQUIPMENT# 5104 T901 RT250322 29 A1469B RT5763 6130 RT1972 6062 6148 12 6046 ML25581 ML25586 ML25472 1824 1832 1426 1828 2777 ML25274 ML25583 RBR2520464 VB27268 RT4994 17272 D375 DATE IN 4/19/2024 4/29/2024 4/30/2024 4/29/2024 4/29/2024 4/30/2024 4/30/2024 4/30/2024 4/26/2024 4/24/2024 4/23/2024 4/25/2024 3/13/2024 2/26/2024 3/14/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 3/14/2024 3/12/2024 4/30/2024 4/30/2024 4/29/2024 4/26/2024 4/30/2024 DATE WASHED 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/30/2024 4/29/2024 4/30/2024 4/30/2024 BILLED TO SCS KURARAY WM CIMA IRONCLAD IRONCLAD NOV CENTERPOINT SPRINT CENTERPOINT NRG NRG SPRINT SPRINT SPRINT NRG KURARAY SET CAMIN PCI SPRINT SPRINT IRONCLAD IRONCLAD DOW MAVIRO MAVIRO WASH TKT # 140301 139913 139936 139916 139914 139940 139942 139937 140422 140377 140354 140405 135874 135924 135495 139941 139938 139927 139930 139935 135496 135857 139928 139929 139911 140449 139926 Appendix 9 Page 44 of 44 APPENDIX 10. SWS DOCUMENTATION OF ACCUMULATED HEELS OF HAZARDOUS WASTE DRUMS FOR LAST 6 MONTHS DATE 11/04/23 11/04/23 11/20/23 11/27/23 11/29/23 12/14/23 12/15/23 12/21/23 12/21/23 12/21/23 12/27/23 12/27/23 01/19/24 01/24/24 02/23/24 02/28/24 02/28/24 02/28/24 02/28/24 02/28/24 02/28/24 02/29/24 03/07/24 03/07/24 03/07/24 03/07/24 03/07/24 03/07/24 03/27/24 03/27/24 03/27/24 04/02/24 04/02/24 04/05/24 TICKET 136898 136902 137035 136733 136500 138055 138079 137330 138214 138223 136570 138100 137232 137469 129317 128499 128550 128652 128661 128575 128578 128849 128601 134546 134547 134550 134972 135100 134556 135485 135260 135213 135726 135402 CUSTOMER REPUBLIC REPUBLIC SCS SCS SCS CIMA CIMA SCS CIMA CIMA REPUBLIC REPUBLIC SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SCS SET SCS CLEAN HARBORS SCS GENERATOR STOLT BARGE STOLT BARGE CHEVRON PHILLIPS SELECT CHEMISTRY EQUISTAR CHEMICAL KINDER MORGAN KINDER MORGAN CHEVRON PHILLIPS KINDER MORGAN ODFJELL TERMINALS SHELL SHELL EQUISTAR CHEMICAL EQUISTAR CHEMICAL CHEVRON PHILLIPS EQUISTAR CHEMICAL EQUISTAR CHEMICAL CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS LUBRIZOL DEER PARK CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS KURARAY AMERICA CHEVRON PHILLIPS CHEVRON PHILLIPS CHEVRON PHILLIPS LYONDELL OCCIDENTAL CHEMICAL KURARAY AMERICA CONTAINER NUMBER VB: SBS-003 VB: SBS-002 SCS-5064 VT-4021 SCS-5063 130 BBL: #36 TANKER #32 TANKER: #5087 VB-2537 VAC-253051 VB-1925054 VB-1925147 SCS-5052 SCS-5128 SCS-5076 SCS-5022 SCS-5173 SCS-5165 SCS-5139 SCS-5135 SCS-5074 SCS-5175 SCS-5155 SCS-5177 SCS-5166 SCS-5119 SCS-5137 SCS-5122 SCS-5124 130BBL: TA-172 SCS-5065 CHVT0723 1-1805 MANIFEST NUMBER 018477046FLE 018919183FLE 028061376JJK 025074814JJK 007237132GBF 018470579FLE 018476383FLE 018446868FLE 018470579FLE 017155680FLE 018476800FLE 018476801FLE 024137247JJK 007370194GBF 025115227JJK 007370192GBF 007371206GBF 024215041JJK 024215032JJK 024215040JJK 024215033JJK 017118700JJK 024215038JJK 024215034JJK 024215037JJK 024215039JJK 024215036JJK 019544021JJK 024215035JJK 019258889FLE 026391247JJK 017556267FLE 018355128FLE 017147496FLE # OF DRUMS 6 8 2 2 13 8 12 1 12 3 2 4 2 5 2 8 14 14 13 11 6 2 6 2 4 5 3 3 4 23 1 2 4 4 Appendix 10 Page 1 of 101 Appendix 10 Page 2 of 101 Appendix 10 Page 3 of 101 Appendix 10 Page 4 of 101 Appendix 10 Page 5 of 101 Appendix 10 Page 6 of 101 Appendix 10 Page 7 of 101 Appendix 10 Page 8 of 101 Appendix 10 Page 9 of 101 Appendix 10 Page 10 of 101 Appendix 10 Page 11 of 101 Appendix 10 Page 12 of 101 Appendix 10 Page 13 of 101 Appendix 10 Page 14 of 101 Appendix 10 Page 15 of 101 Appendix 10 Page 16 of 101 Appendix 10 Page 17 of 101 Appendix 10 Page 18 of 101 Appendix 10 Page 19 of 101 Appendix 10 Page 20 of 101 Appendix 10 Page 21 of 101 Appendix 10 Page 22 of 101 Appendix 10 Page 23 of 101 Appendix 10 Page 24 of 101 Appendix 10 Page 25 of 101 Appendix 10 Page 26 of 101 Appendix 10 Page 27 of 101 Appendix 10 Page 28 of 101 Appendix 10 Page 29 of 101 Appendix 10 Page 30 of 101 Appendix 10 Page 31 of 101 Appendix 10 Page 32 of 101 Appendix 10 Page 33 of 101 Appendix 10 Page 34 of 101 Appendix 10 Page 35 of 101 Appendix 10 Page 36 of 101 Appendix 10 Page 37 of 101 Appendix 10 Page 38 of 101 Appendix 10 Page 39 of 101 Appendix 10 Page 40 of 101 Appendix 10 Page 41 of 101 Appendix 10 Page 42 of 101 Appendix 10 Page 43 of 101 Appendix 10 Page 44 of 101 Appendix 10 Page 45 of 101 Appendix 10 Page 46 of 101 Appendix 10 Page 47 of 101 Appendix 10 Page 48 of 101 Appendix 10 Page 49 of 101 Appendix 10 Page 50 of 101 Appendix 10 Page 51 of 101 Appendix 10 Page 52 of 101 Appendix 10 Page 53 of 101 Appendix 10 Page 54 of 101 Appendix 10 Page 55 of 101 Appendix 10 Page 56 of 101 Appendix 10 Page 57 of 101 Appendix 10 Page 58 of 101 Appendix 10 Page 59 of 101 Appendix 10 Page 60 of 101 Appendix 10 Page 61 of 101 Appendix 10 Page 62 of 101 Appendix 10 Page 63 of 101 Appendix 10 Page 64 of 101 Appendix 10 Page 65 of 101 Appendix 10 Page 66 of 101 Appendix 10 Page 67 of 101 Appendix 10 Page 68 of 101 Appendix 10 Page 69 of 101 Appendix 10 Page 70 of 101 Appendix 10 Page 71 of 101 Appendix 10 Page 72 of 101 Appendix 10 Page 73 of 101 Appendix 10 Page 74 of 101 Appendix 10 Page 75 of 101 Appendix 10 Page 76 of 101 Appendix 10 Page 77 of 101 Appendix 10 Page 78 of 101 Appendix 10 Page 79 of 101 Appendix 10 Page 80 of 101 Appendix 10 Page 81 of 101 Appendix 10 Page 82 of 101 Appendix 10 Page 83 of 101 Appendix 10 Page 84 of 101 Appendix 10 Page 85 of 101 Appendix 10 Page 86 of 101 Appendix 10 Page 87 of 101 Appendix 10 Page 88 of 101 Appendix 10 Page 89 of 101 Appendix 10 Page 90 of 101 Appendix 10 Page 91 of 101 Appendix 10 Page 92 of 101 Appendix 10 Page 93 of 101 Appendix 10 Page 94 of 101 Appendix 10 Page 95 of 101 Appendix 10 Page 96 of 101 Appendix 10 Page 97 of 101 Appendix 10 Page 98 of 101 Appendix 10 Page 99 of 101 Appendix 10 Page 100 of 101 Appendix 10 Page 101 of 101 APPENDIX 11. DOCUMENTATION OF HAZARDOUS WASTE GOING TO SWS'S SECONDARY TRANSFER FACILITY Outbound Shipment #: 90738 Disposal Load #: Order # Generator 564501 Bestolife 564501 Bestolife 564501 564501 Bestolife Bestolife 564501 Bestolife 570806 Bestolife 570806 Bestolife 570806 Bestolife 570806 Bestolife 570806 Bestolife 570806 Bestolife SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Shipment Date: 02-09-2024 Truck #: Disposal Site: US Ecology Texas, Inc. Trailer #: 706 Manifest # 017984261FLE 017984261FLE 017984261FLE 017984261FLE 017984263FLE 017984294FLE 017984294FLE 017984294FLE 017984294FLE 017984296FLE 017984296FLE Manifest Disposal # Profile Name Approval # Debris & PPE contaminated with Lead Debris & PPE contaminated with Lead Grease contaminated with Lead Lead Contaminated Dust Empty Supersacks contaminated with Lead Waste Water from Floor Scrubber Debris & PPE contaminated with Lead Debris & PPE contaminated with Lead Grease contaminated with Lead Empty Supersacks contaminated with Lead Lead Contaminated Dust 090120950-0 090120950-0 090120781-0 090120951-0 090120783-0 090120780-0 090120950-0 090120950-0 090120781-0 090120783-0 090120951-0 Waste Product Code 7002 7002 7001 7001 7001 7001 7002 7002 7001 7001 7001 Container Type DM CF DM DM CF TP CF DM DM CF DM Container Size 55 202 55 55 202 275 202 55 55 202 55 Count Weight (Lbs) 4 426.0 1 183.0 7 4381.02 4 848.0 1 145.0 1 2206.0 2 354.0 11 2160.95 2 1107.0 3 911.01 2 774.0 Appendix 11 Page 1 of 33 Comments: Container Type DM CF TP Container Size 55 202 275 Total Count 30 7 1 38 Pallet Spaces 7.5 7.0 1.25 Drum Spaces 30.0 28.0 5.0 Weight (Lbs) 9,696.97 1,593.01 2,206.00 15.75 63.0 13,495.98 Appendix 11 Page 2 of 33 Appendix 11 Page 3 of 33 Appendix 11 Page 4 of 33 Appendix 11 Page 5 of 33 Appendix 11 Page 6 of 33 SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Outbound Shipment #: 92240 Disposal Load #: Shipment Date: 02-21-2024 Truck #: 664 Disposal Site: US Ecology Texas, Inc. Trailer #: 706 Order # 573696 574520 574522 574949 574980 574980 574980 574980 574980 576557 Generator Manifest # Cotac-Group (fka Hoyer Global) 025757684JJK Third Coast Packaging 025757691JJK Third Coast Packaging 025757693JJK Kuraray America, Inc. - Septon 025757710JJK BU Bestolife 024389997JJK Bestolife 024389998JJK Bestolife 024389998JJK Bestolife 024389998JJK Bestolife CBSL TRANSPORTATION SERVICES 024389998JJK 025757883JJK Manifest Disposal # Profile Name Approval # Non-Haz Amines (pH level needed) Glyoxal 40 CCP 6480 Spent Activated Alumina Empty Supersacks contaminated with Lead Lead Contaminated Dust Debris & PPE contaminated with Lead Debris & PPE contaminated with Lead Grease contaminated with Lead 090135236-0 090140381-0 090140510-0 090106011-0 090120783-0 090120951-0 090120950-0 090120950-0 090120781-0 Waste Product Code 7503 7201 7601 7501 7001 7001 7002 7002 7001 Container Type DF TP TP CF CF DM DM CF DM MALEIC ANHYDRIDE 090140705-0 7500 DM Container Size 55 330 275 1 202 55 55 202 55 55 Count Weight (Lbs) 1 435.0 1 242.0 1 2144.0 4 4544.0 4 560.0 2 590.0 6 1254.0 1 158.0 1 536.0 10 5910.0 Appendix 11 Page 7 of 33 Comments: Container Type DF TP TP CF CF DM Container Size 55 330 275 1 202 55 Total Count 1 1 1 4 5 19 31 Pallet Spaces 0.25 1.75 1.25 0.35 5.0 4.75 Drum Spaces 1.0 7.0 5.0 1.4 20.0 19.0 Weight (Lbs) 435.00 242.00 2,144.00 4,544.00 718.00 8,290.00 13.35 53.4 16,373.00 Appendix 11 Page 8 of 33 Appendix 11 Page 9 of 33 Appendix 11 Page 10 of 33 Appendix 11 Page 11 of 33 Appendix 11 Page 12 of 33 Outbound Shipment #: 93183 Disposal Load #: Order # Generator 576553 576553 576553 576553 Third Coast Packaging Third Coast Packaging Third Coast Packaging Third Coast Packaging Comments: SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Shipment Date: 02-28-2024 Truck #: Disposal Site: US Ecology Texas, Inc. Trailer #: Manifest # 025757876JJK 025757876JJK 025757876JJK 025757876JJK Manifest Disposal # Profile Name Approval # Aminoethylpiperazine (AEP) HAZ (D002) Organic Basic Liquids Ucarsol Mixtures Non-Haz DOT Regulated Liquids (Class 8) 090133986-0 090135518-0 090130991-0 090133140-0 Waste Product Code 7601 7201 7503 7503 Container Type TP TP TP TP Container Size 275 275 275 275 Count Weight (Lbs) 3 2985.0 1 638.0 13 7956.0 5 3685.0 Container Type TP Container Size 275 Total Count 22 22 Pallet Spaces 27.5 Drum Spaces 110.0 Weight (Lbs) 15,264.00 27.5 110.0 15,264.00 Appendix 11 Page 13 of 33 Appendix 11 Page 14 of 33 SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Outbound Shipment #: 97964 Disposal Load #: Shipment Date: 04-04-2024 Truck #: Disposal Site: US Ecology Texas, Inc. Trailer #: 702 Order # 580935 580935 580935 580935 580935 580935 585693 585693 585693 586476 Generator Manifest # Bestolife 025124524JJK Bestolife Bestolife Bestolife Bestolife Bestolife Bestolife 025124524JJK 025124524JJK 025124524JJK 025124524JJK 025124524JJK 025124539JJK Bestolife 025124539JJK Bestolife 025124539JJK NRG Texas Power LLC - WA 025758101JJK Parish Manifest Disposal # Profile Name Approval # Debris & PPE contaminated with Lead Debris & PPE contaminated with Lead Grease contaminated with Lead Waste Water from Floor Scrubber Empty Supersacks contaminated with Lead Lead Contaminated Dust Debris & PPE contaminated with Lead Empty Supersacks contaminated with Lead Debris & PPE contaminated with Lead Debris contaminated with Mercury 090120950-0 090120950-0 090120781-0 090120780-0 090120783-0 090120951-0 090120950-0 090120783-0 090120950-0 090134246-0 Waste Product Code 7002 7002 7001 7001 7001 7001 7002 7001 7002 7002 Container Type DM CF DM TP CF DM DM CF CF DF Container Size 55 202 55 275 202 55 55 202 202 2 Count Weight (Lbs) 11 2365.0 2 334.0 3 1521.0 1 2329.0 1 142.0 2 574.0 4 860.0 1 138.0 4 676.0 1 2.0 Appendix 11 Page 15 of 33 Comments: Container Type DM CF TP DF Container Size 55 202 275 2 Total Count 20 8 1 1 30 Pallet Spaces 5.0 8.0 1.25 0.01 Drum Spaces 20.0 32.0 5.0 0.04 Weight (Lbs) 5,320.00 1,290.00 2,329.00 2.00 14.26 57.04 8,941.00 Appendix 11 Page 16 of 33 Appendix 11 Page 17 of 33 Appendix 11 Page 18 of 33 Appendix 11 Page 19 of 33 Appendix 11 Page 20 of 33 SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Outbound Shipment #: 99262 Disposal Load #: Order # 570521 587749 Generator Brenntag Southwest Inc.Haden Rd Cotac-Group (fka Hoyer Global) Shipment Date: 04-17-2024 Truck #: 661 Disposal Site: Systech Environmental Corporation Trailer #: 705 Manifest # Manifest Disposal # Profile Name 025757618JJK Solvent Flush Approval # Waste Container Product Code Type PQ-221228-023-F 3000 DM Container Size 55 Count Weight (Lbs) 80 33680.0 020119760JJK 2-ETHYLHEXANOL PQ-240208-009-F 3000 DM 55 3 1389.0 Comments: Container Type DM Container Size 55 Total Count 83 83 Pallet Spaces 20.75 Drum Spaces 83.0 Weight (Lbs) 35,069.00 20.75 83.0 35,069.00 Appendix 11 Page 21 of 33 Appendix 11 Page 22 of 33 Appendix 11 Page 23 of 33 SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Outbound Shipment #: 99313 Disposal Load #: Shipment Date: 04-17-2024 Truck #: 661 Disposal Site: US Ecology Texas, Inc. Trailer #: 633037 Order # 586485 587709 587709 Generator Manifest # Bestolife 025124541JJK Kuraray America, Inc. - Septon 020119757JJK BU Kuraray America, Inc. - Septon 020119757JJK BU Manifest Disposal # Profile Name Approval # Used Filters from Dust 090120784-0 Collector PMHS Product (TSF484) 090112386 Spent Activated Alumina 090106011-0 Waste Product Code 7002 7503 7501 Container Type CF TP CF Container Size 202 275 1 Count Weight (Lbs) 10 1900.0 1 2020.0 10 12240.0 Comments: Container Type CF TP CF Container Size 202 275 1 Total Count 10 1 10 21 Pallet Spaces 10.0 1.25 0.88 Drum Spaces 40.0 5.0 3.5 Weight (Lbs) 1,900.00 2,020.00 12,240.00 12.13 48.5 16,160.00 Appendix 11 Page 24 of 33 Appendix 11 Page 25 of 33 SPECIALIZED OUTBOUND SHIPMENT TO MILLER ROAD Outbound Shipment #: 100283 Disposal Load #: Shipment Date: 04-26-2024 Truck #: 658 Disposal Site: Systech Environmental Corporation Trailer #: H04474 Order # 579344 579590 579590 579590 579590 586551 589151 589162 591557 591557 591605 593212 593212 593212 Generator Manifest # Channell 025124521JJK City of Houston- Houston Police Department City of Houston- Houston Police Department City of Houston- Houston Police Department City of Houston- Houston Police Department HOOVER CIRCULAR SOLUTIONS HOUSTON Third Coast Packaging NOV - Conroe Park West SWS019764 SWS019764 SWS019764 SWS019764 020119727JJK 020119790JJK 020119794JJK Third Coast Packaging 020119832JJK Third Coast Packaging 020119832JJK Kuraray America, Inc. - Poval 020119834JJK Plant SPECIALIZED WASTE SYSTEMS, INC. SPECIALIZED WASTE SYSTEMS, INC. SPECIALIZED WASTE SYSTEMS, INC. 020119890JJK 020119890JJK 020119890JJK Manifest Disposal # Profile Name WASHWATER IMPACTED WITH POLYLITE Off Spec Hydrocarbon Fuels Off Spec Hydrocarbon Fuels Off Spec Hydrocarbon Fuels Off Spec Hydrocarbon Fuels Flammable Products Approval # Waste Product Code PQ-240220-006-F 3006 PQ-240213-014-F PQ-240213-014-F PQ-240213-014-F PQ-240213-014-F PQ-230803-026-F 3000 3000 3000 3000 3000 Container Type TP DF DF DM DM DM Flammable liquids Used Methanol Diacetone Alcohol Sample Retains Silver Nitrate Process PVAC Paste (Limit 33 Drums / 6 Totes) Paint & Paint Related Materials UW Paint & Paint Related Materials UW Paint & Paint Related Materials UW PQ-220207-010-F PQ-210104-006-F PQ-240415-006-F PQ-231024-014-F PQ-190409-020-F PQ-170113-002-F PQ-170113-002-F PQ-170113-002-F 3000 DM 3000 DF 3505 DF 3000 DM 3015 DM 3500 DM 3502 DM 3501 DM Container Size 275 95 55 85 55 55 55 14 55 55 30 55 55 55 Count Weight (Lbs) 4 8604.0 3 2526.9 1 480.7 5 3844.5 2 1005.4 5 2245.0 1 460.0 1 70.0 1 10.0 2 280.0 20 4320.0 1 499.79 1 499.78 17 8496.43 Appendix 11 Page 26 of 33 Comments: Container Type TP DF DF DM DM DF DM Container Size 275 95 55 85 55 14 30 Total Count 4 3 2 5 29 1 20 64 Pallet Spaces 5.0 1.12 0.5 1.88 7.25 0.17 5.0 Drum Spaces 20.0 4.5 2.0 7.5 29.0 0.7 20.0 Weight (Lbs) 8,604.00 2,526.90 490.70 3,844.50 13,486.40 70.00 4,320.00 20.92 83.7 33,342.50 Appendix 11 Page 27 of 33 Appendix 11 Page 28 of 33 Appendix 11 Page 29 of 33 Appendix 11 Page 30 of 33 Appendix 11 Page 31 of 33 Appendix 11 Page 32 of 33 Appendix 11 Page 33 of 33 APPENDIX 12. SWS SOPS FOR CONTAINER AND TANK CLEANING Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 Standard Operating Procedure Container Washout Process General This SOP addresses container acceptance, tank cleaning, and washout procedures, general safety, and health requirements for the washout facility. Key Responsibilities Supervisors must evaluate all incoming portable tanks, containers, or work areas to determine if any work areas are confined spaces. The supervisor must inform exposed employees by posting danger signs or by any other equally effective means of the existence and location of and the danger posed by the permit spaces. Note: A sign reading "DANGER - PERMIT-REQUIRED CONFINED SPACE, DO NOT ENTER" or using other similar language would satisfy the requirement for a sign in OSHAs Confined Space standard CFR1910.146. Please refer to the TAS EHS Manual or TAS Confined Space safety program if required. Supervisors must determine, administer, and implement safe work procedures and appropriate safe limits for employee's exposure to hydrocarbon vapors and gases and toxic gases, and required oxygen concentrations both when working outside of tanks and when entering and working inside of tanks (Confined Spaces) during tank cleaning operations, in accordance with applicable OSHA Confined Space standard CFR1910.146. The safe work procedures should include the Control of Hazardous Energy (Lock Out Tag Out) OSHA standard CFR1910.17 if applicable. Please refer to the TAS Lockout Tagout safety program if required. Employees must be familiar with the safe operating functions and major work activities for tank cleaning, washout procedures, key operations, work equipment, or tools that will be used on the job. Employees must comply with all company EHS policies and OSHA regulations, have knowledge of hazards associated with confined space hazards, control of hazardous energy, and other hazards associated with the job. Employees must use ANSI-rated Personal Protective Equipment (PPE) when required. PPE is designed to protect workers from serious workplace injuries or illnesses resulting from contact with chemicals, physical, electrical, mechanical, or other workplace hazards. Besides face shields, safety glasses, hard hats, and safety shoes, protective equipment includes a variety of devices such as goggles, coveralls, gloves, vests, earplugs, and respirators. Employees must wear PPE in accordance with the job they are doing. Please refer to the TAS EHS Manual or TAS Employee Handbook for more information if required. Appendix 12 Page 1 of 8 Page 1 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 Acceptance Procedures ALL INCOMING CONTAINERS The attached Washout Form will be completed fully for each container processed and washed. Must have a Manifest, SDS or BOL to identify "last contained". Equipment such as PPE, atmospheric testing equipment, communications equipment, alarm systems, and rescue equipment must be available if required. Receiving personnel will inspect paperwork to determine if hazardous or nonhazardous materials, chemicals, toxic gas, or flammable vapors are present. Receiving personnel will use proper PPE, and check air quality with a portable multigas detector (e.g., Altair or Drager 4x or 5x gas meter calibrated per the manufacture instructions) and determine if container is RCRA empty. Personal H2S monitors or 4 Gas meters may also be worn during tank cleaning jobs. Receiving personnel will determine that atmospheric readings are less than [LEL or COMB] flammable gas, vapors, or dust are less than (10 percent) [CO]carbon monoxide PEL are less than (50 parts per million) [O2] oxygen concentration below 19.5 percent or above 23.5 percent [H2S] hydrogen sulfide PEL are less than (15 parts per million) If required for confined space. If other toxic gases [OSHA PEL] atmospheric readings are too high, the container will be resealed and is rejected for cleaning. *** Washout only receives RCRA empty containers. Container is then vented OR detergent/deodorizer is put in tank to obtain acceptable atmospheric levels. Additional vapor and gas freeing (degassing) methods may be used to obtain acceptable entry conditions if required. Acceptable entry conditions must be tested and verified through appropriate testing and monitoring prior to tank entry using confined space procedures. When receiving personal determine container is RCRA empty, container proceeds to the washout area. MANAGING HEELS When receiving personal determines if container has heel, customer is notified with further instructions. o Customer will be charged for management of heel based on agreed upon rates. o Customer agrees to retrieve the heel once containerized. Appendix 12 Page 2 of 8 Page 2 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 o Customer requests TAS to transport heel to final disposal one existing profile o Customer requests TAS profile and dispose of heel Non-hazardous heels will be managed as branch-generated material at TAS washout facility, expressed in cubic yards or gallons. Hazardous heels will be managed as generated by Customer and follow standard TAS profiling and waste service processes. Heel volume will be determined by number of drums filled. If heel cannot be profiled and disposed within ten days, it shall be returned to generator location to await profile approval and disposal. o For return to generator, shipped in on manifest or BOL inbound. Shipment to return to generator will be on a generator signed manifest where generator and receiving facility are the same. When receiving personal confirm from customer to remove heel, container proceeds to the washout area. All hazardous heels will be drummed or put in roll off box. The generator will then manifest the heel to be shipped by the generator to approve disposal facility or go back to the generator. All hazardous heels, drums and containers must leave washout within a ten-day period. All non-hazardous heels will be contained at washout and disposed of at approved site. HAZARD IDENTIFICATION All incoming containers for washout must have a manifest, SDS or BOL stating last contained. Labels on incoming containers of hazardous chemicals must not be removed or defaced. Any labels that are damaged must be immediately replaced with labels containing the same identification, warning, and source information. Safety data sheets (SDS) received with incoming containers to be cleaned of hazardous chemicals must be maintained and made readily accessible to washout employees. Manifest received with incoming containers of hazardous chemicals must be maintained and made readily accessible to washout employees. BOL received with incoming containers of hazardous chemicals must be maintained and made readily accessible to washout employees. Appendix 12 Page 3 of 8 Page 3 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 EXPOSURE MONITORING Employee exposures to OSHA-regulated substances shall not exceed the permissible exposure limits specified in 29 CFR Part 1910, Subpart Z: www.osha.gov Employee exposures to any substance regulated by an OSHA standard shall be measured when there is reason to believe that exposure levels routinely exceed the action or permissible level. Washout employees are to notify the Supervisor if there is suspicion for significant exposure. Results of personal monitoring shall be made available to the affected employee. The washout supervisor must document that sampling results are reviewed with the affected worker(s). MEDICAL PROGRAM Medical surveillance, including medical consultation and follow-up, shall be provided under the following circumstances: Where exposure monitoring reveals exposure over the action level (or PEL if there is no action level) for an OSHA regulated substance which has medical surveillance requirements. Whenever a washout employee develops signs or symptoms that may be associated with a hazardous chemical to which the employee may have been exposed to in the washout. Whenever a spill, leak, or explosion results in the likelihood of a hazardous exposure. For any employees using respiratory protection. All medical examinations shall be provided by a licensed physician or under direct supervision of a licensed physician, at no cost to the employee, without loss of pay, and at a reasonable time and place. First aid kits are to be supplied and maintained by the Supervisor. Additional nonemergency medical assistance, if required, is available at Concentra. Emergency medical assistance is available by calling 911. Where medical consultations or examinations are provided, the examining physician shall be provided with the following information: The identity of the hazardous chemical(s) to which the employees may have been exposed. A description of the conditions under which the exposure occurred including quantitative exposure data if available. Appendix 12 Page 4 of 8 Page 4 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 A description of the signs and symptoms of exposure that the employee is experiencing, if any. If the injured washout employee is transported by ambulance and is unable to provide this information at the time of treatment, a coworker should accompany the employee to the hospital. Medical examinations or consultations provided to employees shall be maintained at Concentra and available per the requirements of 1910.20 "Access to Employee Exposure and Medical Records." A written opinion from the examining physician shall be provided to the washout supervisor . It shall include: Recommendations for further medical follow up. Results of the examination and associated tests. Any medical condition that places the employee at increased risk due to exposure to a hazardous substance found in the workplace. A statement that the employee has been informed of the results of the examination or consultation. Near Miss, Incidents, Accidents, or Injuries ALL INCIDENTS MUST BE CALLED IN IMMEDIATELY TO YOUR SUPERVISOR DURING OR AFTER BUSINESS HOURS 24-7. The Supervisor Incident form must be completed immediately by a Supervisor, then uploaded into the EHS Momentum System, with additional documents e.g., photos, JHA, Confined Space Permit, etc. Additionally, you must immediately call a Safety Manager, Safety Director, or Human Resource Manager to verbally report the incident or accident 24-7. Injuries requiring first aid may be treated using the first aid kit provided/maintained by the Supervisor in each area. Emergency transport (ambulance) shall be contacted to respond to injuries requiring more extensive treatment that are life-threatening. EMERGENCY EQUIPMENT Each washout employee shall be familiar with the location, application, and correct ways to operate the following equipment. Fire extinguishers Fire alarms Safety showers Appendix 12 Page 5 of 8 Page 5 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 Eye wash stations First aid kits Chemical response spill kits Emergency shut-off on equipment Location of emergency telephone numbers and telephones. Safety Showers and Eyewashes Safety showers and eyewashes should be within the work area for immediate emergency use if required. Fire Extinguishers It is the responsibility of the general manager to oversee, select, maintain, and properly locate the fire extinguisher(s) in each washout. Fire extinguishers should be provided within 30 feet of travel from the fire hazard(s) and located along normal paths of travel. Access to fire extinguishers must be maintained and the location should be conspicuously marked. The following items should be inspected monthly by washout personnel: o Extinguisher(s) are in designated locations. o Clear unobstructed access is maintained. o The pin should be in place and attached with an unbroken wire. o The indicator should be on full. o There should be no indication of physical damage. First Aid Kits First aid kits should be available and maintained for treatment of minor injuries or for short-term emergency treatment before getting medical assistance. First aid kits are to be inspected monthly and refilled as necessary. EMERGENCY PROCEDURES Prevention is necessary to ensure that emergencies do not occur. No emergency plan will do all things for all emergency situations. Preventive measures include employee training and facility inspection programs. Appendix 12 Page 6 of 8 Page 6 of 8 Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 EMPLOYEE TRAINING Before the initial work assignment begins, the employer must provide proper training for all workers who are required to work in tank cleaning, tank washouts, and confined spaces if required. Additional training is required when: The job duties change, a significant change occurs in the tank cleaning process, confined space program, or confined space operation presents any new hazard; or when an employee's job performance shows deficiencies. In addition to this training, rescue team members also require training in CPR and first aid. Employers must certify that this training has been provided. All washout employees shall be trained on the hazards of chemicals present in their work area. The Supervisor is responsible for assuring all washout employees are appropriately trained. The aim of the training program is to assure that all individuals at risk are adequately informed about the work in the washout, its risks, and what to do if an accident occurs. This training shall be provided at the time of an employee's initial assignment to a work area where hazardous chemicals are present. All employees must also be trained and oriented by the LS/PI concerning washout standard operating procedures. Appendix 12 Page 7 of 8 Page 7 of 8 WASHOUT FORM Subject Policy/SOP name Department Department Effective 00/00/0000 Number 000A.01 Appendix 12 Page 8 of 8 Page 8 of 8