Document evqYJ1abaEyy8kGLwR9yRb37M
Resin Grade
sbestos
Effective, low-cost thickening agent and thixotrope for epoxy resin systems Imparts excellent viscosity control to resin systems (coatings, adhesives, sealants, caulks, mastics)
KMX 02079
... a highly purified fiber product that is an effective, low-cost thickening agent and thixotrope for epoxy resin systems. By means of a special refining technique developed by UNION CARBIDE, CALIDRIA Resin-Grade 144 Asbestos is made completely grit-free and non-abrasive--this latter char acteristic makes it especially valuable in spray application.
Other desirable features of CALIDRIA Resin-Grade 144 Asbestos include:
. Disperses easily in liquid resin or hardener with a "Cowles" Dissolver or similar mixers
. Overmixing will not destroy the thixotropy of the resin-asbestos mixture
Epoxy systems containing CALIDRIA Resin-Grade 144 Asbestos have excellent aging characteristics
. Reduced dust
Unlike other thixotropes, it is effective with amine hardeners
CALIDRIA Resin-Grade 144 Asbestos is substantially lower in cost than commonly used refined silicas or modified clays
No amine salts are necessary for viscosity build-up or thixotropic stabili zation (with the exception of the low-viscosity, cycloaliphatic epoxides)
Typical
physical properties
Specific Gravity.........................................................................2.45 Moisture Content, % by wt..................................... 2.0, maximum Surface Area, sq. meters per gram................................60, appr. Reflectance, G. E. Brightness............................................... 72-76 Nature of Surface Charge......................Electropositive (cationic) pH in Water.................................................................................9.5 Bulking Value, gallons per 100 lb.............................................4.8 Oil Absorption (DOP), pounds per 100 lb.........................120-140 Refractive Index, n025 C................................................1.54-1.56 Wet Bulk Density in Water, ml.
as received, 20 g. per liter; 3-hr. settling..................... .700 after dispersion, 2 g. per liter; 1-hr. settling............900-1,000 Dry Bulk Density, lb. per cubic foot............................................. 4 Shipping Density, lb. per cubic foot..................................... 12-14 Standard Package Weight, lb......................................................35 % Magnetite................................................................................0.6 Screen Size, Typical; % plus 325 mesh.................................... Nil Fiber Diameter, microns........................................................ 0.025 Length/Diameter, microns............................................... 200 avg.
(1000 maximum)
IMPORTANT: This information is not to be taken as a warranty or representation lor which we assume legal responsibility nor as permission or recommendation to practice any patented invention without a license. It is offered solely for your consideration, investiga tion, and verification.
BAKEUTE, CALIDRIA and UNION CARBIDE are trade marks of Union Carbide Corporation, U. S. A.
1967, 1968, 1969 by Union Carbide Corporation.
Typical applications
Einnno 1 thickening efficiency in
riyUl V I LIQUID EPOXY RESINS
Figure 1 illustrates the effective, low-cost thickening and viscosity control properties of CALIDRIA Resin-Grade 144 Asbestos in epoxy resin systems. It compares relative differ ences in viscosity of BAKELITE Epoxy Resin ERL-2774 solu tions containing equivalent concentrations of CALIDRIA R-G 144 Asbestos, micro-crystalline silicate, and pyrogenic silica.
Figure 2 illustrates the ability of CALIDRIA R-G 144 Asbestos to control viscosity in two different solvent-epoxy systems used in many epoxy coatings and paints.
inn no 0 viscosity characteristics of cal/dr/a
nyui 0 4 R-G 144 IN BAKELITE* EPOXY SOLUTIONS
Resin and amine hardener evaluation
METHOD OF INCORPORATING THE THIXOTROPE: In preparing the test samples used in determining data for Tables 1, 2 and 3, the thixotrope--CAL1DRIA Resin-Grade 144 Asbestos--was added to the liquid resin or hardener at 25C. and dispersed in a "Cowles" Dissolver at 2400 rpm. for 5 minutes.
VISCOSITY MEASUREMENTS: Viscosities of the prepared test samples were measured on a Brookfield Model RVF Viscometer at 2 and 20 rpm.
Table 1 shows performance data of bisphenol based resins, BAKELITE ERL-2774 and ERL-2795, with up to 4 PHR. of CALIDR1A Resin-Grade 144 Asbestos. Vertical draw down was excellent, and even higher asbes tos loading should result in even higher verti cal draw-down.
Tallin 1 thickening of bisphenol-based resins
10111V I WITH CAUDRIA RESIN-GRADE 144 ASBESTOS
Ingredient BAKEUTE ERL-2774 CAUDRIA ResinGrade 144 Asbestos Brookfield RVF Viscosity, cps. X 10~*
24 hours 7 days
30 days
Room Temperature 45 days
Parts by Weight
100 100 100 100
12 14
RPM. 2 20
Thixotropic Index
<T. !.)<>
RPM. Thixotropic
(ndix
2 20
(Tele)
RPM. Thixotropic
Index
2 20
(T.l.)
RPM. Thixotropic
Index
2 20
(T.l.)
34 22
1.5 137 39
3.5 250 53
4.7 464 87
5.3
32 20
1.6 132 36
3.6 244 54
4.5 430 76
5.7
<b> (b) (b) (b) (b) (b) (b) (b) (b) 4S0 94 5.1
Vertical Drawdown, mil (c)
<b) (b) <b) 125 (b) (b) (b) 125
Ingredient BAKELITE ERL-2795 CAUDRIA ResinGrade 144 Asbestos
Brookfield RVF Viscosity, cps. X 10~*
24 hours 7 days
30 days
Room Temperature 45 days
100
L
RPM, Thixotropic
2 20 18 3.8
(T.l.) 4.7
16 3.7
4.3
(b) (b)
(b)
Parts by Weight
100 100 100
RPM. 2 20 38 6.3 35 6.8
Thixotropic Index (T.l.)
6.0
5.1
RPM. 2 20 70 h 68 12
Thixotropic Index (T.l.)
6.4
5.5
4
RPM. Thixotropic
Index
2 20
(T.l.)
91 13
6.9
122 22
5.5
(b) (b) (b) (b) (b) (b) 125 25 5.0
Vertical Dratvdown, mil (c)
(b) (b) (b) 80 (b) (b) (b) 70
(a) Thixotropic Index (T. I.)
viscosity at 2 rpm. viscosity at 20 rpm.
(b) Not run.
(c) Vertical Drawdown: A 2-inch wide drawdown wa made on a horizontal sandblasted steel panel. The panel was im mediately raised to a vertical position and any sag noted. If
no sag occurred in 10 minutes, the procedure was repeated
and the thickness increased until sagging occurred.
Table 2 presents data that show the effec tiveness of CAUDRIA Resin-Grade 144 As bestos as a thickener of several types of BAKELITE Amine Hardeners. Generally, other thickeners are not effective with amine hardeners.
UpS calidria Resin-Grade 144
THE DISCOVERY COMPANY
UNION CARBIDE CORPORATION ASBESTOS
270 PARK AVENUE, NEW YORK, N. Y. 10017
Sa/es Offices
United States
ATLANTA, GEORGIA 30329...................................... 17 Executive Park Dr.......................... BALTIMORE, MARYLAND 21207............................. Beltway Bldg., 6707 Whitestone Rd, BOSTON, MASSACHUSETTS 02194...................... 300 First Ave., Needham Hgts......... BUFFALO, NEW YORK 14225..................................3343 Harlem Rd.................................. CHARLOTTE, NORTH CAROLINA 28210................ 6230 Fairview Rd............................... CHICAGO, ILLINOIS 60606......... ............................ 120 South Riverside Plaza.............. CINCINNATI, OHIO 45227......................................West Street and Madisonville Rd... CLEVELAND, OHIO 44114........................................ 1300 Lakeside Ave., N.E..................... CLIFTON. NEW JERSEY 07012............................... 935 Allwood Rd.................................. DALLAS, TEXAS 75207.............................................2710 Stemmons Freeway................. DETROIT, MICHIGAN 48221....................................10421 West Seven Mile Rd................. HOUSTON, TEXAS 77027 ........................................ 3839 West Alabama Ave.................. INDIANAPOLIS, INDIANA 46220............................. 720 Broad Ripple Ave....................... KANSAS CITY (ST. LOUIS SALES OFFICE) ........................................................................... LOS ANGELES, CALIFORNIA 90058.......................2770 Leonis Blvd................................. MEMPHIS (ATLANTA, GA. SALES OFFICE)........................................................................... MINNEAPOLIS, MINNESOTA 55416...................... 3033 Excelsior Blvd............................ MOORESTOWN, NEW JERSEY 08057 .................... Route 38 and Pleasant Valley Rd... NEW YORK, NEW YORK 10017 ............................... 270 Park Ave...................................... PHILADELPHIA (MOORESTOWN. NEW JERSEY SALES OFFICE)....................................... PITTSBURGH, PENNSYLVANIA 15220.................. P'kway Center. 87S Greentree Rd... ST. LOUIS, MISSOURI 63105..................................10 South Brentwood Blvd................. SAN FRANCISCO, CALIFORNIA 94106 .................. 22 Battery SL.................................. SEATTLE, WASHINGTON 98118 ............................. 4726 Rainier Ave., South................
.404-633-6161 .301-944-8211 .617-444-5400 .716-837-6450 .704-364-1400 .312-822-7000 .513-272-0206 .216-6214202
.201-778-2900 .214-631-0010 .313-341-3131 .713-621*1000 .317-255-3181 .913-362-2200 .213-583-3061 .901-396-5375 .612-9274221 .609-235-6200 .212-5514641 215-923-3200 .412-922-5700 314-726-0324 .415-982-1360 .206-723-8660
Asbestos
F-41723B 3/69-3.5 M
PRINTED IN U.S.A.
PRICE LIST:
RG-144
Effective: January 2,1971
I Supersedes: January 31,1970
... a highly refined fiber used as a low-cost, efficient thixotrope and viscosity control agent in epoxy, phenolic, and similar resin compounds used in mastics, adhesives, sealants, caulks, and coatings.
SHIPPING POINTS
King City, Calif. (plant)
Torrance, Calif.
Atlanta, Ga. Cleveland, O. Columbus, 0. Detroit, Mich. Hammond, Ind. St. Louis, Mo. Dallas, Tex. Houston, Tex.
Metuchen, N.J.
NET PRICES - CENTS PER L8. - P.O.B. SHIPPING POINT
Carload, 72,800 lb. 52 pallets
12.0
-
ORDERING QUANTITY Quantities more than 1,400 lb. sold only In full-pallet multiples.
23,800 lb. or moro
17 or more pallets
12.0
8,400 lb. to 22,400 lb.
6 to 16 pallets
15.0
1,400 lb. to 7,000 lb.
1 to 5 pallets
19.0
175 lb. to 1,365 lb.
Less than 1 pallet
25.0
14.0
17.0
21.0
27.0
-
1S.0
18.0
22.0
29.0
-
16.0
19.0
23.0
31.0
PACKAGING INFORMATION
One Package One Pallet 50-ft. Carload 40-ft. Truckload
35 lb. 1,400 lb. 72,800 lb. (52 pallets) 23,800 lb. (17 pallets)
Packages are sealed with polythylene overwrap.
KMX 02080
COMBINED SHIPMENTS - Shipments of one or more pallets of any "Calidria" asbestos product may be combined with one or more pallets of any other "Calidria" product for total quantity price. Less than pallet quantities may not be combined for total quantity price.
IMPORTANT - Payment terms: Net IQth proximo. Minimum order: 175 lb. Prices apply within continental U.S.A. Union Carbide reserves the right to adjust customer's orders to comply with the standard ordering quantities specified above.
UNION CARBIDE CORPORATION * MINING ANO METALS DIVISION 270 PARK AVENUE, NEW YORK, N.Y. 10017
Tni$ oaper cor.;3ns "Calidria'* asbestos T-135, an efficient, low-cost opacifier. It s 80-lb. Fairmount offset produced ov Tileston & Hollingsworth Co., a subsidiary of Diamond International Corporation.