Document emOxxbqRXGEnx9LMxan9VGdpG
CoSlcThLesBteurr,liVngetromnont
Sample Data Summary Package
SDG: 117632
STLS E V E R N
TRENT
November 30, 2006
Mr. Charlie Young Weston Solutions 1400 Weston Way West Chester, PA 19380
STL Burlington 208 South Park Drive, Suite 1 Colchester, VT 05446
Tel: 802 655 1203 Fax: 802 655 1248 www.stl-inc.com
Re: Laboratory Project No. 26000 Case: 26000: SPG: 117632
Dear Mr. Young:
Enclosed are the analytical results for the samples that were received by STL Burlington on October 18th, 2006. Laboratory identification numbers were assigned, and designated as follows:
Lab ID
Client Sample ID
Sample Date
Sample Matrix
Received: 10/18/06 ETR No: 117632
692358 692359 692360 692361 692362 692363 692363DP 692364 692365 692366 692367 692368 692369 692370 692371 692372 692373 692374 692375 692376 692377
DL1F01MSF0030041104 DL1F01MSF0040041104 DL1F01MSF0050041104 DL1F01IPW0010041104 DL1F01IPW0020041104 DL1F01IPW0030041104 DL1 FOI IPW0030REP DL1F01IPW0040041104 DL1F01IPF0020041104 DL1F01IPF0030041104 DL1F01IPF0040041104 DL1F01IPF0050041104 DL3F01MSW0010041105 DL3F01MSW0020041105 DL3F01MSW0030041105 DL3F01MSW0040041105 DL3F01MSW0050041105 DL3F01MSF0010041105 DL3F01MSF0020041105 DL3F01MSF0030041105 DL3F01MSF0040041105
11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/04/04 11/05/04 11/05/04 11/05/04 11/05/04 11/05/04 11/05/04 11/05/04 11/05/04 11/05/04
TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE TISSUE
Documentation of the condition of the samples at the time of their receipt and any exception to the laboratory's Sample Acceptance Policy is documented in the Sample Handling section of this submittal.
Leaders in Environmental Testing
1.1
Severn Trent Laboratories, Inc.
STL
November 30, 2006 Ms. Kelly Spittler Page 2 of 2
In order to accommodate field length limitations in processing the data summary forms, the laboratory did, in certain instances, abbreviate the sample identifiers. Dashes have been removed from the client identifiers in this delivery group. The electronically formatted data provides the full sample identifier.
Lipids: The replicate analysis of the field sample DL2F01IPF0010 yielded a Relative Percent Difference (RPD) that was outside the control limits (0-20%) at 44%. The laboratory attributes this anomaly to sample non-homogeneity.
The analytical results associated with the samples presented in this test report were generated under a quality system that adheres to requirements specified in the NELAC standard. Release of the data in this test report and any associated electronic deliverables is authorized by the Laboratory Director's designee as verified by the following signature.
If there are any questions regarding this submittal, please contact me at 802 655-1203.
S '-------------
Ron pentkowski Project Manager
Enclosure
1 .2
STL Burlington Data Qualifier Definitions
O rg a n ic
U: Compound analyzed but not detected at a concentration above the reporting limit.
J: Estimated value.
N: Indicates presumptive evidence of a compound. This flag is used only for tentatively identified compounds (TICs) where the identification of a compound is based on a mass spectral library search.
P: SW-846: Greater than 40% difference for detected concentrations between two GC columns. Unless otherwise specified the higher of the two values is reported on the Form I.
CLP SOW: Greater than 25% difference for detected concentrations between two GC columns. Unless otherwise specified the lower of the two values is reported on the Form I.
C: Pesticide result whose identification has been confirmed by GC/MS.
B: Analyte is found in the sample and the associated method blank. The flag is used for tentatively identified compounds as well as positively identified compounds.
E: Compounds whose concentrations exceed the upper limit of the calibration range of the instrument for that specific analysis.
D: Concentrations identified from analysis of the sample at a secondary dilution.
A: Tentatively identified compound is a suspected aldol condensation product.
X,Y,Z: Laboratory defined flags that may be used alone or combined, as needed. If used, the description of the flag is defined in the project narrative.
Inorqanic/M etals
E: Reported value is estimated due to the presence of interference.
N: Matrix spike sample recovery is not within control limits.
* Duplicate sample analysis is not within control limits.
B: The result reported is less than the reporting limit but greater than the instrument detection limit.
U: Analyte was analyzed for but not detected above the reporting limit.
Method Codes:
P ICP-AES MS ICP-MS CV Cold Vapor AA AS Semi-Automated Spectrophotometric
FQ A 0 09:04.2 4.06 :3 STL Burlington
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE 3 of 6
PROJECT INFORMATIONClient: W eston Solutions, Inc.
1400 W eston W ay, Bldg. 5-2 W est Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jai K esari
ewe il: i.kesaril5tw estonsolutions.com _
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
\NALYSES REQUESTED
Sampler:
Charles Young
__________
SAMPLE ANALYSIS
P.O. #: Quotation #:
''
Grab Sample Composite No. of Containers PFOA Percent Lipids (STL)*
______ I Collection
ExyLIM S # C lient :Sam jle Identification | l Date DL1 [f T MSF001 0 041104 4-NOV-04
- DL1 Ffo T MSF002 0 041104 4-Nov-04 ~ DL1 F01 M SF003 0 041104 4-Nov-04 DL1 F01 M SF004 0 041104 4-Nov-04 DL1 F01 M SF005 0 041104 4-Nov-04 DL1 F01 IPW001 0 041104 4-Nov-04 DL1 F01 IPW 002 : 0 041104 4-Nov-04 DL1 F01 IPW 003 0 041104 4-Nov-04 DL1 F01 IPW 004 ! 0 041104 4-Nov-04 DL1 F01 IPF002 0 041104 4 -Nov-04
Collection Time 21:00 21:05 21:10 21:15 21:20 21:25 21:30 21:35 21:40 21:45
X X X X X X X X X X
1 1 1 1 1 1 1 1 1
~n
Sample Matrix Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue Tissue
CHAIN OF CUSTODY
.^Relinquished By:
Date a / t/ o y
Cooler ID No.:
T im e
Received By:
cyoo
Fed Ex
Cooler Temp. (C): Date Time
-- j.y '
_________
/// / U . / / ' ------------------ -
H*<tku /fa
-'* L
* Subsample of macerated tissue to be sent to STL for Percent Lipid analyses
C om m ents -
x ; Xi
~X~1 XX XX XX XX XX XX XX XX
PROJECT.REQUIREMENTS . -
Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary Add Raw Data Other:
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE _4_ of _6
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701 -3761 F: 610-701 -7401
Project Manager: Jal Kesari em itil: i.kesari@westonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
A NA LYSES REQ UESTED
I
Sampler:
Charles Young
P.O. #: Quotation #:
Grab Sample Composite No. of Containers
Percent Lipids (STL)*
SAMPLE ANALYSIS
ExyLIMS #
Client Samjpie Identification |
I Collection | Date
DL-1 F01 IPF003 ! 0 041104 4-Nov-04
DL-1 F01 IPF004 0 041104 4-Nov-04
DL-1 F01 IPF005 0 041104 4-Nov-04
DL3 F01 MSW001 0 041105 5-Nov-04
DL3 F01 MSW 002 0 041105 5-Nov-04
DL3 F01 MSW 003 0 041105 5-Nov-04
DL3 F01 MSW 004 0 041105 5-Nov-04
DL3 F01 M SW 005 0 041105 5-Nov-04
DL3 F01 MSF001 0 041105 5-Nov-04
DL3 F01 M SF002 0 041105 S-Nov-04
Collection Tima 21:50 21:55 22:05 7:45 7:47 7:50 7:52 7:55 8:00 8:05
X X X X X X X X X X
Sample
Matrix 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUSTODY
^-"Belinquished tf:
Date
ir ^
C oo ler ID No.:
/T'ifmtde
Received By: Fed Ex
L-- -
Cooler Temp. (C): Date Time
-
Subsample of macerated tissue to be sent to STL for Percent Lipid analyses
Comments
< O Li. 0.
XX XX XX XX XX XX XX XX XX XX
PROJECT REQUIREMENTS
.c Results Deadline:
Laboratory Report Options: Sample Results Only Add C ase Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
1
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3048 Research Drive
State College, PA 16801
PAGE 5 o f 6
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3761 F: 610-701-7401
Project Manager: Jal Kesari emrill: I.kesarliwestonsol utio ns.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler;
Charles Young
P.O. #: Quotation #:
Grab Sample Composite No. Of Containers
PFOA Percent Lipids (STL)*
SAMPLE ANALYSIS
ExyLIMS #
Collection
Client Samipie Identification | | Date DL3 F01 M S F003 0 041105 5-NOV-04 DL3 F01 M SF004 0 041105 5-NOV-04 DL3 F01 M SF005 0 041105 5-N ov-04 DMC F01 IPW 003 0 041105 5-NOV-04 DMC F01 IPW 004 0 041105 5-Nov-04 DMC F01 IPW 005 0 041105 5-NOV-04 DMC F01 M SW 003 0 041105 5-Nov-04 DMC F01 M SW 004 0 041105 5-NOV-04 DMC F01 M S W 005 0 041105 5-Nov-04 DMC F01 M S F002 0 041105 5-Nov-04
Collection
Time 8:10 8:15 8:20 8:20 8:25 8:30 8:45 8:50 8:55 9:10
X X X X X X X X X X!
Sample Matrix 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue 1 Tissue
CHAIN OF CUSTODY
^ -R e lin q u is h e d j*Y :
ate A /r/^ y
s'
Cooler ID No.: y 'w n to
Time
Received By: FedEx
Cooler Temp. (C): Date Time
L ---
-- / / 4 c , / c y /S o o
* Subsample of macerated tissue to be sent to STL for Percent Lipid analyses
Comments XX XX XX XX XX XX XX XX XX XX
PROJECT REQUIREMENTS
t o Results Deadline:
Laboratory Report Options: Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
!|
CHAIN OF CUSTODY / ANALYSIS REQUEST FORM
EXYGEN RESEARCH SAMPLE RECEIVING
T: 814-231-8032
F: 814-231-1580
3117 Research Drive
State College, PA 16801
PAGE _2_ of _4
PROJECT INFORMATION Client: Weston Solutions, Inc.
1400 Weston Way, Bldg. 5-2 West Chester, PA 19380 T: 610-701-3T61 F: 610-701-7401
Project Manager: Jai Kesari email: i.kesari0iwestonsolutions.com
Project Name: Reference No:
Decatur, Alabama 02181-129-081-0001
ANALYSES REQUESTED
Sampler:
Charles Young
P.O. #: Quotation #:
SAMPLE ANALYSIS
ExyLIMS #
Client Sample Identification!"
DL2 F01 IPF003
041021
DL2 F01 IPF004
041021
DL2 F01 IPF005
041021
DL2 F01 IPW001
041021
Collection
Date 21-Oct-04 21 -Oct-04 21 -Oct-04 21-Oct-04
Collection
Time 21:50
22:00
22:10 22:15
1<cS2 o. c zo oo
Sample Matrix Tissue Tissue Tissue Tissue
Comments
DL2 F01 MSF001
041021 21-Oct-04 22:25
Tissue
DL2 F01 MSF002
041021 21-Oct-04 22:30
Tissue
DL2 F01 M SF003
041021 21 -Oct-04 22:35 X
Tissue
DL2 F01 MSF004 DL1 F01 IPF001 DL3 F01 IPF001
CHAIN OF CUSTODY
- R e|inqLH 9h^$y:
Date 10/22/04
041021 21 -Oct-04 22:40
Tissue
041021 21-Oct-04 041021 21 -Oct-04
22:45 22:50
/Jo-Y '?'Tissue
Tissue
CS C d '
' d -
PROJECT REQUIREMENTS
Cooler ID No.:
Cooler Temp. (C):
Time 12:00
Received By: Fed Ex
_----------------------------- ---- -
Date Time 10/22/04 12:00
-***
i/t iotl a m .
0.0
Results Deadline: Laboratory Report Options:
Sample Results Only Add Case Narrative Add Quality Control Summary Add Calibration Summary
Add Raw Data Other:
1
3058 Research Drive
State College, PA 16801 H
Phone: 814-272-1039 Fax: 814-231-1580
Loain
Login Group: L0003772
Login #: Project:
Company Name: Submitted By: Login Type: Started:
3882 P0000760
Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
True True True True
Date Start: Due Date: Login Initiated*:
11/08/2004 11/06/2004
* Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Ammerman, Mark Spread Sample: Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE
Login Notes: Conform Notes: Samples DMC-F01-IPF003-0-041105, DMC-F01-IPF004-0-041105, and DMC-F01-IPF005-0-041105 were not on the chain of custody
. As per Charles young, add the samples to the chain. MSA 11/08/04
Packaae PK0004581
Carton
Date / Condition
Packages / Containers
Shiooer/ ID
Received Date: 11/9/04 8:34 Package & Contents Uncompromised
FEDEX 8443 9556 8032
TemD. Control/Temo.
Dry Ice 0.0
Direction / Handled Bv
RECEIVED Ammerman, Mark
Container# C0049450 C0049451 C0049452 C0049453 C0049454 C0049455 C0049456 C0049457 C0049458 C0049459 C0049460 C0049461 C0049462 C0049463 C0049464 C0049465 C0049466 C0049467
Gross Weiaht 115.30 g 115.40 g 103.20 g 94.40 g 76.80 g 116.50 g 108.30 g 475.60 g 341.90 g 867.10 g 849.30 g 1,415.00 g 1,739.70 g 1,305.70 g
2,149.40 g 71.60 g 165.70 g 77.20 g
Container TvDe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
10/17/2006 Login.rpt
Report Version: O ct12 2006 9:14AM Page 1 of 7
Instance:
R0291811
R0291811
Login
Login Group: L0003772
Login #: Project:
Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*:
3882 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 11/08/2004
11/06/2004
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
True True True True
Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Ammerman, Mark
Spread Sample: Label:
Exygen SD/PI: Flaherty, John
Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE
Login Notes:
Conform Notes: Samples DMC-F01-IPF003-0-041105, DMC-F01-IPF004-0-041105, and DMC-F01-IPF005-0-041105 were not on the chain of custody
. As per Charles young, add the samples to the chain. MSA 11/08/04
Packaae PK0004581
Carton
Packages / Containers
Date / Condition
Shiooer/ ID
Received Date: 11/9/04 8:34 Package & Contents Uncompromised
FEDEX 8443 9556 8032
TemD. Control/TemD.
Dry Ice 0.0
Direction / Handled Bv
RECEIVED Ammerman, Mark
Container# C0049468 C0049469 C0049470 C0049471 C0049472 C0049473 C0049474 C0049475 C0049476 C0049477 C0049478 C0049479 C0049480 C0049481
Gross Weiaht 77.50 g 78.30 g 142.40 g 98.00 g 136.20 g 78.50 g 74.50 g 809.60 g 974.70 g
1,111.20g 1,091.70 g 254.60 g 174.10 g 169.90 g
dH
Container Tvpe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
PK0004582
Received Date: 11/9/04 8:50 Package & Contents Uncompromised
FEDEX 8443 9556 8065
Dry Ice 0.0
RECEIVED Ammerman, Mark
Container# C0049482 C0049483 C0049484 C0049485 C0049486
Gross Weiaht 226.60 g 168.70 g 232.40 g 118.40 g 108.00 g
dH
Container TvDe 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE
Mfa. Lot
Mfa. ID
10/17/2006 Login.rpt
Report Version: O c t1 2 2006 9:14AM Page 2 of 7
Instance:
R0291811
R0291811
Login
Login Group: L0003772
Login #: Project:
Company Name: Submitted By: Login Type: Started: Date Start: Due Date: Login Initiated*:
3882 P0000760 Weston Solutions, Inc. Jaisimha Kesari, P.E., DEE Immediate Receipt of Samples True 11/08/2004
11/06/2004
Conform COC Sample: Conform COC: Conform Sample: Conform Request:
True True True True
* Dates entered into "Login Initiated" field prior to 1/5/06 reflect dates of receipt. The field was formerly called "Received Date"
Received By: Ammerman, Mark Spread Sample: Label: Exygen SD/PI: Flaherty, John Project Title/Type: Analysis of Perfluorooctanoic Acid (PFOA) in Water, Soil, Sediment, Fish, Clams, Vegetation, Small
Mammal Liver and Small Mammal Serum Using LC/MS/MS for the 3M Decatur Monitoring Program / ROUTINE Login Notes: Conform Notes: Samples DMC-F01-IPF003-0-041105, DMC-F01-IPF004-0-041105, and DMC-F01-IPF005-0-041105 were not on the chain of custody
. As per Charles young, add the samples to the chain. MSA 11/08/04
Packaae PK0004582
Carton
Date / Condition
Packages / Containers
ShiDoer/ ID
Received Date: 11/9/04 8:50 Package & Contents Uncompromised
FEDEX 8443 9556 8065
Terno. Control/Tema
Dry Ice 0.0
Direction / Handled Bv
RECEIVED Ammerman, Mark
Container # CO049487 C0049488 C0049489 C0049490 C0049491 C0049492 C0049493 C0049494 C0049495 C0049496 CO049497 C0049498 C0049499 C0049500 C0049501 C0049502 C0049503 CO049504 C0049505
Gross Weiaht 104.50 g 188.20 g 133.20 g 126.50 g 103.70 g 64.20 g 910.20 g 1,094.90 g 983.90 g 112.90 g 111.80 g 88.10 g 177.70 g 67.30 g 69.40 g 45.60 g 232.80 g 287.50 g 222.80 g
dH
Container Type 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag 1 gallon ziploc bag
Preservative NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Mfq. Lot
Mfg. ID
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 3 of 7
Instance:
R0291811
R0291811
Sample ID L0003772-0001
Container C0049450
Matrix SOLID
L0003772-0002
C0049451
SOLID
L0003772-0003
C0049452
SOLID
L0003772-0004
C0049453
SOLID
L0003772-0005
C0049454
SOLID
L0003772-0006
C0049455
SOLID
L0003772-0007
C0049456
SOLID
L0003772-0008
C0049457
SOLID
L0003772-0009
C0049458
SOLID
L0003772-0010
C0049459
SOLID
L0003772-0011
C0049460
SOLID
L0003772-0012
C0049461
SOLID
L0003772-0013
C0049462
SOLID
L0003772-0014
C0049463
SOLID
L0003772-0015
C0049464
SOLID
L0003772-0016
C0049465
SOLID
L0003772-0017
10/17/2006 Login.rpt
SOLID
Login
Fraction Fish
Samples
Sample DBC-F01-MSW001 -0-041104
Date Sampled 11/04/2004
Date Due
Fish DBC-F01-MSW002-0-041104
11/04/2004
11/08/2004
Fish DBC-F01-MSW003-0-041104
11/04/2004
11/08/2004
Fish DBC-F01-MSW004-0-041104
ft
Fish DBC-F01-MSW005-0-041104
ft*: VIfi.
Fish DBC-F01-MSF001-0-041104
Fish DBC-F01-MSF002-0-041104
aS oZ (K$
Fish DBC-F01-IPF004-0-041104 Fish DBC-F01-IPF005-0-041104
sZtoc'_P>. oO5a(7)
Fish DBC-F01 -IPW004-0-041104
11/04/2004 11/04/2004 11/04/2004 11/04/2004 11/04/2004 11/04/2004 11/04/2004
11/08/2004 11/08/2004 11/08/2004 11/08/2004 11/08/2004 11/08/2004 11/08/2004
Fish DBC-F01-IPW005-0-041104
11/04/2004
11/08/2004
Fish DOU-F01-IPW003-0-041104
11/04/2004
11/08/2004
Fish DOU-F01-IPW004-0-041104
11/04/2004
11/08/2004
Fish DOU-F01-I PW005-0-041104
11/04/2004
11/08/2004
Fish DL2-F01-IPW002-0-041104
11/04/2004
11/08/2004
Fish DL1-F01-MSW001 -0-041104
11/04/2004
11/08/2004
Fish DL1-F01-MSW002-0-041104
Report Version: Oct 12 2006 9:14AM Page 4 of 7
11/04/2004
11/08/2004
Instance:
R0291811
R0291811
C0049466
L0003772-0018
C0049467
SOLID
L0003772-0019
C0049468
SOLID
L0003772-0020
C0049469
SOLID
L0003772-0021
C0049470
SOLID
L0003772-0022
C0049471
SOLID
L0003772-0023
C0049472
SOLID
L0003772-0024
C0049473
SOLID
L0003772-0025
C0049474
SOLID
L0003772-0026
C0049475
SOLID
L0003772-0027
C0049476
SOLID
L0003772-0028
C0049477
SOLID
L0003772-0029
C0049478
SOLID
L0003772-0030
C0049479
SOLID
L0003772-0031
C0049480
SOLID
L0003772-0032
C0049481
SOLID
L0003772-0033
C0049482
SOLID
L0003772-0034
SOLID
Login
Fish DL1-F01-MSW003-0-041104 Fish DL1-F01-MSW004-0-041104 Fish DL1-F01-MSW005-0-041104 Fish DL1-F01-MSF001 -0-041104 Fish DL1-F01-MSF002-0-041104 Fish DL1-F01-MSF003-0-041104 Fish DL1-F01-MSF004-0-041104 Fish DL1-F01-MSF005-0-041104 Fish DL1-F01-IPW001-0-041104 Fish DL1-F01-IPW002-0-041104 Fish DL1-F01-IPW003-0-041104 Fish DL1-F01-IPW004-0-041104 Fish DL1-F01-IPF002-0-041104 Fish DL-1-F01-IPF003-0-041104 Fish DL-1-F01 -I PF004-0-041104 Fish DL-1-F01-IPF005-0-041104 Fish DL3-F01-MSW001 -0-041105
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 5 of 7
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Instance:
R0291811
R0291811
C0049483
L0003772-0035
C0049484
SOLID
L0003772-0036
C0049485
SOLID
L0003772-0037
C0049486
SOLID
L0003772-0038
CO049487
SOLID
L0003772-0039
C0049488
SOLID
L0003772-0040
C0049489
SOLID
L0003772-0041
C0049490
SOLID
L0003772-0042
C0049491
SOLID
L0003772-0043
C0049492
SOLID
L0003772-0044
C0049493
SOLID
L0003772-0045
C0049494
SOLID
L0003772-0046
C0049495
SOLID
L0003772-0047
C0049496
SOLID
L0003772-0048
C0049497
SOLID
L0003772-0049
C0049498
SOLID
L0003772-0050
C0049499
SOLID
L0003772-0051
SOLID
10/17/2006 Login.rpt
Login
Fish DL3-F01-MSW002-0-041105 Fish DL3-F01-MSW003-0-041105 Fish DL3-F01-MSW004-0-041105 Fish DL3-F01-MSW005-0-041105 Fish DL3-F01-MSF001-0-041105 Fish DL3-F01-MSF002-0-041105 Fish DL3-F01-MSF003-0-041105 Fish DL3-F01-MSF004-0-041105 Fish DL3-F01-MSF005-0-041105 Fish DMC-F01-IPW003-0-041105 Fish DMC-F01-IPW004-0-041105 Fish DMC-F01-IPW005-0-041105 Fish DMC-F01-MSW003-0-041105 Fish DMC-F01-MSW004-0-041105 Fish DMC-F01-MSW005-0-041105 Fish DMC-F01-MSF002-0-041105 Fish DMC-F01-MSF003-0-041105
Report Version: Oct 12 2006 9:14AM Page 6 of 7
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Instance:
R0291811
R0291811
C0049500
L0003772-0052
C0049501
SOLID
L0003772-0053
C0049502
SOLID
L0003772-0054
C0049503
SOLID
L0003772-0055
C0049504
SOLID
L0003772-0056
C0049505
SOLID
Login
Fish DMC-F01-MSF004-0-041105 Fish DMC-F01-MSF005-0-041105 Fish DMC-F01-IPF003-0-041105 Fish DMC-F01-IPF004-0-041105 Fish DMC-F01-IPF005-0-041105
11/05/2004 11/05/2004 11/05/2004 11/05/2004 11/05/2004
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Login Reviewed By: __________________________________________ Date/Time:
10/17/2006 Login.rpt
Report Version: Oct 12 2006 9:14AM Page 7 of 7
Instance:
R0291811
R0291811
STLS E V E R N
TRENT
Sample Data Summary Package - Geotechnical
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSF0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692358 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.5
Qual.
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSF0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692359 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.4
Qual.
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01MSF0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692360 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.1
Qual. u
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPW0010041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692361 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lip!ds Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL Cone. Qual.
1 0.1
6.6
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPW0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692362 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL Cone. Qual.
1 0.1
10.3
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. OL1F01IPW0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SOGNo.: 117632 Lab Sample ID: 692363 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
Units
DF RL Cone. Qual.
11/27/06
% 1 0.1 13.4
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Duplicate Sample Report Summary
Client Sample No. DL1F01IPW0030REP
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692363DP Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
Sample Result Cone. Qual.
13.4
Duplicate Sample Result
Cone. Qual.
8.6
RPD*
44
* Control Limit for RPD is + /- 20%, unless otherwise specified. Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPW0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692364 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL Cone. Qual.
1 0.1
0.9
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPF0020041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692365 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
8.8
Quai.
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPF0030041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692366 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units
DF RL Cone. Qual.
11/27/06
% 1 0.1 0.1
Printed on: 11/28/06 01:04 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPF0040041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692367 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
1.2
Qual.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL1F01IPF0050041104
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692368 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
3.4
Qual.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSW0010041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSU E % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692369 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
2.7
Qual.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSW0020041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDG No.: 117632 Lab Sample ID: 692370 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/27/06
% 1 0.1 0.9
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSW0030041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692371 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Llpids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/27/06
% 1 0.1 0.9
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSW0040041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692372 Date Received: 10/18/06
Method
LIPIDS
Parameter
VoLipIds Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
1.4
Quai.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSW0050041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692373 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/27/06
% 1 0.1 1.0
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSF0010041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692374 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical
Run Date Batch
Units
DF RL
Cone. Qual.
11/27/06
% 1 0.1 0.2
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSF0020041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692375 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.4
Quai.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSF0030041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692376 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Lipids Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.3
Qual.
Printed on: 11/28/06 01:05 PM
GEOTECHNICAL / GENERAL CHEMISTRY
Sample Report Summary
Client Sample No. DL3F01MSF0040041105
Lab Name: STL BURLINGTON Lab Code: STLVT Matrix: TISSUE % Solids:
Contract: Case No.: 26000 Client: WESTN2
SDGNo.: 117632 Lab Sample ID: 692377 Date Received: 10/18/06
Method
LIPIDS
Parameter
%Liplds Determination
Analytical Analytical Run Date Batch
11/27/06
Units %
DF RL
1 0.1
Cone.
0.3
Quai.
Printed on: 11/28/06 01:05 PM
Percent Lipids Calculations
D ate: Tim e:
11/27/2006 2100
A nalyst: ETR (s):
C lient:
TPB 117632 W ESTN2
S am ple ID
MB112706A 692358 692359 692360 692361 692362 692363 692364 692365 692366 692367 692368 692369 692370 692371 692372 692373 692374 692375 692376 692377
692363DP
Sam ple W eight
(g ) 10.00 9.96 9.98 10.01 10.03 9.99 9.99 10.03 9.98 10.04 9.96 10.05 9.99 10.03 10.00 9.99 10.04 10.00 9.99 10.03 9.96 9.99
D ish ( D ish/R esidue
g) 1.0193 0.9983 1.0098 1.0312 0.9928 0.9936 0.9692 0.9875 1.0288 1.0013 1.0046 0.9984 1.0121 1.0151 1.0196 1.0151 0.9940 0.9988 1.0075 0.9936 0.9961 0.9899
(g ) 1.0188 1.0029 1.0138 1.0321 1.0585 1.0965 1.1030 0.9969 1.1170 1.0028 1.0163 1.0324 1.0388 1.0246 1.0289 1.0286 1.0042 1.0009 1.0115 0.9967 0.9992 1.0761
E x tract Final V olum e (m Ls)
10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10
A liquot U sed in
D eterm ination ( mLs )
1
1 1 1 1 1 1
1
1 1 1 1 1 1 1 1 1 1 1 1 1 1
% L ipids
<0.1 0.5 0.4
<0.1 6.6 10.3 13.4 0.9 8.8
0.1
1.2 3.4 2.7 0.9 0.9 1.4
1.0
0.2 0.4 0.3 0.3 8.6 #DIV/0! #DIV/0! #DIV/0! #DIV/0!
STL Burlington
117632M B112706A
11/28/2006
