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FOR DU PONT USE ONLY Copies co AR226-2763 S, I. du Font de Nemours and Company Haskell Laboratory for Toxicology and Industrial Medicine Elkton Road, Newark, Delaware 19711 HASKELL LABORATORY REPORT NO. 291-81 Material Teeted Octanoic acid, pentadecafluoro-, ammonium salt* Hsskell No. 12,037 t OtherCodes Study Initiated/Completed ------5/20/80 - 6/17/81------ Material Submitted by G. L. Kennedy CR&D Department Baskell Laboratory ORAL LB50 TEST IN GUINEA PIGS Procedure s The teat material, as a auapenaion in corn oil, waa administered by intragastric incubation in single doses Co 6 groups of male end 6 groups of female young adult Duncan Hartley guinea pigs, 10 per group. The surviving guinea pigs were weighed and observed during a 14-day recovery period and thes sacrificed. The LD50 value was calculated from the mortality data using the method of D. J. Finney.** Results: Males Dose Caff/kR) Average Body Weight ) Suspension (7) Average Dose (ml ) Mbrtaiity Ratio LD50*** 1 419 10 2.80 10/10 178 mg/kg 400 492 10 1.97 10/10 300 522 5 3.13 10/10 250 433 5 2.15 9/10 200 461 5 2.13 6/10 150 425 2 3.19 3/10 1 - company Sanillied. Does not contain TSCA CBI Results: (Cont'd.) Females Doee (ng/kg) 670 Averse Body Weight (g) 450 SuBpcnBlon (X) 10 Average Doe (al) 3.02 Mortality Ratio 10/10 LD50*** 217 ag/kg 400 499 10 2.00 10/10 300 477 5 2.86 9/10 250 419 5 2.10 8/10 200 493 5 1.97 1/10 150 411 2 3.09 2/10 Clinical StgM; Malea; Stained and/or wet perineal area, weakneca at all levels tested except 670 and 400 og/kg. Scalned face at 670, 200 and 150 ag/kg. Eyes half closed at 300 and 200 ag/kg. Lacrimatlon at 200 and 150 ag/kg. Salivation at 300 and 150 og/kg. Acaxia at 670 mg/kg. Treaora at 150 mg/kg. Humped posture at 200 og/kg. Height loss at all levels te :d except at 670 and 400 og/kg. All deaths occurred within 1-4 days afeer dofling. 2 - ^mpan3) Sanitized. ^ ^ ^n!l?ii-TSCA cs< Clinical Signs; (Cont'd.) Females; Stained and/or wet perlneal area and weakness at all levels tested except 670 and 400 mg/kg. Convulsions, aeaxia, gasping at 670 ing/kg Eyes half closed at 250 and 150 og/kg. Tremors at 400 ng/kg. Lacrimation at 250 og/kg. Stained face at 200 mg/kg. Lethargy at 150 mg/kg. Weight loss at all levels tested except for 670 ng/kg. All deaths occurred within 1-6 days after dosing. Summary: flfc----j--u----l^------Jft.8 moderately toxic when administered orally te ^%ungaS^^uscBffl'^^^^E"le and resale guinea pigs; its LD50 for males is 178 mg/kg and females 217 ing/kg of body weight. Clinical signs for Bales and females Included: stained and/or wet perineal area, convulsions, gasping, stained face, eyes half-closed, and weight loss. All deaths occurred within 1-6 days after dosing ** Finney, D. J., Probit Analysis, 3rd Ed., 1971, Cambridge University Press. 3 - c^s.----------------- *** 95Z Confidence Limits: Males: Loner: Upper: Slop*: 144 og/kg 202 og/kg 8.9 Feoalea: Lower: Upper: Slope: 187 ag/kg 246 o/kg 8.6 Report by: c\^ '^91} /i y ^' ^^r -- ~ , ^L^U^-^^- ( John A. Hell Technician Reviewed by: Study Director Approved by: Gerald L Kennedy Chief, Acute Invetigtiona Section JAH:jrg Date Issued: June 1, 1981 4 - Company Sanifeed, Qcfis no? Ronlain TSC,S CSs