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EPA Inspection Report - Page 1 of 288
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Region 6 Compliance Assurance and Enforcement Division
INSPECTION REPORT
Inspection Date(s): Media: Regulatory Program(s)
06/27-28/2017 Water
Clean Water Act/ NPDES
Company Name: Facility Name:
Facility Physical Location: (city, state, zip code)
Mailing address:
(city, state, zip code)
County/Parish: Facility Contact:
Wyman-Gordon Forgings, Inc.
Wyman-Gordon - Houston Campus
10825 Telge Road
Houston, Texas 77095
P.O. Box 40456
Houston, Texas 77240-0456
Harries County
Michael O'Brien
) Vice President
mlobrien@wyman.com
FRS Number: Identification/Permit Number: Media Number: NAICS: SIC:
110000462115 TX0042129
3463
Personnel participating in inspection:
Kenneth l. AuBuchon
USEPA/6EN-WMH
Mike O'Brien
Wyman-Gordon- Houston
Jeremy DuMond
Wyman-Gordon- Houston
Aaron Placek
Wyman-Gordon- Houston
Jason Tietze
Wyman-Gordon- Houston
Michael Dupont
Wyman-Gordon
Environmental Engineer Vice President- Houston Director of Operations EHS Manager
EHS I Facilities Manager
Sr. Director, EHS
EPA lead Inspector Signature/Date
Supervisor Signature/Date
Kenneth L Auomhon
Kenneth l. AuBuchon
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Carol Peters
281-983-2151 281-856-3286 281-856-3070 281-856-3264 832-833-6326 508-831-8491
01/08/2018
Date
t/n/>S
Date
6ENFORM-019-R7 (2/15/2017)
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Section I - INTRODUCTION
Wyman-Gordon Forgings / Wyman-Gordon Houston 06/27-28/2017
PURPOSE OF THE INSPECTION
EPA Region 6 inspector Kenneth L. AuBuchon arrived at Wyman-Gordon Forgings Inc. Houston at approximately 9:30 am on June 27, 2017 for an unannounced Compliance Evaluation Inspection (CEI). I met with Aaron Plocek, Wyman-Gordon Houston EHS Manager and Jason Tietze, Wyman-Gordon Houston EHS/Facilities Maintenance Manager, at the Opening Conference. I presented my credentials to both Mr. Plocek and Mr. Tietze and explained that this was an EPA inspection to determine compliance with the facility's National Pollutant Discharge Elimination System (NPDES) permit and Clean Water Act (CWA). The inspection was conducted under the authority of the NPDES permit program, in accordance with the Federal CWA.
This report is based on information supplied by Wyman-Gordon Forgings Inc. representatives (the permittee), observations made by the U.S. EPA inspector, and records and reports maintained by the permittee, the State of Texas, and the U.S. EPA.
FACILITY DESCRIPTION
The Wyman-Gordon Forgings, Inc. facility is located on approximately 330 acres northwest of Houston, Texas and employs approximately 500 people. Wyman-Gordon Forgings, Inc. (Wyman-Gordon) produces two main products: Closed-die forgings used mainly for aerospace applications; and extruded pipe.
The forgings operation begins with metal billets, whose composition are nickel-based and titanium alloys. The billets are heated to forging temperatures and then compressed into the required shape by hydraulic forging presses. After forging, the parts undergo a heat-treating and cooling cycle. The forged parts are then delivered to the onsite machine shop, where various machining processes are preformed prior to product shipment.
The extrusion process starts with metal ingots, mainly composed of carbon steel, although some stainless steel, nickel-based alloys, and titanium alloys are extruded as well. The ingots are heated and extruded into the different types of pipe by the hydraulic extrusion presses. After extrusion, the pipe undergoes a heat-treating and cooling cycle. Various finishing operations are then performed on the pipe prior to shipment, including straightening, sawing, inner and outer diameter grinding, and buffing.
Industrial wastewater is generated from both the forging and the extrusion operations. Pits located at the forging and extrusion process areas collect the operational leaks from the hydraulic press systems, die cooling and cleaning, water quenching, and various water cleaning and cooling operations. Industrial wastewater that accumulates in the pits beneath the forging presses is pumped to storage tanks located on the south side of the Forge Ship. Process wastewater is collected at sumps and pumped to the collection pit at the main wastewater treatment unit (also known as the Baker Unit). The mixed forging and extrusion wastewater passes through a corrugated plate interceptor (CPI) oil/water separator and is then stored in two holding tanks behind the Baker Unit.
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Industrial wastewater drawn from the holding tanks is first mixed with poly-aluminum chloride coagulant. This serves to acidify the wastewater thereby breaking the oil / water emulsion. A flocculent is then added immediately downstream of the coagulant to pull out any suspended solids. The Industrial wastewater is then treated in a Dissolved Air Floatation (DAF) system for removal of the remaining fine solids. Solids are skimmed from the top of the DAF and the treated wastewater is pumped to 1 of 4 industrial treatment wastewater ponds.
After treatment in the Baker Unit, the effluent water is sent to Pond 4, an aerated biodegradation pond, where biological activity further reduces concentrations of BOD, COD, and ammonia. From Pond 4, the wastewater flows to Pond 5, which functions to provide further biodegradation of any remaining organics and ammonia, as well as settling of any suspended biological solids. From Pond 5, the wastewater flows to the Middle Lake (Pond 2). The Middle Lake is the largest of the industrial wastewater ponds and provides a point for final polishing treatment with regards to organics and suspended solids. A portion of the Middle Lake overflows to the Filtered Lake (Pond 3), which is pumped back to the forging and extrusion operations and recycled as wash down water in the process units. Treated wastewater from the Filtered Lake can also be recirculated and utilized as fire suppression system water. Any non-recycled flow is pumped from the Middle Lake to Outfall 002 for discharge. Treated wastewater is only discharged via Outfall 002 when the amount of treated water exceeds the facility's demand for recycled process wastewater.
Storm water from the site is collected in the Storm Water Lake (Pond 1) and discharged through Outfall 001.
Section II - OBSERVATIONS
During the review of the facility's required paperwork, it was recommended that Wyman-Gordon begin implementation of a new prevision under its Draft TPDES Permit TX0042129 (Effective May 1, 2021). This recommended provision requires the permitee to develop and submit a Standard Operating Procedure for calculating and reporting self-monitoring data (Other Requirement No. 11). This recommendation was given due to the inaccurate information submitted on Net-DMRs and the inadequacy of sampling and monitoring conducted and reported by the Wyman-Gordon (Refer to Areas of Concern, Section III of this report).
The following information submitted to TCEQ in Wyman-Gordon's permit renewal application dated February 29, 2016 was not consistent with information provided during the inspection:
1. For Outfall 002's `type of flow measurement device used' the permit application lists a Flow Meter. However, upon review there was no flow meter at Outfall 002. Flow's for outfall 002 are Pump Estimated.
2. The process flow (water balance) provided illustrates a carbon filter and a valve between the Middle Lake (Pond 2) and the Filtered Lake (Pond 3). However, upon review the carbon filter unit had been taken out and/or decommissioned with only an open pipe connecting Ponds 2 and 3.
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3. The process flow (water balance) provided illustrates an API Separator for industrial wastewater that is coming from the Forge Shop before going to the Baker System. However, it was explained that the API Separator was not in use and had been out of operation for some time. 4. Wyman-Gordon listed Blue Bell Manor Utility Company as the waste disposal facility that receives its domestic sewage. However, it was explained that domestic waste is sent to the Gulf Coast Waste Disposal - Washburn Tunnel Facility and no one know where the Blue Bell Manor Utility Company came from. Two oily wastewater streams were reviewed during the inspection. Wyman-Gordon identified the waste streams as a Wastewater Treatment Residual Flocculent (WGF-100015-2450) and an Oily Wastewater (WGF-100015-2451). At the time of the inspection, both were being sent to Petro-Tech Environmental, 8502 Cypress St, Houston, Texas 77012, for oil recovery and disposal. Waste profiling samples were dated April 25, 2012. A tour of the Storm Water Pond (Pond 1), Outfall, the Baker Treatment System, and Ponds 2 through 5 was conducted on 6/28/2017 after the records review was concluded. It was explained that there is no active level alarm at Outfall 001 or its bypass; however, periodical checks are made on the level but not documented. Outfall 001 appeared to have multiple discharge locations due to the non-functional equipment in the area.
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Section III - AREAS OF CONCERN
Requirement A: TPDES Permit No. TX0042129 (Appendices 1); Permit Conditions, 2. Compliance (a) Acceptance of the permit by the person to whom it is issued constitutes acknowledgement and agreement that such person will comply with all terms and conditions embodied in the permit, and the rules and other orders of the Commission. (b) The permittee has a duty to comply with all conditions of the permit. Failure to comply with any permit condition constitutes a violation of the permit and the Texas Water Code or the Texas Health and Safety Code, and is grounds for enforcement action, for permit amendment, revocation, or suspension, or for denial of a permit renewal application or an application for a permit for another facility.
Concern A: The requirements of the permit are not being followed and are not accurately being submitted. Sampling does not adequately represent the facility's discharge. Refer to the following requirements and concerns.
Requirement B: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 002:
Flow Measurement Frequency: Continuous Flow Sample Type: Record.
Concern B: Wyman-Gordon failed to provide a continuous flow measurement device and continuous flow recording device at outfall 002. Flows are `Pump Estimates'.
Requirement C: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 001 and Outfall Number 002: (see Permit)
Concern C1: Wyman-Gordon failed to obtain samples at frequency required by permit. The following table shows flow that was recorded for the month with no samples collected or reported values and no recorded flow. The table was developed from Wyman-Gordon recorded 2016 Outfall Discharges and a 2016 DMR Summary both are contained in Appendices 2.
Month June 2016 (outfall 001) July 2016 (outfall 001) August 2016 (outfall 001) February 2016 (outfall 002) June 2016 (outfall 002) July 2016 (outfall 002) August 2016 (outfall 002)
Recorded Discharge 5,575,500 gallons -0- gallons 10,941,000 gallons 465,000 gallons 522,000 gallons -0- gallons 144,000 gallons
DMR Value NODI-C (No Discharge) DMR has reported values NODI-C (No Discharge) No Sample Data Provided NODI-C (No Discharge) DMR has reported values NODI-C (No Discharge)
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Concern C2: Mr. Plocek explained that, "at a maximum only one sample per month was obtained regardless of flow", this does not meet the requirements of TPDES Permit No. TX0042129. Refer to the following table, which was developed from sample results supplied by Wyman-Gordon contained in Appendices 3. The table shows that only 5 samples were taken for Outfall 002 for the year of 2016. Also it shows the samples were taken with no recorded flows. The table only contains Outfall 002 COD analyses and data but is representative of all required parameters reviewed during the inspection due to the amount of errors with all reporting and sample collection data.)
Sample Collection Date: 3/31/2016 5/24/2016 7/8/2016 8/12/2016 11/11/2016
COD Result mg/L 295 210 244 235 186
Flow at time of sample collection No Recorded Flow No Recorded Flow No Recorded Flow No Recorded Flow No Recorded Flow
DMR Reporting Month 3/2016 5/2016 Not Reported 7/2016 11/2016
DMR Additional Information
No Flow reported in 7/2016 No Flow reported in 8/2016
Concern C3: Wyman-Gordon reported sample results obtained with no discharge on NetDMRs. The following DMR Summary excerpt show COD samples from the above table being reported. This is highlighted by the red box below and Blue numbers above. (The table and DMR excerpt only contain Outfall 002 COD analyses and data but is representative of all required parameters and data reviewed during the inspection).
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Requirement D: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 002: Daily Average (lbs/day) and Daily Maximum (lbs/day). Concern D1: Wyman-Gordon failed to provide loading values as required by the permit for outfall 002 on NetDMRs. During the inspection, no documents were provided of loading calculations and Mr. Plocek stated that, "the numbers that were put on the NetDMRs came directly from the lab reports or the limit on the permit". As explained in Concern C3, invalid data was inputted on NetDMRs. The DMR Summary excerpt and table from Concern C2 shows the COD analytical results provided in mg/L were directly inputted for loading values (lbs/day). This was also observed for all of Outfall 002s reported loading requirements (TSS, Oil & Grease, Ammonia, CBOD). Concern D2: Wyman-Gordon reported erroneous values for results on NetDMRs. During the inspection, no documents were provided of loading calculations and Mr. Plocek stated that, "the numbers that were put on the NetDMRs came directly from the lab reports or the limit on the permit". The blue oval on the following DMR Summary excerpt shows the permit limit value is reported for the Daily MX DMR Values. The DMR excerpt only shows Outfall 002 COD submitted data, but this concern was observed for all submitted data reviewed during the inspection.
Requirement E: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 002: Sample Type is Composite for Total Suspended Solids, Ammonia (as N), Carbonaceous Biochemical Oxygen Demand (5-day), Chemical Oxygen Demand.
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Concern E: Wyman-Gordon failed to properly collect composite samples for Total Suspended Solids, Ammonia (as N), Carbonaceous Biochemical Oxygen Demand (5-day), and Chemical Oxygen Demand. Mr. Plocek said that all samples are collected as grabs and chain of custody records only show single grab samples. Refer to the Chain of Custody records attached to the 2016 Laboratory Analyses for Outfall 002 in Appendices 3.
Requirement F: TPDES Permit No. TX0042129 (Appendices 1); Monitoring and Reporting Requirements; 2. Testing Procedures a. Unless otherwise specified in this permit, test procedures for the analysis of pollutants shall comply with procedures specified in 30 TAC 319.11-319.12...
Concern F1: Wyman-Gordon failed to utilize proper analytical methodology as required by the permit. The method used for Hexavalent Chromium ALS Group USA was SW7196 (a solid waste method) and is not an approved method per 40 CFR 136 for wastewater. See below.
Concern F2: Wyman-Gordon failed to utilize proper analytical methodology as required by permit. Outfall 002 requires a Carbonaceous Biochemical Oxygen Demand (CBOD) analyses to be conducted. ALS Group USA is conducting a Biochemical Oxygen Demand (BOD) and Wyman-Gordon is reporting the BOD as CBOD. See Below.
Requirement G: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 002: Whole Effluent Toxicity (WET); limit 14%; Ceriodaphnia dubia (water flea) [7-day chronic NOEC]
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Concern G: On June 04, 2015 Ceriodaphnia dubia (water flea) failed reproduction testing requirements. On July 14, 2015 Ceriodaphnia dubia (water flea) failed reproduction testing requirements. A TCEQ report dated May 9, 2016 stated: `In the past three years, `Wyman-Gordon' has performed thirteen 24hour acute tests, with seven demonstrations of significate mortality (i.e., seven failures) by the fathead minnow. Therefore, a 24-hour acute WET limit with no compliance period will be added to the permit.' Acute testing by Wyman-Gordon failed on April 18, 2017 and June 6, 2017 (refer to Appendices 4).
Requirement H: TPDES Permit No. TX0042129 (Appendices 1); Effluent Limitations and Monitoring Requirements, Outfall Number 002: Whole Effluent Toxicity (WET); sample type required: 24-hr Composite (refer to Appendices 4).
Concern H: Wyman-Gordon failed to obtain 24-hr Composite samples as required by the permit. Mr. Plocek said that all samples are collected as grabs and chain of custody records only show single grab samples.
Section IV - FOLLOW UP
Due to the amount of unreported, and reported in error data, on NetDMRs, this facility should be reinspected to insure proper reporting procedures have been instituted.
7/19/2017 - E-mail from Jason Tieze regarding documents requested during June 27/28 inspection.
7/21/2017 - FedEx package received with Thumb Drive of documents requested during June 27/28 inspection.
7/24/2017 - E-mail to Jason Tieze regarding receipt of requested documents. Additional request for Bio-monitoring documents was not received.
Section V - LIST OF APPENDICES
Appendices 1 - TPDES Permit No. TX0042129 Appendices 2 - Recorded 2016 Outfall Discharges and 2016 DMR Summary Appendices 3 - 2016 Laboratory Analyses for Outfall 002 Appendices 4 - Whole Effluent Toxicity (WET) Testing Laboratory Results
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Appendix 1 TPDES Permit No. TX0042129
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Appendix 2 Recorded 2016 Outfall Discharges / 2016 DMR Summary
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Outfall 001 1/7/2016 1/8/2016 1/11/2016 1/12/2016
Total AVERAGE
Outfall 001
Total AVERAGE
Outfall 001 3/11/2016 3/14/2016
Total AVERAGE
Outfall 001 4/20-4/22 2016
4/25/2016 4/26/2016 Total AVERAGE
Outfall 001 5/3/2016 5/18/2016 5/19/2016 5/20/2016 5/23/2016 5/31/2016
Total AVERAGE
Outfall 001 6/1/2016 6/2/2016 6/7/2016
Total AVERAGE
Outfall 001 No Discharge Total AVERAGE
Outfall 001 8/17/2016 8/18/2016 8/19/2016 8/22/2016 8/23/2016 8/24/2016 Total AVERAGE
Metals TPDES Limits (mg/l)
AVERAGE
Outfall 001 No Discharge Total AVERAGE
Outfall 001 No Discharge Total AVERAGE
Outfall 001 11/9/2016 Total AVERAGE
Outfall 001 12/5/2016 Total AVERAGE
Start Time 830 730 630 630
Start Time
Stop Time 1700 1600 1630 1230
Stop Time
Start Time 1100 700
Stop Time 3800 1300
Start Time 700 930 630
Start Time 930 1030 630 630 630 615
Start Time 615 515 830
Start Time
Stop Time 5400 1630 1330
Stop Time 1530 2000 2000 2000 800 2000
Stop Time 2000 1315 1300
Stop Time
Start Time 830 700 830 700 630 700
Chromium 2
0
Start Time
Stop Time 1600 1600 1600 1600 1500 1700
Copper 2
0
Stop Time
Start Time
Stop Time
Start Time 630
Stop Time 3030
Start Time 730
Stop Time 3130
Annual Total- gal.
2016 OUTFALL DISCHARGES
Minutes 522 522 600 360
Total Gallons 1,827,000 1,827,000 2,100,000 1,260,000 7,014,000 1,753,500
JANUARY
Outfall 002 1/1-1/4 2016
Total AVERAGE
Minutes 0 0 0
Minutes 1620 360 0
Minutes 2820 420 420
Minutes 360 582 822 822 102 831
Minutes 831 480 282
Minutes 0
Minutes 462 540 462 540 522 600
Total Gallons 0 0 0 0 0
Total Gallons 5,670,000 1,260,000 0 6,930,000 2,310,000
Total Gallons 9,870,000 1,470,000 1,470,000 12,810,000 4,270,000
Total Gallons 1,260,000 2,037,000 2,877,000 2,877,000 357,000 2,908,500 12,316,500 2,052,750
Total Gallons 2,908,500 1,680,000 987,000 5,575,500 1,858,500
Total Gallons 0 0 0
Total Gallons 1,617,000 1,890,000 1,617,000 1,890,000 1,827,000 2,100,000 10,941,000 1,823,500
FEBRUARY
Outfall 002
2/1/2016
2/5/2016
2/8/2016-2/12/2016
Total
AVERAGE
MARCH
Outfall 002
3/21/2016
3/22/2016
3/28/2016
Total
AVERAGE
APRIL
Outfall 002
Total AVERAGE
MAY
Outfall 002 5/4/16 to 5/12/16
Total AVERAGE
JUNE
Outfall 002 6/13/2016 6/20/2016
Total AVERAGE
JULY
Outfall 002
No Discharge
Total
AVERAGE
AUGUST
Outfall 002 8/8/2016
Total AVERAGE
AUGUST 2016 SEMI-ANNUAL AND ANNUAL ANALYSIS
Lead
Manganese
Nickel
Zinc
1.5
3
3
3
0 Minutes
0
Minutes 0
Minutes 1440
Minutes 1440
0
0
0
Total Gallons 0 0 0
SEPTEMBER
Outfall 002
No Discharge
Total
AVERAGE
Total Gallons 0 0 0
Total Gallons 5,040,000 5,040,000 5,040,000
Total Gallons 5,040,000 5,040,000 5,040,000
OCTOBER
Outfall 002
No Discharge
Total
AVERAGE
NOVEMBER
Outfall 002
11/1/2016
Total
AVERAGE
DECEMBER
Outfall 002
12/12/2016
Total
AVERAGE
65,667,000
Start Time 700
Start Time 1300 630 630
Start Time 1100 730 700
Start Time
Start Time 600
Start Time 640 600
Start Time
Start Time 715
TDS 6000
0 Start Time
Start Time
Start Time 630
Start Time 630
Annual Total- gal.
Stop Time 8600
Stop Time 1400 2230 14430
Stop Time 1800 4200 7800
Stop Time
Stop Time 18600
Stop Time 15640 3000
Stop Time
Stop Time 5515
Chlorides 975 0
Stop Time
Stop Time
Stop Time 19830
Stop Time 12630
Minutes 4740 0 0 0
Minutes 60 960
8280
Minutes 420 2082 4260
Minutes 0 0 0
Minutes 10800
0 0 0 0 0
Minutes 9000 1440 0
Minutes 0
Minutes 2880 0 0 0 0 0
Total Gallons 237,000 0 0 0 237,000 59,250
Total Gallons 3,000 48,000
414,000 465,000 155,000
Total Gallons 21,000 104,100 213,000 338,100 112,700
Total Gallons 0 0 0 0 0
Total Gallons 540,000 0 0 0 0 0 540,000 90,000
Total Gallons 450,000 72,000 0 522,000 174,000
Total Gallons 0 0 0
Total Gallons 144,000 0 0 0 0 0 144,000 24,000
Soil Samples-3
Minutes 0
Total Gallons 0 0 0
Minutes 0
Total Gallons 0 0 0
Minutes 11520
Total Gallons 576,000 576,000 576,000
Minutes 7200
Total Gallons 360,000 360,000 360,000
3,182,100
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Outfall 001 1/3/2017 1/18/2017
Total AVERAGE
Outfall 001 2/29/17
Total AVERAGE
Outfall 001
Start Time 700 900
Stop Time 5500 3300
Start Time 600
Stop Time 3000
Start Time
Stop Time
Minutes 2880 1440 0
Minutes 1440
Minutes
2017 OUTFALL DISCHARGES
Total Gallons 10,080,000 5,040,000 0 15,120,000 5,040,000
JANUARY
Outfall 002 1/16/2017 1/23 to 1/27
Total AVERAGE
FEBRUARY
Total Gallons
Outfall 002
5,040,000
4/10/2017
0
5,040,000
Total
2,520,000
AVERAGE
Total Gallons
MARCH
Outfall 002
Start Time 900 700
Stop Time 5300 10900
Start Time 1030
Stop Time 4830
Start Time
Stop Time
Total AVERAGE
Outfall 001 ND
Total AVERAGE
Outfall 001 ND
Total AVERAGE
Outfall 001 6/8/2017
Start Time
Start Time
Start Time 600
Total AVERAGE
Outfall 001
Start Time
Total AVERAGE
Outfall 001
Start Time
Total AVERAGE
Metals TPDES Limits (mg/l)
Chromium 2
0 #DIV/0!
Total AVERAGE
Stop Time
Minutes 0
Total Gallons 0 0 0
APRIL
Outfall 002 ND
Total AVERAGE
Stop Time
Minutes 0
Total Gallons 0 0 0
MAY
Outfall 002 ND
Total AVERAGE
Stop Time 3000
Minutes 1440 0 0 0
Total Gallons 5,040,000 0 0 0 5,040,000 1,260,000
JUNE
Outfall 002 6/9/2017
Total AVERAGE
Stop Time
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
JULY
Outfall 002
Total AVERAGE
Stop Time
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
AUGUST
Outfall 002
Total AVERAGE
AUGUST 2017 SEMI-ANNUAL AND ANNUAL ANALYSIS
Copper
Lead
Manganese
Nickel
Zinc
2
1.5
3
3
3
Start Time
Stop Time
Start Time
Stop Time
Start Time 600
Stop Time 4000
Start Time
Stop Time
Start Time
Stop Time
TDS 6000
Chlorides 975
AVERAGE Outfall 001
Total AVERAGE
Outfall 001
Total AVERAGE
Outfall 001
Total AVERAGE
Outfall 001
Total AVERAGE
0
0
Start Time
Stop Time
Start Time
Stop Time
Start Time
Stop Time
Start Time
Stop Time
Annual Total
0
Minutes 0 0 0 0 0
Minutes 0 0 0 0
Minutes 0 0 0 0
Minutes 0 0 0 0
0
0
0
SEPTEMBER
Total Gallons
Outfall 002
0
0
0
0
0
0
Total
0
AVERAGE
Total Gallons 0 0 0 0 0 0
OCTOBER
Outfall 002
Total AVERAGE
NOVEMBER
Total Gallons
Outfall 002
0
0
0
0
0
Total
0
AVERAGE
DECEMBER
Total Gallons
Outfall 002
0
0
0
0
0
Total
0
AVERAGE
0 Start Time
Start Time Start Time Start Time
25,200,000
Annual Total
0 Stop Time
Stop Time Stop Time Stop Time
Minutes 2640 6120 0
Total Gallons 132,000 306,000 0 438,000 146,000
Minutes 2280
Total Gallons 114,000 0 114,000 57,000
Minutes
Total Gallons
0 #DIV/0!
Minutes 0
Total Gallons 0 0 0
Minutes 0
Total Gallons 0 0 0
Minutes 2040 0 0 0
Total Gallons 102,000 0 0 0 102,000 25,500
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
Minutes 0 0 0 0 0
Total Gallons 0 0 0 0 0 0 0
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
Minutes 0 0 0 0
Total Gallons 0 0 0 0 0 0
654,000
EPA Inspection Report - Page 54 of 288
DMR Summary
Permit TX0042129
Permit Name WYMAN-GORDON FORGINGS LP
Version Nmbr
Curr. Major Minor Status
0 Major
Issue Date 7/18/14
Effective Date
8/1/14
Expiration Date
5/1/18
Version # 0
Outfall 001A
0 00310 BOD, 5-day, 20 deg. C / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Weekly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
C2 Milligrams per Liter DAILY AV 15 C2 0 NODI=C 5.3 NODI=C NODI=C 2 NODI=C 6.2 14.3 3.3 3.3 3.3 5 NODI=C 6 4.2 8.1 NODI=C 3.02 NODI=C NODI=C NODI=C 8.53 4.12 3.08 5.51 NODI=C NODI=C NODI=C
C3 Milligrams per Liter DAILY MX 20 C3 0 NODI=C 5.3 NODI=C NODI=C 3.7 NODI=C 6.2 20 20 20 20 20 NODI=C 20 20 20 NODI=C 20 NODI=C NODI=C NODI=C 20 20 20 20 NODI=C NODI=C NODI=C
0 00340 Oxygen demand, chem. [high level] [COD] / Location 1 / Season 0 / Base
Limit Start Date
6/26/17 3:53 PM
Limit End Date
Sample Type
Frequency of Analysis
Page 1 of 40
EPA Inspection Report - Page 55 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001A
00340 Oxygen demand, chem. [high level] [COD] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Weekly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
C2 Milligrams per Liter DAILY AV 100 C2 20 NODI=C 35 NODI=C NODI=C 15 NODI=C 45 41 33 33 33 27 NODI=C 40 38 37 NODI=C 32 NODI=C NODI=C NODI=C 39 44 33 32 NODI=C NODI=C NODI=C
C3 Milligrams per Liter DAILY MX 150 C3 20 NODI=C 35 NODI=C NODI=C 33 NODI=C 45 150 150 150 150 150 NODI=C 150 150 150 NODI=C 150 NODI=C NODI=C NODI=C 150 150 150 150 NODI=C NODI=C NODI=C
0 00400 pH / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15
Limit End Date 5/1/18
Sample Type GRAB
C1 Standard Units MINIMUM 6 C1 7 NODI=C 7 NODI=C
C3 Standard Units MAXIMUM 9 C3 7 NODI=C 7.1 NODI=C
Frequency of Analysis Daily
6/26/17 3:53 PM
Page 2 of 40
EPA Inspection Report - Page 56 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001A
00400 pH / Location 1 / Season 0 / Base
DMR Values
C1
C3
5/31/15
NODI=C
NODI=C
6/30/15
6
7.1
7/31/15
NODI=C
NODI=C
8/31/15
7.4
7.4
9/30/15
6.98
9
10/31/15
7.35
9
11/30/15
7.35
9
12/31/15
7.08
9
1/31/16
7.3
9
2/29/16
NODI=C
NODI=C
3/31/16
6
9
4/30/16
6
9
5/31/16
7.48
9
6/30/16
NODI=C
NODI=C
7/31/16
6
9
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
6
9
12/31/16
6
9
1/31/17
6
9
2/28/17
6
9
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
0 00530 Solids, total suspended / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16
Limit End Date 5/1/18
Sample Type GRAB
C2 Milligrams per Liter DAILY AV
C2 13.2 NODI=C NODI=F NODI=C NODI=C 2 NODI=C 39 34 24.4 24.4 24 45.6 NODI=C 48.4
C3 Milligrams per Liter DAILY MX 65 C3 13.2 NODI=C NODI=F NODI=C NODI=C 39.2 NODI=C 39 65 65 65 65 65 NODI=C 65
Frequency of Analysis Weekly
6/26/17 3:53 PM
Page 3 of 40
EPA Inspection Report - Page 57 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001A
00530 Solids, total suspended / Location 1 / Season 0 / Base
DMR Values
C2
C3
4/30/16
20
65
5/31/16
43.9
65
6/30/16
NODI=C
NODI=C
7/31/16
10
65
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
40
65
12/31/16
22
65
1/31/17
20
65
2/28/17
12.8
65
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
0 00556 Oil & Grease / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17
Limit End Date 5/1/18
Sample Type GRAB
C2 Milligrams per Liter DAILY AV 10 C2 0 NODI=C 0 NODI=C NODI=C 0 NODI=C 0 0 0 0 0 0 NODI=C 0 0 0 NODI=C 0 NODI=C NODI=C NODI=C 0 0 0 0
C3 Milligrams per Liter DAILY MX 15 C3 0 NODI=C 0 NODI=C NODI=C 0 NODI=C 0 15 15 15 15 15 NODI=C 15 15 15 NODI=C 15 NODI=C NODI=C NODI=C 15 15 15 0
Frequency of Analysis Weekly
6/26/17 3:53 PM
Page 4 of 40
EPA Inspection Report - Page 58 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001A
00556 Oil & Grease / Location 1 / Season 0 / Base
DMR Values
C2
C3
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
5 50050 Flow, in conduit or thru treatment plant / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type ESTIMA
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
A1 Million Gallons per DAILY AV
A2 Million Gallons per DAILY MX
A1 1.516 NODI=C 1.085 NODI=C NODI=C .0375 NODI=C 0 1.89 1.89 1.89 1.89 2.25 NODI=C 1.89 1.89 1.89 NODI=C 1.89 NODI=C NODI=C NODI=C 1.89 1.89 1.89 1.89 NODI=C NODI=C NODI=C
A2 1.75 NODI=C 1.89 NODI=C NODI=C .0375 NODI=C 0 2.31 2.31 2.31 2.31 20 NODI=C 2.31 2.31 2.31 NODI=C 2.31 NODI=C NODI=C NODI=C 2.31 2.31 2.31 2.31 NODI=C NODI=C NODI=C
5 51040 E. coli / Location 1 / Season 0 / Base
Frequency of Analysis Weekly
Limit Start Date 8/1/14 8/1/15
Limit End Date 7/31/15 5/1/18
Sample Type GRAB GRAB
Frequency of Analysis Weekly Weekly
6/26/17 3:53 PM
Page 5 of 40
EPA Inspection Report - Page 59 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001A
51040 E. coli / Location 1 / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
C2
C2
C3
C3
Colony Forming UnitColony Forming UnitColony Forming UnitColony Forming Unit
DAILY AV
DAILY AV
DAILY MX
DAILY MX
126
399
C2
C3
<14
<14
NODI=C
NODI=C
1300
1300
NODI=C
NODI=C
NODI=C
NODI=C
1
140
NODI=C
NODI=C
178
178
126
399
16.7
399
73.58
399
74
399
17
399
NODI=C
NODI=C
387
399
36
399
33
399
NODI=C
NODI=C
126
399
NODI=C
NODI=C
NODI=C
NODI=C
NODI=C
NODI=C
41
399
54
399
45
399
17
399
NODI=C
NODI=C
NODI=C
NODI=C
NODI=C
NODI=C
Outfall 001S
0 01034 Chromium, total [as Cr] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
6/26/17 3:53 PM
Limit End Date 5/1/18
C3 Milligrams per Liter DAILY MX 1 C3 0 .117 0 0
Sample Type GRAB
Frequency of Analysis Once per 6 Months
Page 6 of 40
EPA Inspection Report - Page 60 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001S
01034 Chromium, total [as Cr] / Location 1 / Season 0 / Base 0
01042 Copper, total [as Cu] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C3 Milligrams per Liter DAILY MX 1 C3 .226 .226 .0033 .0033
0 01051 Lead, total [as Pb] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C3 Milligrams per Liter DAILY MX 1 C3 .714 .714 0 0
0 01055 Manganese, total [as Mn] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C3 Milligrams per Liter DAILY MX 2 C3 0 0 .0531 .0531
0 01067 Nickel, total [as Ni] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Once per 6 Months
6/26/17 3:53 PM
Page 7 of 40
EPA Inspection Report - Page 61 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001S
01067 Nickel, total [as Ni] / Location 1 / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C3 Milligrams per Liter DAILY MX 2 C3 .578 .578 0 0
0 01092 Zinc, total [as Zn] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
Limit End Date 5/1/18
C3 Milligrams per Liter DAILY MX 2 C3 .238 .238 .0217 .0217
Sample Type GRAB
Frequency of Analysis Once per 6 Months
Outfall 001Y
0 00940 Chloride [as Cl] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 12/31/15 12/31/16
C3 Milligrams per Liter DAILY MX 975 C3 301 118.2
7 70295 Solids, total dissolved / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 12/31/15
6/26/17 3:53 PM
Limit End Date 5/1/18
C3 Milligrams per Liter DAILY MX 6000 C3 760
Sample Type GRAB
Frequency of Analysis Annual
Page 8 of 40
EPA Inspection Report - Page 62 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 001Y
70295 Solids, total dissolved / Location 1 / Season 0 / Base
DMR Values
C3
12/31/16
285.9
Outfall 002A
0 00300 Oxygen, dissolved [DO] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type GRAB
Frequency of Analysis Twice per Week
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
C1 Milligrams per Liter MO MIN 5 C1 5.92 8.7 6.8 NODI=C NODI=C NODI=C NODI=C NODI=C 5.88 5.31 7.77 7.69 5 9.08 7.53 NODI=C 6.21 NODI=C 6.83 NODI=C NODI=C NODI=C 6.73 6.42 5.92 6 NODI=C NODI=C NODI=C
0 00340 Oxygen demand, chem. [high level] [COD] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Twice per Week
6/26/17 3:53 PM
Page 9 of 40
EPA Inspection Report - Page 63 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
00340 Oxygen demand, chem. [high level] [COD] / Location 1 / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
A1 Pounds per Day DAILY AV 376 A1 76 109.21 53.89 NODI=C NODI=C NODI=C NODI=C NODI=C 41 62 256 256 250 315 295 NODI=C 210 NODI=C 235 NODI=C NODI=C NODI=C 186 264 258 313 NODI=C NODI=C NODI=C
A2 Pounds per Day DAILY MX 563 A2 97.95 127.6 89.32 NODI=C NODI=C NODI=C NODI=C NODI=C 30 271 271 563 563 563 563 NODI=C 563 NODI=C 563 NODI=C NODI=C NODI=C 563 563 563 563 NODI=C NODI=C NODI=C
0 00400 pH / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15
Limit End Date 5/1/18
Sample Type GRAB
C1 Standard Units MINIMUM 6 C1 6.92 7.4 7 NODI=C NODI=C NODI=C NODI=C
C3 Standard Units MAXIMUM 9 C3 7.05 7.6 7.1 NODI=C NODI=C NODI=C NODI=C
Frequency of Analysis Daily
6/26/17 3:53 PM
Page 10 of 40
EPA Inspection Report - Page 64 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
00400 pH / Location 1 / Season 0 / Base
DMR Values
C1
C3
8/31/15
NODI=C
NODI=C
9/30/15
7.5
9
10/31/15
7.28
9
11/30/15
7.38
9
12/31/15
7.44
9
1/31/16
7.45
9
2/29/16
7.7
9
3/31/16
7.48
9
4/30/16
NODI=C
NODI=C
5/31/16
7.23
9
6/30/16
NODI=C
NODI=C
7/31/16
6
9
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
6
9
12/31/16
6
9
1/31/17
6
9
2/28/17
6
9
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
0 00530 Solids, total suspended / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16
Limit End Date 5/1/18
Sample Type COMPOS
A1 Pounds per Day DAILY AV 38 A1 5.42 7.84 1.77 NODI=C NODI=C NODI=C NODI=C NODI=C 38 27 27 27 21.3 21.9 20.4 NODI=C 20.4 NODI=C
A2 Pounds per Day DAILY MX 85 A2 8.41 8.56 2.45 NODI=C NODI=C NODI=C NODI=C NODI=C 45 85 85 85 85 85 85 NODI=C 85 NODI=C
Frequency of Analysis Twice per Week
6/26/17 3:53 PM
Page 11 of 40
EPA Inspection Report - Page 65 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
00530 Solids, total suspended / Location 1 / Season 0 / Base
DMR Values
A1
A2
7/31/16
30
85
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
20.5
85
12/31/16
22.5
85
1/31/17
20.1
85
2/28/17
12.3
85
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
0 00556 Oil & Grease / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
Limit End Date 5/1/18
Sample Type GRAB
A1 Pounds per Day DAILY AV 19 A1 3.16 1.85 .73 NODI=C NODI=C NODI=C NODI=C NODI=C 3.23 5.59 0 0 5.71 9.35 9.79 NODI=C 6.67 NODI=C 0 NODI=C NODI=C NODI=C 2.39 5.82 5.91 10.3 NODI=C NODI=C NODI=C
A2 Pounds per Day DAILY MX 28 A2 3.72 2.04 3.82 NODI=C NODI=C NODI=C NODI=C NODI=C 28 5.59 28 28 28 28 28 NODI=C 28 NODI=C 28 NODI=C NODI=C NODI=C 28 28 28 28 NODI=C NODI=C NODI=C
Frequency of Analysis Twice per Week
6/26/17 3:53 PM
Page 12 of 40
EPA Inspection Report - Page 66 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
00556 Oil & Grease / Location 1 / Season 0 / Base 0
00610 Nitrogen, ammonia total [as N] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Twice per Week
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
A1 Pounds per Day DAILY AV 8 A1 .6 .41 .37 NODI=C NODI=C NODI=C NODI=C NODI=C .41 2.1 .41 .41 8 7 .42 NODI=C .41 NODI=C .41 NODI=C NODI=C NODI=C 8 8 8 8 NODI=C NODI=C NODI=C
A2 Pounds per Day DAILY MX 20 A2 .74 .49 .6 NODI=C NODI=C NODI=C NODI=C NODI=C 20 20 20 20 20 20 20 NODI=C 20 NODI=C 20 NODI=C NODI=C NODI=C 20 20 20 20 NODI=C NODI=C NODI=C
0 01032 Chromium, hexavalent [as Cr] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14 8/1/15
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15
6/26/17 3:53 PM
Limit End Date 7/31/15 5/1/18
Sample Type COMPOS COMPOS
Frequency of Analysis Weekly Weekly
C2 Milligrams per Liter DAILY AV .0132 C2 0
C2 Milligrams per Liter DAILY AV
C3 0
C3 Milligrams per Liter DAILY MX .0279
C3 Milligrams per Liter DAILY MX
Page 13 of 40
EPA Inspection Report - Page 67 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
01032 Chromium, hexavalent [as Cr] / Location 1 / Season 0 / Base
DMR Values
C2
C3
2/28/15
0
0
3/31/15
0
0
4/30/15
NODI=C
NODI=C
5/31/15
NODI=C
NODI=C
6/30/15
NODI=C
NODI=C
7/31/15
NODI=C
NODI=C
8/31/15
NODI=C
NODI=C
9/30/15
.006
.0279
10/31/15
0
.0279
11/30/15
0
.0279
12/31/15
0
.0279
1/31/16
0
.0279
2/29/16
.0023
.0279
3/31/16
0
.0279
4/30/16
NODI=C
NODI=C
5/31/16
0
.0279
6/30/16
NODI=C
NODI=C
7/31/16
0
.0279
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
0
.0279
12/31/16
0
.0279
1/31/17
0
.0279
2/28/17
0
0
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
5 50050 Flow, in conduit or thru treatment plant / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15
Limit End Date 5/1/18
Sample Type Recorder (auto)
A1 Million Gallons per DAILY AV .225 A1 .0347 .045 .02355 NODI=C NODI=C NODI=C NODI=C NODI=C .225 .225 .2 .225
A2 Million Gallons per DAILY MX .55 A2 .045 .045 .03 NODI=C NODI=C NODI=C NODI=C NODI=C .55 .55 .55 .55
Frequency of Analysis Continuous
6/26/17 3:53 PM
Page 14 of 40
EPA Inspection Report - Page 68 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
50050 Flow, in conduit or thru treatment plant / Location 1 / Season 0 / Base
DMR Values
A1
A2
1/31/16
.225
.55
2/29/16
.225
.55
3/31/16
.225
.55
4/30/16
NODI=C
NODI=C
5/31/16
.225
.55
6/30/16
NODI=C
NODI=C
7/31/16
.225
.55
8/31/16
NODI=C
NODI=C
9/30/16
NODI=C
NODI=C
10/31/16
NODI=C
NODI=C
11/30/16
.225
.55
12/31/16
.225
.55
1/31/17
.225
.55
2/28/17
.225
.55
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
5 51040 E. coli / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16
Limit End Date 5/1/18
Sample Type GRAB
C2
C3
Colony Forming UnitColony Forming Unit
DAILY AV
DAILY MX
C2 <14 43 <14 NODI=C NODI=C NODI=C NODI=C NODI=C 129 16.7 73.59 131 70 1 13 NODI=C 54 NODI=C 10 NODI=C NODI=C NODI=C 53
C3 <14 43 <14 NODI=C NODI=C NODI=C NODI=C NODI=C 399 399 399 399 1100 5 399 NODI=C 100 NODI=C 399 NODI=C NODI=C NODI=C 399
Frequency of Analysis Weekly
6/26/17 3:53 PM
Page 15 of 40
EPA Inspection Report - Page 69 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002A
51040 E. coli / Location 1 / Season 0 / Base
DMR Values
C2
C3
12/31/16
121
399
1/31/17
115
399
2/28/17
24
399
3/31/17
NODI=C
NODI=C
4/30/17
NODI=C
NODI=C
5/31/17
NODI=C
NODI=C
8 80082 BOD, carbonaceous [5 day, 20 C] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 1/31/15 2/28/15 3/31/15 4/30/15 5/31/15 6/30/15 7/31/15 8/31/15 9/30/15 10/31/15 11/30/15 12/31/15 1/31/16 2/29/16 3/31/16 4/30/16 5/31/16 6/30/16 7/31/16 8/31/16 9/30/16 10/31/16 11/30/16 12/31/16 1/31/17 2/28/17 3/31/17 4/30/17 5/31/17
Limit End Date 5/1/18
Sample Type COMPOS
A1 Pounds per Day DAILY AV 47 A1 11.47 15.76 11.69 NODI=C NODI=C NODI=C NODI=C NODI=C 41 58 33 46 47 0 0 NODI=C 47 NODI=C 39.7 NODI=C NODI=C NODI=C 46 46 64.7 47 NODI=C NODI=C NODI=C
A2 Pounds per Day DAILY MX 75 A2 15.05 18.77 20.49 NODI=C NODI=C NODI=C NODI=C NODI=C 75 75 75 75 75 71 70 NODI=C 54 NODI=C 75 NODI=C NODI=C NODI=C 75 75 75 74.7 NODI=C NODI=C NODI=C
Frequency of Analysis Twice per Week
Outfall 002S
0 00722 Cyanide, free [amen. to chlorination] / Location 1 / Season 0 / Base
6/26/17 3:53 PM
Page 16 of 40
EPA Inspection Report - Page 70 of 288
DMR Summary
Permit TX0042129
Version # 0 Outfall 002S 00722 Cyanide, free [amen. to chlorination] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .0386 C2 0 0 0 0
C3 Milligrams per Liter DAILY MX .0816 C3 .0816 .0816 .0816 .0816
0 00951 Fluoride, total [as F] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV 1.66 C2 .32 .32 .155 .155
C3 Milligrams per Liter DAILY MX 3.22 C3 3.22 3.22 3.22 3.22
0 01034 Chromium, total [as Cr] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .068 C2 0 0 0 0
C3 Milligrams per Liter DAILY MX .143 C3 .143 .143 .143 .143
0 01042 Copper, total [as Cu] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
6/26/17 3:53 PM
Page 17 of 40
EPA Inspection Report - Page 71 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002S
01042 Copper, total [as Cu] / Location 1 / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .0173 C2 .021 .21 .00796 .00796
C3 Milligrams per Liter DAILY MX .0367 C3 .0367 .05 .0367 .0367
0 01051 Lead, total [as Pb] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .00835 C2 0 0 0 0
C3 Milligrams per Liter DAILY MX .0177 C3 .0177 .0177 .0177 .0177
0 01055 Manganese, total [as Mn] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C3 Milligrams per Liter DAILY MX 2 C3 1.97 0 .591 .591
0 01067 Nickel, total [as Ni] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
C2 Milligrams per Liter DAILY AV .1 C2 .261 .261
C3 Milligrams per Liter DAILY MX .3 C3 .3 .5
Frequency of Analysis Once per 6 Months
Page 18 of 40
EPA Inspection Report - Page 72 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002S
01067 Nickel, total [as Ni] / Location 1 / Season 0 / Base
DMR Values
C2
C3
6/30/16
.0214
.3
12/31/16
.0214
.3
0 01077 Silver, total [as Ag] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .0022 C2 0 0 0 0
C3 Milligrams per Liter DAILY MX .005 C3 .005 .2 .005 .005
0 01092 Zinc, total [as Zn] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .145 C2 .193 .193 .0314 .0314
C3 Milligrams per Liter DAILY MX .307 C3 .307 .5 .307 .307
0 01105 Aluminum, total [as Al] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .834 C2 .35 .35 .372 .372
C3 Milligrams per Liter DAILY MX 1.77 C3 1.77 1 1.77 1.77
7 71900 Mercury, total [as Hg] / Location 1 / Season 0 / Base
6/26/17 3:53 PM
Page 19 of 40
EPA Inspection Report - Page 73 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002S
71900 Mercury, total [as Hg] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Milligrams per Liter DAILY AV .000039 C2 .000039 0 0 0
C3 Milligrams per Liter DAILY MX .000082 C3 .000082 .000082 .000082 .000082
Outfall 002Y
0 00940 Chloride [as Cl] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 12/31/15 12/31/16
C3 Milligrams per Liter DAILY MX 975 C3 301 186
0 00945 Sulfate, total [as SO4] / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 12/31/15 12/31/16
C3 Milligrams per Liter DAILY MX 689 C3 4.87 4.87
7 70295 Solids, total dissolved / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values
6/26/17 3:53 PM
Limit End Date 5/1/18
C3 Milligrams per Liter DAILY MX 6000 C3
Sample Type GRAB
Frequency of Analysis Annual
Page 20 of 40
EPA Inspection Report - Page 74 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall 002Y
70295 Solids, total dissolved / Location 1 / Season 0 / Base
DMR Values
C3
12/31/15
45
12/31/16
432.6
Outfall SO1Y
0 00094 Conductivity / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 micromhos per centi MAXIMUM
C3 1.17 1.16
0 00441 Sulphur, total elemental / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 2.09 79
0 00600 Nitrogen, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr DAILY MX
C3 0 0
0 00620 Nitrogen, nitrate total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
6/26/17 3:53 PM
Page 21 of 40
EPA Inspection Report - Page 75 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO1Y
00620 Nitrogen, nitrate total [as N] / Location S / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 0 0
0 00625 Nitrogen, Kjeldahl, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .13 820
0 00665 Phosphorus, total [as P] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .137 22.1
0 00915 Calcium, dissolved [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .3 29.2
0 00916 Calcium, total [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Page 22 of 40
EPA Inspection Report - Page 76 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO1Y
00916 Calcium, total [as Ca] / Location S / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .005 1140
0 00925 Magnesium, dissolved [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .307 8.13
0 00927 Magnesium, total [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 1.77 342
0 00929 Sodium, total [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0816 0
0 00930 Sodium, dissolved [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Page 23 of 40
EPA Inspection Report - Page 77 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO1Y
00930 Sodium, dissolved [as Na] / Location S / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 2.09 7.08
0 00931 Sodium adsorption ratio / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Ratio MAXIMUM
C3 .143 .299
0 00937 Potassium, total [as K] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0367 108
8 82583 pH, in soil / Location S / Season 0 / Base
Frequency of Analysis Annual
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
Limit End Date 5/1/18
C3 Standard Units MAXIMUM
C3 7.31 7.08
Sample Type COMPOS
Frequency of Analysis Annual
Outfall SO2Y
0 00094 Conductivity / Location S / Season 0 / Base
6/26/17 3:53 PM
Page 24 of 40
EPA Inspection Report - Page 78 of 288
DMR Summary
Permit TX0042129
Version # 0 Outfall SO2Y 00094 Conductivity / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 micromhos per centi MAXIMUM
C3 1.08 1.12
0 00441 Sulphur, total elemental / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 2.11 250
0 00600 Nitrogen, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr DAILY MX
C3 .143 1.61
0 00620 Nitrogen, nitrate total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0367 1.61
0 00625 Nitrogen, Kjeldahl, total [as N] / Location S / Season 0 / Base
6/26/17 3:53 PM
Page 25 of 40
EPA Inspection Report - Page 79 of 288
DMR Summary
Permit TX0042129
Version # 0 Outfall SO2Y 00625 Nitrogen, Kjeldahl, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .125 870
0 00665 Phosphorus, total [as P] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .139 63.9
0 00915 Calcium, dissolved [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .28 80.2
0 00916 Calcium, total [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .004 8850
0 00925 Magnesium, dissolved [as Mg] / Location S / Season 0 / Base
6/26/17 3:53 PM
Page 26 of 40
EPA Inspection Report - Page 80 of 288
DMR Summary
Permit TX0042129
Version # 0 Outfall SO2Y 00925 Magnesium, dissolved [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .298 0
0 00927 Magnesium, total [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 1.81 334
0 00929 Sodium, total [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .102 0
0 00930 Sodium, dissolved [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 2.12 0
0 00931 Sodium adsorption ratio / Location S / Season 0 / Base
6/26/17 3:53 PM
Page 27 of 40
EPA Inspection Report - Page 81 of 288
DMR Summary
Permit TX0042129
Version # 0 Outfall SO2Y 00931 Sodium adsorption ratio / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Ratio MAXIMUM
C3 .154 0
0 00937 Potassium, total [as K] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0384 193
8 82583 pH, in soil / Location S / Season 0 / Base
Frequency of Analysis Annual
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
Limit End Date 5/1/18
C3 Standard Units MAXIMUM
C3 7.21 7.02
Sample Type COMPOS
Frequency of Analysis Annual
Outfall SO3Y
0 00094 Conductivity / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
C3 micromhos per centi MAXIMUM
C3 1.21
Frequency of Analysis Annual
Page 28 of 40
EPA Inspection Report - Page 82 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO3Y
00094 Conductivity / Location S / Season 0 / Base
DMR Values
C3
8/31/16
1.12
0 00441 Sulphur, total elemental / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 2.26 320
0 00600 Nitrogen, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .21 2.56
0 00620 Nitrogen, nitrate total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0418 2.56
0 00625 Nitrogen, Kjeldahl, total [as N] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value
Limit End Date 5/1/18
Sample Type COMPOS
C3 Milligrams per Kilogr MAXIMUM
Frequency of Analysis Annual
6/26/17 3:53 PM
Page 29 of 40
EPA Inspection Report - Page 83 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO3Y
00625 Nitrogen, Kjeldahl, total [as N] / Location S / Season 0 / Base
DMR Values
C3
8/31/15
.128
8/31/16
0
0 00665 Phosphorus, total [as P] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .141 67.3
0 00915 Calcium, dissolved [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .31 107
0 00916 Calcium, total [as Ca] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0046 6210
0 00925 Magnesium, dissolved [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
6/26/17 3:53 PM
Page 30 of 40
EPA Inspection Report - Page 84 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO3Y
00925 Magnesium, dissolved [as Mg] / Location S / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 .314 6.86
0 00927 Magnesium, total [as Mg] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 1.82 297
0 00929 Sodium, total [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0978 0
0 00930 Sodium, dissolved [as Na] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Liter MAXIMUM
C3 2.11 0
0 00931 Sodium adsorption ratio / Location S / Season 0 / Base
Limit Start Date 8/1/14
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Annual
Page 31 of 40
EPA Inspection Report - Page 85 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall SO3Y
00931 Sodium adsorption ratio / Location S / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Ratio MAXIMUM
C3 .149 0
0 00937 Potassium, total [as K] / Location S / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
C3 Milligrams per Kilogr MAXIMUM
C3 .0381 201
8 82583 pH, in soil / Location S / Season 0 / Base
Frequency of Analysis Annual
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 8/31/15 8/31/16
Limit End Date 5/1/18
C3 Standard Units MAXIMUM
C3 7.26 7.21
Sample Type COMPOS
Frequency of Analysis Annual
Outfall TX2Q
2 22414 Whole effluent toxicity / Location U / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMP24
C1 Percent 7 DA MIN 14 C1 >29 >29 29 >29 29
C2 Percent MO AV MN 14 C2 >29 >29 29 >29 29
Frequency of Analysis Quarterly
Page 32 of 40
EPA Inspection Report - Page 86 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
22414 Whole effluent toxicity / Location U / Season 0 / Base
DMR Values
C1
C2
6/30/16
>29
>29
9/30/16
>29
>29
12/31/16
29
29
3/31/17
>29
>29
2 22414 Whole effluent toxicity / Location V / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMP24
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN 14 C1 >29 >29 29 >29 29 17 >29 29 >29
C2 Percent MO AV MN 14 C2 >29 >29 29 >29 29 17 >29 29 >29
2 22415 Whole effluent toxicity - retest #1 / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis See Permit
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Pass=0; Fail=1 7 DA MIN
C1 NODI=9 0 Not Received NODI=9 Not Received Not Received NODI=9 0 NODI=9
C2 Pass=0; Fail=1 MO AV MN
C2 NODI=9 0 Not Received NODI=9 Not Received Not Received NODI=9 0 NODI=9
2 22416 Whole effluent toxicity - retest #2 / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis See Permit
6/26/17 3:53 PM
Page 33 of 40
EPA Inspection Report - Page 87 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
22416 Whole effluent toxicity - retest #2 / Location 1 / Season 0 / Base
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Pass=0; Fail=1 7 DA MIN
C1 NODI=9 0 Not Received NODI=9 Not Received Not Received NODI=9 0 NODI=9
C2 Pass=0; Fail=1 MO AV MN
C2 NODI=9 0 Not Received NODI=9 Not Received Not Received NODI=9 0 NODI=9
T TLP3B Low Flow Pass/Fail Survival Test Static Renewal 7 Day Chronic Ceriodaphnia dubia /
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Pass=0; Fail=1 7 DA MIN
C1 0 0 0 0 0 0 0 0 0
C2 Pass=0; Fail=1 MO AV MN
C2 0 0 0 0 0 0 0 0 0
T TLP6C Low Flow Pass/Fail Survival Test Static Renewal 7 Day Chronic Pimephales promelas
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
C1 Pass=0; Fail=1 7 DA MIN
C2 Pass=0; Fail=1 MO AV MN
C1
C2
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Frequency of Analysis Quarterly
Page 34 of 40
EPA Inspection Report - Page 88 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
TLP6C Low Flow Pass/Fail Survival Test Static Renewal 7 Day Chronic Pimephales promelas
DMR Values
C1
C2
12/31/16
0
0
3/31/17
0
0
T TOP3B NOEC Lethal Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 / Season
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 29 29 29 29 29 29 29 29 29
C2 Percent MO AV MN
C2 29 29 29 29 29 29 29 29 29
T TOP6C NOEC Lethal Static Renewal 7 Day Chronic Pimephales promelas / Location 1 / Seaso
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 29 29 29 29 29 29 29 29 29
C2 Percent MO AV MN
C2 29 29 29 29 29 29 29 29 29
T TPP3B NOEC Sub-Lethal Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 / Sea
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
6/26/17 3:53 PM
Page 35 of 40
EPA Inspection Report - Page 89 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
TPP3B NOEC Sub-Lethal Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 / Sea
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA AVG
C1 22 12 29 22 22 17 9 17 29
C2 Percent MO AV MN
C2 22 12 29 22 22 17 9 17 29
T TPP6C NOEC Sub-Lethal Static Renewal 7 Day Chronic Pimephales promelas / Location 1 / S
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 29 29 29 29 22 29 29 29 29
C2 Percent MO AV MN
C2 29 29 29 29 22 29 29 29 29
T TWP3B Pass/Fail Sub-Lethal Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 /
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
C1 Pass=0; Fail=1 7 DA MIN
C2 Pass=0; Fail=1 MO AV MN
C1
C2
0
0
1
1
0
0
0
0
0
0
1
1
1
1
Frequency of Analysis Quarterly
Page 36 of 40
EPA Inspection Report - Page 90 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
TWP3B Pass/Fail Sub-Lethal Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 /
DMR Values
C1
C2
12/31/16
1
1
3/31/17
0
0
T TWP6C Pass/Fail Sub-Lethal Static Renewal 7 Day Chronic Pinephales promelas / Location 1
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Pass=0; Fail=1 7 DA MIN
C1 0 0 0 0 0 0 0 0 0
C2 Pass=0; Fail=1 MO AV MN
C2 0 0 0 0 0 0 0 0 0
T TXP3B LOEC Lethal Survival Static Renewal 7 Day Chronic Ceriodaphnia dubia / Location 1 /
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 NODI=Q NODI=Q 29 NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q
C2 Percent MO AV MN
C2 NODI=Q NODI=Q 29 NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q
T TXP6C LOEC Lethal Survival Static Renewal 7 Day Chronic Pimephales promelas / Location
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
6/26/17 3:53 PM
Page 37 of 40
EPA Inspection Report - Page 91 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
TXP6C LOEC Lethal Survival Static Renewal 7 Day Chronic Pimephales promelas / Location
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 NODI=Q NODI=Q 29 NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q
C2 Percent MO AV MN
C2 NODI=Q NODI=Q 29 NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q NODI=Q
T TYP3B LOEC Sub-Lethal Reproduction Static Renewal 7 Day Chronic Ceriodaphnia dubia / L
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis Quarterly
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16 12/31/16 3/31/17
C1 Percent 7 DA MIN
C1 29 17 29 NODI=Q 29 22 12 22 NODI=Q
C2 Percent MO AV MN
C2 29 17 29 NODI=Q 29 22 12 22 NODI=Q
T TYP6C LOEC Sub-Lethal Reproduction Static Renewal 7 Day Chronic Pimephales promelas /
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 3/31/15 6/30/15 9/30/15 12/31/15 3/31/16 6/30/16 9/30/16
6/26/17 3:53 PM
Limit End Date 5/1/18
Sample Type COMPOS
C1 Percent 7 DA MIN
C2 Percent MO AV MN
C1 NODI=Q NODI=Q 29 NODI=Q 29 NODI=Q NODI=Q
C2 NODI=Q NODI=Q 29 NODI=Q 29 NODI=Q NODI=Q
Frequency of Analysis Quarterly
Page 38 of 40
EPA Inspection Report - Page 92 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TX2Q
TYP6C LOEC Sub-Lethal Reproduction Static Renewal 7 Day Chronic Pimephales promelas /
DMR Values
C1
C2
12/31/16
NODI=Q
NODI=Q
3/31/17
NODI=Q
NODI=Q
Outfall TXBS
2 22415 Whole effluent toxicity - retest #1 / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis See Permit
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Pass=0; Fail=1 SINGSAMP
C2 NODI=9 NODI=9 1 NODI=9
2 22416 Whole effluent toxicity - retest #2 / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit End Date 5/1/18
Sample Type COMPOS
Frequency of Analysis See Permit
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
C2 Pass=0; Fail=1 SINGSAMP
C2 NODI=9 NODI=9 0 NODI=9
T TIE3D LC50 Pass/Fail Static 24Hr Acute D. Pulex / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
Limit End Date 5/1/18
C2 Pass=0; Fail=1 SINGSAMP
C2 0 0 0 0
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
6/26/17 3:53 PM
Page 39 of 40
EPA Inspection Report - Page 93 of 288
DMR Summary
Permit TX0042129
Version # 0
Outfall TXBS T
TIE6C LC50 Pass/Fail Static 24Hr Acute Pimphales / Location 1 / Season 0 / Base
Limit Start Date 8/1/14
Limit Limit Unit Desc Statistical Base Limit Value DMR Values 6/30/15 12/31/15 6/30/16 12/31/16
Limit End Date 5/1/18
C2 Pass=0; Fail=1 SINGSAMP
C2 0 0 1 0
Sample Type COMPOS
Frequency of Analysis Once per 6 Months
6/26/17 3:53 PM
Page 40 of 40
EPA Inspection Report - Page 94 of 288
Wyman-Gordon Forgings / Wyman-Gordon Houston 06/27-28/2017
Appendix 3 2016 Laboratory Analyses for Outfall 002
EPA Inspection Report - Page 95 of 288
nulronmental
April 25, 2016
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 w w w.alsgloba l. com
Aaron Placek Wyman-Gordon Forgings, LP 10825 Telg ~ Road Houston, TX 77095
Laboratory Results for: Outfall 002
Dear Aaron ,
Work Order: HS16031389
ALS Environmental received 6 sample(s) on Mar 31, 2016 for the analysis presented in the following report .
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested . Results are expressed as "as received" unless otherwise noted .
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please fee l free to call me. Sincerely,
Generated By: Dayna.Fisher
Erica Padilla PM
Page I of27
RIGHT SOLUTIONS I RIGHT PARTNER
EPA Inspection Report - Page 96 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Lab Samp ID HS1603 1389-01
HS 16031389-02
HS16~31369-03
HS1 603 1389-04
HS 16031369-05
HS16031389-06
Client Sample ID Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E.Coli Outfall 002 - Hexavalent Cr
Date : 25-Apr-16
SAMPLE SUMMARY
Mat rix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
TagNo
Collection Date 31-Mar-20 16 11:07 31-Mar-2016 11 :08 31 -Mar-20 16 11 :09 31-Mar-2016 11 :10 31-Mar-2016 11 :11 31-Mar-2016 11:12
Date Received 31-Mar-2016 14:45 31-Mar-2016 14:45 31-Mar-2016 14 :45 31-Mar-2016 14:45 31-Mar-2016 14:45 31-Mar-2016 14:45
Hold
D D D D D D
Page 2 of 27
RIGHT SOLUTIONS I RIGHT PARTNER
EPA Inspection Report - Page 97 of 288
ALS Group USA, Corp
Date: 25-Apr-16
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Work Order Comments
CASE NARRATIVE
The analysis for E.coli was subcontracted to Envirodyne Laboratories. Inc. in Houston. TX.
WetChemistry by Method M25400 Batch ID: R272067
The test results meet requirements of the current NELAP standards . state requirements or programs where applicable.
WetChemistry by Method E1664A Batch ID : R272149
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E410.4 Batch ID : R272103
The test results meet requirements of the current NELAP standards . state requirements or programs where applicable.
WetChemistry by Method SW7196 Batch ID: R271856
The test results meet requirements of the current NELAP standards . state requirements or programs where applicable.
WetChemistry by Method SM5210 B Batch ID: 102887
The test results meet requirements of the current NELAP standards , state requirements or programs where applicable.
Page 3 of27
RIGHT SOLUTIONS l RIGHT PARTNER
EPA Inspection Report - Page 98 of 288
ALS Group USA, Corp
Client Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - COD 31-Mar-2016 11 :07
ANALYSES
RESULT QUAL
CHEMICAL OXYGEN DEMAND BY E410.4
Chemical Oxygen Demand
295
Method:E410.4 +1
I
REPORT LIMIT
15.0
Date: 25-Apr-16
ANALYTICAL REPORT
Work Order: HS 16031389 Lab ID:HS16031389-01 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KMU
06-Apr-2016 17:10
t
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of27 RIGHT SOLUTIONS 1RIGHT PARTNER
EPA Inspection Report - Page 99 of 288
ALS Group USA , Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - BOD 31-Mar-201611 :08
ANALYSES
BOD
Biochem ical Oxygen Demand
RESULT QUAL
Method:SM5210 B 70.0
r
REPORT LIMIT
2.00
Date: 25-Apr-16
ANALYTICAL REPORT Work0rder:HS16031389
Lab ID:HS16031389-02 Matri x:A queous
UNITS
DILUTION DATE FACTOR ANALYZED
Prep:SM5210 B I 01-Apr-2016
Analyst: KMU
mg/L
06-Apr-2016 15:42
f
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of27 RIGHT SOL- TIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 100 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - OG 31-Mar-2016 11 :09
ANALYSES
OIL & GREASE (HEM) BY E1664A Oil and Grease
1
RESULT QUAL
Method:E1664A 9.79
REPORT LIMIT
2.00
r
Date: 25-Apr-16
ANALYTICAL REPORT WorkOrder:HS16031389
Lab ID:HS16031389-03 Matrix:Aqueous
UN ITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 07-Apr-2016 14:15
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of27 RIGHT SOLU110NS 1 RIGHT PARTNER
EPA Inspection Report - Page 101 of 288
ALS Group USA, Corp
Client: Proj ect: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - TSS 31-Mar-2016 11 :10
ANALYSES
RESULT QUAL
TOTAL SUSPENDED SOLIDS BY SM 2540D Suspended Solids (Residue, Non -Filterable)
Method:M2540D 20.4
REPORT LIMIT
2.00
Date: 25-Apr-16
ANALYTICAL REPORT
WorkOrder:HS16031389 Lab ID:HS16031389-04 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH
06-Apr-2016 15:04
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of27 RIGHT SOL.UTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 102 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - E.Coli 31 -Mar-201611 :11
ANALYSES
RESULT QUAL
SUBCONTRACT ANALYSIS - E. COLI
Subcontract Analysis
See Attached
Method:NA
REPORT LIMIT
Date: 25-Apr-16
ANALYTICAL REPORT
Work0rder:HS16031389 Lab ID:HS16031 389-05 Matri x: Aq ueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Analyst: EDL 25-Apr-2016 09:33
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of 27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 103 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - Hexavalent Cr 31-Mar-201611:12
ANALYSES
RESULT QUAL
HEXAVALENT CHROMIUM BY SW7196A Chromium, Hexavalent
Mothod:SW7196
NO
REPORT LIMIT
0.0100
Date: 25-Apr-16
ANALYTICAL REPORT
Work0rder:HS16031389 Lab ID:HS16031389-06 Matrix: Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst JHD 31-Mar-2016 15:55
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 or27 RIGHT S\.il__ TION... 1 RIGHT PARTNER
EPA Inspection Report - Page 104 of 288
ALS Group USA, Corp
Client:
Wyman-Gordon Forgings, LP
Project: Outfall 002
WorkOrder: HS16031389
Batch 10: 102887
SampiD HS16031389-02
Method: BOD
Container 1
Sample WWol
300
Final Volume
300 (mL)
Prep Factor
Date: 25-Apr-16
WEIGHT LOG
Prep: BOD_PR 52108
Page 10 of27 RIGHT SOLU-:-IONS 1 RIGHT PARTNER
EPA Inspection Report - Page 105 of 288
ALS Group USA, Corp
Date: 25-Apr-16
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
DATES REPORT
Sample ID
Client Samp ID
Collection Date
TCLP Date
Prep Date
Analysis Date DF
Batch ID 102887
Test Name : BOD
HS16031389-02 Outfall 002- BOD
31 Mar 2016 11 :08
Batch ID R271856
Test Name : HEXAVALENT CHROMIUM BY SW7196A
HS16031389-06 Outfall 002 - Hexavalent Cr 31 Mar 2016 11:12
Batch ID R272067
Test Name : TOTAL SUSPENDED SOLIDS BY SM 2540D
HS16031389-04 Outfall 002 - TSS
31 Mar201611 :10
Batch ID R272103
Test Name : CHEMICAL OXYGEN DEMAND BY E410.4
H$16031389-01 Outfall 002 - COD
31 Mar 2016 11 :07
Batch ID R272149
Test Name : OIL & GREASE (HEM) BY E1664A
HS16031389-03 Outfall 002 - OG
31 Mar 2016 11 :09
Batch ID R273068
Test Name : SUBCONTRACT ANALYSIS- E. COLI
HS16031389-05 Outfall 002- E.Coli
31 Mar201611 :11
Matrix: Aqueous
01 Apr 2016 15:00
06 Apr 2016 15:42
Matrix: Aqueous
31 Mar 2016 15:55
Matrix: Aqueous
06 Apr 2016 15:04
Matrix: Aqueous
06 Apr 2016 17:10
Matrix: Aqueous
07 Apr 201614:15
Matrix: Aqueous
25 Apr 2016 09:33
Page II of27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 106 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Date: 25-Apr-16
QC BATCH REPORT
Batch ID: 102887
Instrument: ManTech01
Method: SM5210 B
MBLK Client 10:
Analyte
Sample ID:
MBLK-102887
Units: mg/L
Analysis Date: 06-Apr-2016 15:42
Run 10: ManTech01_272101 SeqNo: 3640188 PrepDate: 01-Apr-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
LCS Client ID:
Analyte
Sample ID:
LCS-102887
Units: mg/L
Analysis Date: 06-Apr-2016 15:42
Run 10: ManTech01 272101 SeqNo: 3640187 PrepDate: 01 -Apr-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPKVal
Value %REG
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
174
2 .00
198
0 87.9 85 - 115
LCSD Client ID:
Analyte
Sample 10:
LCSD-102887
Units: mg/L
Analysis Date: 06-Apr-2016 15:42
Run 10: ManTech01_272101 SeqNo: 3640190 PrepDate: 01-Apr-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
175.5
2.00
198
0 88.6 85- 115
174 0.858 20
DUP Client 10:
Analyle
Sample ID:
HS16031394-01DUP
Units: mg/L
Analysis Date: 06-Apr-2016 15:42
Run ID: ManTech01_272101
Result
POL
SPK Val
SeqNo: 3640189
SPK Ref Value %REG
PrepDate: 01-Apr-2016 OF: 1
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
1.9
0 20
Note: See Qualifiers Page for a hst ofquahfiers and the1r explanation
Page 12 of27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 107 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Date: 25-Apr-16
QC BATCH REPORT
Batch ID: R271856
Instrument: UV-2450
Method: SW7196
MBLK Client ID:
Analyte
Sample ID:
MBLK-271856
Units: mg/L
Analysis Date: 31-Mar-2016 15:55
Run ID: UV-2450_271856
SeqNo: 3635073 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
NO
0.0100
LCS Client ID:
Ana lyle
Sample ID:
LCS-271856
Units: mg/L
Analysis Date: 31-Mar-201615:55
Run ID: UV-2450_271856
SeqNo: 3635074 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0.244
0.0100
0.25
0 97.6 80 - 120
MS ClientiD:
Analyte
Sample ID:
HS16031382-15MS
Units: mg/L
Analysis Date: 31-Mar-2016 15:55
Run ID: UV-2450_271856
SeqNo: 3635076 PrepDate:
DF: 1
Result
POL
SPK Val
SPK Ref Value %REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Quat
Chromium, Hexavalent
0.252
0.0100
0.25
-0.005
103 75 - 125
MSD ClientiD:
Analyte
Sample ID:
HS16031382-15MSD
Units: mg/L
Analysis Date: 31-Mar-201615:55
Run ID: UV-2450_271856
SeqNo: 3635077 PrepDate:
OF: 1
Result
PQL
SPK Val
SPK Ref Value %REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
0 .247
0.0100
0.25
-0.005
101 75 - 125
0.252
2 20
Note . See Quahliers Page for a hst of quahliers and the1r explanat1o n
Page 13 of27 RIGHT SOLUTION;;~ 1RIGHT PARTNER
EPA Inspection Report - Page 108 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Date: 25-Apr-16
QC BATCH REPORT
Batch 10: R272067
Instrument: Balance1
Method: M25400
MBLK Client ID:
Analyte
Sample 10:
WBLKW1-040616
Units: mg/L
Analysis Date: 06-Apr-2016 15:04
Run ID: Balance1_272067
SeqNo: 3639407 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
ND
2.00
LCS Client ID:
Analyte
Sample 10:
WLCSW1-040616
Units: mg/L
Analysis Date: 06-Apr-201615:04
Run 10: Balance1_272067
SeqNo: 3639408 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Con trol Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterab le)
89
2.00
100
0 89.0 78- 120
DUP Client 10:
Ana lyte
Sample 10:
HS16040145-01DUP
Units: mg/L
Analysis Date: 06-Apr-2016 15:04
Run 10: Balance1_272067
SeqNo: 3639405 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
33.2
2.00
34.8 4.71 5
DUP Client 10:
Analyte
Sample 10:
HS16040079-01DUP
Units: mg/L
Analysis Date: 06-Apr-2016 15:04
Run 10: Balance1_272067
SeqNo: 3639403 PrepDate:
DF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFil terable
1988
2 .00
19 12
3.9 5
The fullowingsam ples wrreanayzedin thb ba tch:~L_S_I~~J-13_89_-~- ~~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Note: See Qualifiers Page for a I1st of qualifiers and the1r explanation
Page 14 of27
RIGHT SOLU. IONS I RIGHT PARTNER
EPA Inspection Report - Page 109 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forg ings, LP Outfall 002 HS16031389
Date: 25-Apr-16
QC BATCH REPORT
Batch 10: R272103
Instrument: WetChem_HS
Method: E410.4
MBLK Client iD:
Ana lyle
Sample ID:
MBLK-272103
Units: mg/L
Analysis Date: 06-Apr-2016 17:10
Run 10: WetChem_HS_272103 SeqNo: 3640205 PrepDate:
DF. 1
Result
PQL
SPK Val
SPK Ref Value %REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
NO
15.0
LCS Client ID:
Analyte
Sample ID:
LCS-272103
Units: mg/L
Analysis Date: 06-Apr-2016 17:10
Run ID: WetChem_HS_272103 SeqNo: 3640206 PrepDate:
DF : 1
Result
PQL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
946
15.0
1000
0 94.6 85- 115
MS Client 10:
Analyte
Sample ID: Outfall 002 COD
HS16031389-01MS
Units: mgiL
Analysis Date: 06-Apr-2016 17:10
Run 10: WetChem_HS_272103 SeqNo: 3640208 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chemical Oxygen Demand
776
15.0
500
295 96.2 80- 120
DUP ClientiD:
Analyte
Sample ID: Outfall 002- COD
HS16031389-01DUP
Units: mg/L
Analysis Date: 06-Apr-201617:10
Run 10: WetChem_HS_272103 SeqNo: 3640207 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chemical Oxygen Demand
292
15.0
295 1.02 20
Note See Qualifiers Page for a list of qualifiers and the1r explanation
Page 15of27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 110 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Date: 25-Apr-16
QC BATCH REPORT
Batch ID: R272149
Instrument: Balance1
Method: E1664A
MBLK Client iD:
Ana lyte
Sample ID:
WBLKW-040716
Units: mg/L
Analysis Date: 07-Apr-2016 14:15
Run ID: Balance1-272149
Result
PQL
SPKVal
SeqNo: 3640825
SPK Ref Value %REC
PrepDate:
Control Limit
DF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
NO
2.00
LCS Client 10:
Analyte
Sample ID:
WLCSW-040716
Units: mg/L
Analysis Date: 07-Apr-2016 14:15
Run 10: Balance1 - 272149
Result
PQL
SPKVal
SeqNo: 3640827
SPK Ref Value %REC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
38.4
2.00
40
0 96.0 78 - 11 4
LCSD Client 10:
Analyte
Sample 10:
WLCSDW-040716
Units: mg/L
Analysis Date: 07-Apr-2016 14:15
Run ID: Balance1- 272149
Result
PQL
SPK Val
SeqNo: 3640826
SPK Ref Value %REC
Prep Date :
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
36
2.00
40
0
90.0 78 - 114
38.4 6.45 18
MS Client ID:
Analyte
Sample ID:
HS16040227 -04MS
Units: mg/L
Analysis Date: 07-Apr-2016 14:15
Run 10 : Balance1_272149
SeqNo: 3640824 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPKVal
Value %REC
Limit
Value %RPD Limit Qual
Oil and Grease
43.86
2 .00
40
0.7692
108 78- 114
Note . See Qual1fiers Page for a hst of qualifiers and the1r explanation
Page 16 of27 RIGHT SOL_ TIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 111 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002
HS16031389
Date: 25-Apr-16
QUALIFIERS, ACRONYMS, UNITS
Qualifier
a B E H J M n NO 0 P R S U
Description
Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte detected below quantitation limit Manually integrated, see raw data for justification Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 40% RPD above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDUSDL
Acronym
DCS DUP LCS LCSD MBLK MDL MOL MS MSD PDS POL SO SOL TRRP
Description
Delectability Check Study Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Method Blank Method Detection Limit Method Ouantitation Limit Matrix Spike Matrix Spike Duplicate Post Digestion Spike Practical Ouantitaion Limit Serial Dilution Sample Detection Limit Texas Risk Reduction Program
Unit Reported
mg/L
Description
Milligrams per Liter
Page 17 of27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 112 of 288
ALS Group USA, Corp
Agency Arkansas California Illinois Kansas Kentucky Louisiana North Carolina North Dakota Oklahoma Texas
Date: 25-Apr-16
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Number
16-022-0 2919 003622 E-10352 2014-2015 KY 201 5-2016 03087 2015/2016 624 - 2016 R-1 93 2015-2016 20 15-047 T10470423 1- 15- 15
Expire Date
27-Mar-2017 31-Jul-2016 09-May-2016 3 1-Jul-20 16 30-Apr-2016 30-Jun-2016 31-Dec-2016 30-Apr-2016 31-Aug-2016 30-Apr-2016
Page 18 of 27 RIGHT SOLUTION~ 1 RIGHT PARTNER
EPA Inspection Report - Page 113 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16031389
Lab Samp ID
HS16031389-01 HS16031389-02 HS16031389-03 HS16031389-04 HS16031389-05 HS 16031389-06
Client Sample ID
Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002 - E.Coli Outfall 002 - Hexavalent Cr
Date: 25-Apr-16
SAMPLE TRACKING
Action
Login Login Login login login login
Date
3/31/2016 3:09:21 PM 3/31/2016 3:09:21 PM 3/31 /2016 3:09:21 PM 3/3112016 3:09:21 PM 3/3112016 3:09:21 PM 3/31/2016 3:09:21 PM
Person
CGG CGG CGG CGG CGG CGG
New Location
138 138 10E 13B Sub 138
Page 19 of27
RIGHT SOLUTIONS I RIGHT PARTNER
EPA Inspection Report - Page 114 of 288
ALS Group USA, Corp
Client Name: Work Order:
WYMAN-GORDON-HOU HS16031389
Date/Time Received: Received by:
Date: 25-Apr-16
Sample Receipt Checklist al -Mi!c-;!l!!1 l~M~ .tll:il:i
Checklist completed by:
Corey Grandits
eSignature
31-Mar-2016 Date
Reviewed by:
Erica Padilla
eSignature
1-A~-2016
Date
Matrices:
Carrier name:
~
Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? TX1005 solids received in hermetically sealed vials? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature in compliance? Temperature(s)/Thermometer(s): Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water- VOA vials have zero headspace? Water - pH acceptable upon receipt? pH adjusted? pH adjusted by:
Yes 0
Yes D Yes D Yes 0
Yes 0 Yes 0 Yes 0
Yes~
Yes D Yes 0 Yes 0 Yes 0
Yes 0
Yes D
No D No D No D No D
No D No D
No D
No D No D No D No D
No D
Not Present 0
Not Present
00 Not Present
N/A 0
R#S
No
NoD No[!]
No VOA vials submitted
N/A D N/A D
Login Notes:
Client Contacted:
Date Contacted:
Person Contacted:
Contacted By:
0
Regarding:
Comments:
I
I
Corrective Action:
Page 20 of27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 115 of 288
A Enulronmental
Ch1clnnatl, OH + I 513 733 5336
Evertt. WA +I 425 3 56 2600
Customer Information
Purchase Old
W~ Order
Company Name ~yman-Gordon F0111ings, LP
Send Report To !Aaron Placek
Fort Collins, CO +I 9704901 511
Chain of Custody For
HS16031389
Holland, Ml +1 616 399 6070
I Page _ ot _
l
coc ID: 138203
ALS Project Manager:
I Project Name
Project Information Outfall o P 1.-
IA j COD
Wyman-Gordon Forgmgs, LP Outfall 002
1111111111111111111111
Project Number
BIIIToCompany-+lw-W-Yynm-a-n-G-ordOOForgings, LP
fnvolceAttn ~n Placek
~~
C 101 and Grease f o i' T-S--S--
tn,WV 8 0
-
1
_ _ , Addl'"e$5
Clty/stataiZip
108:?5 Telge Road 'Houston, TX 770955038
10825 Telge Road Address
- - -+--C_ttyI_S_ta~ t I Houston, TX 770955038
fe I E.Coll a Hr Hold llme
I' F Hexvalent Chromium 24 Hr Hold Time
I G
- ------------
Phone Fax
Phone i (281) 856-9900
--------J___::____ + - -
1
Fax
e-Mail Addreu !aplocek@WJ!Tlan.eom
No.
Sample o..criptlon
Date
Time
Matrix
Pres.
H -
I
-~
JL
t Bottles A
8
c 0
E 1 F TQ I H
--
J
Hold
1 I Outfall l. -COD
&J~~
/J; 1?'7- Aqueous
1 X
I I
2 Outfall t-800 3 Outfall 'l.-00
-
I ;l:u~
--
-----------1--+--- jl ;r) 9
AQueous Aqueous
1
X
--
2
X
-I
4 Outfall 1..TSS
j(; 10
Aqueou s
---1-----!-----t----1---
X
I
5 Outfall t -E.Coli
I
j/ .'II
Aqueous
2
X
-IJ)
,_ ---
6 I OulfaU J_rl-iexavalent Cr
1/; 1-t.- AQueous
1 i
-t-X
----~--~--~------
----} 7 -
j-
j - -
I l---- I I I t I I I I I I ~----~
10
samt:>ler\S!PteasePrint& sfgn - .JJ1//J
L,_.._ p~ !fvf..K...
RalinquiSilel! by:
Relinquishked by:
A "'""
Ioa~U
DaJ.e':!+'"
IShipment Method 14-.~.- f;~;,.,ey
Time:
j Re<:elved by:
/'l.'t/.h-
Time: '
LoWed by IUboratot)'):
i Datei
-Prese-rva-t-ive -Key: --1---HCI --2--H-NO-, - '3-H-2SO,
n
1 me:
- -4Na0H
- 6-N-a-HSO,
IRequired 1\lmaround Time: (Check Box)
IX! Std lO WK diiYt
n 5 Wl<Oa\S
Notes:
D Otner
n 2WI(0816
-------------r Results Due Data: n 2~-;;;;;-1
10DavTAT.
B ~OC~P~ac~k~~~~~~~~~~----------~ TRRP Chi.1st TRRP Level 4
7-0-th-e-r - -8--4-C---9--~50=35--+-----+---~ OlheriEDO
Notr:
I. Any chang~s mu~t he made in writing once samples and COC Form have been submilled to ALS F.nvironmentnl. 2. Unless otherwise agreed in a fomlHI contruct, service~ provided by ALS Environmental arc expressly limited to the terms and conditions stated on the reverse. 3. The C hain or Custody is a legal document. All information must be completed accnrately.
Page 2 1 of 27
Copyright 2011 by ALS Environmental.
RIGHT SOLUT1ur-J::; 1KIGHT PARTNER
EPA Inspection Report - Page 116 of 288
04 April 2016
[nvirodynt laboratories, Inc I I0 I I Brookltt Dr.,# 230 llouston, TX 77099 281.568.7880 Phont www.tnvirodynt.com
ALS Group USA, Corp. Bern adette Fini 10450 Stancliff Rd. Suite #210 Houston, TX 77099
ALS
Enclosed are the results of analyses for samples received by the laboratory on 31-Mar-16 16:15. The analytical data provided relates only to the samples as received in this laboratory report.
Ell certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client.
The total number of pages in this report is 5
Thank you for selecting Ell for your analytical needs. If you have any questions regarding this report, please contact us.
Sincerely,
Monica Smith Project Manager
Certificate No: TX104704265
Page 22 of 27 RIGHT SOLU fiONS 1RIGHT PARTNER
EPA Inspection Report - Page 117 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16C3601
Sample 10 HS 1603 1389-05 OUTFALL 002
ANALYTICA L R E PO RT FOR SAMP LES
La bono tory ID 16C3601-0 1
Matri Water
E nvirodynr Laboratorirs, Inc 11 0 11 Brooklrt Dr.,# 230 Ho uston, TX 77099 281.568.7880 Phont www.envirodl/nt.com
Rtporttd: 04-Apr-16 13 00
Date Sampltd 31-Mar- 16 II II
Date Rrccivtd 31-Mar-1616 IS
Envirodyne Laboratories, Inc.
A~r,_Jn~
The results m t!Jiv report apply to the ,,omples cmaly:ed m acwn:Jance "llh the <hom of
CUStody document. 7171.' analy/IW/ report nJIL\'t be repnx/uced In tiS etllrf'l!ty.
Page 23 of 27 RIGHT SOLUTIONS t RIGHT PARTNER
EPA Inspection Report - Page 118 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16C3601
Envirodynr Laboratories, Inc II 0 II Brooklet Dr., II 230 Houston, TX 77099 281.568.7880 Phone
www.envirod~nr. com
Reported: 04-Apr- 16 13.00
Analyte
Microbiolo E.coli
Result 13
HS 16031389-05 OUTFALL 002 16C3601-01 (Water) Sampled: 31 -Mar-16 11 : 11
Reporting Limit
Units Dilution
Batch
Prepared
Envirodyne laboratories, Inc.
Analyzed
Method Analyst Notes
MPN100 mL
B6DOI47 31-Mar-1 6
31-lvfar-1 6 16:30
SM9223 B
LTC
Envirodyne Laboratories, Inc.
A~r~Jn:h
The results rn tl11.v rep<m apply to the samples analy=ed rn accordance wtlh the cham of custody dontment. Tlus analyttcal n1por1 must be reproduced m tis ellltrely.
Page 24 of 27 RIGHT SOLUTIONS 1 RIGHT PARTNER
EPA Inspection Report - Page 119 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16C3601
Envirodyne Laboratories, Inc 11 011 Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Pbonr www.e nvi rod yn r .c om
Reported: 04-Apr-16 IJOO
Analyte
Batch 8 600147- Microb iologv Blank (8600147-BLK I)
E.coli
Duplicate (860 01 47-0UPI) E. col i
M icrobiology- Quality Control Envirodyne Laboratories, Inc.
Result
Rcponmg Limit
Units
Spike
Source
%REC
Level
Result
%REC
Li mits
RPD
RPD Limit
Notes
Prepared & Analyzed: 31-Mar-16
<I
I MPN/100 mL
Sourer: 16C2795-0 I
Prepared & Analyzed: 31-Mar-1 6
<2
2 MPN/ 100 mL
<2
0
0479
Envirodyne Laboratories, Inc.
A~r~cfm:h
The rt!sults mthrx report upply to the samples analy:ed m accorclunce wllh the cham of custody document. Thts analytrcal report muxt be reproduced m rt.s enllrety.
Page 25 of27
RIGHT SOLUTIONS I RIGHT PARTNER
EPA Inspection Report - Page 120 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16C3601
Notes and Definitions
DET
Analyte DETECTED
NO
Analyte NOT DETECTED at or above the reportmg h mtt
NR
Not Reported
dry RPD CLT
Sample resulls reported on a dry weoght basts Relau'e Percent Dofference Chent Representative
Envirodynr LAboratorirs, Inc tiOtl Brooklet Dr.,# 230 Houston, T X 77099 281.568.7880 Phone www.cn\irodyne.rom
Reportod :
04-Apr-1 6 13 00
Envirodyne Laboratories, Inc.
_}(6YiioJn :h
The n!s ult.v m thts "'P"" apply to the sample., onaly:ed 111 a ccordonte wllh the cham of
clltody document Tlus unalyllcal l'l!f'VFI must be l'l!p roduced 111 /Is enttrel)
Page 26 of27
RIGHT SOLUTIO S I RIGHT PARTNER
CJ
-.. EPA Inspection Report - Page 121 of 288
-----l uonm
CHAIN OF CUSTODY REGORD
Page 1 of 1
ubcontractor- - - - - - - - Envirodyne Laboratories. lr.-::
Phone
1101 1 Brooklet. Ste 230
281 5687; 80
Houston. TX 77099
Fax
2815688004 - J
I Customer lnfom';,lion
Project lnforma~ion - -- - - l
LP._o_______.~H-5_160_3_1~:9 ----_-_-_-_-_-_-_,+.P:-r-oj::o--ct::-~:-:--a~-o---r.,H""S"'1'""6""03=~-1.=-;g
coc 10
Juo dato
31 Mar 2016
4465
08APR 16
1.~ddro:ss
Houston, TX 77099 - - - - -
t:"-1-~-s-=t--on-. -=rx:::--:::7~-09-9 - - --
Phono
281-530-56!:6
Phone
f281-~3~
Emall1
enca . padilla~alsglobal.com
Email2
---+.~~~~~-~~----~ ~;rr.oke.lawal@~lsg.;bal.com
L...__ _ _ _ ___,_ _ _ _ - - - - - -
-
---
i.ob ID
Oient Sam~ ID
Collection oae
Matri:<
An;:lysls Requested
.F._.s_1_60_3_1_3_89_-_o_s_ _.P..._u_tra_l_ol_o2_:~r:=.c~o~li~~~~~~:~~1~--~/-i~a-r--_,-6~-1-:1_~1'_._-;""__._f_<:;_u_~-ou-_ s~~~~=-J~UB_E. Coli
Commonts
Please anal~ ~ ~ for the analysis hsted a :oove. Send report to the emails shown c:bove
Recolvod by:
Dato!Time:
Coolor IDs:
Roport/QC Lover
Page 27 of 27 RIGHT Sv __ .11..1 .::> 1 RIGHT PARTNER
EPA Inspection Report - Page 122 of 288
June 02, 2016
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com
Aaron Plocek Wyman-Gordon Forgings, LP 10825 Telge Road Houston, TX 77095
Laboratory Results for: Outfall 002
Dear Aaron,
Work Order: HS16051314
ALS Environmental received 6 sample(s) on May 24, 2016 for the analysis presented in the following report.
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced , it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me. Sincerely,
Generated By: Jumoke.lawal
Erica Padilla PM
Page I of27 I HT S ._
HT PARTNER
EPA Inspection Report - Page 123 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Lab Samp ID HS16051314-01 HS160513 14-02 HS16051314-03 HS160513 14-04 HS160513 14-05 HS160513 14-06
Client Sample ID Outfall 002 - COD Outfall 002 -BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002 -E.Coli Outfall 002 - Hexavalent Cr
Date: 02-Jun-16
SAMPLE SUMMARY
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
Tag No
Collection Date 24-May-2016 10:1 0 24-May-2016 10:1 1 24-May-2016 10:1 2 24-May-2016 10:13 24-May-2016 10:14 24-May-2016 10:15
Date Received 24-May-2016 11 :30 24-May-2016 11 :30 24-May-2016 11:30 24-May-2016 11 :30 24-May-2016 11 :30 24-May-2016 11:30
Hold
D D D D D D
Page 2 of27 RIGHT S '-
EPA Inspection Report - Page 124 of 288
ALS Group USA, Corp
Date: 02-Jun-16
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS1605 1314
Work Order Comments
CASE NARRATIVE
The analysis for E.coli was subcontracted to Envirodyne Laboratories, Inc. in Houston, TX.
WetChemistry by Method M2540D Batch ID: R275203
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E410.4 Batch ID: R275412
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E1664A Batch ID: R275401
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method SW7196 Batch ID: R274930
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method SM521 0 B Batch ID: 104677
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
Page 3 of27 urlf
ARTNER
EPA Inspection Report - Page 125 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - COO 24-May-2016 10:10
A N A LY SES
RESULT QUAL
CHEMICAL OXYGEN DEMAND BY E410.4
Chemical Oxygen Demand
21 0
Method:E410.4
REPORT LIMIT
75.0
Date: 02-Jun-16
ANALYTICAL REPORT Wo rk 0 r d e r:HS160513 14
Lab ID:HS16051314-01 Matrix:Aqueous
UNITS
DILUTI ON FACTOR
DATE ANALYZED
mg/L
5
Analyst: KMU 01-Jun-2016 09:30
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of27
t-IT PA TNE=R
EPA Inspection Report - Page 126 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - BOD 24-May-2016 10:11
ANALYSES
BOD Biochemica l Oxygen Demand
RESULT QUAL
Method:SM5210 B 54.0
REPORT LIMIT
2.00
Date: 02-Jun-16
ANALYTICAL REPORT Work0rder:HS16051314
Lab ID:HS16051314-02 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Prep:SM5210 B /25-May-2016
Analyst: KMU
mg/L
30-May-2016 16:22
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of27
EPA Inspection Report - Page 127 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - OG 24-May-2016 10:12
ANALYSES
OIL & GREASE (HEM) BY E1664A Oil and Grease
RESULT QUAL
Method: E1664A 6.67
REPORT LIMIT
2.00
Date: 02-Jun-16
ANALYTICAL REPORT Work0 rder: HS16051314
Lab ID:HS16051314-03 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALVZED
mg/L
Analyst: KAH 31 -May-2016 15:15
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of27
s
EPA Inspection Report - Page 128 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - TSS 24-May-2016 10:13
ANALYSES
RESULT QUAL
TOTAL SUSPENDED SOLIDS BY SM 2540D Suspended Solids (Residue, Non -Filterab le)
Method:M2540D 107
RE P O R T LIMIT
2.00
Date: 02-Jun-16
ANALYTICAL REPORT Work0rder:HS16051314
Lab ID:HS16051314-04 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
m g/ L
Analyst: KAH 27-May-2016 11 :45
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Rl HT c;
Page 7 of27
EPA Inspection Report - Page 129 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - E.Coli 24-May-2016 10:14
ANALYSES
RESULT QUAL
SUBCONTRACT ANALYSIS -E. COLI
Subcontract Analysis
See Attached
Method :NA
REPORT LIMIT
Date: 02-Jun-16
ANALYTICAL REPORT
WorkOrder:HS 16051314 Lab ID:HS1 6051314-05 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Analyst: EDL 31 -May-2016 17:05
Note: See Qualifiers Page for a list of qualifiers and their explanation .
Page 8 of 27
Rl s
, ,HT
EPA Inspection Report - Page 130 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - Hexavalent Cr 24-May-2016 10:15
ANALYSES
RESULT QUAL
HEXAVALENT CHROMIUM BY SW7196A Chromium, Hexavalent
Method :SW7196 ND
REPORT LIMIT
0.0100
Date: 02-Jun-16
ANALYTICAL REPORT Work0rder:HS1 6051314
Lab ID:HS16051314-06 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: JHD 24-May-2016 14:42
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of27
nT P
EPA Inspection Report - Page 131 of 288
ALS Group USA, Corp
Client:
Wyman-Gordon Forgings, LP
Project: Outfall 002
WorkOrder: HS16051314
Batch 10: 104677
SampiD H$16051314-02
Method: BOD
Container
Sample Wt No l
300
Final Volume
300 (ml)
Prep Factor
Date: 02-Jun-16
WEIGHT LOG
Prep: BOD_PR 52108
Page 10 of27
EPA Inspection Report - Page 132 of 288
ALS Group USA, Corp
Date: 02-Jun-16
Client: Project: Wo rkOrde r:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
DATES REPORT
Sample 10
Client Samp 10
Collection Date
TCLP Date
Prep Date
Analysis Date OF
Batch ID 104677
Test Name : BOD
Matrix: Aqueous
HS16051314-02 Outfall 002 - BOD
24 May201610:11
25 May 2016 03:50 30 May 2016 16:22
Batch 10 R274930
Test Name : HEXAVALENT CHROMIUM BY SW7196A
Matrix: Aqueous
HS16051314-06 Outfall 002 - Hexavalent Cr 24 May 2016 10:15
24 May 2016 14:42
Batch ID R275203
Test Name: TOTAL SUSPENDED SOLIDS BY SM 2540D
Matrix: Aqueous
HS1 6051314-04 Outfall 002 - TSS
24 May 201610:13
27 May 201611 :45
Batch 10 R275384
Test Name : SUBCONTRACT ANALYSIS - E. COLI
Matrix: Aqueous
HS16051314-05 Outfall 002- E.Coli
24 May 2016 10:14
31 May 2016 17:05
Batch 10 R275401
Test Name : OIL & GREASE {HEM) BY E1664A
Matrix: Aqueous
H$16051314-03 Outfall 002 - OG
24 May 201610:12
31 May 2016 15:15
Batch ID R275412
Test Name : CHEMICAL OXYGEN DEMAND BY E410.4
Matrix: Aqueous
HS16051314-01 Outfall 002- COD
24 May 2016 10:10
01 Jun 2016 09:30
5
Page II of27
HT PARTNfR
EPA Inspection Report - Page 133 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Date: 02-Jun-16
QC BATCH REPORT
Batch ID: 104677
Instrument: ManTech01
Method: SM5210 8
MBLK Client 10:
Analyte
Sample 10:
MBLK-104677
Units: mg/L
Analysis Date: 30-May-2016 16:22
Run 10: ManTech01_275290 SeqNo: 3703883 PrepDate: 25-May-2016 OF: 1
Result
SPKRef
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
LCS Client 10:
Analyte
Sample ID:
LCS-104677
Units: mg/L
Analysis Date: 30-May-2016 16:22
Run 10 ManTech01_275290 SeqNo: 3703881 PrepDate: 25-May-2016 DF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Biochemical Oxygen Demand
179.5
2.00
198
0 90.7 85- 11 5
LCSD Client 10:
Ana lyte
Sample ID:
LCSD-104677
Units: mg/L
Analysis Date: 30-May-2016 16:22
Run ID ManTech01_275290 SeqNo: 3703884 PrepDate: 25-May-2016 DF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
180.5
2.00
198
0 91 .2 85 - 11 5
179.5 0.556 20
DUP Client 10:
Analyte
Sample ID:
HS16051 324-01DUP
Units: mg/L
Analysis Date: 30-May-2016 16:22
Run ID: ManTech01_275290 SeqNo: 3703882 PrepDate: 25-May-2016 DF 1
Result
PQL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limtt Qual
Biochemical Oxygen Demand
ND
2.00
1.4
0 20
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 12 of27
EPA Inspection Report - Page 134 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Date: 02-Jun-16
QC BATCH REPORT
Batch ID: R274930
Instrument: UV-2450
Method: SW7196
MBLK Client 10 :
Analyte
Sample 10:
MBLK-274930
Units: mg/L
Analysis Date: 24-May-201610:07
Run 10 UV-2450_274930
SeqNo: 3696439 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
NO
0.0100
LCS Client 10:
Analyte
Sample 10:
LCS-274930
Units: mg/L
Ana lysis Date: 24-May-2016 10:07
Run 10: UV-2450_274930
SeqNo: 3696440 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0.263
0 0100
0 .25
0
105 80-120
MS Client 10:
Analyte
Sample ID:
H516051288..05MS Run ID
Result
Units: UV-2450_274930
POL
SPK Val
mg/L
Analysis Date: 24-May-2016 10:07
SeqNo 3696442 PrepDate:
OF 1
SPK Ref Value %REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium , Hexavalent
0.266
0 .0100
0.25
-0.002
107 75- 125
MSD Client 10:
Analyte
Sample 10:
H516051288..05MSD
Units: mg/L
Analysis Date: 24-May-2016 10:07
Run ID. UV-2450_274930
SeqNo: 3696443 PrepDate:
OF: 1
Res ult
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0 254
0.0100
0.25
-0. 002
102 75-125
0.266 4.62 20
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 13 of27 R
EPA Inspection Report - Page 135 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Date: 02-Jun-16
QC BATCH REPORT
Batch 10: R275203
Instrument: Balance1
Method: M2540D
MBLK Client ID:
A nalyte
Sample ID:
WBLKW1 -052716
Units: mg/L
Analysis Date: 27-May-201 6 11 :45
Run ID: Balance 1_275203
SeqNo: 3702094 PrepDate:
DF: 1
Result
PQL
SPKVal
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
ND
2.00
L CS Client iD:
Analyte
Sample ID:
WLCSW1 -052716
Units: mg/L
Analysis Date: 27-May -201611 :45
Run ID: Balance1_275203
SeqNo: 3702095 PrepDate:
DF: 1
Result
PQL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
92
2.00
100
0
92.0 78 - 120
DUP Client ID:
Analyte
Sample ID: Outfa ll 002 - TSS
HS16051314-04DUP
Units: m g/L
Analysis Date: 27-May-201 61 1:45
Run ID: Balance1_275203
SeqNo: 3702089 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
108.3
2.00
106.7 1.55 5
DUP Client ID:
Analyte
Sample ID:
HS16051202-04DUP
Units: mg/L
Analysis Date: 27-May-2016 11 :45
Run ID: Balance1_275203
SeqNo: 3704359 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable
62.67
2.00
64 .67 3.14 5
Thc ~llowingsa~p~s werea na~ed in th ~ batch:L~s__t6_o_s_t3_1_4-_0_4~~~~~~~~~~~~~~~~~~~~~~~~~~~~
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 14 of27
EPA Inspection Report - Page 136 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Date: 02-Jun-16
QC BATCH REPORT
Batch ID: R275401
Instrument: Balance1
Method: E1664A
MBLK Client ID:
Analyte
Sample ID:
W B L K W -053116
Units: mg/L
Analysis Date: 31-May-2016 15:15
Run ID: Balance1- 275401
Result
PQL
SPK Val
SeqNo: 3705633
SPK Ref Value %REG
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
NO
2.00
LCS Client ID:
Analyte
Sample 10:
WLCSW-053116
Units: mg/L
Analysis Date: 31-May-2016 15:1 5
Run 10: Balance1- 275401
Result
PQL
SPK Val
SeqNo: 3705635
SPK Ref Value %REG
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease LCSD Client ID: Analyte
36.8
2.00
40
0 92.0 78- 11 4
Sample ID:
WLCSDW-053116
Units: mg/L
Analysis Date: 31-May-2016 15:15
Run 10: Balance1- 275401
Result
PQL
SPK Val
SeqNo: 3705634
SPK Ref Value %REG
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
MS
Client ID: Ana lyte
35.1
2.00
40
0
87.8 78 - 114
36.8 4.73 18
Sample 10:
HS16051386-01MS
Units: mg/L
Analysis Date: 31-May-2016 15:15
Run 10: Balance1- 275401
Result
PQL
SPK Val
SeqNo: 3705624
SPK Ref Value %REC
Prep Date:
Control Limit
DF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
39.66
2 .0 0
The following samples were anayzed in this batch: f St 605131 4-03
40
0.4494
98.0 78 - 114
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 15 of27 R
EPA Inspection Report - Page 137 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Date: 02-Jun-16
QC BATCH REPORT
Batch 10: R275412
Instrument: WetChem_HS
Method: E410.4
MBLK Client 10:
Analyte
Sample 10:
MBLK-275412
Units: mg/L
Analysis Date: 01-Jun-2016 09:30
Run 10: WetChem_HS_275412 SeqNo: 3706073 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
NO
15.0
LCS Client ID:
Analyte
Sample 10:
LCS-27541 2
Units: mg/L
Analysis Date: 01-Jun-2016 09:30
Run 10: WetChem_HS_275412 SeqNo: 3706074 PrepOate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPO
Value %RPO Limit Qual
Chemical Oxygen Demand
99
15.0
100
0 99.0 65 - 11 5
MS ClientiO:
Analyte
Sample 10 :
HS16051500-01MS
Units: mg/L
Analysis Date: 01-Jun-2016 09:30
Run 10: WetChem_HS_275412 SeqNo: 3706076 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
145
15.0
50
105 60.0 80- 120
DUP Client 10 :
Analyte
Sample 10:
HS16051500-01DUP
Units: mg/L
Analysis Date: 01-Jun-2016 09:30
Run 10: WetChem_HS_275412 SeqNo: 3706075 PrepOate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
104
15 0
105 0.957 20
T~fu~~~~~mp~~uean~ud~th~~~=Lfs__r_~s_J l_r_~_o_r_ __ _ __ _ __ __ _ _ _ __ _ _ _ _ __ __ _ _ __ ~
Note: See Qualifiers Page for a list of qualifiers and their explanation.
R HS
Page 16 of27 ,tiT PARTNI=
EPA Inspection Report - Page 138 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002
HS16051314
Date: 02-Jun-16
QUALIFIERS, ACRONYMS, UNITS
Qualifier
a B E H J M n NO 0 P R S U
Description
Value exceeds Regulatory Limit Not accredited Analyle detected in the assoc1ated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holdmg Time Analyte detected below quantitation limit Manually integrated, see raw data for justification Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 40% RPD above laboratory control hm1t Spike Recovery outside laboratory control limits Analyzed but not detected above the MDUSDL
Acronym
DCS DUP LC S LCSD MBLK MDL MOL MS MSD PDS POL SO SOL TRRP
Description
Delectability Check Study Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Method Blank Method Detection Limit Method Ouantitat1on Limit Matrix Spike Matrix Spike Duplicate Post Digestion Spike Practical Ouanlltaion Limit Serial Dilution Sample Detection Limit Texas Risk Reduction Program
Unit Reported
mg/L
Description
Milligrams per Liter
Page 17 of27 HT
EPA Inspection Report - Page 139 of 288
ALS Group USA, Corp
Ag e n cy Arkansas California Kansas Kentu cky Louisiana North Carolina North Dakota Oklahoma Texas
Date: 02-Jun-16
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Number
16-022-0 2919 E-1 0352 2014-2015 96 2016-2017 03087 2015/2016 624-2016 R193 2016-2017 2015-047 TX104704231-16-17
Expire Date
27-Mar-2017 31-Jul-2016 31-Jul-2016 30-Apr-2017 30-Jun-2016 31-Dec-2016 30-Apr-2017 31-Aug-2016 30-Apr-20 17
Rtmns
Page 18 of27
HT PARTN R
EPA Inspection Report - Page 140 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16051314
Lab Samp 10
HS16051314-01 HS 16051314-02 HS 16051314-03 HS16051314-04 HS16051314-05 HS16051314-06
Client Sample 10
Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002 - E.Coli Outfall 002 - Hexavalent Cr
Date: 02-Jun-16
SAMPLE TRACKING
Action
Login Login Login Login Login Login
Date
5/24/2016 11:48 21 AM 5/24/2016 11:48:21 AM 5/24/2016 11:48:21 AM 5/24/2016 11:48:21 AM 5/24/201611 :4821 AM 5/24/2016 11 :48;21 AM
Person
CGG CGG CGG CGG CGG CGG
New Location
14C 14C 14E 14C Sub 14C
Page 19 of27
RIGHT St
IGI-iT PART~E R
EPA Inspection Report - Page 141 of 288
ALS Group USA, Corp
Client Name: Work Order:
WYMAN-GORDON-HOU HS16051314
Daterfime Received: Received by:
Date: 02-Jun-16
Sample Receipt Checklist
24-May-2016 11:30 J RM
Checklist completed by:
Corey Grandits
eSignature
Matrices:
24-May-2016
I Date
Reviewed by: Carrier name:
Erica Padilla
eSignature
~
27-May-2016
I Date
Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? TX1 005 solids received in hermetically sealed vials? Sufficient sample volume for indicated test? All samples received within holding time? Containerrfemp Blank temperature in compliance? Temperature( s)rfhermometer(s ): Coole r(s )/Kit(s ): Daterfime sample(s) sent to storage: Water - VOA vials have zero headspace? Water pH acceptable upon receipt? pH adjusted? pH adjusted by:
Yes 0 Yes 0 Yes 0 Yes 0
Yes ~ Yes ~
Yes 0
Yes ~
Yes 0
Yes ~ Yes ~ Yes ~
f4.2c/4 .9c uc/c
~608
PS/24/2016 12:05
Yes U
Yes~
Yes O
No D No 0 No 0 No 0 No 0 No 0 No 0 No 0 No D No 0 No 0 No 0
No U
No O No 0
Not Present
0 Not Present 00 Not Present
N/A ~
IIIR#4
00 No VOA vials submitted ~ N/A N/A
Login Notes: Client Contacted:
Date Contacted:
Person Contacted:
Contacted By:
0
Comments:
Regarding:
Corrective Action :
RIGI-iT S
Page 20 of27
EPA Inspection Report - Page 142 of 288
A Enuironmental
Customer Information Purchase Order
Wort< Order
Company Name
1 Send Report To
I
!
Address
~n-GordClrl FOflli!!lil'" LP Aaron Ploc.k 10825 Telge Road
City/State/Zip Phone Fax
Houtton, TX 770955039
Project Name Project Number Bill To Company
Invoice Attn
IPage _ _of _ _ I
COCID: 145"
ALS Project Manager:
Project Information
__outr.n__~o 2...
WYman-Gordon F~gs,_LP
Aaron Plocek
HS160
11111111111111~11111111111111
A ::;QD
B ~00 C ::li anct~rease
D SS
Address 10825 Telge Road City/State/Zip HouttClrl, TX 770955038
E .Coli '9 Hr Hold nme' F r!exw.lent Chromlt.lll '24 HrHold Time' G
Phone (281) 856-9900
H
Fax
I
~
-
-
e-Mail Address No.
aploetkQwyman.eom Sample Description
1
Outfaft -COO
2
Outfan - BOD
3
Outfall -OG
4
Outfall -TSS
5
Outfall -E.Coll
6 Outfall -Hexavalent Cr
7
e-Mail Address aploeek@wyman.eom
J
Date
nme
Matrix
Pres.
II Bottles A
B
c- D
E
F
G
H
I
J
! 2'/h~>
/ P: Io-.,....
Aqueous
1 X
1 1 :/14;,.
Aqueous
1
X
tP: 1'1- 4..,
Aqueous
2
X
1.9; 11 Alii
Aqueous
}'@: i'f liY'
Aqueous
oJ Aqueous JO:IS'Ail\.
1
X
2
X
1
X
Hold
I I I
8
9
10 Sampl e lPiease Print & Sign
-.?.(_
Rell~y:
?r.,..~c..
ReUnqulsl>ed by:
Logged by (Laboratory):
Preservative Key: 1-HCI
~
~
IShipmenb et h od
Jl~ ~;:v..
IRequired Turnaround Time:oheck Box)
00 Std 10 Wr< day;
5 Wr< Dey.~
!:::! UUl<
Q 2Wr<Oe)'!l
0 24Hotr
IResults Due Date:
oSe'.;h~'f, j t,{p
Dafe:
Time: / 1'/(),lh-.
Time:
Received by:
'TM~_A~_g
Received by ( bora ry):
11 : Jco
NotestO OayTAT.
Cooler1D
Cooler Temp.
:lC Packaca:.JCheckOne ilefllalollll.
Date:
Time:
IlLS /{~
Checked by (Loberatory):
~it>OS'
4.2.
Level 3 Std O~ow da
Level 4 SW846IClP
tj TRRP Level4
2-HN03 3-H.so. 4-NaOH 5-Na,.S.03 6-NaHso. 7-0ther a-4c 9-5035
/lUI
CF0 .7
Other/EOO
~ote: 1. Any changes must be made in writing once samples and COC Form have been submilted to ALS Environmental.
....... 2. Unless otherwise ngretd in a rormul contr:Jct, services provided by ALS Environmental ore exl!."cssly Jimitc:d Ill the terms and c-nnrtiflnno ..n''" ' M , ... - -
J. The Chain of Custodv is R IPIllt """"m~nl All :ft~----
L
IJage 2 1 or 2 /
--
Copyright 2011 by ALS Environment"I.
EPA Inspection Report - Page 143 of 288
31 May 2016
Envirodyne Laboratories, Inc 11011 Brooklet Dr.,# 2JO Houston, TX 77099 281.568.7880 I'hone n ww.envirodync.com
ALS Group USA, Corp. Bernadette Fini 10450 Stancliff Rd. Suite #21 0 Houston, TX 77099
ALS
Enclosed are the results of analyses for samples received by the laboratory on 24-May-16 13:30. The analytical data provided relates only to the samples as received in this laboratory report.
Ell certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client.
The total number of pages in this report is 5
Thank you for selecting Ell for your analytical needs. If you have any questions regarding this report, please contact us.
Sincerely,
Monica Smith Project Manager
Certificate No: TX104704265
Page 22 of 27
EPA Inspection Report - Page 144 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16E2970
Sa mple 10 HS 16051314-05 OUTFALL 002- ECOLI
A ALYTICAL REPORT FOR SAM PLES
Labor~lory lD 16E2970-0I
lltatrir Water
Envirodyne Laboratories, Inc 11011 Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone """'.envirodyne.com
Reported: 31-May-16 13:45
Date SamJlled 24-May- 16 10:14
Datt Received 24-May- 16 13:30
Envirodyne Laboratories, Inc.
A~r~Jn:Jt
The results in this report apply to the samples analyzedin accordance K'ith the chain of custody document. This analyltcal report must be reproduced in its entirety.
Page 23 of27 R
EPA Inspection Report - Page 145 of 288
Client: Project: Work Order:
ALS Group USA. Corp. ALS 16E2970
EnvirocJync Laboratories, Inc II0 II Brooklet Or., II 230 Ho usto n, TX 77099 281.568.7880 Phone www.envirocJy n e.c o m
Reported :
31-May-16 13:45
Analyte
Microbiolo E.coli
Result
HS16051314-0S OUTFALL 002- ECOLI 16E2970-0I (Water) Sampled: 24-May-16 10:14
Reponing Limit
Units Dilution
Batch
Prepared
Envirodyne Laboratories, Inc.
Analyzed
Method Analyst Notes
MPNiiOO mL
B6E3100 24-Moy- 16 24-May-16 14: 15
SM9223 B
LTB
Envirodyne Laboratories, Inc.
J {~ (~cf, :hv
Th~ result< in this report apply tn the samples anafr-ed in accordance M'ith the cham of custody document. This analytical report must be reproduced In its ent1ref).
Page 24 of27
EPA Inspection Report - Page 146 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16E2970
Envirodyne Labo ratories, Inc I 101 I Brooklet Dr.,#230 Houston, TX 77099 281.568.7880 Phone W\\"\.envirodyne.com
Repor1td: 31-May- 161 3:45
Analytr
Batch 86E3100 - Microbiology Bhmk (B6E3 100-BLK I) E.coli
Duplicate (B6E3 100-DUPI) E.coli
Micr-obiology - Quality Control
Envirodyne Laboratories, Inc.
Result
Rrponing Limit
Units
Spike Lew I
Source
Result
~.REC
%REC Limits
RPD
RPD Limit
Notes
Prepared & Analyzed: 24-May I6
<I
I MPNIJOOmL
Source: 16E2105-0 I
Prepared & Analyzed: 24-May- 16
2.00
I MPN/100 ml
6.00
100
0.479
J1Envirodyne Laboratories, Inc.
~(d_cSn:iiv
The res11lts in this report apply to the samples analyzed in ac<ordance ..-ith the cham of ctutody document This analytical report must be reproduced in its entirety.
Page 25 of27
EPA Inspection Report - Page 147 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16E2970
DET ND NR dry RPD CLT
Notes a nd Definitions
Analyte DETECT ED Analyte NOT DETECTED at or abo'e the reponing limit Not Reponed Sample results reponed on a dry "eight basis Relative Percent DifTerence Client Representative
Envirodyne Laboratories, Inc II 0 II Brooklet Or.,# 230 Houston, TX 77099 28 1.568.7880 Phone www.cnvirodyne.com
Re p o r t ed : 3 1-May-16 13:45
AEnvirodyne Laboratories, Inc.
~(i_cfrn :h
TM results in this report apply to the samples ana/r-ed In accordance with the chain of custody document. This analytical report must be reproduced in its entirety.
Page 26 of27
ER
---EPA Inspection Report - Page 148 of 288
A 1
subcontractor
1 Enwodyne Laboratones. trc
CHAIN OF CUSTODY REC ORO
Page 1 of 1
11011 Brooklet. Ste 230
I_ _ Houston. TX 77099
L_
Customer Information
E _- - -...----.l1H-'=.S~1~6"o"_-5_=1~~'1:__4-_-_-_-_-_~----_-_-_----ici:=-r-OJ..-e-e,:--N7 aM~
Project lnioi'illatlOn -
E~_oo_5_1:4__ _.:.-._ ~~~_-_-j-1
Company Nbrt~
Address
-
I -~Company Na:'lle
ALS Hc.uston
-
- --+.- --~::----:f--- - - --J.
lnv Attn
vcr.ounts Paywl
10450 Standlff Rd. Ste 210
Address - - - 'i0450 Stanehlf ;'+f,l..--::::S,t.e.-'""'2'""1""0--...,
I~ Ema-=1"1"1'___
Houston, TX 77099 281-530-5656 eriea.padilla@atsglobal com
Em alt2
Houston. TX T: 99
281 -530-565t
rumoke.lawa. ~a globat.com ~-----r--------J
T;Jto
CQCI
oJed o
24 May2016
4726
01 JUN 16
Lab ID
Otent Samp lD
Collection Date
M(.;tnx
Anai(';is Requested
~51605131 4-05 joutfal' 002- E.Coli
~4-May-16 10:14 am ~queous
~UB_E. Coli
~-----L---------------L-------------L-----------1 ------------
Comments
IL, Please analyze lhe analysis listed above Send report to the emails show above
I
I
~~--~--------~
I
Reltn ~uil.llo:! by:
Da t e m t nc
Dat~l nmo:
Cooler IP&:
Roport/QC l evel
STD I
J
Page 27 of27
T PARTNER
P~nP 6 nf R::::J
EPA Inspection Report - Page 149 of 288
July 19, 20 16
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 w w w .alsgloba l. co m
Steve Howard Wyman-Gordon Forgings, LP 10825 Telge Road Houston, TX 77095
Laboratory Results for: Outfall 002
Dear Steve,
Work Order: HS16070273
ALS Environmental received 6 sample(s) on Jul 08, 2016 for the analysis presented in the following report.
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report. please feel free to call me. Sincerely,
Generated By: Dayna.Fisher
Erica Padilla
PM
Page I of27
RIGHT SOL_
IGHT PARTNER
, EPA Inspection Report - Page 150 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Lab Samp ID HS16070273-01 HS 16070273-02 HS16070273-03 HS 16070273-04 HS 16070273-05 HS16070273-06
Client Sample ID Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E.Coli Outfall 002 - Hexavalent Cr
Date:
19-Jul-16
SAMPLE SUMMARY
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
Tag No
Collection Date 08-Jul-2016 10:30 08-Jul-2016 10.31 08-Jul-2016 10:32 08-Jul-2016 10:34 08-Jul-2016 10:35 08-Jul-2016 10:37
Date Received 08-Jul-2016 1202 08-Jul-2016 1202 08-Jul-2016 1202 08-Jul-2016 12:02 08-Jul-2016 12 02 08-Jul-2016 1202
Hold
D D D D D D
Page 2 of27
RIGHT su..__- - 1 R..ut-IT PARTNER
, EPA Inspection Report - Page 151 of 288
ALS Group USA, Corp
Date: 19-Jul-16
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Work Order Comments
CASE NARRATIVE
The analysis for E.coli was subcontracted to Envirodyne Laboratories, Inc. in Houston, TX Final report attached
WetChemistry by Method E1664A Batch ID: R278154
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E410.4 Batch ID: R278263
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable
WetChemistry by Method M2540D Batch ID: R277948
The test results meet requ1rements of the current NELAP standards state requirements or programs where applicable
WetChemistry by Method SW7196 Batch ID: R277822
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable
WetChemistry by Method SM5210 B Batch ID: 106096
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
Page 3 of27
---------------------R-IG~H~T ~su-..-.u I,..., 0.# I ,...,rtT PARTNER
" EPA Inspection Report - Page 152 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - COD 08-Jul-2016 10:30
ANALYSES
RESULT QUAL
CHEMICAL OXYGEN DEMAND BY E410.4
Chemical Oxygen Demand
244
Method:E410.4
REPORT LIMIT
30.0
Date: 19-Jul-16
ANALYTICAL REPORT WorkOrder:HS16070273
Lab ID:HS16070273-01 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
2
Analyst: KMU 18-Jul-2016 18:00
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of27 RIGHT Su.... _ . .., .... utiT PARTNER
" EPA Inspection Report - Page 153 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - BOD 08-Jul-2016 10:31
ANALYSES
BOD Biochemical Oxygen Demand
RESULT QUAL
Method:SM5210 B 61.0
REPORT LIMIT
2.00
Date: 19-Jul-16
ANALYTICAL REPORT Work0rder:HS16070273
Lab ID:HS16070273-02 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Prep:SM5210 B I 08-Jul-2016
Analyst: KMU
mg/L
1
13-Jul-2016 14:42
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of27
RIGHT So._
uHT PARTNER
EPA Inspection Report - Page 154 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - OG 08-Jul-2016 10:32
ANALYSES
OIL & GREASE (HEM) BY E1664A Oil and Grease
RESULT QUAL
Method:E1664A 4 .35
REPORT LIMIT
2.00
Date: 19-Jul-16
ANALYTICAL REPORT
WorkOrder:HS 16070273 Lab ID:HS16070273-03 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 15-Jul-2016 12:25
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 6 of27 RIGHT SC... _. u ...... RIGHT PARTNER
EPA Inspection Report - Page 155 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - TSS 08-Jul-2016 10:34
ANALYSES
RESULT QUAL
TOTAL SUSPENDED SOLIDS BY SM 25400 Suspended Solids (Residue, Non -Filterable)
Method:M2540D 48.0
REP ORT LIMIT
2.00
Date: 19-Jul-16
ANALYTICAL REPORT WorkOrder: HS 16070273
Lab ID:HS16070273-04 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 12-Jul-2016 14:25
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of27
--------------------RI-G-HT~S~O~L~U.~~ 1 ,..;HT PARTNER
EPA Inspection Report - Page 156 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002- E.Coli 08-Jul-2016 10:35
ANALYSES
RESULT QUAL
SUBCONTRACT ANALYSIS -E. COLI
Subcontract Analysis
See Attached
Method :NA
REPORT LIMIT
Date: 19-Jul-16
ANALYTICAL REPORT Wo r kO rd e r:HS 16070273
Lab ID:HS16070273-05 Matrix:Aqueous
UNITS
DILUTION FA CTOR
DATE ANALYZED
Analyst: EDL 12-Jul-2016 12:18
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 8 of27 RIGHT SOL"TIO ~ 1 RIGHT PARTNER
EPA Inspection Report - Page 157 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - Hexavalent Cr 08-Jul-2016 10:37
ANALYSES
RESULT QUAL
HEXAVALENT CHROMIUM BY SW7196A Chromium, Hexavalent
Method :SW7196 NO
REPORT LIMIT
0 .0100
Date: 19-Jul-16
ANALYTICAL REPORT
WorkOrder:HS 16070273 Lab ID:HS1 6070273-06 M a t rix: Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: JHD 08-Jul-2016 15:44
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of27 RIGHT SOLL TION~ RIGHT PARTNER
EPA Inspection Report - Page 158 of 288
ALS Group USA, Corp
Client:
Wyman-Gordon Forgings, LP
Project: Outfall 002
WorkOrder: HS16070273
Batch 10: 106096
SampiD HS1607027 3-02
Method: BOD
Container
Sample WWol
300
Final Volume
300 (ml)
Prep Factor
Date: 19-Jul-16
WEIGHT LOG
Prep: BOD_PR 52108
Page I0 of27
RIGHT Sv,_..,,,..,,
n.:nH PARTNER
EPA Inspection Report - Page 159 of 288
ALS G roup USA, Corp
Date 19-Jul-16
Client: Project: WorkOrder:
Sample ID
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Client Samp ID
Collection Date
TCLP Date
Prep Date
DATES REPORT Analysis Date OF
Batch ID 106096
Test Name : BOD
Matrix: Aqueous
HS16070273-02 Outfall 002- BOD
08 Jul2016 10.31
08 Jul2016 15:20
13 Ju12016 14'42
Batch ID R277822
Test Name : HEXAVALENT CHROMIUM BY SW7196A
Matrix: Aqueous
HS16070273-06 Outfall 002 - Hexavalent Cr 08 Jul2016 10 37
08 Jul2016 15:44
Batch ID R277885
Test Name : SUBCONTRACT ANALYSIS -E. COLI
Matrix: Aqueous
HS16070273-05 Outfall 002- E.Coli
08 Jul2016 10.35
12 Jul2016 12:18
Batch ID R277948
Test Name : TOTAL SUSPENDED SOLIDS BY SM 2540D
Matrix: Aqueous
H$16070273-04 Outfall 002- TSS
08 Jul2016 10 34
12 Jul2016 14.25
Batch ID R278154
Test Name: OIL & GREASE (HEM) BY E1664A
Matrix: Aqueous
HS16070273-03 Outfall 002- OG
08 Jul2016 10 32
15 Jul2016 12 25
Batch ID R278263
Test Name : CHEMICAL OXYGEN DEMAND BY E410 4
Matrix: Aqueous
HS16070273-01 Outfall 002- COD
08 Jul2016 10.30
18 Jul2016 18 00
2
Page II of27
RIGHT Sv-- _ ~ .uHT PARTNER
EPA Inspection Report - Page 160 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Date: 19-Jul-16
QC BATCH REPORT
Batch 10: 106096
Instrument: ManTech01
Method : SM5210 B
MBLK Client 10:
Analyte
Sample 10:
MBLK-106096
Units: mg/L
Analysis Date: 13-Jul-201614:42
Run 10 ManTech01_278009 SeqNo: 3759085 PrepDate: 08-Ju l-2016
OF: 1
Result
PQL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Lim1t Qual
Biochemical Oxygen Demand
NO
2.00
LCS ClientiD:
Analyte
Sample ID
LCS-106096
Units: mg/L
Analysis Date: 13-Jul-201614:42
Run 10 ManTech01_278009 SeqNo: 3759084 PrepDate: 08-Jul-2016
OF: 1
Result
PQL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Biochemical Oxygen Demand
180
2.00
198
0 90.9 85-115
DUP Client iD:
Analyte
Sample ID.
HS16070229-01 DUP
Un1ts. mg/L
Analysis Date: 13-Jul-2016 14:42
Run 10 ManTech01_278009 SeqNo. 3759083 PrepDate: OS..Jul-2016
OF 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
200
1 9
0 20
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 12 of27
-------------------------R-I-G-H-T-S~v-.._..... ..,, .;J I ouHT PARTNER
EPA Inspection Report - Page 161 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Date: 19-Jul-16
QC BATCH REPORT
Batch ID: R277822
Instrument: UV-2450
Method: SW7196
MBLK Client ID:
Analyte
Sample ID:
MBLK-277822
Units: mg/L
Analysis Date: 08-Jul-2016 15:44
Run ID: UV-2450_277822
SeqNo: 3755383 PrepDate:
OF: 1
Result
PQL
SPK Val
SPK Ref Value %R EC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
NO
0.0100
LCS Client ID:
Analyte
Sample ID:
LCS-277822
Units: mg/L
Analysis Date: 08-Jul-2016 15:44
Run ID: UV-2450_ 277822
SeqNo: 3755384 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
0.243
0 .0100
0.25
0
97.2 80- 120
MS Client 10 :
A nalyte
Sample 10:
HS16070272-06MS
Units: mg/L
Analysis Date: 08-Jul-2016 15:44
Run ID: UV-2450_277822
SeqNo: 3755386 PrepDate:
OF: 1
Result
PQL
SPK Val
SPK Ref Value
%REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
0.267
0.0100
0.25
0 .002
106 75- 125
MSD Client 10:
Analyte
Sample 10:
HS16070272-06MSD
Units: mg/L
Analysis Date: 08-Ju l-201615:44
Run 10: UV-2450_277822
SeqNo: 3755387 PrepDate:
OF: 1
Result
PQL
SPK Val
SPK Ref Value %R EC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium , Hexavalent
0 .262
0.0100
0.25
0.002
104 75- 125
0.267 1.89 20
The foll owing sa mples were anal~zed in this batch: Lf_s_J6_o_7_02_7_3-_0_6 _ _ _ _ _ _ _ _ _ _ _ __ _ _ __ _ _ _ _ _ _ _ _ _ __j
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 13 of27 RIGHT Sv--. IONS RIGHT PARTNER
EPA Inspection Report - Page 162 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Date: 19-Jul-16
QC BATCH REPORT
Batch 10: R277948
Instrument: Balance1
Method: M25400
MBLK Client 10:
Analyte
Sample 10:
WBLKW1 -071216
Units: mg/L
Analysis Date: 12-Jul -201614:25
Run 10: Balance1_277948
SeqNo: 3757970 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
NO
2 00
LCS Client 10.
Analyte
Sample 10:
WL CSW1-0 71216
Units: mg/L
Analysis Date: 12-Jul-2016 14:25
Run 10 Balance1_277948
SeqNo: 3757971 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Suspended Solids (Res1due, NonFilterable)
99
2.00
100
0 99 0 78- 120
DUP Client ID:
Analyte
Sample 10
HS16070229-01DUP
Units mg/L
Analysis Date: 12-Jul-201 6 14:25
Run 10 : Balance1-277948
Result
PQL
SPKVal
SeqNo: 3757948
SPK Ref Value %REC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
11 56
2.00
11 78
1.9 5
DUP Client 10
Analyte
Sample 10 :
HS16070208-03DUP
Umts: mg/L
Analysis Date 12-Jul-201614:25
Run 10 Balance1_277948
SeqNo: 3757943 PrepDate
OF: 1
Result
PQL
SPKVal
SPK Ref Value %REC
Control lim1t
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Res1due, NonFilterable
69.09
2.00
71.82 3.87 5
The follo~1 ing s:tmJllcs n cre a nalyzed in this batch : Lr_s_J60_7o_2_7_3-_0_.t _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ __ _ __J
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 14 of27
RIGHT 5(.. __
~ 1 ' tuHT PARTNER
EPA Inspection Report - Page 163 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS1607027 3
Date: 19-Jul-16
QC BATCH REPORT
Batch 10: R278154
Instrument: Balance1
Method: E1664A
MBLK Client ID:
Analyte
Sample ID:
WBLKW-071516
Units: mg/L
Analysis Date: 15-Jul-2016 12:25
Run ID: Balance1_278154
SeqNo: 3762280 PrepDate:
OF: 1
Result
POL
SPKVal
SPK Ref Value
o/oREC
Control Limit
RPD Ref
RPD
Value o/oRPD Limit Qual
Oil and Grease
NO
2.00
LCS Client ID:
Analyte
Sample ID:
WLCSW-071516
Units: mg/L
Analysis Date: 15-Jul-2016 12:25
Run 10 : Balance1 - 278154
Result
PQL
SPKVal
SeqNo: 3762282
SPK Ref Value %REC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value o/oRPD Limit Qual
Oil and Grease
38.2
2.00
40
0
95.5 78- 114
LCSD Client 10:
Analyte
Sample ID:
WLCSDW-071516
Units: mg/L
Analysis Date: 15-Jul-2016 12:25
Run ID: Balance1- 278154
Result
PQL
SPK Val
SeqNo: 3762281
SPK Ref Value
o/oREC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value o/oRPD Limit Qual
Oil and Grease
36
2.00
40
0
90.0 78-11 4
38.2 5 .93 18
MS Client ID:
Analyte
Sample 10:
HS16070212-02MS
Units: mg/L
Analysis Date: 15-Jul-2016 12:25
Run 10: Balance1- 278154
Result
PQL
SPKVal
SeqNo: 3762275
SPK Ref Value o/oREC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value o/oRPD Limit Qual
Oil and Grease
40.44
2.00
40
0.1099
101 78- 114
The following samples were analyzed in this batch:Lf_s_J6_0_70_2_7_3_-0_J_ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ _ _ __ _ _ _ _ ____,
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page IS of27 RIGHT SG~-. ... "";"",._., .., 1 RIGHT PARTNER
EPA Inspection Report - Page 164 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Date: 19-Jul-1 6
QC BATCH REPORT
Batch 10: R278263
Instrument: WetChem_HS
Method: E410.4
MBLK Client 10:
Ana lyte
Sample ID:
MBLK-278263
Units: mg/L
Analysis Date: 18-Jul-2016 18:00
Run ID WetChem_HS_278263 SeqNo: 3764422 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
NO
15 0
LCS Client iD:
Analyte
Sample ID:
LCS-278263
Run ID
Result
Units: mg/L
Analysis Date: 18-Jul-2016 18:00
WetChem_HS_278263 SeqNo: 3764423 PrepDate:
OF 1
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REG
Limit
Value %RPD Limit Qual
Chemical Oxygen Demand
95
15 0
100
0 95.0 85- 115
MS Client 10 :
Analyte
Sample ID:
HS1 6070431-02MS Run iD
Result
Units: mg/L
Analysis Date: 18-Jul-201 6 18:00
WetChem_HS_278263 SeqNo: 3764425 PrepDate:
DF 1
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
112
15 0
50
57
11 0 80 - 120
DUP ClientiD:
Analyte
Sample ID:
HS16070431-020UP
Units mg/L
Analysis Date: 18-Jul-2016 18:00
Run ID. WetChem_HS_278263 SeqNo: 3764424 PrepDate:
DF 1
Res ult
POL
SPK Val
SPK Ref Value %REC
Co nt rol Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chem1cal Oxygen Demand
59
15.0
57 3.45 20
The follon ing samples nere analp.ed in I his balch: ._f_s_I6_0_7_02_7_J-O__I _ _ _ _ _ __ __ _ _ _ __ _ _ __ _ _ _ _ __ _ _ ___,
Note: See Qualifiers Page for a lisl of qualifiers and their explanation.
Page 16 of27
RIGHT SvL-.
ouHT PARTNER
EPA Inspection Report - Page 165 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Date: 19-Jul-16
QUALIFIERS, ACRONYMS, UNITS
Qualifier
a B E H J M n NO 0 P R S U
Descri ption
Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte detected below quanti,tation limit Man ually integrated, see raw data for justification Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 40% RPD above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDL/SOL
Acronym
DCS DUP LCS LC S D MBLK MDL MQL MS MSD PDS PQL SD SOL TRRP
Description
Delectability Check Study Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Method Blank Method Detection Limit Method Quantitation Limit Matrix Spike Matrix Spike Duplicate Post Digestion Spike Practical Quantitaion Limit Serial Dilution Sample Detection limit Texas Risk Reduction Program
Unit Reported
mg/L
Description
Milligrams per Liter
Page 17 of27
--------------------------R-IG-H-T--S-O-L-L~T - S 1 !;,~HT PARTNER
EPA Inspection Report - Page 166 of 288
ALS Group USA, Corp
Agency Arkansas California Il linois Kansas Kentucky Louisiana North Carolina North Dakota Oklahoma Texas
Date: 19-Jul-16
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Number
16-022-0 2919 003872 E-1 0352 2014-2015 96 2016-2017 03087 2016/2017 624.2016 R193 2016-2017 2015-047 TX104704231 -16-17
Expire Date
27 -Mar-2017 31-Jul-2016 09-May-2017 31-Jul-2016 30-Apr-2017 30-Jun-2017 31-Dec:-20 16 30-Apr-2 017 31-Aug-2016 30-Apr-2017
Page 18 of27
RIGHT Sv
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EPA Inspection Report - Page 167 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16070273
Lab Samp ID
HS16070273-01 HS16070273-02 HS16070273-03 HS 16070273-04 HS16070273-05 HS16070273-06
Client Sample ID
Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E.Coli Outfall 002- Hexavalent Cr
Date
19-Jul-16
SAMPLE TRACKING
Action
Logtn Logm Login Login Login Login
Date
7/8/2016 1213:13 PM 7/8/2016 12:13.13 PM 7/8/2016 12.13:13 PM 7/812016 12 13:13 PM 7/8/2016 12:13:13 PM 7/8/2016 12 13:13 PM
Person
CGG CGG CGG CGG CGG CGG
New Location
16C 16C 11E 16C Sub 16C
Page 19 of27
RIGHT Sv--. -
tuHT PARTNER
EPA Inspection Report - Page 168 of 288
ALS Group USA, Corp
Client Name: Work Order:
WYMAN-GORDON-HOU HS16070273
Date/Time Received : Received by:
Date: 19-Jul-16
Sample Receipt Checklist
Q~:Jui-2Q1 12:Q2 CGG
Checklist completed by:
Corey Grandits
eSignature
Matrices:
8-Jul-2016 Date
Reviewed by: Carrier name:
Erica Padilla
eSignature
Client
13-Jul-2016 Date
Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? TX1005 solids received in hermetically sealed vials? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature in compliance? Temperature(s)fThermometer(s): Cooler(s)/Kit(s): Date/Time sample(s) sent to storage: Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? pH adjusted? pH adjusted by :
Yes ~
Yes D Yes D
Yes ~ Yes ~ Yes ~ Yes ~ Yes ~
Yes D
Yes ~
Yes 0 Yes 0
2.3c/2.9c uc/c
25309
07/08/2016 12:30
Yes U
Yes ~
Yes D
No D No D No D No D No D No D No D No D No D No D No D No D
No U
NoD No ~
D Not Present
Not Present ~ Not Present ~
N/A ~ III R #5
No VOA vials submitted bd
N/A D N/A D
Login Notes:
Client Contacted:
Date Contacted:
Person Contacted:
Contacted By: Comments:
Regarding:
Corrective Action:
Page 20 of27 RIGHT SOLL- _ .., 1 IGHT PARTNER
- EPA Inspection Report - Page 169 of 288
IPage _ _ of _ _ I
Enulronmental
Customer Information Purchase Order
Wori( Order
Company Name Send Report To
~Qilorgings,J.e_ __AI!ron_Pio~:.~~k
Project Name Project Number Bill To Company
Invoice Attn
COCID: 142E
ALS Project Manager : Project Information
11~111111111~1~ Ill 11111111 IIII-I
Outfall __Q 1-
,.. - 1-- coo
---- -
Wyman:.Gordon...Eotgings,J.P-
B I ROO
-1- c OILand_Gr.ease _
Aaron Placek__
O TSS
Address
10825 Telge Road
City/State/Zip Phone
Houston, TX 770955038
Fax
e-Mall Address No.
aplocek@wymen.com Sample Description
1
Outfall -COO
2
Outfall -BOO
3
Outfall -OG
4
Outfall -TSS
5
Outfall - E.Coli
6
Outfall -Hexalll!lent Cr
7
tl Address -
City/State/Zip Phone Fax
10825 Telgo Road
E E.Coli ' 8 Hr Hold Tim e
I--
F
- - - - -I-- HeXVlllent Chromium '24 Hr Hold Time
G
Hou~on . TX 77095603~
...._
---
. -----
(281 ) 856-9900 - -
H
-
- .... - --~-
e-Mail Address 11plocek@wyman.com
Date
Time
M a tr i x
Pres.
II Bottles A
B
c D
E
F
G
l/Jb
JO~-
, ,:~\_
,e:Jz,
Aqu eous
--
Aqueous
Aqueou s
1 X
f-- .-
1
X
2
X
,o :N
/0 :3{
Aqu eou s
-- Aqueou s
-1
2
X X
"' ,9; >r -- Aqueous 1
X -
---
H
I
J
I
~ -
Hold
I
8
I
9
_d&_ 10 /\
Samplls) Please Print & Sign
-.rt.J-
IShipment Method 1/nt-; .ikt;,W'
IRequired Turnaround Time: (Check Box)
{XJ Std 10VVKdays
0 SWI<Oays
~ um r 0 2'M<Oeys
D 24 HOlM"
IResults Due Date:
Rellnquit::: "flo~
Di h
Tlme:
Received by:
Notes~Q Oay TAT.
Relinquished by:
- -Oat :g '"
Timo:
Re~tory):)~~ -\6\'U;1_
Coolor iD
Cooler Tomp. lC Po~lut1111: .{Q>eck One QQll Glll11wl
I
Logged by (Laboratory):
Date:
Time:
~Y (Laboro1ory):
1.136'1
"2. '3
~ Lev~l 3 Std OC.Row de Q TRRP Level 4
Levol I SW8A61CLP
j~
Otmr/EOO
I
Preservative Key: 1-HCI 2-HN03 3-H~o. 4-NaOH S-Na2S203 6-NaHso. 7-0ther a-4c 9 -5035
I
:-.!ole: 1. Any c ha nges must be made in writing once samples and COC Fo rm huve b~cn sub mitted to ALS Environmental. 2. Unless otherwise agreed in n formal contract, services provided by ALS Environmenta l arc CXIlressly limited to the terms a nd conditions slated on the reverse.
J. T he Chain of Custody is :t legal document. All information mn<l h P nnniMn.l ~~........... Page 21 o f 27
Copyright 201 1 by ALS Environmental.
EPA Inspection Report - Page 170 of 288
12 July 2016
Envirodync Laboratories, Inc 11011 Brooklet Dr., It 230 Houston, T X 77099 281.568.7880 Phone
"''\\.emirodync.com
ALS Group USA, Corp. Bernadette Fini 10450 Stancliff Rd. Suite #210 Houston, TX 77099
ALS
Enclosed are the results of analyses for samples received by the laboratory on 08-Jul-1 6 12:45. The analytical data provided relates only to the samples as received in this laboratory report.
Ell certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client.
The total number of pages in this report is 5
Thank you for selecting Ell for your analytical needs. If you have any questions regarding this report, please contact us.
Sincerely,
Monica Smith Project Manager
Certificate No TX104704265
Page 22 of27
RIGHT Sv L.
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EPA Inspection Report - Page 171 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16G11 44
SampleiD l iS 16070273-05 OU II \LI 002
ANALYTICAL REPORT FOR SAMPLES
Laborato') ID 16GII 4-I-OI
Matrit
Water
Envirod) ne Laboratories, Inc II 0 II Brooklet Dr., # 230 Houston, TX 77099 281.568.7880 Phone """w.envirod) nc.com
Reporttd: 12-Jul- 16 12:~
l};~te Sampled 08-Jul- 16 I0:35
l}ate Recei.-ed 08-Jul-16 12:-15
Envirodyne Laboratories, Inc.
J{~r,_rJn :fA.
IV
The results "'this report apply to the samples anal)'Zed in accordance >rith the chain of custodl' document. This analytical report m ust be reproduced in/Is entire/)'-
Page 23 of 27
RIGHTs~..,.
uHT PARTNER
EPA Inspection Report - Page 172 of 288
Client: Project: Work Order:
ALS Group USA, Corp.
ALS
16G1144
Envirod) ne Laboratories, Inc II 0 II Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone W\\ \\.CD\ irodyne.co m
Reported:
12-Jul-I6 I2:04
Analyte
l\1icrobiolo [.coli
Result 2-18
H 16070273-05 O UTFALL002
16G II44-0 I (Water) Sampled: 08-Jul-16 10:35
Reporting Limit
Units Dilution
Batch
Prepared
Envirodyne Laboratorie~, Inc.
Analyzed
1\IPN IOOmL
Bl>(oi08K 08-Jul-16
08-Jul-16 14:03
Method Analyst Notes
S\19~23 B
LTB
Envirodyne Laboratories, Inc.
Aomr;_cSn/h
The resufls tn this report apply to the samples analyzed in accordance with the chain of custody document This analytictll report must he reproduced in us entirety.
Page 24 of27
RIGHT Sv
.urlT PARTNER
EPA Inspection Report - Page 173 of 288
Client: Project: Work Order:
ALS Group USA, Corp. A LS 16G1144
Envirod) nc Laboratories, Inc II 0 II Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 l>hone W\\ n .envirod) ne.com
Rtported: 12-Jul-16 12:0-'
Analyte
Batch B6G I088 - Microbiology
Blunk (B6G 101!8-B LK I) !'.coli
l>uplicatc (B6G 1088-DUPI ) E.coli
Microbiolog_\- Quality Control
Envirodyne Laboratories, Inc.
Result
Reponing
[ mill
l nit~
Spike
Sour<:e
%Rt-:C
Le\01
Result
%REC
Limits
RPD
RPD Limit
Pr~pared & Anal)Zed: 08-Jul-16
<I
I MP' IOOml
S ource: 16G06H-Ol
Prepared & Anal) zed: 08-Jul-16
MP:\ 100 ml
:2
0
0.479
Envirodyne Laboratories, Inc.
/(~(d_Jn :h
The results in thts report apply to the samples analy;:ed in accordance wlfh the chain of custody document. This analytical report must be reproduced tn its entirt'fll.
Page 25 of27
RIGHT SC..L T
ouHT PARTNER
===u
EPA Inspection Report - Page 174 of 288
Client: P roject : Work Order:
ALS Group USA, Corp. ALS 16G1144
Notes a nd l)etinitions
OET NO NR dry RPD CLT
Analyoe DETECTED Analyte NOT DETECTED at or abo\e 1~ roporting limit Not Reponed Sample results reported on a dl) "eight 1:>.1''' Relati'< Percent DitTercnce Client Rcpr<senlative
E owirod~ ne Labor,.tories, In c 1101 1 Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone ww".em irod~ne. com
Reported: 12-Jul-16 12:().1
A cSn :h Envirodyne Laboratories, Inc. on-i ( d_
Th rewlts in th1s report apply to the samples anaZv::ed in acconkmce with the cham of custody document This onaZI'lical report must he repmduced in Its em1rety.
RIGHT
Page 26 of27
S 1~I-GH-T -PA-R-TN-ER----------~======~
EPA Inspection Report - Page 175 of 288
Subcontractor
\~&\\~4
.. CHAIN OF CUSTODY RECORD
~t- I
Page 1 of 1
Envirodvne Laboratories. Inc
Phone
1101 ~ Broo~i.::. Ste 230
Ho.sion, .-x 77099
281561!?sav Fax
L__ _ _ _ _ _ __
2815688004
--------::J--1 ~ - - - - - Customer lnfonnaUon
~feet lnfonnauo,;-
LP_o______---''-H-_s_160_7_o_27_3_ __ _ __ _..~_.Project Na-me- -~'J70273
-- ~
Date
c.,c ID
Duo date
Company Name Address -
ALS Houston 10450 Stanr.'iff Rd, Ste 210
Col'lpany Name lnvAitn Address
ALS Houston Accounts Payable 10450 Stancliff Rd, Ste 210
8 Jul2016
4983
20 -~ L 16
Phone Emall1
Houston. TX 77099 281-5.1)-5656 erica.p &dl:ta@alsglobal.com
Phone Emall2
-
Houston. TX 77099 281-530-5656 jumoke.lawal@alsglobat.com
Lab lD
Client 5amp I C
Collection Date
Matrix
AnalysiS Requested
~F_s_16_0_7_02_7_3_-o_s_-L~-u_tf_al_lo_o_z__E_.L~~~~i~~~~~~~~r--_-J_u_l_--1~6~10~-:-3~5~a_m--~--~F~_q-_u-e~oo~_s--~--------~,~-~-B-_-E___c_o_li_ _____________~
Commr..rs
Please ar.:.t ze for tte analysis list.;cl oboVt: $c!'<1 report to the emails shown above.
::..unqulshed by:
Date/Time:
Received by:
Oate/Timo:
Cooler IDs:
Report/QC Level
-------------------------R-IG-H-T-S-O~L-Pa~27of27.u~r-lT--P-A-R-TN-E-R----------------r=~~~2~-:-J,
EPA Inspection Report - Page 176 of 288
August 18, 2016
10450 Stancliff Rd . Suite 210 Houston , TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com
Steve Howard Wyman-Gordon Forgings, LP 10825 Telge Road Houston, TX 77095
Laboratory Results for: Outfall 002
Dear Steve,
Work Order: HS16080566
ALS Environmental received 6 sample(s) on Aug 12, 2016 for the analysis presented in the following report.
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested . Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced , it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me. Sincerely,
Generated By: jumoke.Lawal
Erica Padilla
PM
Page I of27
EPA Inspection Report - Page 177 of 288
ALS Group USA, Corp
Client: Project: Work Order :
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Lab Samp ID HS16080566-01 HS 16080566-02 HS 16080566- 03 HS16080566-04 HS 16080566-05 HS16080566-06
Client Sample ID Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E.Coli Outfall 002 - Hexavalent Cr
Date: 18-Aug-16
SAMPLE SUMMARY
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
Tag No
Collection Date 12-Aug-2016 09:27 12-Aug-2016 09:30 12-Aug-2016 09:28 12-Aug-2016 09:32 12-Aug-2016 0925 12-Aug-2016 09:26
Date Received 12-Aug-201610:15 12-Aug-201610:15 12-Aug-2016 10:15 12-Aug-201610:15 12-Aug-2016 1015 12-Aug-2016 10:15
Hold
D 0 0 0 0 0
Page 2 of27
, EPA Inspection Report - Page 178 of 288
ALS Group USA, Corp
Date: 18-Aug-16
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Work Order Comments
CASE NARRATIVE
The analysis for E.coli was subcontracted to Enwodyne Laboratories, Inc. in Houston, TX. Final report attached.
WetChemistry by Method E410.4 Batch 10: R279884
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E1664A Batch 10: R280023
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable
WetChemistry by Method M25400 Batch 10: R279951
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method SW7196
Batch 10: R279691 Sample ID: Outfall 002 - Hexavalent Cr (HS16080566-06)
Sample Filtered
WetChemistry by Method SM5210 B
Batch ID: 107134 Sample ID: MBLK-107134
The calculated seed correction factor was outside of the acceptance limits.
Page 3 of27
EPA Inspection Report - Page 179 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - COD 12-Aug-2016 09:27
ANALYSES
RESULT QUAL
CHEMICAL OXYGEN DEMAND BY E410.4
Chemical Oxygen Demand
235
Method:E410.4
REPORT LIMIT
15.0
Date: 18-Aug-16
ANALYTICAL REPORT W orkOrder:H S 16080566
Lab ID:HS16080566 01 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst KMU 16-Aug-2016 16 30
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 4 of27
EPA Inspection Report - Page 180 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - BOD 12-Aug-2016 09:30
ANALYSES
BOD Biochemical Oxygen Demand
RESULT QUAL
Method:SM5210 B 39 .7
REPORT LIMIT
2.00
Date: 18-Aug-16
ANALYTICAL REPORT WorkOrder:HS 16080566
Lab IO:HS16080566-02 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Prep:SM521 0 B / 12-Aug-2016
Analyst: KMU
mg/L
11-Aug-2016 15:17
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of27
EPA Inspection Report - Page 181 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - OG 12-Aug-2016 09:28
ANALYSES
OIL & GREASE (HEM) BY E1664A Oil and Grease
RESULT QUAL
Method:E1664A ND
REPORT LIMIT
2.00
Date: 18-Aug-16
ANALYTICAL REPORT WorkOrder: HS16080566
Lab ID:HS16080566-03 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE A NALYZED
mg/L
Analyst KAH 18-Aug-2016 11 .40
Note: See Qualifiers Page for a list of qualifaers and their explanation.
Page 6 of27
EPA Inspection Report - Page 182 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002
Outf~ll C02 - TSS
12-Aug-2016 09:32
ANALYSES
RESULT QUAL
TOTAL SUSPENDED SOLIDS BY SM 25400 Suspended Solids (Residue, Non -Filterable)
Method:M2540D 30.0
REPORT LIMIT
2.00
Date: 18-Aug-16
ANALYTICAL REPORT WorkOrder: HS 16080566
I 'lb l:J.HS16080566-04 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 17-Aug-2016 11:25
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of 27
EPA Inspection Report - Page 183 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - E.Coli 12-Aug-2016 09:25
ANALYSES
RESULT QUAL
SUBCONTRACT ANALYSIS E. COLI
Subcontract Analysis
See Attached
Method :NA
REPORT LIMIT
Date: 18-Aug-1 6
ANALYTICAL REPORT WorkOrder:HS 16080566
Lab ID:HS16080566-05 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Analyst: EDL 16-Aug-2016 07:22
Note: See Qualifiers Page for a list of qualifiers and their explanation .
Page 8 of27
EPA Inspection Report - Page 184 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfali 002 - Hexavalent Cr 12-Aug-2016 09:26
ANALYSES
RESULT QUAL
HEXAVALENT CHROMIUM BY SW7196A Chromium, Hexavalent
Method:SW7196 ND
REPORT LIMIT
0.0100
Date: 18-Aug-16
ANALYTICAL REPORT WorkOrder: HS16080566
Lab ID:HS16080566-06 Matrix:Aqueous
UNITS
DILUTION FACTOR
DA TE ANALYZED
mg/L
Analyst: JHD 12-Aug-2016 10:37
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of27
EPA Inspection Report - Page 185 of 288
ALS Group USA, Corp
Client:
Wyman-Gordon Forgings, LP
Project: Outfall 002
WorkOrdcr: HS16080566
Batch 10: 107134
SampiD HS16080566-02
Method: BOD
Container
Sample WtNol
300
Final Volume
300 (ml)
Prep Factor
Date: 18-Aug-1 6
WEIGHT LOG
Prep: BOD_PR 52108
Page 10 of27
EPA Inspection Report - Page 186 of 288
ALS Group USA, Corp
Date: 18-Aug-16
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP
Outfall 002 HS16080566
DATES REPORT
Sample ID
Client Samp ID
Collection Date
TCLP Date
Prep Date
Analysis Date DF
Batch ID 107134
Test Name : BOD
HS16080566-02 Outfall 002- BOD
12 Aug 2016 09:30
Batch ID R279691
Test Name: HEXAVALENT CHROMIUM BY SW7196A
HS16080566-06 Outfall 002- Hexavalent Cr 12 Aug 2016 09:26
Batch ID R279815
Test Name : SUBCONTRACT ANALYSIS -E. COLI
HS16080566-05 Outfall 002- E.Coli
12 Aug 2016 09:25
Batch ID R279BB4
Test Name : CHEMICAL OXYGEN DEMAND BY E410.4
HS16080566-01 Outfall 002 - COD
12 Aug 2016 09:27
Batch ID R279951
Test Name : TOTAL SUSPENDED SOLIDS BY SM 2540D
HS 160B0566-04 Outfall 002 - TSS
12 Aug 2016 09:32
Batch ID R2B0023
Test Name: OIL & GREASE (HEM) BY E1664A
HS16080566-03 Outfall 002- OG
12 Aug 2016 09:28
Matrix: Aqueous 12 Aug 2016 14:00 17 Aug 201615:17
Matrix: Aqueous 12 Aug 201610:37
Matrix : Aqueous 16 Aug 2016 07:22
Matrix: Aqueous 16 Aug 2016 16:30
Matrix: Aqueous 17 Aug 201611:25
Matrix: Aqueous 18 Aug 2016 11 :40
Page I I of27
EPA Inspection Report - Page 187 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Date: 18-Aug-16
QC BATCH REPORT
Batch 10: 107134
Instrument: ManTech01
Method: SM5210 B
MBLK Client 10:
Ana lyte
Sample ID:
MBLK-107134
Units: mg/L
Analysis Date: 17-Aug-2016 15:17
Run 10: ManTech01 _279981 SeqNo: 3799167 PrepDate: 12-Aug-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
LCS ClientiD:
Analyte
Sample 10.
LCS-107134
Units: mg/L
Analysis Date: 17-Aug-2016 15:17
Run 10: ManTech01_279981 SeqNo: 3799166 PrepDate: 12-Aug-2016 OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control limit
RPD Ref
RPD
Value %RPD limit Qual
Biochemical Oxygen Demand
188.9
2.00
198
0 95.4 85 - 115
DUP Client 10:
Analyte
Sample ID:
HS16080582-01DUP
Units: mg/L
Analysis Date: 17-Aug-2016 15:17
Run 10: ManTech01_279981 SeqNo: 3799165 PrepOate: 12-Aug-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
1.81
0 20
The foll owing samples were analyzed in this butch: Lfs__l6_o_so_s_6_6-_o_2- - - - - - - - - - - - - - - - - - - - - - - -- - - _ . )
Note: See Quali fiers Page for a list ofqualifiers and their explanation.
Page 12 of27
EPA Inspection Report - Page 188 of 288
ALS Group USA, Corp
Client: Project: WcrkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Date: 18-Aug-16
QC BATCH REPORT
Batch 10 : R279691
Instrument: UV-2450
Method: SW7196
MBLK Client ID:
An alyte
Sample ID:
MBLK-279691
Units: mg/L
Analysis Date: 12-Aug-2016 10:37
Run 10 : UV-2450_279691
SeqNo: 3793828 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
NO
0.0100
LCS Client ID:
Analyte
Sample ID:
LCS-279691
Units: mg/L
Analysis Date: 12-Aug-2016 10:37
Run ID: UV-2450_279691
SeqNo: 3793829 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0.251
0.0100
0 .25
0
100 80 - 120
MS Client ID:
Analyte
Sample ID:
HS16080554-06MS
Units: mg/L
Analysis Date: 12-Aug-2016 10:37
Run ID: UV-2450_279691
SeqNo: 3793830 PrepDate:
DF : 1
Re sult
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium , Hexavalent
0.258
0.0100
0.25
-0.002
104 75 - 125
MSD Client ID:
Analyte
Sample ID:
HS16080554 06MSD
Units: mg/L
Analysis Date: 12-Aug-2016 10:37
Run 10: UV-2450_279691
SeqNo: 3793831 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPO
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0.254
0 .0100
0.25
-0.002
102 75- 125
0.258 1.56 20
The followin g samples were a nalyzed in this batch: ._f_s_l60_so_s_6_6-_0_6_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____,
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 13 of27
EPA Inspection Report - Page 189 of 288
ALS Group USA, Corp
Client: Project: Wo rkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS1 6080566
Date: 18-Aug-16
QC BATCH REPORT
Batch ID: R279884
Instrument: WetChem_HS
Method: E410.4
MBLK Client 10 :
Analyte
Sample ID:
MBLK-279884
Units: mg/L
Analysis Date: 16-Aug-2016 16:30
Run ID: WetChem_HS_279884 SeqNo. 3797617 PrepDate:
OF 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPO Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
NO
15.0
LCS Client 10:
Analyte
Sample 10:
LCS -279884
Units: mg/L
Analysis Date: 16-Aug-201616:30
Run 10 : WetChem_HS_279884 SeqNo: 3797618 PrepDate:
OF : 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chemical Oxygen Demand
905
15.0
1000
0 90.5 85-115
MS Client 10.
Analyte
Sample 10:
HS16080650..{)2MS
Units. mg/L
Analysis Date: 16-Aug-2016 16:30
Run 10 : WetChem_HS_279884 SeqNo: 3797620 PrepOate:
OF 5
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPO
Value %RPD Limit Qual
Chemical Oxygen Demand
3555
75.0
2500
1230 93.0 80- 120
DUP Client iD:
Analyte
Sample 10:
HS16080650..{)2DUP
Units: mg/L
Analysis Date: 16-Aug-201 6 16:30
Run 10 WetChem_HS_279884 SeqNo: 3797619 PrepDate:
OF 5
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPO Limit Qual
Chemical Oxygen Demand
1240
75.0
Thefollowing samples were analy-,;ed in this bateh: .f..1.S__I6o__so_5_6_6-_o_l- - - - - - - - - - - - - --
1230 0.81 20 - - - - - - -- -- - - - - - '
Note: See Qualifiers Page for a list of quali fiers and their explanation.
Page 14 of27
EPA Inspection Report - Page 190 of 288
ALS Group USA, Corp
Client: Project: WorkOrdcr:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Date: 18-Aug-16
QC BATCH REPORT
Batch 10: R279951
Instrument: Balance1
Method: M2540D
MBLK Client ID:
Analyte
Sample ID:
WBLKW1-081716
Units: mg/L
Analysis Date: 17-Aug-201611 :25
Run ID: Balance1_279951
SeqNo: 3798863 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
ND
2 .00
LCS Client ID:
Analyte
Sample ID:
WLCSW1-081716
Units: mg/L
Analysis Date: 17-Aug-2016 11 :25
Run ID: Balance1_279951
SeqNo: 3798864 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Con trol Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue , NonFilterable)
102
2.00
100
0
102 78 - 120
DUP Client ID:
Analyte
Sample ID:
HS16080715-09DUP
Units: mg/L
Analysis Date: 17-Aug-201611 :25
Run ID: Balance1 _279951
SeqNo: 3798858 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
152.3
2.00
147.7 3.08 5
DUP Client ID:
Analyte
Sample 10: Outfall 002 - TSS
HS16080566-04DUP
Units: mg/L
Analysis Date: 17-Aug-2016 11:25
Run ID: Balance1_279951
SeqNo: 3798851 PrepDate:
DF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable
29
2.00
30 3.39 5
The rollowing samples were analyzed in this batch:Lf_SI_6_o_so_s_6_6-_0_ 4 _ _ _ _ _ _ _ _ __ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ __J
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 15 of27
EPA Inspection Report - Page 191 of 288
ALS Group USA, Corp
Cl ient: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Date: 16-Aug-16
QC BATCH REPORT
Batch 10: R280023
Instrument: Ba lance1
Metho d: E1664A
MBLK Client 10:
Analyte
Sample 10:
WBLKW-081816
Units: mg/L
Analysis Date: 18-Aug-201611:40
Run 10: Balance1- 280023
Result
POL
SPK Val
SeqNo: 3800102
SPK Ref Value %REC
PrepDate:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
NO
2.00
LCS Client 10:
Analyte
Sample ID:
WLCSW -081816
Units: mg/L
Analysis Date: 18-Aug -2016 11 :40
Run 10: Balance1- 280023
Result
POL
SPK Val
SeqNo: 3800104
SPK Ref Value %REC
PrepDate :
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
36.7
2.00
40
0
91.8 78 - 114
LC SD Client ID:
Analyte
Sample 10:
WLCSDW -08 1816
Units: mg/L
Analysis Date: 18-Aug-201 6 11 :40
Run 10: Balance1- 280023
Result
POL
SPKVal
SeqNo: 3800103
SPK Ref Value
%REC
Prep Date:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPO Limit Qual
Oil and Grease
37.4
2.00
40
0
93 .5 76 - 114
36.7 1.69 18
MS Client 10 :
Analyte
Sample 10:
HS16080587-01 MS
Units: m g/L
Analysis Date: 18-Aug-2016 11 :40
Run 10: Balance1- 280023
Result
POL
SPK Val
SeqNo: 3800081
SPK Ref Value %REC
PrepDate:
Control Limi t
OF : 1
RPD Ref
RPO
Value %RPO Limit Qual
Oil and Grease
39.66
2.00
40
0
99.2 76- 114
T he following samples were analyzed in th is batch: ._fs__l60_s_os_6_6-_o_J_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _____,
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 16 of27
EPA Inspection Report - Page 192 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Date 18-Aug-16
QUALIFIERS, ACRONYMS, UNITS
Qualifier
a
B E H J M n NO 0 p R
s
u
Description
Value exceeds Regulatory Llm1t Not accredited Analyte detected 1n the associated Method Blank above the Reportmg Limit Value above quantita!lon range Analyzed outside of Hold1ng T1me Analyte detected below quant1tat1on hm1t Manually mtegrated, see raw data for JUstification Not offered for accred1tat1on Not Detected at the Report1ng L1m1t Sample amount IS > 4 t1mes amount sp1ked Dual Column results percent difference > 40% RPD above laboratory control hm1t Sp1ke Recovery outside laboratory control hm1ts Analyzed but not detected above the MDUSDL
Acronym
DCS DUP LCS LCSD MBLK MDL MOL MS MSD PDS POL SD SOL TRRP
Description
Delectability Check Study Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Method Blank Method Detect1on L1mit Method Ouanbta!lon L1m1t Matrix Spike Matnx Spike Duplicate Post D1gestion Spike Practical Ouantrtaion Limit Serial Dilution Sample Detect1on L1mit Texas R1sk Reduction Program
Unit Reported mgll
Description
Milligrams per Liter
Page 17 of27
EPA Inspection Report - Page 193 of 288
ALS Group USA, Corp
Agency Arkansas Illinois Kentu cky Louisiana North Carolina North Dakota Oklahoma Te xas
Date: 18-Aug-16
CERTIFICATIONS,ACCREDITATIONS & LICENSES
- ---
Number
16-022-1 003872 96 2016-2017 03087 2016/2017 624-2016 R193 2016-2017 2015-047 TX104704231-16-17
Expire Date
27-Mar-2017 09-May-2017 30-Apr-2017 30-Jun-2017 31-Dec-2016 30-Apr-2017 3 1-Aug-2016 30-Apr-2017
Page 18 of27
EPA Inspection Report - Page 194 of 288
ALS Group USA, Corp
Client: Proj ect: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16080566
Lab Samp ID
HS16080566-01 HS 16080566-02 HS16080566-03 HS 16080566-04 HS16080566-05 HS 16080566-06
Client Sample ID
Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002 - E.Coli Outfall 002 - Hexavalent Cr
Date: 18-Aug-16
SAMPLE TRACKING
Action
Login Login Login Login Login Login
Dat e
8/12/2016 10:46:03 AM 8/12/2016 10:46:03 AM 8/12/2016 10:46:03 AM 8/12/2016 10:46:03 AM 8/12/2016 10:46:03 AM 8/12/2016 10:46:03 AM
Person
CGG CGG CGG CGG CGG CGG
New Location
13C 13C 1E 13C Sub 13C
Page 19 of27
EPA Inspection Report - Page 195 of 288
ALS Group USA, Corp
Client Name: Work Order:
WYMAN-GORDON-HOU HS160B0566
DatefTime Recerved: Received by:
Date: 18-Aug-16
Sample Rec eipt Checklist
12-Auq-2016 10:15 Jared R. Makan
Checklist completed by:
Corey Grandits
eSignature
12-Aug-2016 Date
Reviewed by:
Erica Padilla
eSignature
12-Aug-2016 Date
Matrices:
Carrier name
~
Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper contarner/bottle? Sample containers rntact? TX1005 solids received in hermetically sealed vials? Sufficient sample volume for indicated test? All samples received within holding time? Container/Temp Blank temperature in compliance? Temperature( s)/Thermometer( s ): Cooler(s )/Kit(s): DatefTime sample(s) sent to storage: Water- VOA vials have zero headspace? Water- pH acceptable upon receipt? pH adjusted? pH adjusted by:
Yes 0 Yes O Yes O
Yes ~
Yes ~
Yes 0
Yes ~
Yes 0 Yes O Yes 0
Yes ~ Yes ~
4.2c/4.9c uc/c
23883
08/12/2016 18:10
Yes U
Yes ~
Yes D
No 0 No 0 No D No D No 0
No 0
No 0 No D No D No D No D No 0
No U
No D
No ~
Not Present
0 Not Present 0 Not Present 0
N/A ~
~R#11
D No VOA vials submitted l!j N/A N/A D
Login Notes:
Client Contacted:
Date Contacted:
Person Contacted:
Contacted By: Comments:
Regardrng:
Corrective Action:
Page 20 of27
EPA Inspection Report - Page 196 of 288
Enuironmental
Customer Information Purchase Order
Work Order Company Name : Send Report To
Wyman-Gordon Forgings, LP Aaron Plocek
Address
10825 Telge Road
Project Name Project Number Bill To Company
Invoice Attn
Address
IPage _ _of _ _ I
COCID: 1402
ALS Project Manager:
Project Information
,.111111111110111
Outfall 00?-<-
A COD
I
'
B BOD I
i Wyman-Gordon F orgings, LP
c Oi and Grease
Aaron Placek 0 TSS I
10825 Telge Road
E E.CoU a Hr Hold nrne
F Hexvalent Chrcmlum 24 Hr Hold Time I
~
I
.!
I
City/State/Zip Houston, TX n0955038
City/State/Zip Houston, TX 770955038
G
Phone
Phone (261) 856-9900
H
Fax
Fax
I
e-Mail Address aplocek@wyman.com
No.
Sample OescripUon
1 Outfall -COD
2 Outfall -BOD
3 Outfall -OG
4 Outfall -TSS
e-Mail Address aplocek@wyman.com
Date
~ IZ..
Tlme
Matrix
Pres.
'1: z?- Aqueous
l 7,'"J~ Aqueous
q: zf
Aqueov :~
q: l'l..- Aqueous
II BotUes
J
A
B
X
-1-
X
c D
X X
5 Outfall -E.Coli
tj! 2. 5""...,.-ft Aqueous
6 OutfaH -Hoxavalent Cr 7 8
-J
') .' 2j,AI1-I Aqueous
-
-
- -1--
-
9
.. I
&:R? 10
samJ<s> Please Print
~rt~
Reli~b~/.c..J....
Date:
--
--------
- - - - - .iJ:=p~..t_(,.
Da :
Relinquished by:
Logged by (Uboratory):
Oato:
'Shipment Method
#--e. !J_ t~
IRequired Turnaround Time: (Check Box)
00 Std 10 WK d;m
0 5 WK ~ys
0 Olhar 0 7 WK DaY!i
Timo:
Received by:
Notes:
;v: ~'"""'
Tlme: ' - " - Received by- (l.iiboratory):
10~y TAT.
CooleriD
Cooler Temp.
Tlme:
'JM o'iJ/t 'J..I I t
Checked by (Laboratory):
;o /5
/.flf?
4 -2
lit. II
Preservative Key: 1-HCI 2HN03 3-H~o. 4-NaOH s-N~~o3 6-NaHSO. 7-0ther B-4c 9-5035
CF-0:?
Note: I. Any changes must be mude in wrltinll once snmple.~ and COC Form have been submitted tu ALS F.nimnmentol.
2. Unless other wise llgreecl ln a formttl contract, services provided by ALS Environmenta l arc cxf!ressly limitcjl 12 the terms nnd conditions stntrrl nn th v
3. The Chain nf ru.tnrlv i u '"""' ,.~..-~ " =----
Page 21 of 2 I
I l
I
E F Ql H
! .
I X
X
I
'
-
I ..
. -
-
I
-~
Hold I
I
I
~
-~----
-
1Results Due Dab : r - t
0 24 Hour I
I
QC Package: (Check One Box Below)
I
00 Level 2 Std Qc
0 TRRP ChkUst
I
0 Level 3 Sid QCIRov dP Q TRR P l.evul"'
0 Lavol4 SW84tl/CLP
D Olh&r/EDD
I
Copyright 2011 by ALS Environmental.
EPA Inspection Report - Page 197 of 288
16August 2016
[nvirodync Laboratories, Inc 11011 Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone www.envirodync.com
ALS Group USA, Corp. Bernadette Fini 10450 Stancliff Rd . Suite #210 Houston, TX 77099
ALS
Enclosed are the results of analyses for samples received by the laboratory on 12-Aug-16 13:25. The analytical data provided relates only to the samples as received in this laboratory report.
Ell certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client.
The total number of pages in this report is 5
Thank you for selecting Ell for your analytical needs. If you have any questions regarding this report, please contact us.
Sincerely,
Monica Smith Project Manager
Certificate No TX104704265
Page 22 of27
EPA Inspection Report - Page 198 of 288
Cl ient : Projec t : Work Order:
ALS Group USA, Corp. ALS 16H1903
Sample ID HS16080566-05 OUTFALL 002 E-Coli
ANALYTICAL REPORT FOR SAM PLES
Laboratory I 0 16HI903-0I
Matrix Water
Emirodyne Laboratorirs, Inc II 0 II Brooklet Dr.,# 230 Houston, TX 770941 281.568.7880 Phone www.en\'irodyne.com
Rtporttd: 16-Aug-16 10:14
Date Sampled 12-Aug- 16 09:25
Date Rtceivtd 12-Aug-16 13:25
Envirodyne Laboratories, Inc.
/(s~ird_drn :h
Tlu! resollts in this report app(1to the samples analyud in accordance with the chain of custody document. This analytu:al report must be reproduced in its entirety.
Page 23 of27
EPA Inspection Report - Page 199 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16H1903
Envirodyne Laboratories, Inc II 0 II Brooklet Dr., II 230 Houstoo, TX 77090 28 1.568.7880 Phone www.en\irod) ne.com
R~po rted:
16-Aug-16 I0:14
Analyte
Microbiolo E.coli
HS16080566-05 OUTFALL 002 E-Coli
16H 1903-01 (Water) Sampled: 12-Aug-16 09:25
Result
10
Units Dilution Batch
Prepared
Envirodyne Laboratories, Inc.
Analyzed
M~thod
Analyst Not~
MPN/100 ml
B6HI781 12-Augl6
12Aug-16 14:55
SM9223 B
LTB
Envirodyne Laboratories, Inc.
}I(@Liocfm /h
The rrsults m this report apply to the samples analyzed in accordance with the chain of
custody diXument. This analytcal report must be reproduced m its entirety.
Page 24 of27
EPA Inspection Report - Page 200 of 288
Client: Project: Work Order:
ALS Group USA, Corp. A LS 16H1903
Envirodyne La boratories, Inc II 0 II Brooklet Dr.,# 230 Houston. TX 77099 281.568.7880 Phone www.envirod yne.c om
Rported: 16-Aug-16 10:14
Analyte
Batch 86Hl78 1 - Microbiology Blank (B6H 1781-B LK I)
E.coli
Duplicate (B6HI 781-DUI' I) E.coli
Microbiology - Quality Control Envirodyne Laboratories, Inc.
Result
Reporting Limit
Units
Spike Level
Source Result
% REC
% REC Limits
RPD
RPD Limit
NoleS
Prepared & Analyzed: 12-Aug- 16
<I
I MPNIIOOmL
Source: 16H0955-02
Prepared & Analyzed: 12-Aug-16
137
I MPN/100 mL
107
24.6
0.479
A cfrn :H. Envirodyne Laboratories, Inc. @1i ( ,_
The results in thts report apply ta the samples analyzed in accordance ..-ith the chain of custody document. This analytical report mus/ be reproduced in its entirety
Page 25 of27
EPA Inspection Report - Page 201 of 288
Clie nt:
Project: Work Order:
ALS Group USA, Corp. A LS 16H1903
Notes a nd Definitions
DET NO
Analyte DETECTED Ana lyte NOT DETECTED at or aboe the reporting limit
NR
Not Reported
dry
Sample results reponed on a dry "'eight basis
RPD
Relative Percent Difference
CLT
C lient Representative
Envirod) ne Laboratories, Inc II 0 II Brooklet Dr., #.230 Houston, T ' 77099 28 1.568.7880 Phone , . , .w . env irod yne. com
Repo rted: 16-Aug- 16 10: 14
Envirodyne Laboratories, Inc.
A~(d_~:x
The results in thts report apply to the samples analyzed in accordance "1/h the chain af custOd) document. This anttlytica/ report must be reproduced m its entirety.
Page 26 of27
. .. EPA Inspection Report - Page 202 of 288
Subcontfador - Envirodyne Laboratooes 1~c 11011 Brooklet. Sle 230 Houslon. TX n099
CHAIN OF CUSTODY RECORD
Page 1 of 1
Phone 2815687880
Fu
2815688004
:ate
COC ID Due date
12Aug 2016
5251
22AUG16
10450 Stanciff Rd, Sle 210
dress
Houston. TX n099
Houston. TX 71)99
"P=,h.._on_e-----f~28~1--=5~ 3G-~56~5~ 6 ------+.P=:h- onc _ _ _ _ 81-530-5656 - -- --i
1email1 L-
pac:lilla'@alsglobal com
Email2
.Jmoke lawa~'\lsglobal com
lab ID
Oient Samp 10
CcllectiJfl Date
Mdtnx
Analysis Requested
.-FS--1608_o__56_6 _o_s--.p-ut-faL__:l0_2-~E.~Coli~-~~~~~~~~r-1_2~--A_-ug~----1_6~09-~2~~5~am~~~.F.....Q-. _U-:eO_\-_J-s_-_-_-_-_-_-_._~-u_a__E_._c_o_h_ _
Com ment s
Please analy..:e to.- :he analysis listed above Send report lo the emails show - above.
Page 27 of27
i I EPA Inspection Report - Page 203 of 288
November 21 , 2016
10450 Stancliff Rd. Suite 210 Houston, TX 77099 T: +1 281 530 5656 F: +1 281 530 5887 www.alsglobal.com
Aaron Placek Wyman-Gordon Forgings, LP 10825 Telge Road Houston, TX 77095
Laboratory Results for: Outfall 002
Dear Aaron ,
Work Order: HS1611 0564
ALS Environmental received 6 sample(s) on Nov 11 , 2016 for the analysis presented in the following report.
The analytical data provided relates directly to the samples received by ALS Environmental and for only the analyses requested. Results are expressed as "as received" unless otherwise noted.
QC sample results for this data met EPA or laboratory specifications except as noted in the Case Narrative or as noted with qualifiers in the QC batch information. Should this laboratory report need to be reproduced, it should be reproduced in full unless written approval has been obtained by ALS Environmental. Samples will be disposed in 30 days unless storage arrangements are made.
If you have any questions regarding this report, please feel free to call me. Sincerely,
Generated By: jumoke.lawal
Erica Padilla
PM
Page I of 27
EPA Inspection Report - Page 204 of 288
ALS Group USA, Corp
Client: Pr oj ect: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS16110564
Lab Samp ID HS16110564-01 HS1611 0564-02 HS16110564-03 HS16110564-04 HS161 10564-05 HS16110564-06
Client Sample ID Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E.Coli Outfall 002 - Hexavalent Cr
Date: 21-Nov-16
SAMPLE SUMMARY
Matrix Aqueous Aqueous Aqueous Aqueous Aqueous Aqueous
Tag No
Collection Date 11-Nov-2016 11 :02 11-Nov-2016 11 :03 11-Nov-2016 11 :01 11-Nov-2016 10:57 11-Nov-2016 10:59 11-Nov-2016 10:58
Date Received 11-Nov-201612:00 11-Nov-2016 12:00 11-Nov-2016 12:00 11-Nov-2016 12:00 11-Nov-2 01 6 1 2:00 11-Nov-2016 12:00
Hold
D D D 0 0 D
Page 2 of27
EPA Inspection Report - Page 205 of 288
ALS Group USA, Corp
Date: 21 -Nov-16
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS1 6110564
Work Order Comments
CASE NARRATIVE
The analysis for E.coli was subcontracted to Envirodyne Laboratories, Inc. in Houston, TX. Final report attached.
WetChemistry by Method E410.4 Batch 10: R285113
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method SW7196 Batch 10: R285164
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method M2540D Batch 10: R285108
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method E1664A Batch 10: R285102
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
WetChemistry by Method SM5210 B Batch 10: 109830
The test results meet requirements of the current NELAP standards, state requirements or programs where applicable.
Page 3 of27
EPA Inspection Report - Page 206 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - COD 11-Nov-201611 :02
ANALYSES
RESULT QUAL
CHEMICAL OXYGEN DEMAND BY E410.4
Chemical Oxygen Demand
186
M e t h o d :E410.4
REPORT LIMIT
30.0
Date: 21-Nov-16
ANALYTICAL REPORT
Work0rder:HS16110564 Lab ID:HS16110564-01 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
2
Analyst: KMU 18-Nov-2016 15:30
Note: See Qualifiers Page for a list of qualifiers and their explanation
Page 4 of27
EPA Inspection Report - Page 207 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - BOD 11-Nov-2016 11 :03
ANALYSES
BOD Biochemical Oxygen Demand
RESULT QUAL
Method:SM5210 B 46.0
REPORT LIMIT
2.00
Date: 21-Nov-16
ANALYTICAL REPORT Work0rder:HS161 10564
Lab ID:HS16110564-02 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Prep:SM5210 B / 11 -Nov-2016
Analyst: KMU
mg/L
16-Nov-2016 15:13
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 5 of27
EPA Inspection Report - Page 208 of 288
ALS Group USA, Corp
Client: Project: Sample 10: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - OG 11-Nov-2016 11 :0 1
ANALYSES
OIL & GREASE (HEM) BY E1664A Oil and Grease
RESULT QUAL
Method:E1664A 2.39
REPORT LIMIT
2.00
Date: 21-Nov-16
ANALYTICAL REPORT
Work0rder:HS16110564 Lab ID:HS16110564-03 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 18-Nov-2016 13:50
Note See Qualifiers Page for a list of qualifiers and their explanation
Page 6 of27
EPA Inspection Report - Page 209 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - TSS 11-Nov-2016 10:57
ANALYSES
RESULT QUAL
TOTAL SUSPENDED SOLIDS BY SM 2540D Suspended Solids (Residue, Non -Filterable)
20.5
M e t h o d :M2540D
REPORT LIMIT
2.00
Date: 21-Nov-16
ANALYTICAL REPORT
Work0rder:HS16110564 Lab ID:HS16110564-04 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: KAH 16-Nov-2016 11:30
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 7 of27
EPA Inspection Report - Page 210 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002- E.Coli 11-Nov-2016 10:59
ANALYSES
RESULT QUAL
SUBCONTRACT ANALYSIS - E. COLI
Subcontract Analysis
See Attached
Me thod :NA
REPORT LIMIT
Date: 21-Nov-16
ANALYTICAL REPORT
WorkOrder:HS 16110564 Lab ID:HS16110564-05 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
Analyst: EDL 18-Nov-2016 10 06
Note: See Qualifiers Page for a list of qualifiers and their explanat1on.
Page 8 of27
EPA Inspection Report - Page 211 of 288
ALS Group USA, Corp
Client: Project: Sample ID: Collection Date:
Wyman-Gordon Forgings, LP Outfall 002 Outfall 002 - Hexavalent Cr 11-Nov-2016 10:58
ANALYSES
RESULT QUAL
HEXAVALENT CHROMIUM BY SW7196A Chromium, Hexavalent
Method:SW7196 NO
REPORT LIMIT
0.0100
Date: 21-Nov-16
ANALYTICAL REPORT W o r k 0 r d er: HS 16 11 0564
Lab ID:HS161 10564-06 Matrix:Aqueous
UNITS
DILUTION FACTOR
DATE ANALYZED
mg/L
Analyst: JHD 11-Nov-2016 17:35
Note: See Qualifiers Page for a list of qualifiers and their explanation.
Page 9 of27
EPA Inspection Report - Page 212 of 288
ALS Group USA, Corp
Client:
Wyman-Gordon Forgings, LP
Project: Outfall 002
WorkOrder: HS16110564
Batch 10: 109830
SampiD HS 16 11 0 5 64 -0 2
Method: BOD
Container
Sample WtNol
300
Final Volume
300 (mL)
Prep Factor
Date 21-Nov-16
WEIGHT LOG
Prep: BOD_PR 52108
Page 10 of 27
EPA Inspection Report - Page 213 of 288
ALS G roup USA, Corp
Date: 21-Nov-16
Client: Project: WorkOrder:
Sample ID
Wyman-Gordon Forgings, LP Outfall 002 HS16 110564
Client Samp 10
Collection Date
TCLP Date
Prep Date
DATES REPORT Analysis Date OF
Batch ID 109830
Test Name : BOD
Matrix: Aqueous
HS16110564-02 Outfall 002- BOD
11 Nov 2016 11 :03
11 Nov 2016 13:00 16 Nov 2016 15:13
Batch 10 R285051
Test Name : SUBCONTRACT ANALYSIS -E. COLI
Matrix: Aqueous
H$16110564-05 Outfall 002- E.Coli
11 Nov 2016 10:59
18 Nov 2016 10:06
Batch ID R285102
Test Name: OIL & GREASE (HEM) BY E1664A
Matrix: Aqueous
H$161 10564-03 Outfall 002- OG
11 Nov 2016 11 :01
18 Nov 201613:50
Batch ID R285108
Test Name : TOTAL SUSPENDED SOLIDS BY SM 2540D
Matrix: Aqueous
HS16110564-04 Outfall 002- TSS
11 Nov 2016 1057
18 Nov201611 :30
Batch ID R285113
Test Name : CHEMICAL OXYGEN DEMAND BY E410.4
Matrix: Aqueous
HS16110564-01 Outfall 002- COD
11 Nov 2016 11 :02
18 Nov 201615:30 2
Batch ID R285164
Test Name : HEXAVALENT CHROMIUM BY SW7196A
Matrix: Aqueous
H$16110564-06 Outfall 002- Hexavalent Cr 11 Nov 2016 10:58
11 Nov201617:35
Page II of27
EPA Inspection Report - Page 214 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS 16110564
Date: 21-Nov-16
QC BATCH REPORT
Batch 10: 109830
Instrument: ManTech01
Method: SM5210 B
MBLK Client 10:
Analyte
Sample 10:
MBLK-109830
Units mg/L
Analysis Date: 16-Nov-201615:13
Run 10: ManTec h01_284941 SeqNo: 3895203 PrepDate: 11-Nov-2016 OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
LCS Client 10:
Analyte
Sample 10:
LCS-109830
Units. mg/L
Analysis Date: 16-Nov-2016 15:13
Run 10 . ManTech01_284941 SeqNo: 3895202 PrepDate: 11 -Nov-2016 OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Biochemical Oxygen Demand
178.9
2.00
198
0 90.3 85 - 115
DUP Client ID:
Analyte
Sample 10
HS16110496-01DUP
Units: mg/L
Analysis Date: 16-Nov-2016 15:13
Run 10 ManTech01_284941 SeqNo: 3895201 PrepDate: 11 -Nov-2016 DF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Biochemical Oxygen Demand
NO
2.00
2.05
0 20
The rollowing samples nere ana lyzed in this batch : rl..._s_16_1_10_s_64_-_o_2_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _---'
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page 12 of27
EPA Inspection Report - Page 215 of 288
ALS Group USA, Corp
Client : Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16110564
Date: 21-Nov-16
QC BATCH REPORT
Batch 10: R285102
Instrument: Balance1
Method: E1664A
MBLK Client 10:
Analyte
Sample 10 :
WBLKW-1 11816
Units: mg/L
Analysis Date: 18-Nov-201613:50
Run 10: Balance1- 285102
Result
POL
SPK Val
SeqNo. 3898767
SPK Ref Value %REC
Prep Date:
Control Limit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
NO
2.00
LCS Client 10:
Analyte
Sample ID:
WLCSW-111816
Units: mg/L
Analysis Date: 18-Nov-2016 13:50
Run 10 : Balance1_285102
SeqNo: 3898769 PrepDate:
OF: 1
Result
POL
SPKVal
SPK Ref Value
%REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
37.5
2 00
40
0 93.8 78- 114
LCSD Client ID:
Analyte
Sample 10:
WLCSDW-111816
Units: mg/L
Analysis Date: 18-Nov-201613:50
Run ID: Balance1- 285102
Result
POL
SPKVal
SeqNo: 3898768
SPK Ref Value %REC
PrepDate:
Control Limit
OF 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
37.1
2.00
40
0
92.8 78 - 114
37.5 1.07 18
MS ClientiD:
Analyte
Sample ID
HS1611 0628-03MS
Units: mg/L
Analysis Date: 18-Nov-201613:50
Run 10 Balance1- 285102
Result
POL
SPKVal
SeqNo: 3898765
SPK Ref Value %REC
PrepDate:
Control L1mit
OF: 1
RPD Ref
RPD
Value %RPD Limit Qual
Oil and Grease
39.21
2.00
40
0.2247 97.5 78- 114
The followin g samples were analp ,ed in this bat ch : '-r_sl_6_t_lo_s_64_-_o_J_ _ _ _ __ _ __ _ __ _ _ _ _ _ _ _ __ _ _ _ _ _ ______.
Note: See Qualifiers Page for a list o f qualifiers and their explanation.
Page 13 of27
EPA Inspection Report - Page 216 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS16110564
Date: 21-Nov-16
QC BATCH REPORT
Batch ID: R285108
Instrument: Balance1
Method: M2540D
MBLK Client ID:
Analyle
Sample 10:
WBLKW1 -111816
Units: mg/L
Analysis Date: 18-Nov-2016 11 :30
Run 10 . Balance1_285108
SeqNo: 3898863 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable)
NO
2.00
LCS Client 10:
Analyte
Sample 10:
WLCSW1-111816
Units: mg/L
Analysis Date: 18-Nov-201611:30
Run 10: Balance1_285108
Seq No: 3898864 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Restdue, NonFilterable)
91
2 .00
100
0 91 .0 78- 120
DUP Clienti D:
Analyte
Sample 10:
HS16110680-01DUP
Units: mg/L
Analysis Date: 18-Nov-201611 :30
Run ID Balance1_ 285108
SeqNo: 3898857 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue. NonFilterable)
23.6
2.00
24.8 4.96 5
DUP ClientiD:
Analyte
Sample 10 :
HS16110628-01DUP
Units: mg/L
Analysis Date: 18-Nov-2016 11 :30
Run 10. Balance1_285108
SeqNo: 3898853 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPO Ref
RPD
Value %RPD Limit Qual
Suspended Solids (Residue, NonFilterable
82 .67
2.00
83.56 1.07 5
The foll owing samples were analyzed in this b11tch: rL-s_I 6_I_I0_5_64_-_o_4_ _ __ _ _ _ _ _ _ _ _ _ _ _ _ _ __ __ _ _ __ _ ____J
Note: See Qualifiers Page for a list o f qua lifiers and their explanatio n.
Page 14 of27
EPA Inspection Report - Page 217 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS1611 0564
Date: 21-Nov-16
QC BATCH REPORT
Batch 10: R285113
Instrument: WetChem_HS
Method: E410.4
MBLK Client tO:
Analyte
Sample 10 :
MBLK-285113
Units: mg/L
Analysis Date: 18-Nov-2016 15:30
Run 10. WetChem_HS_28511 3 SeqNo: 3898933 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
NO
15.0
LCS Client 10:
Analyte
Sample 10:
LCS-285113
Units: mg/L
Analysis Date: 18-Nov-2016 15:30
Run 10: WetChem_HS_285113 SeqNo: 3898934 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
POL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chemical Oxygen Demand
91
15.0
100
0 91.0 85- 115
MS ClientiD.
Analyte
Sample 10 :
HS16110817-01MS
Units: mg/L
Analysis Date: 18-Nov -201615:30
Run 10: WetChem_HS_28511 3 SeqNo: 3898936 PrepDate:
OF 1
Result
POL
SPKVal
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
131
15.0
50
82 98.0 80- 120
DUP Client 10 :
Analyte
Sample ID
HS16110817-01 OUP
Units: mg/L
Analysis Date: 18-Nov -2016 15:30
Run 10 : WetChem_HS_285113 SeqNo: 3898935 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chemical Oxygen Demand
79
15.0
82 3.73 20
The following samples were analyzed in this batch : Lr_s_t6_tt_o_s_64_-_o_l_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ __ _ _ _ _ _ _ _ ___,
Note: See Qualifiers Page for a list ofqualifiers and their explanation.
Page IS of27
EPA Inspection Report - Page 218 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002 HS161 10564
Date: 21-Nov-16
QC BATCH REPORT
Batch ID: R285164
Instrument: UV-2450
Method: SW7196
MBLK Client 10:
Analyte
Sample 10:
MBLK-285164
Units: mg/L
Analysis Date: 11 -Nov-201617:35
Run 10: UV-2450_285164
SeqNo: 3899888 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value %REC
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
NO
0,0100
LCS Client 10 :
Analyte
Sample 10:
LCS -285164
Units: mg/L
Analysis Date: 11-Nov-2016 17:35
Run 10: UV-2450_285164
SeqNo: 3899889 PrepDate:
OF: 1
Result
SPK Ref
Control RPD Ref
RPD
PQL
SPK Val
Value %REC
Limit
Value %RPD Limit Qual
Chromium, Hexavalent
0 .275
0 0100
0.25
0
110 80- 120
LCSO Client 10 :
Analyte
Sample 10
L C S 0 -285164
Units: mg/L
Analysis Date: 11-Nov -2016 17:35
Run 10: UV-2450_2851 64
SeqNo 3899890 PrepDate:
OF: 1
Result
PQL
SPK Val
SPK Ref Value %REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
0.272
0 .0100
0.25
0
109 80- 120
0 .275
1.1 20
MS Client ID:
Analyte
Sample 10:
HS16110561-06MS
Units: mg/L
Analysis Date: 11 -Nov -2016 17:35
Run ID UV-2450_285164
SeqNo 3899891 PrepDate:
OF: 1
Result
POL
SPK Val
SPK Ref Value
%REG
Control Limit
RPD Ref
RPD
Value %RPD Limit Qual
Chromium, Hexavalent
0.275
0.0100
0.25
0 .003
109 75- 125
T he fo llowing samples were analyzed in this batch: rL.IS__I6_1_I_os_6_4-_0_6 _ _ _ _ _ _ _ _ __ _ _ _ __ _ _ _ __ _ _ __ _ __ ____,
Note: See Quali tiers Page for a list of qualifiers and their explanation.
Page 16 of27
EPA Inspection Report - Page 219 of 288
ALS Group USA, Corp
Client: Project: WorkOrder:
Wyman-Gordon Forgings, LP Outfall 002
HS16110564
Date: 21-Nov-16
QUALIFIERS, ACRONYMS, UNITS
Qual ifier
a B E H J M n ND 0 P R S U
Description
Value exceeds Regulatory Limit Not accredited Analyte detected in the associated Method Blank above the Reporting Limit Value above quantitation range Analyzed outside of Holding Time Analyte detected below quantitation limit Manually integrated, see raw data for justification Not offered for accreditation Not Detected at the Reporting Limit Sample amount is > 4 times amount spiked Dual Column results percent difference > 40% RPD above laboratory control limit Spike Recovery outside laboratory control limits Analyzed but not detected above the MDUSDL
Acronym
DCS DUP LCS LCSD MBLK MDL MQL MS MSD PDS PQL SO SOL TRRP
Description
Delectability Check Study Method Duplicate Laboratory Control Sample Laboratory Control Sample Duplicate Method Blank Method Detection Limit Method Quantitation Limit Matrix Spike Matrix Spike Duplicate Post Digestion Spike Practical Quantitaion Limit Serial Dilution Sample Detection Limit Texas Risk Reduction Program
Unit Reported
mg/L
Description
Milligrams per Liter
Page 17 of27
EPA Inspection Report - Page 220 of 288
ALS Group USA, Corp
Agency Arkansas California Illinois Kansas Ken tucky Louisiana North Carolina North Dakota Oklahoma Texas
Date: 21-Nov-16
CERTIFICATIONS,ACCREDITATIONS & LICENSES
Number
16-022-1 2919 2016-2018 003872 E-1 0352 2016-2017 96 2016-2017 03087 2016-2017 624-2016 R193 2016-2017 2016-122 TX104704231-16-17
Expire Date
27-Mar-2017 31-Jul-2018 0 9-M a y- 20 17 31-Jul-2017 30-Apr-2017 30-Jun-2017 31-Dec-2016 30-Apr-2017 31-Aug-2017 30-Apr-2017
Page 18 of27
EPA Inspection Report - Page 221 of 288
ALS Group USA, Corp
Client: Project: Work Order:
Wyman-Gordon Forgings, LP Outfall 002 HS1 6110564
Lab Samp 10
HS16 110564-01 HS 16110564-02 HS16 11 0564-03 HS16 110564-04 HS161 10564-05 HS161 10564-06
Client Sample 10
Outfall 002 - COD Outfall 002 - BOD Outfall 002 - OG Outfall 002 - TSS Outfall 002- E .Coli Outfall 002 - Hexavalent Cr
Date: 21-Nov-16
SAMPLE TRACKING
Action
Login Login Login Login Login Login
Date
11/11/2016 2:38:27 PM 11/11/2016 2:38:29 PM 11 /11/2016 2:38:32 PM 11 /11/2016 2:38:35 PM 11/11/2016 2:38:39 PM 11111/2016 2:38:41 PM
Person
JRM JRM JRM JRM JRM JRM
New Location
Disposed Dispo sed 1E Disposed Sub Disposed
Page 19 of27
EPA Inspection Report - Page 222 of 288
ALS Group USA, Corp
Client Name: Work Order:
WYMAN-GORDON-HOU HS16110564
DatefTime Received: Received by:
Date: 21-Nov-16
Sample Receipt Checklist
11-t:jQv -2Q1!i 1 ~:QQ
g._
Checklist completed by:
Jared R. Makan
11-Nov-2016
-eS~ig-n-at~u-re-------------,~~~~~-
Date
Reviewed by:
Matrices:
Carrier name:
Erica Padilla
eSignature
.Qi.W
14-Nov-2016 Date
Shipping container/cooler in good condition? Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? TX1005 solids received in hermetically sealed vials? Sufficient sample volume for indicated test? All samples received within holding time? ContainerfTemp Blank temperature in compliance? Temperature(s)fThermometer(s): Cooler( s)/Kit(s ) : DatefTime sample(s) sent to storage: Water- VOA vials have zero headspace? Water- pH acceptable upon receipt? pH adjusted? pH adjusted by
Yes ~
Yes 0 Yes 0
Yes ~ Yes ~
Yes 0
Yes ~ Yes ~
Yes 0
Yes ~ Yes ~ Yes ~
O.Bc/1.1 c
UC/C
42551
11/11/201614:45
Yes 0
Yes~
Yes O
No 0 No 0 No 0 No 0 No 0
No ~
No 0 No 0 No 0 No 0 No 0 No 0
No 0 No O No O
0 Not Present
Not Present ~ Not Present ~
N/A ~
I!IR11
No VOA vials submitted [!!]
N/A 0
N/A ~
Login Notes:
ample ID differs for all samples: COC =Outfall 001 , Sample container and COC Project Name - Outfall 002. Logged in as Outfall 02.
Client Contacted:
Date Contacted:
Person Contacted:
Contacted By: Comments:
Regarding:
Corrective Action:
Page 20 of27
EPA Inspection Report - Page 223 of 288
A Enuuonmental
'
Cincinnati, c;>H +1 513 733 ? 336
Everen, WA j + I 425 356 2600
I
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i
I
Fort Collins , CO +1 9704901511
Holland, Ml +I 616 399 6070
Chain of Custody Form
IPage _ _ of _ _ I COC ID: 2 6 745
ALS Project Manager:
Houston, TX +1 281 530 56 56
Middletown. PA +1 717 944 5541
Spring City, PA +1 610 948 4 903
Salt lake City, UT + I 801 266 7700
I ALS Work Order #:I
South Charles ton, WV +1 304 356 3168
York, PA +I 717 505 5280
Customer Information
I
Project Information
Parameter/Method Request for Analysis
Purchase Order
I _ _ _ _ _ _ _ _ _ _ _ _ __ _ j_ _
1-------
Woi'X Order
I
- - -1
Company Name
----- ----- ~~~~f''qJ~-~- --
Send Report To ~y_.._..,___lC?%, wL...
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Name
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Project Number
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Sample Descrlptfon
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Isjzt I I Samplds) Please Print & Si~.d
..
I ........,p/..<eft.-
~dby:
Ioa;~''L,_p_& r-~"'' ~-r~ /P. Relinquished by:
Date':
__ Time:
I
Method
h.!.~,_,
Recei~
Required Turnaround Time: (Check BoxJ 0 Other
0 STO 10 Wk Days
0 5 Wk Days
0 2 Wk Days
Notes:
I
Results Due Date:
0 24 Hour
'
CooleriD
Cooler Temp QC Packaae: (Check One Box Belowl
~vr7l7Jl~bro-ratro~ !-!6 Logged by (Laboratory):
Preservative Key; 1-HCI-
2- H N 03
Da te:
- 3- H~so.
Time:
4 NaOH
(_
5-NaaSa0 3
6-NaHso.
7 0ther
W!~ IZ84C 9-5035 -
-'/2...>S'l
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~
(). fl
T
1-0. "\
0 Level 11 Std ac 0 Level lII Std OC/ Raw Date 0 Level IV SW646/CLP
O Other
0 TRAP Checklisl
0 TRAP Level IV
Note:
I. A ny changes must be made in writing once samples lmd COC Form hu\'Cbeen submilled to AU ; Erwironmen tal. 2. Unless otherwise ngreed in a formal co ntr;~ct, scnices prO\idcd by ALS Environmental nrc expressly limited to the terms and t'onditions stuted on the reverse. 3. The Chain nf Custody i s ulcgnl dncumeut. All iurornmtio n must be completed accur a tely.
Page 2 1 of27
Copyright 201 2 by ALS Environmental.
EPA Inspection Report - Page 224 of 288
17 November 2016
En\irodyne Laboratories, Inc II0 II Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone n w".cnvirodyne.com
ALS Group USA, Corp. Bernadette Fini 10450 Stancliff Rd. Suite #210 Houston, TX 77099
ALS
Enclosed are the results of analyses for samples received by the laboratory on 11-Nov-16 15:06. The analytical data provided relates only to the samples as received in this laboratory report.
Ell certifies that all results are NELAP compliant and performed in accordance with the referenced method except as noted in the Case Narrative or as noted with a qualifier. Any reproductions of this laboratory report should be in full and only with the written authorization from the client.
The total number of pages in this report is 5
Thank you for selecting Ell for your analytical needs. If you have any questions regarding this report, please contact us.
Sincerely,
Monica Smith Project Manager
Certificate No. TX104704265
Page 22 of27
EPA Inspection Report - Page 225 of 288
Client: Project: Work Order:
ALS Group USA, Corp . ALS 16K1966
Sample ID liS 16110564-05 Outfall 002- E Coli
ANALYTICAL REPORT FOR SAMPLES
LJiborarory ID 16K I966-01
Matrix Water
Emirodync Laboratories, Inc II 0 I I Brooklet Dr., II 230 Houston, TX 77099 281.568.7880 Phone www .c nv ir o d y n e.co m
Reported: 17-Nov- 1622:15
Date Sampled 11 -Nov-16 I0:59
Dale Receh rd 11-Nov-16 15:06
A cJn :h Envirodyne Laboratories, Inc. oWe ( d_
The reJults in this report apply to the samples analy::ed in accordance with the chain of Cll.stody document Tlti.s analytical report must be repf'()(/uced m its entiret}'.
Page 23 of27
EPA Inspection Report - Page 226 of 288
Client: Proj ect: Work Order:
ALS Group USA, Corp. ALS 16K1966
[ nvirodyne Laboratories, Inc 11 011 Brooklet Or.,# 230 Houston, TX 77099 281.568.7880 Phone www. cnvirody ne.com
Rt p o r t e d : 17-Nov- 16 22: 15
Analyte
M ic ro b io lo [ .coli
Result 53
HS 16 110564-05 Outfa ll 002- E Coli
16K1966-0I (Water) Sampled: 11-Nov-16 10:59
Reponing Limit
Units Dilution
Batch
Prepared
Envirodyne Laborato r ies, Inc.
Analyzed
Method Analyst Notes
MPNI IOOmL
B6KI 798 11 -Nov-16
11 -Nov- 16 I-U5
SMn23 B VLM
Envirodyne Laboratories, Inc.
A~(d_Jrn:x
The JTsults in this rt!port app~ to the samples tma~l'zed in accordanu with the cham of custodydocument. This analytical report must be reproduced in its entirety
Page 24 of27
EPA Inspection Report - Page 227 of 288
C lient: P roj e c t : Work Order:
ALS Group USA, Corp. ALS 16K1966
Envirodyne Laboratories, Inc 11011 Brooklet Or., # 230 Houston, TX 77099 281.568.7880 Phone w" w.envirodyne.com
R~ported :
17-Nov-16 22:15
Analyle
Batch B6K1798 - Microbiologv Blank (B6KI 798-BLKI )
E.coli
Duplicate (B6K 1798-DUPI ) E.coli
Microbiology- Quality Control Envirodyne Laboratories, Inc.
Resuh
Reponing Limil
Unils
Spike
Source
% REC
Le,el
Resuh
%REC
Limils
RPD
RPD Limil
Noles
Prepared & Analyzed: 11-Nov-16
<I
I MPN' IOO ml
Source: 161<1087-02
Prepared & Analyzed: 11 -Nov- 16
<2
:? MPN/100 ml
0
0.6095
Envirodyne Laboratories, Inc.
A~r,_cJn:ftv
The results in tlr/S report apply to the samples anlll)'zed in acrordance Wtlh the chain of ctutody document. This analyiiC'al report must be reproduced in its entirety
Page 25 of27
EPA Inspection Report - Page 228 of 288
Client: Project: Work Order:
ALS Group USA, Corp. ALS 16K1966
Notes and Definitions
DET
Analyte DETECTED
NO
Analyte NOT DETECTED at or abcne the reporting limit
N R
Not Reported
dry RPD CLT
Sample results reponed on a dry weight basis Relative Percent Difference Client Rcpresentatie
Envirodyne Laboratories, Inc 11011 Brooklet Dr.,# 230 Houston, TX 77099 281.568.7880 Phone www.envirodync.com
Repor1cd: 17-Nov- 16 22:15
J1~ Envirodyne Laboratories, Inc.
("c), :h
The results in this report apply to the samples analy:ed tn accordance with the chain af custody document. This analytical report must be reproduced in its entirety
Page 26 of27
EPA Inspection Report - Page 229 of 288
A 1u1ronmentat
Subcontractor Envirodyne Laboratories, Inc. 11011 Brooklet, Ste 230 Houston, TX 77099
CHAIN OF CUSTODY RECORD
Page 1 of 1
Phone 2815687880
FaK
2815688004
r--------~c~u-s.t~o-m-er~l~nf~o-~ ~~ ~
PO
HS16110564
Project Name
Date
coc ID
Due date
Company Name
ALS Houston
A d d res s
10450 Stancliff Rd, Ste 210
Company Name lnvAttn Address
ALS Houston Accounts Payable 10450 Stancliff Rd. Ste 210
Phone Emall1
Houston, TX 77099 281-530-5656 erica.padilla@alsglobal.com
Phone Email2
Houston, TX 77099 281-530-5656 'umoke.lawal@alsglobal.com
Lab 10 HS161 10564-05
Client Samp ID Outfall 002 - E.Coli
Collection Date 11-Nov-16 10:59 am
Matrix queous
Analysis Requested UB_E. Coli
11 Nov 2016
5727
21 NOV 16
Comments
Please analyze for the analysis listed abOve. Send report to the emails shown above.
Relinquished by:
J. 1'1f.ll< ltN
D a tefTim e:
//.'s'/: "o&//(
Received by:
DatefTime:
jkAD~/ "1'"~
""'rCooler IDs:
~ <J/vt'Rd-\3
Report/QC l evel
r
Page 27 of27
EPA Inspection Report - Page 230 of 288
Wyman-Gordon Forgings / Wyman-Gordon Houston 06/27-28/2017
Appendix 4 Whole Effluent Toxicity (WET) Testing Laboratory Results
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