Document e5q4QEa51wDvm5y6ZDaYDLadg
1). V. 904
DATE PRINTED: 1/27/82
>>ft 32
CODE
"OCT 2 5 1982
RT~L&Kb
F'KG
PROCESSES )RT-618-D <T)
APPROVED BY EWi< 12/8/81
( DATE >
(LOT HUMBER
J.3TO
^WED BY: KLW
EST. WT. im#* LBS'. STD/ HRS. _____ TIME 3fl J1
COMTYP JOB NAME: PREPARATION NOTES :___________ ,_________________________
32RTS18DHT
- NON-BLEEDING
NAME: WA'TCHUNG RED Y
CRD:
__BATCHES SINCE SPARKLER LAST
USE LBS
|
I N-CQDE ! AGOT i ! LBS -
|
CLEANED. AFTER 4 BATCHES, CLEAN, DRESS I SPARKLER & PRE-COAT WITH 13# DICALITE
I |
/r~
ILTER AID
j|
BTAIN FORSI 1 2-CHLORO-4-AMINOTOLUENE--5- |
|
SULFONIC ACID
'| |
OBTAIN FOR S24 3-HYBROXY--2-NAPHTHOIC ACID I
|
INSTALL DV A CV RECORDER G CONTROLLER CHART!
[
NOTE: NOTIFY PRESS ROOM AND ROPE OFF AREA ]
!
BEE V-922
^
|I
UN 5 0* (i O0G> WATER'INTO V-jOil... & .AD J TO I
i
-100 DEG F
!!
6 L `"ADD IN 1 -2 MIN. PEESINATEX
\ 5Q , )
R 2 MIN & RECORD : PH,,_/&i,,<9..3--10.5)' i
I
STIR 20 MIN OR LONGER FOR S27
||
77 7-A I f
740-C 1 I
253-C I
5 30-A
/jT~ DO
IN 30 * (o20G 5 WATER INTO V-922 ! WEIGH IN V-924 SODIUM HYDROXIDE & Rig
| i
! TURN ON AGITATOR A STEAM OuMP~iN~FR0ir55 I ?:^^?o l u e n e .....ilk............!i^,,
|
i 7-D i 178 I 740-C | S2&
I
-S-SULFONIC
__________ _ ______
________ l____ _.J
r j ^acC ID
AJiT^Sm? IN ACTIVATED CARBON ? 7?
40 i 1'13-B I 40
DUMP IN DICALITE FILTER AID
*J
J 10
777-A \ 10
HEAT Tp 212-214 DEG F, RECORD HTjgrJjL # F, I
___ DEG F WATCH FOAM
|
I !
I
RECORD BY_fc< + >, IF NECESSARY ABJ TO +BY !
1 SODIUM HYDROXIDE
ASSUME 507 |_______ !
7-D 1
STIR 30 MIN AT 212-214 DEG F, THEN SHUT
|
i
! j OFF STEAM
WATCH FOAM
J
| | NOTE: RECORD: SPARKLER PRESSURE
___ PSI I
I i IJLNO'r ZERO, NOTIFY SUPERVISOR
I
I 1>^j<CIR.bULATE 13 MIN OR LONGER THRU SPARKLER I f* 1 UNTIL SOL'N IS CLEAR. MAINTAIN AT 190-195 F|
OdT 2719821
) ! FOR' 519 & RECORD: HT.....J^^.._DEG F AND i \m
! I RECORDER
.F ^ I
i i RECORD: START J&gZZ.1_, TOTAL MIN,,...^,,fe.______,1 1 J CLARITY^jfefe..... . NOTE: SAMPLE FROM HOSE - !
' i SHOW TO SUPERVISOR FOR C.K,
I
ttaSU IP i MEN!
2 OF 3
CG 32
CODE
MAKING r-. RT-618-D <T>
INSTRUCTIONS:BATCH UNIT
USE LBS
N-CODE i a c c t | LBS
RUN 1* C50O WATER INTO V-904 19^MrfHirSl ? COMPLETE, PUMP IN V-922 THRU
SPARKLER, MAINTAINJ/-922 AT 190-1:95 ,ftG F RECORD: STAftTJyjfci.teTnrOTAL MIN.
WEIGH IN FT FOR S35 SODIUM NITRITE m_____i
121 p. MEASURE ,,.2l <L_..UNITS IN V-928 FOR S33
I HYDROCHLORIC ACID M___ Zfc._ _ _ _ Zh
lHjt\
725-A , 2,8 ~ D
AVn
UN t* <13300 WATER INTO VWEIGH IN V--926 SODIUM HYDROXIDE & RUN IN j
M &&.% .1 J
DUMP IN FROM S3 3-HYDR0XY-2-
LOT. _____jJH______
1
HAPHTHOJQ AC IT
es~>--___ __,___---I
?~D 45G T<S>/Z>
Uttrjsltfj TO 70-90 DEG F X- STIR TO DISSOLVE \p?T I STEAM EJECT V~3ri /931 INTO CV
! i
~o-~- \^\jAw SI 9 COMPLETE, SHUT OFF PUMP & INSERT |
f Vf V-922 FOOT PLUG
I
l/(l| RUN IN 10* C2.07O WATER & HEAT TO 190-195 Fi
CIRCULATE 15 MIN THRU SPARKLER *
j
904 f| PUMP V-922 THRU SPARKLER INTO V-904
|
o"..i i! RUN IN 5" (1030 WATER INTO V-922 & HEAT TO 9 12j&*~f95 F. CIRCULATE 15 MIN THRU SPARKLER
V-922 THRU SPARKLER INTO V-904
\yr\jfflm mt y b l o w o u t s p a r k l e r in t o v -904
l&ZT HEAT TO 185-170 F (SMPL TO SUPVR FOR O.KJ)
JH IN N-28-D FROM S21 IN 12-15 MIN & STIR
S yT5 MIN AT 165-170 DEG F
% I ADJ TO 129* <34090 AT 28-30 DEG F AND
RECORD : TEMP ,7ff T F ___________ " ICE
RUN IN N-725-A FROM S20 AFAR <5-10 MIN)
i | h. RINSE IN P7
136 1 STIR 3 MIN AT 28-35 DEG F MAINTAINING'
( i +CR, +KI FOR S4i AND RECORD:
i I TI ME START tn'MAk. CP
< + ) , K IS. ____ < + >
I i NOTE (1) IF CR-^fXI-f ADD 20* AS IS IN-
40X330:
i I CREMEHTS
HYDROCHLORIC ACID ASSUME 323
} " f RECORD: CR_____ { + ), KI_____ __<-H
! ! (2> IF OR*-, KI -, ADD 20* AS IS INCREMENTS
!' i SODIUM NITRITE.
ASSUME 33% i__
1 [ RECORD : CR . ( t-> , KI________ < + >
II
2S-A .25-A
DUP050060726
MAK 1NG I NSTRUCTIONS: BATCH UNIT
EQUIP -SENT
E 3 OF 3 CG 32 CODE R7-6J8-P <T>
i USE I LBS
"a c c t LBS
CV i DUMP INTO CV BARIUM SULFATE
1 1 iS^TADJ TGJPf* <3l 3.0G) AT 2B-32*F
ICE
TEMP_,,.StCl.-EG F & VOLUME_____\
IN FROM DRUM AMMONIUM CHLORIDE
" mjf'friR 2-3 MIN
| j 33X330
| 212 j
65-A 37-A
165-A
l
| km*
I j 212
\m\ IMMEDIATELY COUPLE DV THRU UNDERSURFACE
j
DISTRIBUTOR INTO CV IN 43-60 MIN. MAINTAIN i
57-A
CV AT 28-32 DG F, RECORD: START J$* , i
TAL MIN
____
j
!
STIR 30 MIN & RECORIU, BASE JX---< + >*
I-
DIAZO
^.-9.8)
I
NAL TEMP ________ DS F
|
IF NECESSARY.. ADJ TO >H 9,9-9,8 AND RECORD i
*
PPL
SODIUM HYDROXIDE
ASSUME 50% |
7"D |,
HYDROCHLORIC ACID
ASSUME 32% }_
28-D |.
HEAT TO (&$"iDEG f IN 65-70 MIN AND
j
RECORD: KT____ DEG F t, RECORDER /2JL...DEG F |
MOTE : AT 174-176 F.. OREM HATER SPRAY
j
1 1/4 TURNS
!
902 fcUN 24* 1618G >WATER INTO V902
i
! TURN ON AGITATOR & STEAM .& DUMP IN BARIUM i 1440
J--CHL0RIDE
I
*7\ HE A'I TO
G STIR TO DISSOLVE
1 6-B 1440
CV WHEN S44 COMPLETE, IMMEDIATELY STRIKE V902 I
13 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN
7-10 MIN* MAINTAIN CV AT
PEG F*
f'6.
: STARI_/,lj52$.T0TAu. MIN /$
-CV TO 198-202 DEG F IN iO-i'^MIN
5 MIN AT 190-202 DEG F
FLOOD TO 1IS8O"-l?i?/j^f'" (+/-] 000G)
RECORD : PHj&jJfl < 9..' -9" * 4 > & STOP AGITATOR
SHUT OFF WATER SPRAYS
i
II
1W
ZZ.^l%i'^'...Z3pZl-Z
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY 1
THRU PRESSING, DUMP IN, STIR 5 MIN & STOP I
AGITATOR* RESUME PRESSING* I-OCTftNOL.
]
I
5S0-A 1 16
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