Document e5LNZ7Rb1mMwOELgvBYqBN3jM

27-CV-10-28862 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM Hennepin County, MN STATE OF MINNESOTA COUNTY OF HENNEPIN State of Minnesota, by its Attorney General, Lori Swanson, its Commissioner of Pollution Control, John Linc Stine, and its Commissioner of Natural Resources, Tom Landwehr, Plaintiff, vs. 3M Company, Defendant. DISTRICT COURT FOURTH JUDICIAL DISTRICT Case Type: Other Civil Judge Kevin S. Burke Court File No. 27-CV-10-28862 PLAINTIFF STATE OF MINNESOTA'S SECOND AMENDED EXHIBIT LIST Plaintiff State of Minnesota ("State") states that it may offer into evidence in its case-inchief at trial of the above captioned matter: (1) the documents identified on the parties' Joint Exhibit List filed January 19, 2018; and (2) the documents identified on the State's Second Amended Exhibit List attached.1 In addition, the State respectfully reserves the right to use or offer as exhibits (1) all documents identified or referenced on Defendant's exhibit list, (2) any publicly-available materials, including articles, reports, or journal publications, and (3) any documents that may be necessary to respond to undisclosed evidence from Defendant, to rebut Defendant's evidence, to impeach Defendant's evidence, or to clarify or correct the record. In addition, the State respectfully reserves the right to submit an amended or supplemental exhibit list, or to withdraw any of the exhibits on the State's Second Amended Exhibit List, as becomes necessary or 1 Please note that the exhibit numbers in the Second Amended Exhibit List are not consecutive and contain gaps due to exhibits that were removed from the State's Initial and Amended Exhibit Lists filed January 19, 2018 and January 31, 2018. The Second Amended Exhibit List contains 777 entries. 1 27-CV-10-28862 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM Hennepin County, MN appropriate, including in light of (1) ongoing discovery, (2) the Court's rulings on other motions filed by the parties, and (3) Defendant's exhibit list. Finally, the State reserves the right to use demonstrative exhibits not listed on the State's Second Amended Exhibit List. DATED: February 14, 2018 Respectfully submitted, LORI SWANSON Attorney General State of Minnesota /s/ Alethea M. Huyser Alethea M. Huyser (No. 0389270) Assistant Solicitor General 445 Minnesota Street, Suite 1100 St. Paul, Minnesota 55101-2127 (651) 757-1243 (Voice) (651) 282-5832 (Fax) alethea.huyser@ag.state.mn.us John E. Hall Anthony Herman Covington & Burling LLP One CityCenter 850 Tenth Street, N.W. Washington, D.C. 20001 (202) 662-6000 ATTORNEYS FOR PLAINTIFF STATE OF MINNESOTA 2 Plaintiff's Ex. No. 1001 1002 1003 1005 1008 1009 1010 1011 1012 1020 1025 1026 1028 1029 1031 1032 Date 3/28/1999 3/28/1999 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Letter from R. Purdy to 3M re: Resignation Email from R. Purdy to E. Reiner et al. re: Rich Purdy's Resignation 3/29/1999 8/24/1948 Email from G. Adams to D. Sonstegard re: 8e Follow up - Fish U.S. Patent Office, Simons, J. H., Fluorination of Organic Compounds, U.S. Patent No. 2,447,717 9/26/1949 1/10/1950 8/22/1950 00/00/1952 3M Company Fluorochemicals Brochure Heptafluorobutyric Acid PFBA LD50 test (3M Toxicology) U.S. Patent Office, Simons, J. H., Electrochemical Process of Making Fluorine-Containing Carbon-Compounds, U.S. Patent No. 2,519,983 State Water Pollution Control Board, Report on the Investigation of Leaching of Ash Dumps: 3-87. 00/00/1953 9/26/1958 7/13/1960 8/9/1960 11/3/1960 4/14/1961 12/1/1961 00/00/1961 State Water Pollution Control Board, Field Investigation of Waste Water In Relation to Ground Water Reclamation: 3-124. Report on Investigation of Waste Disposal Minnesota Mining and Manufacturing Company, Chemolite Plant Washington County September 22-26, 1958 Memorandum from J. Brown to H. Wessel re: Proposed Dump Site Field letter of A. Miller and R. Collins For Geology Department Use Only 3M Interoffice Correspondence from J.T. Ling to Various Recipients re: Chemolite Monthly Water Report with Central Analytical Laboratory Report No. 3873 3M Life Magazine Scotchgard Ad 3M Interoffice Correspondence from L.C. Houdek to H.S. Parkinson re: Rebuilding and Relocation of Sewage Pond Chemolite Plant State Water Pollution Control Board, Effects of Refuse Dumps On Ground Water Quality 1 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00480715 3M_MN01427584 3MA01373218 STATE_07524645 3M_MN03109500 3MA02497530 STATE_07524631 N/A N/A 3MA01933815 3M_MN00000135 3MA00335929 3M_MN00052163 N/A 3MA00456329 N/A Plaintiff's Ex. No. 1033 1035 1042 1043 1044 1046 1052 1053 1054 1058 1062 1064 1065 1068 1070 1079 1083 Date 4/1/1962 5/15/1962 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M Interoffice Correspondence re: Chemolite Waste Disposal Program 3M Report No. 61-22, Supplement Pond Sealant Study 6/15/1963 7/10/1963 7/26/1963 12/2/1963 8/16/1966 9/21/1966 10/6/1966 12/2/1966 3/3/1967 Technical Information 3M Brand Fluorochemical Surfactants FC95, FC-98, FC-128, FC-134, FX-161, FC-170, FX-172 Memorandum from M. C. Goldsmith and K. H. Knoblock to J. A. Brown re: the Woodbury Township Dump Site 3M Interoffice Correspondence from K.R. Knoblock to J.A. Brown re: Woodbury Township Dump Site Present Operations (Woodbury Site) Email from J. T. Lins to D. R. Guthrie re: Proceed to Construct Phase II - Waste Water Treatment Facilities Chemolite Project No. 66-1354 AFE No. 8197 Report to Minnesota Mining and Manufacturing Company Acute Oral Toxicity Studies on Two Materials Results of Residential Well Water Sampling Village of Cottage Grove and Woodbury Township 3M Chronological History St. Paul - Chemolite - Hutchinson Wet Scrap Disposal 3M Interoffice Correspondence from C.E. Kiester to W.W. Watson re: Wet and Dry Scrap Disposal at 3M Plants 6/26/1967 Letter from Dr. Ling to J. Leirfallom re: Application for Permit to Appropriate Water, 3M Property Woodbury Village, Minnesota 11/30/1967 1/11/1968 2/12/1968 7/22/1969 6/15/1970 3M Interoffice Correspondence from C.E. Kiester re: Open Field Burning West Scrap Accumulation Woodbury Meeting Minutes Woodbury Questions by J. Ling and C. Kiester Quarterly Meeting - Board of Directors (3M) Supplementary Engineering Report of Sludge Disposal at Chemolite prepared by R.A. Paschke (Environmental and Civil Engineering) 3M Letter to the Editor of Fire Journal re: Lightwater 2 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00456330 3M_MN00000380 3MA01201629 3MA00335832 3MA00335828 3MA00335802 3MA00456431 3MA01789595 3MA00512637 3MA00512611 3MA00337724 3MA00286355 3MA02603657 3M_MN00050139 3M_MN05374003 3MA00456474 3M_MN02267863 Plaintiff's Ex. No. 1085 1087 1088 1095 1098 1105 1106 1107 1109 1110 1116 1118 1119 1121 1123 1124 Date 10/23/1970 8/31/1971 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Authority for Expenditure for Sludge Dewatering at the Chemolite Sludge Dewatering Facility 3M Interoffice Correspondence from J.T. Ling to H.G. Bryce re: Ecological Aspects of Fluorocarbons 9/13/1971 9/1/1972 4/26/1973 4/24/1974 4/24/1974 3M Interoffice Correspondence from H.G. Bryce to R.M. Adams re: Ecological Aspects of Fluorocarbons - your memo 7/14/71 Bioassay Report: Acute toxicity of Light Water to bluegill (Lepomis marcochirus) 3M Interoffice Correspondence from C.E. Kiester to J.T. Ling re: Woodbury Disposal Site 3M Interoffice Correspondence from L.F. Krank to D.W. Johnson, H.J. Van Noordwyk, and R.E. Edwares re: [Washington County] Landfill Dry Scrap Project Landfill Dry Scrap List. Day 1 4/25/1974 7/8/1974 Log of 3M trucks dumping waste at Washington County Landfill Memorandum and attachment from D. Siddoway, R. Rosen, and B. Fong to various recipients: Report on Disposal of Hydrofluoric Acid 9/17/1974 2/24/1975 3M Permit for Construction and Operation of Disposal System Disposal of Existing Stockpile of HF Tars 8/20/1975 8/29/1975 10/16/1975 G.H. Crawford to L.C. Krogh et al., Record of a Telephone Conversation With William Guy Of The University Of Florida re: Fluorocarbon In Blood Samples From Texas And New York Acute Toxicity to Fish (Bluegill) Cover Letter from Warren S. Guy to R. A. Mitsch and attached manuscript 11/6/1975 12/5/1975 Central Analytical Laboratory, Fluorine-19 NMR of ten samples 1975 Field Letter re: Meeting with DuPont Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00456507 3M_MN03423905 3M_MN03423907 3M_MN01998404 3MA00336067 3MA00276827 3MA00276829 3MA00276832 3MA01201774 3MA00456576 3MA00214086 3MA10034962 3M_MN01658211 3MA00257421 3MA00967400 3MA10024380 3 Plaintiff's Ex. No. 1131 1132 1133 1135 1137 1138 1139 1140 1142 1143 1144 1145 1146 1148 1152 1153 1158 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 8/26/1976 9/16/1976 9/20/1976 11/18/1976 5/4/1977 5/17/1977 6/9/1977 7/1/1977 8/9/1977 8/10/1977 8/26/1977 10/19/1977 11/3/1977 11/30/1977 3M Interoffice Correspondence from Belisle to Freier re: Determination and Characterization of Trace Fluorochemicals Acute Oral Toxicity - Rats T-1585 from Bioresearch to 3M 3M Interoffice Correspondence from Belisle to Long re: Analytical Request A62781 3M Interoffice Correspondence from T.E. Shannon to D.D. Dworak re: Chemolite HF Tar Disposal -- Final Report Technical Report Summary, Analysis of Fluorochemicals from Belisle and D.F. Hagen to B.W. Nippoldt Technical Report Summary: Bioconcentration of FM 3422 in Bluegill Sunfish and in Channel Catfish Report to 3M Company, 28-day Oral Toxicity Study with FC-143 in Albino Mice 3M Interoffice Correspondence from R. C. Johnson to R. L. Ahlness re: Summary Of Work At Chemolite 3M Interoffice Correspondence from Belisle to Freier et al. re: Fluorochemicals in Blood Acute Toxicity to Aquatic Invertebrates (Daphnia Magna) 3M Chronology - Fluorochemicals in Blood 3M Interoffice Correspondence from L. C. Krogh to J.D. La Zerte, 3M, re: Presentation to Corporate Responsibility Committee on Progress - Fluorochemicals in Blood 3M Interoffice Correspondence from Belisle to Freier et al. re: Fluorochemicals in Blood Technical Report Summary re: 1977 Summary 00/00/1978 1/9/1978 2/27/1978 Noordwyk, Hugh et al., Minnesota Mining and Manufacturing Company's Hazardous Waste Program (1978) Technical Report Summary, Fate of Fluorochemicals in the Environment, Biodegradation Studies of Fluorocarbons - II, from E.A. Reiner to D.L. Bacon Technical Report Summary re: Adsorption of FC 95 and FC 143 on Soil 4 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00967404 3M_MN01688827 3MA00967406 3MA01201767 3MA01107188 3M_MN01640103 3M_MN01690370 3MA10035104 3MA10067223 3M_MN01658221 3MA10035028 3M_MN00000479 3MA00967424 3MA00016495 N/A 3M_MN03424083 3MA10036129 Plaintiff's Ex. No. 1162 1164 1165 1166 1168 1170 1171 1172 1173 1174 1175 1176 1177 1178 1179 1180 Date 3/22/1978 4/1/1978 4/1/1978 4/6/1978 4/12/1978 5/5/1978 5/8/1978 5/10/1978 5/16/1978 5/17/1978 5/31/1978 6/1/1978 6/8/1978 6/20/1978 7/19/1978 8/1/1978 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M Interoffice Correspondence from H. J. Van Noordwyk re: Incinerator Ash and Wastewater Treatment Sludge Disposal Meeting Minutes 3M Light Water Ad Brochure 3M Light Water Ad Brochure 3M Interoffice Correspondence from Belisle to Long re: FM3422 Rat Toxicity study Request A67820 3M Interoffice Correspondence from Prokop re: Meeting Minutes - Fluorochemicals Technical Review Committee Acute Oral Toxicity (LD50) Study in Rats FC-143 3M Interoffice Correspondence from J. M. Osborne re: Chemolite Landfill Meeting Minutes and Status Report; File: Chemolite Sludge Disposal 3M Interoffice Correspondence from Prokop re: Results of Animal Studies at I.R.D.C. Central Analytical Laboratory Report No. 6919 re: FC-143 Analysis of IRDC 137-090 Samples 3M Interoffice Correspondence from Prokop re: Meeting Minutes - Review of Animal Studies International Research and Development Corporation, Fluorad Fluorochemical Surfactant FC-95 Chronic Toxicity to Fish (PFOA, FC-116, FC-169, or FC-143) 3M Interoffice Correspondence from Prokop re: Meeting Minutes from May 22, 1978 Meeting to Review Recent Information on Fluorochemicals in Blood of Workers and to Determine Whether this Poses a Substantial Risk Under TSCA Memorandum re: Blood Levels of RF/F in Selected Employees 3M Technical Report Summary, Biodegradation Studies of Fluorocarbons - III by Reiner to Bacon Central Analytical Laboratory Report No. 6962 re: FC in Blood by Belisle 5 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00282200 3M_MN01048940 3M_MN05340691 3MA10035579 3MA10067042 3M_MN01688767 3MA00281139 3MA10066961 3M_MN02343997 3M_MN00053074 3MA00404300 3M_MN01655650 3MA02607386 3M_MN01692291 3MA10054929 3MA00967481 Plaintiff's Ex. No. 1181 1184 1185 1191 1192 1193 1195 1196 1198 1199 1200 1204 1205 1208 1210 1211 Date 8/4/1978 8/16/1978 8/16/1978 12/18/1978 12/19/1978 1/2/1979 2/6/1979 2/14/1979 3/15/1979 3/20/1979 3/23/1979 4/26/1979 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Central Analytical Laboratory Report No. 6967 re: IRDC 137092: FC-95/Monkey Interim Site for Disposal of 3M Chemolite Wastes Technical Report Summary, Evaluation of the Bioconcentration Potential of FN 3422 by Welter Ninety-Day Subacute Rhesus Monkey Toxicity Study on Fluorad Fluorochemical Surfactant FC-95 Letter from R. Susag to Charles Swanson re: 3M's process in obtaining permits and authorizations to operate landfill on Chemolite property Aborted FC95 Monkey Study 3M Internal Correspondence from Belisle to Ubel re: Fluoride Analysis of China Serum (A71011) 3M Interoffice Correspondence from J.M. Osborne to D.E. Pederson re: Sources of Cadmium, Chromium, and Lead Technical Report Summary, Final Comprehensive Report: FC 95 by Welter FC-95, FC-143 and FM-3422 - 90 Day Subacute Toxicity Studies Conducted at IRDC - Review of Final Reports and Summary Technical Report Summary, Final Comprehensive Report: FC 143 by Welter 3M Interoffice Correspondence from Prokop re: Meeting Minutes - Meeting with H.C. Hodges 5/3/1979 5/22/1979 6/7/1979 6/25/1979 An Acute Inhalation Toxicity Study of T-2305 CoC in the Rat Technical Report Summary, Bioaccumulation of Fluorochemicals in Tenn. River Fish by Gagnon 3M Interoffice Correspondence re: Meeting Minutes - Meeting with H.C. Hodge 3M Letter from M. Santoro (3M) to J. Harthum (MPCA) re: request for information pertaining to disposal of materials at Oakdale dumpsite Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN02343995 3MA00456675 3MA10066619 3MA10065004 3MA00280909 3M_MN01663513 3MA00967517 3MA00280139 3MA00176880 3MA00593073 3MA01410327 3MA00967775 3M_MN01688759 3MA01409559 3MA00592803 3M_MN00000353 6 Plaintiff's Ex. No. 1212 1213 1215 1216 1217 1220 1229 1231 1232 1233 1234 1235 1239 1242 1244 1246 1247 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 7/6/1979 7/23/1979 8/1/1979 8/1/1979 8/1/1979 8/27/1979 2/1/1980 3/12/1980 3M Riker Laboratories Interoffice Correspondence from M. T. Case to R. A. Nelson re: Fluorochemical Chronic Toxicity DuPont Memorandum from Kusick to French re: Discussion of Fluorochemicals with 3M Acute Toxicity to Aquatic Invertebrates (Grass Shrimp) from PFOS Acute Toxicity to Fish (Mummichog) from PFOS Acute Toxicity to Aquatic Invertebrates (Eastern Oyster) from PFOS 3M Internal Correspondence from R. A. Prokop to Sam Boyd et al. re: Meeting Minutes Jack Mandel & Leonard Schuman, An Epidemiologic Mortality Study of Employees at the Chemolite Plant Oral Rangefinder Study of T-2998CoC in Pregnant Rats 6/5/1980 6/23/1980 7/10/1980 7/28/1980 8/15/1980 10/28/1980 11/25/1980 12/8/1980 12/18/1980 Letter from Michael B. Ayers (MPCA) to Russell H. Susag (3M) re: requesting 3M submit a detailed breakdown of what specific 3M wastes were or were likely disposed at the Oakdale dumpsite Technical Report Summary, Detection of Fluorochemicals in Decatur Wastewater by Mandel, Schrandt, and Gagnon 3M Interoffice Correspondence from R.E. Ober to R.A. Prokop re: Rural Chinese Manuscript 3M Letter from Osborne to Paul Smith (Met Council) re: 3M Chemolite wastes formerly landfilled in the interim hazardous waste landfill at Chemolite Some Probable Questions on 3M Fluorochemicals with Suggested Answers MPCA Division of Solid Waste Enforcement Section Status of Investigative Study Relating to an Industrial Waste Dump in Oakdale MCPA Status Report of Oakdale Dump Site Dictation Taken from Russ Susag by Phone re: Points to Describe 3M Involvement with Three Sites in Oakdale Oral Teratology Study of FC-95/PFOS in Rats 7 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00593079 3M_MN00053484 3M_MN01656873 3M_MN01656885 3M_MN01656900 3M_MN00000290 3MA00638775 3M_MN02327266 3MA00284881 3MA01406743 3MA10034975 3MA00456729 3MA00472445 3MA02604700 3MA00610634 3MA01248573 3MA00356530 Plaintiff's Ex. No. 1249 1250 1251 1252 1253 1254 1255 1256 1257 1259 1260 1261 1264 1266 1267 1275 Date 1/23/1981 2/12/1981 2/18/1981 2/24/1981 4/15/1981 4/17/1981 5/12/1981 5/29/1981 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Oral Teratology Study of FM-3422 in Rats MPCA Complaint Report at Cottage Grove 3M-Chemolite Plant re: burial of fluorocarbons Oral Teratology Study of FM-3422 in Rats Oral Rangefinder Study of T-2998Coc in Pregnant Rats Third Draft FC-143 Decatur Standby Press Statement by L. Ludford re: Moving Female Workers Recommendation Regarding Fluorochemical Exposure to Females of Childbearing Potential by Ubel Annual Meeting Board of Directors Minnesota Mining and Manufacturing Company 3M Letter from Susag to Louis Breimhurst (MPCA) re: Ayers written request for information on alleged disposal of wastes at Chemolite plant 6/16/1981 Belisle et al., Characterization of Fluorinated Metabolites by a Gas Chromatographic Helium Microwave Plasma Detector The Biotransformation of 1H, 1H, 2H, 2H Perfluorodecanol to Perfluorooctanoate, Analytical Biochemistry 118, 336-343 9/4/1981 3M Internal Correspondence from J.W. Eberlin to J.R. Krall re: Recovery of Perfluorooctanoic Acid (FC-26) Bottoms (FZ-155) 9/8/1981 10/1/1981 11/18/1981 3M Internal Correspondence from L.F. Ludford to L.C. Krogh re: call with a newspaper reporter in Pennsylvania about AFFF Acute Toxicity to Fish (Fathead Minnow) from PFOS Oral Rangefinder Study of T-314CoC in Pregnant Rabbits 12/14/1981 12/15/1981 8/12/1982 3M Internal Correspondence from Ubel to Griffith et al. re: Phone Conversation from Dr. McKusick - DuPont - 12/14/81 Oral Teratology Study of T-2998CoC in Rats 3M Internal Correspondence from D.E. Roach to P.F. Riehle re: 1981 Chemolite Health Evaluations Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00011419 3MA00456742 3MA00326722 3M_MN01691720 3MA00047947 3MA00257790 3M_MN05371968 3MA00456743 3MA00509473 3MA00082742 3MA00065421 3M_MN01657269 3M_MN01691770 3MA00257805 3MA01508403 3M_MN01692296 8 Plaintiff's Ex. No. 1278 1279 1281 1282 1283 1284 1287 1290 1291 1292 1295 1298 Date 3/15/1983 4/8/1983 5/19/1983 5/20/1983 5/20/1983 5/25/1983 7/13/1983 7/26/1983 8/16/1983 9/1/1983 1/11/1984 4/3/1984 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Letter from Michael Tibbetts (MPCA) Fred Robinette (3M) re: Inspection of the 3M Chemolite Incinerator (SW-9) and Boiler Ash Disposal Site (SW-224) 3M Internal Correspondence from A. Norberg and W. Pearlson re: Minutes of Fluorochemical Study Committee Meeting March 16, 1983 3M Letter from J. Osborne to Michael Tibbetts (MPCA) re: MPCA Letter dated March 15, 1983, concerning the March 3, 1983, MPCA inspection of Chemolite incinerator of the 3M Chemolite Incinerator (SW-9) and the Boiler Ash Disposal Site (SW-224) Fate of Fluorochemicals - Phase II prepared by 3M Environmental Laboratory, E.A. Reiner, Editor Letter from Weston Solutions to J. Pilney (3) re: two Weston reports with attachments Preliminary Evaluation of Soil and Ground-Water Analytical Data and Proposed Work Plan Preliminary Evaluation of "New" Drum Site Chemolite Plant 3M Internal Correspondence from R. L. Bohon to J.D. Lazerte re: Fate of Fluorochemicals Phase II Questions and Answers on the Need for the Fate of Fluorochemicals Phase II Study Administrative Order by Consent and Response Order by Consent signed by Robert Adams (3M) Minutes of Meeting Fate of Fluorochemicals August 16, 1983 8:00 A.M. by W.H. Pearlson Technical Report Summary, Environmental Aspects of POSF by Reiner Letter from Larry Christensen (MPCA) to Joseph Ling (3M) re: Notice of Violation, U.S. EPA and MPCA Hazardous Waste Violations Letter from L. Christensen (MPCA) to J. Ling re: Notice of Violation, U.S. EPA and MPCA Hazardous Waste Violations at the 3M Chemolite Facility, Cottage Grove MND006172969 9 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00296066 3MA10067173 3MA00296063 3MA10052935 WE10268751 3MA10065596 3M_MN00000204 3MA00283975 3MA10063227 3MA00193738 3MA00282920 3MA00282913 Plaintiff's Ex. No. 1304 1305 1306 1309 1312 1313 1315 1318 1322 1328 1329 1334 1337 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 6/27/1984 7/9/1984 7/13/1984 7/17/1984 3M Internal Correspondence from J.E. Gagnon to D.M. Schnobrich re: Oakdale Incinerator Ash Oil & Grease Extracts Biodegradation (OECD 301E) of PFOS 3M Internal Correspondence from L.H. Hoffmeier to R.C. Libey et al. re: Treatment of Fluorinated Wastes at Chem. Ctr. Incinerator 3M Internal Correspondence from Santoro to Hoffmeier re: Chemolite Boiler Ash Landfill 8/31/1984 8/31/1984 Data Summary Report on the Tests for Acute & Chronic Toxicity of Fluorochemicals (FC-143) to Daphnia Magna (Water Flea) 3M Internal Correspondence from D. Roach to P. Riehle re: Organic Fluorine Levels 10/4/1984 1/3/1985 5/30/1985 11/00/1985 Remedial Actions to Alleviate Groundwater Pollution from a Former Industrial Waste Disposal Site Presentation by Paschke, Santoro, and Allan Gebhard (Barr), for the 57th Annual Conference of the Water Pollution Control Federation Report on Land Acquisitions for 3M Woodbury Site by Bruce Liesch Response Order by Consent for Chemolite Site, Cottage Grove, Minnesota signed by Robert Adams (3M) 3M Fluorad Fluorochemical Surfactants Product Information Brochure 11/15/1985 10/2/1986 8/29/1987 Letter from T. Kalitowski (MPCA) to M. Forsythe (Honorable Chair of House Appropriations Committee) with MPCA Report on the Use of the Environmental Response, Compensation and Compliance Fund During Fiscal Year 1985 Industrial Chemicals Products Division Fluorad Brand Fluorochemical Surfactant FC-143 Two Year Oral (Diet) Toxicity/Carcinogenicity Study of Fluorochemical FC-143 in Rats, Volume 1 of 4 10 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00300324 3M_MN01657233 3MA00067382 3MA00456910 3M_MN01639470 3M_MN03269963 3MA00296731 3M_MN00000222 3MA00840027 STATE_07543929 N/A 3M_MN01059198 3MA00027126 Plaintiff's Ex. No. 1338 1342 1343 1345 1346 1348 1349 1351 1353 1356 1357 1358 1359 1360 1362 1365 Date 9/00/1987 12/9/1987 1/5/1988 4/6/1988 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M Fluorad Fluorochemical Surfactant FC-143 Product Information Brochure 3M Phone Conversation Report of Robert Gail with Roger Perkins re: Review of FC-143 final report: Leydig cell tumor incidence 3M Internal Correspondence from R. Perkins to F. Griffith re: Summary of the Review of the FC-143 Two-Year Feeding Study Report to be presented at the January 7, 1988 meeting with DuPont Two Year Oral (Diet) Toxicity / Carcinogenicity Study of Fluorochemical FM-3924 in Rats, Volume 1 of 5 6/3/1988 8/11/1988 12/28/1988 12/30/1988 00/00/1989 2/23/1989 4/6/1989 4/25/1989 9/1/1989 10/5/1989 12/22/1989 00/00/1991 Letter from Boots & Coots to 3M re: Foam Systems Testing 3M Chemolite Hazardous Waste Manifest Part B. RCRA Permit Application for 3M Company, MND006172969, 3M Chemolite Center 3M Internal Correspondence from Eric Reiner re: FC-129 Biodegradability Jack Mandel & Leonard Schuman, Mortality Study at the 3M Chemolite Plant 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant Letter from J. Mandel to L. Zobel (3M) re: results of the comparison of cancer incidence between the Minnesota population and the U.S. with attachment Table 5: Observed and Expected Deaths by Cause, Standardizes Morality Ratio (SMR), 95 Percent Confidence Limits and CHi Square Values, Males, Chemical Division Hunting Elevator Company RFRA 3M Brand Technical Information for AFFF FC-783 Memorandum from R. Perkins to A. Sethre re: Ammonium Perfluorooctanoate TSCA 8(e) Submission 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant A Chemical History of 3M 1933-1990 by MacKay 11 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. STATE_07543929 3MA10014327 3MA00631017 3MA00593233 3M_MN01315290 3M_MPCA00006608 3MA00152550 3MA10035965 3MA00632297 3MA00202500 3MA00632313 N/A 3M_MN02369894 3M_MN02323182 3M_MN01044772 3MA00005401 Plaintiff's Ex. No. 1368 1369 1370 1372 1373 1374 1376 1378 1384 1386 1387 1388 1391 1402 1403 1404 Date 4/1/1991 5/10/1991 00/00/1992 2/5/1992 2/28/1992 6/5/1992 8/28/1992 9/15/1992 12/16/1992 12/30/1992 9/00/1993 1/18/1993 3/6/1993 8/3/1993 9/1/1993 9/1/1993 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Study Summary of Environmental Effects of Light Water Brand AFFF and Components - 1991 3M Internal Correspondence from L. Zobel to G. Damerell et al. re: Chemolite Examinations, Fall, 1990 The Solution to Your Problems 3M Brochure 3M Internal Correspondence from R. Howell to C. Olsen re: Fluorochemicals in the Environment with attachments Letter from D. Hall (MPCA) to R. Bringer (3M) with Authorization to Discharge and to Constrict, Install and Operate a Wastewater Disposal System Product Toxicity Summary Sheet Fluorad Brand Fluorochemical Surfactant FC-95 Letter from J. Wallrath (DuPont Human Resources) to Y. Power (Washington Works Polymers) with Interpretation of Epidemiologic Surveillance Data 3M Internal Correspondence from R. Howell to C. Burton re: Environmental Concerns with Fluorochemicals 3M Internal Correspondence from T. Ashenmacher to R. A. Paschke et al. re: Woodbury Update Report Transmittal of Memorandum from Dale Bacon to Butenhoff re: Fluorochemicals Gilliland FD and Mandel JS. 1993. Mortality among employees of a perfluorooctanoic production plant. Journal of Occupational Medicine 35:950-954. Environmentally Responsive Functional Fluorochemicals by Tony Manzara Report on 3M Corp. Programs in Environmental Toxicology by John P. Giesy 3M Internal Correspondence from R. M. Flynn to C. A. Burton et al. re: ECM Meeting Notes with attachments PFOS as Pesticide Frank Gilliland & Jack Mandel, Mortality Among Employees of a Perlfuorooctanoic Acid Production Plant Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN01657097 3M_MN01692315 STATE_07543929 3M_MN00000001 MN.103.0639.000439 3M_MN02252650 N/A 3MA00323897 3M_MN00039613 3M_MN03108995 N/A 3M_MN02470086 3M_MN04734387 3M_MN02470101 3M_MN02470063 3MA00631764 12 Plaintiff's Ex. No. 1408 1409 1413 1415 1418 1420 1421 1431 1445 Date 11/18/1993 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description PFOS, with sections for Disposition, Toxicity Considerations, Environmental Consideration, Kinds of Studies for Human PFOS Aspect 12/7/1993 3M Internal Correspondence from J. Mandel to Fluorochemical Steering Committee Members re: Papers/Dr. Gilliland with attachment "Peripheral Blood Lymphocyte Count in Men Occupationally Exposed to Perfluoroctanoic Acid" by F. Gilliland 4/3/1994 4/19/1994 5/13/1994 7/18/1994 9/6/1994 3/13/1995 12/14/1995 3M Interoffice Memorandum from K. Goebel to I. Denenholz re: List of questions of several fluorochemical products Fluorine Health/Environmental Concerns; FC Concentrations Factors Affecting These Concerns; Proposed Program Operational Committee Draft Health Hazard Summary of Perfluorooctane Sulfonic Acid, Potassium Salt as Represented by FC-95 Locations and Data From Avian Blood Plama Samples by John P. Giesy Health Hazard Summaries and Proposed Testing Program for Several 3M Fluorochemicals 3M Morality Study of Employees at 3M Plant in Decatur, Alabama Major Vision Obstacle Number 1 1446 1451 Various 5/20/1996 Material Safety Data Sheets. 1984, 1989, 1990, 1995, 1996, 1997, 1998, 2000 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant 13 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA10037365 3M_MN00051484 3M_MN04741126 3M_MN00000367 3MA10064687 3MA01404531 3M_MN02345238 3M_MN01661790 3MA00089191 3MA01543444; 3MA01452579; 3MA00085087; 3MA01622491; 3MA01946892; 3MA10082349; 3MA00087197; 3MA00082405; 3MA00202819; 3M_MPCA00041106 3MA10057753 Plaintiff's Ex. No. 1457 1459 1460 1461 1466 1467 1469 1471 1476 1479 1482 1486 1488 1489 1493 1496 1502 1504 Date 9/17/1996 10/24/1996 10/25/1996 11/12/1996 12/12/1996 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M Internal Correspondence from E. Reiner to M. Shiba re: RCRA Email from E. Reiner re: Draft Fluorochemical Waste Disposal Guidance 3M Internal Correspondence from Eric Reiner to Scott Strand et al. re: More Ideas on Draft Fluorochemical Waste Disposal Guidance Email from Tony Manzara to Wendling et al. re: Visit to DuPont 11/12/96 - Technical Impressions of 3M Fax Message re: carcinogenicity label of FC-143 / 1996 Fax and Minutes of Call with Dr. Jung Email from E. Reiner to Scott Strand, Robert Howell, and James 12/12/1996 Johnson re: Draft Fluorochemical Waste Disposal Guidance 1/10/1997 Various 11/5/1997 00/00/1998 1/16/1998 Acute Oral Toxicity Study of T-6669 in Rats (OECD Guidelines) 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant for February 7 & 19, 1997 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant Draft Memorandum re: Fluorochemicals in Human Blood Email from L. Zobel to J. Butenhoff re: Fluorochemical Projects Underway in the Environmental Laboratory 2/9/1998 2/26/1998 2/28/1998 3/18/1998 3/20/1998 Estimation of "Safe" Reference Level (ppb) for PFOS in Plasma FDA Communications Plan; EPA Communication Plan Toxicology Contribution to White Paper by John Butenhoff POSF/C8 Acid Cell Hour Production Worksheet Memorandum from C. Reich to TSCA 8(e) Committee members re: TSCA Section 8(e) Decision 5/1/1998 Environmentally Relevant Properties of 3M Fluorochemicals 5/8/1998 Screening of PFOS levels in Eagles and Albatross - 3M Environmental Laboratory Fluorine Analytical Chemistry Team 14 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A 3MA10051804 3MA10051796 3M_MN02470157 3M_MN03591099 3MA01410733 3M_MN01688780 STATE_07543958 3MA00203395 3MA10082645 3MA00906295 3MA01366219 3MA10063015 3MA10072182 3M_MN04782935 3MA10064459 3MA10071137 3MA01404534 Plaintiff's Ex. No. 1519 1523 1526 1527 1529 1531 1533 1534 1535 1558 1571 1575 1585 1586 1587 1588 1589 Date 9/1/1998 10/16/1998 11/4/1998 11/9/1998 11/16/1998 11/25/1998 12/3/1998 12/3/1998 12/10/1998 2/5/1999 4/8/1999 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Email from D. Schnobrich to M. Falco et al. re: FC's and Past Disposal Sites Occurrence of Perfluorooctane Sulfonate (PFOS) in Wildlife Part I. Eagles and Albatrosses by Rich Purdy 3M Material Safety Data Sheet: FC-118 Fluorad Fluorochemical Surfactant Board of Directors Presentations November 9, 1998, August, 1998, FC Issues 3M Internal Correspondence from D. Sanders to M. McKerlie re: Attached Pathology Review of Reported Tumorigenesis in a Two Year Study of FM-3924 in Rats Email from R. Purdy to G. Adams re: Risk to the environmental due to the presence of PFOS with attachment Pioneer Food Chain Risk Assessment of PFO Pioneer Risk Assessment of Adverse Effects in Marine Mammals from PFOS in the Food Chain by Rich Purdy Science Publication Strategy The Science of Organic Fluorochemistry Letter from M. Ash to D. Sonstegard re: Purdy return to 3M 4/23/1999 5/20/1999 5/21/1999 5/24/1999 PFOS Environmental Risk: Potential TSCA 8( e ) Substantial risk 3M Internal Correspondence from D. Sanders to D. Bacon et al. re: Meeting Minutes of FC Core Team - May 14, 1999 Laboratory Report: Analysis of FCs in Samples of Children's Sera 3M - FC Issue Communications Plan 5/26/1999 Letter from C. Reich to Office of Pollution Prevention and Toxics of the EPA - TSCA 8(e) Supplemental Notice on: SulfonateBased Fluorochemicals Docket Nos. 8EHQ-1180-373; 8EHQ1180-374; 8EHQ-0381-0394; 8EHQ-0598-373 5/26/1999 Email from D. Graham to T. Baltutis re: F-6002 waste water 15 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN00498519 3MA01404529 3M_MN02892806 3MA10081840 3M_MN02980584 3MA10025147 3MA00242688 3MA10031581 3MA00729193 3MA00523419 3M_MN05336314 3MA01238114 3MA01404555 3MA00659721 3M_MN04732222 3M_MN01329658 3M_MN02465688 Plaintiff's Ex. No. 1595 1599 1612 1615 1616 1617 1618 1630 1633 1645 1653 1657 1664 1665 1667 1668 1669 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 6/16/1999 7/9/1999 8/31/1999 9/30/1999 9/30/1999 10/1/1999 3M Internal Correspondence from D. Sanders to T. DiPasquale et al. re: FC Issues Core Team Meeting Minutes - June 8, 1999 Email from R. Purdy to J. Walker re: F-chem 3M Internal Correspondence from G. Adams to EHS&R Working Group re: EHS&R Minutes for August 10, 1999 Products of incomplete combustion of POSF Based Fluorochemicals Email from Sanders to Perry Logan et al. re: Decatur FC Exposure Assessment - Presentation at IH Conference Summary PFOS Oral Rat Toxicology Screen 10/1/1999 11/23/1999 12/15/1999 2/2/2000 3/1/2000 3/16/2000 4/10/2000 4/11/2000 4/20/2000 4/21/2000 4/21/2000 Email from G. Olsen to P. Logan re: Presentation of FC Papers Email D. Mandel on behalf of Dave Sanders to J. Butenhoff et al. re: Scientific Publication Strategy attaching Scientific Publication Strategy, Proposals Draft Information for all Dyneon Employees 3M Waste Stream Profile Program Cover Sheet (w3580) for Cottage Grove Sulfonated Perfluorochemicals in the Environment: Sources, Dispersion, Fate and Effects report Identification of Fluorochemicals in Sera of Children in the United States Charlie Auer Telephone Call Handwritten Email from C. Auer to D. Hakes re: Follow-up on Perfluorochemicals Request Letter from L. Zobel to O . Hernandez re: Writing to Clarify Information contained in the two-generation reproduction Attachments to April 21, 2000 letter to C. Auer from W. Weppner | (Radiolabel Oral Absorption and Intravenous Pharmacokinetics Studies in Rats) Attachments to April 21, 2000 letter to C. Auer from W. Weppner | (Dermal Absorption and Intravenous Pharmacokinetics in Rabbits) 16 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA10082287 3MA00245904 3MA00927118 3MA01412209 3MA01540632 3M_MN02336490 3MA00004617 3MA00467427 3M_MN01524232 3M_MPCA00033120 3MA00045043 3M_MN01661880 3MA00470824 3M_MN02457016 3MA00517725 3MA00251390 3MA00251391 Plaintiff's Ex. No. 1670 1671 1674 1679 1681 1682 1683 1684 1685 1690 1691 1694 1698 1703 1704 1707 1716 1717 1718 1719 1720 Date 4/21/2000 4/21/2000 4/27/2000 5/3/2000 5/4/2000 5/5/2000 5/8/2000 5/9/2000 5/9/2000 5/16/2000 5/16/2000 5/16/2000 5/16/2000 5/19/2000 5/19/2000 6/5/2000 6/26/2000 6/27/2000 6/27/2000 6/28/2000 6/28/2000 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Attachments to April 21, 2000 letter to C. Auer from W. Weppner | (Teratology Studies in Rats and Rabbits) Attachments to April 21, 2000 Letter to C. Auer from W. Weppner (Medical Surveillance and Epidemiology) Letter from R. Sussman (Latham & Watkins) to C. Auer re: Meeting with 3M April 28, 2000 Letter from J. Butenhoff to J. Seed (EPA) re: Serum Measurements for Argus Studies 418-013 (through Lactation) and 418-015 (during Gestation) Letter from W. Weppner to C. Auer re: Information on Perfluorooctane Sulfonate with several attachments Email from C. Auer to D. Hakes et al. re: Follow-up on Perfluorochemicals Meeting on April 28 Handwritten notes 3M Fluorochemical EHS & R Initiative Chuck Kiester's Board of Directors Presentation Annual Meeting Board of Directors Minnesota Mining and Manufacturing Company 3M Phasing out Some of Its Specialty Materials Email from C. Auer to B. Weppner re: Phase-out of PFOS Press Release 3M Phasing out Some of Its Specialty Materials with handwritten notes 3M SEC Form 8-K EPA Says it Pressured 3M over Scotchgard Chemical Email from T. Sloan to T. Brooks et al. re: The New York Times Article Today about the EPA's Version of Why We Abandoned Our FC's... BusinessWeek, 3M's Big Cleanup Summary of Work Performed for the German Government Agency for Military Technology and Procurement on Fire Extinguishing Foam Compounds from Multiple Companies Acute Toxicity to Fish (Bluegill Sunfish) Acute Toxicity to Aquatic Invertebrates (Daphnia Magna). Acute Toxicity to Invertebrates (Grass Shrimp) Acute Toxicity to Aquatic Invertebrates (Eastern Oyster) 17 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00251392 3MA00251393 3M_MN02457023 3MA00254228 MN.039.0016.000280 3MA01135534 3MA00469749 3M_MN05367080 3M_MN05367814 3M_MN02345284 3M_MN02457072 3MA01169714 N/A 3M_MN03112642 3MA01190648 3M_MN02492758 3M_MN01657796 3M_MN00436402 3M_MN01656831 3M_MN00437323 3M_MN00437343 Plaintiff's Ex. No. 1721 1725 1726 1728 1731 1734 1735 1736 1737 1740 1749 1758 1762 1763 Date 6/30/2000 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description DuPont Haskell Laboratory Visit Meeting Minutes 7/11/2000 Oral Developmental Toxicity (Teratology) in Rats and Rabbits 7/11/2000 7/12/2000 7/25/2000 Serum Fluorochemical trends of out-of-county residents in CLUE I (1974) and CLUE II (1989) epidemiologic investigations Email from D. Graham to S. Kruse et al. re: Draining C8 Acid to Sewer Email from M. Elnabarawy to M. Santoro re: Screening-Level Risk Assessment for Organofluorine Substances in Philippines Well Water 8/21/2000 Letter from K. Reed to J. Baskerville re: 3M Company TSCA Section 8(e) Compliance Audit - Disclosure of Phase One Findings Pursuant to "Incentives For Self-Policing, Discovery, Disclosure and Correction and Prevention of Violations," 65 Fed. Reg. 19618 (Apr.11, 2000) 8/21/2000 Current CG FC Waste Status (221272 lbs./yr. as of 8/21/00) 8/21/2000 8/21/2000 9/9/2000 12/26/2000 2/20/2001 3/1/2001 3/2/2001 Letter from K. Reed to J. Baskerville with attachment re: 3M Company TSCA Section 8(e) Compliance Audit - Disclosure of Phase One Findings Pursuant to "Incentives For Self-Policing, Discovery, Disclosure and Correction and Prevention of Violations," 65 Fed. Reg. 19618 (Apr. 11, 2000) Letter from K. Reed to Document Processing Center (7407) re: TSCA Section 8(e) Supplemental Submissions: Docket Nos. 8EHQ-1180-373 and 8EHQ-1180-374 Email from J. Giesy to D. Bacon re: manuscript [Excerpt] Email from D. Bacon to K. Reed re: Stuff with attachment 3M SEC 10-K for the year ended December 31, 2000 3M Internal Correspondence J. Butenhoff to M. Santoro re: Draft Drinking Water Health Advisory (DWHA) - PFOS Letter from Cunningham (Toxicological Sciences) to J. Butenhoff (3M) re: ToxSci 01-002 18 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00469911 3M_MN01660801 3M_MN01661883 3MA01623209 3M_MN01020427 3M_MN01257572 3MA00043765 3MA01220040 3MA01220047 3MA00198538 3MA00186126 N/A 3MA00812416 3M_MN02337242 Plaintiff's Ex. No. 1764 1780 1781 1782 1783 1784 1785 1787 1793 1798 1799 1806 1812 1814 Date 3/7/2001 5/30/2001 6/1/2001 6/1/2001 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Email from M. Santoro to F. Palensky et al. re: Cottage Grove Wells Email from Millet to Gregory et al. re: U.S. News and World Report Magazine Reporter Email from Millet to Renner re: Draft Phase Out Schedule for Reporter Draft - Phase Out Timeline 6/1/2001 6/13/2001 6/19/2001 7/3/2001 9/5/2001 10/9/2001 TSCA Section 8(e) Committee Meeting - Record of Proceedings Letter from K. Reed (3M) to A. Pontius (EPA) re: 3M Company TSCA Section 8(e) Compliance Audit -- Disclosure of Phase Two Findings Centre Analytical Laboratories, Analytical Report: Fluorochemical Characterization of Water Samples - Cottage Grove Potable Water Evaluation (E01-0812) Email from M. Santoro to Palensky et al. re: Cottage Grove Wells Draft FC Communications Plan 2001-2002 Letter from Clark (EPA) to Hatcher (3M) 10/11/2001 11/9/2001 12/18/2001 1/1/2002 Olsen GW, Burlew MM, Burris JM, and Mandel JH. 2001. Final report: Epidemiology, 220-3W-05: A longitudinal analysis of serum perfluorooctanesulfonate (PFOS) and perfluorooctanoate (PFOA) levels in relation to lipid and hepatic clinical chemistry test results from male employee participants of the 1994/95, 1997, and 2000 fluorochemical medical surveillance program. Email from D. Schnobrich to L. Zabel et al. re: Cordova FC Waste Management Review Thomford, Peter, Final Report: 26-Week Capsule Toxicity Study with Ammonium Perfluorooctanoate (APFO) in Cynomolgus Monkeys Report (Covance 6329-231) Protocol Amendment: Cancer Incidence in 3M Workers Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN00000806 3M_MN05342352 3M_MN05342355 3M_MN05367921 3MA02608788 3MA01246311 3MA00853349 3MA00001371 3MA02512798 3MA00383888 3M_MN02482163 3MA00000982 3M_MN02343342 3M_MN02291548 19 Plaintiff's Ex. No. 1818 1822 1823 1824 1831 1833 1836 1845 1848 1855 1864 1872 1881 1883 1887 1889 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 1/11/2002 2/1/2002 2/5/2002 2/18/2002 3/6/2002 3/8/2002 3/11/2002 8/6/2002 9/4/2002 10/17/2002 11/15/2002 1/1/2003 2/10/2003 2/13/2003 3/10/2003 4/7/2003 Thomford, Peter, Final Report: 26-Week Capsule Toxicity Study with Perfluorooctane Sulfonic Acid Potassium Salts (PFOS; T6295) in Cynomolgus Monkeys Report (Covance 6329-223) 3M Cottage Grove Megaphone February 2002: Volume 54, Number 2 U.S. Environmental Protection Agency Application for Permit to Discharge Wastewater Existing Manufacturing, Commercial, Mining and Silvicultural Operations Form 2C NPDES, MND006172969; signed 3M Draft Talking Points Cottage Grove Wells Email from D. Kriens to D. Douglas & M. Rys re: 3M-PFOS and related compounds in discharge Email from D. Schnobrich to S. Ethier et al. re: PFOS/PFOA at Cottage Grove 3M SEC 10-K for the year ended December 31, 2001 Office Memorandum from D. Wetzstein to R. Messing and L. Gust (MDH) re: Request for Development of Industrial Soil HBV for PFOS & PFOA Compounds Cancer Benchmark Dose Calculation for Fluorochemical-143 (FC-143): Ammonium Perfluoroctanoate Subsurface Investigation Work Plan Neutralized HF Tar (D1) Disposal Area 3M Cottage Grove Facility Report Draft summary of PFOA exposure Chronology, Off-Site Waste Disposal Locations - 3M Cottage Grove, Minnesota Memorandum from D. Comeau and P. Book (ERG) to D. Douglas and M. Rhys (MPCA) re: 3M Cottage Grove; Area D1 Initial Groundwater Sampling Results Memorandum from D. Comeau and P. Book (ERG) to D. Douglas and M. Rys (MPCA) re: 3M Cottage Grove; Area D1 Initial Groundwater Sampling Results 3M SEC 10-K for the year ended December 31, 2002 Email from J. Giesy to D. Bacon and W. Reagen re: Paper 20 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN03278834 3MA00064713 3MA00110772 3MA00469948 STATE_02795011 3MA01376827 N/A STATE_02338983 3M_MN02339249 3MA00048084 3M_MN01526194 3MA01243198 3MA00046947 3M_MN01010361 N/A 3MA00194174 Plaintiff's Ex. No. 1897 1898 1907 1908 1910 1912 1918 1920 1925 1926 1927 1928 1930 1932 1933 1937 1938 1939 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 5/7/2003 5/7/2003 8/1/2003 8/5/2003 8/7/2003 9/15/2003 10/27/2003 11/13/2003 12/22/2003 12/22/2003 12/22/2003 12/22/2003 Email from M. Gravdahl to D. Schnobrich re: PFOA Production Letter from M. Santoro (3M) to W. Penberthy (EPA) re: Followup Questions Regarding 3M and Dyneon LOI Environmental Monitoring Commitments Letter from M. Santoro (3M) to U.S. EPA re: Submission of Monitoring Data Pursuant to the 3M LOI Dated March 13, 2003 and APFO Users LOI Dated March 14, 2003 Email from D. Douglas to B. Brott et al. re: EPA Risk Assessment for PFOS/PFOA Draft Talking Points Cottage Grove Wells Email from D. Douglas (MPCA) to J. Kelly (MDH) et al. re: Monitoring of PFOA/PFOS Email from T. Fasking (3M) to R. Mark (MPCA) et al. re: PFOA production in Cottage Grove Letter from D. Douglas (MPCA) to T. Fasking (3M) re: 3M Chemolite Superfund Site Letter from V. Yingling (MDH) to L. Bauer and N. Bauer Letter from V. Yingling (MDH) to D. Eilers Letter from V. Yingling (MDH) to D. Hendrickson Letter from V. Yingling (MDH) to J. Tschida and P. Tschida 1/2/2004 Email from D. Douglas (MPCA) to B. Brott (MPCA) et al. re: Preliminary results for PFOA at Washington County Landfill 1/26/2004 1/27/2004 2/12/2004 2/13/2004 2/25/2004 Letter from R. Paschke (3M) to D. Douglas (MPCA) re: Consent Order Addendum and Facility-wide Fluorochemical Investigation Work Plan, 3M Cottage Grove Site Facility-Wide Flourochemical Investigation Work Plan 3M Cottage Grove Toxicity Test Final Report Event 1, E04-0120 Email from D. Douglas (MPCA) to B. Brott (MPCA) et al. re: 3M Cottage Grove Toxicity Test Final Report Event 2, E04-0126 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00044477 3MA00888342 3MA00048383 STATE_02468135 3MA02600510 STATE_02468963 3MA00406699 MN.303.0085.000274 STATE_01524662 STATE_01524663 STATE_01524664 STATE_01524665 STATE_02496240 3M_MN00044012 3MA00046844 3M_MN01538387 3M_MN00044031 3M_MN01539152 21 Plaintiff's Ex. No. 1940 1941 1942 1946 1948 1949 1955 1957 1958 1959 1964 1966 1969 1972 1976 1979 1984 1985 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 6/20/2001 New environmental toxin destroys the liver - translated article 3/12/2004 Email from P. Book to T. Fasking and D. Comeau re: Cgrove list 4/1/2004 4/26/2004 6/21/2004 6/29/2004 7/20/2004 7/23/2004 7/26/2004 7/29/2004 9/14/2004 9/27/2004 10/12/2004 10/15/2004 11/8/2004 11/21/2004 12/1/2004 12/8/2004 Exygen Research, Fluorochemical Characterization of Aqueous Samples Woodbury Combined Main FC Monitoring (E04-0241) Letter from B. Brott (MPCA) to T. Fasking (3M) re: Reimbursement of Minnesota Pollution Control Agency Costs for the 3M Chemolite State Superfund Site MDH Environmental Laboratory, MPCA Closed Lanfill Assessment Meeting Between KEMI and 3M: Human Risk Characterization for PFOS MDH Chain of Custody Form Email from D. Douglas (MPCA) to D. Kriens (MPCA) re: 3M Cottage Grove/Call from Bob Paschke Letter from T. Fasking (3M) to M. Rys (MPCA) re: Oakdale Disposal Site Email from R. Paschke to M. Santoro et al. re: Phone conversation with Dave Douglas, MPCA FC Core Team 2004 - 2005 Project / Process Priorities Email from J. Butenhoff to M. Falco re: Notes on Proposal to NTP Email from M. Falco (3M) to L. Wendling (3M) et al. MPCA and 3M meeting re: Perfluorochemicals Email from L. Zobel to J. Butenhoff re: Files Associated with Stockholm University Bruce Alexander, Final Report: Bladder Cancer in Perfluorooctanesulfonyl Fluoride Manufacturing Workers Letter from T. Fasking to M. Rys re: Oakdale Pump-out System Discharge Fluorochemical Sampling Email from I. Verhagen to S. Ruotsinoja re: Interview with MPR PFOA timeline at Washington County Landfill Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00452308 3MA00048348 3M_MN00719367 3M_MN00721525 STATE_02091948 3M_MN02317718 MN.303.0003.000060 STATE_02803858 3MA00348164 3MA00886748 3M_MN00838661 3MA00955624 3MA01554012 STATE_02328450 3MA00408335 3MA00755705 3MA01932893 STATE_01200544 22 Plaintiff's Ex. No. 1986 1988 1989 1993 1994 1995 2004 2009 2012 2017 2033 2035 2040 2041 2044 2045 2046 2049 2057 Date 12/10/2004 00/00/2005 00/00/2005 1/24/2005 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Letter from M. Rys to R. Paschke, 3M, re: Oakdale Pump-out System Discharge Fluorochemical Sampling Letter Dated December 1, 2004, Oakdale Disposal Site (the Site) 3M Talking Points - Oakdale Wells 3M's FC Committees Chart MDH. Questions About the Oakdale Public Water Supply 1/24/2005 1/25/2005 2/1/2005 2/18/2005 2/23/2005 3/9/2005 5/26/2005 6/8/2005 6/30/2005 7/1/2005 8/2/2005 Pictures of Scotchgard from Minnesota Public Radio website, http://news.minnesota.publicradio.org/features/2005/01/25_bens onl_oakdale/ Plastics Europe - Q&A On PFOA Edgerly, Mike et al., Toxic Traces, Minnesota Public Radio (2005) Health Consultation 3M Chemolite Perfluorochemical Releases at the 3M - Cottage Grove Facility Email from S. Ethier to R. Paschke et al. re: Fw: MPR Comment from Website SKB Environmental, SKB Rosemount Industrial Waste Facility (2005) 3M FC Manufacturing Update Weston Off-Site Waste Disposal Locations Table - 3M Cottage Grove, Minnesota MPCA PFC Investigation June 30, 2005 Letter from J. Hatcher to D. Ziegel re: Additional Data and Revised Draft Consent Agreement and Final Order Email from M. Gaetz to T. Fasking & T. Galloway re: Fw: Cottage Grove Sludge Sample Results 8/4/2005 8/10/2005 8/26/2005 10/15/2005 Email from M. Geetz to G. Hohenstein re. Cottage Grove Sludge Background Information on PFOS and PFOA 3M Fluorochemicals Chronology and Various Timelines MPCA, Preliminary results of the MPCA PFC Investigation with 2 attachments Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00344317 STATE_02496227 3M_MN00000703 3MA00513900 N/A 3M_MN01525833 3MA01169469 3MA00383006 3MA01242570 WE10336422 3MA01870504 3MA00511276 STATE_01998653 3M_MN00053740 3MA01326865 3MA00866656 3MA00550095 3M_MN04769925 STATE_01998636 23 Plaintiff's Ex. No. 2072 2078 2081 2083 2084 2085 2088 2093 2095 2096 2097 2099 2102 2119 2125 2127 2130 2132 2133 Date 1/7/2006 2/1/2006 2/12/2006 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description S.Beach, S.A., et. al. Ecotoxicological Evaluation of Perfluorooctanesulfonate (PFOS). Reviews of Environmental Contamination and Toxicology (2006) Letter from G. Millet to R. Cheng re: Response to email dated January 23, 2006 Email from J. Giesy to D. Bacon re: ES&T Paper 2/16/2006 2/17/2006 2/21/2006 3/7/2006 3/28/2006 4/1/2006 4/24/2006 4/26/2006 5/25/2006 6/14/2006 10/27/2006 FC Communications Michael Santoro 3M Regulatory Affairs Memorandum from J. Giesy to D. Bacon re: Follow up to February 2, 2006 meeting (revised memo) Email from J. Giesy to D. Bacon re: re: chironomid study DRAFT Key Points - Cottage Grove Fish Data MDH, News Release, Revised fish consumption advice issued for bluegill sunfish in Pool 2 of the Mississippi River Fluorochemical (FC) Data Assessment Report by Weston Settlement agreement between 3M and the U.S. Environmental Protection Agency. Email from S. Sanchez to F. Palensky et al. re: News Coverage TSCA Email from T. DiPasquale to T. Boardman et al. re: 3M and EPA Press Release Cost-benefit analysis of repeating the chronic study of the potential effects of PFOS on reproduction in quail Estimation of "Safe" Reference Level of PFOS in Plasma 12/11/2006 1/31/2007 2/11/2007 2/26/2007 2/26/2007 Email from J. Giesy to W. Reagen & D. Bacon re: Confidential Email from J. Kelly to D. Mandy, et al. re: Testing of consumer GAC filters with attachment Email from W. Nelson to D. Bacon et al. re: Pioneer Press Sunday Memo from H. Goeden to J. Stine re: Health Based Values for Perfluorooctane Sulfonate (PFOS) Discharge of Perfluorocarbons (PFCs) from 3M Cottage Grove Plant 24 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN02255189 3M_MN01524242 3MA01320043 3M_MN01524902 3MA01320414 3MA01320495 3M_MN04799651 STATE_02082048 3MA01551778 N/A 3MA01538872 3MA01562347 3MA02513752 3M_MN00042206 3MA01461356 STATE_01201422 3MA01645376 STATE_01488041 STATE_01995465 Plaintiff's Ex. No. 2134 2137 2138 2144 2145 2146 2147 2155 2158 2161 2162 2163 2164 2168 2174 2177 Date 2/26/2007 3/7/2007 3/13/2007 4/3/2007 4/4/2007 4/17/2007 4/24/2007 5/8/2007 5/22/2007 5/30/2007 6/1/2007 6/18/2007 7/19/2007 8/22/2007 9/24/2007 10/1/2007 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Memo from H. Goeden to J. Stine re: Health Based Values for Perfluorooctanoic acid (PFOA) Email from W. Nelson to D. Bacon et al. re: Pioneer Press, Star Tribune and Link to MPR story Email from J. Giesy to D. Bacon and W. Reagen re: Fwd: Avian toxicity reference values Email from J. Giesy to W. Reagen re: Fwd: Looking for a postdoc candidate Memorandum from J. Stine to T. Scherkenback re: Hazard Determination of PFOA and PFOS Los Angeles Times, U.S. fires company over apparent conflict MPCA, Presentation, Request for Response Actions, Board Presentation, 3M Perfluorochemical Disposal Sites Letter from S. Stevenson to M. Fortado re: 3M Oakdale Site insurance policy 2007 Settlement Agreement and Consent Order, In the matter of Releases and Discharges of Perfluorochemicals At and From Sites in Washington County, Minnesota, and Certain Related Matters Handwritten notes re: MDH MTG Weston, Remedial Investigation Report, Phase 2 Fluorochemical (FC) Data Assessment Report for the Cottage Grove, MN Site Weston, Remedial Investigation Report Soil Supplemental Fluorochemical Data Assessment - Addendum, Oakdale Site Email from J. Giesy to D. Bacon and W. Reagen re: manuscript FYI Lundin, J. and Alexander, B. Final Report: Mortality of employees of an ammonium perfluorooctanoate production facility Presentation, Dyneon APFO Replacement Program Email from G. Olsen to W. Reagen re: Request for comments with attachment 25 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. STATE_02430434 3MA01645741 3M_MN03014876 3M_MN03016361 STATE_02338891 N/A 3MA01839219 3M_MN01313152 3M_MN00568807 3M_MN02324009 3M_MN01483002 3M_MN04969186 3MA02516746 3MA02557439 3M_MN02372412 3MA02540633 Plaintiff's Ex. No. 2191 2192 2194 2204 2206 2207 2209 2219 2222 2231 2232 2233 2295 2297 2300 2301 Date 1/9/2008 1/10/2008 1/28/2008 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Email from J. Sweeney to S. Bernatchez re: Question following presentation on 3M PFC facts Email from K. Andres to G. Olsen re: CG Draft Report with attachment Email from J. Butenhoff to S. Anprar and K. Taolin re: Review Process with attachment 3/26/2008 3/29/2008 3/31/2008 4/1/2008 6/13/2008 6/30/2008 Email from J. Giesy to W. Reagen et al. re: Entrix Consulting Presentation, J. Butenhoff, Toxicological Research Program in Perfluorinated Chemistries Email from W. Reagen to M. Nash re: Entrix Consulting Email from W. Reagen to M. Nash re: Entrix Consulting Email from R. Criswell to W. Keagen et al. re: Comments on Foth Environmental Infrastructure Report (3M Vault) with attachment Delta Environmental Consultants Inc., Perfluorocarbon (PFC)Containing Firefighting Foams and Their Use in Firefighting Training in Minnesota (2008) 8/27/2008 8/29/2008 10/22/2008 3/8/2010 4/7/2010 6/1/2010 7/2/2010 Draft, Ecotoxicology and Environmental Fate Testing of Short Chain Perfluoroalkyl Compounds Related to 3M Chemistries ATSDR, Public Health Assessment for Perfluorochemical Contamination in Lake Elmo and Oakdale, Washington County, Minnesota Delta Consultants, Addendum to Perfluorocarbon (PFC)Containing Firefighting Foams and Their Use in Firefighting Training in Minnesota, Prepared for MPCA (2008) MPCA, Mississippi River Pool 2 Intensive Study of Perfluorochemicals in Fish and Water: 2009 Letter from G. Olsen re: 3M Decatur Buidling 2/49 demolition and disposal project Weston, Construction Completion Report, Former Main Disposal Area, Woodbury Site MPCA to 3M, Request for Response Action 26 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN00567710 3MA02543910 3M_MN02295793 3M_MN00110700 3M_MN03589087 3M_MN05334328 3M_MN05334324 STATE_01782725 STATE_02820958 3M_MN01537089 STATE_01300660 STATE_02826813 STATE_02010400 3M_MN02288255 3M_MN05361976 STATE_02339051 Plaintiff's Ex. No. 2303 2304 2318 2343 2354 2367 2368 2374 2379 2382 2397 2398 2399 2400 2405 Date 7/23/2010 7/28/2010 1/18/2011 12/5/2011 4/11/2012 7/30/2012 7/30/2012 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Weston, Construction Completion Report D1 and D2 Areas, Cottage Grove Site, Cottage Grove, Minnesota Environ, spreadsheet re: bioaccumulation model to predict the concentration of PFOS in fish tissue, including the quantification of the proportion of exposure derived from surface sediment versus the water column Weston, Construction Completion Report D9 Area, Cottage Grove Site, Cottage Grove, Minnesota Probable Link Evaluation of Pregnancy Induced Hypertension and Preeclampsia (2011) Draft Memorandum from L. Zobel to FC Core Team re: Review of FC Manuscripts Probable Link Evaluation of Autoimmune Disease (2012) Probable Link Evaluation of Thyroid disease (2012) 10/29/2012 1/3/2013 2/22/2013 Probable Link Evaluation for heart disease (including high blood pressure, high cholesterol, coronary artery disease) (2012) Email from M. Falco to M. Nash re: Fw: Assessment of Long Chain Fluorochemical Use Newstead, John et al., Spatial and Temporal Trends of Perfluoroalkyl Compounds in Fish Fillets Collected From Pool 2 of the Upper Mississippi River (2013) 11/21/2013 Fish Consumption Guidelines for the General Population, Lakes 12/19/2013 1/27/2014 1/27/2014 Fish Consumption Guidelines for the General Population, River Letter from Jean B. Sweeney to MPCA Commissioner John L. Stine re: Comments on the 2014 MPCA Draft Impaired Waters List 3M Appendix A - Summary Data Report - Pool 2 Fall 2013 Fish Data 6/5/2014 Route, William T. et al, Spatial and Temporal Patterns in Concentrations of Perfluorinated Compounds in Bald Eagle Nestlings in the Upper Midwestern United States (2014) 27 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN01533753 STATE_00942604 3M_MN00716872 N/A 3M_MN04777930 N/A N/A N/A 3M_MN04836974 3M_MN03205198 N/A N/A 3M_MN03203477 3M_MN04813517 N/A Plaintiff's Ex. No. 2406 2421 2431 2435 2436 2437 2440 2448 2450 2455 2475 2476 2477 2487 2491 Date 7/22/2014 10/6/2015 4/00/2016 5/15/2016 5/23/2016 5/23/2016 6/10/2016 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Aqua-Pure Plumbing Wholesale Update Q2 Falco, Fluorochemical EHS Background, The Magic Behind the Innovation Anchor, 2013 Data Summary Report, Mississippi River - Pool 2 and Adjacent Locations The Madrid Statement on Poly- and Perfluoroalkyl Substances (PFASs) EPA Drinking Water Health Advisory for Perfluorooctanoic Acid (PFOA) EPA Drinking Water Health Advisory for Perfluorooctane Sulfonate (PFOS) C8: association between prenatal exposure to perfluorinated compounds 7/19/2016 8/11/2016 10/12/2016 MDH, Fish Consumption Guidelines for Women Who Are or May Become Pregnant, and Children Under Age 15, Lakes Fish Consumption Guidelines for Women Who Are or May Become Pregnant, and Children Under Age 15, Rivers 3M Analysis of Mississippi River Pore Water and Surface Water Samples near the 3M Cottage Grove Facility - September 2016 Sampling 5/3/2017 PFOA_Re-Evaluation_FinalToxReviewWorksheet_May2017.pdf 5/3/2017 PFOS_Re-Evaluation_FinalToxReviewWorksheet_May2017.pdf 5/17/2017 6/7/2017 00/00/0000 Environmental Surveillance and Assessment Memorandum from Nancy Rice (MDH) to James Kelly (MDH) re: Health-Based Values for Perfluorooctane Sulfonate MDH, Notice of Health Risk Advisory for Perfluorochemicals (PFCs), City of Cottage Grove, (2017) APFO summary document Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN05101829 3M_MN03639885 N/A N/A STATE_07081959 STATE_07082062 N/A STATE_04501887 STATE_04513318 3M_MN04844733 STATE_07438004 STATE_07438096 STATE_07457240 N/A 3M_MN01524233 28 Plaintiff's Ex. No. Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 2493 Various Factory Operating Standards. 1973, 1974, 1976, 1978, 1981, 1988, 1989, 1990, 1991, 1992, 1993, 1996, 1997, 1999, 2000 2496 2498 2499 2513 2515 2516 2517 Various 3M Waste Inventory Forms - Chemolite 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 Gilland, Frank and Jack Mandel, Peripheral Blood Lymphocyte Count in Men Occupationally Exposed to Perfluorooctanoic Acid Chart on FC-95 or PFOS Presentation, Basic Studies in Electrochemical Fluorination - A 3M Core Technology Handwritten Notes Bullet-Point Notes Regarding Paper for Submission Presentation, Representative LCM Flow Chart 29 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00050322; 3MA00053311; 3MA00053882; 3MA00056266; 3MA00072899; 3MA00072984; 3MA00081493; 3MA00202292; 3MA00204906; 3MA00204927; 3MA00204957; 3MA00206150; 3MA01168550; 3MA01200731; 3MA01201394; 3MA01201453; 3MA01828643; 3MA10064412; 3MA01986530; 3MA01986529; 3MA01986528; 3MA01986538; 3MA01986532; 3MA01986536; 3MA01986534; 3MA01986531 3MA10016749 3MA10031469 3M_MN00838987 3M_MN02323912 3M_MN02329964 3M_MN02492763 Plaintiff's Ex. No. 2521 2522 2534 2542 2545 2546 2547 2548 2549 2550 2551 2552 2553 2559 2561 2563 2565 2566 2567 Date 00/00/0000 4/10/0000 00/00/0000 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Business Opportunity Memo Questions for Charlie Auer for Monday, April 10 Chronology of PFCs in Blood 00/00/0000 00/00/2017 00/00/2001 10/12/1995 1/13/1997 4/3/1985 7/13/2014 00/00/2001 2/6/1997 12/18/1996 8/25/1954 6/18/1966 2/7/1979 3/8/2010 Toxicology Education Foundation Is It Safe? Dose Makes the Poison Video, available at http://toxedfoundation.org/is-it-safe/ Pictures of 3M products from website, http://docplayer.me/64695777-Deponiseminaret-pfas-i-sigevannfra-deponier-ase-hoisaeter-ngi.html Biegel et al., Mechanisms of Extrahepatic Tumer Induction by Peroxisome Proliferators in Male CD Rats, Toxicological Sciences 60, 44-55 (2001) Email from Perkins to Butenhoff et al. re: APME Meeting Aqua-Pure Video Ad, https://www.youtube.com/watch?v=eer1VSRMmM4 Email from Loushin to Weppner re: FC-143 MSDS Aqua-Pure Video Ad, https://www.youtube.com/watch?v=B55G3ix6ShQ Presentation by Perkins entitled FC-143 and APME Toxicology Related Issues From 1995 to Present Aqua-Pure Video Ad, https://www.youtube.com/watch?v=rU3j_R8Hbik Email from Pickett to Weppner re: FC-143 Issues Potassium Perfluorooctanoate Routine Toxicity Screening Woodbury Event Handwritten Timeline by Dr. Ling "In the long-term human health effects may be correlated with the presence of FM-3422 in the aquatic environment." Mississippi River Pool 2 Intensive Study of Perfluorochemicals in Fish and Water: 2009 2/19/1986 6/27/1979 1986 3M hazardous waste manifest indicating that acid bottoms are classified as D002 hazardous--i.e., corrosive--wastes 3M document indicating WWTP sludge and incineration ash and sludge are hazardous wastes Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00330478 3MA00470823 3MA10039277 N/A N/A N/A 3MA10024469 N/A 3MA00621672 N/A 3MA00194560 N/A 3MA10066727 3MA01828941 3M_MN00000466 3M_MN00000151 3M_MN03043077 3M_MPCA00006161 3MA00280412 30 Plaintiff's Ex. No. 2568 2569 2570 2571 2572 2573 2574 2575 2576 2577 2579 2580 2581 2582 2583 2584 2585 2586 2589 Date 9/13/1960 3/23/1979 12/6/1995 7/18/2006 7/29/2004 5/25/1983 3/9/2006 5/00/2017 5/22/2007 7/3/2001 4/00/2008 1/4/2017 4/15/2012 7/30/2012 12/5/2011 10/1/2014 7/30/2012 1/7/1964 8/23/1966 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M document indicating that by 1960, Building 15 discharged 131,000 gallons of effluent to the chemical sewer per day, which included 206 pounds of HF acid per day March 23, 1979 Technical Report Summary 3M waste stream profile indicating fluorochemical inerts contain PFCs Letter from MPCA (Eckberg, with copy to Kriens) to 3M in which MPCA alleged that 3M violated federal requirements pertaining to its 2002 NPDES permit application July 2004 State emails Fate of Fluorochemicals Phase II Study 3M-EPA Consent Agreement MDH HBV for PFOA and PFOS MPCA Settlement Agreement and Consent Order July 2001 Santoro email to Palensky and Walker, copying others, regarding Cottage Grove Wells April 2008 MDH Fish Consumption Advisory for PFOS 2016 Draft Impaired Waters List C-8 Science Panel Probable Link Report: probable link between PFOA exposure and testicular/kidney cancer C-8 Science Panel Probable Link Report: probable link between PFOA exposure and ulcerative colitis C-8 Science Panel Probably Link Report: Probable link between PFC exposure and pregnancy-induced hypertension/preeclampsia Johnson et al. (2014), The Navigation Guide - Evidence-based medicine meets environmental health: Systematic Review of Human Evidence for PFOA Effects on Fetal Growth C-8 Science Panel Probable Link Report: Probable link between PFOA exposure and thyroid disease and high cholesterol. 3M Correspondence from C. Diets to H. Jones Meeting Minutes re Woodbury Township Meeting 31 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00456289 3MA01410316 3MA10051876 MN.064.0120.000599 STATE_02795716 3MA10065463 N/A N/A MN.064.0103.000002 3MA00348418 STATE_02061740 N/A N/A N/A N/A N/A N/A 3MA00335783 3MA00285494 Plaintiff's Ex. No. 2590 2591 2593 2594 2595 2596 2597 2598 2599 2600 2601 2602 2603 2604 2605 2606 2607 2614 2615 2616 Date 00/00/1954 7/28/1960 8/14/1975 4/12/1978 8/16/1978 5/22/1979 6/23/1980 10/28/1980 5/4/1981 8/31/1984 12/30/1988 5/15/1998 9/2/1998 11/17/2003 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 3M, Documentation of the 3M Exposure Guideline for N-Methylperf/uorobutanesu/fonamidoethanol (N-McFBSE) Letter R.C. Collins and J. Brown re Field Letter Memorandum from G.H. Crawford to C. Krogh et al. re: Fluorocarbons in Human Blood Plasma Animal studies 3M Technical Report Summary, Evaluation of the Bioconcentration Potential of FM 3422 3M Technical Report Summary, Bioaccumulation Studies 3M Technical Report Summary, Detection of Fluorochemicals in Decatur Wastewater MPCA Issue Statement Letter from M. B. Ayers (MPCA) to Dr. R. Susag (3M) re: investigation of a disposal site 3M Internal Correspondence from D.E. Roach, M.D. to P.F. Riehle (Specialty Chemical Division - Chemolite Center 41-1) re Organic Fluorine Levels 3M Technical Report Summary, Effect of Potassium Perfluorooctanesulfonate on Survival, etc. Letter from 3M to EPA re: TSCA Section 8(e) -Perfluorooctane Sulfonate 3M lab notebook Memorandum from T. DiPasquale to J. R. Allison et al. re : FC Meeting - November 11, 2003 2/17/2006 7/18/2006 12/30/2009 5/6/2002 00/00/2017 12/14/1948 Memorandum from J. Giesy (ENTRIX Inc.) to D. Bacon (3M) re: Follow up to February 2, 2006 meeting (revised memo) Letter from MPCA to 3M EPA Report Entitled: "Long-Chain Perfluorinated Chemicals Action Plan" Meeting Minutes West Virginia DEP & DuPont "CATT" Toxicity Team and Report Excerpts Dourson Emails U.S. Patent 2,456,027 32 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA01628937 3M_MN00000231 3M_MN00000293 3MA100666974 3MA00326803 3M_MN01639837 3MA01409767 3M_MN00001391 3MA00334184 3M_MN01655416 3MA10035953 3M_MN02456909 3M_MN04758351 3M_MN04778452 3MA02513749 3M_MN0492289 N/A N/A N/A N/A Plaintiff's Ex. No. 2617 2621 2632 2639 2640 2649 2651 2660 2662 2667 2673 2679 2682 2683 2684 2685 2686 2687 Date 00/00/0000 5/14/1962 10/18/1966 12/28/1966 3/24/1967 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Final Comprehensive Report FC-95 MN Mining Letter from J.T. Ling to D. H. Cochran RE Waste Disposal Woodbury Dump Site Interoffice Letter from J.T. Ling to D.R. Guthrie RE Residence Well Water Sampling Woodbury Township and Cottage Grove Village Water Pollution Problem in Woodbury - 1 page summary regarding investigation of Chemolite Meeting Minutes RE Woodbury Ground Water Problem with Hargraves (MWPC) 8/31/1971 Interoffice Memo from J.T. Ling to H.G. Bryce RE Ecological Aspects of Fluorocarbons - comments on Bryce's draft report 9/13/1971 1/00/1967 00/00/1980 8/18/2017 9/22/2017 11/7/2017 9/24/1993 4/28/2017 6/30/2011 7/3/2017 4/27/2010 7/12/2017 Interoffice Letter from H.G. Bryce to R.M. Adams RE Ecological Aspects of Fluorocarbons - your memo 7/14/1971 Hickok, E. Report titled "Ground Water Investigative Program at Woodbury" Site No. 8 - 3M Company - Woodbury Email from Lucas Martin containing two spreadsheets with East Metro Water Quality Data.xlsx. Kier Soderberg Field Photos: img_0940 - img_1081 Davis Expert Report Figure 5-6: Hazard Indices 3M Combined Air and Hazardous Waste Permit Renewal; Permit No. 23-AI-89-0-6 MPCA Letter from G. Krueger to J. Sweeney RE New Drinking Water Health Advisories for PFOA and PFOS LimnoTech (2011). TMDL Scoping - PFOS in Pool 2 of the Mississippi River Letter from Brewer to MPCA RE Settlement Agreement and Consent Order (SACO), dated May 22, 2017 Email from Balogh to L. Rogacki RE Estimated PFOS loads in Metro effluent and the Mississippi River Letter from Brewer to MPCA RE 3M disputes a reimbursement request for certain expenditures 33 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A 3M_MN00048247 3M_MN00000728 3MA00285419 3MA00285471 3MA02496585 3M_MN00048386 3MA00286008 3MA01934828 N/A N/A N/A 3MA00288649 N/A STATE_01170462 N/A MET0007023 N/A Plaintiff's Ex. No. 2688 2689 2690 2691 2692 2693 2694 2695 2696 2697 2698 2699 2700 2701 2702 2703 2704 Date 7/12/2017 00/00/2016 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description MN AG Letter to Brewer RE 2007 Consent Order and 3M cost reimbursement MPCA, 2016. Fish tissue data provided in spreadsheet. 7/20/2017 12/16/2010 11/21/2017 11/29/2017 00/00/0000 1/1/1998 Letter from Brewer to A. Cohen RE receipt of July 12, 2017 letter Environ, 2010. Review of PFOS Impairment in Pool 2 of the Mississippi River. Prepared for Barnes and Thornburg LLP on behalf of Metropolitan Council Environmental Services, December 16, 2010 Letter from Hogan (MPCA) to G. Hohenstein RE Drinking Water Health Advisory for Cities of Woodbury and Oakdale Municipal Wells Letter from Brewer to M. Kieley (AGO) RE Response to November 21, 2017 letter. Dilks CV 3M Presentation: Environmental Fate and Effects of Fluorochemicals by R. Howell 3/5/2005 2/26/1997 00/00/2003 PFOS Case Study by Butenhoff, Olsen and Pfahles-Hutchens Email from Maendler to Howell, et al. RE Tox/Envt'l Issues DuPont Risk Assessment 2003 Proxy Statement 3/9/1981 6/25/1970 Memo from K.J. Miller to C.D. King RE Drum Liner Disposal Letter from 3M to MCPA RE Oakdale Dump Site 11/17/1981 10/19/1977 00/00/0000 00/00/0000 Letter and Work Plan: Hydrogeological Investigation of Disposal Areas at the 3M Chemolite Plant in Cottage Grove, MN Interoffice Corr. from L.C. Krogh to Lazerte, Sheukrman, Ubel RE Nov 7 presentation and copies of transparencies used in last report. Overview of Potential Dredging Areas (2.2 PPB Threshold, Depth 1 ft.) Dredging Volumes by Area (2.2 PPB PFOS Threshold) 34 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A STATE_07459336 N/A STATE_01178225 N/A N/A N/A 3MA10051826 3MA00762535 3MA00194581 N/A 3MA00150027 3M_MN00049959 3M_MN00001563 3M_MN00000479 N/A N/A Plaintiff's Ex. No. 2705 2706 2707 2708 2709 2710 2711 2712 2713 2714 2715 2716 2717 2718 2719 2720 2721 2722 2723 2724 2725 Date 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 00/00/0000 1/3/2018 11/18/1998 12/00/2009 00/00/1974 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Overview of Potential Dredging Areas (1 PPB Threshold, Depth 1 ft) Dredging Volumes by Area (1 PPB PFOS Threshold) Wetland Bank Service Areas and Major Watersheds for County Boundaries Minnesota Pre-Settlement Wetland Areas Remaining Estimated Cost of Credits Required to Address PFC Wetland Impacts Wetland Bank Price Per Credit from BWSR 2017 RFP Letter from Bilot to Huyser RE PFCs in Minnesota A Review of the Environmental Fate and Effects of Sulfonyl Based Fluorochemicals DRAFT Frisbee, S., et al., The C8 Health Project: Design, Methods, and Participants, 117 Environmental Health Persp. p. 1873 (Dec. 2009) Algicidal Activity Test Substance 12/13/1961 5/29/2007 12/00/1998 4/26/2000 11/2/1998 00/00/0000 5/15/1998 4/26/1979 MN Mining & Manf. Co. Geology Department Report No. 61-22 Consulting Services Agreement FC Toxicity/Safety Testing In Particular PFOS & N-EtFOSE by Nabbefeld, et al. CAS No. 2795-39-3 Potassium Perfluorooctanesulfonate EPA Proposed Meeting Draft by C. Reich DeWitt CV Email from Jerry (?) to J.E. Gregory and J.R. Lewis RE Accumulation and Disposal of Waste Water at Decatur 3M Interoffice Correspondence from Prokop re: Meeting Minutes - Meeting with J.R. Mitchell 7/26/1979 8/23/1978 7/22/1992 Phone Conversation Report from R.A. Prokop to L.C. Krogn and J.D. Lazerte with Eugene Berman, attorney for DuPont 3M Interoffice Correspondence RE Minutes of Meeting with H.C. Hodge, held in Portland, Maine Minutes of Fluorochemical Steering Committee Meeting 35 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A N/A 3M_MN05374965 N/A 3M_MN00436466 3MA00335895 3M_MN00255852 3MA10054016 3MA01657924 3MA10071231 N/A 3MA00905854 3MA10034826 3MA10035034 3MA00967742 3M_MN00000789 Plaintiff's Ex. No. 2726 2727 2728 2729 2730 2731 2732 2733 2734 2735 2736 2737 2738 2739 2740 2741 2742 Date 5/27/1993 1/22/2007 1/9/2007 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description In Search of Non-Industrial Sources of Organic Fluorine In Normal Human Blood from the General Public Email from M.A. Santoro to P. Hoff RE Fw: Considerations for conducting PFOA avian repro study Corporate Messages, Environmental Energy and Safety Issues. Issues: FC - East Metro Drinking Water 4/6/1989 4/25/2006 11/2/2017 00/00/1993 5/23/1997 2/23/2001 8/21/2017 9/8/2017 3/8/2017 Table 6: Observed and Expected Deaths by Cause, Standardized Mortality Ratios (SMR), 95 Percent Confidence Limits and Chi Square Values, Males, Chemolite Plant 2006 EPA press release on TSCA fine for 3M Rotondo, J.C. et al., Environmental doses of perfluorooctanoic acid change the expression of genes in target tissues of common carp. 3M Update Magazine Battelle Presentation: Ecosystem Fate Modeling Acute Toxicity Report in Honey Bee (AR 226-1017) Lower and Upper Pool 2 Maps of Records of Live Lampsilis higginsii surveyed 1999-2017 Map of Records of Live Quadrula nodulata above Pig's Eye WWTP Yingling, G. "Perfluorochemicals (PFCs; aka PFAS) in Grey Cloud Island Township" 12/2/2017 Letter from M. Kieley (AGO) to Brewer RE Response Actions Related to PFC Releases from 3M PFC Disposal Sites 8/00/2005 00/00/2008 00/00/2008 1/9/2008 Washington County and Washington Conservation District, Integrating Groundwater & Surface Water Management Southern Washington County, Prepared by Barr Engineering Olsen. Decatur Medical Surveillance Study Olsen. Decatur Medical Surveillance Study Email advising Jean Sweeney of inaccuracy of statement: "3M no longer manufactures PFOS, PFOA, or PFBA" 36 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN03112528 3M_MN03436924 3M_MN03521906 3MA00632317 N/A N/A 3MA00044881 3MA01429655 MET 0438364 STATE_07507089 STATE_07543913 N/A N/A N/A 3M_MN05372035 3M_MN05372003 3M_MN00567706 Plaintiff's Ex. No. 2743 2744 2745 2746 2747 2748 2749 2750 2751 2752 2753 2754 2755 2756 2757 2758 Date 10/30/2007 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Presentation containing statement: "3M no longer manufactures PFOS, PFOA, or PFBA" 00/00/1999 4/2/1979 00/00/2014 8/26/1958 2/17/1976 6/28/1905 2/9/2017 9/1/1999 00/00/2003 Cottage Grove Chemical Monthly Report. 11/1998 and 06/1999 "St. Paul Megaphone" Landsteiner, A., Huset, C., Williams, A., Johnson, J. Biomonitoring for Perfluorochemicals in a Minnesota Community with Known Drinking Water F.B. Richerson summary RE: Discussion of Chemolite Wastes with Mr. Johannes of the SWPCB Organic Fluorine Compounds in Blood Chronology List of Studies to be Moved to 8(e) Docket 3M SEC 10-K for the year ended December 31, 2016 SMMD FC Waste Management (CY1998) MPCA Annual Report on Washington County Sanitary Landfill 2003 10/9/2017 5/26/1999 Affidavit of Charles Kiester ISO 3M's Response to Opposition to State's Motion to Compel Discovery, with attachment "Fluorochemical Use, Distribution and Release Overview", Prepared by 3M 00/00/1989 5/19/1992 7/23/2013 Various Just, W.W., Gorgas, K., Hartl, F-U., Heinemann, P., Salzer, M., Schimassek, H. Biochemical Effects and Zonal Heterogeneity of Peroxisome Proliferation Induced by Perfluorocarboxylic Acids in Rat Liver. Hepatology Vol. 9 (4) 570-581 Terminated Study Final Report (GLP) Titled: PFOS and POAA Study in Goats. Study No. FACT-TOX-100 Presentation entitled "Status of the PFC Assessment/Remediation Projects in Minnesota" Summary of 3M Hazardous Waste Manifests 1980 - 2008 assigning one or more EPA Hazardous Waste codes to waste characterized as containing PFCs; The Summary compromising underlying exhibits 2758.0001 - 2758.2325. 37 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN00566907 3MA01204490; 3MA00229513 3MA00323984 N/A 3MA00456233 3MA10067216 3MA01220049 N/A 3M_MN02792261 3MA00402203 N/A 3M_MN03270260 3MA00632733 3MA01725206 STATE_02942271 N/A Plaintiff's Ex. No. 2759 2760 2761 2762 2763 2764 2765 2766 2767 2768 2769 2770 2771 Date 11/13/1997 9/00/1996 4/00/2003 10/00/2017 11/9/2017 11/30/2007 11/30/2007 11/30/2007 10/27/1961 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Beach, Susan. Report titled: Results from Analyses of Soil and Groundwater Samples from the E.I. DuPont de Nemours and Company Facility in Parkersburg, WV EPA Monthly Hotline Report MPCA Minnesota Environment Special Report. FY 2002 Superfund Report to the Legislature. "Use of the Minnesota Environmental Response, Compensation and Compliance Account (Superfund)." MDH Website - Current Activities: Perflurochemicals (PFCs) in Minnesota Handwritten equation by Connolly Report on the manufacture, Use, and Releases of PFCs at the 3M Cottage Grove Facility - attachments 2 - 6 Report on the manufacture, Use, and Releases of PFCs at the 3M Cottage Grove Facility - attachment 7 Report on the manufacture, Use, and Releases of PFCs at the 3M Cottage Grove Facility - attachments 8 - 11 3M Life Magazine Scotchgard Ad 4/13/2007 12/9/1999 1/19/1999 8/22/1975 Letter from K. Sather (MPCA) to Board Members RE Request for Issuance of a Request for Response Action (RFRA) to the 3M Company: For the Release and Threatened Release of Hazardous Substances from the 3M Chemolite Disposal Site, 3M Oakdale Disposal Site, and 3M Woodbury Disposal Site 3M/DuPont Meeting Notes for Removing PFOA from Wastewater 3M Draft Company Statement Interoffice Correspondence from J.D. LaZerte to L.C. Krogh RE Telephone Call from Dr. Warren Guy, Uni of Florida RE Fluorochemicals in Human Blood Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN00043306 N/A N/A N/A N/A 3MA02527154 3MA02527167 3MA02527243 N/A STATE_07088102 3M_MN05377877 3M_MN05382332 3M_MN05382159 38 Plaintiff's Ex. No. Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 2772 2773 2774 2775 2776 2777 2778 2779 2780 2781 Various Material Safety Data Sheets from February and March 1997, stating that multiple PFC-containing products can cause cancer. (2772A - 2772P) Summary of Certain 3M Payments for John Giesy Work; The 00/00/0000 Summary comprising underlying exhibits 2773.0001-2773.0147 2/28/1978 Interoffice Correspondence from A.N. Welter to R.A. Prokop RE Fate of Fluorochemical Project, Informational Meeting 2/24/1978 5/00/2017 Fish Consumption Guidelines for the General Population, Lakes 6/00/2016 5/00/2017 6/00/2016 00/00/2001 Fish Consumption Guidelines for the General Population, Rivers Fish Consumption Guidelines for Women who Are or May Become Pregnant, and Children under Age 15, Lake Fish Consumption Guidelines for Women who Are or May Become Pregnant, and Children under Age 15, Rivers 2001 Proxy Statement 00/00/0000 5/00/2000 Undated photograph showing open burning of drums in landfill Project Spring Communication Plan Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN05419460; 3M_MN05421995; 3M_MN05423232; 3M_MN05434588; 3M_MN05435506; 3M_MN05423793; 3M_MN05433545; 3M_MN05419466; 3M_MN05433550; 3M_MN05435511; 3M_MN05423238; 3M_MN05434593; 3M_MN05423799; 3M_MN05419472; 3M_MN05423244; 3M_MN05429408; N/A 3MA10066978 N/A N/A N/A N/A N/A 3M_MN00000473 3M_MN05381646 39 Plaintiff's Ex. No. 2782 2783 2784 2785 2786 2787 2788 2789 2790 2791 2792 2793 2794 2795 2796 Date 6/2/1993 2/17/1975 6/18/2008 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Internal Correspondence from T. Manzara R Microorganism Sources for Degradable F.C. Study Memo to T. Scherkenbach from G. Frazier RE 3M Woodbury Site MPCA Remedy Decision Document - Washington County Landfill, Lake Elmo, MN 6/13/2001 5/11/1983 1/25/1991 12/17/2998 9/5/2001 Letter from K. Reed to EPA re TSCA Section 8(a) Supplemental Submission: Docket Nos 8EHQ-1180-373 and 8EHQ-1180-374 Pilot Rat Teratology Study T-3352 - Final Report Final Report Titled Primary Eye Irritation/Corrosion Study of T5298 in rabbits (OECD Guidelines) Final Report - Protocol 418-011 Oral (Gavage) Developmental Toxicity Study of N-EtFOSE in Rats, Sponsor's Study Number: T-6316.7 Letter from G. Adams (3M) to U.S. EPA re: TSCA 8(e) Supplemental Notice on Sulfonate-based Fluorochemicals, AR226-1038 5/14/1999 11/3/1995 3M Medical Department, Toxicology Services, Report for Study No. T-6316.9; DT21 Fluorochemical (FC) Levels in Nave Rats Product Safety Labs, Wnorowski, G., Primary Eye Irritation 5/30/1997 Stump, D., A Developmental Toxicity Study of 313401 in Rats 11/9/1994 Determination of the Partition Coefficient (N-Octanol/Water) of T5874 by High Performance Liquid Chromatography (HPLC) 11/9/1994 1/10/1979 2/14/1996 Determination of the Partition Coefficient (N-Octanol/Water) of T5869.4 by High Performance Liquid Chromatography (HPLC) Technical Report Summary: Distribution Coefficient of FM 3925 in n-Octanol/Water M.S.I. Report No. 4B223-4B227, Determination of Physicochemical Properties of Sample D-1 by Mitsubishi Chemical Safety Institute Ltd. 40 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN05437251 3M_MN00048377 3MA02645872 MET 0438451 3MA00248286 3M_MN01241251 3MA10083119 MET0438638 3M_MN00428316 3M_MN01062303 3M_MN01062651 3M_MN01532235 3M_MN01639872 3M_MN01640028 3M_MN01640581 Plaintiff's Ex. No. 2797 2798 2799 2800 2801 2802 2803 2804 2805 2806 2807 2808 2809 2810 2811 Date 2/16/1993 2/25/1980 6/11/1999 4/26/2000 4/12/1979 1/11/1999 5/14/1999 1/11/1999 4/15/1998 5/31/1978 11/29/1995 1/14/1987 9/5/1996 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Twenty-eight-day Repeated Dose Oral Toxicity Study of Sample D-1 in Rats Two-Week Oral Range finding Toxicity Study of T-2509CoC in Rats Report of Data for Exploratory 28-day Oral Toxicity Study in Rats: Telomer Alcohol, Telomer Acrylate, PFBS, PFHS, PFOS, Laboratory Report No. FACT-TOX-120.3 Gallagher, S. et al., PFOS: A Dietary LC50 Study with the Northern Bobwhite Bio/Dynamics Inc., Project No. 78-7187, An Acute Inhalation Toxicity Study of T-2308 CoC in the Rat Final Report, Protocol 418-010 Oral (Stomach Tube) Developmental Toxicity Study of N-EtFOSE in Rabbits 3M Medical Department, Toxicology Services, Report for Study No. T-6316.9; DT21 Fluorochemical (FC) Levels in Nave Rats Further Investigation of Rat Chow Final Report, Protocol 418-012 Oral (Stomach Tube) Developmental Toxicity Study of PFOS in Rabbits 104-Week Dietary Chronic Toxicity and Carcinogenicity Study with Perfluorooctane Sulfonic Acid Potassium Salt (PFOS; T6295) in Rats International research and Development Corporation, Fluorad Fluorochemical Surfactant FC-95, Acute Oral Toxicity (LD50) Study in Rats 3M Final Report - Analytical Study, Single-dose Intravenous Pharmacokinetic Study of T-6246 in Rabbits S. Glaza (Hazelton), Primary Eye Irritation Study in Rabbits Method, Summary Raw Data Appendix S. Glaza (Corning Hazelton), Final Report, Primary Eye Irrigation/Corrosion Study of T-6564 in Rabbits (OECD Guidelines) 2/18/1981 1/17/1984 Acute Ocular Irritation Test with T-2960CoC in Albino Rabbits Acute Oral Toxicity Screen with T-3421 in Albino Rats 41 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN01649987 3M_MN01695616 3M_MN02336491 3MA00233956 3MA00234875 3MA00239722 3MA00242650 3MA00353213 3MA00395762 3MA00725705 3MA01502168 3MA10001092 3MA10006895 3MA10008130 3MA10019997 Plaintiff's Ex. No. 2812 2813 2814 2815 2816 2817 2818 3008 3013 3017 3020 3021 3022 3023 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 8/11/1999 Final Report - Epidemiology - Fluorochemical Exposure Assessment of Decatur Chemical and Film Plant Employees 1/19/1983 00/00/0000 1/5/2003 4/1/2014 3/8/2010 5/00/2013 00/00/1950 8/1/1955 00/00/1961 00/00/1963 00/00/1963 00/00/1964 00/00/1965 Absorption and Biotransformation of N-Ethyl FOSE and Tissue Distribution and Elimination of Carbon-14 after Administration of N-Ethyl FOSE-14C in Feed by Riker Laboratories, Inc. Composite Analytical Laboratory Report on the Quantitative Analysis of Fluorochemicals in Environmental Samples, Report No. Fact Gen-021, Gen-024, Gen-030, Gen-033, LRN - W2491, W2845, W3197, E00-1386. Decatur Worker Communication Timeline Concerning Fluorochemical Health and Safety Issue MPCA Responses to the 2014 Impaired Waters List 30-day Public Notice Comments MPCA, Mississippi River Pool 2 Intensive Study of Perfluorochemicals in Fish and Water: 2009 MPCA, Perfluorochemicals in Mississippi River Pool 2, 2012 Update Simons, J. H., 1950. Fluorocarbons and Their Production. Fluorine Chemistry, 1(12): 401-422. Nordby, G. L, et al., 1955. Perfluorooctanoic Acid Interactions With Human Serum Albumin. Journal of Biological Chemistry, (219): 339-404. August 1. Saunders, B.C., 1961. The Physiological Action of Organic Compounds Containing Fluorine. Advances in Fluorine Chemistry, 2: 183-210. Hamilton, J. M., 1963. The Organic Fluorochemicals Industry. Advances in Fluorine Chemistry, 3: 117-180. Hodge, H. C. et al. 1963. Biological Effects of Organic Fluoride. Fluorine Chemistry, 3: 1-55. Bryce, H.G., Industrial and Utilitarian Aspects of Fluorine Chemistry. Taylor, N. F. et al., 1965. Structural Aspects of MonofluoroSteroids. Advances in Fluorine Chemistry, 4: 113-141. 42 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA10050434 3MA10053186 3M_MN01665997 3M_MN05439756 N/A N/A N/A STATE_07525274 3MA00631310 N/A N/A N/A 3M_MN04855110 N/A Plaintiff's Ex. No. 3028 3029 3043 3048 3054 3092 3098 3145 3162 3180 3184 3200 Date 00/00/1973 00/00/1973 00/00/1982 00/00/1985 00/00/1986 1/12/1998 00/00/1998 00/00/2003 00/00/2003 00/00/2004 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Clark, Leland et al., Perfluorocarbons Having a Short Dwell Time in the Liver, Science 181(4100):680-2. Clark, L. C. et al., 1973. PFCs Having a Short Dwell Time in the Liver: Science. 18(4100): 680-682. MPCA Preamble, Statement of Need and Reasonableness (1982) Ikeda T, Aiba K, Fukuda K, Tanaka M: The induction of peroxisome proliferation in rat liver by perfluorinated fatty acids, metabolically inert derivatives of fatty acids. J Biochem 1985, 98(2):475-482. EPA, National Priorities List Fact Book (1986) lntrasuksri, Urusa et al., Mechanisms of Peroxisome Proliferation by Perfluorooctanoic Acid and Endogenous Fatty Acids, Gen. Pharmac. (1998) MPCA, Draft Guidelines Remedy Selection Alexander BH, Olsen GW, Burris JM, Mandel JH, Mandel JS: Mortality of employees of a perfluorooctanesulphonyl fluoride manufacturing facility. Occup Environ Med 2003, 60(10):722729. Thibodeaux JR, Hanson RG, Rogers JM, Grey BE, Barbee BD, Richards JH, Butenhoff JL, Stevenson LA, and Lau C. 2003. Exposure to perfluorooctane sulfonate during pregnancy in rat and mouse: I: maternal and prenatal evaluations. Toxicological Sciences 74:369-381. MPCA Ground-Water Sampling for PFOA near the Washington Co. Landfill 00/00/2005 00/00/2006 Kannan, K., Tao, L., Sinclair, E., Pastva, S.D., Jude, D.J., Giesy, J.P. 2005. Perfluorinated Compounds in Aquatic Organisms at Various Trophic Levels in a Great Lakes Food Chain. Archives of Environmental Contamination and Toxicology 48:59-566. Lau C, Thibodeaux JR, Hanson RG, Narotsky MG, Rogers JM, Lindstrom AB, Strynar MJ: Effects of perfluorooctanoic acid exposure during pregnancy in the mouse. Toxicol Sci 2006, 90(2):510-518. 43 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3MA00631101 N/A N/A N/A 3MA00610364 3M_MN04736476 N/A N/A N/A 3MA00511220 N/A N/A Plaintiff's Ex. No. 3203 3207 3210 3217 3223 3234 3245 3246 3269 Date 00/00/2006 00/00/2006 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Molina, E.D., Balander, R., Fitzgerald, S.D., Giesy, J.P., Kannan, K., Mitchell, R., Bursian, S.J. 2006. Effects of Air Cell Infection of Perfluorooctane Sulfonate Before Incubation on Development of the White Leghorn Chicken (Gallus domesticus) Embryo. Environmental Toxicology and Chemistry 25(1):227-232. Science Advisory Board: SAB Review of EPA's Draft Risk Assessment of Potential Human Health Effects Associated with PFOA and Its Salts. In. Washington, DC: U.S. Environmental Protection Agency; 2006. 00/00/2006 00/00/2006 12/7/2007 00/00/2007 00/00/2007 1/15/2008 00/00/2008 Stevenson, C.N., Macmanus-Spencer, L.A., Luckenbach, T., Luthy, R.G., Epel, D. 2006. New Perspectives on Perfluorochemical Ecotoxicology: Inhibition and Induction of an Efflux Transporter in the Marine Mussel, Mytilus Californians. Environmental Science & Technology 40:5580-5585. City of Oakdale. Update: Perfluorochemicals and the City of Oakdale Public Water Supply. MPCA Investigating PFCs in groundwater near the Washington Co. Landfill Minnesota Cancer Surveillance System: Cancer incidence in Dakota and Washington counties. In: MCSS Epidemiology Report 2007:1. St. Paul, MN: Minnesota Cancer Surveillance System; 2007 MPCA 2007. Perfluorochemicals Past, present and future actions. https://www.pca.state.mn.us/sites/default/files/gp5-18.pdf MDH: Health Risk Limits for Perfluorochemicals. In: Report to the Minnesota Legislature. St. Paul, MN: MDH; 2008. http://www.health.state.mn.us/divs/eh/hazardous/topics/pfcs/final report011508.pdf MDH 2008 Site-Specific Meal Advice for Men and Women Not Planning on Becoming Pregnant Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A 3MA01467679 3M_MN01535036 3M_MN04780535 N/A N/A N/A 44 Plaintiff's Ex. No. 3280 3310 3312 3313 3314 3320 3332 3334 3335 3337 3344 3376 3377 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 00/00/2008 00/00/2009 00/00/2009 00/00/2009 00/00/2009 Minnesota Pollution Control Agency, "Minnesota's Fish Contaminant Monitoring Program," Pollution Prevention/Sustainability Fact Sheet, July 2008, https://www.pca.state.mn.us/sites/default/files/p-p2s4-05.pdf Lundin JI, Alexander BH, Olsen GW, Church TR: Ammonium perfluorooctanoate production and occupational mortality. Epidemiology 2009, 20(6):921-928. MDH, Toxicological summary for perfluorohexane sulfonate (PFHxS) (2009) MDH, Toxicological summary for perfluorooctane sulfonate (PFOS) and salts (2009) MDH, Toxicological summary for perfluorooctanoic acid (PFOA) and salts (2009) 00/00/2009 00/00/2009 2/16/2010 5/1/2010 5/24/2010 00/00/2010 00/00/2011 00/00/2011 Peden-Adams, M.M., Stuckey, J.E., Gaworecki, K.M., BergerRitchie, J., Bryant, K., Jodice, P.G., Scott, T.R., Berrario, J.B., Guan, B., Vigo, C., Boone, J.S., McGuinn, W.D., Dewitt, J.C., Keil, D.E. 2009. Developmental Toxicity in White Leghorn Chickens Following in ovo Exposure to Perfluorooctane Sulfonate (PFOS). Reproductive Toxicology 27:307-318. MPCA, The Lethality Characteristic. A Minnesota specific Hazardous-waste Characteristic Custer, Thomas et al., Perfluorinated Compounds and Polybrominated Diphenyl Ethers in Great Blue Heron Eggs from Three Colonies on the Mississippi River, Minnesota, Waterbirds 33(1):86-95. 2010 Minnesota Pollution Control Agency (MPCA) (2010). Guidance for Perfluorochemicals Analysis EPA, The Presence and Distribution of Perfluorochemicals (PFCs) in Minnesota MPCA, Identifying, Using and Managing PCBs. Waste/Hazardous Waste #4.48a. MPCA, F List of Hazardous Wastes MPCA, Characteristic Hazardous Wastes 45 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A STATE_02770359 N/A STATE_00929284 MET0887473 STATE_07240721 STATE_07239974 STATE_07239985 Plaintiff's Ex. No. 3379 3380 3420 3431 3437 3452 3459 3512 Date 00/00/2011 00/00/2011 00/00/2011 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 2011 Annual Groundwater Report Perfluorochemical (PFC) Groundwater Assessment and Hydraulic Capture Zone Evaluation 3M Woodbury, MN prepared by Weston Solutions, Inc. MPCA, P List of Acute Hazardous Wastes & Managing Acute Hazardous Wastes MDH, Toxicological summary for perfluorobutyrate (PFBA) (2011) 00/00/2011 Wang, M., Chen, J., Lin, K., Chen, Y., Hu, W., Tanguay, R.L., Huang, C., Dong, Q. 2011. Chronic Zebrafish PFOS Exposure Alters Sex Ratio and Maternal Related Effects in F1 Offspring. Environmental Toxicology and Chemistry. 30(9):2073-2080 3/13/2012 Steenland K and Woskie S. Cohort mortality study of workers exposed to perfluorooctanoic acid, Am J Epidemiol. 2012 Nov 15;176(10):909-17. Epub 2012 Oct 18. 00/00/2012 00/00/2012 00/00/2013 Custer, C.M., Custer, T.W., Schoenfuss, H.L., Poganski, B.H., Salem, L. 2012. Exposure and Effects of Perfluoroalkyl Compounds on Tree Swallows Nesting at Lake Johanna in East Central Minnesota, USA. Reproductive Toxicology 33:556-562. Grandjean P, Andersen EW, Budtz-Jorgensen E, Nielsen F, Molbak K, Weihe P, Heilmann C: Serum vaccine antibody concentrations in children exposed to perfluorinated compounds. JAMA : the journal of the American Medical Association 2012, 307(4):391-397. Barry V, Winquist A, and Steenland K. 2013. Perfluorooctanoic acid (PFOA) exposures and incident cancers among adults living near a chemical plant. Environmental Health Perspectives 121:1313-1318. Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. 3M_MN04998484 N/A N/A N/A N/A N/A N/A N/A 46 Plaintiff's Ex. No. 3516 3520 3527 3530 3532 3533 3539 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 00/00/2013 00/00/2013 Fair, A.P., Romano, T., Schaefer, A.M., Reif, J.S., Bossart, G.D., Houde, M., Muir, D., Adams, J., Rice, C., Hulsey, T.C., Peden-Adams, M. 2013. Associations Between Perfluoroalkyl Compounds and Immune and Clinical Chemistry Parameters in Highly Exposed Bottlenose Dolphins (Tursiops truncatus). Environmental Toxicology and Chemistry 32(4):736-746. Granum B, Haug LS, Namork E, Stolevik SB, Thomsen C, Aaberge IS, van Loveren H, Lovik M, Nygaard UC: Pre-natal exposure to perfluoroalkyl substances may be associated with altered vaccine antibody levels and immune-related health outcomes in early childhood. J Immunotoxicol 2013, 10(4):373379. 00/00/2013 Lou, Q.Q., Zhang, Y.F., Zhou, Z., Shi, Y.L., Ge, Y.N., Ren, D.K., Xu, H.M., Zhao, Y.X., Wei, W.J., Qin, Z.F.2013. Effects of Perfluorooctanesulfonate and Perfluorobutanesulfonate on the Growth and Sexual Development of Xenopus laevis. Ecotoxicology 22:1133-11440 00/00/2013 00/00/2013 Minnesota Registration & Certification, Documentation of Death (2013), http://www.health.state.mn.us/divs/chs/osr/deathreg/wksheet.pdf Prez F, Nadal M, Navarro-Ortega A, Fbrega F, Domingo JL, Barcel D, and Farr M. 2013. Accumulation of perfluoroalkyl substances in human tissues. Environment International. 59:354-362. 00/00/2013 00/00/2013 Steenland K, Zhao L, Winquist A, Parks C: Ulcerative colitis and perfluorooctanoic acid (PFOA) in a highly exposed population of community residents and workers in the mid-Ohio valley. Environ Health Perspect 2013, 121(8):900-905. Raleigh, Katherine, Dissertation: Cancer Mortality in 3M Chemical Workers (2013) Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A 3M_MN03059185 47 Plaintiff's Ex. No. 3554 3560 3563 3589 3592 3617 3630 3632 3633 Date 00/00/2014 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Custer, C.M., Custer, T.W., Dummer, P.M., Etterson, M.A., Thogmartin, W.E., Wu, Q., Kannan, K., Trowbridge, A., McKann, P.C. 2014. Exposure and Effects of Perfluoroalkyl Substances in Tree Swallows Nesting in Minnesota and Wisconsin, USA. Archives of Environmental Contamination and Toxicology 66:120-138. 00/00/2014 Hardell E, Karrman A, van Bavel B, Bao J, Carlberg M, Hardell L: Case-control study on perfluorinated alkyl acids (PFAAs) and the risk of prostate cancer. Environ Int 2014, 63:35-39. 00/00/2014 Liu, C., Gin, K.Y.H., Chang, V.W.C. 2014. Multi-biomarker Responses in Green Mussels Exposed to PFCs: Effects at Molecular, Cellular, and Physiological Levels. Environmental Science and Pollution Research 21:2785-2794. 00/00/2015 00/00/2015 12/29/2015 00/00/2015 5/30/2016 8/23/2016 PFC Water Treatment, Recommendation on Perfluorinated Compound Treatment Options for Drinking Water (June 2015). Yingling, V., Karst Influence in the Creation of a PFC Megaplume. 14th Sinkhole Conference MDH: East Metro PFC3 Biomonitoring Project. In. St. Paul, MN: Environmental Public Health Tracking and Biomonitoring, MDH; 2015. Weston, 2014 Annual Perfluorochemicals (PFCs) Groundwater, Pore Water and Surface Water Report for the 3M Cottage Grove Site. (2015) Letter from Morgan (EPA) to Johnson (EPA Administrator) re: SAB Draft Risk Assessment of the Potential Human Health Effects Associated with Exposure to Perfluorooctanoic Acid and its Salts MDH, Health officials move to protect more well owners in east metro from exposure to PFOS, PFOA http://www.health.state.mn.us/news/pressrel/2016/pfc082316.ht ml 48 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A N/A STATE_02972445 N/A 3M_MN01595950 3MA01562402 N/A Plaintiff's Ex. No. 3634 3637 3639 3643 3651 3657 3675 3682 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 8/25/2016 12/15/2016 00/00/2016 00/00/2016 Dalsager L, Christensen N, Husby S, Kyhl H, Nielsen F, Host A, Grandjean P, Jensen TK: Association between prenatal exposure to perfluorinated compounds and symptoms of infections at age 1-4 years among 359 children in the Odense Child Cohort. Environ Int 2016, 96:58-64. USDOJ. 2017. Press Release. Public and Environment to Benefit from $50 Million Proposed Settlement for Natural Resources Harmed by Virginia DuPont Facility. USDOJ Office of Public Affairs. MDH, 3M - Oakdale disposal site, http://www.health.state.mn.us/divs/eh/hazardous/sites/washingto n/oakdale/oakdaledump.html EPA Fact Sheet PFOA & PFOS Drinking Water Health Advisories 00/00/2016 00/00/2016 00/00/2016 Colli-Dula, R.C., Martyniuk, C.J., Streets, S., Denslow, N.D., Lehr, R. 2016. Molecular Impacts of Perfluorinated Chemicals (PFASs) in the Liver and Testis of Male Largemouth Bass (Micropterus salmoides) in Minnesota Lakes. Comparative Biochemistry and Physiology, Part D 19:129-139. IARC. 2016. Monograph 110: Some chemicals used as solvents and in polymer manufacture. IARC monographs on the evaluation of carcinogenic risks to humans. World Health Organization Lyon, France. Stein CR, McGovern KJ, Pajak AM, Maglione PJ, and Wolff MS. 2016. Perfluoroalkyl and Polyfluoroalkyl Substances and Indicators of Immune Function in Children Aged 12 - 19 years: National Health and Nutrition Examination Survey. Pediatric Research 79: 348-357. 1/4/2017 MPCA Responses to the 2016 Draft Impaired Waters List Public Notice https://www.pca.state.mn.us/sites/default/files/wq-iw1-55g.pdf Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A STATE_07354701 N/A N/A N/A N/A 49 Plaintiff's Ex. No. 3684 3688 3692 3693 3694 3695 3697 3699 3711 3714 Date 1/20/2017 5/23/2017 9/7/2017 00/00/2017 00/00/2017 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description Qin, Xiao-Di et al., Association of perfluoroalkyl substances exposure with impaired lung function in children (2017) MDH: MDH issues new guidance on chemicals in some private wells, city water in East Metro, Bemidji. In., vol. 2017. St. Paul, MN: MDH; 2017. Abbott Service Company. Wire Forming Services: https://abbottservicecompany.wordpress.com/wire-formingservices/. Evaluation of Perfluorochemical Removal by a Small, In-home Filter.pdf MPCA, Harmful Substance Compensation Program, https://www.pca.state.mn.us/sites/default/files/c-s1-01.pdf 00/00/2017 00/00/2017 Weston, 2016 Annual Perfluorochemical (PFCs) Groundwater Report for the Oakdale Site. Oakdale, Minnesota. (2017) US Army Corps of Engineers, Lower Pool 2 Channel Management Study: Boulanger Bend to Lock and Dam No. 2, DRAFT 00/00/2017 00/00/2017 00/00/2017 AR-226. 2017. ChemView database on chemical health and safety data received by EPA and EPA's assessments and regulatory actions for specific chemicals under the Toxic Substances Control Act, https://java.epa.gov/chemview. EPA, Per- and polyfluoroalkyl substances (PFASs) under TSCA (2017), https://www.epa.gov/assessing-and-managingchemicals-under-tsca/and-polyfluoroalkyl-substances-pfassunder-tsca Fire Fighting Foam Coalition (FFFC). Fact Sheet on AFFF Fire Fighting Agents, https://docs.wixstatic.com/ugd/331cad_fa5766eb867b4a5080330 ce96db195fa.pdf Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A STATE_07430527 N/A N/A N/A N/A N/A N/A 50 Plaintiff's Ex. No. 3716 3724 3725 3726 3729 3738 3741 3746 3747 3748 3749 3750 Date 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 Grandjean P, Heilmann C, Weihe P, Nielsen F, Mogensen UB, Budtz-Jorgensen E: Serum Vaccine Antibody Concentrations in Adolescents Exposed to Perfluorinated Compounds. Environ Health Perspect 2017, 125(7):077018. MDH, Evaluating concurrent exposures to multiple chemicals (2017), http://www.health.state.mn.us/divs/eh/risk/guidance/gw/additivity. html MDH, Sample letter to well owners concerning drinking water advisory for PFCs (2017) MDH, Toxicological summary for perfluorobutyrate (2017), http://www.health.state.mn.us/divs/eh/risk/guidance/gw/pfba2su mm.pdf National Ground Water Association Press (2017). Groundwater and PFAS: State of Knowledge and Practice. U.S. Army Corps of Engineers. 2017. Endangered Species: Conservation of Native Mussels, St. Paul District, St. Paul, MN 55101 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 00/00/2017 Wielsoe M, Kern P, Bonefeld-Jorgensen EC: Serum levels of environmental pollutants is a risk factor for breast cancer in Inuit: a case control study. Environ Health 2017, 16(1):56. 2017_PFBA_Information Sheet.docx 2017_PFBS_Information Sheet.docx 2017_PFHxS_Information Sheet.docx MDH Background document: Toxicokinetic model for perfluorooctane sulfonate (PFOS) and perfluorooctanoic acid (PFOA) and its use in the derivation of human health-based water guidance values (2017) MDH, Background Document Toxicokinetic Model for Perfluorooctane Sulfonate (PFOS) and Perfluorooctanoic Acid (PFOA) and Its Use in the Derivation of Human Health-Based Water Guidance Values Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A N/A N/A N/A N/A N/A STATE_07429985 STATE_07429981 STATE_07429983 STATE_07436246 STATE_07437954 51 Plaintiff's Ex. No. 3751 3752 3753 3754 3755 3756 3758 3764 3766 3767 3768 3773 3779 Date 00/00/2017 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description MDH, Response to EPA Health Advisory for 2017 PFOS and PFOA 00/00/2017 00/00/2017 MDH, Toxicological Summary for Perfluorooctane Sulfonate MDH, Toxicological Summary for Perfluorooctanoic Acid 00/00/2017 00/00/2017 00/00/2017 00/00/2017 10/00/2008 5/2/2013 MPCA, Hazardous Terms - What They Mean https://www.pca.state.mn.us/sites/default/files/w-hw0-15.pdf PFAS update.docx PFOS_Information Sheet_2017.pdf MPCA, Emergency Program Spill Cleanup Policy https://www.pca.state.mn.us/sites/default/files/c-er4-13.pdf Freshwater Society Guardianship Council, "Water is Life: Protecting A Critical Resource for Future Generations" (October 2008). This report is available at http://www.freshwater.org/images/stories/PDFs/publications/Wat er-is-Life-Report.pdf. Lee I and Viberg H. A single neonatal exposure to perfluorohexane sulfonate (PFHxS) affects the levels of important neuroproteins in the developing mouse brain. NeuroToxicology. 37:190- 196. 1/13/2018 5/20/2016 1/13/2018 7/25/2017 MDH 2017 Site-Specific Meal Advice for Tested Lakes and Rivers, available at http://www.health.state.mn.us/divs/eh/fish/eating/sitespecific.html MDH. Perfluorochemicals (PFCs) and Health. http://www.health.state.mn.us/divs/eh/hazardous/topics/pfcshealt h.html Minnesota's Impaired Waters and TMDLs https://www.pca.state.mn.us/water/minnesotas-impaired-waterslist U.S. EPA. "Basic Information about Per- and Polyfluoroalkyl Substances (PFASs)." Accessed August 29, 2017. https://www.epa.gov/pfas/basic-information-about-andpolyfluoroalkyl-substances-pfass#tab-1 52 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. STATE_07430221 STATE_07534027 STATE_07533992 N/A STATE_07429780 STATE_07429830 N/A N/A N/A N/A N/A N/A N/A Plaintiff's Ex. No. 3780 3781 Date 1/8/2018 27-CV-10-28862 Plaintiff's Second Amended Exhibit List State of Minnesota v. 3M Co. Court File No. 27-CV-10-28862 Description U.S. Fish and Wildlife Service. ECOS Environmental Conservation Online System, Species Profile for Rusty Bumblebee (Bombus affinis). www.fws.gov/midwest/endangered/insects/rpbb. Patched Washington County Department of Public Health and 00/00/2013 Environment, Washington County Groundwater Plan 2003-2013 Filed in Fourth Judicial District Court 2/14/2018 6:14 PM February 1H4e, n2n0e1p8in County, MN Beg. Bates No. N/A N/A 53